#------------------------------------------------------------------------------ #$Date: 2025-02-06 01:11:20 +0200 (Thu, 06 Feb 2025) $ #$Revision: 297604 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/38/1573853.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573853 loop_ _publ_author_name 'Thum, Stefan' 'Townrow, Oliver' 'Langer, Jens' 'Harder, Sjoerd' _publ_section_title ; Tuning the Selectivity of P4 Reduction at Alkaline-Earth Metal Centres ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC08502G _journal_year 2025 _chemical_formula_moiety 'C82 H134 Ca2 N4 O2 P4, 2(C4 H10 O)' _chemical_formula_sum 'C90 H154 Ca2 N4 O4 P4' _chemical_formula_weight 1560.20 _chemical_properties_physical Air-sensitive,Moisture-sensitive _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2024-12-03 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-12-04 deposited with the CCDC. 2025-02-05 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 111.8607(18) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 13.4588(2) _cell_length_b 23.0603(3) _cell_length_c 15.7858(2) _cell_measurement_reflns_used 18244 _cell_measurement_temperature 99.98(12) _cell_measurement_theta_max 72.5060 _cell_measurement_theta_min 5.2000 _cell_volume 4547.04(12) _computing_cell_refinement 'CrysAlisPro 1.171.43.106a (Rigaku OD, 2024)' _computing_data_collection 'CrysAlisPro system (CCD 43.105a 64-bit (release 11-01-2024))' _computing_data_reduction 'CrysAlisPro 1.171.43.106a (Rigaku OD, 2024)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 99.98(12) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2903 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.980 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -82.00 39.00 1.00 2.25 -- -41.40 19.00 120.00 121 2 \w -116.00 -17.00 1.00 2.25 -- -41.40 -38.00 -60.00 99 3 \w 27.00 95.00 1.00 2.25 -- 41.40-125.00 90.00 68 4 \w 28.00 133.00 1.00 9.00 -- 104.66 -30.00 60.00 105 5 \w 76.00 177.00 1.00 9.00 -- 104.66 61.00 120.00 101 6 \w 76.00 178.00 1.00 9.00 -- 104.66 30.00 0.00 102 7 \w 97.00 176.00 1.00 9.00 -- 104.66 125.00 150.00 79 8 \w 97.00 176.00 1.00 9.00 -- 104.66 125.00 90.00 79 9 \w 22.00 106.00 1.00 9.00 -- 104.66 -94.00 90.00 84 10 \w 33.00 113.00 1.00 9.00 -- 104.66-125.00 -90.00 80 11 \w 28.00 133.00 1.00 9.00 -- 104.66 -30.00 60.00 105 12 \w 103.00 178.00 1.00 9.00 -- 104.66 77.00-150.00 75 13 \w -114.00 -45.00 1.00 2.25 -- -41.40 -57.00-150.00 69 14 \w -114.00 -13.00 1.00 2.25 -- -41.40 -57.00 90.00 101 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0801382000 _diffrn_orient_matrix_UB_12 0.0444420000 _diffrn_orient_matrix_UB_13 0.0104178000 _diffrn_orient_matrix_UB_21 0.0297112000 _diffrn_orient_matrix_UB_22 0.0427414000 _diffrn_orient_matrix_UB_23 -0.0617562000 _diffrn_orient_matrix_UB_31 -0.0886019000 _diffrn_orient_matrix_UB_32 -0.0259057000 _diffrn_orient_matrix_UB_33 -0.0845621000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0638 _diffrn_reflns_av_unetI/netI 0.0445 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.980 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 34888 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.980 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.605 _diffrn_reflns_theta_min 3.538 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 2.121 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.79867 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.43.106a (Rigaku Oxford Diffraction, 2024) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear light yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.140 _exptl_crystal_description block _exptl_crystal_F_000 1708 _exptl_crystal_size_max 0.272 _exptl_crystal_size_mid 0.226 _exptl_crystal_size_min 0.194 _refine_diff_density_max 0.768 _refine_diff_density_min -0.375 _refine_diff_density_rms 0.060 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.067 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 717 _refine_ls_number_reflns 8864 _refine_ls_number_restraints 1069 _refine_ls_restrained_S_all 1.035 _refine_ls_R_factor_all 0.0622 _refine_ls_R_factor_gt 0.0584 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0703P)^2^+3.9761P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1529 _refine_ls_wR_factor_ref 0.1569 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8169 _reflns_number_total 8864 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc08502g2.cif _cod_data_source_block hasj240524a _cod_original_cell_volume 4547.02(13) _cod_database_code 1573853 _shelx_shelxl_version_number 2019/3 _chemical_oxdiff_formula C90H154Ca2N4O4P4 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.684 _shelx_estimated_absorpt_t_min 0.596 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, {H16a,H16b,H16c} of C16, All C(H,H) groups At 1.5 times of: All C(H,H,H,H,H,H) groups, {H30a,H30b,H30c} of C30, {H19a,H19b,H19c} of C19, {H35a,H35b,H35c} of C35, {H32A,H32B,H32C} of C32A, {H1a,H1b,H1c} of C1, {H14a,H14b,H14c} of C14, {H5a,H5b,H5c} of C5, {H35D,H35E,H35F} of C35A, {H19D, H19E,H19F} of C19A, {H39D,H39E,H39F} of C39A, {H30D,H30E,H30F} of C30A, {H39a, H39b,H39c} of C39, {H41D,H41E,H41F} of C41A, {H41a,H41b,H41c} of C41, {H43D, H43E,H43F} of C43A, {H32d,H32e,H32f} of C32, {H45A,H45B,H45C} of C45, {H45D, H45E,H45F} of C45A, {H43A,H43B,H43C} of C43 2. Restrained distances O1-C40 \\sim O1A-C40A \\sim O1-C38 \\sim O1A-C38A with sigma of 0.02 C40A-C41A \\sim C41-C40 \\sim C39A-C38A \\sim C39-C38 with sigma of 0.02 C42A-C43A \\sim C42-C43 \\sim C44A-C45A \\sim C45-C44 with sigma of 0.02 O2A-C42A \\sim O2-C42 \\sim O2A-C44A \\sim O2-C44 with sigma of 0.02 Ca1-O1 \\sim Ca1-O1A with sigma of 0.02 C17-C11 \\sim C17A-C11 \\sim C28A-C23 \\sim C28-C23 with sigma of 0.02 C20A-C17A \\sim C20-C17 \\sim C18-C17 \\sim C18A-C17A \\sim C34-C33 \\sim C34A-C33 \\sim C36A-C33 ~ C36-C33 \\sim C29A-C28A \\sim C29-C28 \\sim C31-C28 \\sim C31A-C28A with sigma of 0.02 C37-C36A \\sim C37-C36 \\sim C35A-C34A \\sim C35-C34 \\sim C30A-C29A \\sim C30-C29 \\sim C32A-C31A ~ C32-C31 \\sim C19-C18 \\sim C19A-C18A \\sim C21-C20A \\sim C21-C20 with sigma of 0.02 C34-C36 \\sim C34A-C36A \\sim C20-C18 \\sim C20A-C18A \\sim C31A-C29A \\sim C29-C31 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints P1 \\sim P2 \\sim P1A \\sim P2A: within 2A with sigma of 0.03 and sigma for terminal atoms of 0.6 within 2A O2 \\sim C42 \\sim C43 \\sim C44 \\sim C45 \\sim O2A \\sim C42A \\sim C43A \\sim C44A \\sim C45A: within 3A with sigma of 0.03 and sigma for terminal atoms of 0.06 within 3A O1 \\sim C38 \\sim C40 \\sim C41 \\sim O1A \\sim C38A \\sim C40A \\sim C41A: within 3A with sigma of 0.03 and sigma for terminal atoms of 0.06 within 3A C21 \\sim C17 \\sim C18 \\sim C19 \\sim C20 \\sim C17A \\sim C18A \\sim C19A \\sim C20A: within 4A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 4A C30 \\sim C29A \\sim C29 \\sim C30A \\sim C28A \\sim C28 \\sim C31A \\sim C31 \\sim C32A \\sim C32: within 4A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 4A 4. Rigid body (RIGU) restrains C33, C34A, C35A, C36A, C37 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 P1A, P2A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 O1A, C38A, C40A, C41A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C29, C28, C23, C31 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C20A, C17A, C18A, C11 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Sof(P1A)=Sof(P2A)=1-FVAR(1) Sof(P1)=Sof(P2)=FVAR(1) Sof(O1A)=Sof(C38A)=Sof(H38C)=Sof(H38D)=Sof(C39A)=Sof(H39D)=Sof(H39E)= Sof(H39F)=Sof(C40A)=Sof(H40C)=Sof(H40D)=Sof(C41A)=Sof(H41D)=Sof(H41E)= Sof(H41F)=1-FVAR(2) Sof(O1)=Sof(C38)=Sof(H38a)=Sof(H38b)=Sof(C39)=Sof(H39a)=Sof(H39b)=Sof(H39c)= Sof(C40)=Sof(H40a)=Sof(H40b)=Sof(C41)=Sof(H41a)=Sof(H41b)=Sof(H41c)=FVAR(2) Sof(H33A)=Sof(H37D)=Sof(H37E)=Sof(H37F)=Sof(C34A)=Sof(H34C)=Sof(H34D)= Sof(C35A)=Sof(H35D)=Sof(H35E)=Sof(H35F)=Sof(C36A)=Sof(H36C)=Sof(H36D)=1-FVAR(3) Sof(H33)=Sof(H37a)=Sof(H37b)=Sof(H37c)=Sof(C34)=Sof(H34a)=Sof(H34b)=Sof(C35)= Sof(H35a)=Sof(H35b)=Sof(H35c)=Sof(C36)=Sof(H36a)=Sof(H36b)=FVAR(3) Sof(O2)=Sof(C42)=Sof(H42A)=Sof(H42B)=Sof(C43)=Sof(H43A)=Sof(H43B)=Sof(H43C)= Sof(C44)=Sof(H44A)=Sof(H44B)=Sof(C45)=Sof(H45A)=Sof(H45B)=Sof(H45C)=1-FVAR(4) Sof(O2A)=Sof(C42A)=Sof(H42C)=Sof(H42D)=Sof(C43A)=Sof(H43D)=Sof(H43E)= Sof(H43F)=Sof(C44A)=Sof(H44C)=Sof(H44D)=Sof(C45A)=Sof(H45D)=Sof(H45E)= Sof(H45F)=FVAR(4) Sof(C28A)=Sof(H28A)=Sof(C31A)=Sof(H31A)=Sof(H31B)=Sof(C32A)=Sof(H32A)= Sof(H32B)=Sof(H32C)=Sof(C29A)=Sof(H29C)=Sof(H29D)=Sof(C30A)=Sof(H30D)= Sof(H30E)=Sof(H30F)=1-FVAR(5) Sof(C29)=Sof(H29a)=Sof(H29b)=Sof(C30)=Sof(H30a)=Sof(H30b)=Sof(H30c)=Sof(C28)= Sof(H28)=Sof(C31)=Sof(H31c)=Sof(H31d)=Sof(C32)=Sof(H32d)=Sof(H32e)=Sof(H32f)= FVAR(5) Sof(H21D)=Sof(H21E)=Sof(H21F)=Sof(C17A)=Sof(H17A)=Sof(C18A)=Sof(H18C)= Sof(H18D)=Sof(C19A)=Sof(H19D)=Sof(H19E)=Sof(H19F)=Sof(C20A)=Sof(H20C)= Sof(H20D)=1-FVAR(6) Sof(H21a)=Sof(H21b)=Sof(H21c)=Sof(C17)=Sof(H17)=Sof(C18)=Sof(H18a)=Sof(H18b)= Sof(C19)=Sof(H19a)=Sof(H19b)=Sof(H19c)=Sof(C20)=Sof(H20a)=Sof(H20b)=FVAR(6) 6.a Ternary CH refined with riding coordinates: C12(H12), C28A(H28A), C33(H33), C33(H33A), C17(H17), C17A(H17A), C28(H28) 6.b Secondary CH2 refined with riding coordinates: C13(H13a,H13b), C15(H15a,H15b), C31A(H31A,H31B), C18(H18a,H18b), C20(H20a, H20b), C29(H29a,H29b), C34(H34a,H34b), C36(H36a,H36b), C38(H38a,H38b), C40(H40a,H40b), C18A(H18C,H18D), C20A(H20C,H20D), C29A(H29C,H29D), C34A(H34C, H34D), C36A(H36C,H36D), C38A(H38C,H38D), C40A(H40C,H40D), C42(H42A,H42B), C44(H44A,H44B), C42A(H42C,H42D), C44A(H44C,H44D), C31(H31c,H31d) 6.c Aromatic/amide H refined with riding coordinates: C8(H8), C9(H9), C10(H10), C24(H24), C25(H25), C26(H26) 6.d Idealised Me refined as rotating group: C1(H1a,H1b,H1c), C5(H5a,H5b,H5c), C14(H14a,H14b,H14c), C16(H16a,H16b,H16c), C21(H21a,H21b,H21c), C21(H21D,H21E,H21F), C32A(H32A,H32B,H32C), C37(H37a,H37b, H37c), C37(H37D,H37E,H37F), C19(H19a,H19b,H19c), C30(H30a,H30b,H30c), C35(H35a, H35b,H35c), C39(H39a,H39b,H39c), C41(H41a,H41b,H41c), C19A(H19D,H19E,H19F), C30A(H30D,H30E,H30F), C35A(H35D,H35E,H35F), C39A(H39D,H39E,H39F), C41A(H41D, H41E,H41F), C43(H43A,H43B,H43C), C45(H45A,H45B,H45C), C43A(H43D,H43E,H43F), C45A(H45D,H45E,H45F), C32(H32d,H32e,H32f) ; _shelx_res_file ; TITL hasj240524a_a.res in P2(1)/c hasj240524a.res created by SHELXL-2019/3 at 17:27:14 on 10-Jun-2024 REM Old TITL hasj240524a in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.168, Rweak 0.036, Alpha 0.051 REM 1.116 for 244 systematic absences, Orientation as input REM Formula found by SHELXT: C30 N O3 P2 Ca CELL 1.54184 13.45877 23.060276 15.785781 90 111.8607 90 ZERR 2 0.000209 0.000308 0.000245 0 0.0018 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Ca N O P UNIT 180 308 4 8 8 8 SADI O1 C40 O1A C40A O1 C38 O1A C38A SADI C40A C41A C41 C40 C39A C38A C39 C38 RIGU C33 C34A C35A C36A C37 SIMU 0.03 0.6 2 P1 P2 P1A P2A RIGU P1A P2A SADI C42A C43A C42 C43 C44A C45A C45 C44 SADI O2A C42A O2 C42 O2A C44A O2 C44 SIMU 0.03 0.06 3 O2 > C45A SADI Ca1 O1 Ca1 O1A SIMU 0.03 0.06 3 O1 C38 C40 C41 O1A C38A C40A C41A RIGU O1A C38A C40A C41A SIMU 0.02 0.04 4 C21 C17 > C20 C17A > C20A SIMU 0.02 0.04 4 C30 C29A C29 C30A C28A C28 C31A C31 C32A C32 RIGU C29 C28 C23 C31 RIGU C20A C17A C18A C11 SADI C17 C11 C17A C11 C28A C23 C28 C23 SADI C20A C17A C20 C17 C18 C17 C18A C17A C34 C33 C34A C33 C36A C33 C36 C33 = C29A C28A C29 C28 C31 C28 C31A C28A SADI C37 C36A C37 C36 C35A C34A C35 C34 C30A C29A C30 C29 C32A C31A C32 C31 = C19 C18 C19A C18A C21 C20A C21 C20 SADI C34 C36 C34A C36A C20 C18 C20A C18A C31A C29A C29 C31 L.S. 10 PLAN 18 SIZE 0.194 0.226 0.272 TEMP -173.17(12) CONF CONN 24 Ca1 FREE Ca1 C4 FREE Ca1 C3 FREE Ca1 C2 MORE -1 BOND $H fmap 2 acta REM REM REM WGHT 0.070300 3.976100 FVAR 3.43018 0.90196 0.86690 0.76396 0.48498 0.51117 0.83980 CA1 3 0.547716 0.533694 0.670875 11.00000 0.02248 0.02881 = 0.02543 0.00174 0.01027 -0.00269 N1 4 0.680318 0.490103 0.797591 11.00000 0.02321 0.02692 = 0.02864 0.00344 0.01116 -0.00121 N2 4 0.427749 0.511327 0.741965 11.00000 0.01953 0.02857 = 0.02567 0.00093 0.00918 -0.00212 C1 1 0.770839 0.511488 0.963141 11.00000 0.02660 0.05415 = 0.02905 -0.00052 0.00757 0.00698 AFIX 137 H1A 2 0.832925 0.495521 0.952907 11.00000 -1.50000 H1B 2 0.757274 0.488667 1.010094 11.00000 -1.50000 H1C 2 0.785255 0.551859 0.983398 11.00000 -1.50000 AFIX 0 C2 1 0.672858 0.509020 0.874438 11.00000 0.02451 0.02670 = 0.02758 0.00347 0.00951 -0.00159 C3 1 0.578085 0.529581 0.883960 11.00000 0.02498 0.03262 = 0.02510 -0.00121 0.00984 -0.00151 H3 2 0.592543 0.543387 0.941229 11.00000 0.02502 C4 1 0.467514 0.523858 0.830023 11.00000 0.02327 0.02804 = 0.02933 0.00273 0.01184 -0.00087 C5 1 0.394300 0.532395 0.882405 11.00000 0.02713 0.05480 = 0.02993 -0.00046 0.01415 -0.00207 AFIX 137 H5A 2 0.424348 0.562200 0.929268 11.00000 -1.50000 H5B 2 0.387829 0.495814 0.911531 11.00000 -1.50000 H5C 2 0.323417 0.544687 0.840264 11.00000 -1.50000 AFIX 0 C6 1 0.776534 0.459845 0.803922 11.00000 0.02711 0.03385 = 0.03210 -0.00061 0.01403 0.00046 C7 1 0.855993 0.487192 0.780673 11.00000 0.02342 0.04096 = 0.03562 0.00253 0.00981 0.00001 C8 1 0.950623 0.456752 0.792518 11.00000 0.02983 0.05086 = 0.05902 0.00434 0.02401 0.00234 AFIX 43 H8 2 1.004616 0.475013 0.776723 11.00000 -1.20000 AFIX 0 C9 1 0.966908 0.401529 0.826197 11.00000 0.03731 0.04854 = 0.08795 0.00258 0.03431 0.01067 AFIX 43 H9 2 1.032969 0.382459 0.836533 11.00000 -1.20000 AFIX 0 C10 1 0.887017 0.373637 0.845097 11.00000 0.04246 0.03718 = 0.09455 0.00518 0.03785 0.00807 AFIX 43 H10 2 0.897653 0.334782 0.866613 11.00000 -1.20000 AFIX 0 C11 1 0.790965 0.401468 0.833174 11.00000 0.03293 0.03398 = 0.06048 0.00078 0.02517 0.00288 C12 1 0.844541 0.549178 0.746117 11.00000 0.01957 0.04924 = 0.04527 0.01343 0.00742 -0.00350 AFIX 13 H12 2 0.766122 0.555941 0.713161 11.00000 -1.20000 AFIX 0 C13 1 0.881335 0.592835 0.823592 11.00000 0.03228 0.04339 = 0.06877 0.00301 0.01716 -0.00023 AFIX 23 H13A 2 0.866061 0.632297 0.797204 11.00000 -1.20000 H13B 2 0.838285 0.587222 0.861939 11.00000 -1.20000 AFIX 0 C14 1 0.998304 0.589587 0.884134 11.00000 0.03985 0.06703 = 0.07467 -0.02603 0.00728 -0.01045 AFIX 137 H14A 2 1.042104 0.595600 0.847287 11.00000 -1.50000 H14B 2 1.013984 0.551362 0.913235 11.00000 -1.50000 H14C 2 1.014791 0.619691 0.931200 11.00000 -1.50000 AFIX 0 C15 1 0.897156 0.558572 0.675107 11.00000 0.02776 0.08597 = 0.05040 0.01809 0.01124 -0.01061 AFIX 23 H15A 2 0.975771 0.556213 0.707248 11.00000 -1.20000 H15B 2 0.875517 0.526136 0.630892 11.00000 -1.20000 AFIX 0 C16 1 0.872150 0.613386 0.623407 11.00000 0.04381 0.10559 = 0.07414 0.03805 0.01532 -0.01244 AFIX 137 H16A 2 0.896054 0.611021 0.571967 11.00000 -1.20000 H16B 2 0.909061 0.645463 0.663504 11.00000 -1.20000 H16C 2 0.794710 0.620121 0.600376 11.00000 -1.20000 AFIX 0 C21 1 0.671256 0.307263 0.703860 11.00000 0.04695 0.04133 = 0.07955 0.00030 0.02970 0.00264 PART 1 AFIX 137 H21A 2 0.611448 0.333138 0.671247 71.00000 -1.50000 H21B 2 0.654655 0.267929 0.679101 71.00000 -1.50000 H21C 2 0.736251 0.321091 0.696191 71.00000 -1.50000 AFIX 137 PART 2 H21D 2 0.613140 0.300296 0.644966 -71.00000 -1.50000 H21E 2 0.697058 0.270120 0.734257 -71.00000 -1.50000 H21F 2 0.730086 0.327453 0.693949 -71.00000 -1.50000 AFIX 0 PART 0 C22 1 0.316182 0.496330 0.701637 11.00000 0.02127 0.03839 = 0.02687 -0.00354 0.01151 -0.00604 C23 1 0.240668 0.536741 0.646084 11.00000 0.02303 0.04276 = 0.03382 -0.00023 0.01107 -0.00221 C24 1 0.133393 0.519646 0.610158 11.00000 0.02171 0.06139 = 0.04248 -0.00127 0.00968 -0.00137 AFIX 43 H24 2 0.081134 0.546221 0.573452 11.00000 -1.20000 AFIX 0 C25 1 0.101016 0.465541 0.626247 11.00000 0.02403 0.06334 = 0.04626 -0.01321 0.01239 -0.01383 AFIX 43 H25 2 0.027241 0.455545 0.602033 11.00000 -1.20000 AFIX 0 C26 1 0.175919 0.425851 0.677611 11.00000 0.03134 0.04785 = 0.04264 -0.00985 0.01747 -0.01552 AFIX 43 H26 2 0.153159 0.388230 0.687031 11.00000 -1.20000 AFIX 0 C27 1 0.284290 0.439860 0.715937 11.00000 0.02830 0.03654 = 0.03131 -0.00551 0.01382 -0.00663 PART 2 C28A 1 0.277935 0.594162 0.620992 -61.00000 0.02631 0.05026 = 0.03176 0.00440 0.01832 0.01293 AFIX 13 H28A 2 0.351442 0.589743 0.620075 -61.00000 -1.20000 AFIX 0 C31A 1 0.279837 0.638090 0.693614 -61.00000 0.02606 0.05033 = 0.04243 0.01058 0.00813 -0.00078 AFIX 23 H31A 2 0.309435 0.674707 0.680133 -61.00000 -1.20000 H31B 2 0.331130 0.623807 0.752915 -61.00000 -1.20000 AFIX 0 C32A 1 0.175186 0.652914 0.706401 -61.00000 0.04300 0.05892 = 0.06050 -0.00057 0.02480 0.00024 AFIX 137 H32A 2 0.125906 0.671912 0.651217 -61.00000 -1.50000 H32B 2 0.190423 0.679070 0.758659 -61.00000 -1.50000 H32C 2 0.142373 0.617231 0.717494 -61.00000 -1.50000 AFIX 0 PART 0 C33 1 0.367439 0.393934 0.765665 11.00000 0.03715 0.03335 = 0.03651 -0.00066 0.01353 -0.00920 PART 1 AFIX 13 H33 2 0.426872 0.414472 0.814552 41.00000 -1.20000 AFIX 13 PART 2 H33A 2 0.436879 0.406542 0.762126 -41.00000 -1.20000 AFIX 0 PART 0 C37 1 0.294397 0.367395 0.888743 11.00000 0.05640 0.06181 = 0.05099 -0.00621 0.02857 -0.01344 PART 1 AFIX 137 H37A 2 0.240898 0.398082 0.864526 41.00000 -1.50000 H37B 2 0.356798 0.383002 0.938489 41.00000 -1.50000 H37C 2 0.263380 0.335555 0.911887 41.00000 -1.50000 AFIX 137 PART 2 H37D 2 0.259933 0.334600 0.849250 -41.00000 -1.50000 H37E 2 0.242320 0.398767 0.879666 -41.00000 -1.50000 H37F 2 0.320896 0.354929 0.952678 -41.00000 -1.50000 AFIX 0 PART 1 P1 6 0.386981 0.483066 0.492831 21.00000 0.02262 0.04043 = 0.02839 -0.00320 0.01115 -0.00651 P2 6 0.539238 0.439404 0.533338 21.00000 0.03445 0.03057 = 0.02714 0.00197 0.01132 0.00139 O1 5 0.568971 0.635934 0.706117 31.00000 0.03458 0.02861 = 0.05238 0.00179 0.02226 -0.00250 C17 1 0.705043 0.365969 0.851043 71.00000 0.03336 0.03409 = 0.05936 0.00117 0.02246 0.00010 AFIX 13 H17 2 0.636082 0.387750 0.824353 71.00000 -1.20000 AFIX 0 C18 1 0.729954 0.358287 0.955876 71.00000 0.03528 0.05915 = 0.05548 -0.00556 0.01570 -0.00718 AFIX 23 H18A 2 0.793635 0.333077 0.982238 71.00000 -1.20000 H18B 2 0.748111 0.396645 0.985864 71.00000 -1.20000 AFIX 0 C19 1 0.639076 0.332460 0.977544 71.00000 0.05148 0.06066 = 0.05458 -0.00311 0.02478 -0.01261 AFIX 137 H19A 2 0.575353 0.356919 0.951401 71.00000 -1.50000 H19B 2 0.659545 0.330273 1.043888 71.00000 -1.50000 H19C 2 0.623338 0.293422 0.951407 71.00000 -1.50000 AFIX 0 C20 1 0.688796 0.306697 0.803802 71.00000 0.04144 0.03694 = 0.07406 0.00202 0.03030 0.00010 AFIX 23 H20A 2 0.752379 0.282454 0.836138 71.00000 -1.20000 H20B 2 0.626376 0.287687 0.810866 71.00000 -1.20000 AFIX 0 C29 1 0.202558 0.630834 0.541783 61.00000 0.03268 0.03507 = 0.03735 -0.00309 0.00561 0.00487 AFIX 23 H29A 2 0.129083 0.636694 0.540358 61.00000 -1.20000 H29B 2 0.233878 0.669591 0.541075 61.00000 -1.20000 AFIX 0 C30 1 0.195947 0.598267 0.456127 61.00000 0.02653 0.04480 = 0.03543 0.00706 0.01229 0.00614 AFIX 137 H30A 2 0.136908 0.613892 0.403464 61.00000 -1.50000 H30B 2 0.183317 0.557016 0.463205 61.00000 -1.50000 H30C 2 0.263356 0.602896 0.446489 61.00000 -1.50000 AFIX 0 C34 1 0.416767 0.366178 0.700150 41.00000 0.03742 0.03605 = 0.04689 0.00146 0.02057 0.00265 AFIX 23 H34A 2 0.454240 0.396756 0.679510 41.00000 -1.20000 H34B 2 0.470841 0.337111 0.734617 41.00000 -1.20000 AFIX 0 C35 1 0.335080 0.336835 0.616314 41.00000 0.05833 0.04005 = 0.04473 -0.01027 0.02031 0.00240 AFIX 137 H35A 2 0.282276 0.365475 0.580631 41.00000 -1.50000 H35B 2 0.298722 0.305777 0.635883 41.00000 -1.50000 H35C 2 0.371848 0.320434 0.578656 41.00000 -1.50000 AFIX 0 C36 1 0.328894 0.344846 0.812820 41.00000 0.03353 0.03864 = 0.04265 -0.00078 0.01433 -0.00696 AFIX 23 H36A 2 0.267841 0.324526 0.766640 41.00000 -1.20000 H36B 2 0.387477 0.316385 0.838874 41.00000 -1.20000 AFIX 0 C38 1 0.531134 0.680968 0.637434 31.00000 0.07261 0.03081 = 0.05055 0.00439 0.02840 -0.00212 AFIX 23 H38A 2 0.511440 0.715592 0.664827 31.00000 -1.20000 H38B 2 0.465952 0.667175 0.587297 31.00000 -1.20000 AFIX 0 C39 1 0.613832 0.697794 0.598799 31.00000 0.14951 0.04425 = 0.10467 -0.00857 0.09954 -0.02236 AFIX 137 H39A 2 0.586296 0.729705 0.555327 31.00000 -1.50000 H39B 2 0.629599 0.664400 0.567491 31.00000 -1.50000 H39C 2 0.679428 0.710229 0.648432 31.00000 -1.50000 AFIX 0 C40 1 0.631705 0.659345 0.795694 31.00000 0.02920 0.03226 = 0.06086 -0.00304 0.01462 -0.00135 AFIX 23 H40A 2 0.680425 0.689595 0.788931 31.00000 -1.20000 H40B 2 0.676370 0.627999 0.834104 31.00000 -1.20000 AFIX 0 C41 1 0.563701 0.685222 0.843602 31.00000 0.04318 0.04065 = 0.05084 -0.00970 0.01265 0.00017 AFIX 137 H41A 2 0.519606 0.716514 0.806213 31.00000 -1.50000 H41B 2 0.610141 0.700795 0.902912 31.00000 -1.50000 H41C 2 0.517233 0.655148 0.852766 31.00000 -1.50000 AFIX 0 PART 2 P1A 6 0.436774 0.451246 0.522218 -21.00000 0.05264 0.07930 = 0.06435 0.02776 0.00254 -0.02609 P2A 6 0.601282 0.464907 0.535955 -21.00000 0.05574 0.08112 = 0.10380 -0.04347 0.02154 0.00864 O1A 5 0.583236 0.635046 0.692774 -31.00000 0.03164 0.02517 = 0.02952 -0.00969 0.02017 -0.01161 C17A 1 0.701987 0.371974 0.855290 -71.00000 0.03927 0.03471 = 0.06868 0.00671 0.02912 0.00327 AFIX 13 H17A 2 0.661640 0.401730 0.875711 -71.00000 -1.20000 AFIX 0 C18A 1 0.749740 0.326861 0.931016 -71.00000 0.04145 0.03722 = 0.07241 0.00516 0.01725 -0.00098 AFIX 23 H18C 2 0.772637 0.292800 0.904683 -71.00000 -1.20000 H18D 2 0.814539 0.343639 0.978109 -71.00000 -1.20000 AFIX 0 C19A 1 0.676064 0.306397 0.976703 -71.00000 0.06941 0.05980 = 0.06071 -0.00828 0.02006 0.02532 AFIX 137 H19D 2 0.603239 0.302694 0.931130 -71.00000 -1.50000 H19E 2 0.676442 0.334515 1.023373 -71.00000 -1.50000 H19F 2 0.700467 0.268639 1.005398 -71.00000 -1.50000 AFIX 0 C20A 1 0.628780 0.345585 0.765390 -71.00000 0.04318 0.04807 = 0.06343 0.02333 0.02750 0.00641 AFIX 23 H20C 2 0.588817 0.378140 0.726789 -71.00000 -1.20000 H20D 2 0.575550 0.321782 0.779313 -71.00000 -1.20000 AFIX 0 C29A 1 0.198258 0.611944 0.524770 -61.00000 0.02906 0.05138 = 0.04609 0.01442 0.01285 0.00764 AFIX 23 H29C 2 0.191155 0.579868 0.481211 -61.00000 -1.20000 H29D 2 0.126880 0.619345 0.527134 -61.00000 -1.20000 AFIX 0 C30A 1 0.237195 0.665861 0.492274 -61.00000 0.04711 0.07091 = 0.06388 0.01734 0.02415 0.01163 AFIX 137 H30D 2 0.195641 0.671618 0.427099 -61.00000 -1.50000 H30E 2 0.313092 0.661414 0.502044 -61.00000 -1.50000 H30F 2 0.228101 0.699516 0.526606 -61.00000 -1.50000 AFIX 0 C34A 1 0.335164 0.339636 0.711315 -41.00000 0.04176 0.02484 = 0.04323 0.00109 0.01976 -0.01402 AFIX 23 H34C 2 0.259814 0.329891 0.700644 -41.00000 -1.20000 H34D 2 0.381272 0.306938 0.743852 -41.00000 -1.20000 AFIX 0 C35A 1 0.348386 0.351207 0.621146 -41.00000 0.05723 0.03914 = 0.04544 0.00327 0.02773 -0.00172 AFIX 137 H35D 2 0.298260 0.381601 0.587641 -41.00000 -1.50000 H35E 2 0.333530 0.315594 0.584660 -41.00000 -1.50000 H35F 2 0.421881 0.363875 0.633093 -41.00000 -1.50000 AFIX 0 C36A 1 0.385686 0.388510 0.865383 -41.00000 0.06131 0.04271 = 0.04632 0.00338 0.01575 -0.01166 AFIX 23 H36C 2 0.446849 0.361903 0.893750 -41.00000 -1.20000 H36D 2 0.407264 0.427032 0.894024 -41.00000 -1.20000 AFIX 0 C38A 1 0.596661 0.673940 0.627287 -31.00000 0.04542 0.03438 = 0.03919 -0.00076 0.02892 -0.00587 AFIX 23 H38C 2 0.624705 0.651788 0.587267 -31.00000 -1.20000 H38D 2 0.651176 0.703241 0.660089 -31.00000 -1.20000 AFIX 0 C39A 1 0.496460 0.704918 0.568455 -31.00000 0.12335 0.04359 = 0.05832 -0.00497 0.05866 -0.00670 AFIX 137 H39D 2 0.453828 0.679384 0.518524 -31.00000 -1.50000 H39E 2 0.515629 0.740078 0.543141 -31.00000 -1.50000 H39F 2 0.454587 0.715492 0.605338 -31.00000 -1.50000 AFIX 0 C40A 1 0.555829 0.660575 0.764216 -31.00000 0.04034 0.02424 = 0.02857 -0.00782 0.02148 -0.00588 AFIX 23 H40C 2 0.519093 0.631393 0.788203 -31.00000 -1.20000 H40D 2 0.505837 0.693280 0.739087 -31.00000 -1.20000 AFIX 0 C41A 1 0.653565 0.682051 0.840340 -31.00000 0.06209 0.04924 = 0.03480 -0.02457 0.01547 -0.00535 AFIX 137 H41D 2 0.635065 0.716200 0.868397 -31.00000 -1.50000 H41E 2 0.708470 0.692529 0.816148 -31.00000 -1.50000 H41F 2 0.681123 0.651480 0.886292 -31.00000 -1.50000 AFIX 0 O2 5 0.101498 0.252936 0.635180 -51.00000 0.04598 0.07203 = 0.09340 0.01326 0.03445 0.00286 C42 1 0.051181 0.259413 0.538592 -51.00000 0.04597 0.06230 = 0.07977 0.02099 0.01711 -0.00072 AFIX 23 H42A 2 0.046988 0.301046 0.522321 -51.00000 -1.20000 H42B 2 -0.022600 0.243822 0.517612 -51.00000 -1.20000 AFIX 0 C43 1 0.114164 0.227520 0.492400 -51.00000 0.03738 0.07640 = 0.07619 -0.00167 0.01298 -0.01339 AFIX 137 H43A 2 0.078137 0.231129 0.426067 -51.00000 -1.50000 H43B 2 0.119279 0.186469 0.509566 -51.00000 -1.50000 H43C 2 0.186213 0.244132 0.511400 -51.00000 -1.50000 AFIX 0 C44 1 0.045359 0.278209 0.686537 -51.00000 0.04802 0.05774 = 0.08689 0.00406 0.03032 0.00047 AFIX 23 H44A 2 0.020016 0.317176 0.661441 -51.00000 -1.20000 H44B 2 0.095749 0.283312 0.750364 -51.00000 -1.20000 AFIX 0 C45 1 -0.047665 0.243823 0.686692 -51.00000 0.06076 0.05303 = 0.14259 -0.01662 0.06429 -0.01605 AFIX 137 H45A 2 -0.100182 0.240466 0.624159 -51.00000 -1.50000 H45B 2 -0.080686 0.263229 0.724867 -51.00000 -1.50000 H45C 2 -0.023609 0.205046 0.711151 -51.00000 -1.50000 AFIX 0 PART 1 O2A 5 0.068983 0.246228 0.598902 51.00000 0.07143 0.04697 = 0.09723 0.00466 0.04591 0.00513 C42A 1 0.048998 0.259707 0.507453 51.00000 0.08340 0.09118 = 0.07532 0.01519 0.02062 0.01022 AFIX 23 H42C 2 0.058858 0.301855 0.501566 51.00000 -1.20000 H42D 2 -0.026077 0.249892 0.469529 51.00000 -1.20000 AFIX 0 C43A 1 0.122444 0.227080 0.474015 51.00000 0.09034 0.12640 = 0.12266 -0.05418 0.05424 -0.03542 AFIX 137 H43D 2 0.115508 0.241778 0.413822 51.00000 -1.50000 H43E 2 0.103837 0.185804 0.469330 51.00000 -1.50000 H43F 2 0.196397 0.232153 0.516852 51.00000 -1.50000 AFIX 0 C44A 1 -0.006766 0.272549 0.629182 51.00000 0.05170 0.05833 = 0.08517 -0.00378 0.02054 0.01262 AFIX 23 H44C 2 -0.079087 0.257355 0.593355 51.00000 -1.20000 H44D 2 -0.007374 0.314950 0.619179 51.00000 -1.20000 AFIX 0 C45A 1 0.019738 0.260626 0.727642 51.00000 0.06770 0.06921 = 0.10726 -0.00832 0.05437 -0.01046 AFIX 137 H45D 2 0.014573 0.218867 0.736776 51.00000 -1.50000 H45E 2 -0.030653 0.281315 0.748398 51.00000 -1.50000 H45F 2 0.092783 0.273829 0.762722 51.00000 -1.50000 AFIX 0 C28 1 0.270396 0.599690 0.632895 61.00000 0.01495 0.03671 = 0.04101 0.00584 0.01292 0.00081 AFIX 13 H28 2 0.342018 0.595426 0.628022 61.00000 -1.20000 AFIX 0 C31 1 0.293381 0.640069 0.713473 61.00000 0.02845 0.03403 = 0.03453 -0.00130 0.00124 0.00069 AFIX 23 H31C 2 0.319458 0.677698 0.699712 61.00000 -1.20000 H31D 2 0.350319 0.623192 0.767541 61.00000 -1.20000 AFIX 0 C32 1 0.193225 0.649890 0.734712 61.00000 0.03393 0.04321 = 0.03716 -0.00903 -0.00041 0.00602 AFIX 137 H32D 2 0.139131 0.669855 0.683314 61.00000 -1.50000 H32E 2 0.211160 0.673699 0.789832 61.00000 -1.50000 H32F 2 0.164906 0.612439 0.744663 61.00000 -1.50000 AFIX 0 HKLF 4 REM hasj240524a_a.res in P2(1)/c REM wR2 = 0.1569, GooF = S = 1.067, Restrained GooF = 1.035 for all data REM R1 = 0.0584 for 8169 Fo > 4sig(Fo) and 0.0622 for all 8864 data REM 717 parameters refined using 1069 restraints END WGHT 0.0703 3.9746 REM Highest difference peak 0.768, deepest hole -0.375, 1-sigma level 0.060 Q1 1 0.6389 0.3616 0.8914 11.00000 0.05 0.77 Q2 1 0.4875 0.4766 0.5207 11.00000 0.05 0.77 Q3 1 0.4845 0.3849 0.4824 11.00000 0.05 0.66 Q4 1 0.6516 0.3668 0.7947 11.00000 0.05 0.57 Q5 1 0.2874 0.3913 0.8391 11.00000 0.05 0.52 Q6 1 0.3709 0.3506 0.9253 11.00000 0.05 0.50 Q7 1 0.8480 0.5482 0.5993 11.00000 0.05 0.48 Q8 1 0.6333 0.3042 0.7522 11.00000 0.05 0.43 Q9 1 0.3128 0.4103 0.7663 11.00000 0.05 0.40 Q10 1 0.7384 0.3929 0.7959 11.00000 0.05 0.39 Q11 1 0.9120 0.3841 0.8058 11.00000 0.05 0.32 Q12 1 0.8315 0.3652 0.8019 11.00000 0.05 0.32 Q13 1 0.8548 0.5634 0.7951 11.00000 0.05 0.31 Q14 1 0.7359 0.3252 0.9766 11.00000 0.05 0.30 Q15 1 0.9578 0.6610 0.8745 11.00000 0.05 0.30 Q16 1 0.2380 0.4464 0.7065 11.00000 0.05 0.27 Q17 1 0.8189 0.5908 0.7026 11.00000 0.05 0.26 Q18 1 0.2989 0.4601 0.7045 11.00000 0.05 0.24 ; _shelx_res_checksum 38782 _shelx_hkl_file ; 0 0 2 595190. 3799.96 14 0 0 -2 598804. 3605.56 1 0 0 3 8.34802 36.0728 14 0 0 -3 37.2631 9.94344 3 0 0 -3 60.8787 59.7489 1 0 0 4 4273.19 476.402 14 0 0 -4 4908.79 488.594 1 0 0 -4 5227.54 535.336 3 0 0 5 25.4385 80.3283 14 0 0 -5-38.6957 77.1429 1 0 0 -6 442453. 5731.40 1 0 0 -6 432599. 6124.15 3 0 0 -7 27.1162 27.1217 3 0 0 -7 159.489 138.240 1 0 0 7 43.1160 112.920 14 0 0 -8 2134.09 533.480 3 0 0 -8 2205.74 515.727 1 0 0 8 517.928 374.645 14 0 0 -9 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1 -2 6 4 508.086 172.245 13 -2 -6 4 394.556 186.645 14 2 -6 -4 543.334 131.823 2 2 6 -4 483.514 215.041 1 -2 6 4 442.151 183.408 1 -2 6 3 51998.0 2145.42 1 2 6 -3 48663.9 1815.88 2 2 6 -3 48962.5 1937.41 1 -2 6 3 40516.6 1596.40 13 -2 -6 3 43470.7 1902.47 14 2 -6 -3 48814.2 1288.06 2 -2 6 2 67260.5 2510.89 1 2 6 -2 63292.6 2022.85 1 2 6 -2 66032.5 1924.36 2 -2 6 2 67403.0 2054.44 13 -2 -6 2 61429.6 2036.00 14 2 -6 -2 66553.4 1625.36 2 -2 6 1 11806.9 857.573 13 -2 -6 1 11261.3 837.263 14 -2 6 1 11864.3 1081.39 1 2 6 -1 11649.6 782.697 1 2 6 -1 11748.1 728.507 2 2 6 0 110567. 1957.68 2 2 6 0 107520. 2060.97 1 -2 6 0 109507. 3354.43 1 -2 6 -1 118520. 2779.45 13 2 -6 1 116769. 2796.17 14 2 6 1 122897. 1723.43 2 -2 6 -1 119342. 3611.42 1 2 6 1 124149. 1912.43 1 -2 6 -2 2648.85 577.970 1 2 6 2 2301.53 162.249 2 2 -6 2 597.577 197.857 14 -2 -6 -2 2381.35 459.303 3 -2 6 -2 661.920 210.919 13 2 -6 3 27522.9 1484.71 14 -2 -6 -3 38501.2 1907.20 3 -2 6 -3 40988.2 2423.27 1 -2 6 -3 30481.7 1463.66 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291.548 1 2 11 -4 318.736 227.598 1 -2 -11 4 2654.10 635.268 14 -2 11 3 11957.5 1203.39 13 -2 11 3 9954.92 1170.06 1 2 11 -3 8844.11 1149.75 1 -2 -11 3 12263.3 1353.10 14 -2 11 2 25109.5 1728.33 13 -2 11 2 28172.6 2124.86 1 2 11 -2 26194.0 1895.90 1 -2 -11 2 23016.3 1781.09 14 -2 11 1 44601.4 2765.25 1 2 11 -1 43957.0 2306.80 1 -2 11 1 37866.0 2139.46 13 2 11 0 62361.3 2596.42 1 -2 11 0 59646.2 3237.69 1 -2 11 0 59284.7 2628.04 13 -2 11 -1 11948.9 1540.67 1 -2 11 -1 5663.27 805.449 13 -2 11 -2 37895.3 2806.62 1 -2 11 -2 25810.0 1663.55 13 -2 11 -3 11643.1 1172.09 13 -2 11 -3 11445.9 1614.82 1 2 -11 3 12023.2 1356.70 14 -2 11 -4 12192.7 1225.32 13 -2 11 -4 9619.84 1554.75 1 2 -11 4 12129.9 1395.66 14 2 11 5 1252.14 379.480 13 -2 11 -5 736.917 297.076 13 2 -11 5 1415.86 525.261 14 -2 -11 -6 53882.0 1775.66 9 2 -11 6 52608.8 3202.18 14 -2 11 -6 57929.7 4177.14 1 -2 -11 -6 56037.0 1554.67 10 -2 11 -6 54335.1 1830.89 12 2 -11 7 1243.40 502.660 14 -2 11 -7 929.064 233.174 12 -2 -11 -7 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24528.6 2059.24 14 -3 10 -5 25195.8 1732.10 13 -3 -10 -6 3085.72 424.589 9 -3 10 -6 3881.35 446.158 7 -3 -10 -6 3486.97 399.093 10 -3 -10 -6 3226.21 453.092 8 -3 10 -6 2942.30 409.954 12 3 -10 6 2351.81 638.478 14 -3 -10 -7 28289.3 1366.02 8 -3 10 -7 28479.5 1313.83 12 -3 -10 -7 25250.3 1265.98 9 -3 10 -7 23653.4 1131.58 7 -3 10 -7 23212.9 2881.68 1 -3 -10 -7 26682.3 1128.90 10 -3 10 -7 21733.0 2239.19 3 -3 10 -8 2484.52 392.983 12 -3 -10 -8 2363.92 396.511 9 -3 10 -8 1847.47 321.356 7 -3 10 -8 1624.00 801.709 1 -3 -10 -8 2541.05 359.357 10 -3 10 -8 1218.76 547.215 3 -3 10 -9 2232.59 378.620 12 -3 -10 -9 2398.90 421.456 9 -3 10 -9 2471.37 379.661 7 -3 -10 -9 2461.28 356.044 10 -3 10 -9 2709.80 1019.74 1 -3 10 -9 2641.51 860.262 3 -3 10 -10 2560.47 406.357 12 -3 10 -10 2479.11 419.997 9 -3 -10 -10 2353.47 416.793 9 -3 10 -10 2411.08 373.688 7 -3 -10 -10 2703.33 377.180 10 -3 10 -11 357.687 162.713 9 -3 -10 -11 300.685 157.979 9 -3 10 -11 15.2229 57.2506 12 -3 -10 -11 330.444 136.343 10 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7228.47 692.364 4 4 -14 -4 7701.55 533.899 6 -4 14 4 5905.47 1065.40 13 -4 14 4 7117.73 1200.43 1 4 14 -4 7090.80 1259.81 1 4 14 -3 46.4845 107.410 1 -4 14 3 136.457 326.863 1 4 -14 -3 143.289 55.5186 4 4 -14 -3 145.022 71.0019 6 4 -14 -3 583.243 208.661 11 -4 14 3 605.442 349.825 13 4 -14 -2 389.511 224.396 2 4 -14 -2 346.757 117.834 6 -4 14 2 672.047 406.976 1 4 -14 -2 412.261 186.336 4 -4 14 2 332.035 222.352 13 4 -14 -2 419.291 209.649 11 4 -14 -1 3776.34 575.702 11 4 -14 -1 2287.51 297.051 6 4 -14 -1 1804.76 486.957 2 -4 14 1 2998.89 768.756 13 4 -14 -1 2313.46 433.407 4 -4 14 1 2202.86 796.039 1 -4 14 0 170.505 286.941 1 4 -14 0 1146.36 211.870 6 4 -14 0 1009.39 284.851 4 4 -14 0 3557.16 559.994 11 -4 14 0 2728.28 739.379 13 -4 -14 -1 8529.33 626.464 10 -4 14 -1 7670.59 1242.23 13 4 -14 1 9957.16 624.973 6 -4 14 -1 11544.1 1897.76 1 4 -14 1 9520.17 905.809 4 4 -14 1 7605.60 882.016 11 -4 -14 -2 21442.5 1025.27 10 -4 14 -2 21135.3 1979.94 13 4 -14 2 19803.7 886.109 6 4 -14 2 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1169.98 3 5 5 2 11334.2 909.167 2 -5 5 -2 10314.6 1454.67 1 -5 -5 -3 31078.3 2164.39 3 -5 5 -3 30537.1 2132.13 3 -5 5 -3 32385.5 2589.68 1 -5 5 -4 2334.27 661.456 3 -5 -5 -4 2642.20 685.733 3 -5 5 -4 2639.69 774.248 1 -5 -5 -5 11519.5 1509.34 3 -5 5 -5 11720.0 1560.16 3 -5 5 -5 10499.8 1577.97 1 -5 5 -6 197.638 98.7717 7 -5 -5 -6 435.791 168.958 7 -5 -5 -6 210.874 103.100 8 -5 -5 -6 237.931 104.710 10 -5 5 -6 26.2850 127.801 3 -5 5 -6 398.920 256.455 1 -5 -5 -7 3395.11 501.575 7 -5 -5 -7 4111.09 1000.17 3 -5 5 -7 4238.20 1035.89 3 -5 5 -7 3171.97 457.631 7 -5 -5 -7 2624.08 422.310 8 -5 5 -7 2721.51 404.312 9 -5 -5 -7 2560.33 396.363 9 -5 -5 -7 2741.40 369.329 10 -5 -5 -8 9039.00 1541.68 3 -5 5 -8 9605.61 1618.77 3 -5 -5 -8 7849.10 654.253 10 -5 -5 -8 7211.55 684.506 9 -5 5 -8 7188.29 675.635 9 -5 -5 -8 7801.36 792.292 7 -5 5 -8 7477.71 714.732 7 -5 -5 -8 8420.85 782.664 8 -5 5 -9 1752.55 359.107 7 -5 -5 -9 1831.37 395.748 7 -5 -5 -9 1729.13 365.972 8 -5 -5 -9 2515.04 380.133 10 -5 -5 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1977.84 323.448 4 5 7 -15 1112.23 260.380 12 5 -7 -15 1203.91 276.774 11 -5 7 14 3334.42 418.242 5 5 7 -14 2445.75 391.289 12 5 -7 -14 3595.24 447.929 4 5 -7 -14 2494.05 408.472 11 -5 7 13 5542.94 544.853 5 5 7 -13 3642.56 498.134 12 5 -7 -13 3800.87 507.268 11 5 -7 -13 5423.13 568.290 4 5 7 -12 4786.76 1204.49 1 -5 7 12 2358.54 753.562 14 -5 -7 12 2029.02 709.265 14 5 7 -12 2431.45 391.077 12 5 -7 -12 2520.97 404.960 11 5 -7 -12 4774.32 518.723 4 -5 7 12 4205.49 473.696 5 5 7 -11 682.160 208.654 12 -5 7 11 670.456 377.201 14 -5 -7 11 852.868 493.887 14 5 7 -11 1341.08 620.242 1 -5 7 11 1059.33 245.364 5 5 -7 -11 943.603 254.543 11 5 -7 -11 1444.35 299.846 4 5 -7 -10 2012.03 320.074 4 5 -7 -10 2893.84 406.393 11 5 7 -10 2404.89 356.379 12 -5 7 10 2371.44 336.719 5 -5 7 10 1968.31 633.847 14 -5 -7 10 2035.59 684.030 14 5 7 -10 2368.43 757.992 1 -5 -7 9 10062.2 1422.75 14 -5 7 9 11337.3 1426.70 14 5 7 -8 11666.8 1517.18 1 5 7 -8 9742.58 1284.18 2 -5 -7 8 3658.06 810.338 14 -5 7 8 4050.36 793.098 14 5 -7 -7 14339.9 1080.58 2 5 7 -7 14909.8 1616.57 1 5 7 -7 14649.5 1498.90 2 -5 7 7 17192.7 1473.63 13 -5 -7 7 13475.2 1428.43 14 5 7 -6 19136.2 1702.10 1 5 7 -6 19129.0 1603.03 2 5 -7 -6 18749.5 1243.22 2 -5 7 6 25463.3 1744.63 13 -5 -7 6 27104.0 1961.97 14 5 7 -5 21257.8 1660.83 1 5 7 -5 19729.1 1523.77 2 5 -7 -5 20211.2 1290.94 2 -5 -7 5 25611.0 1843.20 14 -5 7 5 23795.7 1695.45 13 5 7 -4 15555.8 1314.18 2 5 -7 -4 14540.9 1116.33 2 -5 -7 4 16822.1 1343.67 14 -5 7 4 14728.0 1530.75 1 -5 7 4 15831.6 1352.99 13 5 7 -3 13803.5 1138.38 2 5 -7 -3 13600.5 1095.66 2 -5 -7 3 5688.70 732.154 14 -5 7 3 6345.92 861.421 13 -5 7 3 14763.2 1594.61 1 5 7 -2 23298.9 1413.89 2 -5 7 2 21619.0 1579.59 13 5 -7 -2 25449.8 1602.51 2 -5 7 2 23935.7 2064.43 1 5 7 -1 30596.3 1543.40 2 -5 7 1 32089.3 1963.46 13 5 -7 -1 30210.9 1762.68 2 -5 7 1 31548.2 2387.22 1 -5 7 0 11738.0 1195.09 13 5 7 0 12460.6 939.452 2 -5 7 0 12644.0 1600.71 1 5 7 1 25497.0 1272.78 2 -5 7 -1 26410.2 2388.52 1 -5 -7 -1 24792.8 1785.41 3 -5 -7 -2 8826.51 1129.93 3 -5 7 -2 8450.56 1379.16 1 -5 -7 -3 1792.52 530.044 3 -5 7 -3 2377.26 767.148 1 -5 7 -4 20540.6 1983.62 3 -5 -7 -4 19276.1 1837.50 3 -5 7 -4 23406.3 2491.61 1 -5 -7 -5 2653.89 409.319 7 -5 7 -5 2754.07 383.066 7 -5 -7 -5 2947.34 358.955 10 -5 7 -5 2102.21 754.069 1 -5 -7 -5 2738.67 393.969 8 -5 -7 -5 2265.09 667.140 3 -5 7 -5 2453.16 765.507 3 -5 -7 -6 9967.38 833.753 7 -5 7 -6 9510.39 757.560 7 -5 -7 -6 9709.58 691.093 10 -5 -7 -6 8756.42 709.699 9 -5 -7 -6 10603.3 1536.22 3 -5 7 -6 12583.8 1772.47 3 -5 -7 -6 9611.26 774.322 8 -5 7 -6 12925.4 1983.69 1 -5 -7 -7 160.477 130.518 8 -5 7 -7 74.0588 65.5592 7 -5 -7 -7 76.7314 77.9278 7 -5 -7 -7-27.5554 36.0810 9 -5 7 -7 89.2793 70.1550 9 -5 -7 -7 39.7829 71.2827 10 -5 7 -7-72.0616 169.694 3 -5 -7 -7 294.601 243.443 3 -5 -7 -8 1839.01 712.170 3 -5 7 -8 1739.43 717.568 3 -5 7 -8 2395.52 400.878 9 -5 -7 -8 2129.22 370.629 9 -5 -7 -8 2368.05 411.754 8 -5 -7 -8 2614.89 375.476 10 -5 7 -8 2437.89 406.568 7 -5 -7 -8 2620.43 466.472 7 -5 -7 -9 623.267 219.048 9 -5 7 -9 783.094 238.531 9 -5 -7 -9 554.452 233.442 7 -5 7 -9 581.355 203.115 7 -5 -7 -9 526.069 176.591 10 -5 -7 -10 5942.96 634.916 9 -5 7 -10 6625.05 667.314 9 -5 -7 -10 5813.54 561.563 10 -5 -7 -10 5430.11 688.714 7 -5 7 -10 5288.19 601.545 7 -5 -7 -11 983.098 245.601 9 -5 7 -11 720.924 213.289 9 -5 7 -11 822.406 219.068 7 -5 -7 -11 807.906 207.853 10 -5 7 -12 2012.51 326.611 7 -5 7 -12 2366.99 356.009 9 -5 -7 -12 2343.30 363.550 9 -5 7 -13 10.1090 41.2757 9 -5 -7 -13 73.1926 53.4600 9 -5 7 -14 912.095 161.555 9 -5 -7 -14 1193.08 192.578 9 -5 -8 18 708.963 157.461 5 5 8 -18 1043.10 170.686 4 5 8 -17 2106.27 313.900 11 5 -8 -17 2138.15 290.822 11 -5 -8 17 2287.80 342.922 5 5 8 -17 2001.99 283.299 4 5 -8 -17 2003.73 258.612 4 5 8 -17 2075.09 305.485 12 5 -8 -16 1689.88 288.878 11 5 8 -16 1600.35 308.033 11 -5 -8 16 1439.32 326.000 5 5 8 -16 1610.75 295.161 12 5 8 -16 1531.68 274.230 4 5 -8 -16 1779.26 275.549 4 5 8 -15 3116.26 436.626 12 5 -8 -15 3397.75 449.127 11 5 -8 -14 2489.03 369.516 4 5 8 -14 1605.09 320.418 12 5 -8 -14 1575.94 335.643 11 5 -8 -13 2474.39 408.925 11 5 8 -13 2230.26 368.217 12 5 8 -12 2943.50 425.764 12 -5 8 12 3231.39 909.737 14 -5 -8 12 2513.95 849.583 14 5 -8 -12 4338.84 502.024 4 5 -8 -12 2732.35 424.474 11 5 8 -11 21533.7 1127.77 12 -5 -8 11 20652.6 2352.17 14 -5 8 11 21324.2 2260.61 14 5 -8 -11 23373.0 1138.82 4 5 -8 -11 19558.5 1117.13 11 5 -8 -10 2610.73 369.556 4 -5 8 10 2069.07 640.022 14 -5 -8 10 1710.03 630.773 14 5 8 -10 1775.27 308.150 12 5 -8 -10 1896.38 333.207 11 5 8 -10 2437.99 786.835 1 5 -8 -9 9974.26 704.204 4 -5 -8 9 4124.80 947.971 14 -5 8 9 4571.93 928.371 14 5 -8 -9 5088.97 540.396 11 5 8 -9 11220.5 1613.72 1 5 8 -8 37519.0 2778.36 1 -5 -8 8 31605.7 2467.86 14 -5 8 8 33358.7 2122.44 13 5 8 -7 2937.19 684.881 2 5 8 -7 3356.80 790.010 1 5 -8 -7 3071.58 494.354 2 -5 -8 7 1771.21 578.315 14 -5 8 7 2047.51 519.681 13 5 8 -6 6732.37 1060.78 1 5 8 -6 6990.37 1010.33 2 5 -8 -6 5855.31 694.302 2 -5 -8 6 6658.12 1039.73 14 -5 8 6 6134.75 895.620 13 -5 -8 5 858.015 339.536 14 -5 8 5 749.431 311.410 13 5 8 -5 447.728 245.187 2 5 -8 -5 493.882 201.694 2 -5 8 5 375.339 253.048 1 5 8 -5 523.120 256.586 1 -5 -8 4 230768. 5161.81 14 -5 8 4 230619. 5322.80 13 -5 8 4 242871. 6362.42 1 5 8 -4 248180. 5690.18 1 5 8 -4 246155. 5231.32 2 5 -8 -4 244395. 4670.90 2 -5 -8 3 43813.9 2152.77 14 -5 8 3 54961.3 3162.76 1 -5 8 3 42480.6 2283.24 13 5 -8 -3 49328.2 2150.22 2 5 8 -3 48237.5 2319.12 1 5 8 -3 53621.9 2385.14 2 -5 8 2 624.276 357.598 1 5 8 -2 686.690 265.071 1 5 -8 -2 497.788 245.886 2 5 8 -2 442.655 203.510 2 -5 8 1 42759.4 2936.28 1 -5 8 1 40630.0 2254.44 13 5 -8 -1 44632.2 2231.35 2 5 8 -1 42040.5 1826.98 2 5 8 -1 42337.7 1855.94 1 -5 8 0 53.0408 105.787 13 -5 8 0 489.082 361.725 1 5 8 0 192.415 102.839 2 -5 8 -1 46619.4 3270.29 1 -5 8 -1 36810.9 2194.02 13 -5 8 -2 1796.73 664.378 1 -5 8 -2 4286.88 773.884 13 -5 8 -3 52393.9 3717.98 1 -5 -8 -3 49920.1 2986.58 3 -5 8 -4 2627.46 850.193 1 -5 -8 -4 2797.27 744.131 3 -5 8 -5 3200.97 428.164 7 -5 8 -5 3447.54 1038.75 1 -5 -8 -5 3565.06 483.407 7 -5 -8 -5 2997.72 380.039 10 -5 -8 -5 2730.70 399.772 8 -5 8 -5 4088.30 994.869 3 -5 -8 -5 4065.49 948.770 3 -5 -8 -6 614.044 199.057 9 -5 8 -6 654.615 471.468 1 -5 -8 -6 577.161 194.474 7 -5 8 -6 558.706 185.590 7 -5 -8 -6 612.790 200.556 8 -5 -8 -6 1050.15 530.042 3 -5 8 -6 603.424 398.584 3 -5 -8 -6 634.809 173.110 10 -5 8 -7 74.0948 64.1967 9 -5 -8 -7 240.378 152.072 9 -5 8 -7-53.9489 85.8386 7 -5 -8 -7 2.11648 101.543 7 -5 8 -7 62.5620 687.756 1 -5 -8 -7 61.9800 34.2360 10 -5 -8 -7 154.049 207.897 3 -5 8 -7 1.06247 104.862 3 -5 -8 -7 82.7108 100.323 8 -5 -8 -8 12316.5 1028.75 7 -5 -8 -8 11352.9 919.756 8 -5 -8 -8 11171.9 867.112 9 -5 8 -8 12099.4 908.128 9 -5 -8 -8 11630.7 792.558 10 -5 8 -8 11224.2 866.578 7 -5 -8 -9 26208.1 1207.12 10 -5 -8 -9 25525.3 1325.93 9 -5 8 -9 27436.5 1379.75 9 -5 -8 -9 26082.1 1512.56 7 -5 8 -9 25121.6 1309.66 7 -5 -8 -10 1769.17 347.009 9 -5 8 -10 1343.94 292.711 9 -5 8 -10 1544.55 317.428 7 -5 -8 -10 1482.77 278.775 10 -5 -8 -11 1694.25 324.638 9 -5 8 -11 1881.77 332.399 9 -5 8 -11 1902.69 339.768 7 -5 -8 -11 1926.96 314.467 10 -5 8 -12 177.911 87.2286 7 -5 -8 -12 421.099 154.142 9 -5 8 -12 480.545 165.340 9 -5 8 -13 366.332 124.348 9 -5 -8 -13 394.516 126.081 9 5 9 -18 11070.4 531.866 4 -5 -9 18 10412.5 550.913 5 5 9 -17 99.8143 68.3992 11 -5 -9 17 112.854 80.8448 5 5 9 -17 25.3428 10.5731 4 5 9 -17 45.8220 30.5666 12 5 9 -16 115.514 73.5787 12 5 -9 -16 88.4946 83.7552 4 5 -9 -16 5.70914 37.0635 11 -5 -9 16 92.9183 75.1140 5 5 -9 -15 74.3782 61.9864 4 5 9 -15 573.860 186.232 12 5 -9 -15 633.196 192.873 11 5 9 -14 8676.46 731.211 12 5 -9 -14 9654.48 738.988 4 5 -9 -14 9068.54 760.722 11 5 -9 -13 96.7606 76.7281 11 5 9 -13 13.4350 36.2372 12 5 9 -12 990.758 250.022 12 5 -9 -12 1046.74 274.458 11 -5 -9 12 1432.29 678.928 14 -5 9 12 1022.96 516.581 14 5 9 -12 259.507 343.526 1 5 -9 -12 445.040 153.522 4 5 -9 -11 5036.54 527.585 4 5 9 -11 6023.06 1368.48 1 5 -9 -11 4703.62 561.718 11 5 9 -11 4443.74 520.888 12 -5 -9 11 3748.30 1055.47 14 -5 9 11 4138.99 961.441 14 5 -9 -10 1440.81 281.269 4 5 -9 -10 2680.05 404.098 11 5 9 -10 2731.20 390.170 12 -5 -9 10 3463.16 953.628 14 -5 9 10 2850.24 777.688 14 5 9 -10 799.674 417.698 1 5 9 -9 10384.3 1620.42 1 5 -9 -9 8586.17 716.047 11 5 -9 -9 10775.1 733.456 4 -5 -9 9 8318.55 1397.99 14 -5 9 9 7343.64 1168.36 14 -5 -9 8 4518.98 999.731 14 -5 9 8 4340.03 792.135 13 5 9 -8 4155.39 953.768 1 -5 -9 7 18671.0 1826.28 14 -5 9 7 19293.4 1654.43 13 5 9 -6 1658.66 510.284 2 5 -9 -6 1163.26 303.831 2 5 9 -6 1705.27 552.751 1 -5 9 5 845.974 349.239 13 5 9 -5 2683.01 642.682 1 -5 9 5 3300.82 715.985 1 -5 -9 5 826.289 364.925 14 5 9 -5 3276.52 667.695 2 5 -9 -5 3234.26 531.757 2 -5 9 4 2311.38 562.051 13 -5 9 4 6959.71 1117.06 1 5 -9 -4 6207.49 762.704 2 -5 -9 4 2249.73 560.480 14 5 9 -4 6275.79 873.528 2 5 9 -4 5649.07 891.198 1 -5 9 3 6486.40 949.848 13 -5 9 3 8814.49 1338.45 1 5 -9 -3 7987.07 890.807 2 -5 -9 3 5800.23 845.576 14 5 9 -3 8164.35 972.627 1 5 9 -3 7648.32 910.877 2 -5 9 2 6214.99 1128.73 1 5 9 -2 7167.87 864.504 1 5 9 -2 5952.59 748.347 2 5 -9 -2 6619.50 851.503 2 -5 9 2 3744.43 712.479 13 -5 9 1 94988.2 4505.70 1 5 9 -1 92389.2 2783.96 2 5 -9 -1 94832.4 3339.50 2 -5 9 1 94242.6 3532.32 13 -5 9 0 24655.6 1842.59 13 -5 9 0 19927.4 2156.25 1 -5 9 -1 183.253 156.523 13 -5 9 -1 878.757 478.919 1 -5 9 -2 272.352 177.924 13 -5 9 -2 173.846 246.527 1 -5 9 -3 784.543 473.248 1 -5 -9 -4 6474.64 540.801 10 -5 9 -4 6578.62 601.025 7 -5 9 -4 6024.25 560.955 5 -5 -9 -5 20356.2 1107.05 8 -5 9 -5 19805.7 1080.10 7 -5 9 -5 18765.2 2083.68 3 -5 -9 -5 18105.7 1132.69 7 -5 -9 -5 21498.8 1020.28 10 -5 9 -5 17930.8 2436.62 1 -5 -9 -5 19742.2 1065.00 9 -5 -9 -6 3063.14 450.784 8 -5 9 -6 3069.77 440.781 7 -5 9 -6 3334.57 947.024 3 -5 -9 -6 2762.25 462.661 7 -5 -9 -6 3038.94 394.938 10 -5 9 -6 2938.93 1005.42 1 -5 -9 -6 3088.30 435.791 9 -5 -9 -7 4801.78 591.547 8 -5 9 -7 5032.21 578.843 7 -5 9 -7 6051.21 1321.67 3 -5 9 -7 4605.26 550.908 9 -5 -9 -7 4786.63 556.757 9 -5 -9 -7 5092.44 524.165 10 -5 9 -7 4941.33 1339.97 1 -5 -9 -7 5086.45 641.866 7 -5 9 -8 5553.91 610.499 9 -5 -9 -8 5331.31 607.099 9 -5 -9 -8 5450.51 635.739 8 -5 -9 -8 5329.52 548.203 10 -5 9 -8 4933.63 569.642 7 -5 -9 -9 183.491 115.649 9 -5 9 -9 100.558 93.6951 9 -5 -9 -9 199.503 114.894 10 -5 9 -9 62.6236 78.2933 7 -5 -9 -10 420.831 175.918 9 -5 9 -10 261.722 151.703 9 -5 -9 -10 366.602 145.609 10 -5 9 -10 312.786 159.071 7 -5 9 -11 886.807 223.573 9 -5 -9 -11 1085.70 252.020 9 -5 -9 -11 931.237 212.549 10 -5 9 -11 1004.20 235.744 7 -5 9 -12 393.950 136.282 9 -5 -9 -12 417.906 154.118 9 -5 9 -12 279.384 109.321 7 -5 9 -13 257.952 90.9922 9 -5 -9 -13 269.192 102.394 9 5 10 -18 1940.09 232.509 11 5 10 -18 1712.08 199.393 4 -5 -10 18 1936.42 220.149 5 5 10 -17 2123.54 289.501 12 -5 -10 17 2914.26 345.774 5 5 10 -17 3301.52 337.003 4 5 10 -17 2460.34 309.685 11 5 -10 -16 10401.3 697.874 11 5 10 -16 10031.7 700.793 12 5 -10 -16 9402.50 620.443 4 -5 -10 16 9361.31 736.043 5 5 -10 -15 10853.0 786.244 11 -5 -10 15 11318.5 941.036 5 5 -10 -15 11473.9 765.634 4 5 10 -15 10899.2 786.374 12 5 10 -14 651.021 182.109 9 5 -10 -14 483.965 173.778 11 5 10 -14 522.439 169.071 12 5 10 -13 539.735 168.227 9 5 10 -13 586.496 196.665 12 5 -10 -13 987.049 229.340 4 5 -10 -13 470.859 188.686 11 5 10 -12 15942.2 1008.47 12 5 -10 -12 15954.7 968.049 4 5 -10 -12 16056.0 1041.64 11 5 10 -11 8644.01 718.973 12 5 -10 -11 7836.76 733.280 11 -5 -10 11 6546.83 1336.64 14 -5 10 11 7834.06 1358.32 14 5 10 -10 6666.09 1410.28 1 5 -10 -10 6382.56 591.584 4 5 10 -10 4570.76 515.051 12 -5 -10 10 3945.80 983.835 14 -5 10 10 5113.95 1068.11 14 5 -10 -10 5615.04 617.563 11 5 10 -9 6074.71 579.334 12 -5 -10 9 4794.86 1056.00 14 5 -10 -9 3922.03 453.356 4 5 10 -9 2867.30 858.052 1 5 -10 -9 5867.25 605.225 11 -5 10 8 36140.7 2397.94 13 5 -10 -8 38034.2 1498.01 11 -5 -10 8 31767.9 2609.47 14 5 -10 -8 39165.8 1411.05 4 5 10 -8 38375.7 3037.03 1 5 10 -7 1687.57 593.568 1 -5 10 7 2687.02 643.456 13 -5 -10 7 1891.68 581.621 14 -5 10 6 5781.88 921.037 13 5 10 -6 5957.83 1056.48 1 -5 -10 6 5725.32 1011.86 14 5 10 -5 8368.69 1163.74 1 5 10 -5 9192.12 1148.61 2 5 -10 -5 9277.74 912.970 2 -5 10 5 9393.19 1261.04 1 -5 10 5 9376.00 1194.84 13 -5 -10 5 10160.7 1266.38 14 5 10 -4 797.424 329.166 2 5 -10 -4 1034.84 320.116 2 5 10 -4 1069.79 408.109 1 -5 10 4 1101.32 440.500 1 -5 10 4 913.400 378.484 13 -5 -10 4 1212.84 427.959 14 5 10 -3 665.308 269.132 2 5 -10 -3 572.459 253.462 2 -5 -10 3 363.272 255.058 14 -5 10 3 634.016 299.592 13 5 10 -3 758.444 327.968 1 -5 10 3 732.174 333.096 1 -5 10 2 35637.7 2777.76 1 -5 10 2 34540.7 2249.22 13 5 10 -2 35229.4 1904.86 2 5 10 -2 36242.7 2014.29 1 5 -10 -2 36381.8 2048.32 2 -5 10 1 44369.7 3191.65 1 5 10 -1 44477.5 1962.22 2 5 -10 -1 43644.0 2340.01 2 -5 10 0 7309.09 1346.59 1 -5 10 0 3269.75 698.626 13 -5 10 -1 6727.27 1331.20 1 -5 10 -1 6179.68 964.782 13 -5 10 -2 5170.39 1211.09 1 -5 10 -2 2133.75 575.678 13 -5 10 -3 20428.2 2527.45 1 -5 10 -3 18605.2 1734.12 13 -5 -10 -4 597.997 173.432 10 -5 10 -4 489.872 166.157 7 -5 -10 -4 526.446 189.386 9 -5 10 -4 621.915 472.629 1 -5 -10 -4 445.176 187.480 8 -5 10 -5 10381.9 1584.04 3 -5 -10 -5 10106.8 710.774 10 -5 -10 -5 10703.3 807.541 8 -5 10 -5 12121.1 2063.39 1 -5 -10 -5 9430.15 753.700 9 -5 10 -5 10274.2 789.658 7 -5 -10 -6 92.6528 73.1296 8 -5 10 -6-5.29557 18.8801 7 -5 10 -6 332.427 301.789 3 -5 -10 -6 6.53960 43.7016 9 -5 10 -6 148.077 149.773 1 -5 -10 -6 172.791 108.899 10 -5 -10 -7 216.786 124.297 8 -5 10 -7 82.4988 73.0318 7 -5 -10 -7 51.9185 42.3460 9 -5 -10 -7 289.103 133.621 10 -5 10 -7 394.222 137.711 1 -5 10 -8 2747.05 437.214 7 -5 -10 -8 3875.14 522.581 9 -5 10 -8 3632.47 500.231 9 -5 -10 -8 4250.71 487.795 10 -5 10 -9 24876.8 1293.52 9 -5 -10 -9 25377.7 1324.74 9 -5 10 -9 23953.5 1256.91 7 -5 -10 -9 25933.1 1184.29 10 -5 10 -9 26772.8 1224.43 12 -5 -10 -10 2309.86 355.660 10 -5 10 -10 3105.60 447.482 9 -5 -10 -10 2543.64 407.387 9 -5 10 -10 3341.12 450.030 7 -5 10 -11 1113.46 239.675 9 -5 -10 -11 1116.92 250.315 9 -5 10 -11 848.384 203.306 7 -5 -10 -11 1180.49 236.431 10 -5 10 -12 470.137 137.724 7 -5 10 -12 375.445 130.183 9 -5 -10 -12 283.955 120.154 9 -5 -10 -13 1852.96 253.713 9 -5 10 -13 1957.81 255.118 9 5 11 -17 201.008 90.1566 11 -5 -11 17 617.957 144.351 5 5 11 -17 210.846 90.7109 12 5 11 -17 648.115 139.631 4 5 11 -16 742.220 190.550 12 5 -11 -16 804.548 172.829 4 -5 -11 16 690.809 189.003 5 5 -11 -16 787.337 187.025 11 5 11 -15 150.415 91.4937 12 -5 -11 15 153.994 115.958 5 5 -11 -15 126.925 78.1819 11 5 -11 -15 211.971 102.740 4 5 11 -14 2915.19 393.150 9 5 -11 -14 3027.03 433.136 11 5 11 -14 2581.41 396.992 12 5 -11 -14 2963.63 409.113 4 5 11 -13 869.084 222.212 12 5 -11 -13 855.194 228.721 11 5 -11 -13 676.955 200.415 4 5 11 -13 699.179 206.099 9 5 11 -12 331.606 155.693 12 5 11 -12 711.746 213.577 9 5 -11 -12 766.494 206.055 4 5 -11 -12 402.082 180.779 11 5 -11 -11 10566.2 848.093 11 -5 -11 11 9293.01 1587.73 14 -5 11 11 10070.8 1558.64 14 5 11 -11 10094.0 787.121 12 5 -11 -10 7127.67 682.905 11 -5 -11 10 5864.47 1191.74 14 -5 11 10 6017.22 1163.97 14 5 11 -10 7012.89 652.180 12 5 11 -10 4852.01 1246.32 1 5 -11 -10 4806.13 527.051 4 5 -11 -9 20.5007 42.9824 11 -5 -11 9 42.1351 70.2010 14 5 11 -9 67.3395 27.6526 12 5 -11 -9 367.787 146.528 4 5 11 -9 501.614 379.787 1 5 -11 -8 11532.2 784.016 4 5 11 -8 10502.7 1635.00 1 5 11 -8 13861.2 878.449 12 -5 11 8 12458.3 1416.86 13 5 -11 -8 13762.6 926.024 11 -5 -11 8 11178.5 1570.96 14 -5 -11 7 7142.02 1235.55 14 5 11 -7 4491.48 998.193 1 -5 11 7 7274.20 1096.12 13 5 -11 -7 7788.37 680.729 11 5 -11 -7 5479.20 538.239 4 5 11 -6 23460.5 2143.83 1 -5 11 6 18773.2 1756.69 13 -5 -11 6 17648.9 1825.14 14 -5 11 5 1861.61 547.938 13 -5 -11 5 2000.66 584.915 14 5 11 -5 4672.02 886.797 1 5 -11 -5 4779.12 651.831 2 -5 11 5 4556.42 900.692 1 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3302.20 455.140 9 -5 13 -9 3324.23 409.388 12 -5 13 -9 2834.43 408.863 7 -5 -13 -9 3470.73 421.474 10 -5 13 -10 54.1306 77.1411 9 -5 -13 -10 111.729 88.2261 9 -5 13 -10 146.868 97.3294 7 -5 -13 -10 192.924 108.129 10 -5 -13 -11 658.571 156.366 10 -5 13 -11 734.129 177.213 9 -5 -13 -11 476.681 147.636 9 -5 13 -12 1174.13 195.057 9 5 14 -17 1901.01 222.105 11 5 14 -16 2064.09 259.361 12 5 14 -15 3430.63 387.840 12 5 14 -14 4207.17 466.968 12 5 -14 -14 3054.01 396.313 4 5 -14 -14 3891.02 480.214 11 5 -14 -13 674.197 214.436 11 5 14 -13 662.707 182.226 12 5 14 -13 951.520 220.033 9 5 -14 -12 3028.85 436.119 4 5 -14 -12 4075.00 549.252 11 5 14 -12 3539.09 468.030 12 5 -14 -11 1368.69 316.294 11 5 -14 -11 2414.00 395.552 4 5 14 -11 1583.25 306.805 12 5 -14 -10 28387.9 1492.16 11 5 14 -10 28186.4 1351.11 12 5 -14 -10 24875.9 1294.10 4 5 14 -9 17240.7 1056.94 12 5 -14 -9 17153.4 1157.18 11 5 14 -9 23370.4 2808.21 1 -5 -14 9 14755.1 2072.63 14 5 -14 -9 22964.4 1247.29 4 5 14 -8 19436.3 1128.49 12 5 14 -8 9845.10 1716.58 1 5 -14 -8 18976.4 1227.11 11 -5 -14 8 17047.0 2136.12 14 5 -14 -8 12431.9 915.436 4 5 -14 -7 1722.15 347.947 4 -5 14 7 401.102 270.222 13 5 -14 -7 1202.77 211.674 6 5 14 -7 2454.08 836.505 1 5 -14 -7 414.625 151.480 11 -5 -14 7 519.910 371.934 14 5 14 -7 739.944 238.480 12 5 -14 -6 1981.26 367.756 4 -5 14 6 3014.92 789.985 13 5 -14 -6 2540.40 317.511 6 5 14 -6 1925.21 711.807 1 5 -14 -6 2948.00 487.463 11 -5 -14 6 2610.63 799.080 14 5 14 -6 2496.64 450.909 12 5 -14 -5 1449.57 324.257 4 -5 14 5 1317.99 525.037 13 5 14 -5 1127.58 513.957 1 -5 14 5 1713.02 614.756 1 5 -14 -5 1315.11 325.566 11 5 -14 -5 1450.60 239.164 6 5 -14 -4 4534.54 429.294 6 -5 14 4 4372.98 957.487 13 -5 14 4 5799.35 1176.47 1 5 14 -4 4475.77 959.459 1 5 -14 -4 4818.77 651.277 11 5 -14 -4 4814.85 599.687 4 5 -14 -3 9892.22 635.104 6 -5 14 3 9537.49 1417.09 13 -5 14 3 11053.1 1767.51 1 5 -14 -3 9848.54 942.257 11 5 -14 -3 10087.1 881.515 4 -5 14 2 969.453 535.997 1 5 -14 -2 657.588 237.919 4 -5 14 2 904.764 400.227 13 -5 -14 2 829.830 186.951 10 5 -14 -2 365.727 200.837 2 5 -14 -2 741.051 245.911 11 5 -14 -2 755.959 173.467 6 -5 14 1-227.221 302.191 1 -5 -14 1-42.6391 41.5165 10 5 -14 -1 43.2767 40.1595 11 5 -14 -1 60.1257 53.4885 4 5 -14 -1 79.0259 74.1088 6 -5 14 1 123.576 128.093 13 5 -14 -1 23.9692 96.3677 2 5 -14 0 6676.44 766.453 4 -5 14 0 3610.37 859.966 13 5 -14 0 6709.59 530.755 6 5 -14 0 9730.23 1282.13 2 5 -14 0 3798.49 609.201 11 -5 14 0 9980.63 1800.06 1 -5 -14 0 5270.55 498.663 10 -5 -14 -1 5376.87 510.706 10 5 -14 1 6542.33 830.395 11 -5 14 -1 5230.91 1000.75 13 -5 14 -1 4689.81 1286.23 1 5 -14 1 5157.83 685.624 4 5 -14 1 5142.51 466.793 6 5 -14 2 567.596 249.520 4 5 -14 2 1441.00 386.811 11 -5 14 -2 1082.97 448.058 13 5 -14 2 658.227 175.177 6 -5 14 -2 379.887 360.086 1 -5 -14 -2 984.092 226.495 10 5 -14 3 308.464 179.250 4 -5 14 -3 267.083 476.908 1 -5 14 -3-15.3550 62.0539 13 -5 14 -3-94.5220 104.811 12 5 -14 3 273.337 109.299 6 -5 -14 -3 183.345 106.859 10 5 -14 3 58.8016 73.9712 11 -5 14 -4 1269.67 288.397 7 -5 -14 -4 527.172 163.403 10 5 -14 4 1210.39 219.443 6 -5 14 -4 540.417 185.779 12 -5 14 -5 3144.22 457.820 7 -5 -14 -5 3447.71 446.634 10 -5 14 -5 4101.93 500.183 12 -5 -14 -5 4240.17 509.706 8 -5 -14 -5 3528.65 493.223 9 -5 -14 -6 460.527 157.924 10 -5 -14 -6 367.476 165.497 9 -5 14 -6 453.874 165.816 12 -5 14 -6 360.060 168.950 7 -5 -14 -7 4758.67 524.325 10 -5 14 -7 3956.71 503.567 7 -5 14 -7 5314.76 543.532 12 -5 -14 -7 4562.11 558.448 9 -5 -14 -8 3012.58 402.415 10 -5 14 -8 3131.54 426.366 7 -5 -14 -8 3088.65 445.855 9 -5 14 -8 3279.21 456.905 9 -5 14 -8 3032.51 403.465 12 -5 14 -9 6983.18 639.279 9 -5 -14 -9 6850.64 642.868 9 -5 14 -9 6936.46 577.413 12 -5 -14 -9 6782.56 573.193 10 -5 14 -9 6327.16 584.160 7 -5 -14 -10 6979.99 541.863 10 -5 14 -10 7226.72 574.549 7 -5 14 -10 7157.47 594.167 9 -5 14 -11 442.287 136.107 9 -5 -14 -11 859.517 170.028 10 -5 14 -12 705.524 139.453 9 5 15 -16 760.421 145.689 12 5 15 -15 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1775.02 2 -7 7 -2 13535.4 881.347 7 -7 -7 -2 12791.6 811.669 8 -7 7 -2 16388.0 2138.69 1 -7 -7 -2 12063.3 721.935 10 -7 7 -2 12915.6 784.789 5 -7 -7 -3 6490.96 640.072 7 -7 -7 -3 6902.45 1215.94 3 7 -7 3 7315.87 1175.14 2 -7 7 -3 7033.97 1270.65 3 -7 7 -3 7427.77 677.417 7 -7 -7 -3 6317.50 608.982 8 -7 7 -3 7226.61 1444.97 1 -7 -7 -3 6628.42 560.572 10 -7 7 -3 6261.01 575.971 5 -7 -7 -4 7565.71 735.294 7 -7 -7 -4 4253.44 1008.76 3 7 -7 4 4655.54 959.799 2 -7 7 -4 5251.64 1165.06 3 -7 7 -4 7805.47 717.489 7 -7 -7 -4 8627.84 742.439 8 -7 7 -4 4597.25 1154.86 1 -7 -7 -4 10023.3 713.411 10 -7 7 -4 7692.02 663.043 5 -7 7 -5 4178.84 1086.06 3 -7 -7 -5 3952.38 1017.62 3 7 -7 5 4563.11 959.503 2 -7 7 -5 6495.02 674.882 7 -7 -7 -5 7601.94 636.377 10 -7 -7 -5 7052.67 698.937 8 -7 -7 -5 6733.51 718.263 7 -7 -7 -6 119.352 93.5145 10 7 -7 6 288.480 270.768 2 -7 -7 -6 145.717 103.360 8 -7 7 -6 118.513 58.0018 7 -7 -7 -6-8.09699 118.518 7 -7 -7 -7 10908.5 791.375 10 -7 -7 -7 11348.6 981.655 7 -7 7 -7 11055.4 906.792 7 -7 -7 -7 10822.5 906.505 8 -7 -7 -8 968.137 294.924 7 -7 7 -8 1067.67 273.849 7 -7 -7 -8 868.200 222.931 10 -7 -7 -8 903.291 264.125 8 -7 -7 -9 7277.20 628.687 10 -7 7 -9 7475.74 721.834 7 -7 7 -10 706.877 205.762 7 -7 7 -11 866.457 213.359 7 -7 7 -12 1624.92 245.214 7 7 -8 -18 257.091 82.4559 4 7 8 -18 128.625 61.4315 4 7 8 -18 320.901 105.639 11 7 -8 -18 348.116 112.867 11 -7 -8 18 156.853 70.9919 5 7 -8 -17-44.9218 33.4776 4 -7 -8 17 102.326 72.2164 5 7 8 -17 36.6163 31.7996 4 7 -8 -17 40.1415 25.6522 11 7 8 -17 100.239 62.9706 11 7 -8 -16 5440.59 548.983 11 7 8 -16 5312.40 558.196 11 7 -8 -16 5980.91 531.576 4 7 8 -16 5427.16 531.334 4 -7 -8 16 5418.22 529.438 5 7 -8 -15 14347.2 966.216 11 7 -8 -15 13932.4 877.657 4 -7 8 15 14106.1 768.005 5 -7 -8 15 13857.5 942.680 5 -7 8 14 645.346 171.548 5 -7 -8 14 513.225 210.600 5 7 -8 -14 719.179 229.905 11 7 -8 -14 420.260 164.888 4 -7 -8 13 5076.19 621.786 5 -7 8 13 5217.28 518.921 5 7 -8 -13 3768.01 535.367 11 7 -8 -13 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351.432 131.049 7 -7 8 -12 1562.78 227.272 7 7 9 -18 122.231 63.9926 11 -7 -9 18 74.0369 31.2828 5 7 9 -18 45.2783 43.8076 4 7 -9 -17 584.881 143.660 4 7 9 -17 614.171 156.383 4 7 9 -17 283.734 121.037 11 7 -9 -17 47.2168 25.0150 11 -7 -9 17 307.664 107.083 5 7 -9 -16 8791.58 685.063 11 7 9 -16 9652.31 726.886 11 7 9 -16 9260.01 672.317 4 7 -9 -16 9496.50 662.926 4 -7 -9 16 9306.98 668.485 5 -7 -9 15 323.861 124.414 5 7 -9 -15 577.244 191.623 11 7 -9 -15 306.275 129.389 4 7 -9 -14 4609.44 564.532 11 7 -9 -14 4933.97 540.674 4 -7 -9 14 4619.41 552.301 5 -7 -9 13 3772.59 521.213 5 7 -9 -13 4498.96 576.716 11 7 -9 -13 3952.95 491.434 4 -7 9 13 3591.04 417.207 5 -7 -9 12 72.9392 91.0508 5 -7 9 12 113.649 97.8251 5 7 -9 -12 108.188 72.5031 11 7 -9 -12 218.103 126.661 4 7 -9 -11 405.110 163.260 4 -7 -9 11 320.564 152.298 5 -7 9 11 449.880 144.883 5 7 -9 -11 802.688 240.718 11 -7 -9 11 390.164 282.825 14 -7 9 11 233.893 187.330 14 7 9 -11 362.605 317.179 1 7 9 -10 3951.91 1050.05 1 7 -9 -10 3827.21 520.316 11 -7 -9 10 2652.96 816.435 14 -7 9 10 3765.78 874.501 14 7 -9 -10 4169.06 506.618 4 -7 9 10 4189.34 455.078 5 -7 -9 10 4002.83 492.010 5 7 -9 -9 8577.49 702.493 4 7 -9 -9 9120.30 611.814 6 -7 -9 9 7866.74 1340.14 14 -7 9 9 8558.35 1274.46 14 7 -9 -9 9414.40 805.525 11 7 9 -9 9146.16 1582.51 1 -7 9 9 8481.92 631.577 5 -7 -9 9 8592.32 670.063 5 7 -9 -8 6062.90 575.490 4 7 -9 -8 6739.56 524.417 6 -7 -9 8 7994.31 1233.28 14 -7 9 8 8092.77 1194.25 14 7 -9 -8 8910.26 756.605 11 7 9 -8 5656.08 1189.36 1 7 9 -8 5188.89 1071.01 2 -7 9 8 6281.46 532.541 5 7 -9 -7 20329.6 1111.06 11 -7 9 7 21125.8 1907.11 14 -7 -9 7 18830.6 1899.77 14 7 -9 -7 16176.6 921.298 4 7 -9 -7 16563.1 1426.64 2 7 9 -7 15865.1 1776.05 2 7 9 -7 15716.4 1890.30 1 7 -9 -7 17640.0 854.158 6 -7 -9 6 814.148 373.498 14 7 -9 -6 1809.22 504.826 2 7 9 -6 1655.06 540.559 2 7 9 -6 1627.07 554.554 1 7 -9 -5 5874.93 886.386 2 7 9 -5 6035.09 1045.03 1 7 9 -5 6165.70 1007.65 2 -7 -9 5 7615.85 1092.43 14 7 -9 -4 39486.4 2383.92 2 7 9 -4 37125.2 2331.49 2 7 9 -4 37612.2 2477.19 1 -7 9 4 40561.3 3130.04 1 7 9 -3 7.71884 84.2080 2 7 -9 -3 10.6582 78.8108 2 -7 9 3 0.92454 46.8095 1 7 9 -2 11029.6 1202.89 2 7 -9 -2 10838.3 1305.55 2 -7 9 2 10388.7 1640.85 1 7 -9 -1 578.097 329.016 2 -7 9 1 768.152 475.007 1 -7 9 0 7671.79 1514.00 1 7 -9 0 8725.77 1265.91 2 -7 9 -1 1508.59 276.003 5 -7 9 -1 1554.69 303.270 7 -7 -9 -1 1330.76 260.879 8 7 -9 1 1866.26 276.668 6 -7 9 -1 1359.51 679.526 1 7 -9 1 1760.41 575.175 2 -7 -9 -1 1630.40 270.105 10 -7 -9 -2 44807.2 1687.45 7 -7 9 -2 45835.6 1546.06 5 -7 9 -2 41339.4 3003.04 3 7 -9 2 46807.0 3039.14 2 -7 9 -2 47111.8 1682.51 7 -7 9 -2 42592.2 3674.38 1 -7 -9 -2 50391.2 1686.21 8 -7 -9 -2 43949.8 1450.28 10 -7 -9 -3 6406.25 671.376 7 -7 9 -3 6633.57 614.823 5 -7 9 -3 7507.80 704.333 7 -7 -9 -3 6802.31 643.044 8 -7 -9 -3 6604.65 575.247 10 -7 9 -3 6582.37 1491.57 1 -7 9 -3 6451.00 1285.88 3 7 -9 3 7074.97 1208.57 2 7 -9 4 74.3405 131.448 2 -7 -9 -4 116.433 111.742 7 -7 9 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7 -10 -16 807.705 199.550 11 7 -10 -15 25595.0 1239.84 11 -7 -10 15 27587.9 1192.36 5 7 -10 -15 27921.0 1218.56 4 7 -10 -14 557.335 203.719 11 -7 -10 14 178.389 101.852 5 7 -10 -14 359.633 130.908 4 7 -10 -13 135.829 106.308 11 -7 -10 13 272.592 131.648 5 7 -10 -13 65.8957 95.4113 4 7 -10 -12 2722.98 449.982 11 -7 -10 12 2350.64 380.947 5 7 -10 -12 2574.89 403.363 4 -7 10 11 258.346 294.170 14 -7 -10 11-73.7534 196.649 14 -7 -10 11-58.3713 115.741 5 7 -10 -11 99.7417 96.4187 4 7 -10 -11-30.0453 76.8209 11 7 -10 -10 3897.25 488.108 4 -7 10 10 1307.51 570.084 14 -7 -10 10 1659.61 630.142 14 7 10 -10 4945.28 1270.36 1 -7 -10 10 2894.63 411.396 5 7 -10 -10 1806.37 354.201 11 7 10 -9 58828.8 4085.38 1 7 -10 -9 59855.5 1544.60 6 7 -10 -9 59259.3 1876.57 4 -7 -10 9 46306.6 3298.96 14 -7 10 9 49837.3 3208.07 14 -7 10 9 56457.0 1605.97 5 7 -10 -9 55468.8 1956.04 11 7 10 -8 15060.2 1956.63 1 7 10 -8 15461.8 1889.95 2 7 -10 -8 15441.8 805.699 6 7 -10 -8 15681.1 955.671 4 -7 10 8 15466.9 1674.41 14 -7 -10 8 13313.6 1745.56 14 -7 10 8 15066.6 816.439 5 7 -10 -8 16057.7 1034.19 11 7 10 -7 9171.27 1460.60 1 7 10 -7 9828.74 1429.19 2 7 -10 -7 9943.96 755.695 4 7 -10 -7 9676.40 638.549 6 7 -10 -7 10164.6 820.268 11 -7 10 7 9888.38 653.318 5 -7 -10 7 8106.28 1270.06 14 7 10 -6 783.175 406.602 2 7 -10 -6 937.159 378.023 2 7 -10 -6 1400.71 281.267 4 -7 -10 6 1571.33 537.492 14 7 10 -6 595.436 348.309 1 7 -10 -6 1341.04 238.415 6 7 -10 -6 1859.61 335.775 11 7 -10 -5 4413.61 547.296 11 -7 10 5 4200.83 929.119 13 7 -10 -5 6477.72 945.057 2 7 10 -5 6435.11 1052.05 2 7 10 -5 6156.32 1075.71 1 7 -10 -5 5960.25 581.130 4 7 -10 -5 5898.21 494.158 6 -7 -10 5 4258.12 854.166 14 -7 10 4 20103.1 2016.86 13 7 10 -4 18971.5 1732.48 2 7 -10 -4 19993.5 1727.35 2 7 10 -4 19478.1 1804.42 1 7 -10 -4 21007.0 933.759 6 -7 10 4 20128.6 2263.01 1 -7 10 3 28647.7 2407.79 13 7 -10 -3 31727.2 2193.69 2 7 10 -3 31398.7 2113.34 2 -7 10 3 31188.8 2818.68 1 7 -10 -3 31288.4 1143.75 6 -7 10 2 16638.9 1829.81 13 -7 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627.046 225.477 11 8 -6 -13 3583.26 478.674 4 8 -6 -13 4246.80 560.626 11 -8 -6 13 3820.44 505.118 5 -8 6 13 4146.61 487.621 5 -8 -6 12-5.72681 35.8386 5 -8 6 12 120.987 66.0517 5 -8 6 12 98.0885 277.817 14 8 -6 -12 16.7298 94.5955 11 8 -6 -12-26.8732 68.0269 4 8 6 -11 2809.02 856.985 2 8 -6 -11 2012.13 356.322 4 -8 6 11 518.730 285.861 14 -8 -6 11 517.110 357.938 14 -8 6 11 1809.02 323.355 5 -8 -6 11 2034.21 356.427 5 8 6 -11 2624.60 861.232 1 8 -6 -11 879.628 245.063 11 8 -6 -10 12564.2 861.946 4 8 -6 -10 15822.2 1036.88 11 8 6 -10 12786.7 1867.44 1 8 6 -10 13133.9 1768.81 2 -8 6 10 12714.3 826.088 5 -8 -6 10 11940.0 830.066 5 8 -6 -10 13253.8 772.584 6 -8 6 10 15297.9 1786.51 14 -8 -6 10 14020.3 1792.95 14 8 -6 -9 26924.1 1221.85 4 8 -6 -9 27635.8 1117.33 6 -8 6 9 27528.9 2189.85 14 -8 -6 9 30462.7 2557.97 14 -8 6 9 26608.9 1169.80 5 -8 -6 9 25313.5 1152.27 5 8 6 -9 27830.2 2635.51 1 8 -6 -9 27096.1 2027.15 2 8 6 -9 28324.3 2484.13 2 8 -6 -9 28846.9 1362.29 11 8 -6 -8 163.740 82.6640 11 8 -6 -8 312.807 122.165 4 8 -6 -8 271.355 193.327 2 8 6 -8 411.271 255.376 2 -8 -6 8 161.817 125.720 5 -8 6 8 89.1982 44.4768 5 8 -6 -8 173.033 94.3463 6 8 -6 -7 540.415 160.420 4 8 -6 -7 571.267 271.564 2 8 6 -7 177.188 188.015 2 -8 6 7 650.597 177.779 5 8 -6 -7 650.298 162.799 6 8 -6 -6-97.8613 121.244 2 8 6 -6 128.302 81.6253 2 8 6 -5 23942.9 2006.19 2 8 -6 -5 25749.2 2018.80 2 8 -6 -4 281.841 245.973 2 8 6 -4-32.2816 124.058 2 -8 6 3 14248.7 1783.61 1 8 6 -3 12540.8 1366.05 2 8 -6 -3 14731.1 1576.03 2 -8 6 2 54916.2 3684.26 1 8 6 -2 53616.4 2762.15 2 8 -6 -2 52757.1 2972.55 2 -8 6 1 739.124 424.537 1 8 6 -1 443.474 222.595 2 8 -6 -1 576.542 313.924 2 -8 6 1 552.128 319.086 3 -8 6 0 3068.40 906.071 1 -8 6 0 2715.68 385.242 7 -8 -6 0 2841.08 379.802 8 -8 6 0 2707.13 350.031 5 -8 6 0 3327.88 781.452 3 8 -6 0 3296.92 779.035 2 -8 -6 -1 1272.88 263.238 8 -8 6 -1 1760.64 699.723 1 -8 6 -1 1753.62 320.558 7 -8 6 -1 1474.40 273.593 5 -8 6 -1 1563.56 549.684 3 -8 -6 -1 1174.29 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2814.68 320.940 6 8 -18 -7 5990.42 487.449 6 8 -18 -7 6867.51 832.592 11 8 -18 -7 6014.24 721.836 4 8 -18 -6 4596.95 438.387 6 8 -18 -6 4673.38 693.190 11 8 -18 -6 3951.23 600.145 4 8 -18 -5 6114.83 520.682 6 8 -18 -5 6274.11 780.295 4 8 -18 -5 5465.18 771.186 11 8 -18 -4 3837.93 657.962 11 8 -18 -4 3063.19 373.211 6 8 -18 -4 2773.91 527.561 4 8 -18 -3 375.809 130.503 6 8 -18 -3 123.528 83.8342 11 8 -18 -3 378.177 186.072 4 8 -18 -2 10763.6 698.252 6 8 -18 -2 11118.6 1063.19 4 8 -18 -2 9226.35 1048.57 11 8 -18 -1 5099.01 475.287 6 -8 -18 1 5301.46 481.038 10 8 -18 -1 5122.15 709.137 4 8 -18 -1 5955.44 809.145 11 -8 18 0 3956.12 516.737 7 8 -18 0 4372.71 429.687 6 -8 -18 0 3576.79 403.687 10 8 -18 0 3813.75 597.072 4 8 -18 0 3105.11 589.069 11 -8 -18 -1 6217.79 540.186 10 -8 18 -1 5651.24 606.001 7 8 -18 1 6096.27 495.300 6 -8 18 -2 1414.85 307.337 7 -8 -18 -2 1067.83 215.885 10 8 -18 2 1229.69 205.935 6 -8 18 -3 59.6103 75.0960 7 8 -18 3 56.4282 44.0979 6 -8 -18 -3 64.7684 36.9366 10 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881.956 254.602 4 8 -20 -8 361.790 185.540 11 8 -20 -7 16016.3 735.099 6 8 -20 -7 16520.2 1233.66 11 8 -20 -7 16710.6 1166.31 4 8 -20 -6 339.380 183.081 4 8 -20 -6 336.452 166.742 11 8 -20 -6 261.981 100.383 6 8 -20 -5 810.456 273.248 4 8 -20 -5 933.859 312.809 11 8 -20 -5 678.462 163.359 6 8 -20 -4 104.326 127.200 4 8 -20 -4 57.2871 119.416 11 8 -20 -4 147.879 72.0913 6 8 -20 -3 123.292 110.999 4 8 -20 -3 295.877 223.942 11 8 -20 -3 127.157 71.9046 6 8 -20 -2 2423.44 318.270 6 8 -20 -2 2918.08 565.543 11 8 -20 -2 2446.64 479.033 4 8 -20 -1 10916.8 649.962 6 -8 20 1 10907.2 822.384 7 8 -20 -1 11071.2 1056.00 11 8 -20 -1 10908.0 988.168 4 -8 -20 0 1266.28 226.372 10 -8 20 0 632.184 211.926 7 8 -20 0 802.318 172.554 6 -8 -20 -1 1570.78 240.781 10 -8 20 -1 1835.72 324.313 7 8 -20 1 1849.91 248.203 6 -8 -20 -2 88.2957 59.9368 10 -8 20 -2 90.6435 80.0005 7 8 -20 2 32.5352 22.4463 6 -8 -20 -3 26.1284 16.8245 10 -8 20 -3 156.646 86.7358 7 -8 20 -4 5078.07 449.905 7 -8 -20 -4 4334.21 361.829 10 -8 20 -5 2841.98 312.901 7 -8 -20 -5 2438.41 255.244 10 8 -21 -11 1003.06 223.423 11 8 -21 -11 954.826 204.559 4 8 -21 -10 329.411 144.275 11 8 -21 -10 160.927 90.2218 4 8 -21 -9 2879.17 428.567 4 8 -21 -9 2207.80 398.420 11 8 -21 -8 148.959 50.9412 6 8 -21 -8 320.547 151.347 11 8 -21 -8 252.002 124.555 4 8 -21 -7 54.9601 45.6346 6 8 -21 -7 40.5850 78.6143 4 8 -21 -7 117.259 105.852 11 8 -21 -6 4381.37 375.330 6 8 -21 -6 5446.73 703.585 11 8 -21 -6 4841.77 613.250 4 8 -21 -5 1353.42 215.491 6 8 -21 -5 1613.43 410.930 11 8 -21 -5 1439.05 348.465 4 8 -21 -4 556.671 143.390 6 8 -21 -4 586.711 237.807 11 8 -21 -4 387.016 184.061 4 8 -21 -3 2036.59 275.652 6 8 -21 -3 2237.31 444.655 4 8 -21 -3 1398.81 366.763 11 8 -21 -2 9057.54 567.492 6 8 -21 -2 7883.51 872.531 11 8 -21 -2 8633.29 857.737 4 -8 21 1 99.0634 62.9083 7 8 -21 -1 71.2515 50.7858 6 -8 -21 0 1679.53 235.466 10 -8 21 0 1797.04 301.935 7 8 -21 0 1792.41 241.610 6 -8 -21 -1 491.916 125.029 10 -8 21 -1 596.155 172.362 7 8 -21 1 491.250 119.061 6 -8 -21 -2 64.6877 44.4048 10 -8 21 -2 127.277 74.4079 7 8 -21 2 138.261 56.4902 6 -8 21 -3 2270.32 300.445 7 -8 -21 -3 1792.58 225.074 10 -8 21 -4 1.87730 22.6702 7 -8 -21 -4 124.476 60.5856 10 8 -22 -10 824.768 202.286 11 8 -22 -10 148.894 75.1502 4 8 -22 -9 1492.00 308.001 11 8 -22 -9 1562.66 287.533 4 8 -22 -8 439.952 93.2185 6 8 -22 -8 572.757 177.997 4 8 -22 -8 336.521 152.694 11 8 -22 -7 11785.6 536.647 6 8 -22 -7 14067.7 1047.69 11 8 -22 -7 12339.3 905.611 4 8 -22 -6 1403.26 342.456 11 8 -22 -6 987.716 165.945 6 8 -22 -6 807.360 241.781 4 8 -22 -5 1534.32 360.011 11 8 -22 -5 1009.05 174.799 6 8 -22 -5 1142.79 293.142 4 8 -22 -4 1102.14 316.535 11 8 -22 -4 598.502 134.615 6 8 -22 -4 713.105 241.749 4 8 -22 -3 320.215 152.209 11 8 -22 -3 474.783 119.613 6 8 -22 -3 486.163 217.353 4 -8 22 2 271.110 118.796 7 8 -22 -2 151.116 69.5221 6 -8 22 1 12970.8 780.735 7 8 -22 -1 12644.3 619.437 6 -8 22 0 1690.65 281.399 7 8 -22 0 1644.27 214.887 6 -8 -22 0 1568.04 207.264 10 -8 22 -1 1248.58 229.278 7 8 -22 1 1347.17 179.897 6 -8 -22 -1 1564.19 198.787 10 8 -22 2 399.806 93.8138 6 -8 -22 -2 305.559 89.4314 10 -8 22 -2 318.841 108.899 7 -8 22 -3 426.248 112.414 7 -8 -22 -3 403.112 95.8186 10 8 -23 -9 1390.74 264.595 11 8 -23 -9 1493.30 254.834 4 8 -23 -8 280.487 132.866 11 8 -23 -8 254.583 113.909 4 8 -23 -7 280.435 131.409 11 8 -23 -7 299.547 114.988 4 8 -23 -7 233.658 65.1821 6 8 -23 -6 2273.35 377.607 4 8 -23 -6 2032.57 215.404 6 8 -23 -6 2533.67 416.704 11 8 -23 -5 4520.33 541.355 4 8 -23 -5 4175.08 323.200 6 8 -23 -5 3971.38 541.856 11 8 -23 -4 430.255 107.515 6 8 -23 -4 225.326 94.5043 4 -8 23 3 55.9499 48.6365 7 8 -23 -3 111.249 51.9568 6 -8 23 2 149.835 67.3986 7 8 -23 -2 261.896 85.6968 6 -8 23 1 492.241 145.071 7 8 -23 -1 297.235 86.6691 6 -8 23 0 634.063 156.252 7 8 -23 0 522.870 110.240 6 -8 23 -1 659.102 152.616 7 8 -23 1 499.289 100.175 6 -8 23 -2 595.825 132.264 7 8 -24 -7 3654.73 404.576 4 8 -24 -7 4134.04 462.554 11 8 -24 -6 564.628 166.469 4 8 -24 -6 715.945 111.646 6 8 -24 -5 45.6600 30.1345 6 8 -24 -5 38.8166 22.6967 11 8 -24 -5 83.3616 82.3368 4 8 -24 -4 28.9502 24.6338 6 -8 24 4 19.9854 15.5215 7 8 -24 -3 140.485 57.7779 6 -8 24 3-3.95649 35.0969 7 -8 24 2 3624.55 347.764 7 8 -24 -2 3421.37 273.146 6 -8 24 1 2631.75 294.349 7 8 -24 -1 2460.61 225.906 6 8 -24 0 53.7451 36.2826 6 -8 24 0 128.915 51.9860 7 8 -25 -3 51.1100 36.1750 6 -8 25 3 157.741 65.0617 7 9 0 -19 5.49690 24.4653 4 -9 0 19-12.7383 8.64837 5 9 0 -19 38.3078 32.9203 11 -9 0 18 3216.85 329.364 5 9 0 -18 3417.49 354.779 4 9 0 -17-28.5509 39.1965 11 -9 0 17-0.16628 17.0465 5 9 0 -17 22.1859 43.1596 4 9 0 -16 125.214 115.125 11 -9 0 16 204.037 111.389 5 9 0 -16 437.001 159.441 4 9 0 -15-37.6633 69.4242 11 9 0 -15 246.087 134.451 4 -9 0 15 51.0260 98.1941 5 -9 0 14 29241.4 1355.01 5 9 0 -14 27621.9 1356.53 4 9 0 -13 97.7427 95.6992 11 -9 0 13 107.318 102.898 5 9 0 -13 192.906 108.229 4 9 0 -12 2301.96 714.217 2 -9 0 12 2860.29 434.410 5 9 0 -12 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717.537 3 -9 6 -3 3486.18 504.939 7 -9 6 -3 2931.80 419.560 5 -9 -6 -3 3946.93 462.039 10 -9 -6 -3 3014.60 478.045 7 -9 -6 -4 16485.4 1092.36 8 -9 -6 -4 16870.8 956.406 10 -9 -6 -4 15624.9 1094.83 7 -9 6 -4 16194.4 1097.50 7 -9 -6 -5 18911.1 1176.74 8 -9 -6 -5 18278.4 1007.68 10 -9 6 -5 18522.6 1194.52 7 -9 -6 -5 16741.7 1158.94 7 -9 -6 -6 1624.98 306.134 10 -9 -6 -6 1500.99 335.412 8 -9 -6 -6 1833.00 383.538 7 -9 6 -6 1729.59 356.870 7 -9 6 -7 5472.91 634.203 7 -9 -6 -7 5461.00 654.631 7 -9 -6 -7 4495.10 564.394 8 -9 6 -8 1738.11 336.427 7 -9 6 -9 1129.28 248.399 7 -9 6 -10 3169.64 369.452 7 9 -7 -18 598.879 147.722 11 9 7 -18 617.144 142.602 11 -9 -7 18 789.154 145.419 5 9 -7 -18 806.131 156.870 4 9 7 -18 952.619 168.806 4 9 -7 -17-28.7499 51.5911 11 9 7 -17-1.70677 46.8063 4 9 7 -17 82.1723 82.6230 11 -9 7 17 92.8432 54.4734 5 -9 -7 17-16.3545 33.2703 5 9 -7 -17-44.7819 44.0324 4 9 -7 -16 885.971 231.618 11 -9 7 16 1219.58 208.155 5 9 7 -16 877.311 223.956 11 -9 -7 16 1176.80 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740.326 8 -11 -2 -7 964.045 223.460 7 -11 2 -7 862.916 219.141 7 -11 2 -8 1176.65 226.770 7 11 -3 -18 3617.30 344.186 11 11 3 -18 3601.03 343.577 11 11 3 -18 3406.65 297.143 4 11 -3 -18 3738.63 327.275 4 -11 3 18 4215.02 302.621 5 -11 -3 18 3783.07 300.509 5 11 -3 -17 277.434 108.433 4 11 -3 -17 287.196 94.8479 11 11 3 -17 301.478 103.026 4 11 3 -17 307.952 117.180 11 -11 3 17 296.902 98.5478 5 -11 -3 17 280.214 100.018 5 11 -3 -16 393.871 144.152 4 11 3 -16 242.071 106.842 4 11 3 -16 331.770 142.608 11 11 -3 -16 255.143 120.966 11 -11 3 16 379.470 121.290 5 -11 -3 16 224.481 98.4117 5 -11 3 15 12287.0 758.770 5 -11 -3 15 11512.0 748.853 5 11 -3 -15 10042.2 794.474 11 11 3 -15 9300.91 738.050 11 11 -3 -15 12066.6 781.838 4 11 3 -15 13053.6 828.832 4 -11 -3 14 5927.73 568.801 5 -11 3 14 6188.93 574.099 5 11 -3 -14 7379.73 714.643 11 11 3 -14 6943.06 670.995 11 11 -3 -14 5552.69 557.621 4 11 3 -14 5859.69 570.208 4 11 -3 -13 7791.50 574.888 6 11 -3 -13 9842.19 835.268 11 11 3 -13 9610.98 813.166 11 11 -3 -13 7138.30 648.037 4 11 3 -13 6976.45 643.979 4 -11 -3 13 7688.27 663.333 5 -11 3 13 8074.12 678.041 5 11 -3 -12 1072.76 259.500 4 11 3 -12 864.839 230.904 4 11 -3 -12 273.059 148.208 11 11 3 -12 110.210 110.311 11 11 -3 -12 846.372 210.505 6 -11 3 12 762.395 210.421 5 -11 -3 12 582.338 192.783 5 11 -3 -11 583.626 171.758 6 -11 3 11 842.812 227.362 5 -11 -3 11 710.434 219.337 5 11 -3 -11 599.865 189.462 4 11 -3 -11 326.148 170.131 11 11 -3 -10 275.555 116.796 6 -11 3 10 134.063 103.587 5 -11 -3 10 137.915 60.7402 5 11 -3 -10 335.539 134.517 4 11 -3 -9 3453.32 444.863 6 -11 -3 9 3617.92 447.987 5 -11 3 9 3639.46 466.218 5 -11 3 8 2009.30 345.587 5 -11 -3 8 1996.05 326.579 5 -11 -3 8 1544.97 295.196 8 11 -3 -8 1888.61 334.891 6 11 -3 -8 2961.69 845.670 2 11 3 -8 2711.06 836.585 2 -11 3 7 3531.65 453.994 5 -11 -3 7 3476.79 437.867 5 -11 -3 7 4508.65 500.881 8 11 -3 -7 3767.88 478.113 6 11 -3 -7 2064.40 682.016 2 11 3 -7 2631.94 815.129 2 -11 3 6 15604.3 932.377 5 -11 -3 6 15100.8 885.020 5 -11 3 6 12973.4 840.166 8 -11 -3 6 13789.2 876.700 8 11 -3 -6 15237.3 935.694 6 11 -3 -6 20832.0 2232.70 2 11 3 -6 19082.7 2148.48 2 11 -3 -5 306.321 149.358 6 -11 -3 5 364.932 159.240 8 -11 3 5 186.230 106.523 8 -11 3 5 349.590 148.458 5 -11 -3 5 467.206 147.288 5 11 -3 -5 456.467 382.542 2 11 3 -5 312.048 296.028 2 -11 -3 4 2298.36 371.262 8 -11 3 4 2318.56 359.435 8 -11 3 4 1928.45 332.497 5 -11 -3 4 2018.01 316.119 5 11 -3 -4 2155.34 351.053 6 11 -3 -4 1815.31 628.488 2 11 3 -4 1497.86 597.687 2 -11 -3 3 2297.47 376.841 8 -11 -3 3 1923.63 329.891 5 -11 3 3 1861.18 345.342 5 -11 3 3 2052.02 346.038 8 11 -3 -3 1841.47 318.701 6 11 -3 -3 1094.71 494.459 2 11 3 -3 1594.07 572.659 2 11 -3 -2 564.547 166.221 6 -11 3 2 265.138 114.561 8 -11 -3 2 330.423 157.363 8 -11 -3 2 658.638 188.821 5 -11 3 2 514.425 180.500 5 11 -3 -2 683.091 421.607 2 11 3 -2 908.959 469.990 2 -11 3 1 25499.8 1241.17 8 -11 -3 1 27208.2 1349.39 8 -11 -3 1 27626.3 1153.13 5 -11 3 1 26119.7 1222.42 5 11 -3 -1 27887.3 1180.79 6 -11 3 0 4363.27 523.565 8 -11 -3 0 3993.18 523.663 8 -11 3 0 4337.65 501.214 5 -11 3 0 4543.32 533.912 7 -11 -3 -1 5333.98 614.561 8 -11 3 -1 5569.47 590.957 8 -11 3 -1 5212.73 583.113 7 -11 3 -1 4688.83 526.759 5 -11 -3 -2 24.4082 57.7370 7 -11 3 -2 105.942 104.463 7 -11 3 -2 196.635 108.226 5 -11 -3 -2 121.009 110.735 8 -11 3 -2 88.3979 94.8648 8 -11 -3 -3 6915.35 701.106 7 -11 3 -3 6112.95 656.734 7 -11 3 -3 6227.96 623.700 8 -11 -3 -3 6625.72 689.816 8 -11 -3 -4 889.118 245.321 7 -11 3 -4 944.930 263.450 7 -11 3 -4 718.771 206.419 8 -11 -3 -4 939.380 245.254 8 -11 3 -5 19244.4 1121.73 7 -11 -3 -5 17648.6 1080.91 7 -11 3 -5 15865.6 914.976 8 -11 -3 -5 16520.6 1019.11 8 -11 -3 -6 1205.98 272.520 7 -11 3 -6 1508.20 305.505 7 -11 -3 -6 1193.96 277.401 8 -11 3 -6 1232.50 228.419 8 -11 -3 -7 914.884 222.122 7 -11 3 -7 926.797 226.606 7 -11 3 -8-25.8661 32.9246 7 11 -4 -18 570.396 126.741 4 11 -4 -18 480.717 123.953 11 11 4 -18 479.582 118.326 11 -11 -4 18 692.989 125.122 5 11 4 -17 985.440 188.927 4 11 -4 -17 1653.01 264.604 11 11 4 -17 1818.75 272.269 11 11 -4 -17 938.882 183.512 4 -11 -4 17 1380.01 209.328 5 -11 4 17 1307.29 197.366 5 11 -4 -16 405.356 154.245 11 -11 -4 16 1304.39 231.138 5 -11 4 16 1350.30 227.331 5 11 -4 -16 1792.15 288.058 4 11 4 -16 1831.07 283.023 4 11 4 -16 468.846 152.073 11 11 -4 -15 1024.36 222.695 4 11 4 -15 1145.35 238.786 4 11 4 -15 602.052 187.552 11 -11 4 15 1025.69 217.802 5 -11 -4 15 993.246 216.294 5 11 -4 -15 749.094 206.267 11 11 -4 -14 7204.01 635.783 4 11 4 -14 6944.64 617.186 4 -11 -4 14 7564.65 630.090 5 -11 4 14 7660.19 620.651 5 11 -4 -14 8958.55 781.606 11 11 4 -14 9037.56 760.082 11 -11 4 13 4391.18 487.795 5 -11 -4 13 3942.04 465.106 5 11 -4 -13 5022.10 595.629 11 11 4 -13 5486.12 604.789 11 11 -4 -13 3884.24 487.976 4 11 4 -13 3568.77 440.422 4 11 -4 -13 4083.56 403.001 6 -11 -4 12 15789.4 952.918 5 -11 4 12 17822.8 1008.96 5 11 -4 -12 14447.3 1018.46 11 11 4 -12 14484.9 990.177 11 11 -4 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4 5 13715.8 863.865 8 -11 -4 5 14575.7 926.446 8 11 -4 -5 14085.8 898.434 6 11 -4 -5 14467.5 1846.78 2 11 4 -5 13270.4 1780.99 2 -11 4 4 1206.40 272.903 5 -11 -4 4 1281.04 246.096 5 11 -4 -4 1087.02 520.034 2 11 4 -4 840.620 433.443 2 -11 4 4 1424.58 283.488 8 -11 -4 4 1307.66 283.135 8 11 -4 -4 1089.09 250.360 6 -11 -4 3 3140.26 405.000 5 -11 4 3 2737.83 423.339 5 -11 4 3 2620.09 387.080 8 11 -4 -3 2699.00 831.917 2 11 4 -3 1871.43 648.228 2 -11 -4 3 2539.95 397.853 8 11 -4 -3 2266.78 355.440 6 11 4 -2 6006.07 1132.10 2 11 -4 -2 6804.84 1308.78 2 -11 -4 2 8303.79 730.445 8 -11 4 2 7731.24 671.352 8 -11 4 2 6901.21 632.080 5 11 -4 -2 7059.62 617.785 6 -11 -4 1 1952.21 365.818 8 -11 4 1 2030.26 344.967 8 11 -4 -1 1921.00 310.319 6 -11 4 1 1607.22 305.602 5 -11 4 0 14107.8 943.551 7 -11 -4 0 13137.9 958.381 8 -11 4 0 12635.2 882.463 8 -11 4 0 14620.6 925.673 5 -11 -4 -1 395.047 152.307 8 -11 4 -1 359.696 137.441 8 -11 4 -1 318.073 161.815 7 -11 4 -1 485.483 173.557 5 -11 4 -2 5268.63 603.270 7 -11 -4 -2 4476.31 565.620 8 -11 4 -2 4641.32 532.881 8 -11 4 -2 4270.68 510.254 5 -11 -4 -3-15.9790 97.5604 7 -11 4 -3-11.4210 25.5150 7 -11 4 -3 215.781 125.671 8 -11 -4 -3 125.764 113.591 8 -11 4 -4 6336.94 594.695 8 -11 -4 -4 6926.85 690.662 8 -11 4 -4 7069.82 697.251 7 -11 -4 -4 6799.78 683.312 7 -11 4 -5 4083.97 449.138 8 -11 -4 -5 4298.81 523.497 8 -11 -4 -5 3498.03 478.370 7 -11 4 -5 4020.42 510.476 7 -11 -4 -6 7144.76 633.596 8 -11 4 -6 8252.83 704.091 7 -11 -4 -6 8228.70 691.387 7 -11 4 -7 104.995 66.5813 7 -11 4 -8 51.2699 51.6292 7 11 -5 -18 2677.19 267.431 4 11 -5 -18 3894.26 346.787 11 11 -5 -17 525.793 137.261 4 11 5 -17 527.222 133.483 4 11 -5 -17 516.975 150.245 11 11 5 -17 437.464 127.157 11 -11 5 17 442.246 111.821 5 -11 -5 17 389.126 105.700 5 11 -5 -16 5062.06 512.084 11 11 5 -16 4729.43 467.822 11 11 -5 -16 6498.86 537.408 4 11 5 -16 6106.59 505.666 4 -11 -5 16 5820.93 475.271 5 -11 5 16 6312.06 471.585 5 11 -5 -15 1041.20 243.759 11 -11 -5 15 1484.55 258.713 5 -11 5 15 1662.49 267.431 5 11 5 -15 1630.03 278.108 4 11 -5 -15 1424.44 266.599 4 11 5 -15 1057.79 237.651 11 11 -5 -14 18796.8 1100.53 11 11 5 -14 18524.2 1078.39 11 11 -5 -14 17861.9 1002.44 4 11 5 -14 17440.5 939.924 4 -11 -5 14 17950.9 952.777 5 -11 5 14 18791.2 954.340 5 11 -5 -13 143.724 99.5621 4 11 5 -13 169.278 73.6477 4 11 -5 -13-48.4167 47.3623 6 11 5 -13 99.1196 25.4039 11 -11 5 13 52.4140 43.5430 5 -11 -5 13 201.549 117.798 5 11 -5 -12 442.651 182.407 4 11 5 -12 446.739 174.311 4 11 -5 -12 538.848 155.631 6 11 5 -12 515.400 188.144 11 -11 5 12 406.921 146.860 5 -11 -5 12 219.239 96.9230 5 11 -5 -12 777.692 234.626 11 -11 -5 11 3173.09 420.662 5 -11 5 11 3224.53 431.559 5 11 -5 -11 1947.82 371.321 11 11 -5 -11 3885.85 491.376 4 11 -5 -11 2976.40 384.990 6 -11 5 10 18367.3 1038.88 5 -11 -5 10 17955.2 985.250 5 11 -5 -10 17716.9 1108.99 11 11 -5 -10 17667.7 1024.78 4 11 -5 -10 19804.1 1040.03 6 11 -5 -9 6.84088 21.0990 6 11 -5 -9-85.1336 88.6513 11 11 -5 -9 127.918 75.3671 4 -11 -5 9 145.434 102.738 8 -11 5 9 203.788 106.959 5 -11 -5 9 34.2229 36.3935 5 11 -5 -8 3011.85 416.346 6 -11 5 8 3249.19 432.426 5 -11 -5 8 2617.60 365.271 5 -11 -5 8 2968.62 398.355 8 11 -5 -7 2773.05 798.845 2 11 5 -7 2316.84 778.781 2 -11 -5 7 3231.31 417.538 8 11 -5 -7 3022.42 422.370 6 -11 5 7 2780.75 396.161 5 -11 -5 7 2642.36 369.595 5 -11 5 6 79.5441 81.6017 5 -11 -5 6 129.448 45.4055 5 11 -5 -6-80.1098 53.4081 6 11 5 -6-135.469 198.443 2 -11 -5 6-120.316 91.9005 8 -11 5 6 41.1333 53.0343 8 11 -5 -5 18126.8 2074.44 2 11 5 -5 17119.8 2005.99 2 -11 5 5 12444.9 819.730 8 -11 -5 5 12990.4 879.862 8 11 -5 -5 14349.2 910.368 6 -11 -5 5 15296.7 845.692 5 -11 5 5 14759.3 914.046 5 -11 5 4 766.156 211.346 5 -11 -5 4 896.583 241.661 8 -11 5 4 608.379 172.838 8 11 -5 -4 1057.65 518.159 2 11 5 -4 1096.86 518.470 2 11 -5 -4 772.361 200.381 6 -11 5 3 288.207 138.382 5 11 -5 -3 468.377 288.793 2 11 5 -3 397.757 267.397 2 -11 5 3 280.721 133.043 8 -11 -5 3 137.861 98.0730 8 11 -5 -3 309.198 118.826 6 -11 -5 2 3089.16 456.395 8 -11 5 2 3055.75 414.639 8 11 -5 -2 2447.08 355.943 6 -11 5 2 2668.32 397.489 5 -11 -5 1 5195.58 594.307 8 -11 5 1 4849.27 529.317 8 -11 5 1 5298.89 561.989 7 11 -5 -1 5100.29 496.687 6 -11 5 1 4934.35 532.920 5 -11 -5 0 4269.75 547.543 8 -11 5 0 3523.05 462.619 8 -11 5 0 3734.13 485.633 7 -11 5 0 3765.44 475.440 5 -11 5 -1 2665.23 429.446 7 -11 -5 -1 3037.70 477.598 8 -11 5 -1 3134.49 436.251 8 -11 5 -1 2554.93 389.641 5 -11 5 -2 707.430 198.967 5 -11 -5 -2 1085.96 277.857 8 -11 5 -2 854.867 236.029 8 -11 5 -2 855.095 241.881 7 -11 5 -3 5380.75 547.026 8 -11 -5 -3 5758.21 642.160 8 -11 5 -3 4936.48 581.570 7 -11 -5 -3 5156.34 580.755 7 -11 -5 -4 6472.31 666.853 8 -11 5 -4 6096.12 643.118 7 -11 -5 -4 5584.36 602.824 7 -11 -5 -5 3693.18 487.160 8 -11 -5 -5 3802.08 487.411 7 -11 5 -5 3999.86 501.933 7 -11 -5 -6 6642.72 605.687 8 -11 5 -6 7470.15 655.472 7 -11 5 -7 724.658 185.097 7 -11 5 -8 407.550 128.764 7 -11 6 17 96.6213 49.4787 5 -11 -6 17 69.9761 35.8751 5 11 -6 -17 292.961 120.385 11 11 6 -17 124.247 70.6077 4 11 6 -17 388.758 119.737 11 11 -6 -17 126.651 62.9525 4 -11 6 16 95.1173 59.2670 5 -11 -6 16 32.4633 45.4877 5 11 6 -16 75.4853 48.6627 4 11 -6 -16 127.052 82.8471 11 11 -6 -16 2.63225 34.1406 4 11 -6 -15 1337.43 283.238 11 -11 -6 15 1552.01 253.774 5 -11 6 15 1558.24 248.478 5 11 6 -15 1201.22 248.193 11 11 -6 -15 1503.20 278.295 4 11 6 -15 1673.97 281.141 4 -11 -6 14 935.978 185.079 8 11 6 -14 935.390 214.315 4 -11 6 14 987.082 211.603 5 -11 -6 14 858.087 201.998 5 11 -6 -14 875.040 226.774 11 11 6 -14 952.006 249.448 11 11 -6 -14 854.656 233.302 4 -11 -6 13 1031.56 208.750 8 -11 6 13 898.633 215.236 5 -11 -6 13 1082.22 234.866 5 11 6 -13 739.302 206.831 4 11 6 -13 1092.39 268.066 11 11 -6 -13 729.243 221.893 4 11 -6 -13 1303.36 295.234 11 11 -6 -12 18835.7 899.181 6 11 -6 -12 19047.1 1154.94 11 -11 -6 12 17452.9 955.807 5 -11 6 12 19028.5 1012.66 5 11 -6 -12 17139.7 1017.05 4 11 6 -12 15798.4 911.279 4 -11 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6037.68 607.476 7 -11 -6 -6 93.1313 72.8004 8 -11 6 -6 61.0695 40.8671 7 -11 6 -7 4855.63 476.550 7 -11 6 -8 266.736 101.265 7 -11 -7 17 243.591 77.7937 5 11 7 -17 280.110 96.8563 4 11 -7 -17 396.625 134.934 11 11 7 -17 351.577 114.877 11 11 -7 -17 301.070 101.650 4 11 7 -16 7674.44 573.184 11 11 -7 -16 7082.30 596.687 11 -11 7 16 8802.64 505.127 5 -11 -7 16 7731.19 494.907 5 11 7 -16 8134.13 545.535 4 11 -7 -16 8382.99 603.278 4 -11 7 15 501.291 134.720 5 -11 -7 15 399.742 121.546 5 11 7 -15 324.861 107.412 4 11 7 -15 618.432 178.201 11 11 -7 -15 537.620 167.544 4 11 -7 -15 416.975 161.953 11 -11 7 14 20379.6 945.332 5 -11 -7 14 18579.1 902.078 5 11 -7 -14 17071.8 1045.00 11 11 7 -14 17115.6 977.091 11 11 7 -14 20699.4 991.179 4 11 -7 -14 20554.8 1064.84 4 -11 -7 13 1766.80 293.236 5 -11 7 13 1884.61 306.575 5 11 7 -13 1030.15 251.196 11 11 7 -13 2171.70 328.011 4 11 -7 -13 2224.56 373.622 4 11 -7 -13 1159.90 283.408 11 11 -7 -12 2923.67 343.069 6 -11 -7 12 2548.70 352.524 5 -11 7 12 2987.16 391.821 5 11 -7 -12 4137.09 544.166 11 11 -7 -12 2789.45 422.966 4 -11 -7 12 3193.56 368.972 8 11 -7 -11 1745.58 281.150 6 -11 7 11 1799.20 312.407 5 -11 -7 11 1725.36 299.930 5 11 -7 -11 2336.47 411.541 11 11 -7 -11 1390.79 290.499 4 -11 -7 11 2246.72 322.199 8 11 -7 -10 6890.85 592.943 6 11 -7 -10 7569.78 737.665 11 -11 -7 10 6288.17 557.741 5 -11 7 10 6740.97 615.907 5 11 -7 -10 6277.68 636.274 4 -11 -7 10 7345.28 596.205 8 11 -7 -9 1058.58 293.008 11 -11 7 9 1378.71 279.590 5 -11 -7 9 1342.08 250.994 5 11 -7 -9 1214.87 249.373 6 11 -7 -9 1588.74 314.616 4 -11 -7 9 1076.18 223.818 8 11 -7 -8 10705.0 767.923 6 -11 7 8 10400.4 771.984 5 -11 -7 8 9906.69 726.219 8 11 -7 -8 11852.2 861.360 4 -11 7 7 4153.71 498.306 5 11 -7 -7 4618.66 508.836 6 -11 -7 7 4648.66 510.200 8 11 -7 -6 250.501 97.7776 6 -11 -7 6 184.061 101.009 8 -11 7 6 270.229 117.579 8 -11 7 6 400.082 161.680 5 -11 7 5 5374.68 563.578 5 -11 7 5 4871.15 498.117 8 -11 -7 5 4966.85 537.925 8 11 -7 -5 4933.27 525.640 6 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372.763 11 -11 13 9 1955.98 302.745 5 11 -13 -9 1902.55 275.285 6 11 -13 -9 1809.90 363.134 4 11 -13 -8 14843.7 1052.33 4 -11 13 8 18419.0 931.949 5 11 -13 -8 17046.4 860.588 6 11 -13 -8 16879.1 1211.91 11 11 -13 -7 48.4072 54.9426 6 -11 13 7 59.0814 28.6216 5 11 -13 -7 263.357 155.910 11 11 -13 -7 102.903 94.0506 4 11 -13 -6 3423.88 399.706 6 11 -13 -6 3693.99 532.685 4 -11 13 6 3874.37 440.434 5 11 -13 -6 3339.49 529.198 11 -11 13 5 1532.89 287.349 7 -11 13 5 1674.44 298.595 5 11 -13 -5 1355.92 253.596 6 -11 13 4 25827.7 1220.43 7 11 -13 -4 26555.5 1116.61 6 -11 13 4 26130.7 1179.70 5 -11 13 3 4448.93 518.144 7 11 -13 -3 4757.95 466.547 6 -11 13 3 4612.31 508.454 5 -11 13 2 2438.22 388.662 7 11 -13 -2 2581.96 337.883 6 -11 13 2 2292.67 357.926 5 -11 13 1 3229.24 444.913 7 11 -13 -1 3267.42 363.273 6 -11 13 1 3173.93 421.390 5 -11 13 0 5067.38 554.529 7 11 -13 0 5025.99 416.773 6 -11 -13 0 5825.77 560.533 8 -11 13 0 5309.67 542.788 5 -11 13 -1 217.081 118.027 7 -11 -13 -1 138.745 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524.186 8 -12 7 4 5650.65 585.277 5 -12 7 3 174.367 113.482 5 12 -7 -3 88.7705 86.7007 6 -12 -7 3 87.0116 79.0024 8 -12 7 3-6.22018 11.9691 8 12 -7 -2 7956.75 611.660 6 -12 7 2 6771.10 605.629 8 -12 -7 2 7331.01 697.388 8 -12 7 2 7702.21 677.532 5 -12 7 1 316.235 118.652 5 -12 7 1 349.241 162.536 7 -12 -7 1 459.008 179.282 8 -12 7 1 397.106 146.712 8 12 -7 -1 315.824 120.288 6 -12 7 0 11914.6 841.372 5 -12 -7 0 10786.3 863.154 8 -12 7 0 10424.3 785.826 7 -12 7 -1 219.210 109.153 7 -12 -7 -1 259.993 129.249 8 -12 7 -1 199.244 106.836 5 -12 -7 -2 1106.24 275.559 8 -12 7 -2 1102.87 257.362 7 -12 -7 -3 181.140 121.427 8 -12 7 -3 260.122 113.205 7 -12 7 -4 14763.9 859.957 7 -12 -7 -4 13965.3 869.639 8 -12 -7 -5 452.266 143.089 8 -12 7 -5 734.283 183.226 7 -12 7 -6 1199.97 212.456 7 12 -8 -16 2327.87 309.780 11 12 -8 -16 2522.59 295.486 4 12 -8 -15 634.693 181.064 11 -12 8 15 1066.56 173.081 5 -12 -8 15 975.725 160.193 5 12 -8 -15 1152.73 223.123 4 -12 8 14 88.8669 57.0158 5 -12 -8 14 90.7438 59.0303 5 12 -8 -14 289.140 119.233 11 12 -8 -14 121.471 86.9793 4 -12 8 13 14970.1 777.719 5 -12 -8 13 15073.4 731.421 5 12 -8 -13 15481.4 982.984 11 12 -8 -13 14425.3 654.307 6 12 -8 -13 15072.0 896.737 4 -12 8 12 6906.77 556.464 5 -12 -8 12 6955.50 517.150 5 12 -8 -12 6840.75 671.250 11 12 -8 -12 6855.16 498.458 6 12 -8 -12 6151.81 588.284 4 12 -8 -11 369.990 129.846 6 -12 8 11 451.276 149.995 5 12 -8 -11 230.218 97.7082 11 -12 -8 11 391.444 134.072 8 12 -8 -11 368.179 146.276 4 12 -8 -10 1562.53 311.556 4 -12 8 10 1665.89 295.602 5 12 -8 -10 1324.20 288.201 11 -12 -8 10 1668.88 276.417 8 12 -8 -10 1572.25 269.141 6 12 -8 -9 1439.06 290.107 4 12 -8 -9 1202.28 279.178 11 -12 8 9 1375.50 273.770 5 12 -8 -9 1591.52 283.889 6 -12 -8 9 1451.86 272.935 8 -12 8 8 85.1738 93.0535 5 12 -8 -8 98.4107 92.8864 6 -12 -8 8 129.076 84.2572 8 -12 8 8 85.9749 42.8770 8 12 -8 -7 4919.74 513.809 6 -12 -8 7 5825.70 570.683 8 -12 8 7 5212.75 547.742 5 -12 8 7 5490.39 529.898 8 12 -8 -6 3872.51 457.081 6 -12 -8 6 4068.87 485.360 8 -12 8 6 3820.80 481.342 5 -12 8 6 4375.21 480.551 8 -12 8 5 228.949 118.616 5 12 -8 -5 428.283 156.393 6 -12 8 5 139.955 89.1142 8 -12 -8 5 322.453 156.795 8 -12 8 4 1054.95 259.553 5 12 -8 -4 1263.64 261.491 6 -12 8 4 1351.09 265.597 8 -12 -8 4 1401.00 300.399 8 -12 8 3 255.305 122.763 5 -12 8 3 405.145 156.064 8 -12 -8 3 220.274 116.512 8 12 -8 -3 256.858 107.851 6 -12 8 2 1345.39 266.232 7 -12 8 2 1209.99 266.066 5 -12 -8 2 1114.00 277.233 8 12 -8 -2 1594.29 280.364 6 12 -8 -1 1835.55 284.262 6 -12 8 1 1800.87 327.545 5 -12 -8 1 2624.70 433.506 8 -12 8 1 1913.44 329.203 7 -12 8 0 62.0974 61.7734 5 -12 -8 0 294.056 139.923 8 -12 8 0 224.874 95.4800 7 -12 -8 -1 7624.51 709.554 8 -12 8 -1 8053.42 679.643 5 -12 8 -1 8220.14 695.029 7 -12 -8 -2 26.8331 80.0363 8 -12 8 -2 108.173 105.063 7 -12 -8 -3 398.508 164.283 8 -12 8 -3 419.063 156.478 7 -12 -8 -4 550.038 180.277 8 -12 8 -4 410.990 142.685 7 -12 8 -5 4504.61 430.857 7 -12 -8 -5 3861.21 403.073 8 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364.145 136.201 8 -12 -9 7 436.581 153.154 8 12 -9 -7 326.346 149.954 6 -12 9 6 156.099 91.7143 5 -12 9 6 178.344 92.0271 8 -12 -9 6 217.212 113.167 8 12 -9 -6 99.9792 59.6888 6 -12 9 5 1329.93 281.388 5 12 -9 -5 1291.51 244.515 6 -12 9 5 1379.93 263.577 8 -12 -9 5 1113.45 251.660 8 12 -9 -4 11013.8 744.539 6 -12 9 4 11021.6 800.230 5 -12 -9 4 11093.6 825.585 8 -12 9 3 444.686 166.263 5 -12 -9 3 366.009 154.930 8 12 -9 -3 403.755 143.998 6 12 -9 -2 21656.6 987.714 6 -12 9 2 21755.6 1129.93 5 -12 -9 2 25114.4 1262.36 8 -12 9 2 22931.1 1132.99 7 -12 9 1 447.969 173.230 5 12 -9 -1 470.208 140.628 6 -12 9 1 508.507 167.733 7 -12 -9 1 782.664 229.072 8 -12 9 0 728.370 195.581 7 -12 -9 0 695.186 217.080 8 -12 9 0 606.688 185.578 5 -12 -9 -1-84.9023 92.1335 8 -12 9 -1-12.8253 60.4822 7 -12 -9 -2 581.129 190.165 8 -12 9 -2 522.421 176.823 7 -12 -9 -3 442.448 162.231 8 -12 9 -3 315.146 131.906 7 -12 9 -4 9204.52 641.579 7 -12 -9 -4 7361.34 595.776 8 -12 9 -5 774.908 170.668 7 12 -10 -15 1088.48 223.573 11 12 -10 -15 1852.22 270.314 4 -12 10 14 1298.27 184.715 5 12 -10 -14 1192.35 236.929 4 12 -10 -13 5192.41 559.988 11 12 -10 -13 6482.10 580.703 4 -12 10 13 6736.35 473.767 5 12 -10 -12 2073.23 371.141 11 12 -10 -12 2516.94 371.960 4 12 -10 -12 2315.55 266.956 6 -12 10 12 2582.04 311.833 5 12 -10 -11 2766.11 433.034 11 12 -10 -11 2527.04 385.483 4 12 -10 -11 2594.42 312.451 6 -12 10 11 2663.68 333.372 5 12 -10 -10 6789.02 643.222 4 12 -10 -10 7063.67 551.389 6 12 -10 -10 6341.24 670.681 11 -12 10 10 7144.58 578.615 5 -12 10 9 7051.01 591.582 5 -12 10 9 6924.45 551.716 8 12 -10 -9 7150.91 682.011 4 12 -10 -9 6539.33 710.496 11 12 -10 -9 6723.15 555.869 6 -12 10 8 96.0002 69.4763 5 12 -10 -8 151.383 98.3597 6 -12 10 8 56.5367 67.2812 8 12 -10 -7 10190.7 708.603 6 -12 10 7 10211.9 690.892 8 -12 -10 7 10620.6 725.545 8 -12 10 7 11093.4 832.625 5 12 -10 -6 1609.87 279.798 6 -12 -10 6 2165.48 338.008 8 -12 10 6 1764.60 316.556 5 12 -10 -5 7254.42 601.080 6 -12 10 5 7247.51 642.540 5 -12 -10 5 5977.00 577.585 8 -12 10 4 93.7135 81.7489 5 -12 -10 4 107.931 102.852 8 12 -10 -4 115.222 79.9797 6 12 -10 -3 7665.92 594.922 6 -12 -10 3 6865.94 632.945 8 -12 10 3 7160.91 643.529 5 -12 10 3 7073.55 610.646 7 -12 10 2 245.059 122.514 5 -12 -10 2 411.988 162.868 8 12 -10 -2 267.558 108.936 6 -12 10 2 387.805 153.845 7 12 -10 -1 2238.52 292.613 6 -12 10 1 2617.54 389.307 7 -12 -10 1 2514.20 405.499 8 -12 10 1 2491.38 380.875 5 -12 10 0 1622.57 302.779 7 -12 -10 0 1834.98 341.349 8 -12 10 0 1424.65 278.628 5 -12 10 -1 134.611 73.3558 7 -12 -10 -1 197.593 116.369 8 -12 10 -2 31.8314 47.1079 7 -12 -10 -2-12.4937 52.8182 8 -12 10 -3 1306.44 252.727 7 -12 -10 -3 1022.76 230.517 8 -12 10 -4 1033.98 210.087 7 -12 -10 -4 965.334 203.918 8 -12 10 -5 2535.15 293.182 7 12 -11 -15 9733.40 601.775 4 -12 11 15 9817.12 447.504 8 12 -11 -15 9797.95 653.380 11 12 -11 -14 2270.45 312.132 4 12 -11 -14 1672.78 294.733 11 -12 11 13 8.97732 30.5617 5 12 -11 -13 25.9110 49.1395 11 12 -11 -13 79.6159 82.2079 4 -12 11 12 6579.67 476.649 5 12 -11 -12 6552.32 601.359 4 12 -11 -12 6387.85 421.690 6 12 -11 -12 5719.16 616.575 11 12 -11 -11 1279.24 297.050 11 12 -11 -11 1282.51 212.858 6 -12 11 11 1387.01 231.755 5 12 -11 -11 1102.09 250.274 4 12 -11 -10 1920.70 341.820 4 -12 11 10 1899.79 281.199 5 -12 11 10 1875.95 275.446 8 12 -11 -10 2448.21 422.835 11 12 -11 -10 1987.26 280.040 6 -12 11 9 7061.27 582.866 5 -12 11 9 6703.41 521.315 8 12 -11 -9 6886.04 676.527 4 12 -11 -9 6428.43 695.769 11 12 -11 -9 7523.56 576.897 6 -12 11 8 10944.4 780.078 5 -12 11 8 10022.0 639.362 8 12 -11 -8 9404.02 782.999 4 12 -11 -8 9556.88 669.159 6 12 -11 -8 9790.49 861.596 11 12 -11 -7 473.523 150.685 6 -12 11 7 610.351 189.347 5 12 -11 -6 6792.32 572.673 6 -12 11 6 7182.63 622.079 5 -12 -11 6 6169.56 548.801 8 -12 11 5 688.901 190.098 5 -12 -11 5 602.441 182.416 8 12 -11 -5 944.988 216.942 6 -12 11 4 1155.20 256.457 5 12 -11 -4 1545.33 270.976 6 -12 -11 4 1334.61 273.686 8 -12 11 3 293.865 133.500 5 -12 -11 3 393.296 137.541 8 12 -11 -3 143.359 76.7091 6 -12 11 3 223.248 118.720 7 12 -11 -2 30912.0 1117.33 6 -12 -11 2 28583.6 1280.82 8 -12 11 2 30941.6 1296.89 7 -12 11 2 29655.2 1276.32 5 -12 11 1 648.969 200.008 5 -12 -11 1 941.508 224.291 8 -12 11 1 855.589 215.954 7 12 -11 -1 884.716 179.406 6 -12 -11 0-41.5263 53.9556 8 -12 11 0-48.0596 73.7267 7 -12 11 0 25.4084 55.5470 5 -12 -11 -1 826.607 209.454 8 -12 11 -1 1062.74 234.110 7 -12 -11 -2 523.443 155.396 8 -12 11 -2 614.111 176.460 7 -12 -11 -3 834.759 198.878 8 -12 11 -3 762.996 188.720 7 -12 11 -4 4513.63 418.643 7 -12 11 -5 3204.42 312.005 7 12 -12 -15 3083.76 325.828 4 12 -12 -15 2926.15 340.099 11 12 -12 -14 358.691 121.853 4 12 -12 -14 300.413 111.208 11 -12 12 14 364.862 87.6707 8 12 -12 -13 3151.99 389.702 4 12 -12 -13 3196.91 429.381 11 -12 12 13 3230.20 289.333 8 12 -12 -12 415.066 144.420 4 12 -12 -12 18.4546 57.4020 11 -12 12 12 598.223 147.895 5 12 -12 -12 336.211 92.2261 6 -12 12 12 229.728 84.3002 8 -12 12 11 3214.06 350.792 5 12 -12 -11 2149.69 378.322 11 12 -12 -11 2648.30 400.433 4 12 -12 -11 2499.79 278.757 6 -12 12 11 2450.69 279.998 8 12 -12 -10 3094.28 472.586 11 12 -12 -10 3496.34 471.787 4 -12 12 10 4021.01 421.931 5 12 -12 -10 3471.55 352.642 6 -12 12 10 3718.93 357.113 8 -12 12 9 10111.9 670.147 5 12 -12 -9 9399.84 777.613 4 12 -12 -9 8481.68 796.835 11 12 -12 -9 9092.42 597.461 6 12 -12 -8 283.119 153.105 11 -12 12 8 62.1694 74.6014 5 12 -12 -8 190.204 116.166 4 12 -12 -8 141.498 79.5968 6 -12 12 7 8325.17 635.325 5 12 -12 -7 7939.00 597.981 6 -12 12 6 2980.80 387.100 5 12 -12 -6 3251.38 391.346 6 -12 12 5 6388.02 569.911 5 12 -12 -5 6704.76 548.118 6 12 -12 -4 14327.9 789.130 6 -12 -12 4 14318.5 850.460 8 -12 12 4 13552.6 845.006 5 -12 12 3 1674.26 295.729 5 -12 -12 3 1391.59 269.117 8 -12 12 3 1586.42 280.343 7 12 -12 -3 1856.29 275.761 6 -12 -12 2 811.293 213.030 8 -12 12 2 847.083 223.634 5 -12 12 2 763.341 197.482 7 12 -12 -2 806.752 174.447 6 12 -12 -1 9034.78 552.969 6 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460.363 4 12 -14 -9 3953.22 526.159 11 12 -14 -9 3855.15 357.121 6 -12 14 9 3953.97 355.339 5 12 -14 -8 2999.66 434.478 4 12 -14 -8 2915.32 453.614 11 12 -14 -8 3510.83 356.458 6 -12 14 8 3773.10 369.397 5 12 -14 -7 3607.00 470.374 4 12 -14 -7 2863.43 442.151 11 12 -14 -7 3807.64 383.787 6 -12 14 7 4042.83 398.654 5 12 -14 -6 10005.6 627.224 6 -12 14 6 10473.2 658.721 5 12 -14 -5 3558.97 373.411 6 -12 14 5 3558.40 390.736 5 -12 14 4 1146.15 228.241 5 -12 14 4 1056.04 217.659 7 12 -14 -4 1208.22 215.076 6 -12 14 3 221.191 79.8053 5 12 -14 -3 289.577 96.6309 6 -12 14 3 283.924 126.058 7 12 -14 -2 12082.6 627.966 6 -12 14 2 11856.0 733.335 5 -12 14 2 12041.3 754.229 7 12 -14 -1 9634.59 519.674 6 -12 14 1 8691.84 634.697 7 -12 14 0 3914.38 418.483 7 -12 14 -1 298.630 110.920 7 -12 14 -2 3187.21 344.548 7 -12 14 -3 54.2551 48.6991 7 12 -15 -13 2491.60 324.565 11 12 -15 -13 2199.89 281.634 4 12 -15 -12 738.652 181.367 4 12 -15 -12 1379.20 268.689 11 12 -15 -11 1486.11 175.796 6 12 -15 -11 1316.18 252.334 4 12 -15 -10 3583.48 436.634 4 12 -15 -10 3730.14 309.272 6 12 -15 -9 1346.27 203.393 6 12 -15 -9 1543.76 290.792 4 12 -15 -8 2162.10 355.414 4 12 -15 -8 1627.27 325.037 11 12 -15 -8 2179.39 265.043 6 12 -15 -7 2778.42 408.384 4 12 -15 -7 1937.25 372.022 11 12 -15 -7 2788.65 311.725 6 -12 15 6 341.884 112.951 5 12 -15 -6 376.279 113.399 6 12 -15 -5 2335.48 286.534 6 -12 15 5 2464.01 301.894 5 12 -15 -4 9453.02 574.390 6 -12 15 4 9721.83 617.887 5 -12 15 4 9015.34 615.779 7 12 -15 -3 4115.73 361.180 6 -12 15 3 3825.49 393.362 5 -12 15 3 3643.06 392.529 7 12 -15 -2 1520.78 211.822 6 -12 15 2 1412.14 245.285 7 12 -15 -1 589.676 121.350 6 -12 15 1 543.602 146.732 7 -12 15 0 1820.53 267.708 7 -12 15 -1 2073.17 274.851 7 -12 15 -2 481.821 121.610 7 12 -16 -12 4123.32 425.779 11 12 -16 -12 2924.57 333.588 4 12 -16 -11 3098.17 367.473 4 12 -16 -11 3338.70 234.741 6 12 -16 -11 3500.26 416.179 11 12 -16 -10 466.842 97.8792 6 12 -16 -10 395.226 140.363 4 12 -16 -10 61.6098 83.6244 11 12 -16 -9 339.703 95.7178 6 12 -16 -9 277.491 112.377 4 12 -16 -9 535.765 188.529 11 12 -16 -8 1066.52 174.571 6 12 -16 -8 1129.03 254.826 4 12 -16 -8 1178.34 274.334 11 12 -16 -7 4245.48 513.820 11 12 -16 -7 5125.21 398.318 6 12 -16 -7 4866.45 511.143 4 12 -16 -6 3500.73 336.379 6 12 -16 -5 6092.54 441.494 6 12 -16 -4 350.483 102.655 6 -12 16 4 320.568 116.745 7 12 -16 -3 626.819 136.410 6 -12 16 3 322.653 119.267 7 12 -16 -2 10651.2 527.538 6 -12 16 2 10917.8 648.910 7 12 -16 -1 1249.43 167.948 6 -12 16 1 1159.51 210.209 7 -12 16 0 980.693 182.136 7 -12 16 -1 82.3031 56.6969 7 12 -17 -11 2476.38 326.552 11 12 -17 -10 415.210 83.4775 6 12 -17 -10 577.570 156.906 4 12 -17 -10 559.614 149.767 11 12 -17 -9-20.2640 52.0778 4 12 -17 -9-82.8056 35.7438 11 12 -17 -8 844.431 145.314 6 12 -17 -8 812.882 193.634 4 12 -17 -8 1042.30 248.217 11 12 -17 -7 652.649 135.631 6 12 -17 -7 497.262 149.992 4 12 -17 -7 913.559 226.692 11 12 -17 -6 98.6198 50.9795 6 12 -17 -5 464.583 114.196 6 -12 17 5 160.404 53.2114 7 12 -17 -4 1491.51 202.677 6 -12 17 4 1379.02 216.999 7 12 -17 -3 1953.37 223.959 6 -12 17 3 1856.92 253.660 7 12 -17 -2 3102.27 265.803 6 -12 17 2 2796.21 308.291 7 12 -17 -1 282.269 72.9796 6 -12 17 1 249.218 95.0335 7 -12 17 0 667.071 141.944 7 12 -18 -9 300.766 71.9556 6 12 -18 -8 254.952 72.0066 6 12 -18 -8 224.317 97.9503 4 12 -18 -8 354.607 119.787 11 12 -18 -7 769.437 133.693 6 12 -18 -6 2987.62 266.647 6 12 -18 -5 1442.53 187.238 6 -12 18 4 1981.99 236.395 7 12 -18 -4 2152.97 224.456 6 -12 18 3 72.5147 36.4223 7 12 -18 -3 87.2887 30.1458 6 -12 18 2 2333.24 255.844 7 12 -18 -2 2330.98 205.938 6 -12 18 1 56.0999 46.7650 7 12 -19 -8 208.915 58.8906 6 12 -19 -7 66.9479 30.5041 6 12 -19 -6 70.3225 41.8494 6 12 -19 -5 52.7290 33.0723 6 12 -19 -4 1568.68 173.359 6 12 -19 -3 318.505 73.7250 6 -13 0 17 43.8702 28.4500 5 -13 0 16 3873.63 333.668 5 13 0 -16 2897.62 298.992 11 -13 0 16 3560.26 304.550 8 13 0 -16 3109.01 298.985 4 -13 0 15 26.5151 16.4115 5 -13 0 15 20.3829 26.7376 8 13 0 -15-19.4825 21.8124 4 -13 0 14 1084.43 206.696 8 -13 0 14 1079.24 209.042 5 13 0 -14 839.842 163.322 6 -13 0 13 194.334 92.7721 8 -13 0 13 86.2943 72.6776 5 13 0 -13 218.394 108.158 6 -13 0 12 3434.72 416.435 5 13 0 -12 3462.15 414.266 6 -13 0 12 3405.33 409.212 8 -13 0 11 0.78244 46.7686 8 -13 0 11-51.6780 52.7491 5 13 0 -11 64.4432 66.4703 6 -13 0 10 219.975 106.191 8 -13 0 10 284.704 123.015 5 13 0 -10 254.494 123.636 6 -13 0 9 174.748 99.0686 8 -13 0 9 21.5862 31.0520 5 13 0 -9 130.729 84.1606 6 -13 0 8 1997.12 326.094 5 13 0 -8 2231.20 371.638 6 -13 0 8 1953.51 331.405 8 -13 0 7 836.177 253.442 8 -13 0 7 303.177 147.592 5 13 0 -7 548.562 209.659 6 -13 0 6 1903.17 322.782 5 13 0 -6 1685.14 327.952 6 -13 0 6 2448.81 393.591 8 -13 0 5 9.47298 68.6812 5 13 0 -5-133.357 83.5553 6 -13 0 5-14.3008 57.6216 8 -13 0 4 1623.85 293.678 5 13 0 -4 1866.10 325.151 6 -13 0 4 1885.09 368.517 8 -13 0 3 45.8189 46.8475 5 -13 0 3 199.590 143.706 8 13 0 -3 140.418 102.564 6 13 0 -2 5457.39 501.951 6 -13 0 2 5573.86 539.018 5 -13 0 2 4765.67 558.215 8 -13 0 1 237.727 140.550 8 -13 0 1 33.8060 38.8009 5 -13 0 0 9331.40 767.041 8 -13 0 0 9254.29 670.458 5 -13 0 -1 8.84515 17.7891 8 -13 0 -2 726.499 207.227 8 -13 0 -3 47.5488 56.1179 8 -13 0 -4 4076.54 404.667 8 -13 1 17 54.1152 34.7379 5 13 -1 -16 214.151 73.8804 11 -13 1 16 329.866 98.4001 5 -13 -1 16 310.543 98.2183 5 -13 -1 16 159.551 61.0116 8 -13 1 16 218.166 72.8013 8 13 -1 -16 254.169 80.4682 4 -13 1 15 2121.11 274.222 5 -13 -1 15 1968.68 262.493 5 13 -1 -15 1632.40 254.807 11 -13 -1 15 1981.96 253.197 8 -13 1 15 1903.80 250.273 8 13 -1 -15 1601.61 234.496 4 13 -1 -14 170.553 62.7429 6 13 1 -14 277.678 100.960 6 13 -1 -14 76.8543 41.2423 11 -13 1 14 242.160 90.8488 5 -13 -1 14 291.745 114.277 5 13 -1 -14 329.409 116.369 4 -13 -1 14 201.481 84.5161 8 13 1 -13 7232.30 548.428 6 13 -1 -13 7246.44 536.104 6 -13 1 13 7493.31 586.569 5 -13 -1 13 7650.27 589.264 5 -13 -1 13 7056.69 556.717 8 13 -1 -12 29.2506 43.9504 6 13 1 -12 48.0214 61.7109 6 -13 -1 12 88.3017 71.6106 8 -13 1 12 202.906 104.974 8 -13 1 12-0.94518 29.8083 5 -13 -1 12-21.5085 40.7042 5 13 -1 -11 2208.15 345.385 6 13 1 -11 2341.51 361.427 6 -13 -1 11 2712.54 373.935 8 -13 1 11 2695.97 371.541 8 -13 1 11 2371.43 357.386 5 -13 -1 11 2416.15 357.093 5 13 -1 -10 3179.64 431.720 6 13 1 -10 3114.03 432.271 6 -13 -1 10 3189.31 414.204 8 -13 1 10 3135.03 413.796 8 -13 1 10 3090.17 408.638 5 -13 -1 10 3053.93 397.168 5 13 -1 -9 8838.55 719.846 6 13 1 -9 9320.48 748.981 6 -13 1 9 8733.00 688.270 5 -13 -1 9 8729.85 684.091 5 -13 -1 9 9858.38 743.259 8 -13 1 9 8955.85 703.637 8 13 -1 -8 143.078 105.522 6 13 1 -8 218.571 119.782 6 -13 -1 8 164.245 105.810 8 -13 1 8 140.837 100.019 8 -13 1 8 256.275 128.449 5 -13 -1 8 132.138 68.9380 5 13 -1 -7 44921.3 1645.23 6 13 1 -7 46833.3 1684.69 6 -13 -1 7 46236.7 1687.97 8 -13 1 7 43325.5 1634.33 8 -13 1 7 45635.1 1596.74 5 -13 -1 7 44077.5 1535.42 5 -13 1 6 3.81330 32.8852 5 -13 -1 6-54.5412 51.5325 5 -13 -1 6 127.413 125.609 8 -13 1 6 117.997 91.7569 8 13 -1 -6 210.479 129.122 6 13 1 -6 129.864 101.299 6 -13 -1 5-72.2798 39.5470 5 -13 1 5 67.9295 76.5489 5 13 -1 -5 32.5757 75.5631 6 13 1 -5 78.6004 78.7618 6 -13 -1 5 39.2381 35.9347 8 -13 1 5 12.1032 53.4651 8 13 -1 -4 2985.11 415.894 6 13 1 -4 3113.58 417.415 6 -13 1 4 3416.76 469.003 8 -13 -1 4 3408.88 471.861 8 -13 -1 4 3438.19 427.931 5 -13 1 4 3141.70 417.966 5 13 1 -3 2353.76 348.462 6 13 -1 -3 2025.74 322.345 6 -13 -1 3 2232.82 387.131 8 -13 1 3 1989.08 355.749 8 -13 -1 3 2000.76 317.349 5 -13 1 3 2169.21 345.781 5 -13 -1 2 203.316 117.391 5 -13 1 2 208.388 116.524 5 -13 -1 2 290.040 145.397 8 -13 1 2 234.983 123.415 8 13 -1 -2 189.967 107.914 6 13 1 -2 252.326 106.911 6 -13 -1 1 19991.9 1138.12 8 -13 1 1 19669.7 1108.95 8 -13 -1 1 20790.9 1000.71 5 -13 1 1 20588.5 1036.36 5 -13 -1 0 576.659 210.463 8 -13 1 0 211.007 115.616 8 -13 -1 0 205.212 116.082 5 -13 1 0 178.943 107.722 5 -13 -1 -1 482.862 177.413 8 -13 1 -1 202.914 117.968 8 -13 1 -2 23.6208 41.1918 8 -13 -1 -2 234.549 121.170 8 -13 1 -3 1975.48 300.824 8 -13 -1 -3 1965.04 306.712 8 -13 1 -4 660.961 154.364 8 -13 -1 -4 497.196 133.415 8 -13 1 -4 495.650 145.599 7 13 -2 -16 311.151 98.9491 11 -13 -2 16 291.227 82.7125 8 -13 2 16 264.825 86.2491 8 -13 2 16 205.353 79.9627 5 -13 -2 16 171.071 71.1944 5 13 -2 -15 64.0766 54.2481 11 -13 2 15 99.4640 52.5862 5 -13 -2 15 65.3032 50.2182 5 -13 -2 15 50.9945 35.5590 8 13 -2 -15 56.2737 29.3081 4 13 -2 -14 494.819 121.441 6 13 2 -14 322.741 98.1207 6 13 -2 -14 674.312 169.738 11 -13 2 14 459.559 128.572 5 -13 -2 14 380.554 126.399 5 13 -2 -14 419.240 120.343 4 -13 -2 14 544.402 141.635 8 13 -2 -13 91.9666 69.1378 6 13 2 -13 13.7873 50.1063 6 -13 -2 13 28.8958 12.8049 8 -13 2 13 74.7067 77.7366 5 -13 -2 13 40.1970 38.4609 5 13 2 -12 2235.62 332.007 6 13 -2 -12 2523.00 344.007 6 -13 -2 12 2803.57 366.910 8 -13 2 12 2691.87 368.637 5 -13 -2 12 2646.41 355.660 5 13 -2 -11 4254.89 471.502 6 13 2 -11 4048.75 471.157 6 -13 2 11 3988.30 460.901 5 -13 -2 11 4133.61 456.434 5 -13 -2 11 3801.37 442.109 8 -13 2 11 4047.39 457.835 8 13 -2 -10 574.298 180.651 6 -13 -2 10 431.862 148.514 8 -13 2 10 565.941 173.301 8 -13 2 10 820.212 209.948 5 -13 -2 10 598.450 179.841 5 13 -2 -9 229.139 118.571 6 -13 -2 9 111.732 83.9305 8 -13 2 9 109.096 101.749 8 -13 2 9 19.7506 80.3920 5 -13 -2 9 159.376 85.0218 5 13 -2 -8 2243.07 366.895 6 -13 2 8 2471.62 370.416 5 -13 -2 8 2095.33 330.198 5 -13 2 8 1809.94 327.527 8 -13 -2 8 1819.81 326.787 8 -13 -2 7-1.89366 34.9406 8 -13 2 7 54.9099 20.5503 8 -13 2 7 0.21376 35.0696 5 -13 -2 6 21691.2 1082.42 5 -13 2 6 21584.7 1129.74 5 -13 -2 6 20627.0 1139.48 8 -13 2 6 21016.9 1141.16 8 13 -2 -6 20733.7 1105.84 6 13 -2 -5 3535.39 450.156 6 13 2 -5 3619.34 455.103 6 -13 -2 5 3436.21 463.054 8 -13 -2 5 4175.69 467.185 5 -13 2 5 3684.19 465.610 5 -13 2 5 3316.14 453.030 8 13 -2 -4 2037.52 338.521 6 13 2 -4 1926.21 321.721 6 -13 -2 4 2353.04 340.955 5 -13 2 4 2132.09 341.287 5 -13 2 4 2232.33 368.614 8 -13 -2 4 1950.62 367.340 8 -13 -2 3 172.781 96.6404 5 -13 2 3 126.774 100.365 5 13 -2 -3 193.993 94.7441 6 13 2 -3 113.691 83.7820 6 -13 -2 3 201.059 118.298 8 -13 2 3 126.357 65.8512 8 13 -2 -2 9735.04 655.552 6 -13 2 2 9691.39 779.154 8 -13 -2 2 9489.20 799.380 8 -13 -2 2 10546.8 708.947 5 -13 2 2 9905.59 737.988 5 -13 -2 1 578.034 168.240 5 -13 2 1 328.059 124.746 5 -13 -2 1 345.992 151.663 8 -13 2 1 173.667 108.082 8 -13 -2 0 31533.2 1426.65 8 -13 2 0 31162.7 1363.38 8 -13 2 0 31085.6 1264.73 5 -13 -2 -1 98.6032 88.0318 8 -13 2 -1 157.977 102.610 8 -13 2 -2 48.5078 41.4859 8 -13 -2 -2 83.7245 66.3278 8 -13 2 -3-34.6885 46.0439 8 -13 -2 -3-11.1756 28.1240 8 -13 2 -3 90.1324 46.3726 7 -13 2 -4 9015.10 585.541 7 -13 2 -4 8094.58 528.897 8 -13 -2 -4 9427.81 637.140 8 -13 -2 -5 66.8136 59.1331 8 13 -3 -16 67.0292 6.45189 11 -13 3 16 222.440 80.2158 8 13 -3 -16 98.7440 63.5231 4 -13 3 16 168.325 70.3779 5 -13 -3 16 142.221 60.9640 5 13 -3 -15 285.829 115.228 11 -13 3 15 375.382 107.653 5 -13 -3 15 314.512 101.289 5 -13 -3 15 411.461 109.108 8 13 -3 -15 379.136 119.035 4 13 3 -14 421.228 115.710 6 13 -3 -14 441.882 111.787 6 13 -3 -14 359.932 128.992 11 -13 3 14 387.802 122.953 5 -13 -3 14 356.576 114.326 5 -13 -3 14 396.873 107.934 8 13 -3 -14 447.126 139.344 4 13 -3 -13 636.703 152.572 6 13 3 -13 532.444 147.533 6 13 -3 -13 759.831 206.221 11 -13 3 13 747.773 179.206 5 -13 -3 13 837.522 184.820 5 13 -3 -13 538.640 139.181 4 -13 -3 13 781.982 179.767 8 13 -3 -12 1214.08 229.138 6 13 3 -12 1235.52 245.829 6 -13 -3 12 1580.99 272.080 5 -13 -3 12 1252.79 237.588 8 -13 3 12 1286.71 252.886 5 13 -3 -11 803.536 211.602 6 -13 -3 11 643.954 173.687 8 -13 3 11 828.701 207.694 8 -13 3 11 854.889 214.962 5 -13 -3 11 603.373 159.461 5 13 -3 -10 1203.09 259.906 6 -13 -3 10 1134.96 244.640 8 -13 3 10 1198.74 251.640 8 -13 3 10 937.706 229.693 5 -13 -3 10 1100.95 234.356 5 13 -3 -9 322.504 152.839 6 -13 -3 9 343.173 140.015 8 -13 3 9 426.801 163.403 8 -13 3 9 302.001 129.925 5 -13 -3 9 364.320 138.804 5 13 -3 -8 2137.60 359.322 6 -13 3 8 1917.38 320.719 8 -13 -3 8 1733.15 321.984 8 -13 3 8 1942.50 331.160 5 -13 -3 8 2156.32 332.676 5 13 -3 -7 7638.40 672.254 6 -13 -3 7 7927.35 698.831 8 -13 3 7 7898.37 682.453 8 -13 3 7 7682.90 661.034 5 -13 -3 7 7855.69 624.837 5 -13 -3 6 514.358 179.103 5 -13 3 6 306.203 143.543 5 13 -3 -6 398.924 167.385 6 -13 -3 6 388.055 161.886 8 -13 3 6 334.347 140.725 8 13 -3 -5 1900.64 334.015 6 -13 -3 5 2203.43 333.229 5 -13 3 5 1883.78 340.742 5 -13 -3 5 2099.62 366.363 8 -13 3 5 2012.03 350.860 8 -13 -3 4 1013.63 223.647 5 -13 3 4 840.217 222.740 5 13 -3 -4 791.656 207.625 6 13 3 -4 779.148 214.988 6 -13 -3 4 1199.81 278.531 8 -13 3 4 1000.61 244.618 8 -13 -3 3 12.2378 43.1587 5 -13 3 3 69.0296 68.5210 5 13 3 -3 154.206 108.352 6 13 -3 -3 150.253 85.8234 6 -13 -3 3 202.142 122.028 8 -13 3 3 55.6201 75.7265 8 -13 3 2 249.862 112.139 5 -13 -3 2 128.941 58.8693 8 -13 3 2 77.5859 66.1016 8 13 -3 -2 88.6272 91.0511 6 -13 -3 1 8794.76 758.187 8 -13 3 1 8230.03 696.052 8 -13 3 1 9281.43 708.442 5 -13 -3 0 187.661 132.308 8 -13 3 0 184.453 125.755 8 -13 3 0 260.216 120.155 5 -13 -3 -1 2399.76 388.204 8 -13 3 -1 2227.15 342.148 8 -13 3 -2 1057.01 222.511 8 -13 -3 -2 1172.21 259.925 8 -13 3 -2 1198.63 235.726 7 -13 3 -3 139.446 78.1282 8 -13 -3 -3 62.7348 49.5844 8 -13 3 -3 195.872 104.350 7 -13 3 -4 1901.26 264.999 7 -13 -3 -4 1835.41 282.435 8 -13 -3 -5 3425.24 333.451 8 13 -4 -16 384.672 109.384 11 -13 4 16 490.620 112.545 8 13 -4 -16 556.204 130.210 4 -13 4 16 613.279 122.928 5 -13 -4 16 685.564 127.320 5 13 -4 -15 384.585 131.475 11 -13 4 15 385.528 109.544 5 -13 -4 15 370.325 107.786 5 -13 -4 15 462.797 108.354 8 13 -4 -15 385.632 120.778 4 13 4 -14 119.783 69.1150 6 13 -4 -14-55.0013 83.3566 11 -13 4 14 185.940 82.4636 5 -13 -4 14 82.0084 54.5890 5 -13 -4 14 117.853 59.2560 8 13 -4 -14 8.97138 10.7948 4 13 -4 -13 31.3283 29.2861 6 13 4 -13 51.6317 51.9686 6 13 -4 -13-11.3869 10.2485 11 -13 4 13 82.3436 65.3117 5 -13 -4 13 70.3456 55.5592 5 13 -4 -13 1.17112 53.3042 4 -13 -4 13 18.1292 5.87593 8 13 -4 -12 210.844 85.6398 6 -13 -4 12 200.159 95.8852 8 -13 4 12 113.888 74.7990 5 -13 -4 12 201.787 94.5884 5 13 -4 -11 3665.40 417.326 6 -13 4 11 3839.94 441.687 8 -13 -4 11 3631.97 412.433 8 -13 4 11 3890.84 445.773 5 -13 -4 11 3727.82 415.821 5 -13 4 10-16.5732 64.3943 5 -13 -4 10 43.5154 20.5903 5 -13 -4 10 111.534 94.6847 8 -13 4 10 85.3948 61.2057 8 13 -4 -10 17.7633 41.5419 6 -13 4 9 109.808 74.4677 5 -13 -4 9-104.914 65.4013 5 -13 -4 9 147.504 94.7445 8 -13 4 9-38.2689 18.2429 8 13 -4 -9 128.740 75.5400 6 -13 4 8 457.761 157.362 5 -13 -4 8 247.110 99.7039 5 -13 -4 8 366.143 138.638 8 -13 4 8 421.219 152.736 8 13 -4 -8 371.218 152.460 6 -13 4 7 284.221 112.698 5 -13 -4 7 429.145 148.963 5 13 -4 -7 521.364 196.050 6 -13 -4 7 400.788 160.309 8 -13 4 7 342.518 147.079 8 13 -4 -6 20571.3 1086.03 6 -13 -4 6 21236.3 1139.03 8 -13 -4 6 24693.5 1150.55 5 -13 4 6 22084.7 1148.03 5 -13 4 6 20126.4 1100.89 8 13 -4 -5 5985.20 573.831 6 -13 -4 5 6285.67 630.982 8 -13 -4 5 6658.27 559.990 5 -13 4 5 6681.90 631.035 5 -13 4 5 6034.32 593.421 8 13 -4 -4 890.960 214.392 6 -13 4 4 740.250 211.230 8 -13 -4 4 761.218 226.348 8 -13 4 4 866.797 222.242 5 13 -4 -3 121.519 62.1202 6 13 4 -3 113.561 100.971 6 -13 4 3-80.9311 69.0581 5 -13 -4 3 49.7459 84.8059 8 -13 4 3 54.1971 78.0715 8 -13 4 2 1507.84 288.001 5 -13 -4 2 1235.19 280.577 8 -13 4 2 1451.46 291.109 8 13 -4 -2 1449.46 244.607 6 -13 -4 1 2165.09 376.601 8 -13 4 1 1976.83 329.376 8 -13 4 1 2109.27 343.843 5 -13 -4 0 33007.5 1457.38 8 -13 4 0 31959.6 1326.44 8 -13 4 0 33311.8 1320.80 5 -13 4 -1 2030.03 324.267 8 -13 -4 -1 2247.77 377.063 8 -13 4 -2 1262.73 231.626 8 -13 -4 -2 1412.70 281.309 8 -13 4 -2 1361.47 255.417 7 -13 -4 -3 3345.58 410.831 8 -13 4 -3 3498.26 386.158 7 -13 -4 -4 4288.73 428.534 8 -13 4 -4 4578.25 409.677 7 -13 5 16 885.546 148.266 8 -13 5 16 847.798 137.972 5 -13 -5 16 723.657 125.289 5 13 -5 -15 3441.67 377.998 11 -13 5 15 3634.36 332.435 5 -13 -5 15 3472.40 311.975 5 13 -5 -15 3435.85 351.741 4 13 -5 -14 1856.93 277.457 4 13 -5 -14 1745.88 282.428 11 -13 5 14 2052.49 274.040 5 -13 -5 14 1933.85 256.422 5 -13 -5 14 2131.01 261.760 8 13 5 -14 1528.99 223.235 6 13 -5 -13 2983.79 364.879 4 -13 5 13 2846.68 344.160 5 -13 -5 13 2606.69 313.903 5 13 -5 -13 1733.58 304.605 11 -13 -5 13 2735.62 320.403 8 13 5 -13 2898.14 345.274 6 13 -5 -13 2946.49 313.785 6 13 -5 -12 1628.99 251.245 6 -13 5 12 1704.11 281.153 5 -13 -5 12 1777.66 270.065 5 -13 -5 12 1706.42 268.019 8 13 -5 -11 250.893 113.228 6 -13 -5 11 253.715 99.2453 8 -13 5 11 256.916 116.138 8 -13 5 11 231.835 106.737 5 -13 -5 11 239.704 102.491 5 13 -5 -10 369.886 137.317 6 -13 -5 10 377.802 152.742 8 -13 5 10 401.326 151.123 8 -13 5 10 294.295 134.205 5 -13 -5 10 207.217 102.685 5 13 -5 -9 5785.20 558.004 6 -13 5 9 5485.63 538.600 8 -13 -5 9 5090.83 534.204 8 -13 5 9 5659.57 558.346 5 -13 -5 9 5420.42 493.553 5 13 -5 -8 2228.88 354.087 6 -13 5 8 1926.22 322.898 8 -13 -5 8 2000.61 334.675 8 -13 5 8 2126.44 347.482 5 -13 -5 8 2013.69 301.034 5 13 -5 -7 11632.1 804.613 6 -13 5 7 10777.2 778.386 5 -13 -5 7 12136.2 736.525 5 -13 -5 7 11069.8 800.777 8 -13 5 7 10855.8 778.509 8 -13 5 6 1712.88 330.688 5 -13 -5 6 1716.78 324.391 8 -13 5 6 1506.59 288.453 8 13 -5 -6 1485.32 288.571 6 -13 5 5 141.576 104.218 5 13 -5 -5 303.718 142.338 6 -13 5 5 78.1318 77.5343 8 -13 -5 5 208.708 122.766 8 13 -5 -4 5015.74 505.501 6 -13 -5 4 4948.23 567.952 8 -13 5 4 5401.82 557.826 8 -13 5 4 4779.33 530.856 5 -13 5 3-38.8159 47.4379 5 13 5 -3-50.1533 68.1016 6 13 -5 -3 111.581 91.6956 6 -13 -5 3 151.162 101.378 8 -13 5 3 42.7432 78.9868 8 -13 5 2 1155.43 253.564 5 -13 -5 2 799.631 231.138 8 -13 5 2 899.251 222.447 8 13 -5 -2 1091.49 208.975 6 -13 -5 1 6501.46 662.281 8 -13 5 1 5880.18 555.532 8 -13 5 1 6516.70 596.458 5 -13 -5 0 519.803 212.919 8 -13 5 0 139.414 103.807 8 -13 5 0 324.356 131.437 5 -13 5 -1 1023.64 216.275 8 -13 -5 -1 1185.21 268.543 8 -13 5 -1 959.065 212.521 7 -13 -5 -2 1490.97 289.328 8 -13 5 -2 1299.99 248.973 7 -13 -5 -3 1393.84 261.095 8 -13 5 -3 951.675 197.216 7 -13 -5 -4 4253.35 419.911 8 -13 5 -4 3692.75 363.826 7 -13 6 16 1885.43 207.314 8 -13 6 16 1737.21 189.060 5 13 -6 -15 1010.25 208.154 11 -13 -6 15 890.501 147.714 5 -13 6 15 1104.82 177.042 5 13 -6 -15 1066.93 197.597 4 13 -6 -14 160.661 105.981 11 -13 6 14 323.061 108.590 5 -13 -6 14 169.185 71.9204 5 13 6 -14 135.935 59.8708 6 13 -6 -14 189.816 84.0358 4 13 -6 -13 2286.93 313.620 4 13 -6 -13 2688.71 374.596 11 -13 6 13 2668.03 324.579 5 -13 -6 13 2392.05 288.729 5 -13 -6 13 2850.21 319.937 8 13 -6 -13 2501.07 272.301 6 13 -6 -12 2620.07 350.755 4 -13 6 12 2846.75 359.753 5 -13 -6 12 2683.28 322.450 5 13 -6 -12 2946.05 399.701 11 -13 -6 12 3130.19 357.305 8 13 -6 -12 2963.19 337.101 6 13 -6 -11 2002.42 294.267 6 -13 6 11 1923.62 303.409 8 -13 -6 11 2246.70 318.215 8 -13 6 11 1906.80 307.802 5 -13 -6 11 1813.63 267.202 5 13 -6 -10 2502.92 347.155 6 -13 6 10 2304.61 341.109 8 -13 -6 10 2771.51 369.771 8 -13 6 10 2759.48 380.838 5 -13 -6 10 2543.21 321.524 5 -13 6 9 1234.43 255.236 5 -13 -6 9 1295.11 231.430 5 -13 -6 9 1030.83 229.005 8 -13 6 9 1210.82 242.708 8 13 -6 -9 1246.97 245.898 6 -13 6 8 915.878 220.113 5 13 -6 -8 808.617 207.884 6 -13 -6 8 871.923 224.942 8 -13 6 8 706.365 195.064 8 13 -6 -7 3785.50 454.616 6 -13 -6 7 4342.50 502.689 8 -13 6 7 4601.19 519.732 5 -13 6 7 4183.16 482.557 8 13 -6 -6 15877.9 920.796 6 -13 -6 6 15950.5 977.803 8 -13 6 6 16741.9 991.389 5 -13 6 6 15836.5 935.665 8 13 -6 -5 16120.8 915.435 6 -13 -6 5 17645.7 1043.95 8 -13 6 5 17290.6 969.501 8 -13 6 5 17083.7 990.062 5 -13 6 4 3.24830 20.5120 5 13 -6 -4 39.0357 15.8757 6 -13 -6 4 64.6431 70.8955 8 -13 6 4 144.309 110.719 8 -13 6 3 821.969 221.894 5 13 -6 -3 1004.12 212.642 6 -13 -6 3 647.473 201.746 8 -13 6 3 698.722 199.739 8 -13 6 2 109.409 97.7496 5 -13 -6 2 333.248 137.287 8 -13 6 2 144.785 83.5814 8 13 -6 -2 232.349 114.051 6 -13 -6 1 3080.92 448.999 8 -13 6 1 3157.24 400.316 8 -13 6 1 2545.35 371.202 5 -13 -6 0 7049.13 663.649 8 -13 6 0 7202.58 578.177 8 -13 6 0 7696.15 631.928 5 -13 6 -1 3147.17 385.658 7 -13 -6 -1 3200.71 429.201 8 -13 -6 -2 142.846 84.0895 8 -13 6 -2-21.0757 20.1814 7 -13 6 -3 2008.79 283.448 7 -13 -6 -3 2199.88 320.907 8 -13 -6 -4 334.183 115.992 8 -13 6 -4 282.338 99.3680 7 -13 7 16 1012.24 142.630 8 13 -7 -15 9407.71 615.940 11 13 -7 -15 8252.92 532.059 4 -13 7 15 9853.43 516.115 8 -13 7 15 9833.58 499.281 5 13 -7 -14 1224.17 235.628 11 -13 7 14 1114.27 188.424 5 13 7 -14 986.858 171.932 6 -13 -7 14 988.003 160.332 5 13 -7 -14 1164.01 219.576 4 13 -7 -13 1002.65 221.033 11 -13 7 13 647.494 157.977 5 -13 -7 13 474.995 118.610 5 13 -7 -13 614.973 133.580 6 13 -7 -13 581.271 163.059 4 13 -7 -12 658.055 149.177 6 13 -7 -12 504.364 156.249 11 -13 7 12 719.749 178.997 5 -13 -7 12 666.025 147.663 5 13 -7 -12 707.403 188.696 4 -13 -7 12 727.144 166.696 8 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13604.1 732.882 6 -13 -7 2 14363.9 942.230 8 -13 7 2 12513.9 778.430 8 -13 7 2 13837.2 871.019 5 -13 -7 1 292.123 148.979 8 -13 7 1 582.440 178.548 5 -13 7 0 627.925 177.673 7 -13 -7 0 477.693 162.285 8 -13 7 0 583.006 175.636 5 -13 -7 -1 1050.60 241.886 8 -13 7 -1 860.347 197.862 7 -13 -7 -2 2160.48 338.292 8 -13 7 -2 1838.72 280.962 7 -13 -7 -3 1625.77 277.040 8 -13 7 -3 1428.09 234.136 7 -13 -7 -4 4956.35 428.168 8 -13 7 -4 4564.19 381.066 7 13 -8 -15 1122.04 197.632 4 -13 8 15 1241.70 164.837 5 -13 8 15 1430.81 189.428 8 13 -8 -15 1635.36 252.812 11 -13 8 14 1404.52 201.537 5 13 8 -14 991.006 164.026 6 13 -8 -14 1468.13 262.245 11 13 -8 -14 1395.99 236.168 4 -13 8 14 1414.00 204.025 8 13 -8 -13 411.820 98.3715 6 13 -8 -13 450.140 157.060 11 -13 8 13 425.383 117.690 5 13 -8 -13 521.234 162.443 4 -13 8 13 484.956 122.426 8 13 -8 -12 849.358 163.379 6 13 -8 -12 1057.88 243.770 11 -13 8 12 885.748 187.883 5 13 -8 -12 600.995 173.623 4 -13 8 12 982.406 192.925 8 -13 8 11 2071.87 303.312 5 -13 -8 11 2181.70 286.486 8 13 -8 -11 1768.57 265.133 6 13 -8 -11 1546.05 284.933 4 -13 8 11 2065.42 292.892 8 13 -8 -10 12179.8 722.217 6 -13 8 10 12686.7 746.389 8 -13 8 10 11915.4 747.153 5 -13 -8 10 14090.0 776.828 8 13 -8 -9 10323.1 698.468 6 -13 8 9 9248.33 645.105 8 -13 8 9 10855.8 734.118 5 -13 -8 9 9171.11 652.826 8 -13 8 8 927.997 221.511 5 13 -8 -8 1052.98 235.655 6 -13 8 8 1080.11 226.408 8 -13 -8 8 1004.75 220.476 8 13 -8 -7 4379.50 470.491 6 -13 8 7 4884.31 490.843 8 -13 8 7 4084.82 478.154 5 -13 -8 7 4515.24 491.560 8 13 -8 -6 1553.13 283.486 6 -13 8 6 1805.47 301.951 8 -13 -8 6 1721.35 312.989 8 -13 8 6 1796.03 326.836 5 13 -8 -5 14885.0 843.095 6 -13 8 5 16443.9 889.244 8 -13 -8 5 16859.9 993.630 8 -13 8 5 14776.8 904.792 5 13 -8 -4 3969.45 426.819 6 -13 8 4 3498.36 404.662 8 -13 -8 4 3266.96 433.941 8 -13 8 4 3763.11 457.183 5 13 -8 -3 5600.93 487.361 6 -13 -8 3 4514.24 519.495 8 -13 8 3 5272.48 537.025 5 13 -8 -2 1824.74 259.614 6 -13 -8 2 1659.23 328.235 8 -13 8 2 2071.86 333.042 5 -13 -8 1 2439.14 384.434 8 -13 8 1 2345.65 355.645 5 -13 8 0 1173.28 227.495 7 -13 -8 0 1336.85 281.067 8 -13 8 0 1296.23 258.389 5 -13 8 -1 2060.50 297.857 7 -13 -8 -1 2192.12 346.729 8 -13 8 -2 452.169 131.554 7 -13 -8 -2 321.134 126.294 8 -13 8 -3 732.981 163.934 7 -13 -8 -3 670.494 171.237 8 -13 -8 -4 536.712 134.162 8 -13 9 15 9245.98 441.492 8 13 -9 -14 4738.94 461.084 11 -13 9 14 7230.06 425.175 5 13 -9 -14 6169.09 479.099 4 13 9 -14 5167.04 362.707 6 -13 9 14 6541.88 417.575 8 13 -9 -13 696.376 124.419 6 13 -9 -13 1006.14 228.873 11 -13 9 13 993.759 173.425 5 13 -9 -13 894.237 194.282 4 -13 9 13 969.158 178.473 8 13 -9 -12 615.515 130.364 6 13 -9 -12 446.681 151.183 11 -13 9 12 798.597 165.990 5 -13 9 12 668.984 154.187 8 13 -9 -12 755.153 182.786 4 -13 9 11 2181.24 297.739 5 -13 9 11 2419.61 303.945 8 13 -9 -11 1812.55 301.459 4 13 -9 -11 2356.87 373.283 11 13 -9 -11 1952.86 266.048 6 -13 9 10 2595.89 341.870 5 -13 9 10 2174.08 293.150 8 13 -9 -10 2795.47 334.432 6 13 -9 -9 1237.94 244.308 6 -13 9 9 1583.42 259.170 8 -13 9 9 1552.83 279.830 5 -13 -9 9 1531.02 259.471 8 13 -9 -8 6802.52 564.750 6 -13 9 8 7875.35 595.841 8 -13 9 8 8821.12 707.649 5 -13 -9 8 7260.99 581.427 8 -13 9 7 350.288 145.912 5 13 -9 -7 193.418 114.659 6 -13 9 7 387.612 139.716 8 -13 -9 7 260.864 111.510 8 13 -9 -6 6086.91 534.148 6 -13 9 6 6264.56 581.651 5 -13 9 6 5745.63 502.929 8 -13 -9 6 5771.58 553.277 8 -13 9 5 265.992 124.884 5 -13 -9 5 424.951 150.818 8 -13 9 5 366.785 134.238 8 13 -9 -5 336.230 131.500 6 -13 9 4 369.512 140.490 5 -13 -9 4 477.010 169.502 8 13 -9 -4 403.230 130.609 6 -13 9 3 161.429 83.7664 5 -13 -9 3 119.620 67.2920 8 13 -9 -3 209.757 107.491 6 13 -9 -2 3170.52 333.465 6 -13 -9 2 3264.28 439.534 8 -13 9 2 3272.99 410.508 5 -13 -9 1 8770.37 703.754 8 -13 9 1 8541.44 619.147 7 -13 9 1 9337.53 687.373 5 -13 9 0 182.987 101.006 7 -13 -9 0 180.459 119.546 8 -13 9 -1 73.1972 29.2839 7 -13 -9 -1 153.982 68.1258 8 -13 9 -2 1149.33 212.447 7 -13 -9 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699.354 8 -13 10 7 9753.31 691.801 5 -13 10 6 1175.08 245.456 5 13 -10 -6 1168.05 229.329 6 -13 -10 6 930.601 206.159 8 13 -10 -5 2637.48 336.645 6 -13 10 5 2778.09 376.629 5 -13 -10 5 3351.71 410.415 8 -13 10 4 1122.05 239.969 5 13 -10 -4 1200.30 223.716 6 -13 -10 4 1239.92 256.233 8 13 -10 -3 11684.1 658.578 6 -13 -10 3 10682.6 768.041 8 -13 10 3 11219.7 749.992 5 13 -10 -2 176.811 82.8249 6 -13 10 2 166.363 96.4193 5 -13 -10 2 306.595 146.677 8 -13 10 1 744.669 194.807 5 -13 -10 1 526.239 160.702 8 -13 10 1 563.584 147.571 7 -13 -10 0 1039.94 232.852 8 -13 10 0 817.712 190.345 7 -13 -10 -1 608.451 167.638 8 -13 10 -1 472.833 132.460 7 -13 -10 -2 209.944 97.6145 8 -13 10 -2 194.847 80.7125 7 -13 -10 -3 667.887 144.803 8 -13 10 -3 980.384 171.179 7 -13 11 13 1081.33 157.348 5 13 -11 -13 865.813 192.068 11 -13 11 13 1056.84 157.145 8 13 -11 -13 1011.88 192.645 4 13 -11 -12 125.256 75.5950 4 13 -11 -12 296.561 129.914 11 -13 11 12 251.929 87.5710 5 13 -11 -12 1.79352 16.4957 6 -13 11 12 35.5110 26.5470 8 -13 11 11 2141.94 268.403 5 13 -11 -11 1554.25 292.526 11 13 -11 -11 1979.39 303.982 4 13 -11 -11 1919.56 235.630 6 -13 11 11 1803.14 226.304 8 -13 11 10 1878.10 246.239 8 13 -11 -10 2293.39 274.119 6 -13 11 10 2572.03 315.291 5 13 -11 -9 1294.19 225.980 6 -13 11 9 1195.18 227.995 5 13 -11 -8 7935.60 566.794 6 -13 11 8 7914.60 585.617 5 -13 11 7 62.4593 79.4737 5 13 -11 -7 113.255 74.7137 6 -13 11 6-31.8709 61.1404 5 13 -11 -6 39.1184 45.7125 6 -13 -11 6-46.0528 67.4619 8 13 -11 -5 4184.56 409.608 6 -13 11 5 4508.04 467.501 5 -13 -11 5 4304.40 447.139 8 13 -11 -4 653.102 154.321 6 -13 11 4 442.787 141.081 5 -13 -11 4 456.270 154.514 8 -13 11 3 345.696 136.361 5 13 -11 -3 197.180 85.4212 6 -13 -11 3 177.852 94.8833 8 13 -11 -2 6061.01 433.675 6 -13 -11 2 6323.03 550.806 8 -13 11 2 6367.86 557.194 5 -13 11 1 6348.52 511.245 7 -13 -11 1 5866.73 524.553 8 -13 -11 0 741.509 172.790 8 -13 11 0 717.650 166.120 7 -13 -11 -1 319.648 110.418 8 -13 11 -1 378.068 123.879 7 -13 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105.038 8 -13 12 0 518.165 135.566 7 -13 -12 0 725.549 165.150 8 -13 12 -1 60.0192 29.8642 7 -13 -12 -1 100.168 73.5863 8 13 -13 -12 213.481 71.7349 11 13 -13 -12 287.628 69.7102 6 13 -13 -12 297.245 113.635 4 13 -13 -11 317.529 121.900 11 13 -13 -11 627.717 119.092 6 13 -13 -11 496.248 144.912 4 13 -13 -10 2781.38 348.136 4 13 -13 -10 1858.68 304.844 11 -13 13 10 2798.49 275.690 5 13 -13 -10 2907.43 279.506 6 13 -13 -9 484.302 126.884 6 -13 13 9 557.139 131.519 5 -13 13 8 16635.2 760.599 5 13 -13 -8 15503.5 716.937 6 13 -13 -7 281.853 98.6186 6 -13 13 7 510.950 135.373 5 -13 13 6 1471.16 236.860 5 13 -13 -6 1407.96 224.428 6 -13 13 5 3962.66 397.082 5 13 -13 -5 3922.70 363.771 6 13 -13 -4 79.8233 35.8268 6 -13 13 4 66.4894 51.0972 5 13 -13 -3 2063.96 246.237 6 -13 13 3 1925.38 276.517 5 13 -13 -2 1913.10 218.727 6 -13 13 2 1607.49 233.894 7 -13 13 1 1190.96 199.289 7 -13 -13 0 88.1700 54.7821 8 -13 13 0-5.21491 39.8583 7 -13 13 -1 683.034 141.850 7 13 -14 -11 555.195 145.065 11 13 -14 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34.9309 52.9114 6 -14 0 4 434.555 161.136 8 -14 0 4 437.857 138.630 5 14 0 -4 341.950 123.464 6 -14 0 3 71.9659 73.8245 8 -14 0 3-26.7591 44.4518 5 14 0 -3 113.405 72.9256 6 -14 0 2 13573.3 875.225 8 -14 0 2 13866.4 779.877 5 -14 0 1-35.7625 47.2354 8 -14 0 1 219.635 83.0198 5 -14 0 0 11564.1 771.250 8 -14 0 -1 116.054 71.3586 8 -14 0 -2 70.4813 57.8751 8 -14 0 -3-17.8369 26.5284 8 -14 1 15 2311.30 246.881 8 -14 -1 15 2706.71 265.753 8 -14 1 15 2526.10 260.570 5 -14 -1 15 2133.15 236.473 5 -14 1 14 810.900 162.331 5 -14 -1 14 845.415 159.974 5 -14 -1 14 858.801 167.347 8 -14 1 14 1061.32 186.557 8 14 -1 -14 608.574 121.813 6 14 1 -14 541.595 120.938 6 -14 1 13 14565.2 737.312 8 -14 -1 13 14018.9 719.695 8 -14 1 13 14231.1 735.149 5 -14 -1 13 14084.9 712.731 5 14 -1 -13 13050.9 657.380 6 14 1 -13 13352.5 684.551 6 -14 -1 12 451.535 138.081 8 -14 1 12 492.016 139.755 8 -14 1 12 675.343 169.134 5 -14 -1 12 462.515 129.419 5 14 -1 -12 582.197 159.168 6 14 1 -12 424.036 133.670 6 -14 -1 11 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137.784 5 14 -2 -8 271.786 130.778 6 14 2 -8 259.131 129.570 6 -14 2 7 1873.54 330.329 8 -14 -2 7 2017.01 307.859 5 -14 2 7 2085.24 364.754 5 -14 -2 7 1848.64 325.970 8 14 2 -7 1823.28 328.494 6 14 -2 -7 2006.52 334.648 6 -14 -2 6 25048.9 1071.34 5 -14 2 6 24530.5 1119.10 5 -14 2 6 23177.9 1134.95 8 -14 -2 6 24290.3 1196.73 8 14 2 -6 24083.2 1120.37 6 14 -2 -6 23333.9 1093.58 6 -14 -2 5 2866.52 357.873 5 -14 2 5 2750.79 369.680 5 -14 2 5 2726.84 400.090 8 -14 -2 5 3190.37 443.418 8 14 2 -5 2627.13 364.845 6 14 -2 -5 2888.78 377.105 6 -14 -2 4 6415.54 526.911 5 -14 2 4 6164.75 556.737 5 -14 -2 4 6212.01 615.188 8 -14 2 4 6346.38 600.851 8 14 2 -4 6060.95 524.653 6 14 -2 -4 6581.90 533.396 6 -14 -2 3 267.348 122.192 8 -14 2 3 198.485 114.636 8 -14 -2 3 365.798 123.296 5 -14 2 3 305.951 125.318 5 14 -2 -3 396.532 120.488 6 14 2 -3 195.281 76.1862 6 -14 -2 2 12119.0 837.272 8 -14 2 2 12052.3 803.553 8 -14 2 2 12660.2 769.275 5 -14 -2 1 1442.91 291.827 8 -14 2 1 1144.44 242.369 8 -14 2 1 1229.16 233.158 5 -14 -2 0 9866.83 723.923 8 -14 2 0 9809.48 683.919 8 -14 2 -1-3.78524 37.4544 8 -14 -2 -1-33.4577 38.6505 8 -14 2 -2 130.294 72.8781 8 -14 -2 -2 93.7578 61.8310 8 -14 -2 -3 922.908 176.757 8 -14 3 15 34.4432 27.8751 5 -14 -3 15 72.1055 43.5555 5 -14 -3 15 52.4333 26.2243 8 -14 3 15 100.408 60.9978 8 -14 3 14 2658.17 289.579 8 -14 -3 14 2414.34 267.454 8 -14 3 14 2564.71 287.377 5 -14 -3 14 2041.67 242.617 5 14 -3 -14 1780.79 193.748 6 14 3 -14 1695.54 211.836 6 -14 3 13 8809.98 571.910 8 -14 -3 13 8939.59 568.540 8 -14 3 13 8972.48 577.586 5 -14 -3 13 8550.17 534.376 5 14 3 -13 7558.29 516.180 6 14 -3 -13 7791.51 480.166 6 -14 3 12 3221.59 360.222 8 -14 -3 12 3462.22 380.613 8 -14 3 12 3862.04 395.728 5 -14 -3 12 3797.22 374.523 5 14 3 -12 3717.26 395.188 6 14 -3 -12 3529.04 365.360 6 -14 -3 11 152.514 99.3118 8 -14 3 11 71.7705 62.0987 8 -14 3 11 228.243 107.514 5 -14 -3 11 122.222 76.2783 5 14 -3 -11 121.786 97.4590 6 14 3 -11 201.026 102.108 6 -14 -3 10 835.790 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7528.33 656.687 8 14 4 -6 7113.14 597.500 6 14 -4 -6 6849.52 575.242 6 -14 4 5 6474.31 577.874 5 -14 4 5 6213.17 573.588 8 -14 -4 5 6028.75 598.317 8 14 4 -5 5656.32 519.559 6 14 -4 -5 6315.45 532.926 6 -14 -4 4 311.088 130.070 8 -14 4 4 519.472 165.951 8 -14 4 4 568.136 173.733 5 14 4 -4 528.555 160.159 6 14 -4 -4 523.821 148.573 6 -14 -4 3 56.0494 71.1884 8 -14 4 3-2.34784 8.86015 8 -14 4 3 40.5576 40.1474 5 14 4 -3 93.3028 83.6906 6 14 -4 -3-36.8240 16.0756 6 -14 -4 2 993.903 239.951 8 -14 4 2 921.973 213.426 8 -14 4 2 1002.87 217.898 5 -14 -4 1 58.0731 57.7497 8 -14 4 1 39.9039 63.7159 8 -14 4 1 6.17442 27.5971 5 -14 4 0 13000.2 729.037 8 -14 -4 0 14192.2 855.277 8 -14 4 -1 5708.56 440.890 8 -14 -4 -1 6829.48 567.602 8 -14 -4 -2 30.5463 25.0509 8 -14 -4 -3 7358.20 493.228 8 -14 5 15 897.106 142.121 8 -14 5 15 946.941 143.584 5 -14 5 14 3293.04 308.646 8 -14 -5 14 2893.32 263.437 8 -14 5 14 3279.02 307.763 5 -14 -5 14 2921.31 264.602 5 14 5 -14 2510.95 251.379 6 -14 5 13 13637.5 680.915 8 -14 -5 13 12607.8 627.739 8 -14 5 13 12840.5 660.458 5 -14 -5 13 11563.8 569.907 5 14 5 -13 11639.4 632.513 6 14 -5 -13 11166.0 540.928 6 -14 5 12 4182.85 395.579 8 -14 -5 12 4555.11 408.919 8 -14 5 12 4770.05 426.445 5 -14 -5 12 4639.05 380.944 5 14 5 -12 4660.00 434.370 6 14 -5 -12 4504.27 388.522 6 -14 5 11 326.198 116.084 5 -14 -5 11 184.462 81.7347 5 -14 -5 11 92.3776 72.7138 8 -14 5 11 293.729 114.994 8 14 -5 -11 264.258 112.707 6 14 5 -11 335.590 131.039 6 -14 -5 10 1502.09 257.187 8 -14 5 10 1621.82 268.753 8 -14 5 10 1549.66 268.626 5 -14 -5 10 1691.15 247.283 5 14 -5 -10 1632.42 263.113 6 -14 -5 9 480.904 144.227 8 -14 5 9 419.273 135.648 8 -14 -5 9 449.133 134.727 5 -14 5 9 562.279 168.434 5 14 -5 -9 414.649 140.575 6 -14 5 8 278.165 127.820 8 -14 -5 8 147.777 102.749 8 -14 5 8 208.250 119.661 5 14 -5 -8 213.794 97.3478 6 -14 5 7 7987.22 634.121 8 -14 5 7 7672.61 628.999 5 -14 -5 7 7951.54 660.361 8 14 -5 -7 7282.27 589.613 6 -14 5 6 3163.68 400.950 5 -14 5 6 2612.12 362.489 8 -14 -5 6 2785.45 397.082 8 14 5 -6 3159.14 399.596 6 14 -5 -6 2968.62 373.742 6 -14 5 5 4893.87 499.028 5 -14 5 5 4825.25 497.934 8 -14 -5 5 4421.89 507.871 8 14 5 -5 4800.05 472.009 6 14 -5 -5 4896.44 463.590 6 -14 -5 4 330.112 149.126 8 -14 5 4 495.385 156.361 8 -14 5 4 203.591 109.257 5 14 5 -4 420.652 142.161 6 14 -5 -4 202.718 107.095 6 -14 -5 3 33.7585 20.3670 8 -14 5 3-12.3098 44.6117 8 -14 5 3 54.5486 43.8604 5 14 -5 -3 62.3272 51.2106 6 -14 -5 2 3453.54 449.165 8 -14 5 2 2884.53 364.780 8 -14 5 2 2811.71 369.215 5 -14 -5 1 5052.91 524.403 8 -14 5 1 5151.39 471.446 8 -14 5 1 6266.39 531.800 5 -14 5 0 3328.70 352.996 8 -14 -5 0 3457.49 419.377 8 -14 -5 -1 415.985 136.647 8 -14 -5 -2 1390.18 232.219 8 -14 -5 -3 219.016 75.0966 8 -14 6 15 1843.38 196.862 8 -14 6 14 6684.87 427.765 8 -14 6 14 6576.34 418.002 5 -14 6 13 341.114 105.268 8 -14 -6 13 487.460 118.176 8 -14 6 13 334.242 98.4009 5 -14 -6 13 373.984 99.6366 5 14 6 -13 406.960 124.738 6 14 -6 -13 296.896 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37.4685 8 14 6 -4 63.6738 31.9706 6 14 -6 -4 103.655 61.7513 6 -14 6 4-9.93002 21.4224 5 -14 6 3 2869.53 372.427 5 -14 -6 3 2681.59 385.842 8 -14 6 3 2222.36 312.126 8 14 -6 -3 2856.18 314.883 6 -14 -6 2 48.0344 73.2704 8 -14 6 2-37.2526 38.7249 8 -14 6 2 87.0664 72.7339 5 -14 -6 1 143.508 82.1689 8 -14 6 1 211.399 103.876 5 -14 -6 0 302.958 133.184 8 -14 -6 -1 3479.37 389.705 8 -14 -6 -2-34.6277 50.5553 8 -14 7 14 4279.14 325.432 8 -14 7 14 4484.55 337.316 5 -14 7 13 6468.94 437.179 5 14 7 -13 5706.80 419.909 6 14 -7 -13 5698.42 353.356 6 -14 7 12 7266.90 493.579 8 -14 7 12 7662.56 512.147 5 -14 -7 12 7384.13 468.787 8 14 7 -12 7193.52 524.274 6 14 -7 -12 7063.98 452.589 6 -14 7 11 298.216 111.549 8 -14 -7 11 243.635 95.3904 8 -14 7 11 420.411 134.830 5 14 -7 -11 449.665 127.993 6 -14 7 10 2960.75 352.532 8 -14 -7 10 3159.63 355.167 8 -14 7 10 2804.76 346.143 5 14 -7 -10 2871.62 330.877 6 -14 7 9 3078.80 364.037 8 -14 -7 9 3303.99 383.766 8 -14 7 9 3077.65 389.116 5 14 -7 -9 2810.68 345.583 6 -14 7 8 5022.97 470.921 8 -14 7 8 5817.06 523.540 5 -14 -7 8 5350.65 497.668 8 14 -7 -8 5882.96 500.399 6 -14 7 7 2027.78 312.496 5 -14 -7 7 2106.18 324.502 8 -14 7 7 2236.39 312.173 8 14 -7 -7 2039.19 296.256 6 -14 7 6 2472.10 348.690 5 -14 7 6 2045.81 306.979 8 -14 -7 6 2289.59 345.781 8 14 -7 -6 2519.07 327.268 6 -14 -7 5 30.6517 46.1485 8 -14 7 5 49.4422 21.4195 8 14 -7 -5 53.6366 51.4066 6 -14 7 5 17.2611 21.2008 5 -14 7 4 2941.58 384.176 5 -14 -7 4 3410.33 429.904 8 -14 7 4 3188.82 372.735 8 14 7 -4 2728.44 324.647 6 14 -7 -4 2989.10 339.869 6 -14 7 3 1628.85 271.800 5 -14 -7 3 1754.93 309.228 8 -14 7 3 1516.16 244.886 8 14 -7 -3 1561.99 225.918 6 -14 -7 2 3445.91 429.756 8 -14 7 2 3135.26 376.671 5 -14 -7 1 91.8622 61.5757 8 -14 7 1 84.0612 76.1779 5 -14 -7 0 2588.47 343.847 8 -14 -7 -1 1287.56 227.841 8 -14 -7 -2 81.5917 68.2602 8 -14 8 14 5240.37 342.873 8 -14 8 14 5575.56 362.829 5 -14 8 13 516.212 132.783 5 -14 8 13 576.529 130.671 8 14 8 -13 262.555 95.6089 6 14 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1714.90 245.324 8 -15 -6 0-31.5443 41.0716 8 -15 7 12 10725.6 517.327 8 -15 7 12 11325.0 538.128 5 15 7 -12 10031.2 524.386 6 15 -7 -12 10289.0 454.809 6 -15 7 11-48.7468 29.1830 8 -15 -7 11-28.2290 36.5500 8 -15 7 11 119.711 70.2027 5 15 7 -11 71.4843 61.8106 6 15 -7 -11 173.059 69.9686 6 -15 7 10 634.715 137.100 8 -15 -7 10 788.174 161.332 8 -15 7 10 641.745 142.841 5 15 7 -10 411.541 128.613 6 15 -7 -10 558.855 132.170 6 -15 -7 9 138.940 60.9036 8 -15 7 9 221.260 73.2987 8 -15 7 9 286.111 97.7616 5 15 7 -9 174.054 77.9500 6 15 -7 -9 150.604 69.4139 6 -15 -7 8 368.659 121.963 8 -15 7 8 260.771 88.7566 8 -15 7 8 384.133 116.729 5 15 7 -8 292.374 107.204 6 15 -7 -8 286.231 91.5423 6 -15 -7 7 1102.42 202.377 8 15 7 -7 1077.35 194.945 6 -15 7 7 1397.32 227.230 5 -15 7 7 1204.64 201.862 8 15 -7 -7 1332.08 208.929 6 -15 7 6 5883.68 470.109 5 -15 -7 6 5357.16 461.343 8 -15 7 6 5504.33 436.621 8 15 7 -6 5175.82 408.605 6 15 -7 -6 6308.23 442.932 6 -15 7 5 2514.87 304.397 5 -15 -7 5 2452.04 317.632 8 -15 7 5 2155.18 257.844 8 15 7 -5 2189.98 247.747 6 15 -7 -5 2533.86 260.814 6 -15 -7 4 500.726 146.433 8 -15 7 4 365.132 110.943 5 15 -7 -4 516.156 112.216 6 -15 -7 3-52.6289 42.0963 8 -15 7 3 0.93705 37.7359 5 -15 -7 2 171.113 81.1966 8 -15 -7 1 7.84838 26.7345 8 15 8 -12 143.334 59.0493 6 -15 8 12 197.045 70.0814 5 -15 8 11 5558.68 383.808 5 -15 8 11 5065.06 350.125 8 15 8 -11 4842.39 378.134 6 15 -8 -11 5309.00 344.980 6 -15 8 10 812.562 146.584 8 15 8 -10 713.424 160.448 6 -15 8 10 951.736 170.173 5 15 -8 -10 1038.69 166.680 6 -15 8 9 1668.68 230.187 5 -15 8 9 1412.93 202.322 8 -15 -8 9 1353.77 200.500 8 15 8 -9 1340.82 217.890 6 15 -8 -9 1699.60 221.428 6 -15 8 8 124.119 65.0639 5 -15 -8 8 119.337 57.1015 8 -15 8 8 81.4470 44.5005 8 15 8 -8-15.0279 10.6989 6 15 -8 -8 56.1744 34.2272 6 -15 8 7 1093.86 195.395 5 -15 -8 7 886.595 172.885 8 -15 8 7 963.464 175.167 8 15 8 -7 1141.15 193.705 6 15 -8 -7 1278.66 193.970 6 -15 -8 6-17.7897 53.0476 8 15 8 -6 88.4020 57.0917 6 15 -8 -6 147.430 71.0307 6 -15 8 6 71.6956 58.0673 5 -15 8 5 8476.06 556.048 5 -15 -8 5 7924.39 550.697 8 15 8 -5 6920.01 419.427 6 15 -8 -5 7733.38 446.935 6 -15 -8 4 294.985 97.8930 8 -15 8 4 387.220 115.116 5 15 -8 -4 263.801 73.0125 6 -15 -8 3 2654.09 309.182 8 -15 8 3 2747.29 301.143 5 -15 -8 2 299.472 102.215 8 -15 -8 1 4036.30 345.435 8 -15 9 11 243.814 69.9739 5 15 9 -11 253.734 84.7839 6 15 -9 -11 119.303 43.5786 6 -15 9 10 155.638 60.6830 5 15 9 -10 162.858 73.2185 6 15 -9 -10 241.031 78.3867 6 -15 9 9 542.287 128.018 5 15 9 -9 461.373 118.265 6 15 -9 -9 609.239 123.910 6 -15 9 8 765.933 158.231 5 -15 -9 8 671.787 140.630 8 15 9 -8 538.449 137.118 6 15 -9 -8 804.214 148.957 6 -15 9 7 515.092 133.438 5 -15 -9 7 503.256 127.164 8 15 9 -7 315.826 95.5660 6 15 -9 -7 499.933 114.686 6 -15 9 6 915.560 174.177 5 -15 -9 6 877.972 170.167 8 15 9 -6 633.797 125.873 6 15 -9 -6 884.387 150.224 6 -15 9 5 933.440 174.752 5 -15 -9 5 904.064 173.008 8 15 -9 -5 964.828 151.347 6 -15 9 4 229.884 89.5770 5 -15 -9 4 149.389 74.8356 8 15 -9 -4 87.6954 39.8970 6 -15 -9 3 400.435 117.216 8 -15 -9 2 308.875 92.5792 8 15 10 -11 930.803 149.020 6 -15 10 10 7219.01 407.710 5 15 10 -10 6418.88 414.871 6 15 -10 -10 7307.95 388.495 6 15 10 -9 649.692 139.159 6 -15 10 9 694.227 132.602 5 15 -10 -9 606.690 116.588 6 15 10 -8 209.934 81.0574 6 -15 10 8 262.508 84.2699 5 15 -10 -8 385.136 102.128 6 15 10 -7 459.779 106.601 6 -15 10 7 659.376 139.424 5 15 -10 -7 606.569 119.837 6 15 10 -6 334.670 86.9275 6 -15 10 6 480.496 121.535 5 15 -10 -6 535.680 111.426 6 -15 10 5 8164.36 499.716 5 -15 -10 5 6658.19 426.293 8 15 -10 -5 7675.16 399.308 6 -15 10 4 83.2279 40.7609 5 15 11 -10 945.538 151.218 6 15 -11 -9 1395.40 168.474 6 15 11 -9 1098.97 165.695 6 15 11 -8 68.9179 34.7238 6 -15 11 8 122.103 52.5402 5 15 -11 -8 135.768 49.1930 6 -15 11 7 3222.09 290.763 5 15 -11 -7 3440.93 272.809 6 -15 11 6 2123.68 239.069 5 15 -11 -6 2177.70 210.909 6 -15 11 5 544.666 117.806 5 15 -11 -5 492.314 91.5263 6 15 -12 -8 103.097 44.0770 6 15 -12 -7 31.6399 31.0286 6 -16 0 12 999.746 153.761 8 -16 0 11 121.337 63.7561 8 16 0 -11 217.053 84.2247 6 -16 0 11 126.073 57.8741 5 -16 0 10 4525.23 329.978 5 -16 0 10 4698.20 384.581 8 16 0 -10 4420.76 344.780 6 -16 0 9-49.6995 22.5939 8 16 0 -9-20.5152 23.5204 6 -16 0 8 7403.09 440.985 5 -16 0 8 8324.88 542.807 8 16 0 -8 7943.69 472.143 6 -16 0 7 80.6037 35.5929 8 16 0 -7 70.2878 57.1029 6 -16 0 7-41.8860 20.4748 5 -16 0 6 2026.76 224.137 5 -16 0 6 1810.93 257.747 8 16 0 -6 1662.08 196.367 6 -16 0 5 0.66621 31.2075 8 -16 0 5 14.9883 9.58204 5 -16 0 4 6029.19 454.924 8 -16 0 3-22.5958 30.1668 8 -16 1 12 1575.93 193.834 8 -16 1 11 7734.83 421.557 5 -16 1 11 7563.55 458.551 8 -16 -1 11 7807.58 462.322 8 16 -1 -11 7841.53 430.473 6 16 1 -11 7808.96 437.293 6 16 -1 -10 903.443 151.336 6 -16 -1 10 941.568 143.592 5 -16 1 10 1038.98 162.280 5 -16 -1 10 1087.91 183.834 8 -16 1 10 1068.79 183.747 8 16 1 -10 1075.02 173.010 6 -16 -1 9 2349.26 235.981 5 -16 1 9 2230.66 242.815 5 -16 -1 9 2179.58 268.969 8 -16 1 9 2121.26 264.708 8 16 -1 -9 2571.16 266.454 6 16 1 -9 2411.54 262.275 6 -16 -1 8-85.2906 55.7981 8 -16 1 8 140.636 69.8151 8 16 1 -8 78.4094 52.2293 6 16 -1 -8 134.910 64.2851 6 -16 -1 8 100.374 49.4764 5 -16 1 8-25.3039 34.9468 5 -16 -1 7 1914.76 212.166 5 -16 1 7 1987.01 234.153 5 -16 -1 7 2366.60 296.087 8 -16 1 7 2168.24 280.978 8 16 -1 -7 1931.48 229.285 6 16 1 -7 2058.62 236.906 6 -16 -1 6 700.475 162.824 8 -16 1 6 867.489 173.693 8 -16 1 6 727.768 137.032 5 16 -1 -6 616.656 121.872 6 16 1 -6 582.847 118.532 6 -16 -1 5 321.075 103.735 8 -16 1 5 260.961 92.0250 8 -16 1 5 272.593 77.3052 5 -16 -1 4-13.0504 30.3510 8 -16 1 4-88.4080 65.3060 8 -16 1 3 263.176 89.7005 8 -16 -1 3 397.249 111.241 8 -16 2 11 3968.17 303.021 5 -16 2 11 3941.71 327.226 8 -16 -2 11 3952.05 321.887 8 16 -2 -11 3908.54 298.584 6 16 2 -11 3771.07 302.817 6 -16 2 10 1537.79 198.901 5 -16 -2 10 1904.17 239.590 8 -16 2 10 1722.18 226.324 8 16 -2 -10 1464.72 196.563 6 16 2 -10 1488.37 201.150 6 -16 -2 9 57.2237 40.0060 8 -16 2 9 100.945 69.5840 8 16 2 -9 149.984 63.9949 6 16 -2 -9 202.871 75.3227 6 -16 2 9 62.4790 30.2979 5 -16 2 8 3272.50 300.010 5 -16 2 8 3397.36 342.573 8 -16 -2 8 3596.11 356.662 8 16 -2 -8 3236.57 298.183 6 16 2 -8 3078.46 293.955 6 -16 2 7 1364.16 196.339 5 -16 -2 7 1368.09 220.649 8 -16 2 7 1472.38 223.747 8 16 -2 -7 1498.98 197.316 6 16 2 -7 1527.84 200.845 6 -16 -2 6 892.913 182.035 8 -16 2 6 684.887 152.046 8 -16 2 6 537.888 121.072 5 16 2 -6 579.043 115.769 6 16 -2 -6 522.256 111.325 6 -16 -2 5 513.533 136.539 8 -16 2 5 632.453 147.642 8 -16 2 5 692.503 132.680 5 -16 -2 4 165.863 75.0930 8 -16 2 4 164.759 75.1928 8 -16 -2 3 178.938 79.8362 8 -16 3 11 5158.51 344.912 5 -16 -3 11 4484.42 335.690 8 -16 3 11 4654.89 348.072 8 16 -3 -11 5107.89 331.297 6 16 3 -11 4752.83 339.400 6 -16 3 10 2583.21 256.689 5 -16 -3 10 2927.45 295.895 8 -16 3 10 2813.44 285.414 8 16 -3 -10 2331.37 239.568 6 16 3 -10 2318.09 249.827 6 -16 3 9 1648.49 211.810 5 -16 3 9 1293.80 197.983 8 -16 -3 9 1285.93 204.993 8 16 -3 -9 1597.80 203.222 6 16 3 -9 1496.03 205.061 6 -16 -3 8 57.6270 57.6096 8 -16 3 8 33.2911 27.4558 8 16 3 -8 3.53530 22.0857 6 -16 3 8 83.4037 42.8465 5 -16 -3 7 3010.05 323.493 8 -16 3 7 2833.64 304.224 8 -16 3 7 2951.57 292.804 5 16 -3 -7 2534.26 249.852 6 16 3 -7 2414.06 250.275 6 -16 -3 6 3313.85 342.022 8 -16 3 6 3117.52 317.721 8 -16 3 6 2673.72 273.780 5 16 -3 -6 2627.51 247.179 6 16 3 -6 2297.89 223.664 6 -16 -3 5 3596.72 356.479 8 -16 3 5 3442.42 330.748 8 -16 3 5 3688.84 317.157 5 -16 -3 4 687.953 146.922 8 -16 3 4 697.708 142.891 8 -16 -3 3 126.418 53.4197 8 -16 4 11 6477.98 395.847 8 -16 4 11 6618.18 385.442 5 16 -4 -11 6198.60 358.241 6 16 4 -11 5689.50 362.464 6 -16 -4 10 824.112 148.865 8 -16 4 10 828.263 154.126 8 16 4 -10 650.325 130.601 6 -16 4 10 869.850 148.835 5 16 -4 -10 657.878 128.736 6 -16 -4 9 275.106 94.4576 8 -16 4 9 238.334 82.4463 8 16 4 -9 391.460 109.134 6 16 -4 -9 422.697 101.190 6 -16 4 9 383.606 98.8159 5 -16 4 8 2977.44 288.780 5 -16 4 8 2961.11 300.461 8 -16 -4 8 2976.96 308.615 8 16 -4 -8 2975.95 273.305 6 16 4 -8 2974.33 281.181 6 -16 4 7 4618.52 361.448 5 -16 -4 7 4362.08 379.720 8 -16 4 7 4460.76 369.856 8 16 -4 -7 4517.37 330.498 6 16 4 -7 4299.82 324.052 6 -16 -4 6 226.857 86.8582 8 -16 4 6 140.498 54.8958 8 -16 4 6 282.520 85.9422 5 16 4 -6 214.122 67.5634 6 16 -4 -6 288.018 80.4872 6 -16 -4 5 440.007 126.309 8 -16 4 5 344.068 97.7772 8 -16 4 5 566.957 121.126 5 -16 -4 4 184.005 71.3164 8 -16 -4 3 372.806 105.680 8 -16 5 10 2384.08 238.957 5 -16 5 10 2531.58 250.407 8 16 -5 -10 2361.25 227.809 6 16 5 -10 2154.96 233.367 6 -16 -5 9 175.721 69.7359 8 -16 5 9 194.537 65.9824 8 -16 5 9 186.477 66.7782 5 16 5 -9 138.509 58.2306 6 16 -5 -9 218.141 76.3558 6 -16 -5 8 60.0142 47.9458 8 -16 5 8 113.586 51.2327 8 -16 5 8 97.3853 60.3971 5 16 5 -8 46.1255 29.7994 6 16 -5 -8 155.364 66.2515 6 -16 -5 7 398.108 117.157 8 -16 5 7 441.200 113.764 8 16 5 -7 412.147 101.001 6 16 -5 -7 333.781 87.9380 6 -16 5 7 340.232 94.3826 5 -16 5 6 1236.72 184.859 5 -16 -5 6 1286.42 207.398 8 -16 5 6 1227.15 177.787 8 16 -5 -6 1192.99 152.563 6 -16 5 5 1739.88 216.861 5 -16 -5 5 1531.58 220.569 8 -16 -5 4 1190.86 189.277 8 -16 6 10 1565.59 185.389 5 16 -6 -10 1445.88 166.113 6 16 6 -10 1382.63 179.210 6 -16 6 9 41.1464 40.5715 5 16 6 -9 64.0651 42.2383 6 16 -6 -9 133.507 56.2811 6 -16 -6 8 472.334 109.734 8 16 6 -8 586.371 118.316 6 16 -6 -8 630.726 116.964 6 -16 6 8 661.756 130.341 5 -16 6 7 3930.75 323.386 5 -16 -6 7 3666.87 325.090 8 16 -6 -7 3681.56 274.433 6 -16 -6 6 289.587 91.5419 8 -16 6 6 367.716 98.3450 5 -16 -6 5 1276.82 192.800 8 -16 6 5 1227.34 180.249 5 16 -7 -9 713.250 117.628 6 -16 7 9 614.546 119.111 5 -16 7 8 80.8802 47.9825 5 16 -7 -8 152.033 54.8797 6 16 -7 -7 1682.87 178.710 6 -16 7 7 1909.15 217.532 5 -16 7 6 7079.15 420.071 5 -16 7 5 642.314 125.149 5 0 0 0 0.00 0.00 0 TITL hasj240524a in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 13.458770 23.060276 15.785781 90.0000 111.8607 90.0000 ZERR 2.00 0.000209 0.000308 0.000245 0.0000 0.0018 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O P Ca UNIT 180.00 308.00 8.00 8.00 8.00 4.00 REM CrysAlisPro recorded range (K): Min=99.9; max=100.1; aver:100.0 TEMP -173 SIZE 0.19 0.23 0.27 TREF HKLF 4 END ; _shelx_hkl_checksum 20478 _olex2_date_sample_data_collection 2024-05-24 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.870 _oxdiff_exptl_absorpt_empirical_full_min 0.615 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ca1 Ca 0.54772(3) 0.53369(2) 0.67087(3) 0.02518(13) Uani 1 1 d D . . . . N1 N 0.68032(15) 0.49010(8) 0.79759(13) 0.0258(4) Uani 1 1 d . . . . . N2 N 0.42775(14) 0.51133(8) 0.74196(13) 0.0244(4) Uani 1 1 d . . . . . C1 C 0.7708(2) 0.51149(13) 0.96314(17) 0.0374(6) Uani 1 1 d . . . . . H1A H 0.832925 0.495521 0.952907 0.056 Uiso 1 1 calc R U . . . H1B H 0.757274 0.488667 1.010094 0.056 Uiso 1 1 calc R U . . . H1C H 0.785255 0.551859 0.983398 0.056 Uiso 1 1 calc R U . . . C2 C 0.67286(18) 0.50902(10) 0.87444(15) 0.0263(4) Uani 1 1 d . . . . . C3 C 0.57808(18) 0.52958(10) 0.88396(16) 0.0274(5) Uani 1 1 d . . . . . H3 H 0.593(2) 0.5434(12) 0.941(2) 0.025(6) Uiso 1 1 d . . . . . C4 C 0.46751(18) 0.52386(10) 0.83002(15) 0.0263(4) Uani 1 1 d . . . . . C5 C 0.3943(2) 0.53240(13) 0.88240(17) 0.0363(6) Uani 1 1 d . . . . . H5A H 0.424348 0.562200 0.929268 0.054 Uiso 1 1 calc R U . . . H5B H 0.387829 0.495814 0.911531 0.054 Uiso 1 1 calc R U . . . H5C H 0.323417 0.544687 0.840264 0.054 Uiso 1 1 calc R U . . . C6 C 0.77653(19) 0.45985(11) 0.80392(16) 0.0302(5) Uani 1 1 d . . . . . C7 C 0.85599(19) 0.48719(12) 0.78067(17) 0.0337(5) Uani 1 1 d . . . . . C8 C 0.9506(2) 0.45675(14) 0.7925(2) 0.0444(6) Uani 1 1 d . . . . . H8 H 1.004616 0.475013 0.776723 0.053 Uiso 1 1 calc R U . . . C9 C 0.9669(2) 0.40153(15) 0.8262(3) 0.0548(8) Uani 1 1 d . . . . . H9 H 1.032969 0.382459 0.836533 0.066 Uiso 1 1 calc R U . . . C10 C 0.8870(2) 0.37364(14) 0.8451(3) 0.0545(8) Uani 1 1 d . . . . . H10 H 0.897653 0.334782 0.866613 0.065 Uiso 1 1 calc R U . . . C11 C 0.7910(2) 0.40147(12) 0.8332(2) 0.0402(6) Uani 1 1 d D . . . . C12 C 0.84454(19) 0.54918(13) 0.74612(19) 0.0394(6) Uani 1 1 d . . . . . H12 H 0.766122 0.555941 0.713161 0.047 Uiso 1 1 calc R U . . . C13 C 0.8813(2) 0.59284(14) 0.8236(2) 0.0486(7) Uani 1 1 d . . . . . H13A H 0.866061 0.632297 0.797204 0.058 Uiso 1 1 calc R U . . . H13B H 0.838285 0.587222 0.861939 0.058 Uiso 1 1 calc R U . . . C14 C 0.9983(3) 0.58959(18) 0.8841(3) 0.0646(10) Uani 1 1 d . . . . . H14A H 1.042104 0.595600 0.847287 0.097 Uiso 1 1 calc R U . . . H14B H 1.013984 0.551362 0.913235 0.097 Uiso 1 1 calc R U . . . H14C H 1.014791 0.619691 0.931200 0.097 Uiso 1 1 calc R U . . . C15 C 0.8972(2) 0.55857(18) 0.6751(2) 0.0557(9) Uani 1 1 d . . . . . H15A H 0.975771 0.556213 0.707248 0.067 Uiso 1 1 calc R U . . . H15B H 0.875517 0.526136 0.630892 0.067 Uiso 1 1 calc R U . . . C16 C 0.8722(3) 0.6134(2) 0.6234(3) 0.0764(13) Uani 1 1 d . . . . . H16A H 0.896054 0.611021 0.571967 0.092 Uiso 1 1 calc R U . . . H16B H 0.909061 0.645463 0.663504 0.092 Uiso 1 1 calc R U . . . H16C H 0.794710 0.620121 0.600376 0.092 Uiso 1 1 calc R U . . . C21 C 0.6713(3) 0.30726(14) 0.7039(3) 0.0542(8) Uani 1 1 d D U . . . H21A H 0.611448 0.333138 0.671247 0.081 Uiso 0.840(6) 1 calc R U P A 1 H21B H 0.654655 0.267929 0.679101 0.081 Uiso 0.840(6) 1 calc R U P A 1 H21C H 0.736251 0.321091 0.696191 0.081 Uiso 0.840(6) 1 calc R U P A 1 H21D H 0.613140 0.300296 0.644966 0.081 Uiso 0.160(6) 1 calc R U P A 2 H21E H 0.697058 0.270120 0.734257 0.081 Uiso 0.160(6) 1 calc R U P A 2 H21F H 0.730086 0.327453 0.693949 0.081 Uiso 0.160(6) 1 calc R U P A 2 C22 C 0.31618(18) 0.49633(11) 0.70164(15) 0.0281(5) Uani 1 1 d . . . . . C23 C 0.24067(19) 0.53674(11) 0.64608(17) 0.0331(5) Uani 1 1 d D . . . . C24 C 0.1334(2) 0.51965(14) 0.6102(2) 0.0425(6) Uani 1 1 d . . . . . H24 H 0.081134 0.546221 0.573452 0.051 Uiso 1 1 calc R U . . . C25 C 0.1010(2) 0.46554(14) 0.6262(2) 0.0447(7) Uani 1 1 d . . . . . H25 H 0.027241 0.455545 0.602033 0.054 Uiso 1 1 calc R U . . . C26 C 0.1759(2) 0.42585(13) 0.67761(19) 0.0395(6) Uani 1 1 d . . . . . H26 H 0.153159 0.388230 0.687031 0.047 Uiso 1 1 calc R U . . . C27 C 0.28429(19) 0.43986(11) 0.71594(16) 0.0313(5) Uani 1 1 d . . . . . C28A C 0.2779(14) 0.5942(5) 0.6210(9) 0.034(3) Uani 0.489(8) 1 d D U P B 2 H28A H 0.351442 0.589743 0.620075 0.041 Uiso 0.489(8) 1 calc R U P B 2 C31A C 0.2798(12) 0.6381(9) 0.6936(9) 0.041(3) Uani 0.489(8) 1 d D U P B 2 H31A H 0.309435 0.674707 0.680133 0.049 Uiso 0.489(8) 1 calc R U P B 2 H31B H 0.331130 0.623807 0.752915 0.049 Uiso 0.489(8) 1 calc R U P B 2 C32A C 0.1752(11) 0.6529(9) 0.7064(9) 0.053(3) Uani 0.489(8) 1 d D U P B 2 H32A H 0.125906 0.671912 0.651217 0.079 Uiso 0.489(8) 1 calc R U P B 2 H32B H 0.190423 0.679070 0.758659 0.079 Uiso 0.489(8) 1 calc R U P B 2 H32C H 0.142373 0.617231 0.717494 0.079 Uiso 0.489(8) 1 calc R U P B 2 C33 C 0.3674(2) 0.39393(11) 0.76567(18) 0.0357(5) Uani 1 1 d D . . . . H33 H 0.426872 0.414472 0.814552 0.043 Uiso 0.764(6) 1 calc R U P C 1 H33A H 0.436879 0.406542 0.762126 0.043 Uiso 0.236(6) 1 calc R U P C 2 C37 C 0.2944(3) 0.36739(16) 0.8887(2) 0.0539(8) Uani 1 1 d D . . . . H37A H 0.240898 0.398082 0.864526 0.081 Uiso 0.764(6) 1 calc R U P C 1 H37B H 0.356798 0.383002 0.938489 0.081 Uiso 0.764(6) 1 calc R U P C 1 H37C H 0.263380 0.335555 0.911887 0.081 Uiso 0.764(6) 1 calc R U P C 1 H37D H 0.259933 0.334600 0.849250 0.081 Uiso 0.236(6) 1 calc R U P C 2 H37E H 0.242320 0.398767 0.879666 0.081 Uiso 0.236(6) 1 calc R U P C 2 H37F H 0.320896 0.354929 0.952678 0.081 Uiso 0.236(6) 1 calc R U P C 2 P1 P 0.38698(6) 0.48307(3) 0.49283(5) 0.0300(3) Uani 0.902(3) 1 d . U P D 1 P2 P 0.53924(6) 0.43940(3) 0.53334(5) 0.0308(2) Uani 0.902(3) 1 d . U P D 1 O1 O 0.5690(5) 0.63593(14) 0.7061(3) 0.0368(9) Uani 0.867(5) 1 d D U P D 1 C17 C 0.7050(4) 0.3660(2) 0.8510(3) 0.0408(10) Uani 0.840(6) 1 d D U P A 1 H17 H 0.636082 0.387750 0.824353 0.049 Uiso 0.840(6) 1 calc R U P A 1 C18 C 0.7300(3) 0.3583(2) 0.9559(3) 0.0503(10) Uani 0.840(6) 1 d D U P A 1 H18A H 0.793635 0.333077 0.982238 0.060 Uiso 0.840(6) 1 calc R U P A 1 H18B H 0.748111 0.396645 0.985864 0.060 Uiso 0.840(6) 1 calc R U P A 1 C19 C 0.6391(4) 0.3325(2) 0.9775(3) 0.0541(11) Uani 0.840(6) 1 d D U P A 1 H19A H 0.575353 0.356919 0.951401 0.081 Uiso 0.840(6) 1 calc R U P A 1 H19B H 0.659545 0.330273 1.043888 0.081 Uiso 0.840(6) 1 calc R U P A 1 H19C H 0.623338 0.293422 0.951407 0.081 Uiso 0.840(6) 1 calc R U P A 1 C20 C 0.6888(3) 0.30670(15) 0.8038(3) 0.0483(9) Uani 0.840(6) 1 d D U P A 1 H20A H 0.752379 0.282454 0.836138 0.058 Uiso 0.840(6) 1 calc R U P A 1 H20B H 0.626376 0.287687 0.810866 0.058 Uiso 0.840(6) 1 calc R U P A 1 C29 C 0.2026(9) 0.6308(4) 0.5418(6) 0.0372(19) Uani 0.511(8) 1 d D U P B 1 H29A H 0.129083 0.636694 0.540358 0.045 Uiso 0.511(8) 1 calc R U P B 1 H29B H 0.233878 0.669591 0.541075 0.045 Uiso 0.511(8) 1 calc R U P B 1 C30 C 0.1959(4) 0.5983(2) 0.4561(4) 0.0354(14) Uani 0.511(8) 1 d D U P B 1 H30A H 0.136908 0.613892 0.403464 0.053 Uiso 0.511(8) 1 calc R U P B 1 H30B H 0.183317 0.557016 0.463205 0.053 Uiso 0.511(8) 1 calc R U P B 1 H30C H 0.263356 0.602896 0.446489 0.053 Uiso 0.511(8) 1 calc R U P B 1 C34 C 0.4168(3) 0.36618(16) 0.7001(3) 0.0387(9) Uani 0.764(6) 1 d D . P C 1 H34A H 0.454240 0.396756 0.679510 0.046 Uiso 0.764(6) 1 calc R U P C 1 H34B H 0.470841 0.337111 0.734617 0.046 Uiso 0.764(6) 1 calc R U P C 1 C35 C 0.3351(13) 0.3368(5) 0.6163(6) 0.047(2) Uani 0.764(6) 1 d D . P C 1 H35A H 0.282276 0.365475 0.580631 0.071 Uiso 0.764(6) 1 calc R U P C 1 H35B H 0.298722 0.305777 0.635883 0.071 Uiso 0.764(6) 1 calc R U P C 1 H35C H 0.371848 0.320434 0.578656 0.071 Uiso 0.764(6) 1 calc R U P C 1 C36 C 0.3289(3) 0.34485(15) 0.8128(2) 0.0382(9) Uani 0.764(6) 1 d D . P C 1 H36A H 0.267841 0.324526 0.766640 0.046 Uiso 0.764(6) 1 calc R U P C 1 H36B H 0.387477 0.316385 0.838874 0.046 Uiso 0.764(6) 1 calc R U P C 1 C38 C 0.5311(4) 0.68097(15) 0.6374(3) 0.0497(9) Uani 0.867(5) 1 d D U P D 1 H38A H 0.511440 0.715592 0.664827 0.060 Uiso 0.867(5) 1 calc R U P D 1 H38B H 0.465952 0.667175 0.587297 0.060 Uiso 0.867(5) 1 calc R U P D 1 C39 C 0.6138(5) 0.6978(2) 0.5988(4) 0.0844(19) Uani 0.867(5) 1 d D . P D 1 H39A H 0.586296 0.729705 0.555327 0.127 Uiso 0.867(5) 1 calc R U P D 1 H39B H 0.629599 0.664400 0.567491 0.127 Uiso 0.867(5) 1 calc R U P D 1 H39C H 0.679428 0.710229 0.648432 0.127 Uiso 0.867(5) 1 calc R U P D 1 C40 C 0.6317(3) 0.65934(14) 0.7957(3) 0.0414(8) Uani 0.867(5) 1 d D U P D 1 H40A H 0.680425 0.689595 0.788931 0.050 Uiso 0.867(5) 1 calc R U P D 1 H40B H 0.676370 0.627999 0.834104 0.050 Uiso 0.867(5) 1 calc R U P D 1 C41 C 0.5637(3) 0.68522(15) 0.8436(2) 0.0463(9) Uani 0.867(5) 1 d D U P D 1 H41A H 0.519606 0.716514 0.806213 0.069 Uiso 0.867(5) 1 calc R U P D 1 H41B H 0.610141 0.700795 0.902912 0.069 Uiso 0.867(5) 1 calc R U P D 1 H41C H 0.517233 0.655148 0.852766 0.069 Uiso 0.867(5) 1 calc R U P D 1 P1A P 0.4368(9) 0.4512(6) 0.5222(8) 0.071(4) Uani 0.098(3) 1 d . U P D 2 P2A P 0.6013(10) 0.4649(6) 0.5360(10) 0.083(5) Uani 0.098(3) 1 d . U P D 2 O1A O 0.583(3) 0.6350(7) 0.6928(19) 0.026(5) Uani 0.133(5) 1 d D U P D 2 C17A C 0.7020(17) 0.3720(11) 0.8553(14) 0.045(4) Uani 0.160(6) 1 d D U P A 2 H17A H 0.661640 0.401730 0.875711 0.054 Uiso 0.160(6) 1 calc R U P A 2 C18A C 0.7497(14) 0.3269(9) 0.9310(12) 0.051(4) Uani 0.160(6) 1 d D U P A 2 H18C H 0.772637 0.292800 0.904683 0.062 Uiso 0.160(6) 1 calc R U P A 2 H18D H 0.814539 0.343639 0.978109 0.062 Uiso 0.160(6) 1 calc R U P A 2 C19A C 0.676(2) 0.3064(11) 0.9767(17) 0.065(6) Uani 0.160(6) 1 d D U P A 2 H19D H 0.603239 0.302694 0.931130 0.097 Uiso 0.160(6) 1 calc R U P A 2 H19E H 0.676442 0.334515 1.023373 0.097 Uiso 0.160(6) 1 calc R U P A 2 H19F H 0.700467 0.268639 1.005398 0.097 Uiso 0.160(6) 1 calc R U P A 2 C20A C 0.6288(13) 0.3456(7) 0.7654(10) 0.049(3) Uani 0.160(6) 1 d D U P A 2 H20C H 0.588817 0.378140 0.726789 0.059 Uiso 0.160(6) 1 calc R U P A 2 H20D H 0.575550 0.321782 0.779313 0.059 Uiso 0.160(6) 1 calc R U P A 2 C29A C 0.1983(9) 0.6119(4) 0.5248(7) 0.043(2) Uani 0.489(8) 1 d D U P B 2 H29C H 0.191155 0.579868 0.481211 0.051 Uiso 0.489(8) 1 calc R U P B 2 H29D H 0.126880 0.619345 0.527134 0.051 Uiso 0.489(8) 1 calc R U P B 2 C30A C 0.2372(6) 0.6659(3) 0.4923(5) 0.060(2) Uani 0.489(8) 1 d D U P B 2 H30D H 0.195641 0.671618 0.427099 0.089 Uiso 0.489(8) 1 calc R U P B 2 H30E H 0.313092 0.661414 0.502044 0.089 Uiso 0.489(8) 1 calc R U P B 2 H30F H 0.228101 0.699516 0.526606 0.089 Uiso 0.489(8) 1 calc R U P B 2 C34A C 0.3352(9) 0.3396(4) 0.7113(7) 0.035(3) Uani 0.236(6) 1 d D . P C 2 H34C H 0.259814 0.329891 0.700644 0.043 Uiso 0.236(6) 1 calc R U P C 2 H34D H 0.381272 0.306938 0.743852 0.043 Uiso 0.236(6) 1 calc R U P C 2 C35A C 0.348(4) 0.3512(18) 0.6211(18) 0.045(6) Uani 0.236(6) 1 d D . P C 2 H35D H 0.298260 0.381601 0.587641 0.067 Uiso 0.236(6) 1 calc R U P C 2 H35E H 0.333530 0.315594 0.584660 0.067 Uiso 0.236(6) 1 calc R U P C 2 H35F H 0.421881 0.363875 0.633093 0.067 Uiso 0.236(6) 1 calc R U P C 2 C36A C 0.3857(10) 0.3885(6) 0.8654(7) 0.051(3) Uani 0.236(6) 1 d D . P C 2 H36C H 0.446849 0.361903 0.893750 0.062 Uiso 0.236(6) 1 calc R U P C 2 H36D H 0.407264 0.427032 0.894024 0.062 Uiso 0.236(6) 1 calc R U P C 2 C38A C 0.5967(17) 0.6739(9) 0.6273(13) 0.036(4) Uani 0.133(5) 1 d D U P D 2 H38C H 0.624705 0.651788 0.587267 0.043 Uiso 0.133(5) 1 calc R U P D 2 H38D H 0.651176 0.703241 0.660089 0.043 Uiso 0.133(5) 1 calc R U P D 2 C39A C 0.496(2) 0.7049(11) 0.5685(16) 0.068(9) Uani 0.133(5) 1 d D . P D 2 H39D H 0.453828 0.679384 0.518524 0.102 Uiso 0.133(5) 1 calc R U P D 2 H39E H 0.515629 0.740078 0.543141 0.102 Uiso 0.133(5) 1 calc R U P D 2 H39F H 0.454587 0.715492 0.605338 0.102 Uiso 0.133(5) 1 calc R U P D 2 C40A C 0.5558(15) 0.6606(7) 0.7642(11) 0.029(4) Uani 0.133(5) 1 d D U P D 2 H40C H 0.519093 0.631393 0.788203 0.034 Uiso 0.133(5) 1 calc R U P D 2 H40D H 0.505837 0.693280 0.739087 0.034 Uiso 0.133(5) 1 calc R U P D 2 C41A C 0.6536(17) 0.6821(11) 0.8403(14) 0.049(6) Uani 0.133(5) 1 d D U P D 2 H41D H 0.635065 0.716200 0.868397 0.074 Uiso 0.133(5) 1 calc R U P D 2 H41E H 0.708470 0.692529 0.816148 0.074 Uiso 0.133(5) 1 calc R U P D 2 H41F H 0.681123 0.651480 0.886292 0.074 Uiso 0.133(5) 1 calc R U P D 2 O2 O 0.1015(7) 0.2529(5) 0.6352(7) 0.068(2) Uani 0.515(10) 1 d D U P E 2 C42 C 0.0512(11) 0.2594(7) 0.5386(9) 0.064(3) Uani 0.515(10) 1 d D U P E 2 H42A H 0.046988 0.301046 0.522321 0.077 Uiso 0.515(10) 1 calc R U P E 2 H42B H -0.022600 0.243822 0.517612 0.077 Uiso 0.515(10) 1 calc R U P E 2 C43 C 0.1142(13) 0.2275(9) 0.4924(12) 0.066(4) Uani 0.515(10) 1 d D U P E 2 H43A H 0.078137 0.231129 0.426067 0.099 Uiso 0.515(10) 1 calc R U P E 2 H43B H 0.119279 0.186469 0.509566 0.099 Uiso 0.515(10) 1 calc R U P E 2 H43C H 0.186213 0.244132 0.511400 0.099 Uiso 0.515(10) 1 calc R U P E 2 C44 C 0.0454(6) 0.2782(3) 0.6865(7) 0.063(2) Uani 0.515(10) 1 d D U P E 2 H44A H 0.020016 0.317176 0.661441 0.075 Uiso 0.515(10) 1 calc R U P E 2 H44B H 0.095749 0.283312 0.750364 0.075 Uiso 0.515(10) 1 calc R U P E 2 C45 C -0.0477(8) 0.2438(3) 0.6867(8) 0.078(3) Uani 0.515(10) 1 d D U P E 2 H45A H -0.100182 0.240466 0.624159 0.117 Uiso 0.515(10) 1 calc R U P E 2 H45B H -0.080686 0.263229 0.724867 0.117 Uiso 0.515(10) 1 calc R U P E 2 H45C H -0.023609 0.205046 0.711151 0.117 Uiso 0.515(10) 1 calc R U P E 2 O2A O 0.0690(9) 0.2462(5) 0.5989(9) 0.068(2) Uani 0.485(10) 1 d D U P E 1 C42A C 0.0490(19) 0.2597(11) 0.5075(11) 0.086(5) Uani 0.485(10) 1 d D U P E 1 H42C H 0.058858 0.301855 0.501566 0.103 Uiso 0.485(10) 1 calc R U P E 1 H42D H -0.026077 0.249892 0.469529 0.103 Uiso 0.485(10) 1 calc R U P E 1 C43A C 0.122(2) 0.2271(14) 0.474(2) 0.109(8) Uani 0.485(10) 1 d D U P E 1 H43D H 0.115508 0.241778 0.413822 0.163 Uiso 0.485(10) 1 calc R U P E 1 H43E H 0.103837 0.185804 0.469330 0.163 Uiso 0.485(10) 1 calc R U P E 1 H43F H 0.196397 0.232153 0.516852 0.163 Uiso 0.485(10) 1 calc R U P E 1 C44A C -0.0068(7) 0.2725(4) 0.6292(7) 0.066(2) Uani 0.485(10) 1 d D U P E 1 H44C H -0.079087 0.257355 0.593355 0.080 Uiso 0.485(10) 1 calc R U P E 1 H44D H -0.007374 0.314950 0.619179 0.080 Uiso 0.485(10) 1 calc R U P E 1 C45A C 0.0197(8) 0.2606(5) 0.7276(7) 0.075(3) Uani 0.485(10) 1 d D U P E 1 H45D H 0.014573 0.218867 0.736776 0.113 Uiso 0.485(10) 1 calc R U P E 1 H45E H -0.030653 0.281315 0.748398 0.113 Uiso 0.485(10) 1 calc R U P E 1 H45F H 0.092783 0.273829 0.762722 0.113 Uiso 0.485(10) 1 calc R U P E 1 C28 C 0.2704(11) 0.5997(4) 0.6329(9) 0.030(2) Uani 0.511(8) 1 d D U P B 1 H28 H 0.342018 0.595426 0.628022 0.036 Uiso 0.511(8) 1 calc R U P B 1 C31 C 0.2934(11) 0.6401(8) 0.7135(8) 0.035(2) Uani 0.511(8) 1 d D U P B 1 H31C H 0.319458 0.677698 0.699712 0.042 Uiso 0.511(8) 1 calc R U P B 1 H31D H 0.350319 0.623192 0.767541 0.042 Uiso 0.511(8) 1 calc R U P B 1 C32 C 0.1932(11) 0.6499(7) 0.7347(7) 0.042(2) Uani 0.511(8) 1 d D U P B 1 H32D H 0.139131 0.669855 0.683314 0.063 Uiso 0.511(8) 1 calc R U P B 1 H32E H 0.211160 0.673699 0.789832 0.063 Uiso 0.511(8) 1 calc R U P B 1 H32F H 0.164906 0.612439 0.744663 0.063 Uiso 0.511(8) 1 calc R U P B 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ca1 0.0225(2) 0.0288(2) 0.0254(2) 0.00174(16) 0.01027(17) -0.00269(16) N1 0.0232(9) 0.0269(9) 0.0286(9) 0.0034(7) 0.0112(7) -0.0012(7) N2 0.0195(9) 0.0286(9) 0.0257(9) 0.0009(7) 0.0092(7) -0.0021(7) C1 0.0266(12) 0.0542(16) 0.0290(12) -0.0005(11) 0.0076(10) 0.0070(11) C2 0.0245(11) 0.0267(11) 0.0276(11) 0.0035(8) 0.0095(9) -0.0016(8) C3 0.0250(11) 0.0326(12) 0.0251(11) -0.0012(9) 0.0098(9) -0.0015(9) C4 0.0233(10) 0.0280(11) 0.0293(11) 0.0027(9) 0.0118(9) -0.0009(8) C5 0.0271(12) 0.0548(16) 0.0299(12) -0.0005(11) 0.0141(10) -0.0021(11) C6 0.0271(11) 0.0339(12) 0.0321(12) -0.0006(9) 0.0140(9) 0.0005(9) C7 0.0234(11) 0.0410(14) 0.0356(12) 0.0025(10) 0.0098(10) 0.0000(10) C8 0.0298(13) 0.0509(16) 0.0590(17) 0.0043(14) 0.0240(12) 0.0023(11) C9 0.0373(15) 0.0485(17) 0.088(2) 0.0026(16) 0.0343(16) 0.0107(13) C10 0.0425(16) 0.0372(15) 0.095(3) 0.0052(16) 0.0378(17) 0.0081(12) C11 0.0329(13) 0.0340(13) 0.0605(17) 0.0008(12) 0.0252(12) 0.0029(10) C12 0.0196(11) 0.0492(15) 0.0453(14) 0.0134(12) 0.0074(10) -0.0035(10) C13 0.0323(14) 0.0434(15) 0.069(2) 0.0030(14) 0.0172(13) -0.0002(12) C14 0.0398(17) 0.067(2) 0.075(2) -0.0260(19) 0.0073(16) -0.0105(15) C15 0.0278(13) 0.086(2) 0.0504(17) 0.0181(16) 0.0112(12) -0.0106(14) C16 0.0438(18) 0.106(3) 0.074(2) 0.038(2) 0.0153(17) -0.0124(19) C21 0.0470(16) 0.0413(15) 0.080(2) 0.0003(15) 0.0297(16) 0.0026(13) C22 0.0213(10) 0.0384(12) 0.0269(11) -0.0035(9) 0.0115(9) -0.0060(9) C23 0.0230(11) 0.0428(14) 0.0338(12) -0.0002(10) 0.0111(10) -0.0022(10) C24 0.0217(12) 0.0614(18) 0.0425(14) -0.0013(13) 0.0097(11) -0.0014(11) C25 0.0240(12) 0.0633(19) 0.0463(15) -0.0132(13) 0.0124(11) -0.0138(12) C26 0.0313(13) 0.0478(15) 0.0426(14) -0.0099(12) 0.0175(11) -0.0155(11) C27 0.0283(11) 0.0365(13) 0.0313(11) -0.0055(10) 0.0138(10) -0.0066(10) C28A 0.026(4) 0.050(4) 0.032(4) 0.004(3) 0.018(3) 0.013(3) C31A 0.026(4) 0.050(5) 0.042(5) 0.011(4) 0.008(4) -0.001(4) C32A 0.043(6) 0.059(5) 0.061(8) -0.001(6) 0.025(6) 0.000(5) C33 0.0371(13) 0.0334(13) 0.0365(13) -0.0007(10) 0.0135(11) -0.0092(10) C37 0.0564(18) 0.062(2) 0.0510(17) -0.0062(15) 0.0286(15) -0.0134(15) P1 0.0226(4) 0.0404(5) 0.0284(4) -0.0032(3) 0.0112(3) -0.0065(3) P2 0.0345(5) 0.0306(4) 0.0271(3) 0.0020(3) 0.0113(3) 0.0014(3) O1 0.0346(18) 0.0286(14) 0.052(2) 0.0018(12) 0.0223(14) -0.0025(10) C17 0.0334(18) 0.034(2) 0.059(2) 0.0012(16) 0.0225(16) 0.0001(15) C18 0.0353(17) 0.059(2) 0.055(2) -0.0056(18) 0.0157(15) -0.0072(16) C19 0.051(2) 0.061(3) 0.055(2) -0.003(2) 0.0248(19) -0.013(2) C20 0.0414(18) 0.0369(17) 0.074(2) 0.0020(16) 0.0303(17) 0.0001(14) C29 0.033(3) 0.035(4) 0.037(3) -0.003(3) 0.006(2) 0.005(3) C30 0.027(2) 0.045(3) 0.035(3) 0.007(2) 0.0123(19) 0.006(2) C34 0.0374(18) 0.0361(18) 0.047(2) 0.0015(15) 0.0206(16) 0.0026(14) C35 0.058(5) 0.040(6) 0.045(3) -0.010(2) 0.020(2) 0.002(3) C36 0.0335(17) 0.0386(18) 0.0426(19) -0.0008(14) 0.0143(15) -0.0070(14) C38 0.073(3) 0.0308(16) 0.051(2) 0.0044(15) 0.0284(18) -0.0021(16) C39 0.150(5) 0.044(2) 0.105(4) -0.009(2) 0.100(4) -0.022(3) C40 0.0292(17) 0.0323(16) 0.061(2) -0.0030(16) 0.0146(16) -0.0013(13) C41 0.0432(18) 0.0406(17) 0.0508(19) -0.0097(15) 0.0126(15) 0.0002(14) P1A 0.053(6) 0.079(7) 0.064(6) 0.028(5) 0.003(5) -0.026(6) P2A 0.056(6) 0.081(9) 0.104(9) -0.043(7) 0.022(6) 0.009(6) O1A 0.032(10) 0.025(7) 0.030(7) -0.010(5) 0.020(6) -0.012(6) C17A 0.039(6) 0.035(7) 0.069(7) 0.007(6) 0.029(6) 0.003(6) C18A 0.041(6) 0.037(6) 0.072(7) 0.005(6) 0.017(6) -0.001(6) C19A 0.069(11) 0.060(11) 0.061(10) -0.008(9) 0.020(9) 0.025(10) C20A 0.043(6) 0.048(6) 0.063(6) 0.023(5) 0.028(5) 0.006(5) C29A 0.029(3) 0.051(5) 0.046(5) 0.014(4) 0.013(3) 0.008(4) C30A 0.047(4) 0.071(5) 0.064(4) 0.017(3) 0.024(3) 0.012(3) C34A 0.042(6) 0.025(5) 0.043(5) 0.001(4) 0.020(5) -0.014(4) C35A 0.057(13) 0.039(18) 0.045(9) 0.003(8) 0.028(10) -0.002(11) C36A 0.061(7) 0.043(7) 0.046(5) 0.003(5) 0.016(6) -0.012(6) C38A 0.045(9) 0.034(8) 0.039(8) -0.001(6) 0.029(7) -0.006(7) C39A 0.12(3) 0.044(13) 0.058(16) -0.005(12) 0.059(18) -0.007(15) C40A 0.040(8) 0.024(7) 0.029(7) -0.008(6) 0.021(6) -0.006(6) C41A 0.062(12) 0.049(12) 0.035(9) -0.025(9) 0.015(8) -0.005(10) O2 0.046(4) 0.072(5) 0.093(6) 0.013(4) 0.034(4) 0.003(3) C42 0.046(4) 0.062(5) 0.080(9) 0.021(7) 0.017(6) -0.001(4) C43 0.037(5) 0.076(7) 0.076(7) -0.002(6) 0.013(5) -0.013(4) C44 0.048(4) 0.058(4) 0.087(6) 0.004(4) 0.030(4) 0.000(3) C45 0.061(5) 0.053(4) 0.143(8) -0.017(5) 0.064(6) -0.016(4) O2A 0.071(6) 0.047(4) 0.097(8) 0.005(5) 0.046(5) 0.005(4) C42A 0.083(7) 0.091(7) 0.075(8) 0.015(8) 0.021(7) 0.010(6) C43A 0.090(11) 0.126(13) 0.123(14) -0.054(10) 0.054(9) -0.035(9) C44A 0.052(5) 0.058(4) 0.085(6) -0.004(4) 0.021(4) 0.013(4) C45A 0.068(6) 0.069(5) 0.107(7) -0.008(5) 0.054(6) -0.010(5) C28 0.015(3) 0.037(3) 0.041(4) 0.006(3) 0.013(3) 0.001(3) C31 0.028(4) 0.034(3) 0.035(4) -0.001(3) 0.001(3) 0.001(3) C32 0.034(4) 0.043(4) 0.037(5) -0.009(4) 0.000(4) 0.006(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ca Ca 0.3641 1.2855 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -2 1 -1 0.1044 0 -2 -1 0.1185 0 2 1 0.0817 1 2 9 0.0848 0 0 -10 0.0997 -5 -8 8 0.1178 -6 -8 -3 0.1077 5 7 -8 0.1343 4 6 6 0.0883 3 -12 -6 0.1093 -1 1 0 0.1029 7 -4 2 0.1015 1 -15 -2 0.1078 -1 2 -1 0.1082 5 -5 5 0.0886 2 -14 1 0.1073 -1 12 -6 0.1205 1 -1 2 0.0843 -8 4 6 0.0945 9 -2 -3 0.1226 0 1 1 0.0724 -4 7 9 0.0852 6 -7 -8 0.1254 8 0 -7 0.1314 6 -3 -10 0.1206 -8 4 2 0.0938 -1 14 -2 0.1111 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Ca1 P1 107.44(5) . 3_666 ? N1 Ca1 P1 131.99(5) . . ? N1 Ca1 P2 96.68(5) . . ? N1 Ca1 P2 148.73(5) . 3_666 ? N1 Ca1 O1 103.53(15) . . ? N1 Ca1 P1A 113.5(3) . . ? N1 Ca1 P1A 124.5(3) . 3_666 ? N1 Ca1 P2A 151.5(2) . 3_666 ? N1 Ca1 P2A 94.1(3) . . ? N1 Ca1 O1A 104.3(9) . . ? N2 Ca1 N1 86.48(6) . . ? N2 Ca1 P1 88.76(5) . . ? N2 Ca1 P1 147.82(5) . 3_666 ? N2 Ca1 P2 109.57(5) . . ? N2 Ca1 P2 119.26(5) . 3_666 ? N2 Ca1 O1 98.53(11) . . ? N2 Ca1 P1A 142.55(19) . 3_666 ? N2 Ca1 P1A 90.2(2) . . ? N2 Ca1 P2A 128.7(3) . . ? N2 Ca1 P2A 102.3(3) . 3_666 ? N2 Ca1 O1A 106.5(6) . . ? P1 Ca1 P1 60.18(2) 3_666 . ? P1 Ca1 P2 41.36(2) 3_666 3_666 ? P1 Ca1 P1A 18.2(3) 3_666 3_666 ? P1 Ca1 P1A 55.52(17) . 3_666 ? P1 Ca1 P2A 24.4(3) . 3_666 ? P1 Ca1 P2A 52.6(2) 3_666 3_666 ? P2 Ca1 P1 41.29(2) . . ? P2 Ca1 P1 41.27(2) 3_666 . ? P2 Ca1 P1 41.49(2) . 3_666 ? P2 Ca1 P2 59.65(2) . 3_666 ? P2 Ca1 P1A 25.1(2) 3_666 3_666 ? P2 Ca1 P1A 52.2(2) . 3_666 ? P2 Ca1 P2A 54.9(2) . 3_666 ? P2 Ca1 P2A 18.7(3) 3_666 3_666 ? O1 Ca1 P1 105.80(9) . 3_666 ? O1 Ca1 P1 124.41(14) . . ? O1 Ca1 P2 90.62(12) . 3_666 ? O1 Ca1 P2 146.23(10) . . ? O1 Ca1 P1A 94.0(3) . 3_666 ? O1 Ca1 P2A 101.8(3) . 3_666 ? P1A Ca1 P2A 40.6(3) . 3_666 ? P2A Ca1 P1A 43.0(4) . . ? P2A Ca1 P2A 59.1(4) . 3_666 ? O1A Ca1 P1A 139.5(8) . . ? O1A Ca1 P2A 99.0(8) . 3_666 ? O1A Ca1 P2A 122.8(6) . . ? C2 N1 Ca1 110.17(15) . . ? C2 N1 C6 117.86(19) . . ? C6 N1 Ca1 130.03(15) . . ? C4 N2 Ca1 111.98(14) . . ? C4 N2 C22 117.72(18) . . ? C22 N2 Ca1 129.32(14) . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? N1 C2 C1 121.1(2) . . ? N1 C2 C3 125.6(2) . . ? C3 C2 C1 113.2(2) . . ? C2 C3 H3 110.7(17) . . ? C4 C3 C2 133.5(2) . . ? C4 C3 H3 114.7(17) . . ? N2 C4 C3 125.1(2) . . ? N2 C4 C5 120.7(2) . . ? C3 C4 C5 114.2(2) . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C7 C6 N1 121.1(2) . . ? C7 C6 C11 119.2(2) . . ? C11 C6 N1 119.6(2) . . ? C6 C7 C8 118.8(2) . . ? C6 C7 C12 122.2(2) . . ? C8 C7 C12 119.0(2) . . ? C7 C8 H8 119.2 . . ? C9 C8 C7 121.6(3) . . ? C9 C8 H8 119.2 . . ? C8 C9 H9 120.2 . . ? C8 C9 C10 119.6(3) . . ? C10 C9 H9 120.2 . . ? C9 C10 H10 119.5 . . ? C9 C10 C11 121.1(3) . . ? C11 C10 H10 119.5 . . ? C6 C11 C17 123.4(3) . . ? C6 C11 C17A 118.4(11) . . ? C10 C11 C6 119.4(2) . . ? C10 C11 C17 117.2(3) . . ? C10 C11 C17A 122.1(11) . . ? C7 C12 H12 106.3 . . ? C7 C12 C13 112.1(2) . . ? C7 C12 C15 112.3(3) . . ? C13 C12 H12 106.3 . . ? C13 C12 C15 113.0(2) . . ? C15 C12 H12 106.3 . . ? C12 C13 H13A 108.4 . . ? C12 C13 H13B 108.4 . . ? H13A C13 H13B 107.5 . . ? C14 C13 C12 115.3(3) . . ? C14 C13 H13A 108.4 . . ? C14 C13 H13B 108.4 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C12 C15 H15A 108.1 . . ? C12 C15 H15B 108.1 . . ? H15A C15 H15B 107.3 . . ? C16 C15 C12 116.7(3) . . ? C16 C15 H15A 108.1 . . ? C16 C15 H15B 108.1 . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? H21D C21 H21E 109.5 . . ? H21D C21 H21F 109.5 . . ? H21E C21 H21F 109.5 . . ? C20 C21 H21A 109.5 . . ? C20 C21 H21B 109.5 . . ? C20 C21 H21C 109.5 . . ? C20A C21 H21D 109.5 . . ? C20A C21 H21E 109.5 . . ? C20A C21 H21F 109.5 . . ? C23 C22 N2 120.4(2) . . ? C27 C22 N2 118.6(2) . . ? C27 C22 C23 120.9(2) . . ? C22 C23 C28A 120.3(7) . . ? C22 C23 C28 122.8(6) . . ? C24 C23 C22 117.4(2) . . ? C24 C23 C28A 122.1(7) . . ? C24 C23 C28 119.5(6) . . ? C23 C24 H24 119.0 . . ? C25 C24 C23 122.1(3) . . ? C25 C24 H24 119.0 . . ? C24 C25 H25 120.1 . . ? C24 C25 C26 119.9(2) . . ? C26 C25 H25 120.1 . . ? C25 C26 H26 119.4 . . ? C25 C26 C27 121.3(3) . . ? C27 C26 H26 119.4 . . ? C22 C27 C33 120.8(2) . . ? C26 C27 C22 118.3(2) . . ? C26 C27 C33 120.7(2) . . ? C23 C28A H28A 109.8 . . ? C23 C28A C31A 107.3(13) . . ? C23 C28A C29A 108.1(9) . . ? C31A C28A H28A 109.8 . . ? C31A C28A C29A 111.9(9) . . ? C29A C28A H28A 109.8 . . ? C28A C31A H31A 107.5 . . ? C28A C31A H31B 107.5 . . ? C28A C31A C32A 119.2(13) . . ? H31A C31A H31B 107.0 . . ? C32A C31A H31A 107.5 . . ? C32A C31A H31B 107.5 . . ? C31A C32A H32A 109.5 . . ? C31A C32A H32B 109.5 . . ? C31A C32A H32C 109.5 . . ? H32A C32A H32B 109.5 . . ? H32A C32A H32C 109.5 . . ? H32B C32A H32C 109.5 . . ? C27 C33 H33 106.9 . . ? C27 C33 H33A 106.9 . . ? C27 C33 C34 110.8(2) . . ? C27 C33 C36 116.2(2) . . ? C34 C33 H33 106.9 . . ? C36 C33 H33 106.9 . . ? C36 C33 C34 108.7(2) . . ? C34A C33 C27 106.6(5) . . ? C34A C33 H33A 106.9 . . ? C34A C33 C36A 115.6(6) . . ? C36A C33 C27 113.4(6) . . ? C36A C33 H33A 106.9 . . ? H37A C37 H37B 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? H37D C37 H37E 109.5 . . ? H37D C37 H37F 109.5 . . ? H37E C37 H37F 109.5 . . ? C36 C37 H37A 109.5 . . ? C36 C37 H37B 109.5 . . ? C36 C37 H37C 109.5 . . ? C36A C37 H37D 109.5 . . ? C36A C37 H37E 109.5 . . ? C36A C37 H37F 109.5 . . ? Ca1 P1 Ca1 119.82(2) 3_666 . ? P2 P1 Ca1 68.77(3) . . ? P2 P1 Ca1 69.17(3) 3_666 3_666 ? P2 P1 Ca1 69.51(3) . 3_666 ? P2 P1 Ca1 69.05(3) 3_666 . ? P2 P1 P2 89.39(3) . 3_666 ? Ca1 P2 Ca1 120.35(2) . 3_666 ? P1 P2 Ca1 69.68(3) 3_666 3_666 ? P1 P2 Ca1 69.94(3) . . ? P1 P2 Ca1 69.14(3) . 3_666 ? P1 P2 Ca1 69.34(3) 3_666 . ? P1 P2 P1 90.61(3) . 3_666 ? C38 O1 Ca1 123.3(3) . . ? C38 O1 C40 112.1(3) . . ? C40 O1 Ca1 124.2(3) . . ? C11 C17 H17 107.5 . . ? C11 C17 C18 112.1(3) . . ? C11 C17 C20 111.6(4) . . ? C18 C17 H17 107.5 . . ? C20 C17 H17 107.5 . . ? C20 C17 C18 110.3(4) . . ? C17 C18 H18A 108.7 . . ? C17 C18 H18B 108.7 . . ? H18A C18 H18B 107.6 . . ? C19 C18 C17 114.2(3) . . ? C19 C18 H18A 108.7 . . ? C19 C18 H18B 108.7 . . ? C18 C19 H19A 109.5 . . ? C18 C19 H19B 109.5 . . ? C18 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C21 C20 C17 116.1(3) . . ? C21 C20 H20A 108.3 . . ? C21 C20 H20B 108.3 . . ? C17 C20 H20A 108.3 . . ? C17 C20 H20B 108.3 . . ? H20A C20 H20B 107.4 . . ? H29A C29 H29B 107.6 . . ? C30 C29 H29A 108.7 . . ? C30 C29 H29B 108.7 . . ? C30 C29 C28 114.4(8) . . ? C28 C29 H29A 108.7 . . ? C28 C29 H29B 108.7 . . ? C29 C30 H30A 109.5 . . ? C29 C30 H30B 109.5 . . ? C29 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C33 C34 H34A 108.7 . . ? C33 C34 H34B 108.7 . . ? H34A C34 H34B 107.6 . . ? C35 C34 C33 114.2(6) . . ? C35 C34 H34A 108.7 . . ? C35 C34 H34B 108.7 . . ? C34 C35 H35A 109.5 . . ? C34 C35 H35B 109.5 . . ? C34 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C33 C36 H36A 109.1 . . ? C33 C36 H36B 109.1 . . ? C37 C36 C33 112.5(3) . . ? C37 C36 H36A 109.1 . . ? C37 C36 H36B 109.1 . . ? H36A C36 H36B 107.8 . . ? O1 C38 H38A 109.1 . . ? O1 C38 H38B 109.1 . . ? O1 C38 C39 112.4(4) . . ? H38A C38 H38B 107.9 . . ? C39 C38 H38A 109.1 . . ? C39 C38 H38B 109.1 . . ? C38 C39 H39A 109.5 . . ? C38 C39 H39B 109.5 . . ? C38 C39 H39C 109.5 . . ? H39A C39 H39B 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? O1 C40 H40A 109.0 . . ? O1 C40 H40B 109.0 . . ? O1 C40 C41 113.1(3) . . ? H40A C40 H40B 107.8 . . ? C41 C40 H40A 109.0 . . ? C41 C40 H40B 109.0 . . ? C40 C41 H41A 109.5 . . ? C40 C41 H41B 109.5 . . ? C40 C41 H41C 109.5 . . ? H41A C41 H41B 109.5 . . ? H41A C41 H41C 109.5 . . ? H41B C41 H41C 109.5 . . ? Ca1 P1A Ca1 120.1(3) . 3_666 ? P2A P1A Ca1 68.4(4) . . ? P2A P1A Ca1 74.1(5) 3_666 . ? P2A P1A P2A 89.1(6) 3_666 . ? Ca1 P2A Ca1 120.9(4) . 3_666 ? P1A P2A Ca1 68.6(5) . . ? P1A P2A Ca1 74.8(5) 3_666 . ? P1A P2A P1A 90.9(6) 3_666 . ? C38A O1A Ca1 125.6(14) . . ? C38A O1A C40A 116.7(16) . . ? C40A O1A Ca1 114.8(11) . . ? C11 C17A H17A 109.5 . . ? C11 C17A C18A 110.1(16) . . ? C18A C17A H17A 109.5 . . ? C20A C17A C11 104.8(15) . . ? C20A C17A H17A 109.5 . . ? C20A C17A C18A 113.2(15) . . ? C17A C18A H18C 108.5 . . ? C17A C18A H18D 108.5 . . ? H18C C18A H18D 107.5 . . ? C19A C18A C17A 115.3(17) . . ? C19A C18A H18C 108.5 . . ? C19A C18A H18D 108.5 . . ? C18A C19A H19D 109.5 . . ? C18A C19A H19E 109.5 . . ? C18A C19A H19F 109.5 . . ? H19D C19A H19E 109.5 . . ? H19D C19A H19F 109.5 . . ? H19E C19A H19F 109.5 . . ? C21 C20A H20C 106.6 . . ? C21 C20A H20D 106.6 . . ? C17A C20A C21 122.9(15) . . ? C17A C20A H20C 106.6 . . ? C17A C20A H20D 106.6 . . ? H20C C20A H20D 106.6 . . ? C28A C29A H29C 109.6 . . ? C28A C29A H29D 109.6 . . ? H29C C29A H29D 108.1 . . ? C30A C29A C28A 110.4(8) . . ? C30A C29A H29C 109.6 . . ? C30A C29A H29D 109.6 . . ? C29A C30A H30D 109.5 . . ? C29A C30A H30E 109.5 . . ? C29A C30A H30F 109.5 . . ? H30D C30A H30E 109.5 . . ? H30D C30A H30F 109.5 . . ? H30E C30A H30F 109.5 . . ? C33 C34A H34C 110.5 . . ? C33 C34A H34D 110.5 . . ? C33 C34A C35A 106.3(15) . . ? H34C C34A H34D 108.7 . . ? C35A C34A H34C 110.5 . . ? C35A C34A H34D 110.5 . . ? C34A C35A H35D 109.5 . . ? C34A C35A H35E 109.5 . . ? C34A C35A H35F 109.5 . . ? H35D C35A H35E 109.5 . . ? H35D C35A H35F 109.5 . . ? H35E C35A H35F 109.5 . . ? C33 C36A H36C 108.0 . . ? C33 C36A H36D 108.0 . . ? C37 C36A C33 117.2(7) . . ? C37 C36A H36C 108.0 . . ? C37 C36A H36D 108.0 . . ? H36C C36A H36D 107.2 . . ? O1A C38A H38C 108.6 . . ? O1A C38A H38D 108.6 . . ? O1A C38A C39A 115(2) . . ? H38C C38A H38D 107.6 . . ? C39A C38A H38C 108.6 . . ? C39A C38A H38D 108.6 . . ? C38A C39A H39D 109.5 . . ? C38A C39A H39E 109.5 . . ? C38A C39A H39F 109.5 . . ? H39D C39A H39E 109.5 . . ? H39D C39A H39F 109.5 . . ? H39E C39A H39F 109.5 . . ? O1A C40A H40C 109.4 . . ? O1A C40A H40D 109.4 . . ? O1A C40A C41A 111(2) . . ? H40C C40A H40D 108.0 . . ? C41A C40A H40C 109.4 . . ? C41A C40A H40D 109.4 . . ? C40A C41A H41D 109.5 . . ? C40A C41A H41E 109.5 . . ? C40A C41A H41F 109.5 . . ? H41D C41A H41E 109.5 . . ? H41D C41A H41F 109.5 . . ? H41E C41A H41F 109.5 . . ? C44 O2 C42 115.1(10) . . ? O2 C42 H42A 109.7 . . ? O2 C42 H42B 109.7 . . ? O2 C42 C43 109.8(12) . . ? H42A C42 H42B 108.2 . . ? C43 C42 H42A 109.7 . . ? C43 C42 H42B 109.7 . . ? C42 C43 H43A 109.5 . . ? C42 C43 H43B 109.5 . . ? C42 C43 H43C 109.5 . . ? H43A C43 H43B 109.5 . . ? H43A C43 H43C 109.5 . . ? H43B C43 H43C 109.5 . . ? O2 C44 H44A 108.7 . . ? O2 C44 H44B 108.7 . . ? O2 C44 C45 114.2(8) . . ? H44A C44 H44B 107.6 . . ? C45 C44 H44A 108.7 . . ? C45 C44 H44B 108.7 . . ? C44 C45 H45A 109.5 . . ? C44 C45 H45B 109.5 . . ? C44 C45 H45C 109.5 . . ? H45A C45 H45B 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? C42A O2A C44A 111.5(13) . . ? O2A C42A H42C 109.5 . . ? O2A C42A H42D 109.5 . . ? O2A C42A C43A 110.8(19) . . ? H42C C42A H42D 108.1 . . ? C43A C42A H42C 109.5 . . ? C43A C42A H42D 109.5 . . ? C42A C43A H43D 109.5 . . ? C42A C43A H43E 109.5 . . ? C42A C43A H43F 109.5 . . ? H43D C43A H43E 109.5 . . ? H43D C43A H43F 109.5 . . ? H43E C43A H43F 109.5 . . ? O2A C44A H44C 109.5 . . ? O2A C44A H44D 109.5 . . ? O2A C44A C45A 110.6(8) . . ? H44C C44A H44D 108.1 . . ? C45A C44A H44C 109.5 . . ? C45A C44A H44D 109.5 . . ? C44A C45A H45D 109.5 . . ? C44A C45A H45E 109.5 . . ? C44A C45A H45F 109.5 . . ? H45D C45A H45E 109.5 . . ? H45D C45A H45F 109.5 . . ? H45E C45A H45F 109.5 . . ? C23 C28 C29 117.7(8) . . ? C23 C28 H28 102.9 . . ? C29 C28 H28 102.9 . . ? C31 C28 C23 116.7(11) . . ? C31 C28 C29 111.0(8) . . ? C31 C28 H28 102.9 . . ? C28 C31 H31C 109.5 . . ? C28 C31 H31D 109.5 . . ? C28 C31 C32 110.9(12) . . ? H31C C31 H31D 108.1 . . ? C32 C31 H31C 109.5 . . ? C32 C31 H31D 109.5 . . ? C31 C32 H32D 109.5 . . ? C31 C32 H32E 109.5 . . ? C31 C32 H32F 109.5 . . ? H32D C32 H32E 109.5 . . ? H32D C32 H32F 109.5 . . ? H32E C32 H32F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ca1 N1 2.3533(19) . ? Ca1 N2 2.3413(18) . ? Ca1 P1 3.0683(8) . ? Ca1 P1 3.0482(8) 3_666 ? Ca1 P2 3.0447(8) . ? Ca1 P2 3.0557(8) 3_666 ? Ca1 O1 2.415(3) . ? Ca1 P1A 3.151(12) 3_666 ? Ca1 P1A 2.957(12) . ? Ca1 P2A 2.952(11) . ? Ca1 P2A 3.132(14) 3_666 ? Ca1 O1A 2.385(15) . ? N1 C2 1.328(3) . ? N1 C6 1.441(3) . ? N2 C4 1.322(3) . ? N2 C22 1.438(3) . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? C1 C2 1.526(3) . ? C2 C3 1.420(3) . ? C3 H3 0.91(3) . ? C3 C4 1.419(3) . ? C4 C5 1.517(3) . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C7 1.403(3) . ? C6 C11 1.413(4) . ? C7 C8 1.404(4) . ? C7 C12 1.517(4) . ? C8 H8 0.9500 . ? C8 C9 1.366(5) . ? C9 H9 0.9500 . ? C9 C10 1.378(4) . ? C10 H10 0.9500 . ? C10 C11 1.392(4) . ? C11 C17 1.526(5) . ? C11 C17A 1.526(16) . ? C12 H12 1.0000 . ? C12 C13 1.518(4) . ? C12 C15 1.548(4) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C13 C14 1.509(4) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C15 C16 1.474(5) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C21 H21D 0.9800 . ? C21 H21E 0.9800 . ? C21 H21F 0.9800 . ? C21 C20 1.506(5) . ? C21 C20A 1.570(12) . ? C22 C23 1.417(4) . ? C22 C27 1.415(3) . ? C23 C24 1.397(3) . ? C23 C28A 1.520(11) . ? C23 C28 1.540(9) . ? C24 H24 0.9500 . ? C24 C25 1.376(5) . ? C25 H25 0.9500 . ? C25 C26 1.379(4) . ? C26 H26 0.9500 . ? C26 C27 1.393(3) . ? C27 C33 1.528(4) . ? C28A H28A 1.0000 . ? C28A C31A 1.523(11) . ? C28A C29A 1.553(11) . ? C31A H31A 0.9900 . ? C31A H31B 0.9900 . ? C31A C32A 1.534(11) . ? C32A H32A 0.9800 . ? C32A H32B 0.9800 . ? C32A H32C 0.9800 . ? C33 H33 1.0000 . ? C33 H33A 1.0000 . ? C33 C34 1.559(4) . ? C33 C36 1.547(4) . ? C33 C34A 1.488(8) . ? C33 C36A 1.505(9) . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C37 H37D 0.9800 . ? C37 H37E 0.9800 . ? C37 H37F 0.9800 . ? C37 C36 1.529(4) . ? C37 C36A 1.490(10) . ? P1 P2 2.1584(10) 3_666 ? P1 P2 2.1555(11) . ? O1 C38 1.450(5) . ? O1 C40 1.454(6) . ? C17 H17 1.0000 . ? C17 C18 1.571(6) . ? C17 C20 1.533(6) . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C18 C19 1.510(5) . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9900 . ? C20 H20B 0.9900 . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C29 C30 1.520(8) . ? C29 C28 1.562(10) . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C34 C35 1.528(10) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9900 . ? C36 H36B 0.9900 . ? C38 H38A 0.9900 . ? C38 H38B 0.9900 . ? C38 C39 1.506(6) . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9900 . ? C40 H40B 0.9900 . ? C40 C41 1.510(5) . ? C41 H41A 0.9800 . ? C41 H41B 0.9800 . ? C41 H41C 0.9800 . ? P1A P2A 2.120(19) 3_666 ? P1A P2A 2.166(17) . ? O1A C38A 1.430(15) . ? O1A C40A 1.437(14) . ? C17A H17A 1.0000 . ? C17A C18A 1.534(15) . ? C17A C20A 1.521(15) . ? C18A H18C 0.9900 . ? C18A H18D 0.9900 . ? C18A C19A 1.503(14) . ? C19A H19D 0.9800 . ? C19A H19E 0.9800 . ? C19A H19F 0.9800 . ? C20A H20C 0.9900 . ? C20A H20D 0.9900 . ? C29A H29C 0.9900 . ? C29A H29D 0.9900 . ? C29A C30A 1.511(10) . ? C30A H30D 0.9800 . ? C30A H30E 0.9800 . ? C30A H30F 0.9800 . ? C34A H34C 0.9900 . ? C34A H34D 0.9900 . ? C34A C35A 1.522(15) . ? C35A H35D 0.9800 . ? C35A H35E 0.9800 . ? C35A H35F 0.9800 . ? C36A H36C 0.9900 . ? C36A H36D 0.9900 . ? C38A H38C 0.9900 . ? C38A H38D 0.9900 . ? C38A C39A 1.503(16) . ? C39A H39D 0.9800 . ? C39A H39E 0.9800 . ? C39A H39F 0.9800 . ? C40A H40C 0.9900 . ? C40A H40D 0.9900 . ? C40A C41A 1.497(15) . ? C41A H41D 0.9800 . ? C41A H41E 0.9800 . ? C41A H41F 0.9800 . ? O2 C42 1.427(11) . ? O2 C44 1.423(10) . ? C42 H42A 0.9900 . ? C42 H42B 0.9900 . ? C42 C43 1.500(12) . ? C43 H43A 0.9800 . ? C43 H43B 0.9800 . ? C43 H43C 0.9800 . ? C44 H44A 0.9900 . ? C44 H44B 0.9900 . ? C44 C45 1.483(9) . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? O2A C42A 1.401(12) . ? O2A C44A 1.414(10) . ? C42A H42C 0.9900 . ? C42A H42D 0.9900 . ? C42A C43A 1.487(14) . ? C43A H43D 0.9800 . ? C43A H43E 0.9800 . ? C43A H43F 0.9800 . ? C44A H44C 0.9900 . ? C44A H44D 0.9900 . ? C44A C45A 1.485(11) . ? C45A H45D 0.9800 . ? C45A H45E 0.9800 . ? C45A H45F 0.9800 . ? C28 H28 1.0000 . ? C28 C31 1.513(10) . ? C31 H31C 0.9900 . ? C31 H31D 0.9900 . ? C31 C32 1.522(11) . ? C32 H32D 0.9800 . ? C32 H32E 0.9800 . ? C32 H32F 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ca1 N1 C2 C1 -151.88(19) . . . . ? Ca1 N1 C2 C3 26.9(3) . . . . ? Ca1 N1 C6 C7 59.2(3) . . . . ? Ca1 N1 C6 C11 -120.2(2) . . . . ? Ca1 N2 C4 C3 -21.8(3) . . . . ? Ca1 N2 C4 C5 159.25(18) . . . . ? Ca1 N2 C22 C23 -63.4(3) . . . . ? Ca1 N2 C22 C27 114.3(2) . . . . ? Ca1 O1 C38 C39 -89.4(5) . . . . ? Ca1 O1 C40 C41 -108.3(4) . . . . ? Ca1 O1A C38A C39A 94(3) . . . . ? Ca1 O1A C40A C41A 115(2) . . . . ? N1 C2 C3 C4 18.1(4) . . . . ? N1 C6 C7 C8 176.8(2) . . . . ? N1 C6 C7 C12 -1.2(4) . . . . ? N1 C6 C11 C10 -175.7(3) . . . . ? N1 C6 C11 C17 5.6(4) . . . . ? N1 C6 C11 C17A 1.3(10) . . . . ? N2 C22 C23 C24 -179.1(2) . . . . ? N2 C22 C23 C28A 5.9(7) . . . . ? N2 C22 C23 C28 -5.8(7) . . . . ? N2 C22 C27 C26 179.2(2) . . . . ? N2 C22 C27 C33 -5.6(3) . . . . ? C1 C2 C3 C4 -163.1(3) . . . . ? C2 N1 C6 C7 -103.3(3) . . . . ? C2 N1 C6 C11 77.3(3) . . . . ? C2 C3 C4 N2 -21.7(4) . . . . ? C2 C3 C4 C5 157.2(3) . . . . ? C4 N2 C22 C23 104.2(3) . . . . ? C4 N2 C22 C27 -78.0(3) . . . . ? C6 N1 C2 C1 13.9(3) . . . . ? C6 N1 C2 C3 -167.4(2) . . . . ? C6 C7 C8 C9 -0.2(5) . . . . ? C6 C7 C12 C13 85.5(3) . . . . ? C6 C7 C12 C15 -146.0(3) . . . . ? C6 C11 C17 C18 -104.5(4) . . . . ? C6 C11 C17 C20 131.1(4) . . . . ? C6 C11 C17A C18A -148.5(13) . . . . ? C6 C11 C17A C20A 89.5(17) . . . . ? C7 C6 C11 C10 4.9(4) . . . . ? C7 C6 C11 C17 -173.8(3) . . . . ? C7 C6 C11 C17A -178.1(10) . . . . ? C7 C8 C9 C10 3.2(6) . . . . ? C7 C12 C13 C14 63.2(4) . . . . ? C7 C12 C15 C16 167.9(3) . . . . ? C8 C7 C12 C13 -92.4(3) . . . . ? C8 C7 C12 C15 36.1(3) . . . . ? C8 C9 C10 C11 -2.1(6) . . . . ? C9 C10 C11 C6 -2.0(5) . . . . ? C9 C10 C11 C17 176.8(4) . . . . ? C9 C10 C11 C17A -178.8(11) . . . . ? C10 C11 C17 C18 76.7(5) . . . . ? C10 C11 C17 C20 -47.7(5) . . . . ? C10 C11 C17A C18A 28(2) . . . . ? C10 C11 C17A C20A -93.6(14) . . . . ? C11 C6 C7 C8 -3.8(4) . . . . ? C11 C6 C7 C12 178.2(3) . . . . ? C11 C17 C18 C19 170.2(4) . . . . ? C11 C17 C20 C21 -50.9(5) . . . . ? C11 C17A C18A C19A 164(2) . . . . ? C11 C17A C20A C21 49(2) . . . . ? C12 C7 C8 C9 177.8(3) . . . . ? C13 C12 C15 C16 -64.1(4) . . . . ? C15 C12 C13 C14 -64.9(4) . . . . ? C22 N2 C4 C3 168.4(2) . . . . ? C22 N2 C4 C5 -10.5(3) . . . . ? C22 C23 C24 C25 -0.9(4) . . . . ? C22 C23 C28A C31A -91.0(10) . . . . ? C22 C23 C28A C29A 148.2(7) . . . . ? C22 C23 C28 C29 152.3(8) . . . . ? C22 C23 C28 C31 -71.9(12) . . . . ? C22 C27 C33 C34 -80.0(3) . . . . ? C22 C27 C33 C36 155.3(2) . . . . ? C22 C27 C33 C34A -134.4(4) . . . . ? C22 C27 C33 C36A 97.2(5) . . . . ? C23 C22 C27 C26 -3.0(3) . . . . ? C23 C22 C27 C33 172.2(2) . . . . ? C23 C24 C25 C26 -1.5(4) . . . . ? C23 C28A C31A C32A -61.8(16) . . . . ? C23 C28A C29A C30A -174.5(9) . . . . ? C23 C28 C31 C32 -65.6(14) . . . . ? C24 C23 C28A C31A 94.3(10) . . . . ? C24 C23 C28A C29A -26.6(13) . . . . ? C24 C23 C28 C29 -34.5(13) . . . . ? C24 C23 C28 C31 101.2(10) . . . . ? C24 C25 C26 C27 1.7(4) . . . . ? C25 C26 C27 C22 0.5(4) . . . . ? C25 C26 C27 C33 -174.7(2) . . . . ? C26 C27 C33 C34 95.1(3) . . . . ? C26 C27 C33 C36 -29.6(4) . . . . ? C26 C27 C33 C34A 40.7(5) . . . . ? C26 C27 C33 C36A -87.7(5) . . . . ? C27 C22 C23 C24 3.2(4) . . . . ? C27 C22 C23 C28A -171.8(7) . . . . ? C27 C22 C23 C28 176.5(7) . . . . ? C27 C33 C34 C35 -59.2(6) . . . . ? C27 C33 C36 C37 -62.7(3) . . . . ? C27 C33 C34A C35A 67(2) . . . . ? C27 C33 C36A C37 65.2(10) . . . . ? C28A C23 C24 C25 174.0(7) . . . . ? C31A C28A C29A C30A 67.5(15) . . . . ? C18 C17 C20 C21 -176.2(3) . . . . ? C20 C17 C18 C19 -64.7(5) . . . . ? C29 C28 C31 C32 73.0(16) . . . . ? C30 C29 C28 C23 -54.4(14) . . . . ? C30 C29 C28 C31 167.5(10) . . . . ? C34 C33 C36 C37 171.5(3) . . . . ? C36 C33 C34 C35 69.6(6) . . . . ? C38 O1 C40 C41 78.8(4) . . . . ? C40 O1 C38 C39 83.7(4) . . . . ? C18A C17A C20A C21 -71(2) . . . . ? C20A C17A C18A C19A -79(2) . . . . ? C29A C28A C31A C32A 56.6(19) . . . . ? C34A C33 C36A C37 -58.4(12) . . . . ? C36A C33 C34A C35A -166(2) . . . . ? C38A O1A C40A C41A -83(3) . . . . ? C40A O1A C38A C39A -66(3) . . . . ? C42 O2 C44 C45 77.3(14) . . . . ? C44 O2 C42 C43 -176.1(13) . . . . ? C42A O2A C44A C45A -176.6(15) . . . . ? C44A O2A C42A C43A -174.3(19) . . . . ? C28 C23 C24 C25 -174.4(7) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -1.9984 0.9998 -0.9991 0.1942 0.0451 0.2356 -0.0006 -1.9988 -0.9992 -0.0992 -0.0237 0.1363 0.0006 1.9988 0.9992 0.0992 0.0237 -0.1363 1.1140 1.7437 8.8731 0.0807 -0.4403 -0.8942 0.1033 -0.0265 -9.5474 -0.1089 0.5915 0.7989 -5.4762 -7.6346 8.0007 0.1829 -0.9831 0.0064 -5.6325 -8.0511 -2.7079 0.0654 -0.3442 0.9366 5.3583 7.4641 -8.1717 -0.1828 0.9829 0.0229 4.0246 5.8234 5.8242 -0.0030 0.0088 -1.0000 2.5466 -11.9880 -6.0534 -0.7999 -0.0629 0.5968 -0.9990 0.9995 0.0000 0.1245 0.0130 0.0626 7.1437 -3.5712 1.8914 -0.7115 -0.0572 -0.7004 0.6869 -14.7233 -1.7573 -0.7277 -0.5004 0.4692 -0.9990 1.9996 -0.9989 0.1585 0.1175 0.1212 4.8702 -4.8615 5.1506 -0.5527 -0.3812 -0.7411 1.6505 -14.3299 1.3333 -0.7552 -0.6458 0.1122 -0.5011 11.8867 -5.5358 0.5108 0.8350 0.2046 0.9994 -1.0005 1.9981 -0.1037 -0.1365 -0.2316 -8.1567 4.0837 5.8099 0.8957 -0.4266 0.1256 8.6781 -1.5377 -3.0290 -0.7953 0.3792 -0.4729 0.0004 0.9992 0.9991 0.0548 -0.0190 -0.1104 -4.4236 7.1815 8.7286 0.7646 -0.3635 -0.5322 5.6801 -6.6560 -8.3270 -0.8377 0.3985 0.3733 8.2967 0.4656 -6.6255 -0.7132 0.6756 -0.1869 5.6421 -2.7313 -9.5078 -0.6726 0.6381 0.3748 -8.3235 3.7572 1.9134 0.8539 -0.2049 0.4783 -0.8785 14.3183 -2.2003 0.6838 0.7218 -0.1070