#------------------------------------------------------------------------------ #$Date: 2025-02-06 01:11:20 +0200 (Thu, 06 Feb 2025) $ #$Revision: 297604 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/38/1573855.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573855 loop_ _publ_author_name 'Thum, Stefan' 'Townrow, Oliver' 'Langer, Jens' 'Harder, Sjoerd' _publ_section_title ; Tuning the Selectivity of P4 Reduction at Alkaline-Earth Metal Centres ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC08502G _journal_year 2025 _chemical_formula_moiety 'C126 H201 Ca3 N6 O3 P7, 1(C5 H10 O)' _chemical_formula_sum 'C131 H211 Ca3 N6 O4 P7' _chemical_formula_weight 2271.08 _chemical_properties_physical Air-sensitive,Moisture-sensitive _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2024-12-03 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-12-04 deposited with the CCDC. 2025-02-05 downloaded from the CCDC. ; _cell_angle_alpha 70.084(2) _cell_angle_beta 81.755(2) _cell_angle_gamma 64.564(3) _cell_formula_units_Z 2 _cell_length_a 20.4699(6) _cell_length_b 20.4809(5) _cell_length_c 21.4594(5) _cell_measurement_reflns_used 37090 _cell_measurement_temperature 100.0(2) _cell_measurement_theta_max 72.5740 _cell_measurement_theta_min 3.8600 _cell_volume 7638.6(4) _computing_cell_refinement 'CrysAlisPro 1.171.43.106a (Rigaku OD, 2024)' _computing_data_collection 'CrysAlisPro system (CCD 43.105a 64-bit (release 11-01-2024))' _computing_data_reduction 'CrysAlisPro 1.171.43.106a (Rigaku OD, 2024)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.0(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2903 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.969 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -70.00 32.00 1.00 8.00 -- -41.40 57.00 60.00 102 2 \w -114.00 -13.00 1.00 8.00 -- -41.40 -57.00 -90.00 101 3 \w -66.00 33.00 1.00 8.00 -- -41.40 38.00-150.00 99 4 \w -86.00 -6.00 1.00 8.00 -- -41.40 125.00 120.00 80 5 \w 33.00 113.00 1.00 32.00 -- 104.66-125.00-180.00 80 6 \w 33.00 113.00 1.00 32.00 -- 104.66-125.00 0.00 80 7 \w 76.00 178.00 1.00 32.00 -- 104.66 30.00 120.00 102 8 \w 28.00 133.00 1.00 32.00 -- 104.66 -30.00 150.00 105 9 \w 76.00 178.00 1.00 32.00 -- 104.66 30.00-150.00 102 10 \w 97.00 176.00 1.00 32.00 -- 104.66 125.00 120.00 79 11 \w 32.00 134.00 1.00 32.00 -- 104.66 -61.00 30.00 102 12 \w 33.00 113.00 1.00 32.00 -- 104.66-125.00-180.00 80 13 \w 22.00 106.00 1.00 32.00 -- 104.66 -94.00 30.00 84 14 \w 29.00 137.00 1.00 32.00 -- 104.66 -77.00 150.00 108 15 \w -114.00 -13.00 1.00 8.00 -- -41.40 -57.00 150.00 101 16 \w -114.00 -13.00 1.00 8.00 -- -41.40 -57.00 -30.00 101 17 \w -114.00 -13.00 1.00 8.00 -- -41.40 -57.00 60.00 101 18 \w 6.00 81.00 1.00 8.00 -- 41.40 -99.00 -90.00 75 19 \w 76.00 130.00 1.00 32.00 -- 104.66 61.00 30.00 54 20 \w 52.00 178.00 1.00 32.00 -- 104.66 15.00 -30.00 126 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0707804000 _diffrn_orient_matrix_UB_12 0.0561669000 _diffrn_orient_matrix_UB_13 0.0214925000 _diffrn_orient_matrix_UB_21 -0.0091260000 _diffrn_orient_matrix_UB_22 0.0574500000 _diffrn_orient_matrix_UB_23 -0.0702054000 _diffrn_orient_matrix_UB_31 -0.0430372000 _diffrn_orient_matrix_UB_32 -0.0350993000 _diffrn_orient_matrix_UB_33 -0.0209659000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0293 _diffrn_reflns_av_unetI/netI 0.0296 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.969 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 85219 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.969 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.723 _diffrn_reflns_theta_min 3.817 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.970 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.464 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.43.106a (Rigaku Oxford Diffraction, 2024) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 0.987 _exptl_crystal_description block _exptl_crystal_F_000 2472 _exptl_crystal_size_max 0.297 _exptl_crystal_size_mid 0.189 _exptl_crystal_size_min 0.145 _refine_diff_density_max 0.526 _refine_diff_density_min -0.427 _refine_diff_density_rms 0.039 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.052 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 1589 _refine_ls_number_reflns 29465 _refine_ls_number_restraints 623 _refine_ls_restrained_S_all 1.053 _refine_ls_R_factor_all 0.0424 _refine_ls_R_factor_gt 0.0369 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0510P)^2^+1.5889P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0955 _refine_ls_wR_factor_ref 0.0991 _reflns_Friedel_coverage 0.000 _reflns_number_gt 25778 _reflns_number_total 29465 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4sc08502g2.cif _cod_data_source_block hasj240506a _cod_original_cell_volume 7638.7(4) _cod_database_code 1573855 _shelx_shelxl_version_number 2019/3 _chemical_oxdiff_formula C131H211Ca3N6O4P7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C136-O4A \\sim O4A-C132 \\sim O4-C131 \\sim O4-C127 with sigma of 0.02 C127-C128 \\sim C129-C128 \\sim C129-C130 \\sim C130-C131 \\sim C133-C132 \\sim C133-C134 \\sim C135- C134 \\sim C136-C135 with sigma of 0.02 C128-O4 \\sim O4-C130 \\sim C133-O4A \\sim O4A-C135 with sigma of 0.02 C134-O4A \\sim O4-C129 with sigma of 0.02 C127-C129 \\sim C129-C131 \\sim C132-C134 \\sim C134-C136 with sigma of 0.02 C69-C64 \\sim C65-C64 \\sim C65A-C64 with sigma of 0.02 C66A-C65A \\sim C66-C65 \\sim C69-C68A \\sim C69-C68 with sigma of 0.02 C67-C66 \\sim C67A-C66A \\sim C68-C67 \\sim C68A-C67A with sigma of 0.02 C70-C65 \\sim C70A-C65A \\sim C27-C33A \\sim C27-C33 with sigma of 0.01 C65-C68 \\sim C65A-C68A with sigma of 0.02 C67A-C64 \\sim C64-C67 with sigma of 0.02 C66-C68 \\sim C66A-C68A with sigma of 0.02 3. Restrained planarity C65, C66, C67, C68, C69, C64 with sigma of 0.1 C65A, C64, C69, C68A, C67A, C66A with sigma of 0.1 4. Uiso/Uaniso restraints and constraints O4A \\sim C132 \\sim C133 \\sim C134 \\sim C135 \\sim C136 \\sim O4 \\sim C127 \\sim C128 \\sim C129 \\sim C130 \\sim C131: within 3A with sigma of 0.03 and sigma for terminal atoms of 0.06 within 3A C70 \\sim C70A \\sim C65 \\sim C65A \\sim C64 \\sim C66 \\sim C66A \\sim C67 \\sim C67A \\sim C68 \\sim C68A \\sim C69: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A 5. Rigid body (RIGU) restrains O4A, C132, C133, C134, C135, C136 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Others Sof(C70A)=Sof(H70A)=Sof(C71A)=Sof(H71c)=Sof(H71d)=Sof(C72A)=Sof(H72d)= Sof(H72e)=Sof(H72f)=Sof(C73A)=Sof(H73c)=Sof(H73d)=Sof(C74A)=Sof(H74d)= Sof(H74e)=Sof(H74f)=Sof(C68A)=Sof(H68A)=Sof(C67A)=Sof(H67A)=Sof(C66A)= Sof(H66A)=Sof(C65A)=1-FVAR(1) Sof(C65)=Sof(C66)=Sof(H66)=Sof(C67)=Sof(H67)=Sof(C68)=Sof(H68)=Sof(C70)= Sof(H70)=Sof(C71)=Sof(H71a)=Sof(H71b)=Sof(C72)=Sof(H72a)=Sof(H72b)=Sof(H72c)= Sof(C73)=Sof(H73a)=Sof(H73b)=Sof(C74)=Sof(H74a)=Sof(H74b)=Sof(H74c)=FVAR(1) Sof(C33A)=Sof(H33A)=Sof(C34A)=Sof(H34c)=Sof(H34d)=Sof(C35A)=Sof(H35d)= Sof(H35e)=Sof(H35f)=Sof(C36A)=Sof(H36c)=Sof(H36d)=Sof(C37A)=Sof(H37d)= Sof(H37e)=Sof(H37f)=1-FVAR(2) Sof(C33)=Sof(H33)=Sof(C34)=Sof(H34a)=Sof(H34b)=Sof(C35)=Sof(H35a)=Sof(H35b)= Sof(H35c)=Sof(C36)=Sof(H36a)=Sof(H36b)=Sof(C37)=Sof(H37a)=Sof(H37b)=Sof(H37c)= FVAR(2) Sof(O4A)=Sof(C132)=Sof(H13c)=Sof(H13d)=Sof(C133)=Sof(H13e)=Sof(H13f)= Sof(C134)=Sof(H13g)=Sof(H13h)=Sof(C135)=Sof(H13i)=Sof(H13j)=Sof(C136)= Sof(H13k)=Sof(H13l)=1-FVAR(3) Sof(O4)=Sof(C127)=Sof(H12p)=Sof(H12q)=Sof(C128)=Sof(H12r)=Sof(H12s)=Sof(C129)= Sof(H12t)=Sof(H12u)=Sof(C130)=Sof(H13m)=Sof(H13n)=Sof(C131)=Sof(H13o)= Sof(H13p)=FVAR(3) 7.a Ternary CH refined with riding coordinates: C12(H12), C17(H17), C28(H28), C54(H54), C59(H59), C75(H75), C96(H96), C101(H101), C112(H112), C117(H117), C33(H33), C70(H70), C33A(H33A), C70A(H70A) 7.b Secondary CH2 refined with riding coordinates: C13(H13a,H13b), C15(H15a,H15b), C18(H18a,H18b), C20(H20a,H20b), C29(H29a, H29b), C31(H31a,H31b), C38(H38a,H38b), C39(H39a,H39b), C40(H40a,H40b), C41(H41a,H41b), C42(H42a,H42b), C55(H55a,H55b), C57(H57a,H57b), C60(H60a,H60b), C62(H62a,H62b), C76(H76a,H76b), C78(H78a,H78b), C80(H80a,H80b), C81(H81a, H81b), C82(H82a,H82b), C83(H83a,H83b), C84(H84a,H84b), C97(H97a,H97b), C99(H99a,H99b), C102(H10d,H10e), C104(H10i,H10j), C113(H11a,H11b), C115(H11f, H11g), C118(H11k,H11l), C120(H12a,H12b), C122(H12f,H12g), C123(H12h,H12i), C124(H12j,H12k), C125(H12l,H12m), C126(H12n,H12o), C34(H34a,H34b), C36(H36a, H36b), C71(H71a,H71b), C73(H73a,H73b), C34A(H34c,H34d), C36A(H36c,H36d), C71A(H71c,H71d), C73A(H73c,H73d), C132(H13c,H13d), C133(H13e,H13f), C134(H13g, H13h), C135(H13i,H13j), C136(H13k,H13l), C127(H12p,H12q), C128(H12r,H12s), C129(H12t,H12u), C130(H13m,H13n), C131(H13o,H13p) 7.c Aromatic/amide H refined with riding coordinates: C8(H8), C9(H9), C10(H10), C24(H24), C25(H25), C26(H26), C50(H50), C51(H51), C52(H52), C66(H66), C67(H67), C68(H68), C92(H92), C93(H93), C94(H94), C108(H108), C109(H109), C110(H110), C68A(H68A), C67A(H67A), C66A(H66A) 7.d Idealised Me refined as rotating group: C1(H1a,H1b,H1c), C5(H5a,H5b,H5c), C14(H14a,H14b,H14c), C16(H16a,H16b,H16c), C19(H19a,H19b,H19c), C21(H21a,H21b,H21c), C30(H30a,H30b,H30c), C32(H32a,H32b, H32c), C43(H43a,H43b,H43c), C47(H47a,H47b,H47c), C56(H56a,H56b,H56c), C58(H58a, H58b,H58c), C61(H61a,H61b,H61c), C63(H63a,H63b,H63c), C77(H77a,H77b,H77c), C79(H79a,H79b,H79c), C85(H85a,H85b,H85c), C89(H89a,H89b,H89c), C98(H98a,H98b, H98c), C100(H10a,H10b,H10c), C103(H10f,H10g,H10h), C105(H10k,H10l,H10m), C114(H11c,H11d,H11e), C116(H11h,H11i,H11j), C119(H11m,H11n,H11o), C121(H12c, H12d,H12e), C35(H35a,H35b,H35c), C37(H37a,H37b,H37c), C72(H72a,H72b,H72c), C74(H74a,H74b,H74c), C35A(H35d,H35e,H35f), C37A(H37d,H37e,H37f), C72A(H72d, H72e,H72f), C74A(H74d,H74e,H74f) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL hasj240506a_a.res in P-1 hasj240506a.res created by SHELXL-2019/3 at 16:04:52 on 02-Dec-2024 REM Old TITL hasj240506a in P-1 REM SHELXT solution in P-1: R1 0.175, Rweak 0.010, Alpha 0.088 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C57 C11 O8 P7 CELL 1.54184 20.469911 20.480922 21.459449 70.0843 81.7552 64.5639 ZERR 2 0.000553 0.00054 0.000493 0.0023 0.0021 0.0026 LATT 1 SFAC C H Ca N O P UNIT 262 422 6 12 8 14 SADI C136 O4A O4A C132 O4 C131 O4 C127 SADI C127 C128 C129 C128 C129 C130 C130 C131 C133 C132 C133 C134 C135 C134 = C136 C135 SADI C128 O4 O4 C130 C133 O4A O4A C135 SADI C134 O4A O4 C129 SADI C127 C129 C129 C131 C132 C134 C134 C136 SIMU 0.03 0.06 3 O4A > C131 RIGU O4A > C136 SADI C69 C64 C65 C64 C65A C64 SADI C66A C65A C66 C65 C69 C68A C69 C68 SADI C67 C66 C67A C66A C68 C67 C68A C67A SADI 0.01 C70 C65 C70A C65A C27 C33A C27 C33 SADI C65 C68 C65A C68A SIMU C70 C70A C65 C65A C64 C66 C66A C67 C67A C68 C68A C69 SADI C67A C64 C64 C67 SADI C66 C68 C66A C68A FLAT C65 C66 C67 C68 C69 C64 FLAT C65A C64 C69 C68A C67A C66A L.S. 10 PLAN 89 TEMP -173 CONF MORE -1 BOND $H ABIN fmap 2 acta OMIT -1 1 1 OMIT -1 2 2 OMIT 0 2 1 OMIT 0 2 2 REM REM REM WGHT 0.051000 1.588900 FVAR 0.26355 0.53417 0.76236 0.73731 CA1 3 0.855352 0.709668 0.218278 11.00000 0.02631 0.01890 = 0.02791 -0.00211 -0.00560 -0.01100 CA2 3 0.549336 0.738732 0.207370 11.00000 0.02493 0.02283 = 0.02967 -0.00138 -0.00441 -0.01210 CA3 3 0.793406 0.429854 0.317836 11.00000 0.02841 0.01848 = 0.02817 -0.00211 -0.00537 -0.01021 P1 6 0.724924 0.693450 0.156704 11.00000 0.02849 0.02314 = 0.02665 0.00020 -0.00659 -0.01248 P2 6 0.698317 0.590699 0.190675 11.00000 0.02975 0.02323 = 0.03050 -0.00470 -0.00612 -0.01277 P3 6 0.813181 0.575853 0.197584 11.00000 0.02787 0.02199 = 0.02989 -0.00396 -0.00211 -0.01119 P4 6 0.692179 0.740076 0.238182 11.00000 0.02661 0.01893 = 0.03155 -0.00246 -0.00613 -0.01022 P5 6 0.657299 0.582684 0.290361 11.00000 0.02658 0.02118 = 0.03143 -0.00191 -0.00325 -0.01189 P6 6 0.827102 0.567108 0.298434 11.00000 0.02702 0.01974 = 0.03010 -0.00027 -0.00787 -0.01058 P7 6 0.715608 0.635074 0.320557 11.00000 0.02986 0.02171 = 0.02640 -0.00267 -0.00441 -0.01136 O1 5 0.973387 0.644367 0.267083 11.00000 0.03062 0.02626 = 0.03753 -0.00204 -0.01157 -0.01129 O2 5 0.492235 0.871154 0.195189 11.00000 0.03030 0.02256 = 0.04320 -0.00185 -0.00702 -0.01084 O3 5 0.719737 0.361431 0.366798 11.00000 0.03819 0.02541 = 0.03948 -0.00479 0.00244 -0.01828 N1 4 0.904804 0.759614 0.112705 11.00000 0.02742 0.02196 = 0.02982 -0.00441 -0.00319 -0.01388 N2 4 0.834641 0.829405 0.228335 11.00000 0.03307 0.02213 = 0.02776 -0.00358 -0.00666 -0.01437 N3 4 0.488265 0.758676 0.110320 11.00000 0.02792 0.02660 = 0.03170 -0.00013 -0.00703 -0.01385 N4 4 0.445473 0.717127 0.260299 11.00000 0.02693 0.03386 = 0.03667 -0.00752 0.00090 -0.01682 N5 4 0.858351 0.340406 0.258986 11.00000 0.03275 0.02008 = 0.02916 -0.00387 -0.00577 -0.01208 N6 4 0.888596 0.341876 0.396767 11.00000 0.03493 0.01758 = 0.02785 -0.00216 -0.00743 -0.00816 C1 1 0.820049 0.824403 0.017589 11.00000 0.03131 0.03007 = 0.02909 -0.00588 -0.00457 -0.01444 AFIX 137 H1A 2 0.825616 0.776784 0.011917 11.00000 -1.50000 H1B 2 0.852315 0.844346 -0.013093 11.00000 -1.50000 H1C 2 0.769831 0.861685 0.008275 11.00000 -1.50000 AFIX 0 C2 1 0.839257 0.809504 0.088410 11.00000 0.03056 0.02002 = 0.02793 -0.00189 -0.00507 -0.01562 C3 1 0.782152 0.849360 0.125219 11.00000 0.02798 0.02107 = 0.02997 -0.00242 -0.00662 -0.01242 H3 2 0.736926 0.876264 0.101673 11.00000 0.03358 C4 1 0.781396 0.867131 0.183803 11.00000 0.03060 0.01872 = 0.03083 -0.00252 -0.00452 -0.01352 C5 1 0.711936 0.930378 0.195210 11.00000 0.03826 0.02530 = 0.03643 -0.00979 -0.00815 -0.00732 AFIX 137 H5A 2 0.683045 0.957456 0.154394 11.00000 -1.50000 H5B 2 0.723447 0.965969 0.207825 11.00000 -1.50000 H5C 2 0.684370 0.908637 0.230793 11.00000 -1.50000 AFIX 0 C6 1 0.959691 0.738360 0.064392 11.00000 0.02628 0.02659 = 0.03089 -0.00446 -0.00360 -0.01212 C7 1 0.996476 0.785897 0.032751 11.00000 0.02820 0.02827 = 0.03787 -0.00458 -0.00218 -0.01492 C8 1 1.045260 0.768285 -0.017542 11.00000 0.03467 0.03363 = 0.04538 -0.00608 0.00449 -0.01906 AFIX 43 H8 2 1.069359 0.800505 -0.039572 11.00000 -1.20000 AFIX 0 C9 1 1.059579 0.705360 -0.036274 11.00000 0.03788 0.03862 = 0.04247 -0.01127 0.01002 -0.01751 AFIX 43 H9 2 1.092146 0.695148 -0.071484 11.00000 -1.20000 AFIX 0 C10 1 1.025987 0.657413 -0.003210 11.00000 0.03711 0.03142 = 0.04082 -0.01182 0.00442 -0.01469 AFIX 43 H10 2 1.036846 0.613299 -0.015249 11.00000 -1.20000 AFIX 0 C11 1 0.976477 0.672213 0.047462 11.00000 0.02883 0.02690 = 0.03291 -0.00546 -0.00090 -0.01369 C12 1 0.984376 0.854811 0.052302 11.00000 0.03333 0.02789 = 0.04238 -0.00539 -0.00312 -0.01798 AFIX 13 H12 2 0.969732 0.844007 0.099970 11.00000 -1.20000 AFIX 0 C13 1 1.054392 0.867371 0.047624 11.00000 0.03985 0.03802 = 0.05923 -0.00898 -0.00410 -0.02493 AFIX 23 H13A 2 1.069980 0.878868 0.000752 11.00000 -1.20000 H13B 2 1.043588 0.912321 0.061581 11.00000 -1.20000 AFIX 0 C14 1 1.116642 0.799644 0.089724 11.00000 0.03592 0.04861 = 0.07316 -0.01254 -0.01053 -0.02267 AFIX 137 H14A 2 1.159187 0.811410 0.083823 11.00000 -1.50000 H14B 2 1.128261 0.754927 0.075929 11.00000 -1.50000 H14C 2 1.102513 0.789040 0.136496 11.00000 -1.50000 AFIX 0 C15 1 0.923059 0.928731 0.013450 11.00000 0.03516 0.02769 = 0.04782 -0.00560 -0.00217 -0.01721 AFIX 23 H15A 2 0.876569 0.923734 0.026025 11.00000 -1.20000 H15B 2 0.921018 0.971129 0.027096 11.00000 -1.20000 AFIX 0 C16 1 0.930322 0.949620 -0.061972 11.00000 0.04132 0.03374 = 0.04774 -0.00088 0.00124 -0.01908 AFIX 137 H16A 2 0.891893 0.999563 -0.082503 11.00000 -1.50000 H16B 2 0.926165 0.911268 -0.076780 11.00000 -1.50000 H16C 2 0.977562 0.951414 -0.074966 11.00000 -1.50000 AFIX 0 C17 1 0.943795 0.615715 0.084452 11.00000 0.03131 0.02580 = 0.03395 -0.00954 0.00229 -0.01463 AFIX 13 H17 2 0.896369 0.644863 0.102465 11.00000 -1.20000 AFIX 0 C18 1 0.991481 0.555966 0.144472 11.00000 0.03579 0.02846 = 0.03902 -0.00808 -0.00156 -0.01493 AFIX 23 H18A 2 0.996439 0.582865 0.172882 11.00000 -1.20000 H18B 2 0.966057 0.523777 0.170693 11.00000 -1.20000 AFIX 0 C19 1 1.067014 0.504111 0.128354 11.00000 0.03923 0.03978 = 0.05111 -0.01082 -0.00481 -0.00774 AFIX 137 H19A 2 1.093364 0.534999 0.103116 11.00000 -1.50000 H19B 2 1.063124 0.475189 0.101949 11.00000 -1.50000 H19C 2 1.093104 0.468812 0.169636 11.00000 -1.50000 AFIX 0 C20 1 0.927850 0.577630 0.041549 11.00000 0.03850 0.03295 = 0.04252 -0.01632 0.00279 -0.01846 AFIX 23 H20A 2 0.973399 0.550869 0.020618 11.00000 -1.20000 H20B 2 0.910586 0.538979 0.070522 11.00000 -1.20000 AFIX 0 C21 1 0.871970 0.632854 -0.012224 11.00000 0.05160 0.04627 = 0.04832 -0.02202 -0.00693 -0.02043 AFIX 137 H21A 2 0.864223 0.604918 -0.037489 11.00000 -1.50000 H21B 2 0.889235 0.670463 -0.042011 11.00000 -1.50000 H21C 2 0.826321 0.658889 0.008059 11.00000 -1.50000 AFIX 0 C22 1 0.831974 0.865699 0.276026 11.00000 0.03554 0.02185 = 0.03187 -0.00520 -0.01026 -0.01131 C23 1 0.802525 0.845943 0.339514 11.00000 0.03121 0.02823 = 0.03544 -0.00917 -0.00694 -0.01094 C24 1 0.796559 0.887138 0.381473 11.00000 0.04025 0.03863 = 0.03792 -0.01599 -0.00226 -0.01633 AFIX 43 H24 2 0.777128 0.874162 0.424584 11.00000 -1.20000 AFIX 0 C25 1 0.818218 0.946563 0.361998 11.00000 0.04620 0.03660 = 0.05043 -0.02204 -0.00721 -0.01613 AFIX 43 H25 2 0.811137 0.975781 0.390497 11.00000 -1.20000 AFIX 0 C26 1 0.850124 0.963008 0.300969 11.00000 0.05296 0.02957 = 0.04424 -0.00943 -0.01172 -0.02080 AFIX 43 H26 2 0.865965 1.003051 0.288127 11.00000 -1.20000 AFIX 0 C27 1 0.859602 0.922090 0.257754 11.00000 0.05481 0.02785 = 0.03324 -0.00312 -0.01158 -0.02192 C28 1 0.780457 0.779529 0.362487 11.00000 0.03952 0.03646 = 0.03165 -0.01154 -0.00168 -0.02090 AFIX 13 H28 2 0.763953 0.776825 0.322127 11.00000 -1.20000 AFIX 0 C29 1 0.847539 0.704579 0.389165 11.00000 0.05029 0.03126 = 0.03843 -0.00798 -0.00573 -0.02070 AFIX 23 H29A 2 0.832886 0.661648 0.401005 11.00000 -1.20000 H29B 2 0.883493 0.698802 0.353059 11.00000 -1.20000 AFIX 0 C30 1 0.883999 0.698414 0.449103 11.00000 0.05964 0.03736 = 0.05067 -0.00877 -0.01925 -0.01872 AFIX 137 H30A 2 0.900787 0.739250 0.437591 11.00000 -1.50000 H30B 2 0.925373 0.648988 0.462716 11.00000 -1.50000 H30C 2 0.849339 0.703031 0.485640 11.00000 -1.50000 AFIX 0 C31 1 0.717424 0.788022 0.411246 11.00000 0.05181 0.05753 = 0.04117 -0.01917 0.00731 -0.03419 AFIX 23 H31A 2 0.707616 0.741852 0.424090 11.00000 -1.20000 H31B 2 0.731588 0.791592 0.451786 11.00000 -1.20000 AFIX 0 C32 1 0.648374 0.857542 0.383317 11.00000 0.04122 0.07438 = 0.06711 -0.03222 0.00958 -0.02817 AFIX 137 H32A 2 0.632862 0.853477 0.344169 11.00000 -1.50000 H32B 2 0.657481 0.903588 0.370816 11.00000 -1.50000 H32C 2 0.610327 0.860318 0.416986 11.00000 -1.50000 AFIX 0 C38 1 1.021025 0.683377 0.247428 11.00000 0.04541 0.03017 = 0.06463 0.00058 -0.02522 -0.02029 AFIX 23 H38A 2 1.027089 0.698328 0.284781 11.00000 -1.20000 H38B 2 0.999195 0.730259 0.209811 11.00000 -1.20000 AFIX 0 C39 1 1.094515 0.632641 0.227152 11.00000 0.03911 0.05280 = 0.07092 0.00490 -0.01365 -0.02756 AFIX 23 H39A 2 1.126831 0.659698 0.215376 11.00000 -1.20000 H39B 2 1.088979 0.620925 0.187610 11.00000 -1.20000 AFIX 0 C40 1 1.128271 0.558604 0.283712 11.00000 0.03497 0.04397 = 0.06130 -0.00695 -0.01558 -0.01262 AFIX 23 H40A 2 1.173091 0.523489 0.268115 11.00000 -1.20000 H40B 2 1.141155 0.569463 0.320710 11.00000 -1.20000 AFIX 0 C41 1 1.075322 0.521510 0.307751 11.00000 0.03770 0.03001 = 0.04425 -0.00451 -0.01528 -0.00904 AFIX 23 H41A 2 1.069104 0.502724 0.273131 11.00000 -1.20000 H41B 2 1.095057 0.477288 0.347914 11.00000 -1.20000 AFIX 0 C42 1 1.002860 0.576875 0.323545 11.00000 0.03620 0.03375 = 0.03688 0.00119 -0.01173 -0.01009 AFIX 23 H42A 2 0.968809 0.551854 0.336971 11.00000 -1.20000 H42B 2 1.008299 0.591655 0.361243 11.00000 -1.20000 AFIX 0 C43 1 0.524095 0.647188 0.071552 11.00000 0.04094 0.03175 = 0.03618 -0.00503 -0.00678 -0.01630 AFIX 137 H43A 2 0.572087 0.644182 0.054757 11.00000 -1.50000 H43B 2 0.488855 0.676882 0.035189 11.00000 -1.50000 H43C 2 0.525495 0.595760 0.090111 11.00000 -1.50000 AFIX 0 C44 1 0.502251 0.685371 0.124951 11.00000 0.02368 0.02826 = 0.03498 -0.00301 -0.00842 -0.01165 C45 1 0.502152 0.636406 0.190347 11.00000 0.02911 0.02362 = 0.03643 -0.00256 -0.00678 -0.01349 H45 2 0.520275 0.584957 0.193504 11.00000 0.02556 C46 1 0.468185 0.650913 0.249371 11.00000 0.02769 0.03196 = 0.03651 -0.00205 -0.00422 -0.01837 C47 1 0.464692 0.581170 0.303010 11.00000 0.05254 0.04023 = 0.04030 -0.00499 0.00330 -0.03151 AFIX 137 H47A 2 0.512856 0.547500 0.322511 11.00000 -1.50000 H47B 2 0.448194 0.553952 0.283534 11.00000 -1.50000 H47C 2 0.430775 0.597130 0.337538 11.00000 -1.50000 AFIX 0 C48 1 0.473326 0.804399 0.041990 11.00000 0.03298 0.02697 = 0.03228 0.00032 -0.01011 -0.01361 C49 1 0.526785 0.822388 -0.000058 11.00000 0.03184 0.02909 = 0.03363 -0.00177 -0.00926 -0.01389 C50 1 0.509711 0.864474 -0.066667 11.00000 0.03671 0.03925 = 0.03401 0.00155 -0.00935 -0.01896 AFIX 43 H50 2 0.545869 0.875688 -0.095565 11.00000 -1.20000 AFIX 0 C51 1 0.441038 0.890187 -0.091411 11.00000 0.04363 0.04261 = 0.03517 0.00605 -0.01707 -0.02054 AFIX 43 H51 2 0.430463 0.918084 -0.136954 11.00000 -1.20000 AFIX 0 C52 1 0.388475 0.874938 -0.049452 11.00000 0.03694 0.04220 = 0.04387 0.00553 -0.01934 -0.01894 AFIX 43 H52 2 0.341183 0.893833 -0.066403 11.00000 -1.20000 AFIX 0 C53 1 0.402479 0.832419 0.017495 11.00000 0.03498 0.03347 = 0.04187 0.00460 -0.01424 -0.01792 C54 1 0.600808 0.800202 0.026198 11.00000 0.03180 0.03091 = 0.02936 0.00239 -0.00935 -0.01591 AFIX 13 H54 2 0.609234 0.755176 0.066865 11.00000 -1.20000 AFIX 0 C55 1 0.599833 0.864438 0.048978 11.00000 0.03222 0.03235 = 0.03550 -0.00097 -0.00902 -0.01584 AFIX 23 H55A 2 0.557961 0.878024 0.078774 11.00000 -1.20000 H55B 2 0.644161 0.844350 0.075319 11.00000 -1.20000 AFIX 0 C56 1 0.595481 0.936906 -0.006047 11.00000 0.03690 0.03206 = 0.04535 0.00046 -0.00925 -0.01583 AFIX 137 H56A 2 0.638066 0.925050 -0.034590 11.00000 -1.50000 H56B 2 0.593960 0.974315 0.013560 11.00000 -1.50000 H56C 2 0.551620 0.957902 -0.032455 11.00000 -1.50000 AFIX 0 C57 1 0.663389 0.775412 -0.020619 11.00000 0.03447 0.03767 = 0.03498 -0.00235 -0.00736 -0.01489 AFIX 23 H57A 2 0.654972 0.817182 -0.063114 11.00000 -1.20000 H57B 2 0.708703 0.766252 -0.001069 11.00000 -1.20000 AFIX 0 C58 1 0.672662 0.703697 -0.034264 11.00000 0.04479 0.05092 = 0.05454 -0.01885 -0.00191 -0.01837 AFIX 137 H58A 2 0.713975 0.689913 -0.063826 11.00000 -1.50000 H58B 2 0.628719 0.713007 -0.055329 11.00000 -1.50000 H58C 2 0.681262 0.661997 0.007579 11.00000 -1.50000 AFIX 0 C59 1 0.342293 0.818462 0.062012 11.00000 0.03439 0.04455 = 0.04784 0.00983 -0.01558 -0.02173 AFIX 13 H59 2 0.356440 0.808075 0.108266 11.00000 -1.20000 AFIX 0 C60 1 0.269992 0.888951 0.047923 11.00000 0.03510 0.04900 = 0.04897 0.00433 -0.01231 -0.02246 AFIX 23 H60A 2 0.251853 0.897959 0.004082 11.00000 -1.20000 H60B 2 0.234378 0.878209 0.081583 11.00000 -1.20000 AFIX 0 C61 1 0.274210 0.961196 0.048330 11.00000 0.03903 0.05270 = 0.05922 -0.00328 -0.00961 -0.02190 AFIX 137 H61A 2 0.302316 0.977643 0.010098 11.00000 -1.50000 H61B 2 0.297764 0.951135 0.089292 11.00000 -1.50000 H61C 2 0.225268 1.001335 0.045863 11.00000 -1.50000 AFIX 0 C62 1 0.333218 0.747857 0.061511 11.00000 0.04052 0.04257 = 0.08106 0.01323 -0.02128 -0.02393 AFIX 23 H62A 2 0.376020 0.702069 0.083420 11.00000 -1.20000 H62B 2 0.290427 0.745394 0.088623 11.00000 -1.20000 AFIX 0 C63 1 0.324270 0.744257 -0.005943 11.00000 0.09389 0.05184 = 0.10553 0.00632 -0.05490 -0.03901 AFIX 137 H63A 2 0.367557 0.743358 -0.032594 11.00000 -1.50000 H63B 2 0.281902 0.789041 -0.028344 11.00000 -1.50000 H63C 2 0.317562 0.698043 -0.000530 11.00000 -1.50000 AFIX 0 C64 1 0.398609 0.729756 0.315327 11.00000 0.03245 0.03575 = 0.03933 -0.00798 0.00379 -0.01807 PART 1 C65 1 0.326204 0.738778 0.315934 21.00000 0.03338 0.03069 = 0.03686 -0.00126 -0.00039 -0.01794 C66 1 0.280131 0.754157 0.367820 21.00000 0.03359 0.02771 = 0.04336 0.00015 0.00627 -0.01826 AFIX 43 H66 2 0.230275 0.765733 0.364818 21.00000 -1.20000 AFIX 0 C67 1 0.306531 0.752629 0.423140 21.00000 0.03792 0.02430 = 0.03864 0.00340 0.00413 -0.00933 AFIX 43 H67 2 0.274684 0.764877 0.458234 21.00000 -1.20000 AFIX 0 C68 1 0.379725 0.733287 0.428670 21.00000 0.04317 0.02723 = 0.04205 0.00368 -0.00293 -0.00994 AFIX 43 H68 2 0.399006 0.725412 0.469627 21.00000 -1.20000 AFIX 0 PART 0 C69 1 0.424985 0.725408 0.374117 11.00000 0.03272 0.02834 = 0.03540 -0.00136 0.00197 -0.01230 C75 1 0.504619 0.704397 0.383565 11.00000 0.03205 0.04138 = 0.03151 -0.00539 0.00023 -0.01141 AFIX 13 H75 2 0.532097 0.677173 0.350970 11.00000 -1.20000 AFIX 0 C76 1 0.520626 0.775231 0.366890 11.00000 0.03942 0.05075 = 0.03846 -0.00624 0.00136 -0.02173 AFIX 23 H76A 2 0.573197 0.758296 0.372379 11.00000 -1.20000 H76B 2 0.508647 0.804676 0.319627 11.00000 -1.20000 AFIX 0 C77 1 0.480238 0.828097 0.408255 11.00000 0.05403 0.05687 = 0.04801 -0.01388 0.00527 -0.03088 AFIX 137 H77A 2 0.493405 0.871708 0.393539 11.00000 -1.50000 H77B 2 0.493307 0.800472 0.455060 11.00000 -1.50000 H77C 2 0.428011 0.846130 0.402786 11.00000 -1.50000 AFIX 0 C78 1 0.534153 0.649429 0.452794 11.00000 0.03892 0.04765 = 0.03418 -0.00534 -0.00335 -0.01160 AFIX 23 H78A 2 0.586469 0.636672 0.454331 11.00000 -1.20000 H78B 2 0.509807 0.675691 0.486159 11.00000 -1.20000 AFIX 0 C79 1 0.523652 0.576412 0.471467 11.00000 0.05868 0.03995 = 0.04147 -0.00199 -0.00410 -0.00758 AFIX 137 H79A 2 0.549243 0.548892 0.439762 11.00000 -1.50000 H79B 2 0.471948 0.588357 0.470627 11.00000 -1.50000 H79C 2 0.542959 0.544662 0.516114 11.00000 -1.50000 AFIX 0 C80 1 0.416172 0.908010 0.177922 11.00000 0.03129 0.02992 = 0.05343 0.00212 -0.01041 -0.00990 AFIX 23 H80A 2 0.398426 0.869025 0.181008 11.00000 -1.20000 H80B 2 0.409709 0.942168 0.131581 11.00000 -1.20000 AFIX 0 C81 1 0.372701 0.953257 0.223205 11.00000 0.04172 0.03704 = 0.07358 -0.00790 0.00961 -0.01103 AFIX 23 H81A 2 0.375799 0.918543 0.269052 11.00000 -1.20000 H81B 2 0.321280 0.979469 0.209353 11.00000 -1.20000 AFIX 0 C82 1 0.400641 1.011945 0.221478 11.00000 0.06659 0.03394 = 0.06917 -0.01706 0.01931 -0.01664 AFIX 23 H82A 2 0.390697 1.051336 0.177439 11.00000 -1.20000 H82B 2 0.375208 1.037197 0.255264 11.00000 -1.20000 AFIX 0 C83 1 0.481740 0.973358 0.235170 11.00000 0.07412 0.03337 = 0.04803 -0.00742 -0.00146 -0.02852 AFIX 23 H83A 2 0.500408 1.012557 0.228438 11.00000 -1.20000 H83B 2 0.490811 0.940448 0.281908 11.00000 -1.20000 AFIX 0 C84 1 0.521244 0.926096 0.190237 11.00000 0.03985 0.02478 = 0.04925 -0.00239 -0.00808 -0.01515 AFIX 23 H84A 2 0.516991 0.959853 0.143869 11.00000 -1.20000 H84B 2 0.573206 0.898977 0.202270 11.00000 -1.20000 AFIX 0 C85 1 0.945450 0.373732 0.175562 11.00000 0.03771 0.02996 = 0.03125 -0.00875 -0.00059 -0.01695 AFIX 137 H85A 2 0.913151 0.422317 0.145670 11.00000 -1.50000 H85B 2 0.951169 0.332178 0.159467 11.00000 -1.50000 H85C 2 0.992785 0.374438 0.176926 11.00000 -1.50000 AFIX 0 C86 1 0.913319 0.361754 0.244638 11.00000 0.03062 0.01716 = 0.03037 -0.00272 -0.00495 -0.00885 C87 1 0.942027 0.380057 0.289159 11.00000 0.02844 0.02159 = 0.03253 -0.00384 -0.00369 -0.01168 H87 2 0.974110 0.400601 0.269436 11.00000 0.02772 C88 1 0.938696 0.361439 0.359808 11.00000 0.03095 0.01664 = 0.03333 -0.00431 -0.00915 -0.00580 C89 1 0.996309 0.369808 0.389972 11.00000 0.03755 0.03113 = 0.03687 -0.00691 -0.01081 -0.01388 AFIX 137 H89A 2 1.033738 0.374473 0.356907 11.00000 -1.50000 H89B 2 1.018142 0.324918 0.428364 11.00000 -1.50000 H89C 2 0.974215 0.415433 0.404105 11.00000 -1.50000 AFIX 0 C90 1 0.847278 0.302345 0.218910 11.00000 0.03468 0.02245 = 0.02960 -0.00543 -0.00085 -0.01539 C91 1 0.789793 0.339349 0.172919 11.00000 0.03294 0.02470 = 0.03041 -0.00559 -0.00084 -0.01603 C92 1 0.779702 0.298080 0.137829 11.00000 0.03768 0.03111 = 0.03698 -0.00851 -0.00402 -0.01829 AFIX 43 H92 2 0.741332 0.322681 0.106537 11.00000 -1.20000 AFIX 0 C93 1 0.824320 0.222439 0.147750 11.00000 0.04863 0.03089 = 0.04398 -0.01402 -0.00212 -0.02178 AFIX 43 H93 2 0.816549 0.195140 0.123646 11.00000 -1.20000 AFIX 0 C94 1 0.880456 0.186419 0.192933 11.00000 0.04734 0.02401 = 0.04510 -0.00992 -0.00639 -0.01297 AFIX 43 H94 2 0.911181 0.134313 0.199194 11.00000 -1.20000 AFIX 0 C95 1 0.893299 0.224387 0.229619 11.00000 0.04107 0.02399 = 0.03621 -0.00602 -0.00450 -0.01437 C96 1 0.737873 0.422016 0.161233 11.00000 0.03111 0.02505 = 0.03483 -0.00706 -0.00618 -0.01321 AFIX 13 H96 2 0.761840 0.444904 0.179798 11.00000 -1.20000 AFIX 0 C97 1 0.666964 0.429685 0.200219 11.00000 0.03337 0.03578 = 0.04052 -0.01113 -0.00147 -0.01614 AFIX 23 H97A 2 0.679506 0.401001 0.247515 11.00000 -1.20000 H97B 2 0.639006 0.483958 0.196966 11.00000 -1.20000 AFIX 0 C98 1 0.617864 0.402438 0.178809 11.00000 0.03924 0.05742 = 0.05763 -0.01967 0.00146 -0.02724 AFIX 137 H98A 2 0.604873 0.430052 0.131988 11.00000 -1.50000 H98B 2 0.573868 0.411957 0.205769 11.00000 -1.50000 H98C 2 0.643273 0.347781 0.184899 11.00000 -1.50000 AFIX 0 C99 1 0.722243 0.469740 0.087859 11.00000 0.03790 0.02824 = 0.03616 -0.00654 -0.00829 -0.01342 AFIX 23 H99A 2 0.706243 0.443838 0.065718 11.00000 -1.20000 H99B 2 0.681985 0.519786 0.085077 11.00000 -1.20000 AFIX 0 C100 1 0.786881 0.482467 0.050937 11.00000 0.04604 0.03307 = 0.03959 -0.00170 -0.00239 -0.01549 AFIX 137 H10A 2 0.772985 0.514374 0.005035 11.00000 -1.50000 H10B 2 0.826154 0.433332 0.051316 11.00000 -1.50000 H10C 2 0.803261 0.507918 0.072609 11.00000 -1.50000 AFIX 0 C101 1 0.954744 0.180720 0.280296 11.00000 0.04762 0.02220 = 0.04313 -0.00634 -0.01284 -0.00967 AFIX 13 H101 2 0.942223 0.208476 0.313634 11.00000 -1.20000 AFIX 0 C102 1 0.961261 0.099304 0.318712 11.00000 0.06335 0.02311 = 0.04593 -0.00592 -0.01729 -0.01078 AFIX 23 H10D 2 0.974705 0.069789 0.287216 11.00000 -1.20000 H10E 2 1.000949 0.074588 0.351527 11.00000 -1.20000 AFIX 0 C103 1 0.893120 0.095646 0.354480 11.00000 0.07254 0.03045 = 0.04725 -0.00317 -0.01439 -0.02431 AFIX 137 H10F 2 0.854771 0.114903 0.322031 11.00000 -1.50000 H10G 2 0.877809 0.126887 0.384131 11.00000 -1.50000 H10H 2 0.902593 0.042777 0.380472 11.00000 -1.50000 AFIX 0 C104 1 1.028509 0.178480 0.251355 11.00000 0.04693 0.03381 = 0.05295 -0.01079 -0.01249 -0.00769 AFIX 23 H10I 2 1.025844 0.230927 0.236667 11.00000 -1.20000 H10J 2 1.065018 0.147632 0.287290 11.00000 -1.20000 AFIX 0 C105 1 1.054994 0.146794 0.193847 11.00000 0.05300 0.06164 = 0.06360 -0.02589 -0.00423 -0.01159 AFIX 137 H10K 2 1.021435 0.179054 0.156418 11.00000 -1.50000 H10L 2 1.057534 0.094979 0.207309 11.00000 -1.50000 H10M 2 1.103165 0.145827 0.180569 11.00000 -1.50000 AFIX 0 C106 1 0.898945 0.313733 0.467538 11.00000 0.03857 0.02425 = 0.02806 -0.00199 -0.00791 -0.01166 C107 1 0.937970 0.235106 0.498279 11.00000 0.04622 0.02312 = 0.03381 -0.00260 -0.01051 -0.00864 C108 1 0.950712 0.209253 0.566275 11.00000 0.06461 0.02273 = 0.03516 0.00086 -0.01651 -0.00721 AFIX 43 H108 2 0.978147 0.156610 0.587292 11.00000 -1.20000 AFIX 0 C109 1 0.924625 0.257921 0.603795 11.00000 0.07011 0.03027 = 0.02921 0.00053 -0.01555 -0.01376 AFIX 43 H109 2 0.935030 0.239207 0.649884 11.00000 -1.20000 AFIX 0 C110 1 0.883188 0.334205 0.573877 11.00000 0.05833 0.02843 = 0.02904 -0.00469 -0.00737 -0.01395 AFIX 43 H110 2 0.863459 0.367331 0.600192 11.00000 -1.20000 AFIX 0 C111 1 0.869693 0.363651 0.505744 11.00000 0.04228 0.02298 = 0.02937 -0.00216 -0.00685 -0.01158 C112 1 0.965155 0.179069 0.458919 11.00000 0.04805 0.02131 = 0.03523 -0.00279 -0.01269 -0.00668 AFIX 13 H112 2 0.929885 0.200588 0.421875 11.00000 -1.20000 AFIX 0 C113 1 1.039041 0.170686 0.426688 11.00000 0.04722 0.02927 = 0.04487 -0.01034 -0.01414 -0.00642 AFIX 23 H11A 2 1.053749 0.132368 0.403312 11.00000 -1.20000 H11B 2 1.033597 0.219837 0.392957 11.00000 -1.20000 AFIX 0 C114 1 1.099381 0.147330 0.474085 11.00000 0.05220 0.05516 = 0.06356 -0.02192 -0.02058 -0.00706 AFIX 137 H11C 2 1.143822 0.145156 0.449000 11.00000 -1.50000 H11D 2 1.107646 0.097110 0.506061 11.00000 -1.50000 H11E 2 1.085580 0.184667 0.497754 11.00000 -1.50000 AFIX 0 C115 1 0.966230 0.100346 0.499407 11.00000 0.06226 0.02094 = 0.04350 -0.00188 -0.01399 -0.00849 AFIX 23 H11F 2 0.982688 0.067863 0.470195 11.00000 -1.20000 H11G 2 1.002303 0.076571 0.535487 11.00000 -1.20000 AFIX 0 C116 1 0.894159 0.100923 0.529830 11.00000 0.07565 0.02792 = 0.05059 -0.00336 -0.00132 -0.01798 AFIX 137 H11H 2 0.857170 0.126865 0.495002 11.00000 -1.50000 H11I 2 0.879920 0.127808 0.562889 11.00000 -1.50000 H11J 2 0.898986 0.048466 0.551187 11.00000 -1.50000 AFIX 0 C117 1 0.820642 0.446826 0.474616 11.00000 0.04467 0.02177 = 0.02711 -0.00186 -0.00719 -0.00985 AFIX 13 H117 2 0.837273 0.462117 0.427867 11.00000 -1.20000 AFIX 0 C118 1 0.742602 0.455138 0.470909 11.00000 0.04513 0.02995 = 0.03410 -0.00438 -0.00615 -0.01036 AFIX 23 H11K 2 0.712889 0.508288 0.444987 11.00000 -1.20000 H11L 2 0.743249 0.421825 0.446305 11.00000 -1.20000 AFIX 0 C119 1 0.706048 0.435864 0.537184 11.00000 0.05451 0.04496 = 0.04097 -0.00817 0.00030 -0.02019 AFIX 137 H11M 2 0.659515 0.436524 0.530041 11.00000 -1.50000 H11N 2 0.697995 0.473508 0.559166 11.00000 -1.50000 H11O 2 0.737036 0.385117 0.565130 11.00000 -1.50000 AFIX 0 C120 1 0.823945 0.501398 0.507206 11.00000 0.06122 0.02288 = 0.03257 -0.00447 -0.00777 -0.01238 AFIX 23 H12A 2 0.788733 0.553609 0.484919 11.00000 -1.20000 H12B 2 0.809374 0.486838 0.554199 11.00000 -1.20000 AFIX 0 C121 1 0.898619 0.501517 0.504092 11.00000 0.06928 0.03354 = 0.04231 -0.00743 -0.01504 -0.02237 AFIX 137 H12C 2 0.912809 0.517488 0.457670 11.00000 -1.50000 H12D 2 0.933706 0.450175 0.526684 11.00000 -1.50000 H12E 2 0.897442 0.536964 0.525917 11.00000 -1.50000 AFIX 0 C122 1 0.649502 0.385233 0.397925 11.00000 0.04277 0.03575 = 0.03960 -0.01141 0.00818 -0.02153 AFIX 23 H12F 2 0.627250 0.441374 0.386605 11.00000 -1.20000 H12G 2 0.655435 0.363349 0.446670 11.00000 -1.20000 AFIX 0 C123 1 0.599871 0.359742 0.375450 11.00000 0.04624 0.05646 = 0.04998 -0.02072 0.01341 -0.03261 AFIX 23 H12H 2 0.589024 0.386618 0.327651 11.00000 -1.20000 H12I 2 0.553676 0.373419 0.399990 11.00000 -1.20000 AFIX 0 C124 1 0.634455 0.274242 0.387310 11.00000 0.06954 0.06015 = 0.05786 -0.02788 0.02259 -0.04840 AFIX 23 H12J 2 0.604277 0.260185 0.366623 11.00000 -1.20000 H12K 2 0.636959 0.247238 0.435526 11.00000 -1.20000 AFIX 0 C125 1 0.710433 0.249810 0.358112 11.00000 0.06542 0.04139 = 0.05252 -0.01852 0.01500 -0.03491 AFIX 23 H12L 2 0.734342 0.193567 0.371152 11.00000 -1.20000 H12M 2 0.707294 0.269790 0.309133 11.00000 -1.20000 AFIX 0 C126 1 0.755306 0.279385 0.382457 11.00000 0.05027 0.02583 = 0.04324 -0.00484 0.00422 -0.01842 AFIX 23 H12N 2 0.762295 0.255655 0.431004 11.00000 -1.20000 H12O 2 0.803533 0.265140 0.361299 11.00000 -1.20000 AFIX 0 PART 1 C33 1 0.908128 0.931223 0.195156 31.00000 0.05148 0.02205 = 0.02733 -0.00040 -0.00787 -0.02307 AFIX 13 H33 2 0.900315 0.904378 0.167650 31.00000 -1.20000 AFIX 0 C34 1 0.887498 1.014113 0.151431 31.00000 0.04926 0.02906 = 0.03405 -0.00467 -0.00772 -0.02239 AFIX 23 H34A 2 0.891491 1.043588 0.177813 31.00000 -1.20000 H34B 2 0.922000 1.015752 0.114146 31.00000 -1.20000 AFIX 0 C35 1 0.811736 1.050699 0.124189 31.00000 0.05498 0.03361 = 0.04604 -0.00700 -0.01803 -0.01834 AFIX 137 H35A 2 0.803955 1.099787 0.090424 31.00000 -1.50000 H35B 2 0.776856 1.058690 0.160172 31.00000 -1.50000 H35C 2 0.805137 1.017409 0.104259 31.00000 -1.50000 AFIX 0 C36 1 0.990082 0.892085 0.212221 31.00000 0.04278 0.02820 = 0.03771 -0.01040 -0.00099 -0.01656 AFIX 23 H36A 2 1.001781 0.838486 0.239346 31.00000 -1.20000 H36B 2 1.017529 0.891486 0.170346 31.00000 -1.20000 AFIX 0 C37 1 1.016879 0.927205 0.248708 31.00000 0.03958 0.03203 = 0.04124 -0.00951 -0.00655 -0.01483 AFIX 137 H37A 2 1.006877 0.980037 0.222167 31.00000 -1.50000 H37B 2 1.069111 0.898309 0.256249 31.00000 -1.50000 H37C 2 0.992053 0.926078 0.291404 31.00000 -1.50000 AFIX 0 C70 1 0.296249 0.732903 0.258405 21.00000 0.02565 0.03240 = 0.04032 0.00008 -0.00051 -0.01303 AFIX 13 H70 2 0.332656 0.730568 0.221861 21.00000 -1.20000 AFIX 0 C71 1 0.283298 0.659407 0.279857 21.00000 0.03403 0.03712 = 0.03681 -0.00216 -0.00318 -0.01612 AFIX 23 H71A 2 0.322026 0.618677 0.311234 21.00000 -1.20000 H71B 2 0.236742 0.668446 0.303843 21.00000 -1.20000 AFIX 0 C72 1 0.281563 0.631688 0.223214 21.00000 0.04706 0.04743 = 0.04338 -0.00001 -0.00765 -0.02960 AFIX 137 H72A 2 0.242751 0.671133 0.192218 21.00000 -1.50000 H72B 2 0.272754 0.585315 0.240787 21.00000 -1.50000 H72C 2 0.328062 0.620709 0.200042 21.00000 -1.50000 AFIX 0 C73 1 0.225253 0.802293 0.231883 21.00000 0.02996 0.03663 = 0.04573 -0.00124 -0.00364 -0.01462 AFIX 23 H73A 2 0.211664 0.799846 0.190539 21.00000 -1.20000 H73B 2 0.186552 0.799175 0.264686 21.00000 -1.20000 AFIX 0 C74 1 0.228751 0.878879 0.217670 21.00000 0.03776 0.03485 = 0.04209 -0.00143 -0.00249 -0.01161 AFIX 137 H74A 2 0.184918 0.919678 0.193897 21.00000 -1.50000 H74B 2 0.271275 0.879770 0.190418 21.00000 -1.50000 H74C 2 0.232311 0.886435 0.259555 21.00000 -1.50000 AFIX 0 PART 2 C33A 1 0.874508 0.960184 0.188227 -31.00000 0.06513 0.01616 = 0.03722 0.00244 -0.02334 -0.01323 AFIX 13 H33A 2 0.892221 0.920784 0.165061 -31.00000 -1.20000 AFIX 0 C34A 1 0.811777 1.025385 0.148934 -31.00000 0.05959 0.04125 = 0.04435 -0.00638 0.00024 -0.02455 AFIX 23 H34C 2 0.782361 1.003993 0.136407 -31.00000 -1.20000 H34D 2 0.831154 1.050527 0.107335 -31.00000 -1.20000 AFIX 0 C35A 1 0.761537 1.086022 0.177707 -31.00000 0.04716 0.03664 = 0.06483 0.00084 -0.01957 -0.01060 AFIX 137 H35D 2 0.727665 1.127685 0.143428 -31.00000 -1.50000 H35E 2 0.789443 1.105393 0.194326 -31.00000 -1.50000 H35F 2 0.734490 1.064831 0.214272 -31.00000 -1.50000 AFIX 0 C36A 1 0.937094 0.974884 0.194326 -31.00000 0.03472 0.03539 = 0.05504 -0.00900 -0.00118 -0.01948 AFIX 23 H36C 2 0.920321 1.016369 0.214343 -31.00000 -1.20000 H36D 2 0.954410 0.993834 0.149129 -31.00000 -1.20000 AFIX 0 C37A 1 0.999846 0.909821 0.233829 -31.00000 0.04392 0.05625 = 0.07493 -0.03364 -0.00612 -0.02861 AFIX 137 H37D 2 1.014912 0.866512 0.217122 -31.00000 -1.50000 H37E 2 0.985855 0.895268 0.280467 -31.00000 -1.50000 H37F 2 1.040077 0.924858 0.229901 -31.00000 -1.50000 AFIX 0 C70A 1 0.286629 0.781350 0.236330 -21.00000 0.02939 0.07057 = 0.04700 -0.00323 -0.00908 -0.01725 AFIX 13 H70A 2 0.317640 0.800248 0.201029 -21.00000 -1.20000 AFIX 0 C71A 1 0.286280 0.710895 0.224113 -21.00000 0.04059 0.08864 = 0.04846 -0.01879 -0.00761 -0.02861 AFIX 23 H71C 2 0.261823 0.727985 0.181285 -21.00000 -1.20000 H71D 2 0.336956 0.675519 0.220048 -21.00000 -1.20000 AFIX 0 C72A 1 0.249363 0.667545 0.277587 -21.00000 0.06150 0.10558 = 0.06821 -0.02582 0.00230 -0.05380 AFIX 137 H72D 2 0.249579 0.625821 0.264856 -21.00000 -1.50000 H72E 2 0.199325 0.702094 0.282754 -21.00000 -1.50000 H72F 2 0.275379 0.646768 0.319634 -21.00000 -1.50000 AFIX 0 C73A 1 0.210643 0.844883 0.225993 -21.00000 0.03733 0.07104 = 0.05994 -0.00023 -0.01065 -0.02409 AFIX 23 H73C 2 0.178652 0.828078 0.260657 -21.00000 -1.20000 H73D 2 0.192248 0.852898 0.182577 -21.00000 -1.20000 AFIX 0 C74A 1 0.205333 0.920771 0.227934 -21.00000 0.04902 0.06641 = 0.07908 0.00217 -0.01357 -0.01787 AFIX 137 H74D 2 0.238095 0.937230 0.194926 -21.00000 -1.50000 H74E 2 0.218934 0.914800 0.272154 -21.00000 -1.50000 H74F 2 0.155559 0.959035 0.217970 -21.00000 -1.50000 AFIX 0 O4A 5 0.431908 0.301460 0.389211 -41.00000 0.10223 0.11263 = 0.06032 -0.01413 -0.01005 0.00389 C132 1 0.377954 0.384363 0.379403 -41.00000 0.12778 0.11471 = 0.09061 -0.02922 -0.02566 -0.00895 AFIX 23 H13C 2 0.373168 0.396212 0.421308 -41.00000 -1.20000 H13D 2 0.396364 0.418906 0.345045 -41.00000 -1.20000 AFIX 0 C133 1 0.307253 0.396935 0.359317 -41.00000 0.10385 0.10293 = 0.06800 -0.03701 -0.01375 0.01646 AFIX 23 H13E 2 0.272795 0.448888 0.358873 -41.00000 -1.20000 H13F 2 0.311154 0.395502 0.313239 -41.00000 -1.20000 AFIX 0 C134 1 0.276652 0.344425 0.399263 -41.00000 0.11303 0.12786 = 0.08419 -0.03747 -0.01538 0.00715 AFIX 23 H13G 2 0.232183 0.354376 0.377761 -41.00000 -1.20000 H13H 2 0.263365 0.351956 0.443294 -41.00000 -1.20000 AFIX 0 C135 1 0.328202 0.266874 0.407246 -41.00000 0.11494 0.12537 = 0.07959 -0.02973 -0.01406 -0.00688 AFIX 23 H13I 2 0.335067 0.257536 0.363950 -41.00000 -1.20000 H13J 2 0.308131 0.231772 0.438398 -41.00000 -1.20000 AFIX 0 C136 1 0.398988 0.249654 0.432226 -41.00000 0.10838 0.11849 = 0.08510 -0.02641 -0.01908 -0.00562 AFIX 23 H13K 2 0.432078 0.196505 0.435133 -41.00000 -1.20000 H13L 2 0.393020 0.253981 0.477454 -41.00000 -1.20000 AFIX 0 PART 1 O4 5 0.443382 0.342276 0.330359 41.00000 0.09613 0.12598 = 0.09705 -0.05400 0.01638 -0.05698 C127 1 0.389756 0.417930 0.334257 41.00000 0.09648 0.07511 = 0.06971 -0.01933 -0.00475 -0.04599 AFIX 23 H12P 2 0.407351 0.432892 0.365584 41.00000 -1.20000 H12Q 2 0.384268 0.456582 0.290107 41.00000 -1.20000 AFIX 0 C128 1 0.318616 0.415351 0.356822 41.00000 0.07740 0.05785 = 0.07379 -0.02699 -0.02742 -0.00835 AFIX 23 H12R 2 0.298563 0.405844 0.323096 41.00000 -1.20000 H12S 2 0.284450 0.465022 0.362012 41.00000 -1.20000 AFIX 0 C129 1 0.326595 0.353438 0.421818 41.00000 0.07216 0.09145 = 0.07382 -0.02847 0.00829 -0.02684 AFIX 23 H12T 2 0.340267 0.366499 0.456940 41.00000 -1.20000 H12U 2 0.279803 0.349079 0.434155 41.00000 -1.20000 AFIX 0 C130 1 0.382690 0.279787 0.416710 41.00000 0.11892 0.07252 = 0.07743 0.00268 -0.00139 -0.02914 AFIX 23 H13M 2 0.366047 0.264000 0.385406 41.00000 -1.20000 H13N 2 0.389568 0.240472 0.460629 41.00000 -1.20000 AFIX 0 C131 1 0.454505 0.284784 0.393031 41.00000 0.05220 0.06071 = 0.07087 -0.01672 -0.00858 0.00101 AFIX 23 H13O 2 0.473146 0.297559 0.425343 41.00000 -1.20000 H13P 2 0.490451 0.235232 0.388918 41.00000 -1.20000 AFIX 0 PART 2 C68A 1 0.373678 0.748475 0.422134 -21.00000 0.03046 0.02223 = 0.02004 0.00355 0.00176 -0.00381 AFIX 43 H68A 2 0.390044 0.750187 0.460562 -21.00000 -1.20000 AFIX 0 C67A 1 0.300750 0.768714 0.416036 -21.00000 0.03315 0.01993 = 0.03582 0.00361 0.00815 -0.00275 AFIX 43 H67A 2 0.268380 0.778070 0.451560 -21.00000 -1.20000 AFIX 0 C66A 1 0.276567 0.774873 0.357251 -21.00000 0.03463 0.03510 = 0.04529 0.00245 0.00350 -0.01907 AFIX 43 H66A 2 0.226356 0.788898 0.353028 -21.00000 -1.20000 AFIX 0 C65A 1 0.320947 0.761867 0.302990 -21.00000 0.03203 0.04877 = 0.04261 -0.00074 0.00394 -0.02427 HKLF 4 REM hasj240506a_a.res in P-1 REM wR2 = 0.0991, GooF = S = 1.052, Restrained GooF = 1.053 for all data REM R1 = 0.0369 for 25778 Fo > 4sig(Fo) and 0.0424 for all 29465 data REM 1589 parameters refined using 623 restraints END WGHT 0.0510 1.5812 REM Highest difference peak 0.526, deepest hole -0.427, 1-sigma level 0.039 Q1 1 0.7184 0.7156 0.2073 11.00000 0.05 0.53 Q2 1 0.8220 0.4111 0.2889 11.00000 0.05 0.50 Q3 1 0.5374 0.7435 0.2487 11.00000 0.05 0.42 Q4 1 0.6827 0.5854 0.2406 11.00000 0.05 0.40 Q5 1 0.8410 0.5564 0.1664 11.00000 0.05 0.39 Q6 1 0.7538 0.6122 0.2960 11.00000 0.05 0.34 Q7 1 0.8833 0.6893 0.1885 11.00000 0.05 0.34 Q8 1 0.7223 0.5688 0.1580 11.00000 0.05 0.31 Q9 1 0.7574 0.6663 0.1312 11.00000 0.05 0.30 Q10 1 1.0429 0.8677 0.0891 11.00000 0.05 0.29 Q11 1 1.0771 0.7145 -0.0090 11.00000 0.05 0.27 Q12 1 0.8562 0.5509 0.2701 11.00000 0.05 0.26 Q13 1 1.0430 0.7662 0.0192 11.00000 0.05 0.26 Q14 1 0.7737 0.6290 0.1775 11.00000 0.05 0.26 Q15 1 0.9614 0.2067 0.4783 11.00000 0.05 0.25 Q16 1 0.7987 0.5925 0.2423 11.00000 0.05 0.25 Q17 1 0.8657 0.9482 0.2156 11.00000 0.05 0.25 Q18 1 0.2817 0.3919 0.3662 11.00000 0.05 0.24 Q19 1 0.8234 0.8479 0.3129 11.00000 0.05 0.24 Q20 1 0.2197 0.3250 0.3700 11.00000 0.05 0.24 Q21 1 0.4179 0.3347 0.2907 11.00000 0.05 0.24 Q22 1 0.9615 0.6477 0.0641 11.00000 0.05 0.24 Q23 1 0.7912 0.8448 0.1556 11.00000 0.05 0.23 Q24 1 0.9828 0.1781 0.2491 11.00000 0.05 0.23 Q25 1 0.9384 0.3510 0.2188 11.00000 0.05 0.22 Q26 1 0.4631 0.5842 0.3503 11.00000 0.05 0.22 Q27 1 0.8835 0.2836 0.2008 11.00000 0.05 0.22 Q28 1 0.6552 0.5829 0.3286 11.00000 0.05 0.22 Q29 1 0.8539 0.4005 0.4923 11.00000 0.05 0.22 Q30 1 0.4694 0.7764 0.1475 11.00000 0.05 0.22 Q31 1 0.7603 0.5713 0.2192 11.00000 0.05 0.22 Q32 1 0.9226 0.2165 0.1984 11.00000 0.05 0.22 Q33 1 0.9417 0.3679 0.3211 11.00000 0.05 0.22 Q34 1 0.5208 0.7836 0.1850 11.00000 0.05 0.22 Q35 1 0.9400 0.2212 0.5285 11.00000 0.05 0.22 Q36 1 0.8085 0.8702 0.3503 11.00000 0.05 0.22 Q37 1 0.6970 0.6821 0.2914 11.00000 0.05 0.22 Q38 1 0.7725 0.3768 0.1595 11.00000 0.05 0.22 Q39 1 0.7301 0.6832 0.2667 11.00000 0.05 0.21 Q40 1 0.9590 0.8883 0.0339 11.00000 0.05 0.21 Q41 1 0.4882 0.6729 0.1601 11.00000 0.05 0.21 Q42 1 0.9864 0.2177 0.5590 11.00000 0.05 0.21 Q43 1 0.9518 0.5893 0.0610 11.00000 0.05 0.21 Q44 1 0.8864 0.3391 0.4881 11.00000 0.05 0.21 Q45 1 0.6265 0.6328 0.2691 11.00000 0.05 0.21 Q46 1 0.8314 0.7440 0.1986 11.00000 0.05 0.21 Q47 1 0.9254 0.2652 0.4869 11.00000 0.05 0.21 Q48 1 0.8763 0.3474 0.5353 11.00000 0.05 0.21 Q49 1 0.7012 0.7396 0.1336 11.00000 0.05 0.20 Q50 1 0.9987 0.1819 0.4487 11.00000 0.05 0.20 Q51 1 0.8808 0.5842 0.2818 11.00000 0.05 0.20 Q52 1 0.3791 0.8776 -0.0069 11.00000 0.05 0.20 Q53 1 0.9652 0.2588 0.5856 11.00000 0.05 0.20 Q54 1 1.0035 0.6609 0.0286 11.00000 0.05 0.20 Q55 1 0.5786 0.7135 0.1766 11.00000 0.05 0.20 Q56 1 0.8822 0.2086 0.1208 11.00000 0.05 0.20 Q57 1 0.9239 0.0933 0.3218 11.00000 0.05 0.20 Q58 1 0.8299 0.9483 0.2700 11.00000 0.05 0.20 Q59 1 0.8327 0.2760 0.1097 11.00000 0.05 0.20 Q60 1 0.8069 0.8181 0.1208 11.00000 0.05 0.20 Q61 1 0.8507 0.9376 0.2799 11.00000 0.05 0.20 Q62 1 0.4991 0.3565 0.3033 11.00000 0.05 0.20 Q63 1 0.6900 0.6466 0.3682 11.00000 0.05 0.20 Q64 1 0.4883 0.6479 0.2177 11.00000 0.05 0.20 Q65 1 0.8378 0.7131 0.2637 11.00000 0.05 0.20 Q66 1 0.9210 0.1807 0.1609 11.00000 0.05 0.20 Q67 1 0.8395 0.8441 0.2508 11.00000 0.05 0.19 Q68 1 0.8959 0.3389 0.2537 11.00000 0.05 0.19 Q69 1 0.7526 0.7727 0.3875 11.00000 0.05 0.19 Q70 1 0.4207 0.2452 0.3874 11.00000 0.05 0.19 Q71 1 0.5135 0.6624 0.0993 11.00000 0.05 0.19 Q72 1 0.4980 0.8642 -0.0281 11.00000 0.05 0.19 Q73 1 0.7214 0.3651 0.4064 11.00000 0.05 0.19 Q74 1 0.7858 0.8192 0.3509 11.00000 0.05 0.19 Q75 1 0.8139 0.3253 0.1417 11.00000 0.05 0.19 Q76 1 0.7820 0.3186 0.1625 11.00000 0.05 0.19 Q77 1 0.8364 0.3434 0.2969 11.00000 0.05 0.18 Q78 1 0.4818 0.7286 0.1112 11.00000 0.05 0.18 Q79 1 0.9447 0.3580 0.2708 11.00000 0.05 0.18 Q80 1 0.6754 0.6313 0.2306 11.00000 0.05 0.18 Q81 1 0.8395 0.8976 0.2682 11.00000 0.05 0.18 Q82 1 1.1017 0.1329 0.2548 11.00000 0.05 0.18 Q83 1 0.4018 0.4000 0.3416 11.00000 0.05 0.18 Q84 1 0.8178 0.7432 0.3716 11.00000 0.05 0.18 Q85 1 0.8532 0.3335 0.2891 11.00000 0.05 0.18 Q86 1 1.0303 0.1598 0.2203 11.00000 0.05 0.18 Q87 1 1.0171 0.4009 0.3632 11.00000 0.05 0.18 Q88 1 0.9279 0.3723 0.2780 11.00000 0.05 0.18 Q89 1 1.0172 0.8531 0.0451 11.00000 0.05 0.17 ; _shelx_res_checksum 87542 _shelx_hkl_file ; 0 0 2 3867.43 19.69 0 0 -2 3886.24 17.63 0 0 -2 3875.11 13.34 0 0 -2 3830.65 14.10 0 0 -3 59.09 2.67 0 0 3 54.75 3.05 0 0 -3 54.31 2.02 0 0 -3 59.93 3.30 0 0 -3 55.48 2.11 0 0 4 2997.64 24.12 0 0 -4 2912.19 21.40 0 0 4 3051.27 24.70 0 0 -4 2831.04 16.35 0 0 -4 2875.65 17.15 0 0 -4 2948.22 25.88 0 0 5 2347.05 24.57 0 0 5 2399.71 24.55 0 0 -5 2382.68 21.67 0 0 -5 2286.05 16.78 0 0 -5 2309.40 25.17 0 0 -5 2296.92 17.50 0 0 6 39.81 3.73 0 0 6 42.55 3.81 0 0 -6 39.31 3.32 0 0 -6 36.47 2.31 0 0 -6 34.48 3.58 0 0 -6 38.81 2.45 0 0 7 1309.13 22.24 0 0 7 1281.20 21.78 0 0 -7 1294.76 15.19 0 0 -7 1312.85 15.66 0 0 -7 1325.99 22.32 0 0 8 211.69 9.76 0 0 8 212.72 9.72 0 0 -8 213.51 6.63 0 0 -8 225.30 7.24 0 0 -8 215.55 9.90 0 0 9 73.54 6.60 0 0 9 72.10 6.49 0 0 -9 72.13 4.27 0 0 -9 75.24 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63.68 7.70 0 -11 -11 61.07 3.66 0 -11 -11 63.14 7.24 0 -11 -12 28.07 4.96 0 -11 -12 29.90 5.55 0 -11 -12 31.04 2.54 0 -11 -12 31.55 2.56 0 -11 -12 33.20 2.94 0 11 12 33.89 6.26 0 -11 -13 495.26 21.46 0 11 13 481.37 22.87 0 -11 -13 486.99 10.49 0 -11 -13 448.23 9.59 0 -11 -13 496.68 21.11 0 -11 -13 453.99 9.65 0 -11 -14 13.86 1.96 0 -11 -14 13.67 2.11 0 -11 -14 12.64 2.00 0 -11 -14 12.97 3.56 0 -11 -14 13.86 4.68 0 11 14 9.43 4.40 0 -11 -15 8.30 1.75 0 -11 -15 8.79 2.00 0 -11 -15 11.03 4.03 0 -11 -15 6.75 1.57 0 -11 -15 12.70 5.03 0 11 15 8.62 4.30 0 -11 -16 12.89 2.04 0 -11 -16 19.83 2.47 0 -11 -16 13.69 1.97 0 -11 -16 14.48 4.57 0 -11 -16 23.15 5.73 0 11 16 18.72 6.72 0 -11 -17 125.99 5.47 0 -11 -17 130.50 5.90 0 -11 -17 118.02 5.39 0 -11 -18 82.36 4.52 0 -11 -18 83.60 4.90 0 -11 -18 84.10 4.53 0 -11 -19 159.29 6.05 0 -11 -19 171.00 6.63 0 -11 -19 153.90 6.09 0 -11 -20 1.50 1.16 0 -11 -20 2.20 1.29 0 -11 -20 1.17 0.99 0 -11 -21 112.63 4.82 0 -11 -21 99.01 4.95 0 -11 -21 111.40 4.88 0 -11 -22 29.92 2.45 0 -11 -22 30.70 2.54 0 -11 -22 32.03 2.78 0 -11 -23 43.18 2.69 0 -11 -23 38.31 2.56 0 -11 -23 36.18 2.70 0 -11 -23 41.45 2.70 0 -11 -24 3.85 0.93 0 -11 -24 2.19 0.93 0 -11 -24 1.81 0.76 0 -11 -25 1.99 0.66 0 -11 -25 1.55 0.64 0 -11 -25 2.87 0.73 0 -11 -25 2.15 0.74 0 12 -16 27.69 1.89 0 12 -15 1.50 0.88 0 -12 15 0.91 0.75 0 12 -14 1.95 1.24 0 -12 14 -0.39 0.83 0 12 -13 13.82 2.24 0 12 -13 13.06 2.22 0 -12 13 13.98 1.39 0 -12 13 13.43 1.74 0 12 -12 107.28 5.60 0 12 -12 103.28 5.82 0 -12 12 105.67 3.72 0 -12 12 99.66 4.42 0 12 -11 2.65 1.55 0 12 -11 0.66 1.60 0 -12 11 -0.38 0.97 0 12 -10 19.66 2.81 0 -12 10 18.78 2.05 0 12 -9 39.18 3.79 0 -12 9 40.26 3.03 0 -12 8 2.04 1.24 0 12 -8 0.29 1.55 0 12 -7 11.93 3.30 0 12 -7 17.77 4.27 0 12 -7 14.42 2.36 0 -12 7 16.28 1.93 0 12 -6 15.45 2.44 0 -12 6 16.99 2.06 0 12 -6 18.75 4.01 0 12 -6 17.70 4.16 0 -12 6 13.48 4.04 0 -12 6 16.04 1.90 0 12 -5 572.52 13.20 0 -12 5 562.16 10.34 0 12 -5 561.46 20.00 0 12 -5 566.73 20.84 0 -12 5 523.81 20.93 0 -12 5 551.29 9.93 0 12 -4 40.15 3.50 0 -12 4 43.18 2.90 0 12 -4 43.02 5.37 0 12 -4 42.30 5.73 0 -12 4 46.45 6.40 0 -12 4 44.45 2.93 0 12 -3 66.46 4.35 0 -12 3 69.73 3.56 0 12 -3 60.85 6.48 0 12 -3 73.63 6.64 0 -12 3 68.36 7.48 0 -12 3 59.81 3.32 0 12 -2 261.41 8.11 0 -12 2 253.30 13.61 0 -12 2 250.77 6.35 0 -12 2 263.09 6.58 0 12 -2 265.40 12.68 0 12 -2 275.08 12.04 0 -12 1 16.25 1.86 0 -12 1 16.78 1.89 0 12 -1 15.12 3.18 0 12 -1 18.37 3.04 0 12 0 92.06 6.88 0 -12 0 87.55 3.75 0 -12 -1 10.23 2.75 0 12 1 8.16 2.08 0 -12 -2 4.41 2.07 0 12 2 5.59 2.47 0 12 3 163.51 9.95 0 -12 -3 176.41 9.92 0 -12 -3 182.40 10.25 0 12 4 174.88 10.14 0 -12 -4 167.58 9.56 0 -12 -4 158.41 8.44 0 -12 -4 168.91 10.23 0 12 5 351.93 14.72 0 -12 -5 329.47 13.51 0 -12 -5 332.32 11.49 0 -12 -5 360.87 15.22 0 12 6 64.14 6.64 0 -12 -6 65.73 6.22 0 -12 -6 69.05 5.16 0 -12 -6 77.17 7.40 0 12 7 205.60 11.97 0 -12 -7 191.76 10.97 0 -12 -7 202.21 11.94 0 12 8 91.50 8.39 0 -12 -8 83.87 7.27 0 -12 -8 99.22 8.73 0 12 9 -0.71 3.01 0 -12 -9 0.95 1.72 0 -12 -9 0.47 2.01 0 -12 -10 194.51 11.97 0 -12 -10 170.76 5.66 0 12 10 196.70 13.13 0 -12 -10 172.27 6.15 0 -12 -10 193.10 12.76 0 -12 -11 152.78 11.18 0 12 11 136.50 11.58 0 -12 -11 129.37 5.06 0 -12 -11 130.91 5.46 0 -12 -11 142.24 11.35 0 -12 -12 7.29 3.33 0 12 12 5.83 3.44 0 -12 -12 4.46 1.55 0 -12 -12 7.40 3.30 0 -12 -13 168.23 12.93 0 12 13 179.69 14.46 0 -12 -13 176.80 6.01 0 -12 -13 176.45 6.71 0 -12 -13 185.16 13.68 0 -12 -13 174.01 5.90 0 -12 -14 13.80 4.46 0 -12 -14 10.69 1.84 0 12 14 15.36 5.68 0 -12 -14 7.91 1.76 0 -12 -14 7.82 1.55 0 -12 -14 10.70 4.22 0 -12 -15 131.39 12.48 0 -12 -15 130.37 5.38 0 -12 -15 132.22 11.70 0 -12 -15 124.91 5.36 0 12 15 131.73 14.23 0 -12 -15 139.24 5.99 0 -12 -16 143.22 5.73 0 -12 -16 146.64 6.27 0 -12 -16 139.30 5.65 0 -12 -17 36.46 3.10 0 -12 -17 41.05 3.46 0 -12 -17 34.34 2.93 0 -12 -18 4.18 1.49 0 -12 -18 4.55 1.77 0 -12 -18 2.51 1.13 0 -12 -19 4.65 1.15 0 -12 -19 7.03 1.82 0 -12 -19 5.82 1.47 0 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91.31 4.30 0 -13 4 85.66 4.07 0 13 -4 95.82 5.50 0 13 -4 87.94 8.36 0 13 -4 87.83 8.06 0 -13 3 228.21 6.60 0 -13 3 236.55 6.52 0 13 -3 236.86 8.42 0 13 -3 227.04 13.15 0 -13 2 102.54 4.29 0 -13 2 94.40 4.12 0 13 -2 95.64 5.19 0 13 -2 96.18 8.32 0 -13 1 64.40 3.47 0 13 -1 69.59 6.48 0 -13 1 67.21 3.44 0 13 -1 74.93 4.58 0 -13 0 664.74 10.35 0 -13 0 673.31 21.32 0 13 0 671.58 13.05 0 -13 0 666.47 10.67 0 -13 -1 2.64 1.80 0 -13 -1 3.64 1.00 0 -13 -1 3.35 1.02 0 13 1 1.05 2.12 0 13 1 2.58 1.52 0 -13 -2 410.83 7.66 0 -13 -2 408.60 8.30 0 13 2 401.69 16.31 0 -13 -2 383.22 15.66 0 13 2 402.86 10.04 0 13 3 13.97 2.34 0 13 3 13.48 3.45 0 -13 -3 13.56 1.66 0 -13 -3 11.03 3.04 0 -13 -3 10.69 2.75 0 -13 -4 151.64 8.61 0 13 4 154.86 10.23 0 13 4 150.32 6.32 0 -13 -4 161.25 9.95 0 -13 -4 162.85 10.53 0 13 5 12.92 2.30 0 -13 -5 16.20 3.56 0 -13 -5 13.23 3.02 0 13 5 16.59 4.19 0 -13 -5 14.91 1.85 0 -13 -5 11.71 2.25 0 -13 -6 61.09 7.11 0 -13 -6 53.59 5.89 0 13 6 59.80 4.13 0 -13 -6 55.36 3.12 0 13 6 55.35 6.79 0 -13 -6 53.14 2.96 0 -13 -7 4.20 1.24 0 -13 -7 1.91 1.25 0 -13 -7 1.36 2.09 0 13 7 3.63 2.68 0 -13 -7 4.36 1.39 0 13 7 5.00 1.98 0 -13 -7 3.12 1.51 0 -13 -8 308.99 6.94 0 -13 -8 297.83 8.02 0 -13 -8 317.82 16.28 0 13 8 310.99 10.57 0 -13 -8 314.01 7.39 0 -13 -8 314.46 14.59 0 13 8 338.81 16.99 0 -13 -9 21.47 2.43 0 -13 -9 19.90 4.31 0 -13 -9 21.51 4.46 0 -13 -9 18.30 2.07 0 -13 -9 20.35 2.00 0 13 9 24.99 5.26 0 -13 -10 94.63 4.68 0 -13 -10 99.46 8.95 0 -13 -10 89.22 8.84 0 -13 -10 90.59 4.21 0 -13 -10 95.43 3.94 0 13 10 106.69 10.03 0 -13 -11 47.71 6.98 0 -13 -11 47.40 3.56 0 13 11 56.81 8.35 0 -13 -11 48.92 3.28 0 -13 -11 52.99 6.90 0 -13 -12 8.57 3.34 0 -13 -12 9.64 1.90 0 13 12 10.50 4.58 0 -13 -12 10.07 1.71 0 -13 -12 6.16 2.46 0 -13 -13 27.59 5.64 0 -13 -13 26.47 2.85 0 13 13 29.52 7.06 0 -13 -13 23.28 4.83 0 -13 -13 23.39 2.47 0 -13 -14 5.72 1.65 0 -13 -14 4.92 1.30 0 -13 -14 1.94 3.04 0 -13 -14 3.35 1.57 0 13 14 5.92 4.22 0 -13 -14 3.59 1.23 0 -13 -14 5.13 3.33 0 -13 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13.82 2.37 0 -14 11 11.41 1.57 0 14 -11 14.24 2.05 0 14 -10 30.26 3.36 0 -14 10 28.35 2.34 0 14 -10 29.61 3.06 0 14 -9 28.29 3.13 0 -14 9 29.59 2.44 0 -14 8 76.74 3.98 0 14 -8 72.09 4.86 0 14 -7 22.55 2.93 0 -14 7 24.04 2.38 0 -14 6 317.98 7.90 0 14 -6 325.39 10.32 0 14 -5 119.62 6.26 0 -14 5 114.23 4.73 0 14 -4 1.19 1.64 0 -14 4 3.19 1.18 0 14 -3 0.06 1.66 0 -14 3 1.53 1.14 0 -14 3 0.76 1.05 0 -14 2 197.29 6.15 0 -14 2 189.77 5.97 0 -14 2 194.10 12.35 0 14 -2 200.12 7.71 0 -14 1 4.32 2.54 0 -14 1 4.72 1.27 0 -14 1 2.13 1.07 0 14 -1 1.98 1.34 0 14 -1 1.81 3.03 0 -14 0 563.71 9.77 0 14 0 567.53 12.89 0 14 0 567.25 21.00 0 -14 0 568.76 20.72 0 -14 0 531.78 19.39 0 -14 0 552.68 9.97 0 -14 -1 236.87 6.22 0 14 1 254.36 8.32 0 14 1 250.09 14.05 0 -14 -1 232.62 12.81 0 -14 -1 227.26 12.38 0 -14 -1 243.84 6.72 0 -14 -2 244.84 6.22 0 -14 -2 238.74 6.69 0 14 2 258.49 13.98 0 -14 -2 253.95 13.53 0 -14 -2 234.78 12.14 0 14 2 238.55 8.35 0 14 3 238.40 8.14 0 14 3 236.45 13.47 0 -14 -3 235.43 6.61 0 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16 -3 75.69 5.02 1 -16 3 72.82 3.83 -1 16 -4 7.92 2.05 1 -16 4 9.47 1.56 -1 16 -5 123.25 6.08 1 -16 5 121.46 4.68 -1 16 -6 19.65 2.56 1 -16 6 13.64 1.68 -1 16 -7 27.76 2.80 1 -16 7 28.23 2.21 -1 16 -8 1.94 1.22 1 -16 8 2.22 1.01 -1 16 -9 36.52 3.09 1 -16 9 39.06 2.41 -1 16 -9 38.83 2.80 1 -16 10 -0.09 0.70 -1 16 -10 0.66 1.14 -1 16 -11 39.96 2.44 -1 15 23 0.97 0.92 1 -15 -23 1.50 0.76 1 -15 -23 2.19 0.64 1 -15 -22 4.06 0.88 -1 15 22 4.98 1.68 1 -15 -22 4.63 0.81 1 -15 -22 6.72 1.30 1 -15 -22 4.95 0.80 1 -15 -21 2.06 0.74 1 -15 -21 2.13 0.87 1 -15 -21 2.23 0.73 1 -15 -20 49.57 2.86 1 -15 -20 47.55 3.23 1 -15 -19 7.97 1.46 1 -15 -19 7.60 1.60 1 -15 -18 165.02 5.43 1 -15 -18 154.19 6.00 1 -15 -17 9.28 1.55 1 -15 -17 9.85 2.01 1 -15 -16 3.30 1.10 1 -15 -16 0.37 1.27 1 -15 -15 83.92 4.15 1 -15 -15 90.81 4.85 1 -15 -14 9.88 1.64 -1 15 14 3.78 2.50 1 -15 -14 7.79 1.85 1 -15 -13 221.99 6.72 -1 15 13 211.05 9.68 1 -15 -13 200.67 5.77 1 -15 -13 225.90 7.55 1 -15 -12 153.66 5.47 -1 15 12 153.26 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306.19 14.60 1 -13 -2 149.06 4.82 1 -13 -2 159.02 10.37 1 -13 -2 159.86 5.43 -1 13 2 154.21 6.52 -1 13 2 147.53 10.13 1 -13 -1 15.29 1.92 -1 13 1 14.80 2.33 1 -13 -1 13.62 3.29 1 -13 -1 14.80 1.79 -1 13 1 17.34 3.91 1 -13 0 8.30 1.51 -1 13 0 8.11 2.09 1 -13 0 13.60 3.68 -1 13 0 10.86 3.73 1 -13 0 7.87 1.32 -1 13 -1 2.17 1.60 1 -13 1 2.18 1.12 -1 13 -1 3.05 2.13 1 -13 1 2.06 1.07 -1 13 -2 -1.94 1.49 1 -13 2 0.69 0.91 -1 13 -2 1.17 2.37 1 -13 2 0.47 0.93 -1 13 -3 4.30 1.86 1 -13 3 2.51 0.99 1 -13 3 2.48 1.04 -1 13 -4 20.52 2.83 1 -13 4 20.66 2.19 1 -13 4 17.42 2.06 -1 13 -5 46.80 4.22 1 -13 5 47.97 3.15 1 -13 5 50.61 3.33 -1 13 -6 95.58 5.84 1 -13 6 94.08 4.49 1 -13 6 92.57 4.31 -1 13 -7 124.73 6.58 1 -13 7 127.70 4.99 -1 13 -8 44.79 4.12 1 -13 8 41.49 2.91 -1 13 -9 157.70 7.11 1 -13 9 161.97 5.61 -1 13 -10 6.74 1.58 1 -13 10 4.86 1.28 -1 13 -11 25.02 3.14 -1 13 -11 27.27 2.92 1 -13 11 28.43 2.37 -1 13 -12 23.04 2.85 -1 13 -12 25.08 2.77 1 -13 12 26.10 2.17 -1 13 -13 9.85 1.85 -1 13 -13 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1 -12 -14 -0.51 0.99 1 -12 -14 -0.78 2.54 1 -12 -13 30.45 5.84 -1 12 13 35.53 7.71 1 -12 -13 34.59 2.41 1 -12 -13 33.62 3.17 1 -12 -13 28.52 5.53 1 -12 -12 20.43 4.85 -1 12 12 17.62 5.37 1 -12 -12 17.03 1.74 1 -12 -12 17.58 2.14 1 -12 -12 16.85 2.33 1 -12 -12 16.29 4.74 1 -12 -11 54.38 6.74 -1 12 11 50.13 7.67 1 -12 -11 48.67 2.97 1 -12 -11 55.79 3.46 1 -12 -11 52.65 3.58 1 -12 -11 49.64 6.95 1 -12 -10 22.63 4.75 -1 12 10 15.48 4.76 1 -12 -10 18.07 1.86 1 -12 -10 14.66 1.73 1 -12 -10 17.05 2.40 1 -12 -10 20.08 4.35 1 -12 -9 11.35 3.36 -1 12 9 17.49 4.92 1 -12 -9 11.15 1.50 1 -12 -9 11.50 3.86 1 -12 -9 12.19 1.92 1 -12 -9 11.98 1.73 1 -12 -8 8.33 1.64 -1 12 8 10.46 3.93 1 -12 -8 7.88 3.17 1 -12 -8 6.87 2.75 -1 12 7 32.55 5.31 1 -12 -7 31.57 5.05 1 -12 -7 34.32 5.01 -1 12 6 346.19 15.63 1 -12 -6 360.37 15.93 1 -12 -6 357.95 14.82 1 -12 -5 276.12 10.64 -1 12 5 268.86 13.55 1 -12 -5 278.18 13.93 1 -12 -5 273.33 12.74 1 -12 -4 9.83 3.26 -1 12 4 4.22 2.81 1 -12 -4 8.28 2.76 -1 12 3 423.47 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-17 151.77 5.42 2 -14 -17 166.85 6.34 2 -14 -16 8.77 1.47 2 -14 -16 9.33 1.91 2 -14 -15 7.38 1.45 2 -14 -15 4.56 1.56 2 -14 -15 5.28 1.27 2 -14 -14 27.76 2.47 2 -14 -14 27.09 2.83 2 -14 -14 27.36 2.22 2 -14 -13 1.33 1.14 2 -14 -13 1.86 1.53 2 -14 -13 1.56 0.98 2 -14 -12 35.28 2.54 2 -14 -12 35.10 3.18 2 -14 -12 34.35 2.68 -2 14 12 28.05 3.84 2 -14 -11 83.06 9.26 2 -14 -11 76.12 3.87 2 -14 -11 74.03 4.42 2 -14 -11 73.51 3.66 2 -14 -11 68.62 8.75 -2 14 11 76.52 6.09 2 -14 -10 210.31 14.65 2 -14 -10 201.61 7.25 -2 14 10 204.52 9.15 2 -14 -10 200.24 6.04 2 -14 -10 185.70 13.09 2 -14 -10 198.87 6.11 -2 14 10 198.61 15.59 2 -14 -9 2.89 0.93 2 -14 -9 2.80 1.17 2 -14 -9 2.06 2.24 2 -14 -9 3.04 2.76 -2 14 9 3.52 2.15 -2 14 9 -1.57 3.56 2 -14 -8 18.97 1.92 2 -14 -8 16.72 2.00 -2 14 8 16.91 2.49 -2 14 8 18.97 4.72 2 -14 -8 18.67 4.82 2 -14 -8 19.03 4.40 2 -14 -7 6.55 1.35 2 -14 -7 12.95 3.84 -2 14 7 6.33 2.05 -2 14 7 4.02 3.45 2 -14 -7 5.34 2.91 2 -14 -6 365.23 8.46 -2 14 6 389.82 11.14 2 -14 -6 393.31 18.49 -2 14 6 358.39 18.97 2 -14 -6 377.86 17.25 -2 14 5 113.31 10.31 -2 14 5 134.23 6.66 2 -14 -5 128.61 10.15 2 -14 -4 16.10 3.90 -2 14 4 14.42 4.31 -2 14 4 15.87 2.49 2 -14 -3 62.35 7.22 -2 14 3 68.11 4.73 -2 14 3 66.28 8.08 2 -14 -3 63.92 3.20 2 -14 -3 62.42 3.68 2 -14 -3 57.86 6.21 2 -14 -2 64.72 3.27 2 -14 -2 55.26 3.44 -2 14 2 61.27 4.45 -2 14 2 64.20 7.57 2 -14 -2 50.37 6.40 2 -14 -1 62.53 3.62 -2 14 1 70.80 4.72 2 -14 -1 66.21 7.35 -2 14 1 67.80 7.71 2 -14 -1 63.41 3.39 -2 14 0 10.88 4.00 -2 14 0 9.86 2.26 2 -14 0 10.31 1.62 2 -14 0 12.61 1.72 2 -14 0 5.46 2.22 2 -14 1 317.20 7.88 -2 14 -1 314.14 10.07 2 -14 1 311.63 16.32 2 -14 1 327.83 7.88 2 -14 2 3.53 1.38 2 -14 2 1.72 1.19 -2 14 -2 1.79 1.47 2 -14 3 52.44 3.32 2 -14 3 50.07 3.22 -2 14 -3 49.24 4.27 2 -14 4 -0.79 1.11 2 -14 4 1.37 0.99 -2 14 -4 2.31 1.80 2 -14 5 66.60 3.60 2 -14 5 65.64 3.79 -2 14 -5 65.97 4.88 -2 14 -6 32.42 3.49 2 -14 6 36.88 2.82 2 -14 7 34.16 2.60 -2 14 -7 38.05 3.62 2 -14 8 16.82 1.90 -2 14 -8 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2 -13 -14 184.00 5.67 2 -13 -14 183.17 6.97 2 -13 -14 178.19 6.25 2 -13 -13 1.72 1.19 2 -13 -13 2.54 1.03 2 -13 -13 3.81 2.85 2 -13 -13 2.63 2.58 2 -13 -13 2.06 1.27 2 -13 -12 1.38 2.21 2 -13 -12 0.01 1.10 2 -13 -12 1.64 1.13 2 -13 -12 1.90 2.08 2 -13 -12 2.55 1.50 -2 13 12 7.52 5.28 2 -13 -11 11.63 4.02 2 -13 -11 14.78 1.89 2 -13 -11 11.86 1.75 2 -13 -11 14.52 4.31 2 -13 -11 14.85 2.05 -2 13 11 11.87 5.24 -2 13 10 9.00 4.31 2 -13 -10 3.83 2.97 2 -13 -10 6.00 1.31 2 -13 -10 8.11 1.52 2 -13 -10 6.68 3.61 2 -13 -10 6.66 1.80 -2 13 10 3.79 2.20 -2 13 9 204.42 9.28 2 -13 -9 200.96 6.94 2 -13 -9 204.25 13.06 2 -13 -9 193.47 6.00 2 -13 -9 193.55 5.94 2 -13 -9 199.04 13.55 -2 13 9 196.98 14.16 -2 13 8 18.65 4.65 2 -13 -8 18.04 4.08 2 -13 -8 21.66 2.15 2 -13 -8 21.17 2.10 2 -13 -8 17.38 4.05 2 -13 -8 20.09 2.55 -2 13 8 20.27 2.87 2 -13 -7 45.81 2.82 2 -13 -7 48.65 3.08 2 -13 -7 42.34 6.15 -2 13 7 47.92 4.18 -2 13 7 46.86 6.64 2 -13 -7 43.89 6.11 2 -13 -6 15.37 1.79 2 -13 -6 12.07 3.25 2 -13 -6 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11.38 2 -7 -10 175.83 8.60 2 -7 -10 175.89 10.19 2 -7 -9 96.64 7.48 2 -7 -9 96.37 6.00 -2 7 9 93.15 8.27 2 -7 -9 101.68 7.60 2 -7 -8 442.70 15.05 2 -7 -8 422.85 14.39 2 -7 -8 454.58 11.70 -2 7 8 434.99 15.57 2 -7 -7 1196.65 17.54 -2 7 7 1223.59 24.51 2 -7 -6 87.25 6.03 2 -7 -6 98.37 4.77 -2 7 6 95.93 7.24 2 -7 -5 31.31 3.76 -2 7 5 30.01 4.11 -2 7 5 31.46 2.30 2 -7 -5 28.52 2.61 2 -7 -4 144.83 7.29 -2 7 4 152.39 7.84 2 -7 -4 154.57 5.18 -2 7 4 150.55 4.86 -2 7 3 5.10 2.17 -2 7 3 4.77 1.23 2 -7 -3 4.46 2.01 2 -7 -3 3.53 1.24 2 -7 -2 112.75 4.13 -2 7 2 112.75 6.29 -2 7 2 103.17 4.68 2 -7 -2 112.12 6.76 2 -7 -1 149.00 4.79 2 -7 -1 163.75 8.28 -2 7 1 146.07 5.94 2 -7 0 547.22 9.72 -2 7 0 534.74 11.87 -2 7 0 522.13 12.49 2 -7 1 2.84 2.40 2 -7 1 2.45 1.44 -2 7 -1 3.65 1.78 -2 7 -1 3.60 1.81 2 -7 2 13.32 3.10 2 -7 2 12.31 1.75 -2 7 -2 15.60 2.77 -2 7 -2 14.37 2.42 -2 7 -3 88.27 6.21 -2 7 -3 93.30 6.06 2 -7 3 81.34 6.64 -2 7 -4 3.86 1.74 2 -7 4 2.86 2.26 -2 7 -5 3.06 1.58 2 -7 5 3.64 2.17 -2 7 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37.53 2.53 3 -10 -17 33.45 2.94 3 -10 -17 34.00 3.26 3 -10 -17 33.90 2.92 3 -10 -16 49.39 3.00 3 -10 -16 44.78 3.32 3 -10 -16 43.31 3.31 3 -10 -16 50.86 3.93 3 -10 -15 -0.08 1.50 3 -10 -15 2.70 2.46 -3 10 15 1.15 5.82 3 -10 -15 -0.93 1.07 3 -10 -15 0.20 1.07 3 -10 -15 1.44 1.03 3 -10 -15 -0.81 2.25 3 -10 -14 206.96 7.38 3 -10 -14 193.26 6.41 3 -10 -14 196.47 13.74 3 -10 -14 204.62 14.93 -3 10 14 187.24 16.80 3 -10 -14 196.26 6.53 3 -10 -14 198.39 5.76 3 -10 -13 99.47 5.08 3 -10 -13 99.16 9.76 3 -10 -13 100.02 4.48 3 -10 -13 95.59 9.52 -3 10 13 91.15 11.94 3 -10 -13 102.85 4.57 3 -10 -13 100.62 4.18 3 -10 -12 37.71 5.88 3 -10 -12 44.14 2.73 -3 10 12 34.09 7.04 3 -10 -12 41.18 3.32 3 -10 -12 42.96 6.51 3 -10 -11 27.62 4.88 3 -10 -11 26.37 2.22 -3 10 11 28.58 6.19 3 -10 -11 27.31 2.74 3 -10 -11 22.17 4.58 3 -10 -10 43.79 5.74 3 -10 -10 45.56 2.72 -3 10 10 47.53 7.22 3 -10 -10 43.14 6.04 3 -10 -10 49.17 3.34 3 -10 -9 12.75 3.50 -3 10 9 11.52 3.87 3 -10 -9 11.23 3.39 3 -10 -9 14.21 2.04 3 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66.01 8.67 5 -10 -13 56.69 7.95 5 -10 -12 1.76 1.03 -5 10 12 5.88 4.83 5 -10 -12 3.15 1.61 5 -10 -12 3.08 1.94 5 -10 -12 -1.37 2.20 5 -10 -11 25.04 2.31 -5 10 11 29.91 7.33 5 -10 -11 28.53 2.86 5 -10 -11 25.96 5.11 5 -10 -11 28.59 5.27 5 -10 -10 63.71 3.47 -5 10 10 58.81 9.20 5 -10 -10 59.46 3.96 5 -10 -10 57.60 7.37 5 -10 -10 59.24 7.26 5 -10 -9 37.14 2.69 -5 10 9 33.46 6.51 5 -10 -9 38.67 3.24 5 -10 -9 33.78 5.55 5 -10 -9 29.06 5.05 5 -10 -8 33.67 2.58 -5 10 8 28.42 6.25 5 -10 -8 32.63 2.89 5 -10 -8 30.33 5.51 5 -10 -8 33.82 5.28 5 -10 -7 145.85 10.96 5 -10 -7 146.72 10.19 5 -10 -7 143.83 5.07 5 -10 -7 142.30 5.83 -5 10 7 136.79 11.27 -5 10 7 138.38 7.49 5 -10 -6 0.65 2.06 5 -10 -6 -1.64 1.17 -5 10 6 2.77 1.89 -5 10 6 0.26 2.49 5 -10 -6 -1.63 2.06 -5 10 5 234.53 13.18 5 -10 -5 240.26 6.47 -5 10 5 239.73 8.64 5 -10 -5 242.39 12.60 5 -10 -5 234.63 13.16 -5 10 4 99.72 8.59 5 -10 -4 103.80 4.39 -5 10 4 113.34 5.80 5 -10 -4 127.55 9.28 5 -10 -4 109.54 9.03 5 -10 -3 163.99 10.62 5 -10 -3 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74.89 4.69 -5 9 16 44.47 3.50 5 -9 -16 36.33 2.67 5 -9 -16 44.31 3.60 5 -9 -15 22.12 2.67 -5 9 15 22.66 2.63 5 -9 -15 23.12 2.18 5 -9 -14 37.89 3.39 -5 9 14 31.98 8.45 5 -9 -14 35.11 6.71 5 -9 -14 31.99 2.58 5 -9 -14 34.15 6.11 -5 9 14 33.59 2.99 5 -9 -13 14.35 4.55 5 -9 -13 23.21 2.19 -5 9 13 24.41 6.93 5 -9 -13 25.00 2.76 5 -9 -13 21.05 5.19 5 -9 -12 11.37 3.86 -5 9 12 11.92 5.24 5 -9 -12 16.98 2.25 5 -9 -12 14.59 1.85 5 -9 -12 13.10 4.09 5 -9 -11 105.43 9.54 5 -9 -11 94.35 9.19 5 -9 -11 97.98 4.21 5 -9 -11 109.91 5.21 -5 9 11 96.04 11.45 5 -9 -10 -0.39 2.32 5 -9 -10 -0.22 0.97 -5 9 10 4.86 3.36 5 -9 -10 2.82 1.34 5 -9 -10 -2.38 2.07 5 -9 -9 5.82 2.38 -5 9 9 -2.23 3.09 5 -9 -9 3.98 1.37 5 -9 -9 4.33 1.10 5 -9 -9 5.19 3.01 5 -9 -8 132.57 9.61 5 -9 -8 125.94 9.72 5 -9 -8 136.87 4.70 5 -9 -8 138.48 5.41 -5 9 8 138.16 11.15 5 -9 -7 49.50 5.86 -5 9 7 41.17 5.99 5 -9 -6 5.63 2.31 -5 9 6 5.53 2.79 5 -9 -5 132.86 8.78 -5 9 5 134.92 9.53 5 -9 -4 264.78 12.76 -5 9 4 254.28 12.91 -5 9 3 14.83 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9.39 1.73 7 -11 1 7.24 1.47 -7 11 -1 8.47 2.31 7 -11 2 4.57 1.31 7 -11 2 3.92 1.32 -7 11 -2 7.24 2.32 7 -11 3 1.22 0.97 7 -11 3 0.88 1.07 -7 11 -3 0.27 1.60 7 -11 4 2.07 1.14 7 -11 4 -1.57 1.10 -7 11 -4 1.08 1.67 7 -11 5 37.91 2.98 7 -11 5 33.20 2.50 -7 11 -5 33.66 3.85 7 -11 6 4.23 1.44 7 -11 6 4.14 1.12 -7 11 -6 3.57 2.12 7 -11 7 5.55 1.34 7 -11 7 4.95 1.09 -7 11 -7 6.39 2.12 -7 11 -8 0.57 1.55 7 -11 8 0.37 1.05 -7 11 -9 12.29 2.43 7 -11 9 11.42 1.67 7 -11 10 41.95 2.72 -7 11 -10 39.29 3.66 -7 11 -11 17.04 2.47 -7 11 -12 20.91 2.26 -7 11 -12 22.91 2.53 7 -11 12 23.14 1.67 -7 11 -13 43.48 3.11 7 -11 13 43.64 1.96 -7 11 -13 37.22 2.33 -7 11 -14 6.10 1.22 -7 10 22 1.44 1.14 7 -10 -22 3.24 0.73 7 -10 -21 0.88 0.69 7 -10 -21 1.07 0.63 7 -10 -20 24.62 1.84 7 -10 -20 22.69 1.72 7 -10 -19 8.44 1.30 7 -10 -19 5.50 1.15 7 -10 -18 5.12 1.16 7 -10 -18 6.89 1.58 7 -10 -17 71.36 3.42 7 -10 -17 72.12 4.35 7 -10 -16 11.59 1.63 7 -10 -16 12.51 2.03 7 -10 -15 14.26 1.93 -7 10 15 15.68 2.11 7 -10 -15 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21.83 2.18 -7 9 12 13.74 5.23 7 -9 -12 16.61 4.60 7 -9 -11 59.62 4.08 7 -9 -11 53.26 7.49 -7 9 11 55.41 3.91 7 -9 -11 60.44 3.51 -7 9 11 58.56 10.54 7 -9 -11 56.74 7.93 7 -9 -10 85.36 4.76 -7 9 10 75.08 10.89 7 -9 -10 78.29 8.40 7 -9 -10 78.08 9.06 7 -9 -10 81.06 3.97 -7 9 10 78.88 4.57 -7 9 9 -0.45 3.80 7 -9 -9 1.10 2.15 -7 9 9 -1.68 1.53 7 -9 -9 2.43 2.00 7 -9 -9 2.19 0.99 -7 9 8 6.59 3.95 -7 9 8 1.24 1.98 -7 9 8 0.45 1.40 7 -9 -8 3.32 2.81 7 -9 -8 0.15 0.95 -7 9 7 24.55 2.66 7 -9 -7 25.49 2.37 7 -9 -7 25.08 4.77 -7 9 7 25.71 3.52 -7 9 7 24.99 5.93 -7 9 6 78.14 8.53 -7 9 6 88.26 5.87 -7 9 6 95.93 4.92 7 -9 -6 91.42 4.35 7 -9 -6 92.27 8.09 7 -9 -5 40.75 5.67 7 -9 -5 37.65 2.76 -7 9 5 37.63 3.81 -7 9 5 39.98 6.13 -7 9 4 -0.99 2.72 7 -9 -4 -0.07 1.69 7 -9 -4 0.92 0.90 7 -9 -4 0.30 0.98 -7 9 4 -0.45 1.55 7 -9 -3 -0.57 1.65 -7 9 3 3.30 1.64 7 -9 -3 1.95 0.86 7 -9 -3 0.06 1.06 7 -9 -2 50.67 2.94 -7 9 2 51.52 3.97 7 -9 -2 49.70 5.99 7 -9 -2 49.83 3.14 7 -9 -1 60.96 3.22 -7 9 1 68.27 4.67 7 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45.16 5.67 -8 8 5 55.81 7.57 8 -8 -5 50.09 3.15 -8 8 5 43.34 3.29 -8 8 5 41.99 3.84 8 -8 -4 105.33 8.52 -8 8 4 109.42 5.81 8 -8 -4 114.39 4.77 8 -8 -4 102.37 4.06 8 -8 -3 38.90 2.58 -8 8 3 41.14 3.68 8 -8 -3 37.78 2.82 8 -8 -3 43.13 5.65 8 -8 -2 29.78 2.38 8 -8 -2 36.28 2.81 -8 8 2 27.96 3.04 8 -8 -2 29.90 4.70 8 -8 -1 39.23 5.29 8 -8 -1 35.46 2.56 -8 8 1 35.89 4.69 -8 8 1 35.91 3.42 8 -8 -1 39.65 2.88 8 -8 0 -1.36 1.87 8 -8 0 -0.26 0.95 8 -8 0 1.15 1.07 -8 8 0 0.75 1.84 -8 8 0 3.25 1.74 8 -8 1 39.25 2.84 -8 8 -1 47.04 3.88 8 -8 1 42.94 2.88 -8 8 -1 42.17 5.13 8 -8 1 38.71 5.88 8 -8 2 5.04 1.34 -8 8 -2 3.57 1.75 8 -8 2 4.56 1.34 -8 8 -2 6.75 2.79 8 -8 2 5.02 2.94 8 -8 3 8.11 1.59 -8 8 -3 7.51 1.94 8 -8 3 8.50 1.45 8 -8 3 9.19 3.37 -8 8 -3 8.73 3.05 -8 8 -4 18.14 2.95 8 -8 4 17.56 2.13 8 -8 4 14.14 4.10 -8 8 -4 18.45 3.89 -8 8 -5 6.99 1.78 8 -8 5 8.22 1.62 8 -8 5 6.51 3.46 -8 8 -5 5.45 2.79 -8 8 -6 12.67 2.62 8 -8 6 11.86 1.79 8 -8 6 10.90 4.53 -8 8 -6 12.78 3.42 -8 8 -7 8.86 2.53 8 -8 7 5.07 1.35 -8 8 -8 97.30 6.05 8 -8 8 101.55 4.65 -8 8 -9 0.15 1.73 8 -8 9 1.46 1.15 -8 8 -10 11.76 2.39 8 -8 10 9.97 1.70 -8 8 -11 -0.66 1.57 -8 8 -11 -0.54 1.44 8 -8 11 1.13 1.03 -8 8 -12 11.83 2.42 8 -8 12 13.93 1.80 -8 8 -13 22.49 2.90 8 -8 13 19.30 1.91 -8 8 -13 21.60 2.43 -8 8 -14 12.32 2.13 8 -8 15 41.30 2.29 -8 8 -15 42.40 3.32 8 -8 16 95.58 3.12 8 -8 17 62.22 2.16 8 -7 -23 0.97 0.60 -8 7 22 8.61 1.24 8 -7 -22 10.07 1.20 8 -7 -22 6.84 0.91 8 -7 -22 7.59 1.05 8 -7 -21 59.49 2.82 8 -7 -21 51.76 2.43 8 -7 -21 57.54 2.88 -8 7 21 53.69 3.05 8 -7 -20 37.92 2.52 8 -7 -20 41.15 2.60 8 -7 -20 42.73 2.40 -8 7 20 43.14 2.94 8 -7 -19 13.93 1.58 -8 7 19 18.61 2.23 8 -7 -18 3.12 1.32 -8 7 18 3.10 1.55 8 -7 -18 0.07 0.94 8 -7 -17 41.50 3.31 8 -7 -17 38.32 2.87 -8 7 17 39.45 3.49 8 -7 -16 5.06 1.69 -8 7 16 0.77 1.33 8 -7 -16 4.51 1.26 8 -7 -15 312.19 9.08 8 -7 -15 326.00 7.92 8 -7 -14 26.80 2.58 8 -7 -14 32.33 3.21 8 -7 -13 92.56 4.97 8 -7 -13 77.95 9.56 -8 7 13 81.18 11.86 -8 7 13 102.72 5.31 8 -7 -13 95.75 4.30 8 -7 -13 93.18 9.62 8 -7 -12 1.70 1.17 8 -7 -12 4.74 2.40 8 -7 -12 2.49 2.23 8 -7 -12 4.42 3.16 -8 7 12 0.68 3.56 -8 7 12 0.28 1.28 8 -7 -12 -0.71 1.45 8 -7 -11 31.38 2.97 8 -7 -11 23.94 4.31 8 -7 -11 25.71 5.04 -8 7 11 26.04 7.02 -8 7 11 23.80 2.85 8 -7 -11 29.18 2.43 8 -7 -10 -0.14 1.36 8 -7 -10 2.35 2.53 8 -7 -10 -0.32 1.94 -8 7 10 0.05 4.29 -8 7 10 0.26 1.49 8 -7 -10 2.42 1.02 8 -7 -9 80.94 8.10 8 -7 -9 85.49 7.10 -8 7 9 80.81 4.51 -8 7 9 70.02 9.42 8 -7 -9 82.89 4.58 8 -7 -9 83.26 4.00 8 -7 -8 50.82 5.33 -8 7 8 51.19 3.64 -8 7 8 49.55 7.72 8 -7 -8 51.92 3.10 8 -7 -8 55.82 6.70 8 -7 -7 37.09 4.49 -8 7 7 35.01 3.08 8 -7 -7 34.64 4.95 8 -7 -7 38.86 2.71 -8 7 7 31.42 5.96 8 -7 -6 5.16 2.08 -8 7 6 4.99 1.85 -8 7 6 5.81 3.50 -8 7 6 1.73 1.47 8 -7 -6 2.68 1.12 8 -7 -6 2.87 1.93 -8 7 5 0.99 1.69 8 -7 -5 0.77 1.03 -8 7 5 -0.22 3.08 8 -7 -5 2.67 2.00 -8 7 5 1.42 1.30 8 -7 -5 1.69 1.44 8 -7 -4 58.15 6.20 8 -7 -4 49.88 3.06 -8 7 4 49.50 6.30 8 -7 -4 49.22 5.01 -8 7 4 51.47 4.00 -8 7 3 52.16 3.90 8 -7 -3 54.19 5.84 -8 7 3 52.78 5.35 8 -7 -3 52.88 5.07 8 -7 -3 59.39 3.28 8 -7 -2 10.71 1.52 -8 7 2 10.55 1.90 8 -7 -2 7.53 2.61 -8 7 2 9.25 2.48 8 -7 -2 11.54 2.72 8 -7 -1 244.25 6.57 -8 7 1 241.06 8.08 8 -7 -1 234.24 6.00 8 -7 -1 264.46 12.99 -8 7 1 233.24 11.01 -8 7 0 9.15 2.64 -8 7 0 7.36 1.81 8 -7 0 14.02 3.58 8 -7 0 9.37 2.15 8 -7 0 9.71 1.49 8 -7 0 10.76 1.64 -8 7 -1 200.58 10.65 -8 7 -1 214.09 7.53 8 -7 1 203.48 12.41 8 -7 1 214.76 9.90 8 -7 1 210.27 6.04 8 -7 1 204.31 6.08 -8 7 -2 96.23 5.23 -8 7 -2 96.07 7.79 8 -7 2 88.52 6.44 8 -7 2 88.79 4.02 8 -7 2 86.65 8.36 8 -7 3 25.43 2.41 -8 7 -3 26.86 3.15 -8 7 -3 34.37 5.05 8 -7 3 24.02 4.89 8 -7 4 376.86 8.41 -8 7 -4 372.64 10.49 -8 7 -4 384.72 15.95 8 -7 4 367.40 18.07 8 -7 5 2.04 1.27 -8 7 -5 1.15 1.50 -8 7 -5 0.03 1.77 8 -7 5 3.34 2.59 8 -7 6 23.16 2.38 -8 7 -6 24.96 3.07 -8 7 -6 23.33 4.41 8 -7 6 19.74 4.83 8 -7 7 7.37 1.55 -8 7 -7 11.48 2.48 -8 7 -7 8.83 3.09 8 -7 8 2.96 1.32 -8 7 -8 1.15 1.59 8 -7 9 9.28 1.74 -8 7 -9 10.36 2.34 8 -7 10 221.01 6.83 -8 7 -10 199.99 8.55 8 -7 11 75.54 3.99 -8 7 -11 67.43 5.19 -8 7 -12 6.58 2.07 8 -7 12 3.59 1.23 -8 7 -12 3.42 1.69 -8 7 -13 7.29 2.21 8 -7 13 6.00 1.37 -8 7 -13 6.02 1.90 -8 7 -14 139.72 6.67 -8 7 -15 4.32 1.69 8 -7 16 143.26 4.16 -8 7 -16 145.09 5.90 8 -7 17 19.09 1.48 8 -7 18 110.97 2.96 8 -6 -23 17.34 1.37 8 -6 -23 16.59 1.32 8 -6 -22 2.58 0.84 8 -6 -22 0.70 0.54 8 -6 -22 1.46 0.75 -8 6 21 53.47 3.10 8 -6 -21 48.16 2.76 8 -6 -21 49.80 2.79 8 -6 -21 46.27 2.40 -8 6 20 4.15 1.33 8 -6 -20 3.32 0.97 8 -6 -19 27.75 2.26 8 -6 -19 28.05 2.40 -8 6 19 30.50 2.70 8 -6 -18 3.80 1.24 8 -6 -18 1.55 1.16 -8 6 18 0.33 1.22 8 -6 -17 -0.16 0.92 8 -6 -17 1.84 1.37 -8 6 17 0.47 1.25 8 -6 -16 9.63 1.63 8 -6 -16 10.41 2.02 -8 6 16 9.58 2.13 8 -6 -15 20.00 2.27 -8 6 15 16.50 2.46 8 -6 -15 14.99 2.21 8 -6 -14 89.37 10.71 8 -6 -14 88.73 8.84 -8 6 14 101.54 5.12 8 -6 -14 113.52 5.44 8 -6 -14 101.34 4.55 8 -6 -13 9.90 1.53 8 -6 -13 9.46 3.90 8 -6 -13 3.33 2.31 -8 6 13 11.38 2.13 -8 6 13 11.37 5.71 8 -6 -13 6.60 3.18 8 -6 -13 8.45 1.83 8 -6 -12 12.57 2.12 8 -6 -12 9.60 4.00 8 -6 -12 6.50 2.83 -8 6 12 5.84 4.71 8 -6 -12 8.64 1.53 -8 6 12 9.44 1.98 8 -6 -11 87.28 9.12 8 -6 -11 72.94 7.28 -8 6 11 81.00 10.90 -8 6 11 78.31 4.39 8 -6 -11 79.60 3.94 8 -6 -11 78.09 4.42 8 -6 -10 57.50 7.06 8 -6 -10 58.86 6.14 -8 6 10 58.93 3.82 -8 6 10 49.03 7.77 8 -6 -10 61.78 3.50 8 -6 -10 59.97 3.78 8 -6 -9 40.14 5.67 8 -6 -9 33.51 4.63 -8 6 9 31.24 2.86 8 -6 -9 32.32 2.79 8 -6 -9 34.87 2.61 -8 6 9 29.88 6.20 8 -6 -8 4.73 2.11 -8 6 8 5.93 3.72 -8 6 8 6.18 1.42 8 -6 -8 7.12 1.47 8 -6 -8 6.55 1.30 8 -6 -8 8.33 2.46 8 -6 -7 306.55 13.74 8 -6 -7 289.08 6.89 -8 6 7 278.64 16.20 8 -6 -7 294.30 11.91 8 -6 -6 62.69 6.36 -8 6 6 67.73 7.82 8 -6 -6 74.39 5.95 -8 6 5 128.64 8.14 8 -6 -5 131.80 8.76 -8 6 5 122.11 9.69 8 -6 -5 127.85 7.66 -8 6 4 133.88 7.85 8 -6 -4 137.72 8.89 -8 6 4 140.97 10.20 8 -6 -4 139.86 7.72 8 -6 -3 -0.72 1.40 -8 6 3 3.52 1.46 8 -6 -3 -0.38 1.48 -8 6 3 3.68 2.83 8 -6 -2 10.17 2.19 -8 6 2 9.25 2.26 8 -6 -2 10.45 2.67 -8 6 1 47.69 4.80 8 -6 -1 53.62 5.72 8 -6 -1 53.24 5.91 8 -6 -1 59.02 5.27 -8 6 0 485.61 15.42 8 -6 0 480.12 18.02 8 -6 0 478.39 14.56 -8 6 -1 151.06 8.80 8 -6 1 162.65 10.76 8 -6 1 161.31 8.40 -8 6 -2 115.93 7.96 8 -6 2 136.72 8.08 8 -6 2 113.43 9.23 -8 6 -3 4.03 1.39 -8 6 -3 4.40 1.95 8 -6 3 4.60 2.18 8 -6 3 7.30 3.12 8 -6 3 5.09 1.35 -8 6 -4 120.79 5.80 -8 6 -4 119.62 8.60 8 -6 4 126.53 4.69 8 -6 4 123.65 10.02 8 -6 4 137.94 8.24 -8 6 -5 5.81 1.79 -8 6 -5 6.68 2.48 8 -6 5 5.16 2.17 8 -6 5 5.67 1.45 8 -6 5 6.46 3.27 -8 6 -6 3.64 1.77 -8 6 -6 3.58 1.88 8 -6 6 2.70 1.88 8 -6 6 4.41 1.27 8 -6 6 6.28 3.75 -8 6 -7 30.22 3.28 -8 6 -7 33.55 5.00 8 -6 7 30.70 4.58 8 -6 7 32.23 2.57 8 -6 7 32.49 6.09 8 -6 8 110.04 4.77 -8 6 -8 109.06 6.05 -8 6 -8 100.33 8.97 8 -6 8 98.31 10.11 8 -6 9 7.02 1.61 -8 6 -9 5.08 1.92 -8 6 -9 3.17 1.76 8 -6 9 3.71 2.49 8 -6 10 319.15 8.12 -8 6 -10 313.00 10.55 8 -6 11 1.31 1.03 -8 6 -11 1.99 1.90 8 -6 12 3.26 1.15 -8 6 -12 4.42 2.04 -8 6 -12 0.50 1.55 -8 6 -13 5.40 2.19 8 -6 13 6.33 1.42 -8 6 -13 5.52 1.57 -8 6 -14 20.17 2.93 -8 6 -14 18.86 2.61 8 -6 14 18.84 1.86 -8 6 -15 50.78 4.17 8 -6 16 161.70 4.80 -8 6 -16 161.75 6.67 8 -6 17 61.99 2.88 8 -6 18 289.88 5.44 8 -6 19 1.70 0.60 8 -5 -23 7.41 0.95 8 -5 -23 8.04 1.01 8 -5 -23 7.22 0.81 -8 5 23 7.65 1.12 8 -5 -22 2.65 0.88 -8 5 22 2.36 1.02 8 -5 -22 1.36 0.68 8 -5 -22 2.22 0.68 8 -5 -21 4.71 0.94 -8 5 21 6.12 1.47 8 -5 -20 17.96 1.78 -8 5 20 18.17 2.12 8 -5 -19 11.83 1.61 -8 5 19 13.20 1.95 8 -5 -18 2.55 1.01 8 -5 -18 2.90 1.10 -8 5 18 4.53 1.66 8 -5 -17 62.26 3.85 8 -5 -17 57.84 3.41 -8 5 17 62.05 4.11 8 -5 -16 33.79 3.03 8 -5 -16 35.08 2.73 -8 5 16 38.64 3.42 8 -5 -15 11.79 2.05 -8 5 15 8.50 1.91 8 -5 -15 11.47 1.69 8 -5 -14 5.33 1.45 8 -5 -14 1.39 2.20 8 -5 -14 6.57 3.24 8 -5 -14 7.82 1.83 -8 5 14 3.69 5.24 -8 5 14 2.92 1.65 8 -5 -14 -0.35 2.64 8 -5 -13 47.75 3.14 8 -5 -13 44.57 6.43 8 -5 -13 43.51 6.23 -8 5 13 49.26 3.63 -8 5 13 40.13 8.35 8 -5 -13 52.55 7.88 8 -5 -13 54.95 3.84 8 -5 -12 53.61 3.59 8 -5 -12 46.17 6.11 8 -5 -12 42.63 6.90 -8 5 12 62.39 9.69 8 -5 -12 52.63 3.19 -8 5 12 51.43 3.68 8 -5 -11 28.73 2.71 8 -5 -11 27.45 5.46 8 -5 -11 19.40 3.93 -8 5 11 25.86 6.44 8 -5 -11 28.34 2.40 -8 5 11 27.95 2.81 8 -5 -10 110.32 9.42 -8 5 10 100.71 4.70 8 -5 -10 99.37 4.23 8 -5 -10 104.35 4.84 8 -5 -10 98.60 7.73 -8 5 10 96.52 10.85 8 -5 -9 63.41 6.91 -8 5 9 61.76 8.55 8 -5 -9 64.76 3.36 8 -5 -9 63.18 3.77 -8 5 9 62.59 3.71 8 -5 -9 57.96 5.94 8 -5 -8 88.08 7.63 -8 5 8 73.40 8.97 8 -5 -8 76.65 6.39 8 -5 -7 7.89 2.15 8 -5 -7 6.47 1.98 -8 5 7 8.24 3.77 8 -5 -6 24.03 3.96 -8 5 6 19.32 3.39 8 -5 -6 20.73 3.34 -8 5 6 21.43 5.07 8 -5 -5 25.18 3.87 -8 5 5 27.87 4.02 8 -5 -5 27.39 3.53 -8 5 5 22.59 5.04 -8 5 4 48.43 4.77 8 -5 -4 53.67 5.28 -8 5 4 57.50 6.41 8 -5 -4 49.87 4.65 8 -5 -3 100.19 7.27 -8 5 3 91.31 6.36 -8 5 3 91.06 7.64 8 -5 -3 92.93 6.18 -8 5 2 10.53 3.10 -8 5 2 8.35 2.25 8 -5 -2 5.77 2.01 8 -5 -2 7.48 2.03 -8 5 1 10.63 2.47 8 -5 -1 2.08 1.69 8 -5 -1 7.23 2.19 8 -5 -1 7.89 2.29 -8 5 0 174.64 8.86 8 -5 0 200.81 10.84 8 -5 0 191.27 8.80 -8 5 -1 136.65 8.11 8 -5 1 133.94 9.11 8 -5 1 142.58 7.99 -8 5 -2 141.10 8.41 8 -5 2 141.47 9.61 8 -5 2 155.88 8.43 -8 5 -3 56.82 5.57 8 -5 3 60.22 5.41 8 -5 3 54.90 6.17 -8 5 -4 207.40 10.81 8 -5 4 194.96 9.88 8 -5 4 173.94 11.21 -8 5 -5 15.64 2.20 -8 5 -5 14.08 3.22 8 -5 5 15.50 3.38 8 -5 5 14.37 1.73 8 -5 5 9.78 3.44 8 -5 6 156.94 5.26 -8 5 -6 163.99 6.74 -8 5 -6 168.38 10.41 8 -5 6 157.66 11.45 8 -5 7 59.49 3.43 -8 5 -7 55.86 4.26 -8 5 -7 69.05 6.87 8 -5 7 58.83 7.47 8 -5 8 86.85 4.13 -8 5 -8 80.00 5.16 -8 5 -8 74.59 7.44 8 -5 8 79.69 8.72 8 -5 9 56.93 3.47 -8 5 -9 53.34 4.36 -8 5 -9 59.17 6.82 8 -5 9 60.00 8.11 8 -5 10 63.52 9.01 -8 5 -10 59.02 4.71 -8 5 -10 58.96 7.11 8 -5 10 68.60 3.69 -8 5 -11 14.64 2.70 8 -5 11 14.78 2.02 8 -5 12 217.36 6.60 -8 5 -12 194.78 8.15 -8 5 -12 209.41 8.74 8 -5 13 34.56 2.66 -8 5 -13 31.38 3.47 -8 5 -13 35.09 3.95 8 -5 14 10.78 1.34 -8 5 -14 13.65 2.34 -8 5 -15 44.89 4.04 -8 5 -15 49.53 3.80 -8 5 -16 1.27 1.43 -8 5 -16 1.03 1.39 -8 5 -17 120.25 5.78 8 -5 17 129.58 4.30 8 -5 18 75.37 3.06 8 -5 19 159.84 4.02 8 -4 -23 0.75 0.65 8 -4 -23 0.30 0.53 -8 4 23 -1.24 0.80 8 -4 -23 0.63 0.61 8 -4 -22 -0.54 0.65 -8 4 22 0.18 0.86 8 -4 -22 1.13 0.78 8 -4 -22 0.38 0.64 -8 4 21 6.08 1.44 8 -4 -21 6.75 1.13 -8 4 20 10.66 1.80 8 -4 -20 8.05 1.32 -8 4 19 3.44 1.58 8 -4 -19 -0.91 0.94 -8 4 18 4.89 1.66 8 -4 -18 3.56 1.19 -8 4 17 29.20 2.88 8 -4 -17 30.22 2.55 -8 4 16 184.45 7.04 8 -4 -16 184.28 6.55 8 -4 -16 189.03 6.13 -8 4 15 37.03 3.18 8 -4 -15 29.95 2.60 8 -4 -15 34.03 2.99 8 -4 -14 -0.09 1.32 8 -4 -14 -0.83 2.78 -8 4 14 3.80 5.28 8 -4 -14 3.23 2.58 -8 4 14 4.10 1.55 8 -4 -14 1.37 1.07 8 -4 -14 -1.80 2.67 8 -4 -13 2.06 2.53 -8 4 13 7.16 5.57 8 -4 -13 6.54 1.78 -8 4 13 5.19 1.65 8 -4 -13 8.00 1.61 8 -4 -13 3.49 2.25 8 -4 -12 1.32 2.64 -8 4 12 2.69 4.26 -8 4 12 -0.26 1.27 8 -4 -12 -0.51 1.10 8 -4 -12 -0.21 0.97 8 -4 -12 -0.78 1.73 8 -4 -11 263.17 15.05 8 -4 -11 241.60 7.23 -8 4 11 254.75 7.33 8 -4 -11 241.82 6.54 8 -4 -11 216.23 12.08 -8 4 11 240.59 17.28 8 -4 -10 14.64 3.84 -8 4 10 9.25 4.80 8 -4 -10 11.31 1.73 8 -4 -10 12.93 1.70 8 -4 -10 9.19 2.59 -8 4 10 10.07 1.82 8 -4 -9 54.28 6.36 8 -4 -9 51.55 5.35 -8 4 9 37.31 6.83 8 -4 -8 16.02 3.55 -8 4 8 22.66 3.71 8 -4 -8 19.24 2.54 8 -4 -8 14.28 2.93 -8 4 8 16.55 4.44 -8 4 7 273.59 11.86 8 -4 -7 285.59 12.62 -8 4 7 266.39 15.13 8 -4 -7 275.29 11.47 -8 4 6 116.02 7.90 8 -4 -6 120.96 7.93 -8 4 6 112.24 9.65 8 -4 -6 111.48 7.08 8 -4 -5 0.60 1.32 -8 4 5 2.04 1.65 8 -4 -5 1.84 1.63 8 -4 -4 430.88 14.14 -8 4 4 418.12 16.14 8 -4 -4 440.37 13.24 -8 4 4 453.58 14.02 8 -4 -3 316.41 11.90 -8 4 3 306.27 13.04 8 -4 -3 308.77 10.89 -8 4 3 297.46 11.19 8 -4 -2 68.64 5.73 -8 4 2 58.00 5.64 8 -4 -2 56.05 4.80 -8 4 2 67.11 5.36 -8 4 1 174.59 8.50 8 -4 -1 190.24 9.31 8 -4 -1 180.69 9.66 -8 4 1 175.52 8.43 8 -4 -1 184.65 8.41 -8 4 0 136.24 7.53 8 -4 0 126.85 8.30 8 -4 0 117.03 7.03 -8 4 -1 435.39 13.68 8 -4 1 431.41 15.43 8 -4 1 439.14 13.89 8 -4 2 58.98 5.04 8 -4 2 59.16 5.96 -8 4 -2 48.97 4.81 -8 4 -3 5.57 1.96 8 -4 3 8.85 2.87 8 -4 3 6.65 2.26 -8 4 -4 0.77 1.39 8 -4 4 -0.39 1.85 8 -4 4 1.64 1.73 -8 4 -5 110.75 7.66 8 -4 5 110.11 8.88 -8 4 -6 3.75 1.74 8 -4 6 1.57 1.95 8 -4 7 1.94 1.06 -8 4 -7 1.79 1.27 -8 4 -7 6.05 2.19 8 -4 7 1.80 2.30 8 -4 8 144.69 5.10 -8 4 -8 148.45 6.71 -8 4 -8 149.94 9.98 8 -4 8 153.74 11.90 8 -4 9 61.20 3.43 -8 4 -9 55.90 4.31 -8 4 -9 51.64 6.09 8 -4 9 55.16 7.36 8 -4 10 34.72 2.68 -8 4 -10 35.73 3.66 -8 4 -10 35.85 5.31 8 -4 10 37.11 6.74 8 -4 11 127.81 12.01 -8 4 -11 125.22 6.50 -8 4 -11 129.70 10.05 -8 4 -12 34.54 3.69 8 -4 12 27.30 2.39 8 -4 13 204.24 6.22 -8 4 -13 191.40 8.02 -8 4 -13 189.33 8.38 -8 4 -14 111.14 6.34 -8 4 -14 107.54 5.93 -8 4 -15 0.91 1.68 -8 4 -15 3.51 1.68 -8 4 -16 163.57 7.31 -8 4 -16 157.54 6.66 8 -4 17 0.18 0.92 -8 4 -17 1.84 1.69 -8 4 -17 1.32 1.28 8 -4 18 90.87 3.57 8 -4 19 12.47 1.46 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-8 -6 -16 5.44 2.16 -8 -6 -16 0.82 1.54 8 6 16 0.72 3.01 -8 -6 -16 2.26 1.13 -8 -6 -17 13.13 1.92 -8 -6 -17 14.75 2.81 -8 -6 -17 11.08 2.55 8 6 17 11.91 5.17 -8 -6 -17 13.45 1.81 -8 -6 -18 106.94 4.73 -8 -6 -18 100.36 5.92 -8 -6 -18 104.70 4.61 -8 -6 -18 96.70 5.92 -8 -6 -19 5.96 1.42 -8 -6 -19 6.70 2.26 -8 -6 -19 9.07 1.63 -8 -6 -19 9.16 2.12 -8 -6 -20 174.86 7.60 -8 -6 -20 181.06 5.76 -8 -6 -20 181.19 5.68 -8 -6 -21 6.54 1.89 -8 -6 -21 4.33 1.13 -8 -6 -21 4.58 1.04 -8 -6 -22 1.70 1.23 -8 -6 -23 39.62 3.08 -8 -6 -24 25.47 2.26 -8 -6 -25 18.82 1.62 -8 -7 20 9.22 1.17 8 7 -20 12.01 1.18 -8 -7 19 1.33 0.91 8 7 -19 2.43 0.81 -8 -7 18 9.53 1.43 8 7 -18 9.23 1.41 -8 -7 18 8.47 1.74 -8 -7 17 62.44 3.29 8 7 -17 56.53 3.26 -8 -7 17 58.64 4.01 -8 -7 16 35.52 2.63 8 7 -16 37.28 2.81 -8 -7 16 35.82 3.29 -8 -7 15 5.89 1.83 -8 -7 15 5.48 1.34 8 7 -15 5.68 1.52 8 7 -14 13.02 2.01 -8 -7 14 12.59 2.17 -8 -7 14 13.39 1.87 -8 -7 13 246.93 6.69 8 7 -13 253.35 7.68 -8 -7 13 263.26 8.19 8 7 -12 200.82 11.89 -8 -7 12 203.41 7.02 -8 -7 12 202.67 5.81 8 7 -12 226.93 7.38 8 7 -11 30.49 2.98 -8 -7 11 34.78 2.87 -8 -7 11 28.41 2.78 -8 -7 11 30.42 2.36 8 7 -11 33.77 4.78 -8 -7 10 23.38 2.28 -8 -7 10 21.25 2.35 8 7 -10 20.53 2.50 -8 -7 10 17.73 1.80 8 7 -10 13.34 3.40 8 7 -10 20.36 3.66 8 7 -9 57.72 5.81 -8 -7 9 54.18 3.40 8 7 -9 60.41 3.93 -8 -7 9 54.68 3.20 -8 -7 9 53.65 2.89 -8 -7 8 22.18 1.97 -8 -7 8 22.52 3.54 8 7 -8 14.80 2.81 8 7 -8 25.89 3.80 8 7 -7 126.06 8.04 8 7 -7 123.89 8.40 -8 -7 7 125.02 7.68 8 7 -6 744.47 18.54 8 7 -6 701.01 18.41 -8 -7 6 690.25 17.20 8 7 -5 411.62 13.13 8 7 -5 378.01 12.48 -8 -7 5 385.90 12.56 8 7 -4 152.81 7.67 -8 -7 4 154.65 7.77 8 7 -4 156.12 7.63 -8 -7 3 11.17 2.37 8 7 -3 9.36 2.09 8 7 -3 13.49 2.49 -8 -7 2 4.95 2.13 8 7 -2 1.90 1.31 8 7 -2 3.24 1.59 -8 -7 1 198.31 8.49 8 7 -1 199.00 7.35 8 7 -1 193.18 7.81 8 7 0 936.75 15.12 -8 -7 0 954.44 18.07 8 7 0 899.46 15.87 8 7 1 27.84 2.93 -8 -7 -1 32.54 3.77 8 7 1 33.64 3.28 -8 -7 -1 26.25 3.28 -8 -7 -2 1889.21 25.73 -8 -7 -2 1829.53 23.95 8 7 2 1842.71 21.35 -8 -7 -3 5.70 1.98 8 7 3 11.29 1.99 -8 -7 -3 9.31 3.56 -8 -7 -3 11.71 2.31 -8 -7 -4 1021.17 17.62 -8 -7 -4 1043.77 24.05 8 7 4 1100.03 16.48 -8 -7 -4 1052.80 18.25 -8 -7 -5 9.08 2.25 -8 -7 -5 4.57 2.97 8 7 5 3.62 2.07 -8 -7 -5 5.64 2.04 -8 -7 -6 410.13 10.63 -8 -7 -6 386.94 11.22 8 7 6 382.27 9.39 -8 -7 -6 452.50 16.75 8 7 6 457.10 14.26 -8 -7 -7 0.91 1.25 8 7 7 3.55 1.67 -8 -7 -7 5.22 3.09 8 7 7 0.81 2.45 -8 -7 -7 4.01 1.61 -8 -7 -8 59.18 4.01 8 7 8 63.98 6.14 -8 -7 -8 65.14 4.91 -8 -7 -8 63.23 6.84 -8 -7 -9 64.90 4.33 -8 -7 -9 59.78 6.62 8 7 9 69.33 6.93 -8 -7 -10 273.78 8.70 -8 -7 -10 275.68 14.21 8 7 10 272.04 13.91 -8 -7 -11 8.07 3.19 8 7 11 7.13 2.60 -8 -7 -12 5.82 3.24 8 7 12 6.20 3.33 -8 -7 -13 13.34 3.86 8 7 13 8.78 3.87 8 7 14 41.75 7.16 -8 -7 -14 44.84 7.22 -8 -7 -14 34.38 2.64 -8 -7 -14 40.33 3.59 -8 -7 -14 45.40 4.95 -8 -7 -14 37.99 2.80 8 7 15 89.60 10.66 -8 -7 -15 100.24 10.07 -8 -7 -15 87.56 4.24 -8 -7 -15 97.23 5.76 -8 -7 -15 96.23 5.47 -8 -7 -15 89.04 4.36 8 7 16 116.07 12.82 -8 -7 -16 120.03 5.04 -8 -7 -16 116.17 6.40 -8 -7 -16 124.18 6.52 -8 -7 -16 118.63 5.09 8 7 17 25.97 7.04 -8 -7 -17 21.10 2.27 -8 -7 -17 15.97 1.97 -8 -7 -17 17.87 2.86 -8 -7 -17 20.60 2.97 -8 -7 -18 305.44 8.13 -8 -7 -18 304.39 8.06 -8 -7 -18 312.03 10.46 -8 -7 -18 318.12 10.35 -8 -7 -19 1.60 1.02 -8 -7 -19 0.18 1.01 -8 -7 -19 0.95 1.55 -8 -7 -19 1.37 1.66 -8 -7 -20 145.57 5.39 -8 -7 -20 146.21 5.31 -8 -7 -20 140.99 6.71 -8 -7 -20 141.71 6.57 -8 -7 -21 33.23 2.52 -8 -7 -21 34.91 3.36 -8 -7 -21 33.08 2.58 -8 -7 -22 8.80 1.31 -8 -7 -22 7.56 1.24 -8 -7 -22 7.93 1.95 -8 -7 -23 -0.30 1.21 -8 -7 -24 -0.26 0.92 -8 -7 -25 13.29 1.47 8 8 -20 1.15 0.51 -8 -8 19 29.18 1.83 8 8 -19 33.09 1.94 -8 -8 18 6.31 1.52 -8 -8 18 7.52 1.20 8 8 -18 8.16 1.26 -8 -8 17 -1.26 0.94 8 8 -17 -0.55 0.90 -8 -8 17 0.04 1.20 -8 -8 17 -0.82 0.80 -8 -8 16 2.73 1.08 8 8 -16 0.32 1.08 -8 -8 16 0.92 1.24 -8 -8 15 90.74 5.03 -8 -8 15 89.71 3.95 8 8 -15 94.28 4.44 -8 -8 14 40.63 3.44 -8 -8 14 42.40 2.77 8 8 -14 37.84 3.00 -8 -8 13 121.05 5.73 -8 -8 13 127.38 4.71 -8 -8 12 2.73 1.28 8 8 -12 1.73 1.47 -8 -8 12 1.12 1.22 -8 -8 11 18.45 2.29 8 8 -11 17.25 3.58 -8 -8 11 20.29 2.01 8 8 -11 20.54 2.56 -8 -8 11 23.97 2.45 -8 -8 10 4.46 1.38 8 8 -10 3.53 1.93 8 8 -10 3.08 1.57 -8 -8 10 2.47 1.17 -8 -8 10 3.04 1.06 8 8 -9 34.33 4.87 -8 -8 9 26.90 2.16 -8 -8 9 30.59 2.51 -8 -8 9 30.19 2.65 8 8 -9 32.92 3.15 -8 -8 8 65.81 3.47 -8 -8 8 59.11 5.65 8 8 -8 68.58 4.26 8 8 -8 64.55 6.31 8 8 -8 57.74 5.76 -8 -8 8 64.18 3.52 -8 -8 7 17.51 3.09 8 8 -7 27.61 4.39 8 8 -7 31.78 4.31 8 8 -6 369.66 13.50 8 8 -6 376.70 13.83 -8 -8 6 384.91 13.43 8 8 -5 45.65 4.86 8 8 -5 50.44 4.88 -8 -8 5 40.17 4.42 8 8 -4 220.78 9.88 -8 -8 4 208.29 9.52 8 8 -3 129.95 6.61 8 8 -3 130.55 7.13 -8 -8 3 116.46 6.93 8 8 -2 1487.72 20.88 8 8 -2 1450.30 22.85 8 8 -1 247.90 8.17 -8 -8 1 235.54 9.37 8 8 0 526.33 12.70 -8 -8 0 523.56 14.08 -8 -8 -1 187.23 8.19 8 8 1 186.91 7.43 -8 -8 -2 279.47 10.00 8 8 2 255.07 8.16 -8 -8 -2 257.94 9.63 -8 -8 -2 265.93 12.24 -8 -8 -3 128.43 6.54 8 8 3 122.88 5.54 -8 -8 -3 111.92 6.35 -8 -8 -3 119.51 8.37 -8 -8 -4 372.24 11.17 8 8 4 368.15 9.30 -8 -8 -4 376.47 10.82 -8 -8 -4 393.44 15.24 -8 -8 -5 53.44 4.41 8 8 5 49.71 3.30 -8 -8 -5 47.01 4.02 -8 -8 -5 50.94 6.06 -8 -8 -6 142.68 6.98 8 8 6 136.90 6.42 -8 -8 -6 120.13 5.77 -8 -8 -6 138.29 9.59 8 8 7 230.52 10.88 -8 -8 -7 226.65 8.79 8 8 7 256.33 8.80 -8 -8 -7 232.52 8.15 -8 -8 -7 223.74 7.54 -8 -8 -7 231.86 12.16 8 8 8 327.97 14.01 -8 -8 -8 322.92 10.65 -8 -8 -8 337.15 15.01 -8 -8 -8 349.40 9.35 -8 -8 -8 337.99 10.88 -8 -8 -9 53.78 4.83 8 8 9 72.05 7.29 -8 -8 -9 60.58 6.77 -8 -8 -9 68.35 5.11 8 8 10 171.99 11.49 -8 -8 -10 162.52 11.08 -8 -8 -10 157.24 8.37 8 8 11 22.17 4.71 -8 -8 -11 21.10 4.18 -8 -8 -11 21.14 3.42 8 8 12 312.61 16.67 -8 -8 -12 294.09 15.50 -8 -8 -12 292.20 12.67 -8 -8 -13 24.17 5.07 -8 -8 -13 22.57 2.73 8 8 13 24.69 5.49 8 8 14 70.17 9.42 -8 -8 -14 78.26 8.79 -8 -8 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-17 128.01 4.35 -8 -9 17 122.91 4.12 -8 -9 17 122.94 5.24 -8 -9 16 0.94 0.95 -8 -9 16 0.37 1.10 8 9 -16 0.00 0.89 -8 -9 15 1.11 1.04 8 9 -15 0.12 1.00 -8 -9 15 0.34 1.11 -8 -9 14 137.63 4.78 -8 -9 14 139.43 5.95 8 9 -14 133.48 5.50 -8 -9 13 10.99 1.54 8 9 -13 12.16 1.96 -8 -9 13 11.20 2.05 -8 -9 12 392.59 7.97 -8 -9 12 407.28 9.98 8 9 -12 395.13 9.97 -8 -9 11 3.61 1.64 8 9 -11 3.37 1.76 -8 -9 11 3.73 1.13 8 9 -11 7.33 2.97 -8 -9 11 5.08 1.78 8 9 -10 3.71 1.56 -8 -9 10 4.18 1.39 8 9 -10 2.38 1.91 -8 -9 10 1.86 1.10 -8 -9 9 42.62 2.89 8 9 -9 45.61 3.69 -8 -9 9 47.39 3.23 8 9 -9 47.58 5.81 -8 -9 8 30.81 2.44 -8 -9 8 36.98 4.96 8 9 -8 36.03 4.77 -8 -9 8 33.84 2.73 8 9 -8 34.76 3.17 8 9 -7 392.03 9.93 -8 -9 7 377.01 7.72 -8 -9 7 366.56 7.95 8 9 -7 363.36 14.66 -8 -9 6 13.76 3.22 8 9 -6 9.28 2.53 -8 -9 5 207.52 10.35 8 9 -5 197.33 10.18 -8 -9 4 16.79 3.09 8 9 -4 20.51 3.23 -8 -9 3 51.95 4.88 8 9 -3 47.73 4.71 -8 -9 2 104.69 6.96 8 9 -2 94.77 6.28 -8 -9 1 621.02 15.88 8 9 -1 619.16 14.99 -8 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-23 4.74 1.08 -8 -9 -24 15.03 1.89 -8 -9 -24 12.83 1.28 -8 -9 -24 13.59 1.38 -8 -9 -25 2.76 0.97 -8 -9 -25 3.45 0.71 -8 -9 -25 5.50 0.81 -8 -9 -26 -0.12 0.56 8 10 -19 9.58 0.91 8 10 -18 69.96 2.72 -8 -10 18 64.58 3.42 8 10 -17 33.85 2.13 -8 -10 17 35.26 2.77 8 10 -16 136.65 4.61 -8 -10 16 147.08 4.30 -8 -10 16 143.75 5.69 -8 -10 15 20.49 2.48 8 10 -15 18.93 2.06 -8 -10 15 19.49 1.78 -8 -10 14 9.85 1.42 -8 -10 14 9.56 1.89 8 10 -14 9.55 1.72 -8 -10 13 1.65 0.97 -8 -10 13 3.71 1.51 8 10 -13 2.19 1.35 -8 -10 12 6.34 1.56 8 10 -12 8.00 1.88 -8 -10 11 112.81 5.19 -8 -10 11 115.98 5.09 8 10 -11 109.32 5.35 -8 -10 10 444.66 9.33 8 10 -10 425.86 10.99 -8 -10 10 440.16 10.04 8 10 -9 18.39 2.74 -8 -10 9 17.28 2.07 -8 -10 9 19.49 2.25 8 10 -9 24.61 4.50 8 10 -8 225.14 12.45 -8 -10 8 229.32 6.42 -8 -10 8 211.51 6.50 8 10 -8 227.27 7.84 -8 -10 8 212.78 11.84 8 10 -7 84.55 7.44 -8 -10 7 71.83 3.64 -8 -10 7 78.07 3.81 8 10 -7 72.03 4.63 8 10 -6 214.71 11.35 -8 -10 6 206.51 5.72 -8 -10 6 210.41 5.87 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8 11 -7 39.48 3.70 -8 -11 7 33.78 5.10 -8 -11 7 35.39 2.58 -8 -11 7 28.85 2.47 8 11 -6 -0.23 1.64 8 11 -6 -1.64 1.53 -8 -11 6 1.58 1.01 -8 -11 6 1.71 1.16 -8 -11 6 2.00 1.57 8 11 -5 181.12 10.50 -8 -11 5 194.26 5.63 -8 -11 5 186.80 10.98 8 11 -5 206.36 7.67 -8 -11 5 177.27 5.34 8 11 -4 53.02 5.57 -8 -11 4 51.51 5.63 -8 -11 4 61.01 3.23 8 11 -3 232.05 11.08 -8 -11 3 229.08 11.50 8 11 -2 100.92 7.15 -8 -11 2 107.92 7.72 8 11 -1 830.61 19.56 -8 -11 1 801.55 20.34 8 11 0 118.34 7.16 -8 -11 0 129.27 8.13 8 11 1 200.56 8.90 -8 -11 -1 190.58 9.49 -8 -11 -2 5.69 2.93 -8 -11 -2 6.44 2.27 8 11 2 6.92 1.72 -8 -11 -3 46.48 5.89 8 11 3 46.78 4.01 -8 -11 -3 44.59 4.68 8 11 4 -0.45 1.35 -8 -11 -4 1.89 1.37 -8 -11 -4 2.82 2.91 -8 -11 -5 73.51 5.47 -8 -11 -5 72.12 7.03 -8 -11 -6 276.27 10.59 -8 -11 -6 285.99 13.97 8 11 7 5.88 2.46 -8 -11 -7 4.99 1.92 -8 -11 -7 2.50 2.07 8 11 8 506.15 15.67 -8 -11 -8 469.28 13.69 -8 -11 -8 477.19 19.02 -8 -11 -9 32.55 5.41 8 11 9 38.16 4.62 -8 -11 -9 36.26 3.98 -8 -11 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1.74 -8 -11 -18 1.42 1.63 -8 -11 -18 0.46 1.05 -8 -11 -18 1.11 1.24 -8 -11 -19 50.14 4.55 -8 -11 -19 56.75 3.26 -8 -11 -19 53.82 3.43 -8 -11 -19 53.09 4.15 -8 -11 -19 58.26 3.70 -8 -11 -20 0.19 0.96 -8 -11 -20 1.13 1.44 -8 -11 -20 -0.01 0.95 -8 -11 -21 2.44 1.08 -8 -11 -21 -0.06 1.34 -8 -11 -21 1.19 1.02 -8 -11 -22 22.51 2.05 -8 -11 -22 19.71 2.43 -8 -11 -22 25.42 2.20 -8 -11 -23 9.74 1.37 -8 -11 -23 8.37 1.28 -8 -11 -23 6.32 1.54 -8 -11 -24 40.31 2.77 -8 -11 -24 39.66 2.29 -8 -11 -24 41.47 2.41 -8 -11 -25 6.49 1.23 -8 -11 -25 6.12 0.87 -8 -11 -25 4.85 0.83 -8 -11 -26 15.42 1.35 8 12 -17 5.03 0.82 -8 -12 17 3.76 1.06 8 12 -16 2.99 0.88 -8 -12 16 1.56 0.93 8 12 -15 12.04 1.50 -8 -12 15 14.14 1.87 8 12 -14 31.03 2.37 -8 -12 14 33.06 2.70 8 12 -13 38.94 2.97 -8 -12 13 40.55 3.10 8 12 -12 -1.06 1.29 -8 -12 12 1.34 1.33 -8 -12 11 408.86 9.78 8 12 -11 417.59 10.19 -8 -12 11 429.53 9.53 -8 -12 10 49.52 3.54 8 12 -10 54.33 4.18 -8 -12 10 54.16 3.56 -8 -12 9 128.77 5.42 -8 -12 9 129.95 5.10 8 12 -9 129.56 6.08 8 12 -8 54.67 4.27 -8 -12 8 51.77 6.40 -8 -12 8 53.58 3.42 -8 -12 8 57.51 3.66 8 12 -8 69.84 7.71 8 12 -7 205.18 7.86 -8 -12 7 208.01 12.51 8 12 -7 191.00 12.11 -8 -12 7 209.17 6.22 -8 -12 7 194.81 6.21 8 12 -6 47.64 4.49 -8 -12 6 34.40 5.16 -8 -12 6 40.09 2.72 -8 -12 6 38.69 2.72 8 12 -6 46.27 5.70 -8 -12 5 34.94 5.41 8 12 -5 40.48 3.74 -8 -12 5 33.66 2.50 -8 -12 5 32.99 2.51 8 12 -5 35.38 4.96 -8 -12 4 157.93 10.35 8 12 -4 182.49 7.21 -8 -12 4 179.04 5.50 -8 -12 4 174.56 5.31 8 12 -4 177.67 10.65 -8 -12 3 86.07 7.34 -8 -12 3 83.52 3.59 -8 -12 3 92.17 3.75 8 12 -3 88.51 7.30 8 12 -2 577.52 17.74 -8 -12 2 570.54 9.29 -8 -12 2 561.86 18.56 8 12 -1 374.47 13.78 -8 -12 1 391.58 15.09 8 12 0 1017.20 21.90 -8 -12 0 950.12 23.03 8 12 1 914.29 20.00 -8 -12 -1 895.23 22.10 8 12 2 366.39 12.12 -8 -12 -2 364.71 15.79 -8 -12 -2 332.23 12.89 8 12 3 45.63 4.12 -8 -12 -3 42.68 5.63 -8 -12 -3 40.87 4.63 -8 -12 -4 77.00 7.61 -8 -12 -4 71.92 5.98 -8 -12 -5 202.67 12.13 -8 -12 -5 193.85 9.61 -8 -12 -6 137.73 10.08 -8 -12 -6 137.48 7.84 -8 -12 -7 235.53 13.60 -8 -12 -7 224.43 9.88 8 12 7 247.79 11.15 8 12 8 3.56 2.08 -8 -12 -8 2.74 1.58 -8 -12 -8 4.09 3.04 -8 -12 -9 341.85 16.88 8 12 9 344.80 14.12 -8 -12 -9 305.73 11.44 -8 -12 -10 506.78 21.09 -8 -12 -10 467.13 14.13 8 12 11 32.89 5.18 -8 -12 -11 25.86 5.18 -8 -12 -11 26.23 2.32 -8 -12 -11 25.08 2.23 -8 -12 -11 25.84 2.75 -8 -12 -11 27.43 3.03 -8 -12 -12 54.03 3.13 -8 -12 -12 51.54 4.05 -8 -12 -12 58.07 7.67 -8 -12 -12 54.68 3.26 -8 -12 -12 53.49 3.29 -8 -12 -12 55.79 3.99 -8 -12 -12 54.03 3.58 -8 -12 -13 3.09 1.48 -8 -12 -13 4.46 1.36 -8 -12 -13 9.41 3.87 -8 -12 -13 5.25 1.29 -8 -12 -13 3.38 1.12 -8 -12 -13 3.67 1.57 -8 -12 -13 4.72 1.58 -8 -12 -14 13.24 4.57 -8 -12 -14 8.15 1.57 -8 -12 -14 8.94 1.74 -8 -12 -14 8.85 1.63 -8 -12 -14 9.30 2.41 8 12 14 6.02 4.59 -8 -12 -14 8.88 2.05 -8 -12 -15 24.65 5.59 -8 -12 -15 18.72 2.27 -8 -12 -15 18.89 2.26 -8 -12 -15 17.98 1.95 -8 -12 -15 18.43 3.18 8 12 15 12.15 5.38 -8 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-15 -0.37 0.75 -8 -13 15 1.15 0.93 -8 -13 14 7.30 1.55 8 13 -14 6.17 1.21 -8 -13 13 14.26 1.86 8 13 -13 14.29 1.79 -8 -13 12 5.18 1.41 8 13 -12 4.27 1.35 -8 -13 11 7.37 1.69 8 13 -11 6.41 1.60 -8 -13 11 6.85 1.53 8 13 -10 140.42 6.28 -8 -13 10 130.30 5.48 -8 -13 10 143.65 5.51 8 13 -9 127.92 6.09 -8 -13 9 121.62 5.27 -8 -13 9 127.48 5.05 8 13 -8 79.93 5.01 -8 -13 8 77.47 4.21 -8 -13 8 76.32 3.91 8 13 -7 2.93 1.78 -8 -13 7 1.41 1.11 -8 -13 7 0.76 1.14 8 13 -6 253.52 13.98 -8 -13 6 256.66 6.85 -8 -13 6 246.26 13.94 -8 -13 6 256.74 6.98 -8 -13 5 4.55 1.19 8 13 -5 2.93 1.56 -8 -13 5 2.98 1.83 -8 -13 5 4.23 1.22 8 13 -5 3.44 1.83 -8 -13 4 0.19 0.90 8 13 -4 3.93 2.39 -8 -13 4 0.85 1.90 -8 -13 4 0.34 0.97 8 13 -4 -0.29 2.01 -8 -13 3 18.87 1.87 8 13 -3 19.84 4.09 -8 -13 3 15.70 3.43 -8 -13 3 20.13 2.05 8 13 -3 18.43 2.66 -8 -13 2 241.36 12.81 -8 -13 2 237.63 6.34 -8 -13 2 240.99 5.96 8 13 -2 246.96 12.10 -8 -13 1 193.05 11.27 -8 -13 1 190.00 5.52 -8 -13 0 445.44 16.85 -8 -13 0 440.64 8.32 8 13 0 428.75 15.08 8 13 1 135.45 8.17 -8 -13 -1 113.05 8.22 -8 -13 -2 1131.04 29.13 -8 -13 -2 1098.37 24.89 -8 -13 -3 105.59 7.64 -8 -13 -3 131.48 10.04 -8 -13 -4 341.28 13.34 -8 -13 -4 353.45 16.69 -8 -13 -5 86.17 6.62 -8 -13 -5 94.90 8.76 -8 -13 -6 116.67 7.66 8 13 6 124.40 8.17 -8 -13 -6 120.41 9.73 8 13 7 17.94 3.39 -8 -13 -7 16.71 2.94 -8 -13 -7 18.01 4.06 -8 -13 -8 58.03 5.30 8 13 8 65.67 6.47 -8 -13 -8 64.33 7.45 -8 -13 -9 105.94 7.06 -8 -13 -9 113.91 10.02 -8 -13 -10 30.30 2.56 -8 -13 -10 37.44 6.14 -8 -13 -10 32.35 4.03 -8 -13 -10 31.02 2.39 -8 -13 -10 29.14 3.13 -8 -13 -10 33.27 2.92 8 13 10 23.85 4.71 -8 -13 -10 30.74 2.50 -8 -13 -11 80.97 8.91 8 13 11 75.61 7.73 -8 -13 -11 78.03 3.86 -8 -13 -11 73.01 4.86 -8 -13 -11 73.64 3.60 -8 -13 -11 74.86 4.38 -8 -13 -11 79.24 3.98 -8 -13 -12 174.01 13.60 -8 -13 -12 168.27 5.80 -8 -13 -12 170.58 7.42 -8 -13 -12 159.01 5.36 -8 -13 -12 174.60 6.74 -8 -13 -12 160.26 5.99 -8 -13 -12 168.01 5.82 -8 -13 -13 20.22 2.27 -8 -13 -13 22.02 5.11 -8 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3.92 10 -11 -12 42.39 2.87 -10 11 11 24.86 3.33 10 -11 -11 26.39 2.37 -10 11 10 8.97 2.23 10 -11 -10 10.89 1.74 -10 11 9 -1.35 1.94 10 -11 -9 2.26 1.03 -10 11 8 10.94 2.39 10 -11 -8 15.81 1.99 -10 11 7 126.80 6.70 10 -11 -7 128.65 5.21 -10 11 6 10.89 2.40 10 -11 -6 8.94 1.67 -10 11 5 6.39 2.14 10 -11 -5 9.76 1.73 10 -11 -4 343.08 8.73 -10 11 4 342.68 10.86 10 -11 -4 343.69 7.38 10 -11 -3 202.98 6.20 -10 11 3 187.94 7.97 10 -11 -3 202.80 5.81 10 -11 -2 128.33 4.88 -10 11 2 130.34 6.68 10 -11 -2 127.71 4.70 10 -11 -1 1.88 1.02 -10 11 1 2.21 1.56 10 -11 -1 2.73 1.08 10 -11 0 0.33 1.04 -10 11 0 -0.19 1.45 10 -11 0 0.03 0.86 10 -11 1 1.49 0.94 10 -11 1 2.50 1.08 -10 11 -1 1.09 1.57 10 -11 2 23.26 2.13 -10 11 -2 26.56 3.30 10 -11 3 76.95 3.79 -10 11 -3 74.01 5.06 10 -11 4 25.84 2.32 -10 11 -4 26.84 3.16 10 -11 5 3.65 1.11 -10 11 -5 4.90 1.88 10 -11 6 32.54 2.45 -10 11 -6 32.66 3.37 10 -11 7 4.76 1.05 -10 11 -7 8.64 2.15 10 -11 8 15.54 1.62 -10 11 -8 12.40 2.11 10 -11 9 58.03 2.81 -10 11 -9 52.11 3.58 -10 11 -10 40.80 2.94 -10 11 -11 70.63 3.54 10 -10 -19 7.30 0.98 -10 10 19 7.38 1.28 -10 10 18 12.10 1.98 10 -10 -18 11.66 1.32 -10 10 17 17.21 2.53 10 -10 -17 16.37 1.59 -10 10 17 20.77 2.11 -10 10 16 39.92 3.65 10 -10 -16 41.69 2.58 -10 10 16 48.17 3.41 -10 10 15 32.13 3.46 10 -10 -15 34.54 2.44 -10 10 15 30.47 2.83 -10 10 14 23.25 3.24 10 -10 -14 21.43 2.11 -10 10 14 24.55 2.71 -10 10 13 19.24 3.07 10 -10 -13 26.66 2.33 -10 10 13 19.11 2.66 -10 10 12 7.88 2.22 10 -10 -12 11.95 1.68 -10 10 12 6.86 2.06 10 -10 -11 16.50 2.04 -10 10 11 14.79 2.60 10 -10 -10 14.60 1.92 -10 10 10 12.36 2.65 10 -10 -9 2.22 1.04 -10 10 9 2.01 1.84 10 -10 -8 5.83 1.51 -10 10 8 6.80 2.30 10 -10 -7 118.09 5.10 -10 10 7 109.12 6.35 10 -10 -6 472.29 10.09 -10 10 6 493.96 13.02 10 -10 -5 34.28 2.86 10 -10 -5 35.00 2.32 -10 10 5 28.55 3.28 10 -10 -4 140.83 5.54 10 -10 -4 141.48 4.83 -10 10 4 132.78 6.89 10 -10 -3 3.49 1.31 -10 10 3 7.27 2.31 10 -10 -3 4.98 1.19 10 -10 -2 682.12 11.43 -10 10 2 659.28 14.86 10 -10 -2 658.87 10.85 10 -10 -1 3.26 1.13 -10 10 1 3.37 1.93 10 -10 -1 3.80 1.31 10 -10 0 72.13 3.58 -10 10 0 70.01 4.94 10 -10 0 68.86 3.70 10 -10 1 11.79 1.68 -10 10 -1 11.92 2.34 10 -10 1 12.53 1.79 -10 10 -2 70.16 4.88 10 -10 2 72.33 3.80 -10 10 -3 29.31 3.28 10 -10 3 33.08 2.63 -10 10 -4 201.99 8.16 10 -10 4 188.04 6.12 -10 10 -5 12.68 2.37 10 -10 5 16.82 2.00 -10 10 -6 16.01 2.58 10 -10 6 18.21 2.15 -10 10 -7 8.63 2.07 10 -10 7 6.22 1.42 -10 10 -8 1.51 1.45 10 -10 8 1.26 1.04 -10 10 -9 46.91 3.77 -10 10 -9 43.22 3.36 10 -10 9 45.48 2.73 -10 10 -10 2.65 1.31 10 -10 10 0.30 0.74 -10 10 -11 89.32 4.48 10 -10 12 57.04 2.22 -10 10 -12 55.86 3.35 -10 10 -13 48.25 2.68 -10 9 20 0.52 0.90 10 -9 -20 -0.03 0.49 -10 9 19 22.32 2.51 10 -9 -19 23.56 1.66 -10 9 19 27.75 2.15 -10 9 18 1.41 1.21 10 -9 -18 1.48 0.83 -10 9 18 1.40 1.08 -10 9 17 5.05 1.81 10 -9 -17 1.88 0.87 -10 9 17 5.23 1.52 -10 9 16 97.54 6.01 10 -9 -16 104.10 4.09 -10 9 16 107.38 5.04 10 -9 -15 7.58 1.42 -10 9 15 9.54 2.55 -10 9 15 12.04 2.33 -10 9 14 15.81 2.30 10 -9 -14 16.26 1.87 -10 9 14 17.94 3.09 -10 9 13 7.80 1.93 10 -9 -13 11.12 1.68 -10 9 13 6.98 2.14 -10 9 12 140.67 6.54 10 -9 -12 148.63 5.38 -10 9 12 133.60 7.37 -10 9 11 17.71 2.59 10 -9 -11 18.48 2.15 -10 9 11 18.96 3.24 -10 9 10 64.03 4.68 10 -9 -10 65.30 3.79 -10 9 10 61.06 5.10 -10 9 9 -0.57 1.55 -10 9 9 3.32 1.84 10 -9 -9 1.65 1.11 -10 9 8 2.57 1.65 10 -9 -8 3.27 1.25 -10 9 7 26.24 3.39 10 -9 -7 24.26 2.59 -10 9 6 365.31 11.30 10 -9 -6 386.48 9.08 10 -9 -5 120.01 5.15 -10 9 5 129.73 6.69 10 -9 -5 125.72 4.49 10 -9 -4 17.52 2.11 10 -9 -4 17.00 1.84 10 -9 -3 142.91 5.63 -10 9 3 135.58 6.83 10 -9 -3 132.21 4.83 10 -9 -2 252.42 7.44 -10 9 2 238.58 8.77 10 -9 -2 241.48 6.62 10 -9 -1 39.40 3.14 -10 9 1 40.52 3.95 10 -9 -1 36.23 2.67 10 -9 0 548.32 10.05 -10 9 0 540.72 13.13 10 -9 0 534.38 10.07 10 -9 1 2.48 1.26 -10 9 -1 0.72 1.47 10 -9 1 1.83 1.08 -10 9 -2 23.94 3.17 10 -9 2 21.54 2.29 -10 9 -3 28.04 3.36 10 -9 3 30.25 2.68 -10 9 -4 93.58 5.66 10 -9 4 92.78 4.42 -10 9 -5 14.69 2.52 10 -9 5 17.92 2.16 -10 9 -6 110.77 6.32 10 -9 6 117.17 4.93 -10 9 -7 3.13 2.00 10 -9 7 7.72 1.57 -10 9 -8 0.55 1.54 10 -9 8 2.57 1.23 -10 9 -9 2.22 1.67 10 -9 9 2.39 1.14 -10 9 -10 2.33 1.65 10 -9 10 3.42 1.04 -10 9 -10 4.33 1.51 10 -9 11 0.27 0.71 -10 9 -11 -0.84 1.50 -10 9 -11 0.06 1.22 -10 9 -12 3.28 1.33 -10 9 -13 21.06 2.23 10 -9 13 25.84 1.68 -10 9 -14 7.61 1.39 10 -9 14 11.02 1.00 10 -8 -21 0.53 0.49 -10 8 20 26.03 2.04 -10 8 20 21.96 2.32 10 -8 -20 26.26 1.68 -10 8 19 9.36 1.46 -10 8 19 10.70 1.98 10 -8 -19 10.20 1.23 -10 8 18 58.65 4.51 10 -8 -18 60.34 2.94 -10 8 17 66.88 5.35 10 -8 -17 79.86 3.58 -10 8 16 7.63 1.88 -10 8 16 9.08 2.68 10 -8 -16 5.24 1.21 -10 8 15 292.87 8.91 10 -8 -15 294.14 7.23 -10 8 14 15.19 2.41 -10 8 14 12.40 2.94 10 -8 -14 19.01 1.99 -10 8 13 23.84 3.09 -10 8 13 18.38 3.44 10 -8 -13 21.45 2.27 -10 8 12 30.86 3.13 -10 8 12 26.25 3.63 10 -8 -12 34.01 2.67 -10 8 11 114.81 5.93 -10 8 11 134.60 8.09 10 -8 -11 123.83 5.00 -10 8 10 21.15 2.86 10 -8 -10 23.33 2.30 -10 8 10 21.27 3.67 10 -8 -9 3.18 1.33 -10 8 9 2.64 1.44 -10 8 9 3.51 2.14 -10 8 8 -0.43 1.60 -10 8 8 2.31 2.05 10 -8 -8 1.21 1.04 10 -8 -8 2.01 1.99 -10 8 7 0.12 1.65 10 -8 -7 0.28 1.12 -10 8 7 0.61 1.80 10 -8 -7 0.77 2.47 10 -8 -6 67.57 3.92 10 -8 -6 64.46 7.58 -10 8 6 70.59 5.04 10 -8 -5 14.87 1.63 10 -8 -5 12.57 1.79 10 -8 -5 9.66 2.86 -10 8 5 12.73 2.40 10 -8 -4 12.59 1.58 10 -8 -4 12.12 1.90 10 -8 -4 17.07 4.58 -10 8 4 14.75 2.60 10 -8 -3 10.29 1.54 10 -8 -3 10.87 1.84 10 -8 -3 7.59 3.26 -10 8 3 10.02 2.12 10 -8 -2 92.70 4.18 10 -8 -2 105.40 4.71 10 -8 -2 112.75 9.55 -10 8 2 101.50 5.75 10 -8 -1 234.81 6.50 10 -8 -1 236.16 7.04 10 -8 -1 218.33 13.45 -10 8 1 230.33 8.54 10 -8 0 4.55 1.34 10 -8 0 3.28 1.23 10 -8 0 6.60 2.51 -10 8 0 7.07 2.12 10 -8 1 73.16 3.78 -10 8 -1 63.84 7.11 -10 8 -1 70.90 4.88 10 -8 1 69.11 7.67 -10 8 -2 26.15 3.34 -10 8 -2 15.97 3.69 10 -8 2 19.98 4.51 10 -8 2 21.73 2.18 -10 8 -3 49.02 4.16 10 -8 3 41.97 3.05 -10 8 -4 8.56 2.26 10 -8 4 6.48 1.47 -10 8 -5 15.91 2.77 10 -8 5 18.10 2.17 -10 8 -6 235.12 9.03 10 -8 6 231.41 7.03 -10 8 -7 4.71 2.03 10 -8 7 3.93 1.39 -10 8 -8 1.65 1.59 10 -8 8 3.87 1.35 -10 8 -9 2.76 1.91 10 -8 9 0.73 1.10 -10 8 -10 0.16 1.45 10 -8 10 1.23 0.97 -10 8 -11 1.42 1.58 -10 8 -11 1.10 1.45 10 -8 11 1.34 1.05 -10 8 -12 2.28 1.51 10 -8 12 0.49 0.73 -10 8 -12 -1.73 1.47 -10 8 -13 0.29 1.18 10 -8 14 15.43 1.40 -10 8 -14 13.92 1.91 10 -8 15 3.36 0.70 -10 8 -15 1.03 0.93 -10 7 21 26.77 1.91 -10 7 21 22.30 2.07 10 -7 -21 25.08 1.46 -10 7 20 0.50 1.21 10 -7 -20 -0.47 0.61 -10 7 20 1.79 1.07 10 -7 -19 2.14 0.76 -10 7 19 1.90 1.03 -10 7 19 2.66 1.18 -10 7 18 98.11 4.62 10 -7 -18 95.52 3.71 -10 7 17 93.84 4.74 10 -7 -17 89.36 3.84 -10 7 16 32.06 3.19 10 -7 -16 31.34 2.44 -10 7 15 176.48 7.00 10 -7 -15 173.30 5.70 -10 7 14 128.36 6.09 10 -7 -14 105.68 4.53 -10 7 13 173.91 7.11 10 -7 -13 176.54 5.85 -10 7 12 61.40 4.40 10 -7 -12 59.22 3.58 -10 7 11 1.53 1.49 10 -7 -11 0.43 1.15 10 -7 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7.01 10 -5 8 64.81 3.75 -10 5 -8 70.65 5.04 10 -5 9 53.17 3.45 -10 5 -9 52.56 4.49 10 -5 10 41.12 3.08 -10 5 -10 34.88 3.64 10 -5 11 94.57 4.38 -10 5 -11 84.87 5.61 -10 5 -12 63.50 4.76 10 -5 12 72.26 3.88 -10 5 -12 63.00 4.75 -10 5 -13 -2.81 1.71 10 -5 13 0.06 0.87 -10 5 -13 -0.97 1.46 -10 5 -14 26.44 3.10 -10 5 -14 24.52 2.82 10 -5 14 29.32 2.25 -10 5 -15 54.65 4.12 -10 5 -15 50.07 3.69 -10 5 -16 2.69 1.53 -10 5 -16 5.32 1.61 10 -5 17 202.90 4.87 10 -5 18 5.76 0.91 10 -4 -22 3.47 0.74 10 -4 -22 4.31 0.72 -10 4 22 1.63 0.78 10 -4 -22 4.01 0.80 10 -4 -21 0.83 0.57 -10 4 21 -0.22 0.91 10 -4 -20 4.16 0.96 -10 4 20 5.58 1.41 10 -4 -19 13.68 1.63 -10 4 19 14.70 2.09 10 -4 -18 2.13 0.87 -10 4 18 1.06 1.22 10 -4 -17 29.60 2.46 -10 4 17 30.43 2.94 10 -4 -16 18.06 2.20 -10 4 16 23.72 2.92 10 -4 -15 225.19 6.63 -10 4 15 228.42 7.68 -10 4 14 8.22 1.91 10 -4 -14 4.79 1.50 -10 4 13 2.87 1.76 10 -4 -13 1.88 1.15 -10 4 12 19.58 2.63 -10 4 12 10.17 4.98 10 -4 -12 15.01 4.19 10 -4 -12 16.02 2.10 10 -4 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5 9 595.37 20.49 -10 -5 -10 47.51 4.63 10 5 10 40.54 5.82 -10 -5 -11 93.10 6.59 10 5 11 101.44 9.62 -10 -5 -12 112.95 5.59 -10 -5 -12 122.53 5.96 -10 -5 -12 117.16 7.47 10 5 12 120.88 10.74 -10 -5 -13 11.61 2.29 -10 -5 -13 9.63 2.29 -10 -5 -13 7.47 2.18 10 5 13 9.65 3.75 10 5 14 -2.77 3.92 -10 -5 -14 0.90 1.51 -10 -5 -14 -1.03 1.75 10 5 15 -2.34 3.05 -10 -5 -15 1.62 1.68 -10 -5 -15 2.47 1.70 10 5 16 -0.53 3.10 -10 -5 -16 1.90 1.85 -10 -5 -16 2.68 1.96 -10 -5 -17 182.30 7.83 -10 -5 -17 192.51 8.38 10 5 17 204.35 5.52 -10 -5 -18 13.50 2.46 -10 -5 -18 14.41 2.71 10 5 18 12.53 1.59 -10 -5 -19 32.25 3.57 10 5 19 33.53 2.19 -10 -5 -20 21.73 2.88 10 5 20 22.70 1.80 -10 -5 -21 0.91 1.22 -10 -5 -22 64.17 3.95 -10 -5 -23 10.13 1.72 -10 -5 -24 58.78 2.82 10 6 -20 24.74 1.59 -10 -6 20 22.99 1.65 10 6 -19 0.35 0.69 -10 -6 19 -0.26 0.86 -10 -6 19 1.48 0.83 -10 -6 18 20.50 1.95 10 6 -18 21.04 1.93 -10 -6 17 3.63 1.65 -10 -6 17 1.96 1.08 10 6 -17 1.88 1.06 -10 -6 16 35.96 3.43 -10 -6 16 36.61 2.76 10 6 -16 37.84 2.72 -10 -6 15 12.13 2.29 -10 -6 15 10.85 1.83 10 6 -15 11.35 1.76 -10 -6 14 192.84 7.44 10 6 -14 192.55 6.27 -10 -6 14 202.19 6.38 10 6 -13 29.71 2.68 -10 -6 13 28.20 2.72 -10 -6 13 29.02 2.92 -10 -6 12 68.33 4.46 10 6 -12 61.22 6.57 10 6 -12 65.11 3.87 10 6 -12 54.31 6.86 -10 -6 12 66.76 3.77 -10 -6 11 256.73 8.15 10 6 -11 263.23 13.04 10 6 -11 246.33 7.15 -10 -6 11 253.88 6.88 -10 -6 10 99.33 4.39 10 6 -10 108.81 8.33 -10 -6 10 110.49 5.24 -10 -6 10 101.74 4.34 10 6 -10 95.45 9.17 10 6 -10 91.70 4.45 10 6 -9 1.42 1.72 10 6 -9 2.20 1.24 -10 -6 9 1.44 1.08 -10 -6 9 -0.98 1.07 -10 -6 9 2.77 1.38 10 6 -9 0.71 2.49 10 6 -8 161.59 10.23 10 6 -8 155.59 5.51 -10 -6 8 171.16 5.28 -10 -6 8 167.09 5.93 10 6 -8 184.00 10.22 10 6 -7 373.83 13.65 10 6 -7 352.24 14.28 -10 -6 6 87.76 6.35 10 6 -6 77.86 6.57 10 6 -6 81.37 6.29 -10 -6 5 4.20 1.58 10 6 -5 3.03 1.46 10 6 -5 3.87 1.72 -10 -6 4 4.45 1.79 10 6 -4 3.97 1.95 10 6 -4 5.53 1.69 10 6 -3 47.60 4.52 -10 -6 3 51.65 4.86 10 6 -3 54.58 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81.18 7.59 10 7 -11 89.95 4.62 -10 -7 11 89.08 4.85 -10 -7 11 87.77 4.10 10 7 -10 288.17 13.89 -10 -7 10 285.59 7.56 10 7 -10 294.78 7.98 -10 -7 10 274.93 6.82 -10 -7 10 283.18 8.24 10 7 -9 3.19 2.11 -10 -7 9 3.87 1.38 -10 -7 9 3.96 1.27 10 7 -9 3.56 1.38 -10 -7 9 4.53 1.42 10 7 -9 -0.71 1.72 10 7 -8 9.24 2.67 -10 -7 8 11.04 1.92 10 7 -8 12.71 1.99 -10 -7 8 11.24 1.58 -10 -7 8 9.78 1.48 10 7 -8 8.67 2.45 10 7 -7 25.86 4.04 -10 -7 7 32.17 4.24 -10 -7 7 32.61 2.40 10 7 -6 125.44 7.99 10 7 -6 114.47 8.15 -10 -7 5 2.28 1.41 10 7 -5 3.42 2.09 10 7 -5 2.13 1.57 10 7 -4 105.63 6.87 -10 -7 4 113.05 7.22 10 7 -4 117.28 7.27 10 7 -3 93.76 6.37 10 7 -3 90.64 6.20 -10 -7 3 86.98 6.36 -10 -7 2 16.35 2.94 10 7 -2 20.00 2.89 10 7 -2 22.13 3.04 10 7 -1 74.58 5.30 10 7 -1 74.10 5.15 -10 -7 1 73.38 5.58 -10 -7 1 74.75 6.72 10 7 0 2.85 1.63 -10 -7 0 3.54 1.93 -10 -7 0 1.06 1.88 10 7 0 3.76 1.57 10 7 1 23.66 3.14 -10 -7 -1 21.13 3.09 -10 -7 -1 13.36 2.68 10 7 1 19.97 2.89 10 7 2 16.23 2.51 -10 -7 -2 17.56 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4.95 10 11 -8 33.11 3.56 -10 -11 8 24.69 2.40 -10 -11 8 27.68 2.68 -10 -11 7 130.44 5.50 10 11 -7 131.80 9.85 -10 -11 7 131.08 5.30 -10 -11 7 115.84 8.89 -10 -11 7 129.31 4.94 10 11 -6 4.22 2.33 10 11 -6 1.82 1.42 -10 -11 6 2.26 1.19 -10 -11 6 4.18 2.15 -10 -11 6 2.55 1.30 -10 -11 6 2.06 1.07 10 11 -5 24.64 4.43 10 11 -5 25.85 2.70 -10 -11 5 21.07 2.42 -10 -11 5 20.30 2.15 -10 -11 5 22.97 2.19 -10 -11 5 22.05 3.94 -10 -11 4 83.72 7.46 -10 -11 4 74.20 4.02 10 11 -4 72.68 6.69 -10 -11 4 84.12 3.71 -10 -11 4 73.96 3.56 -10 -11 3 42.94 5.42 -10 -11 3 49.70 2.91 10 11 -3 40.67 4.80 -10 -11 2 66.54 6.65 10 11 -2 66.07 5.91 10 11 -1 20.70 3.30 -10 -11 1 15.93 3.16 -10 -11 0 602.40 18.08 10 11 0 646.60 17.27 -10 -11 -1 297.23 12.87 10 11 1 298.42 11.08 -10 -11 -2 73.21 6.26 10 11 2 71.70 5.46 10 11 3 12.89 2.32 -10 -11 -3 9.42 2.45 -10 -11 -4 232.06 10.83 -10 -11 -4 241.12 14.48 10 11 4 263.28 9.63 -10 -11 -5 500.01 15.45 10 11 5 539.23 13.21 -10 -11 -5 519.59 21.12 -10 -11 -6 86.08 6.55 10 11 6 70.09 5.31 -10 -11 -6 88.15 8.87 -10 -11 -7 246.07 10.85 -10 -11 -7 274.64 15.77 -10 -11 -8 1467.07 37.10 -10 -11 -8 1463.43 26.41 10 11 9 44.90 5.98 -10 -11 -9 58.10 5.36 -10 -11 -10 310.22 10.13 -10 -11 -10 332.55 18.35 -10 -11 -10 314.35 12.81 -10 -11 -10 294.30 7.14 -10 -11 -10 305.94 8.44 -10 -11 -10 292.71 7.06 -10 -11 -11 5.04 1.64 -10 -11 -11 5.68 1.06 -10 -11 -11 5.01 3.07 -10 -11 -11 6.58 1.27 -10 -11 -11 4.68 2.16 -10 -11 -11 8.31 2.07 -10 -11 -12 129.61 7.08 -10 -11 -12 121.85 5.67 -10 -11 -12 124.01 5.23 -10 -11 -12 122.62 5.25 -10 -11 -12 132.00 12.05 -10 -11 -12 121.77 5.61 -10 -11 -12 116.60 6.64 -10 -11 -13 144.30 6.41 -10 -11 -13 135.66 5.24 -10 -11 -13 136.21 6.78 -10 -11 -13 140.30 6.32 -10 -11 -13 139.59 5.33 -10 -11 -14 12.39 2.43 -10 -11 -14 16.20 4.48 -10 -11 -14 14.24 1.88 10 11 14 11.93 4.33 -10 -11 -14 13.87 2.69 -10 -11 -14 14.99 2.39 -10 -11 -14 13.84 1.81 -10 -11 -15 60.29 4.88 -10 -11 -15 73.47 9.70 -10 -11 -15 68.29 3.86 -10 -11 -15 63.16 3.67 10 11 15 54.12 9.15 -10 -11 -15 60.08 4.40 -10 -11 -16 8.57 2.18 -10 -11 -16 2.71 3.84 -10 -11 -16 9.13 1.69 -10 -11 -16 7.07 1.46 10 11 16 7.48 4.06 -10 -11 -16 9.56 2.18 -10 -11 -17 74.07 4.05 -10 -11 -17 71.12 4.85 -10 -11 -17 63.69 5.06 -10 -11 -17 71.42 4.05 -10 -11 -18 1.37 1.18 -10 -11 -18 2.46 1.96 -10 -11 -18 1.37 1.08 -10 -11 -18 3.38 1.87 -10 -11 -19 42.39 3.15 -10 -11 -19 36.95 3.53 -10 -11 -19 43.04 3.15 -10 -11 -19 45.84 4.29 -10 -11 -20 0.94 0.97 -10 -11 -20 -0.72 1.43 -10 -11 -20 -0.07 1.49 -10 -11 -20 0.51 0.94 -10 -11 -21 2.63 1.47 -10 -11 -21 2.64 1.02 -10 -11 -21 2.55 1.12 -10 -11 -22 34.02 2.46 -10 -11 -22 32.94 2.99 -10 -11 -22 32.20 2.35 -10 -11 -23 30.10 2.03 -10 -11 -23 31.35 2.76 -10 -11 -23 31.87 2.09 -10 -11 -24 13.31 1.24 -10 -11 -24 11.73 1.58 -10 -11 -24 13.19 1.23 -10 -11 -25 0.66 0.78 10 12 -16 15.92 1.40 -10 -12 16 15.37 1.81 10 12 -15 0.08 0.67 -10 -12 15 0.64 1.02 10 12 -14 71.68 3.28 -10 -12 14 71.41 3.92 10 12 -13 76.25 3.69 -10 -12 13 77.74 4.23 -10 -12 12 23.83 2.60 10 12 -12 22.85 2.26 -10 -12 11 14.21 1.92 -10 -12 11 15.12 2.25 10 12 -11 17.96 2.27 -10 -12 10 422.73 9.46 -10 -12 10 431.35 9.86 10 12 -10 434.23 9.90 10 12 -9 3.35 1.49 -10 -12 9 0.24 1.10 -10 -12 9 0.37 1.19 -10 -12 9 0.66 1.11 10 12 -8 173.66 6.53 -10 -12 8 189.66 6.56 -10 -12 8 175.89 5.86 10 12 -7 0.09 1.30 -10 -12 7 -0.92 2.18 10 12 -7 0.61 2.09 -10 -12 7 5.73 1.65 -10 -12 7 -0.47 1.18 -10 -12 7 1.62 1.17 -10 -12 6 620.54 11.57 10 12 -6 601.80 20.85 -10 -12 6 598.73 10.94 -10 -12 6 590.10 21.47 -10 -12 6 597.16 10.52 10 12 -5 3.12 2.51 10 12 -5 3.13 1.73 -10 -12 5 1.51 1.05 -10 -12 5 1.42 1.15 -10 -12 5 0.75 1.14 -10 -12 5 5.01 2.98 -10 -12 4 63.65 6.97 -10 -12 4 61.78 3.69 10 12 -4 70.46 6.66 -10 -12 4 64.24 3.37 -10 -12 4 65.39 3.47 -10 -12 3 13.20 1.76 -10 -12 3 14.61 2.01 -10 -12 3 12.81 1.63 -10 -12 3 14.64 3.85 10 12 -3 11.36 3.07 -10 -12 2 135.04 5.21 -10 -12 2 139.60 9.89 10 12 -2 139.92 9.03 -10 -12 2 140.60 4.81 10 12 -1 3.29 1.44 -10 -12 1 2.62 1.88 -10 -12 1 3.89 1.12 -10 -12 0 303.40 13.50 10 12 0 297.20 12.23 -10 -12 -1 51.98 5.59 10 12 1 50.93 5.05 -10 -12 -2 126.61 8.71 10 12 2 124.28 7.56 10 12 3 9.19 2.02 -10 -12 -3 4.80 2.03 -10 -12 -4 76.57 6.27 -10 -12 -4 74.14 8.18 10 12 4 76.45 5.52 -10 -12 -5 27.72 4.01 -10 -12 -5 23.58 4.84 -10 -12 -6 20.26 3.46 -10 -12 -6 22.27 4.70 -10 -12 -7 244.17 11.18 -10 -12 -7 258.26 15.40 -10 -12 -8 50.54 5.12 -10 -12 -8 50.81 7.18 -10 -12 -9 661.15 10.52 -10 -12 -9 651.52 18.09 -10 -12 -9 672.89 14.92 -10 -12 -9 661.06 12.28 -10 -12 -9 660.03 10.72 -10 -12 -9 697.66 26.81 -10 -12 -10 208.78 6.24 -10 -12 -10 220.27 8.91 -10 -12 -10 240.67 15.99 -10 -12 -10 214.24 10.47 -10 -12 -10 224.45 7.99 -10 -12 -10 225.71 7.46 -10 -12 -10 209.99 6.14 -10 -12 -11 30.38 2.59 -10 -12 -11 32.14 3.67 -10 -12 -11 33.39 4.32 -10 -12 -11 29.63 2.46 -10 -12 -11 29.01 3.13 -10 -12 -11 30.53 2.30 -10 -12 -11 39.15 7.11 10 12 11 35.45 6.01 -10 -12 -12 48.34 3.55 10 12 12 56.59 8.09 -10 -12 -12 47.55 3.08 -10 -12 -12 51.91 4.25 -10 -12 -12 49.63 2.82 -10 -12 -12 61.45 8.55 -10 -12 -12 48.57 3.70 -10 -12 -12 53.83 3.33 -10 -12 -13 159.38 6.60 -10 -12 -13 158.39 5.65 -10 -12 -13 166.99 14.13 -10 -12 -13 160.56 5.78 -10 -12 -13 154.23 6.70 -10 -12 -13 174.36 7.67 -10 -12 -13 163.75 5.11 -10 -12 -14 3.12 1.76 -10 -12 -14 2.58 2.05 -10 -12 -14 3.37 2.68 -10 -12 -14 2.42 1.12 -10 -12 -14 3.30 1.22 -10 -12 -14 3.46 1.47 -10 -12 -15 -0.20 3.37 -10 -12 -15 0.57 1.02 -10 -12 -15 -0.52 1.07 -10 -12 -15 -0.49 1.73 10 12 15 -1.05 3.42 -10 -12 -15 2.79 2.08 10 12 16 42.81 8.41 -10 -12 -16 43.06 4.15 -10 -12 -16 51.26 8.60 -10 -12 -16 43.22 3.14 -10 -12 -16 42.18 3.08 -10 -12 -16 40.86 3.70 -10 -12 -17 16.10 2.14 -10 -12 -17 16.94 2.16 -10 -12 -17 13.93 2.82 -10 -12 -17 15.87 2.67 -10 -12 -18 0.61 1.07 -10 -12 -18 0.68 1.18 -10 -12 -18 -0.77 1.80 -10 -12 -18 0.17 1.49 -10 -12 -19 1.50 0.97 -10 -12 -19 1.38 1.08 -10 -12 -19 0.36 1.58 -10 -12 -19 -0.17 1.40 -10 -12 -20 5.26 1.35 -10 -12 -20 6.36 2.20 -10 -12 -20 6.62 1.45 -10 -12 -20 7.37 1.93 -10 -12 -21 56.96 3.29 -10 -12 -21 56.91 3.25 -10 -12 -21 54.44 3.87 -10 -12 -22 119.71 4.44 -10 -12 -22 112.82 5.11 -10 -12 -22 115.75 4.27 -10 -12 -23 9.87 1.72 -10 -12 -23 7.85 1.25 -10 -12 -23 8.29 1.23 -10 -12 -24 25.72 1.74 -10 -12 -24 26.13 1.73 -10 -12 -24 26.96 2.17 -10 -12 -25 -0.49 0.70 -10 -13 16 20.48 1.78 10 13 -16 19.69 1.29 -10 -13 15 8.49 1.36 10 13 -15 7.99 1.03 -10 -13 14 45.41 2.92 10 13 -14 44.53 2.42 10 13 -13 1.02 0.81 -10 -13 13 1.66 1.15 -10 -13 12 55.93 3.53 10 13 -12 55.92 3.21 -10 -13 11 15.76 2.19 10 13 -11 17.73 2.02 -10 -13 10 103.54 4.75 -10 -13 10 103.75 4.79 10 13 -10 96.93 4.68 -10 -13 9 5.23 1.48 10 13 -9 6.88 1.70 -10 -13 9 3.57 1.39 10 13 -8 228.45 7.53 -10 -13 8 236.73 7.23 -10 -13 8 220.80 6.67 -10 -13 7 80.16 4.05 -10 -13 7 89.19 4.51 10 13 -6 2.12 2.68 -10 -13 6 -2.83 2.64 -10 -13 6 1.08 1.16 -10 -13 6 1.23 1.23 10 13 -5 4.14 2.19 10 13 -5 2.20 1.83 -10 -13 5 4.14 2.61 -10 -13 5 2.36 1.42 -10 -13 5 2.41 1.40 -10 -13 4 34.21 2.64 -10 -13 4 33.53 2.78 -10 -13 4 30.53 5.06 10 13 -4 29.89 4.78 -10 -13 4 32.80 2.50 -10 -13 3 38.02 2.75 -10 -13 3 39.62 3.08 -10 -13 3 36.92 5.48 -10 -13 3 37.90 2.70 10 13 -3 35.53 5.01 -10 -13 2 152.73 10.60 -10 -13 2 156.45 5.33 -10 -13 2 169.02 5.94 -10 -13 2 170.02 5.22 10 13 -2 171.70 10.38 10 13 -1 260.30 12.39 -10 -13 1 274.02 14.11 -10 -13 1 273.57 7.48 -10 -13 1 273.22 6.73 -10 -13 0 1.02 0.88 10 13 0 -0.64 1.42 -10 -13 0 0.23 1.11 -10 -13 0 -0.90 1.83 -10 -13 -1 67.14 3.16 10 13 1 70.25 6.10 -10 -13 -1 66.53 3.33 -10 -13 -1 63.01 3.18 -10 -13 -1 63.62 6.56 -10 -13 -2 6.81 1.22 10 13 2 5.67 1.64 -10 -13 -2 3.21 2.02 -10 -13 -2 5.57 1.26 -10 -13 -2 5.65 1.14 -10 -13 -3 28.82 4.47 -10 -13 -4 30.78 4.23 -10 -13 -4 31.22 5.53 -10 -13 -5 71.25 6.34 -10 -13 -5 69.97 8.28 -10 -13 -6 109.23 7.72 -10 -13 -6 110.52 10.32 -10 -13 -7 157.31 5.14 -10 -13 -7 159.87 7.28 -10 -13 -7 148.23 9.03 -10 -13 -7 155.05 5.09 -10 -13 -7 175.88 13.23 -10 -13 -8 2.62 2.25 -10 -13 -8 4.44 3.40 -10 -13 -8 2.51 1.07 -10 -13 -8 -1.25 1.29 -10 -13 -8 1.56 1.07 -10 -13 -8 0.28 1.08 -10 -13 -9 38.94 2.75 -10 -13 -9 38.16 3.85 -10 -13 -9 38.00 2.64 -10 -13 -9 40.78 7.02 -10 -13 -9 41.70 3.13 -10 -13 -9 39.50 4.60 -10 -13 -9 36.45 2.44 -10 -13 -9 36.29 3.42 -10 -13 -10 16.62 1.87 -10 -13 -10 15.94 4.48 -10 -13 -10 18.07 3.34 -10 -13 -10 17.67 1.94 -10 -13 -10 17.01 2.24 -10 -13 -10 18.70 2.68 -10 -13 -10 16.75 1.71 -10 -13 -11 158.72 9.47 -10 -13 -11 137.78 5.22 -10 -13 -11 144.50 6.70 -10 -13 -11 134.48 4.69 -10 -13 -11 149.65 13.19 -10 -13 -11 135.19 6.06 -10 -13 -11 133.85 5.23 -10 -13 -12 69.54 3.76 10 13 12 66.66 8.87 -10 -13 -12 69.22 4.87 -10 -13 -12 65.94 3.35 -10 -13 -12 74.09 9.43 -10 -13 -12 69.29 4.44 -10 -13 -12 67.64 3.75 -10 -13 -13 31.26 3.04 -10 -13 -13 27.87 2.61 10 13 13 37.80 7.40 -10 -13 -13 30.20 3.52 -10 -13 -13 31.00 2.36 -10 -13 -13 23.87 6.16 -10 -13 -13 30.78 3.15 -10 -13 -13 33.23 2.82 10 13 14 147.39 14.13 -10 -13 -14 186.08 15.46 -10 -13 -14 157.46 5.89 -10 -13 -14 168.82 7.69 -10 -13 -14 169.13 5.31 -10 -13 -14 161.93 6.68 -10 -13 -14 161.40 5.95 -10 -13 -15 5.53 4.65 -10 -13 -15 3.07 1.16 -10 -13 -15 1.52 1.07 -10 -13 -15 1.07 1.57 -10 -13 -15 2.82 1.30 -10 -13 -15 3.71 1.94 10 13 15 1.09 3.03 -10 -13 -16 114.69 6.54 -10 -13 -16 114.97 4.43 -10 -13 -16 118.24 5.12 -10 -13 -16 110.78 5.76 -10 -13 -16 115.81 5.11 -10 -13 -17 88.87 5.84 -10 -13 -17 87.67 3.85 -10 -13 -17 99.88 4.71 -10 -13 -17 92.95 5.37 -10 -13 -17 98.70 4.77 -10 -13 -18 34.23 3.91 -10 -13 -18 33.96 2.83 -10 -13 -18 33.85 3.32 -10 -13 -18 31.94 2.78 -10 -13 -19 61.86 4.90 -10 -13 -19 59.70 4.30 -10 -13 -19 63.63 3.83 -10 -13 -19 64.85 3.79 -10 -13 -20 9.14 1.65 -10 -13 -20 7.43 1.85 -10 -13 -20 8.68 1.55 -10 -13 -21 9.39 1.52 -10 -13 -21 9.17 1.89 -10 -13 -21 8.85 1.45 -10 -13 -22 44.07 2.75 -10 -13 -22 45.21 2.73 -10 -13 -22 41.60 3.13 -10 -13 -23 25.58 1.93 -10 -13 -23 26.64 1.96 -10 -13 -23 23.46 2.26 -10 -13 -24 56.55 2.49 -10 -13 -24 57.25 2.47 -10 -13 -24 62.42 3.17 -10 -13 -25 20.99 1.35 -10 -13 -25 20.29 1.26 -10 -13 -25 18.67 1.55 10 14 -15 11.85 1.04 -10 -14 15 9.64 1.26 -10 -14 14 9.34 1.38 10 14 -14 9.57 1.14 10 14 -13 33.73 2.13 -10 -14 13 34.90 2.61 -10 -14 12 21.86 2.15 10 14 -12 20.49 1.96 -10 -14 11 43.93 3.12 10 14 -11 42.82 2.80 10 14 -10 2.62 1.14 -10 -14 10 3.35 1.33 -10 -14 10 4.49 1.40 10 14 -9 15.85 2.22 -10 -14 9 16.14 2.04 -10 -14 9 16.25 2.11 -10 -14 8 269.29 7.32 -10 -14 8 297.00 8.11 10 14 -8 281.19 8.14 10 14 -7 0.98 1.38 -10 -14 7 3.80 1.42 -10 -14 7 2.26 1.24 -10 -14 6 385.50 8.92 -10 -14 6 367.41 8.32 10 14 -5 58.63 4.08 -10 -14 5 55.03 3.39 -10 -14 5 48.36 3.29 10 14 -4 31.47 4.68 -10 -14 4 38.35 5.74 -10 -14 4 38.51 2.77 -10 -14 4 41.65 2.93 10 14 -3 1.20 1.76 -10 -14 3 -0.22 1.81 -10 -14 3 -0.69 1.10 -10 -14 3 -0.24 1.10 -10 -14 2 248.23 6.37 -10 -14 2 226.23 13.40 -10 -14 2 263.98 6.92 10 14 -2 239.43 12.76 10 14 -1 29.21 4.45 -10 -14 1 22.08 4.53 -10 -14 1 29.09 2.46 -10 -14 1 29.49 2.20 -10 -14 0 163.96 5.37 -10 -14 0 171.98 11.46 10 14 0 166.76 10.05 -10 -14 -1 3.55 2.44 -10 -14 -1 1.79 1.28 -10 -14 -1 0.17 0.87 10 14 1 -0.93 1.86 -10 -14 -2 7.80 2.87 -10 -14 -2 7.63 1.38 -10 -14 -2 8.94 1.82 -10 -14 -2 7.02 1.21 -10 -14 -2 8.40 1.49 -10 -14 -3 43.80 5.71 -10 -14 -3 44.93 3.08 -10 -14 -3 39.88 2.58 -10 -14 -3 43.98 2.85 -10 -14 -3 39.04 2.56 -10 -14 -4 18.79 3.05 -10 -14 -4 19.66 3.92 -10 -14 -4 19.81 5.05 -10 -14 -4 16.81 2.10 -10 -14 -4 17.82 1.83 -10 -14 -4 18.08 2.07 -10 -14 -4 19.03 1.91 -10 -14 -5 66.91 4.89 -10 -14 -5 69.68 6.61 -10 -14 -5 84.38 9.26 -10 -14 -5 69.62 3.94 -10 -14 -5 66.75 3.26 -10 -14 -5 69.12 3.42 -10 -14 -5 68.49 3.40 -10 -14 -6 17.69 2.40 -10 -14 -6 20.99 1.90 -10 -14 -6 19.20 1.83 -10 -14 -6 22.77 5.25 -10 -14 -6 18.24 2.87 -10 -14 -6 20.41 1.99 10 14 6 14.76 3.31 -10 -14 -6 19.42 3.53 -10 -14 -7 6.62 2.94 -10 -14 -7 2.18 0.95 -10 -14 -7 3.29 1.18 -10 -14 -7 2.08 1.97 -10 -14 -7 2.38 0.98 10 14 7 1.45 1.54 -10 -14 -7 3.08 1.09 -10 -14 -8 374.13 8.29 -10 -14 -8 378.78 14.70 -10 -14 -8 368.71 8.07 -10 -14 -8 425.76 8.70 10 14 8 444.79 16.75 -10 -14 -8 371.10 9.35 -10 -14 -8 398.33 20.77 -10 -14 -9 9.43 3.76 -10 -14 -9 10.74 1.61 -10 -14 -9 9.49 1.76 -10 -14 -9 10.79 1.64 -10 -14 -9 11.84 2.31 -10 -14 -9 12.35 1.61 -10 -14 -9 9.99 2.80 -10 -14 -10 139.08 9.02 -10 -14 -10 148.54 13.14 -10 -14 -10 138.81 5.30 -10 -14 -10 138.98 6.53 -10 -14 -10 142.20 4.89 -10 -14 -10 136.24 5.98 -10 -14 -10 131.35 5.02 -10 -14 -11 191.76 15.12 -10 -14 -11 180.35 6.08 -10 -14 -11 171.47 7.40 -10 -14 -11 165.33 5.37 -10 -14 -11 172.57 6.93 -10 -14 -11 176.36 5.87 -10 -14 -12 25.86 6.43 -10 -14 -12 20.80 2.29 -10 -14 -12 22.40 3.09 -10 -14 -12 21.10 2.09 -10 -14 -12 26.25 3.02 -10 -14 -12 24.68 2.35 -10 -14 -13 1.24 0.95 -10 -14 -13 3.02 1.98 -10 -14 -13 1.00 1.42 -10 -14 -13 1.22 0.95 -10 -14 -13 1.70 0.98 -10 -14 -13 -0.21 3.06 -10 -14 -14 53.34 3.07 -10 -14 -14 52.59 4.68 -10 -14 -14 52.47 3.66 -10 -14 -14 51.59 3.39 -10 -14 -14 51.57 3.73 -10 -14 -14 55.20 8.93 -10 -14 -15 72.66 4.15 -10 -14 -15 82.80 4.31 -10 -14 -15 77.01 4.55 -10 -14 -15 78.69 5.50 -10 -14 -15 75.78 3.71 -10 -14 -16 34.44 2.91 -10 -14 -16 27.65 2.60 -10 -14 -16 32.24 3.11 -10 -14 -16 31.86 2.47 -10 -14 -16 32.37 3.63 -10 -14 -17 137.68 5.60 -10 -14 -17 144.48 5.61 -10 -14 -17 128.69 6.98 -10 -14 -17 136.67 4.81 -10 -14 -17 129.79 5.87 -10 -14 -18 6.96 1.63 -10 -14 -18 3.91 1.50 -10 -14 -18 4.24 1.24 -10 -14 -18 4.54 2.10 -10 -14 -18 4.07 1.27 -10 -14 -19 95.90 4.56 -10 -14 -19 94.25 4.43 -10 -14 -19 96.57 5.04 -10 -14 -19 95.68 3.82 -10 -14 -20 82.64 4.18 -10 -14 -20 79.54 4.04 -10 -14 -20 74.67 4.39 -10 -14 -21 9.48 1.60 -10 -14 -21 12.67 1.92 -10 -14 -21 8.38 1.36 -10 -14 -22 12.89 1.58 -10 -14 -22 11.84 1.74 -10 -14 -22 13.24 1.54 -10 -14 -23 68.76 3.09 -10 -14 -23 67.50 3.01 -10 -14 -23 71.00 3.56 -10 -14 -24 12.50 1.27 -10 -14 -24 13.40 1.27 -10 -14 -24 10.87 1.43 -10 -14 -25 121.09 3.04 -10 -14 -25 126.61 3.66 -10 -14 -25 121.71 3.02 -10 -15 14 1.74 0.83 10 15 -13 43.26 2.10 -10 -15 13 45.30 2.71 -10 -15 12 3.30 1.14 10 15 -12 2.02 0.78 10 15 -11 -0.14 0.91 -10 -15 11 -0.34 0.96 -10 -15 10 25.74 2.46 10 15 -10 25.96 2.34 -10 -15 10 24.93 2.31 10 15 -9 2.77 1.23 -10 -15 9 -0.08 1.06 -10 -15 9 1.06 1.09 -10 -15 8 40.32 2.92 10 15 -8 35.40 2.94 -10 -15 8 43.28 3.12 -10 -15 7 323.05 7.83 -10 -15 7 327.75 8.33 -10 -15 6 98.50 4.43 -10 -15 6 99.47 4.68 -10 -15 5 253.98 6.90 -10 -15 5 263.52 7.23 -10 -15 4 26.95 2.45 -10 -15 4 26.89 2.50 -10 -15 3 59.59 3.40 -10 -15 3 59.83 3.55 10 15 -3 54.41 6.38 -10 -15 2 2.04 2.38 10 15 -2 1.04 2.25 -10 -15 2 3.04 1.33 -10 -15 2 1.32 0.96 -10 -15 1 4.20 2.65 10 15 -1 8.24 2.69 -10 -15 1 6.24 1.31 -10 -15 1 5.31 1.45 -10 -15 0 4.29 1.37 -10 -15 0 4.38 3.26 -10 -15 -1 9.52 1.57 -10 -15 -1 9.44 2.95 -10 -15 -2 149.13 4.98 -10 -15 -2 156.16 5.31 -10 -15 -2 148.73 5.07 -10 -15 -2 158.91 11.03 -10 -15 -3 27.62 2.31 -10 -15 -3 27.54 2.21 -10 -15 -3 26.08 2.15 -10 -15 -3 27.92 4.81 -10 -15 -4 58.78 6.59 -10 -15 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3.75 1.34 11 -7 -4 4.40 2.69 -11 7 3 6.51 2.14 11 -7 -3 6.37 1.27 11 -7 -3 6.48 1.58 11 -7 -3 3.86 2.25 -11 7 2 8.17 2.03 11 -7 -2 5.93 1.28 11 -7 -2 4.45 1.38 11 -7 -2 6.34 2.26 -11 7 1 54.59 3.97 11 -7 -1 58.49 3.34 -11 7 1 58.43 4.30 11 -7 -1 55.67 7.00 11 -7 -1 63.90 3.63 11 -7 0 69.99 3.91 -11 7 0 72.93 4.86 11 -7 0 82.75 8.38 11 -7 0 69.38 3.91 -11 7 0 73.74 7.56 11 -7 1 124.53 9.99 11 -7 1 130.84 5.21 -11 7 -1 119.15 9.61 -11 7 -1 126.29 6.25 -11 7 -2 22.14 3.06 11 -7 2 24.18 2.42 -11 7 -2 23.00 4.36 11 -7 2 29.24 5.43 -11 7 -3 8.13 2.07 11 -7 3 8.65 1.71 -11 7 -3 6.49 2.05 11 -7 4 0.94 1.10 -11 7 -4 -0.53 1.53 11 -7 5 114.38 5.01 -11 7 -5 119.76 6.45 11 -7 6 53.78 3.54 -11 7 -6 55.67 4.48 11 -7 7 178.17 6.14 -11 7 -7 171.44 7.76 11 -7 8 108.98 4.82 -11 7 -8 106.69 6.15 11 -7 9 12.45 1.82 -11 7 -9 12.23 2.57 -11 7 -10 36.31 3.59 11 -7 10 40.17 2.92 -11 7 -11 84.66 5.02 11 -7 11 101.15 4.16 -11 7 -11 92.55 5.47 11 -7 12 6.54 1.29 -11 7 -12 5.80 1.83 -11 7 -12 3.51 1.40 -11 7 -13 3.99 1.49 -11 7 -13 3.85 1.57 11 -7 13 4.30 0.97 -11 7 -14 -0.57 1.09 11 -7 15 7.60 0.99 -11 7 -15 5.15 1.21 11 -6 -21 69.79 2.30 11 -6 -20 3.16 0.73 -11 6 20 3.32 1.13 -11 6 20 3.49 1.04 11 -6 -19 15.18 1.53 -11 6 19 12.02 2.05 -11 6 18 13.13 1.94 -11 6 18 9.13 1.55 11 -6 -18 14.06 1.58 -11 6 18 13.32 2.25 -11 6 17 11.16 1.96 11 -6 -17 11.10 1.51 -11 6 16 5.33 1.68 11 -6 -16 2.93 1.02 -11 6 15 27.96 3.00 11 -6 -15 28.44 2.49 -11 6 14 8.76 2.17 11 -6 -14 7.75 1.57 11 -6 -13 144.54 5.32 -11 6 13 155.44 6.69 11 -6 -12 97.71 4.41 -11 6 12 105.48 5.61 -11 6 11 6.19 2.04 11 -6 -11 5.17 1.39 -11 6 11 4.62 2.57 -11 6 10 12.71 2.31 -11 6 10 16.67 3.12 11 -6 -10 15.63 1.98 11 -6 -9 4.56 1.30 -11 6 9 2.70 1.70 11 -6 -9 2.01 3.52 -11 6 9 2.81 2.01 11 -6 -9 2.87 3.02 11 -6 -8 182.60 6.05 11 -6 -8 163.95 12.05 -11 6 8 184.09 7.40 -11 6 8 185.54 8.25 11 -6 -8 165.68 10.83 11 -6 -7 0.86 1.11 -11 6 7 -1.57 2.02 11 -6 -7 3.27 2.00 11 -6 -7 -0.48 1.99 -11 6 7 -0.31 1.93 11 -6 -6 377.10 8.61 -11 6 6 374.52 11.07 11 -6 -6 388.03 16.11 11 -6 -6 348.57 16.42 -11 6 6 380.59 10.46 11 -6 -5 15.36 1.99 -11 6 5 18.15 2.72 11 -6 -5 13.33 2.91 11 -6 -5 17.46 3.85 -11 6 5 15.57 2.52 11 -6 -4 12.93 1.89 -11 6 4 10.57 2.29 11 -6 -4 12.23 2.85 11 -6 -4 12.74 3.60 -11 6 4 12.70 2.41 11 -6 -3 10.22 1.71 11 -6 -3 10.71 3.22 11 -6 -3 8.57 2.90 -11 6 3 9.56 2.06 -11 6 2 16.51 2.50 11 -6 -2 19.86 4.06 11 -6 -2 18.21 2.10 11 -6 -2 14.66 3.43 -11 6 2 15.99 3.91 -11 6 1 19.74 2.53 11 -6 -1 18.93 4.10 11 -6 -1 25.78 2.44 -11 6 1 15.42 3.60 11 -6 -1 18.11 3.15 -11 6 0 15.95 3.73 11 -6 0 19.41 4.43 -11 6 0 12.95 2.18 -11 6 0 15.30 2.36 11 -6 0 16.97 3.74 11 -6 0 20.95 2.48 11 -6 0 14.23 1.88 11 -6 1 88.41 8.35 11 -6 1 71.84 3.84 -11 6 -1 80.59 4.96 11 -6 1 75.59 7.00 -11 6 -1 68.09 7.18 -11 6 -2 2.80 2.01 -11 6 -2 2.69 1.76 11 -6 2 -0.32 1.04 11 -6 2 0.24 2.09 11 -6 2 -0.12 1.96 11 -6 2 0.06 2.13 11 -6 3 184.89 6.07 -11 6 -3 192.91 7.77 -11 6 -3 187.88 12.07 11 -6 3 184.04 13.32 -11 6 -4 73.65 4.90 -11 6 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11 -5 -12 0.22 1.13 -11 5 12 -1.76 1.56 -11 5 11 43.95 3.79 11 -5 -11 47.67 3.22 -11 5 10 5.00 1.93 11 -5 -10 5.47 1.37 11 -5 -10 5.81 3.17 -11 5 9 8.26 1.87 11 -5 -9 9.45 2.80 -11 5 9 11.90 2.83 11 -5 -9 12.09 1.83 11 -5 -8 186.85 6.03 -11 5 8 194.14 8.85 11 -5 -8 177.42 11.11 11 -5 -8 183.36 12.08 -11 5 8 194.04 7.30 11 -5 -7 35.78 2.69 11 -5 -7 35.96 5.37 -11 5 7 38.90 4.02 11 -5 -7 43.81 6.00 -11 5 7 39.69 3.54 11 -5 -6 13.17 1.68 -11 5 6 8.19 1.79 11 -5 -6 5.04 1.75 11 -5 -6 10.26 2.89 -11 5 6 9.14 2.18 11 -5 -5 287.93 7.30 -11 5 5 291.07 9.37 11 -5 -5 278.17 13.99 -11 5 5 273.60 8.68 11 -5 -5 278.93 13.43 11 -5 -4 4.34 2.30 -11 5 4 6.15 2.02 11 -5 -4 5.27 1.34 11 -5 -4 5.74 2.60 -11 5 4 6.30 1.84 -11 5 4 6.13 2.55 11 -5 -3 34.65 4.60 -11 5 3 37.89 3.40 11 -5 -3 36.55 2.80 11 -5 -3 31.16 4.63 -11 5 3 32.50 3.26 -11 5 3 33.66 4.99 11 -5 -2 6.84 2.25 -11 5 2 5.54 1.83 11 -5 -2 5.25 2.56 -11 5 2 8.70 3.13 11 -5 -2 7.14 1.50 11 -5 -1 12.91 3.07 -11 5 1 12.06 2.01 11 -5 -1 14.05 3.40 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213.63 6.48 -11 5 -11 202.35 8.33 11 -5 12 37.60 2.72 -11 5 -12 28.79 3.33 -11 5 -12 30.66 3.51 11 -5 13 79.04 3.63 -11 5 -13 71.76 4.74 -11 5 -13 75.71 4.86 11 -5 14 2.04 0.88 -11 5 -14 1.92 1.33 -11 5 -14 0.90 1.35 -11 5 -15 1.41 1.40 -11 5 -15 0.18 1.21 11 -5 16 35.75 2.11 -11 5 -16 34.84 2.85 -11 5 -16 30.93 2.48 11 -5 17 5.75 0.89 11 -4 -21 11.88 1.11 11 -4 -21 12.04 1.21 -11 4 21 12.31 1.52 11 -4 -21 9.80 1.06 11 -4 -20 17.91 1.51 -11 4 20 15.87 1.83 11 -4 -19 3.44 0.89 -11 4 19 1.44 1.20 -11 4 18 100.77 4.80 11 -4 -18 92.10 3.88 -11 4 17 40.30 3.32 11 -4 -17 38.85 2.63 11 -4 -16 9.76 1.59 -11 4 16 10.64 2.11 11 -4 -15 17.10 2.16 -11 4 15 17.78 2.53 11 -4 -14 13.35 1.86 -11 4 14 10.37 2.02 11 -4 -13 1.49 1.03 -11 4 13 2.27 1.50 11 -4 -12 2.91 1.16 -11 4 12 1.65 1.67 11 -4 -11 4.90 2.63 -11 4 11 8.31 2.04 -11 4 11 10.87 6.31 11 -4 -11 2.95 1.22 -11 4 10 47.61 3.94 11 -4 -10 48.89 3.27 -11 4 10 43.07 8.42 11 -4 -10 45.53 5.94 -11 4 9 43.89 3.65 11 -4 -9 44.72 3.04 -11 4 9 40.49 7.89 11 -4 -9 41.11 5.75 11 -4 -8 121.11 9.21 -11 4 8 121.41 5.80 11 -4 -8 137.56 5.20 11 -4 -7 174.27 5.67 11 -4 -7 165.42 10.39 11 -4 -7 176.97 11.24 -11 4 7 171.97 6.69 -11 4 7 167.25 7.86 -11 4 6 37.78 3.77 11 -4 -6 37.85 2.69 -11 4 6 29.31 5.08 11 -4 -6 36.20 5.04 11 -4 -6 30.70 4.64 -11 4 6 35.94 3.21 -11 4 5 159.07 6.75 11 -4 -5 152.23 5.33 -11 4 5 155.76 10.60 11 -4 -5 155.70 9.83 11 -4 -5 154.75 9.67 -11 4 5 152.53 6.21 -11 4 4 103.57 5.38 11 -4 -4 103.81 4.29 -11 4 4 93.50 8.10 11 -4 -4 102.76 7.93 11 -4 -4 100.11 7.78 -11 4 4 98.43 5.04 -11 4 3 7.18 1.71 11 -4 -3 6.46 1.34 -11 4 3 4.12 2.43 11 -4 -3 6.06 2.46 11 -4 -3 5.49 2.37 -11 4 3 9.02 2.15 -11 4 2 14.79 2.14 11 -4 -2 12.77 1.67 -11 4 2 11.90 3.04 11 -4 -2 15.88 3.32 11 -4 -2 13.56 2.98 -11 4 2 10.52 1.92 11 -4 -1 -0.08 1.63 11 -4 -1 1.08 0.94 -11 4 1 -0.25 1.33 11 -4 -1 -2.24 1.86 -11 4 1 0.62 1.54 -11 4 0 10.18 2.80 11 -4 0 13.70 3.36 11 -4 0 14.51 3.38 11 -4 0 10.12 1.54 -11 4 0 11.47 1.76 -11 4 0 13.33 2.15 -11 4 -1 45.03 3.55 -11 4 -1 41.88 3.30 11 -4 1 41.35 4.92 11 -4 1 28.08 4.61 11 -4 1 40.57 5.35 11 -4 1 43.80 2.84 -11 4 -1 39.48 5.21 -11 4 -2 85.81 7.60 11 -4 2 76.87 6.84 -11 4 -2 83.67 4.72 11 -4 2 79.43 3.75 11 -4 2 63.07 7.14 -11 4 -3 28.67 2.86 11 -4 3 35.49 4.82 -11 4 -3 26.40 4.50 11 -4 3 36.67 6.47 -11 4 -4 31.04 3.23 11 -4 4 29.06 2.58 11 -4 4 30.33 4.72 -11 4 -4 34.75 5.10 11 -4 4 32.29 5.64 -11 4 -5 6.19 1.68 -11 4 -5 7.73 1.89 11 -4 5 7.26 1.63 11 -4 5 8.61 3.19 -11 4 -5 7.52 3.02 11 -4 5 4.16 2.58 -11 4 -6 0.39 1.26 11 -4 6 1.08 1.17 -11 4 -6 0.84 1.53 11 -4 6 -3.33 2.49 -11 4 -6 1.70 2.50 11 -4 6 -0.65 2.23 11 -4 7 25.76 2.36 -11 4 -7 26.99 3.10 11 -4 7 25.81 5.57 -11 4 -7 27.61 5.06 11 -4 7 30.84 5.25 -11 4 -8 121.33 6.32 11 -4 8 124.55 9.83 11 -4 8 123.55 11.29 -11 4 -8 119.34 10.04 11 -4 8 122.05 5.10 11 -4 9 44.19 3.23 -11 4 -9 38.18 3.85 11 -4 10 80.76 4.15 -11 4 -10 73.37 5.15 11 -4 11 91.67 4.31 -11 4 -11 83.16 5.49 11 -4 12 47.37 3.13 -11 4 -12 54.60 4.51 -11 4 -13 119.62 6.31 -11 4 -13 113.95 6.34 11 -4 14 24.44 1.86 -11 4 -14 36.48 3.64 -11 4 -14 33.67 3.32 -11 4 -15 -1.63 1.55 -11 4 -15 2.36 1.55 -11 4 -16 24.89 2.72 -11 4 -16 26.13 2.74 -11 4 -17 1.02 1.00 11 -4 17 3.01 0.94 11 -4 18 54.75 2.31 11 -3 -21 0.10 0.51 -11 3 21 0.87 0.94 11 -3 -20 0.16 0.65 -11 3 20 0.10 0.94 11 -3 -19 18.34 1.69 -11 3 19 17.98 2.06 11 -3 -18 1.37 1.00 -11 3 18 1.04 1.21 11 -3 -17 1.33 1.02 -11 3 17 0.41 1.34 11 -3 -16 34.44 2.65 -11 3 16 35.77 3.27 11 -3 -15 50.55 3.23 -11 3 15 51.65 3.94 11 -3 -14 2.09 1.04 -11 3 14 -3.64 1.60 11 -3 -13 239.40 6.89 -11 3 13 263.86 8.51 -11 3 12 28.58 2.85 11 -3 -12 29.25 2.46 -11 3 11 51.86 8.40 -11 3 11 74.95 4.56 11 -3 -11 67.95 3.79 11 -3 -11 55.74 6.93 -11 3 10 117.27 5.56 11 -3 -10 91.30 8.66 -11 3 10 91.88 11.00 11 -3 -10 101.98 4.56 -11 3 9 3.45 3.57 11 -3 -9 0.32 2.14 11 -3 -9 4.49 1.31 -11 3 9 3.02 1.77 -11 3 8 247.72 7.86 -11 3 8 236.76 15.76 11 -3 -8 239.48 12.58 11 -3 -8 240.39 6.64 11 -3 -7 1.37 1.60 -11 3 7 5.53 2.64 -11 3 7 4.20 3.62 11 -3 -7 7.38 1.56 11 -3 -7 3.44 2.09 -11 3 7 5.80 1.74 -11 3 6 55.65 6.68 11 -3 -6 53.00 5.77 11 -3 -6 53.12 3.16 -11 3 6 59.30 3.96 11 -3 -6 60.54 6.30 -11 3 6 56.06 4.30 -11 3 5 340.75 8.83 -11 3 5 332.53 15.00 11 -3 -5 349.48 14.34 11 -3 -5 360.74 14.12 11 -3 -5 345.19 7.57 -11 3 4 1.74 1.52 11 -3 -4 1.59 1.49 -11 3 4 1.88 1.96 11 -3 -4 1.00 1.73 11 -3 -4 2.43 1.01 -11 3 3 599.57 19.51 11 -3 -3 634.18 18.20 -11 3 3 624.74 11.93 11 -3 -3 637.52 18.67 -11 3 2 70.14 6.74 11 -3 -2 87.64 7.06 11 -3 -2 80.36 6.46 -11 3 2 84.54 4.44 11 -3 -1 241.08 11.25 11 -3 -1 228.44 11.28 -11 3 1 225.24 7.17 -11 3 1 218.60 11.31 11 -3 0 19.98 3.46 -11 3 0 17.15 3.33 11 -3 0 18.60 3.61 11 -3 0 6.96 1.94 11 -3 1 18.32 3.34 11 -3 1 16.60 3.10 11 -3 1 11.71 2.74 -11 3 -1 22.41 4.01 11 -3 2 41.03 5.04 11 -3 2 27.04 4.05 -11 3 -2 38.37 4.87 11 -3 3 60.93 6.25 11 -3 3 49.53 6.00 -11 3 -3 64.59 4.02 -11 3 -3 62.70 6.41 11 -3 4 386.51 15.59 11 -3 4 360.52 16.87 -11 3 -4 359.88 9.47 -11 3 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1.42 11 4 -14 1.71 1.09 -11 -4 13 310.77 8.29 11 4 -13 310.93 7.91 11 4 -12 6.57 2.55 11 4 -12 4.88 3.07 -11 -4 12 6.55 1.60 -11 -4 12 8.80 2.03 11 4 -12 3.01 1.23 11 4 -11 326.00 7.97 11 4 -11 313.00 16.18 -11 -4 11 332.61 9.97 11 4 -11 320.30 14.07 -11 -4 11 337.49 8.32 11 4 -10 58.50 3.36 11 4 -10 56.92 7.26 -11 -4 10 65.76 4.43 11 4 -10 52.23 5.63 -11 -4 10 59.16 3.49 11 4 -9 420.25 8.62 -11 -4 9 445.84 10.75 11 4 -9 427.42 17.31 11 4 -9 415.82 15.04 -11 -4 9 416.39 8.84 11 4 -8 5.53 2.22 -11 -4 8 6.14 1.58 11 4 -8 10.01 1.39 11 4 -8 10.78 3.10 -11 -4 8 8.31 1.45 11 4 -7 0.26 1.09 11 4 -7 1.07 1.60 11 4 -6 166.54 8.98 11 4 -6 142.23 8.92 11 4 -5 273.12 11.00 11 4 -5 266.82 11.94 11 4 -4 0.44 1.72 -11 -4 4 0.72 1.84 11 4 -4 1.91 1.31 -11 -4 4 1.73 1.48 11 4 -3 844.62 18.67 -11 -4 3 913.25 20.90 11 4 -3 865.50 19.65 -11 -4 3 884.20 23.86 -11 -4 2 2.25 1.51 11 4 -2 1.39 1.48 -11 -4 2 0.94 1.81 -11 -4 1 222.65 10.10 11 4 -1 213.48 9.33 -11 -4 1 199.11 10.65 11 4 0 3.27 1.77 -11 -4 0 4.02 2.04 11 4 1 37.19 4.02 -11 -4 -1 28.97 4.07 11 4 2 274.86 10.63 -11 -4 -2 258.12 11.26 11 4 3 696.32 16.88 -11 -4 -3 687.04 17.74 11 4 4 1.67 1.39 11 4 4 0.78 1.58 -11 -4 -4 0.28 1.64 -11 -4 -5 448.97 14.42 11 4 5 480.63 14.77 11 4 5 460.97 14.23 -11 -4 -6 -0.04 1.62 11 4 6 2.76 2.43 -11 -4 -7 266.16 11.29 11 4 7 303.70 13.60 -11 -4 -8 287.74 11.88 11 4 8 258.24 13.32 -11 -4 -9 159.52 8.84 11 4 9 187.76 11.98 -11 -4 -10 44.98 3.61 -11 -4 -10 42.93 4.91 11 4 10 51.07 7.26 -11 -4 -11 34.88 3.38 -11 -4 -11 24.46 3.80 11 4 11 33.06 6.03 -11 -4 -12 22.06 3.75 11 4 12 24.81 5.21 -11 -4 -12 23.89 2.79 -11 -4 -12 18.98 2.74 -11 -4 -13 180.84 10.41 11 4 13 190.12 14.85 -11 -4 -13 184.64 7.79 -11 -4 -13 179.10 7.51 11 4 14 339.82 20.38 -11 -4 -14 323.21 10.58 -11 -4 -14 337.76 10.18 11 4 15 571.58 27.12 -11 -4 -15 546.09 13.25 -11 -4 -15 587.82 14.32 -11 -4 -16 1.27 1.55 -11 -4 -16 0.02 1.76 -11 -4 -17 3.45 1.62 -11 -4 -17 5.98 2.23 -11 -4 -18 3.72 1.64 11 4 18 2.33 0.98 -11 -4 -19 2.10 1.74 11 4 19 1.87 0.88 -11 -4 -20 12.40 2.29 11 4 20 13.33 1.45 -11 -4 -21 0.31 1.21 11 4 21 0.83 0.70 -11 -4 -22 14.40 1.89 -11 -4 -23 3.54 1.03 -11 -5 20 23.00 1.83 -11 -5 20 23.80 1.69 -11 -5 19 27.76 2.27 -11 -5 19 29.43 2.12 11 5 -19 26.61 1.93 -11 -5 18 60.96 3.26 11 5 -18 63.82 3.12 -11 -5 17 31.99 2.55 11 5 -17 29.70 2.35 -11 -5 16 30.75 2.59 11 5 -16 33.57 2.56 -11 -5 15 -0.44 1.13 -11 -5 15 -0.72 1.47 11 5 -15 0.38 1.07 -11 -5 14 48.82 3.42 -11 -5 14 48.65 4.03 11 5 -14 52.24 3.36 -11 -5 13 18.43 2.21 11 5 -13 19.83 2.23 -11 -5 13 15.17 2.50 -11 -5 12 260.82 7.42 11 5 -12 253.27 13.02 11 5 -12 271.43 7.39 -11 -5 12 256.71 8.76 11 5 -11 816.22 12.45 -11 -5 11 788.71 12.54 11 5 -11 789.00 22.49 -11 -5 11 814.74 15.06 11 5 -10 46.24 3.15 -11 -5 10 41.78 2.94 11 5 -10 43.17 5.99 11 5 -10 36.89 4.92 -11 -5 10 42.83 3.54 11 5 -9 309.80 7.40 11 5 -9 292.18 13.25 -11 -5 9 279.61 7.07 11 5 -9 299.65 14.93 -11 -5 9 283.75 8.49 11 5 -8 6.88 1.29 11 5 -8 5.80 2.12 -11 -5 8 7.99 1.70 -11 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2.53 -11 -5 -11 4.77 1.60 -11 -5 -11 1.16 1.39 -11 -5 -11 2.77 1.39 11 5 12 -0.45 2.52 -11 -5 -12 1.12 1.82 -11 -5 -12 0.75 1.30 -11 -5 -12 0.40 1.50 11 5 13 26.58 6.63 -11 -5 -13 21.80 3.12 -11 -5 -13 17.61 3.08 -11 -5 -13 18.74 2.75 -11 -5 -14 186.15 7.83 -11 -5 -14 203.90 8.32 11 5 14 195.34 15.38 -11 -5 -15 2.49 1.88 -11 -5 -15 2.09 2.00 11 5 15 -0.56 3.70 -11 -5 -16 224.00 8.67 -11 -5 -16 231.03 9.25 -11 -5 -17 108.14 6.02 -11 -5 -17 104.44 6.27 11 5 18 6.06 1.09 -11 -5 -18 6.76 1.82 -11 -5 -18 7.76 2.27 -11 -5 -19 3.85 1.80 -11 -5 -20 -1.10 1.46 -11 -5 -21 5.96 1.59 -11 -5 -22 5.75 1.49 -11 -5 -23 37.34 2.55 -11 -5 -24 0.90 0.81 11 6 -20 10.43 1.03 -11 -6 19 71.36 2.95 11 6 -19 72.46 2.84 -11 -6 19 66.78 3.21 -11 -6 18 0.90 0.91 11 6 -18 0.97 0.86 -11 -6 18 -0.34 0.86 -11 -6 17 108.36 4.35 11 6 -17 116.18 4.28 -11 -6 16 11.17 1.94 -11 -6 16 5.64 1.74 11 6 -16 9.70 1.59 -11 -6 15 90.35 4.27 -11 -6 15 81.25 5.19 11 6 -15 89.03 4.08 -11 -6 14 19.79 2.18 -11 -6 14 18.35 2.56 11 6 -14 23.57 2.29 -11 -6 13 130.55 5.31 -11 -6 13 127.62 6.30 11 6 -13 132.44 5.25 -11 -6 12 210.16 6.62 11 6 -12 222.22 6.73 -11 -6 12 203.29 7.54 11 6 -11 61.25 3.77 -11 -6 11 71.62 3.85 11 6 -11 73.96 7.17 -11 -6 11 74.78 4.72 11 6 -10 170.78 5.86 11 6 -10 178.06 10.78 -11 -6 10 173.16 5.75 11 6 -10 175.05 12.28 -11 -6 10 176.67 6.92 11 6 -9 18.15 2.08 11 6 -9 20.66 4.87 -11 -6 9 16.10 2.22 -11 -6 9 16.15 2.01 -11 -6 9 13.47 1.87 11 6 -9 15.19 3.37 11 6 -8 96.23 7.55 -11 -6 8 103.71 4.94 -11 -6 8 95.84 4.12 -11 -6 8 102.63 4.36 11 6 -8 94.15 8.15 11 6 -8 105.89 4.40 11 6 -7 58.06 5.75 -11 -6 7 59.84 3.65 11 6 -7 51.91 3.05 -11 -6 7 54.88 2.98 11 6 -7 47.56 5.78 11 6 -6 19.16 3.66 -11 -6 6 20.47 3.23 11 6 -6 17.58 3.28 11 6 -5 207.21 10.47 -11 -6 5 209.77 10.19 11 6 -5 226.62 10.45 11 6 -4 107.20 7.29 11 6 -4 101.88 6.90 -11 -6 4 106.74 7.18 11 6 -3 37.24 4.44 -11 -6 3 39.76 4.33 11 6 -3 32.16 3.80 -11 -6 3 31.73 4.98 11 6 -2 549.09 15.20 -11 -6 2 535.62 15.74 11 6 -2 552.51 14.91 -11 -6 2 542.91 18.46 -11 -6 1 19.48 3.83 11 6 -1 18.75 2.84 11 6 -1 24.60 3.31 -11 -6 1 23.40 3.54 11 6 0 156.43 7.79 -11 -6 0 142.26 8.21 -11 -6 0 142.87 9.09 11 6 1 51.17 4.59 -11 -6 -1 47.19 4.72 -11 -6 -1 54.43 5.68 11 6 2 215.77 9.09 -11 -6 -2 204.69 9.69 -11 -6 -2 215.51 10.20 11 6 3 170.36 8.32 -11 -6 -3 143.29 8.35 -11 -6 -3 150.62 8.53 -11 -6 -4 63.02 5.47 -11 -6 -4 61.05 5.50 11 6 4 61.95 5.11 -11 -6 -5 12.88 2.65 11 6 5 18.47 2.89 -11 -6 -6 190.09 9.19 11 6 6 192.57 9.16 -11 -6 -7 1.55 1.24 11 6 7 2.10 2.07 -11 -6 -8 174.43 9.03 11 6 8 187.61 10.89 -11 -6 -9 1.13 1.13 11 6 9 0.21 2.44 -11 -6 -10 266.66 11.42 11 6 10 299.72 15.68 -11 -6 -11 104.85 5.42 -11 -6 -11 114.57 7.56 -11 -6 -11 103.84 5.43 -11 -6 -12 295.88 12.13 -11 -6 -12 293.24 8.45 -11 -6 -12 294.00 9.41 -11 -6 -12 283.63 9.19 -11 -6 -12 295.78 9.48 11 6 12 311.63 17.55 -11 -6 -13 43.29 3.84 -11 -6 -13 45.57 3.84 11 6 13 55.47 8.59 -11 -6 -14 35.75 3.81 -11 -6 -14 34.13 3.53 11 6 14 32.07 5.94 -11 -6 -15 14.60 2.84 -11 -6 -15 10.71 2.39 11 6 15 11.44 4.95 -11 -6 -16 2.65 1.69 -11 -6 -16 3.28 1.69 -11 -6 -17 55.07 4.73 -11 -6 -17 53.66 4.50 -11 -6 -18 85.00 5.72 -11 -6 -18 82.87 5.22 -11 -6 -19 -0.30 1.54 -11 -6 -19 3.13 1.69 -11 -6 -20 2.81 1.80 -11 -6 -21 1.65 1.53 -11 -6 -22 0.66 1.25 -11 -6 -23 23.20 2.30 -11 -6 -24 24.81 1.91 -11 -7 19 6.62 1.07 11 7 -19 10.07 1.11 -11 -7 19 7.36 1.05 -11 -7 18 2.66 0.90 11 7 -18 3.59 0.82 -11 -7 18 3.13 0.88 -11 -7 17 10.21 1.60 -11 -7 17 11.53 1.49 11 7 -17 13.01 1.49 -11 -7 16 6.41 1.54 -11 -7 16 9.47 1.59 11 7 -16 8.11 1.45 -11 -7 15 62.41 4.41 -11 -7 15 62.98 3.60 11 7 -15 70.00 3.64 -11 -7 14 9.96 2.02 -11 -7 14 7.36 1.48 11 7 -14 12.04 1.81 -11 -7 13 54.34 4.02 11 7 -13 59.82 3.58 -11 -7 13 54.81 3.39 11 7 -12 24.04 2.44 -11 -7 12 26.56 2.50 -11 -7 12 26.01 2.96 -11 -7 11 736.42 11.87 11 7 -11 757.56 12.65 11 7 -11 709.14 24.75 -11 -7 11 741.84 14.12 -11 -7 10 87.16 4.92 -11 -7 10 92.94 4.18 11 7 -10 76.58 7.58 11 7 -10 92.94 8.96 11 7 -10 107.24 4.67 11 7 -9 290.86 7.55 -11 -7 9 274.72 8.21 -11 -7 9 263.97 6.86 -11 -7 9 276.35 7.32 11 7 -9 257.72 13.06 11 7 -8 61.75 3.44 -11 -7 8 59.46 3.70 -11 -7 8 56.52 3.15 -11 -7 8 62.58 3.43 11 7 -8 57.48 6.02 11 7 -7 83.07 4.01 -11 -7 7 76.65 4.02 11 7 -7 68.56 6.38 -11 -7 7 76.47 3.67 11 7 -6 7.66 2.07 -11 -7 6 9.78 3.00 11 7 -6 9.51 2.26 11 7 -5 36.02 4.68 11 7 -5 39.26 4.51 -11 -7 5 31.90 4.05 11 7 -4 1.54 1.66 -11 -7 4 1.48 1.69 11 7 -4 3.30 1.63 11 7 -3 52.77 4.98 -11 -7 3 45.13 5.12 11 7 -3 51.01 4.79 11 7 -2 211.35 9.54 11 7 -2 188.05 8.92 -11 -7 2 204.86 9.93 11 7 -1 36.10 3.99 -11 -7 1 34.63 4.18 -11 -7 1 33.12 4.73 11 7 -1 38.84 4.02 11 7 0 25.23 3.43 11 7 0 20.11 2.94 -11 -7 0 16.98 3.57 -11 -7 0 23.25 3.66 11 7 1 2.39 1.37 -11 -7 -1 2.58 2.27 11 7 1 1.92 1.29 -11 -7 -1 1.73 1.72 11 7 2 36.86 3.86 -11 -7 -2 39.72 4.74 -11 -7 -2 33.90 4.04 11 7 3 1.21 1.34 -11 -7 -3 1.69 1.96 -11 -7 -3 3.00 1.87 11 7 4 2.41 1.80 -11 -7 -4 6.85 2.38 -11 -7 -4 3.61 2.02 11 7 5 0.20 1.29 -11 -7 -5 4.17 2.03 -11 -7 -5 -0.34 1.66 -11 -7 -6 2.13 1.82 11 7 6 0.02 1.54 -11 -7 -7 33.65 3.81 11 7 7 24.71 3.59 -11 -7 -8 6.72 2.07 11 7 8 0.05 2.08 -11 -7 -9 12.33 2.76 11 7 9 9.29 3.17 -11 -7 -10 15.23 2.80 11 7 10 20.04 4.12 -11 -7 -11 174.66 6.97 -11 -7 -11 182.47 7.16 -11 -7 -11 178.38 6.42 -11 -7 -12 56.51 3.12 -11 -7 -12 60.05 3.17 -11 -7 -12 57.63 4.50 -11 -7 -12 52.50 4.11 -11 -7 -12 55.92 4.14 -11 -7 -12 57.36 3.93 11 7 12 43.69 6.50 -11 -7 -13 284.71 7.05 -11 -7 -13 279.14 9.39 -11 -7 -13 285.02 7.03 -11 -7 -13 301.99 10.12 -11 -7 -13 278.50 8.63 -11 -7 -13 300.14 9.71 -11 -7 -14 1.10 0.81 -11 -7 -14 2.71 1.58 -11 -7 -14 2.35 1.01 -11 -7 -14 4.05 2.35 -11 -7 -15 131.22 6.72 -11 -7 -15 135.31 4.89 -11 -7 -15 131.49 4.87 -11 -7 -15 129.09 6.71 11 7 15 128.39 12.66 -11 -7 -16 9.59 2.29 -11 -7 -16 12.13 2.71 -11 -7 -16 7.85 1.29 -11 -7 -16 8.79 1.42 -11 -7 -17 17.08 2.73 -11 -7 -17 19.17 3.10 -11 -7 -18 26.81 3.34 -11 -7 -18 25.86 3.40 -11 -7 -19 82.35 5.13 -11 -7 -19 86.00 5.47 -11 -7 -20 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11 8 -7 10.58 2.41 -11 -8 7 16.46 1.89 -11 -8 6 54.52 3.32 11 8 -6 54.38 5.61 11 8 -6 54.29 3.15 11 8 -6 38.54 4.92 -11 -8 6 58.06 6.00 -11 -8 6 51.24 2.90 11 8 -5 136.97 8.81 -11 -8 5 122.11 8.22 11 8 -4 37.69 4.49 11 8 -4 31.51 4.14 -11 -8 4 35.84 4.60 11 8 -3 124.88 7.55 11 8 -3 121.07 7.61 -11 -8 3 108.03 7.51 11 8 -2 96.35 6.34 11 8 -2 111.55 7.16 -11 -8 2 94.90 6.99 11 8 -1 431.24 13.19 -11 -8 1 436.31 14.70 11 8 -1 414.52 13.08 11 8 0 26.58 3.26 11 8 0 28.12 3.48 -11 -8 0 27.06 3.83 -11 -8 0 29.46 4.58 11 8 1 3.28 1.85 -11 -8 -1 8.94 3.05 11 8 1 2.95 1.43 -11 -8 -1 3.74 1.83 11 8 2 372.61 11.62 -11 -8 -2 343.64 12.83 -11 -8 -2 345.75 13.57 11 8 2 364.15 11.51 -11 -8 -3 15.42 2.80 11 8 3 20.13 2.93 -11 -8 -3 24.38 3.86 11 8 3 22.78 2.96 -11 -8 -4 171.15 8.97 11 8 4 181.45 8.31 -11 -8 -4 171.04 9.22 -11 -8 -5 1.09 1.49 -11 -8 -5 0.04 1.39 11 8 5 0.83 1.50 -11 -8 -6 39.89 4.22 -11 -8 -6 35.56 4.28 11 8 6 39.18 4.30 11 8 7 17.97 3.09 -11 -8 -7 14.96 2.91 -11 -8 -7 14.36 2.53 11 8 8 30.07 4.28 -11 -8 -8 40.31 4.31 11 8 9 170.07 10.81 -11 -8 -9 221.88 9.73 11 8 10 46.97 6.64 -11 -8 -11 196.99 7.47 -11 -8 -11 196.11 6.85 -11 -8 -11 199.92 7.95 -11 -8 -12 159.24 5.33 -11 -8 -12 158.64 5.20 -11 -8 -12 160.39 6.87 -11 -8 -12 159.70 6.92 -11 -8 -12 155.88 6.38 -11 -8 -12 157.94 7.36 -11 -8 -13 32.35 2.43 -11 -8 -13 31.39 2.45 11 8 13 25.87 5.55 -11 -8 -13 29.53 3.37 -11 -8 -13 30.57 3.32 -11 -8 -13 31.75 3.19 -11 -8 -13 35.21 3.84 -11 -8 -14 77.64 3.78 -11 -8 -14 75.18 5.08 -11 -8 -14 78.03 5.33 11 8 14 78.32 9.90 -11 -8 -14 76.47 3.80 -11 -8 -15 43.26 2.91 -11 -8 -15 48.16 4.15 -11 -8 -15 46.20 4.24 11 8 15 50.05 8.01 -11 -8 -15 48.58 3.12 -11 -8 -16 211.28 6.42 -11 -8 -16 200.23 8.48 -11 -8 -16 196.98 8.47 11 8 16 186.05 15.78 -11 -8 -16 206.68 6.48 -11 -8 -17 208.64 8.80 -11 -8 -17 228.19 6.66 -11 -8 -17 220.04 8.84 -11 -8 -17 225.00 6.51 -11 -8 -18 26.70 3.33 -11 -8 -18 27.07 2.28 -11 -8 -18 29.56 2.49 -11 -8 -18 29.05 3.39 -11 -8 -19 2.65 0.94 -11 -8 -19 1.60 1.70 -11 -8 -19 0.67 1.59 -11 -8 -19 2.39 1.06 -11 -8 -20 159.65 7.15 -11 -8 -20 155.49 6.81 -11 -8 -21 29.77 3.14 -11 -8 -21 30.52 2.95 -11 -8 -22 30.42 2.82 -11 -8 -23 -2.56 1.27 -11 -8 -24 17.79 1.83 -11 -8 -25 0.87 0.64 11 9 -18 3.16 0.82 -11 -9 17 39.55 2.40 11 9 -17 48.56 2.45 -11 -9 16 51.51 3.69 -11 -9 16 51.04 3.08 -11 -9 16 57.23 2.81 11 9 -16 57.41 2.87 -11 -9 15 7.01 1.67 -11 -9 15 7.62 1.60 -11 -9 15 6.77 1.29 11 9 -15 6.41 1.34 -11 -9 14 0.26 1.15 -11 -9 14 -0.47 1.12 -11 -9 14 -0.01 0.88 11 9 -14 0.46 0.93 -11 -9 13 4.69 1.69 -11 -9 13 2.81 1.26 11 9 -13 3.43 1.27 -11 -9 13 2.66 1.11 11 9 -12 0.72 1.06 -11 -9 12 1.49 1.28 -11 -9 12 2.84 1.40 11 9 -11 8.54 1.61 -11 -9 11 6.92 1.82 -11 -9 10 140.19 5.49 11 9 -10 132.00 5.42 -11 -9 10 124.65 5.64 11 9 -9 0.27 1.30 -11 -9 9 2.33 1.29 -11 -9 9 -0.60 1.15 11 9 -9 1.73 1.76 -11 -9 8 28.45 2.57 -11 -9 8 35.20 3.01 11 9 -8 31.85 5.13 -11 -9 7 26.46 2.39 11 9 -7 32.37 2.74 -11 -9 7 29.30 2.59 11 9 -7 29.77 4.69 11 9 -6 164.62 5.75 -11 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-11 -9 -11 217.05 8.54 -11 -9 -11 210.21 5.95 -11 -9 -11 220.77 7.88 -11 -9 -11 202.09 15.14 -11 -9 -11 218.65 7.28 -11 -9 -11 214.92 6.11 -11 -9 -12 58.53 3.27 -11 -9 -12 58.78 4.25 -11 -9 -12 60.26 3.30 11 9 12 48.16 7.25 -11 -9 -12 57.07 4.27 -11 -9 -12 62.42 8.64 -11 -9 -12 54.03 4.48 -11 -9 -12 61.19 4.06 -11 -9 -13 4.31 1.79 -11 -9 -13 4.52 1.80 11 9 13 4.17 2.73 -11 -9 -13 3.66 1.96 -11 -9 -13 6.33 4.02 -11 -9 -13 3.70 1.20 -11 -9 -13 4.00 1.42 -11 -9 -13 5.35 1.34 -11 -9 -14 82.32 5.48 -11 -9 -14 78.80 3.95 -11 -9 -14 77.47 3.91 -11 -9 -14 83.83 5.29 11 9 15 27.69 6.31 -11 -9 -15 37.03 2.82 -11 -9 -15 36.79 3.88 -11 -9 -15 38.08 2.85 -11 -9 -15 36.55 3.68 -11 -9 -16 4.00 1.19 -11 -9 -16 3.17 2.00 -11 -9 -16 1.62 1.05 11 9 16 3.79 3.03 -11 -9 -16 5.99 2.18 -11 -9 -17 36.54 2.80 -11 -9 -17 39.22 2.98 -11 -9 -17 38.80 3.86 -11 -9 -17 36.28 3.91 -11 -9 -18 108.23 4.68 -11 -9 -18 110.99 4.67 -11 -9 -18 111.64 6.31 -11 -9 -18 107.11 6.33 -11 -9 -19 176.83 5.85 -11 -9 -19 174.56 5.68 -11 -9 -19 172.98 7.49 -11 -9 -19 168.77 7.71 -11 -9 -20 206.83 5.98 -11 -9 -20 198.12 8.00 -11 -9 -20 206.80 7.92 -11 -9 -20 207.00 5.93 -11 -9 -21 1.20 0.78 -11 -9 -21 1.07 1.33 -11 -9 -21 1.22 0.88 -11 -9 -21 -0.38 1.22 -11 -9 -22 148.14 6.07 -11 -9 -23 4.38 1.41 -11 -9 -24 21.17 1.96 -11 -9 -25 2.11 0.75 11 10 -18 0.32 0.46 11 10 -17 1.45 0.76 11 10 -16 33.88 2.10 -11 -10 16 29.45 2.61 11 10 -15 18.50 1.77 -11 -10 15 17.73 1.97 -11 -10 15 16.66 2.20 11 10 -14 32.42 2.43 -11 -10 14 28.95 2.72 -11 -10 14 31.72 2.87 11 10 -13 32.18 2.56 -11 -10 13 33.23 2.98 -11 -10 13 37.26 3.38 11 10 -12 56.02 3.44 -11 -10 12 56.63 3.91 -11 -10 12 59.79 3.92 11 10 -11 16.24 2.11 -11 -10 11 17.90 2.39 -11 -10 11 15.86 1.96 11 10 -10 9.00 1.75 -11 -10 10 11.82 1.97 -11 -10 10 10.75 1.94 -11 -10 10 12.06 2.03 -11 -10 9 99.24 5.10 -11 -10 9 100.05 4.78 11 10 -9 108.58 5.13 -11 -10 9 100.64 5.16 11 10 -8 26.93 2.70 11 10 -8 27.99 4.66 -11 -10 8 34.53 2.97 -11 -10 8 30.82 2.97 -11 -10 8 33.57 2.70 -11 -10 7 520.52 9.53 -11 -10 7 501.43 11.04 11 10 -7 547.56 19.57 -11 -10 7 532.12 10.62 -11 -10 6 33.47 2.95 11 10 -6 32.53 4.82 -11 -10 6 33.26 4.73 -11 -10 6 43.64 2.91 -11 -10 6 39.06 2.97 -11 -10 5 190.45 6.59 11 10 -5 200.56 11.00 -11 -10 5 195.50 5.59 -11 -10 5 204.12 6.29 11 10 -4 140.93 9.08 -11 -10 4 126.78 4.44 -11 -10 4 135.02 5.48 11 10 -3 333.30 13.37 -11 -10 3 339.36 8.29 -11 -10 3 346.16 7.02 -11 -10 3 342.24 14.34 -11 -10 2 2.26 1.67 11 10 -2 0.99 1.33 -11 -10 1 1.42 1.83 11 10 -1 0.64 1.18 -11 -10 0 12.58 2.94 11 10 0 10.88 2.27 -11 -10 -1 2.82 1.81 11 10 1 3.11 1.26 -11 -10 -2 16.64 3.03 11 10 2 17.80 2.84 11 10 3 251.07 9.88 -11 -10 -3 250.30 11.25 -11 -10 -4 24.94 3.71 11 10 4 24.11 3.03 -11 -10 -4 17.47 3.32 -11 -10 -5 359.37 13.00 11 10 5 370.32 11.42 -11 -10 -5 362.73 13.62 -11 -10 -6 50.23 4.98 -11 -10 -6 52.36 7.26 -11 -10 -6 37.95 4.44 11 10 6 49.89 4.18 -11 -10 -7 854.46 21.09 -11 -10 -7 893.87 29.73 -11 -10 -8 5.75 3.01 -11 -10 -8 7.68 2.30 -11 -10 -9 121.45 11.52 -11 -10 -9 112.80 7.85 -11 -10 -10 50.27 3.86 -11 -10 -10 45.98 2.77 -11 -10 -10 57.56 8.14 -11 -10 -10 44.13 3.96 -11 -10 -10 46.41 2.90 -11 -10 -10 46.65 3.40 -11 -10 -11 22.19 2.76 -11 -10 -11 26.07 2.19 11 10 11 23.54 4.91 -11 -10 -11 31.14 6.23 -11 -10 -11 24.80 3.29 -11 -10 -11 27.39 2.72 -11 -10 -11 24.90 2.27 -11 -10 -12 427.29 9.01 -11 -10 -12 433.55 10.97 -11 -10 -12 422.07 8.83 11 10 12 404.50 19.88 -11 -10 -12 446.04 22.86 -11 -10 -12 424.86 12.61 -11 -10 -12 448.12 11.75 -11 -10 -12 452.36 10.71 -11 -10 -13 76.50 3.95 -11 -10 -13 84.20 5.00 -11 -10 -13 71.57 3.78 11 10 13 57.84 7.97 -11 -10 -13 81.12 10.23 -11 -10 -13 81.05 5.75 -11 -10 -13 71.86 4.79 -11 -10 -13 82.68 5.40 -11 -10 -14 52.40 4.18 -11 -10 -14 49.28 3.19 -11 -10 -14 49.29 4.32 -11 -10 -14 46.50 8.08 -11 -10 -14 47.51 3.21 -11 -10 -14 46.13 3.75 11 10 15 40.48 8.17 -11 -10 -15 46.34 8.34 -11 -10 -15 40.10 3.87 -11 -10 -15 40.08 2.87 -11 -10 -15 38.38 2.90 -11 -10 -15 39.48 3.82 11 10 16 63.07 10.03 -11 -10 -16 62.40 3.72 -11 -10 -16 66.96 3.75 -11 -10 -16 62.90 5.01 -11 -10 -16 58.32 4.66 -11 -10 -17 245.07 7.20 -11 -10 -17 247.26 7.18 -11 -10 -17 244.19 8.92 -11 -10 -17 248.97 9.58 -11 -10 -18 5.80 1.36 -11 -10 -18 5.61 1.45 -11 -10 -18 6.21 2.06 -11 -10 -18 7.64 2.24 -11 -10 -19 51.73 3.31 -11 -10 -19 56.07 3.48 -11 -10 -19 50.92 4.09 -11 -10 -19 52.98 4.44 -11 -10 -20 3.30 1.19 -11 -10 -20 3.42 1.06 -11 -10 -20 3.42 1.76 -11 -10 -20 1.93 1.48 -11 -10 -21 62.35 3.25 -11 -10 -21 65.14 3.25 -11 -10 -21 67.68 4.47 -11 -10 -21 60.86 4.33 -11 -10 -22 2.02 0.75 -11 -10 -22 1.54 0.83 -11 -10 -22 3.12 1.40 -11 -10 -23 79.91 2.89 -11 -10 -23 84.19 2.93 -11 -10 -23 78.11 4.02 -11 -10 -24 6.00 1.26 -11 -10 -25 -0.83 0.70 11 11 -17 2.47 0.65 -11 -11 16 27.15 2.34 11 11 -16 26.98 1.75 -11 -11 15 92.82 4.42 11 11 -15 97.50 3.52 -11 -11 14 14.65 1.94 -11 -11 14 17.19 1.95 11 11 -14 12.81 1.59 -11 -11 13 53.33 3.70 -11 -11 13 53.17 3.35 11 11 -13 52.37 3.10 -11 -11 12 18.24 2.36 -11 -11 12 22.29 2.42 11 11 -12 17.40 2.04 -11 -11 11 201.86 7.04 -11 -11 11 188.76 6.85 11 11 -11 195.03 6.33 -11 -11 10 2.79 1.29 11 11 -10 2.28 1.35 -11 -11 10 2.54 1.42 -11 -11 10 3.19 1.37 -11 -11 9 17.56 2.29 -11 -11 9 16.60 2.29 11 11 -9 14.72 2.15 -11 -11 9 15.65 2.10 -11 -11 8 88.00 4.63 -11 -11 8 94.96 4.96 -11 -11 8 92.35 4.40 -11 -11 7 105.56 5.11 -11 -11 7 123.18 9.32 11 11 -7 113.25 9.15 -11 -11 7 116.01 5.06 -11 -11 7 117.52 4.71 -11 -11 6 82.45 4.55 -11 -11 6 88.47 8.13 11 11 -6 102.67 4.99 11 11 -6 85.05 7.83 -11 -11 6 92.47 4.10 -11 -11 6 87.18 4.35 -11 -11 5 104.59 4.94 -11 -11 5 99.09 8.40 11 11 -5 108.69 8.56 -11 -11 5 104.59 4.26 -11 -11 5 92.41 4.32 -11 -11 4 211.40 6.87 -11 -11 4 211.41 11.86 11 11 -4 230.68 11.97 -11 -11 4 209.40 5.95 -11 -11 4 225.55 6.36 11 11 -3 134.57 8.78 -11 -11 3 134.83 5.37 -11 -11 3 135.79 4.62 -11 -11 3 130.75 9.29 11 11 -2 121.57 8.26 -11 -11 2 118.03 4.92 -11 -11 2 112.40 8.35 -11 -11 2 119.44 4.25 11 11 -1 682.39 18.66 -11 -11 1 669.71 20.05 11 11 0 88.94 6.47 -11 -11 0 80.10 6.83 11 11 1 6.10 1.70 -11 -11 -1 6.48 2.30 11 11 2 2.19 1.18 -11 -11 -2 1.02 1.42 11 11 3 200.69 8.96 -11 -11 -3 192.60 10.19 11 11 4 413.00 12.64 -11 -11 -4 363.89 14.09 11 11 5 37.26 3.77 -11 -11 -5 46.77 5.17 -11 -11 -6 693.67 19.13 -11 -11 -6 750.38 27.13 -11 -11 -7 639.93 18.30 -11 -11 -7 658.58 25.83 -11 -11 -8 182.51 9.96 -11 -11 -8 221.60 15.45 -11 -11 -9 364.11 7.84 -11 -11 -9 385.38 11.02 -11 -11 -9 386.09 14.56 -11 -11 -9 384.73 8.08 -11 -11 -9 373.83 9.35 -11 -11 -9 381.09 19.86 -11 -11 -10 36.95 3.81 -11 -11 -10 40.78 7.08 -11 -11 -10 35.70 3.33 -11 -11 -10 39.10 2.69 -11 -11 -10 38.47 3.19 -11 -11 -10 37.98 2.61 -11 -11 -11 217.73 9.03 -11 -11 -11 217.47 6.25 -11 -11 -11 230.65 15.94 -11 -11 -11 211.88 6.29 -11 -11 -11 213.81 7.38 -11 -11 -11 224.41 8.31 -11 -11 -12 193.66 7.95 -11 -11 -12 202.33 7.24 -11 -11 -12 200.48 6.13 -11 -11 -12 202.11 15.10 11 11 12 234.48 15.39 -11 -11 -12 204.66 6.33 -11 -11 -12 200.44 7.29 -11 -11 -12 202.75 9.05 11 11 13 -2.38 4.57 -11 -11 -13 2.37 1.59 -11 -11 -13 4.36 3.62 -11 -11 -13 1.65 0.91 -11 -11 -13 1.80 1.68 -11 -11 -13 0.24 1.26 -11 -11 -13 2.25 1.10 11 11 14 19.58 6.02 -11 -11 -14 14.27 2.50 -11 -11 -14 22.55 6.35 -11 -11 -14 16.98 2.08 -11 -11 -14 17.71 2.54 -11 -11 -14 18.82 2.57 -11 -11 -14 16.11 2.07 -11 -11 -15 113.66 4.92 11 11 15 101.00 11.88 -11 -11 -15 106.35 4.70 -11 -11 -15 105.22 5.85 -11 -11 -15 117.28 12.46 -11 -11 -15 108.98 6.43 -11 -11 -16 18.14 2.26 -11 -11 -16 14.76 2.60 -11 -11 -16 15.33 2.93 -11 -11 -16 18.82 2.15 -11 -11 -17 74.47 4.10 -11 -11 -17 72.78 3.99 -11 -11 -17 70.25 5.31 -11 -11 -17 66.61 4.85 -11 -11 -18 6.30 1.55 -11 -11 -18 8.26 2.10 -11 -11 -18 5.94 1.42 -11 -11 -18 4.12 1.93 -11 -11 -19 12.94 1.79 -11 -11 -19 9.26 2.10 -11 -11 -19 11.20 1.76 -11 -11 -19 13.33 2.80 -11 -11 -20 6.88 1.42 -11 -11 -20 7.31 1.88 -11 -11 -20 7.22 1.37 -11 -11 -20 6.40 1.93 -11 -11 -21 3.75 1.01 -11 -11 -21 3.89 1.64 -11 -11 -21 4.03 1.11 -11 -11 -21 5.63 1.83 -11 -11 -22 4.79 1.50 -11 -11 -22 4.14 1.02 -11 -11 -22 3.56 0.94 -11 -11 -23 12.90 1.85 -11 -11 -23 11.64 1.26 -11 -11 -23 10.30 1.18 -11 -11 -24 68.34 2.39 -11 -11 -24 68.15 2.42 -11 -11 -24 69.05 3.39 -11 -11 -25 0.65 0.63 11 12 -16 25.41 1.58 -11 -12 16 25.68 2.15 11 12 -15 9.86 1.17 -11 -12 15 8.84 1.46 11 12 -14 150.18 4.46 -11 -12 14 151.84 5.54 11 12 -13 3.86 1.13 -11 -12 13 1.68 0.98 11 12 -12 115.40 4.53 -11 -12 12 118.07 5.33 -11 -12 11 88.71 4.36 -11 -12 11 89.37 4.68 11 12 -11 91.00 4.22 -11 -12 10 210.69 6.72 -11 -12 10 201.18 6.72 -11 -12 10 198.42 6.81 11 12 -10 202.01 6.52 -11 -12 9 167.43 5.85 -11 -12 9 152.89 5.95 -11 -12 9 156.80 6.14 11 12 -9 169.69 6.23 -11 -12 8 0.99 1.30 -11 -12 8 1.12 1.20 -11 -12 8 1.42 1.09 -11 -12 7 167.94 6.11 -11 -12 7 170.08 5.71 -11 -12 7 165.43 6.28 -11 -12 6 84.12 4.50 11 12 -6 101.53 8.57 -11 -12 6 80.86 7.79 11 12 -6 97.81 4.88 -11 -12 6 86.21 4.06 -11 -12 6 96.35 4.58 -11 -12 5 10.27 1.95 -11 -12 5 11.66 1.79 11 12 -5 10.08 3.13 -11 -12 5 12.59 1.92 -11 -12 5 9.68 3.02 -11 -12 4 60.28 3.86 -11 -12 4 58.71 3.22 -11 -12 4 60.16 7.10 -11 -12 4 64.67 3.57 11 12 -4 71.78 7.03 -11 -12 3 2.47 1.46 -11 -12 3 1.64 0.94 11 12 -3 -1.29 1.52 -11 -12 3 0.55 1.85 -11 -12 3 0.56 0.96 11 12 -2 189.57 10.61 -11 -12 2 179.80 6.26 -11 -12 2 175.51 5.51 -11 -12 2 178.89 11.17 11 12 -1 264.21 12.11 -11 -12 1 275.81 7.59 -11 -12 1 295.76 6.66 -11 -12 1 270.72 13.30 11 12 0 178.95 9.86 -11 -12 0 183.53 5.27 -11 -12 0 183.73 6.06 -11 -12 0 173.70 10.55 11 12 1 110.34 7.51 -11 -12 -1 109.04 8.24 -11 -12 -1 111.96 4.13 -11 -12 -1 108.87 3.95 11 12 2 0.19 1.44 -11 -12 -2 1.47 1.52 11 12 3 138.27 7.76 -11 -12 -3 138.53 9.05 11 12 4 74.91 5.58 -11 -12 -4 74.16 6.58 -11 -12 -5 2.94 1.96 -11 -12 -5 1.46 2.65 -11 -12 -6 533.52 17.22 -11 -12 -6 609.53 24.84 -11 -12 -7 6.67 3.55 -11 -12 -7 4.97 1.85 -11 -12 -7 4.57 1.07 -11 -12 -7 5.07 1.13 -11 -12 -8 1405.06 15.31 -11 -12 -8 1468.69 16.11 -11 -12 -8 1474.68 18.21 -11 -12 -8 1426.72 38.56 -11 -12 -8 1411.89 21.51 -11 -12 -9 157.23 7.50 -11 -12 -9 161.60 13.09 -11 -12 -9 161.57 9.50 -11 -12 -9 155.61 5.25 -11 -12 -9 153.38 6.61 -11 -12 -9 148.90 6.06 -11 -12 -9 144.53 5.00 -11 -12 -10 399.55 12.08 -11 -12 -10 396.91 21.07 -11 -12 -10 414.64 15.67 -11 -12 -10 393.01 8.33 -11 -12 -10 403.33 8.58 -11 -12 -10 388.92 9.81 -11 -12 -10 391.67 10.72 -11 -12 -11 49.31 3.09 -11 -12 -11 50.74 7.83 -11 -12 -11 51.11 4.86 -11 -12 -11 50.83 3.19 -11 -12 -11 46.15 3.62 -11 -12 -11 50.01 4.11 -11 -12 -12 357.42 10.77 -11 -12 -12 379.81 21.43 -11 -12 -12 363.22 8.33 -11 -12 -12 366.67 8.52 -11 -12 -12 372.56 10.07 -11 -12 -13 82.16 4.79 -11 -12 -13 76.24 3.93 -11 -12 -13 81.26 5.48 -11 -12 -13 79.71 10.03 -11 -12 -13 83.96 4.98 -11 -12 -13 83.23 4.21 -11 -12 -14 0.28 1.00 11 12 14 -3.19 4.15 -11 -12 -14 0.07 2.00 -11 -12 -14 5.89 4.34 -11 -12 -14 -2.15 1.28 -11 -12 -14 -0.62 1.47 -11 -12 -14 1.63 1.63 -11 -12 -15 66.43 3.82 -11 -12 -15 70.63 5.23 -11 -12 -15 66.69 3.89 -11 -12 -15 66.72 9.71 -11 -12 -15 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34.11 2.78 -11 -15 3 54.71 3.19 -11 -15 3 53.37 3.30 -11 -15 2 4.18 1.19 11 15 -2 3.79 2.45 -11 -15 2 1.94 1.22 -11 -15 1 11.16 2.73 11 15 -1 11.45 2.99 -11 -15 1 12.43 1.86 -11 -15 0 43.48 3.18 -11 -15 0 41.50 2.83 -11 -15 0 42.88 6.33 -11 -15 -1 1.64 1.14 -11 -15 -1 2.55 1.23 -11 -15 -1 1.87 2.40 -11 -15 -2 38.62 3.23 -11 -15 -2 34.14 2.63 -11 -15 -2 38.17 5.63 -11 -15 -3 12.60 1.88 -11 -15 -3 10.52 1.61 -11 -15 -3 10.24 1.61 -11 -15 -3 12.63 1.82 -11 -15 -3 9.38 2.64 -11 -15 -4 21.37 2.03 -11 -15 -4 25.78 2.71 -11 -15 -4 21.03 1.96 -11 -15 -4 22.32 2.09 -11 -15 -4 26.83 4.95 -11 -15 -5 283.98 14.12 -11 -15 -5 268.63 6.66 -11 -15 -5 283.81 8.20 -11 -15 -5 285.20 6.91 -11 -15 -5 266.66 6.76 -11 -15 -6 14.49 1.78 -11 -15 -6 17.03 2.37 -11 -15 -6 16.01 5.14 -11 -15 -6 15.17 3.49 -11 -15 -6 11.99 1.55 -11 -15 -6 18.16 1.99 11 15 6 7.96 1.70 -11 -15 -7 30.86 2.44 -11 -15 -7 36.67 6.84 -11 -15 -7 29.19 4.53 -11 -15 -7 34.63 3.28 -11 -15 -7 28.72 2.37 -11 -15 -7 25.57 2.09 -11 -15 -8 107.62 8.66 -11 -15 -8 108.13 4.41 -11 -15 -8 117.78 11.97 -11 -15 -8 110.11 5.33 -11 -15 -8 89.88 4.75 -11 -15 -8 106.63 4.45 -11 -15 -9 3.54 1.50 -11 -15 -9 2.27 1.13 -11 -15 -9 2.23 3.73 -11 -15 -9 -0.45 1.22 -11 -15 -9 2.31 1.50 -11 -15 -9 0.45 1.74 -11 -15 -9 1.22 0.99 -11 -15 -10 61.75 6.32 -11 -15 -10 65.43 3.77 -11 -15 -10 66.93 4.75 -11 -15 -10 76.49 10.07 -11 -15 -10 71.91 3.89 -11 -15 -10 70.88 4.48 -11 -15 -10 67.35 3.86 -11 -15 -11 3.16 1.19 -11 -15 -11 1.75 1.67 -11 -15 -11 3.43 1.82 -11 -15 -11 2.78 1.34 -11 -15 -11 2.82 1.19 -11 -15 -12 41.23 3.05 -11 -15 -12 38.49 3.93 -11 -15 -12 41.95 2.77 -11 -15 -12 38.22 2.86 -11 -15 -12 41.23 7.40 -11 -15 -12 40.11 3.59 -11 -15 -13 42.86 3.13 -11 -15 -13 37.94 3.97 -11 -15 -13 40.11 2.84 -11 -15 -13 43.25 3.10 -11 -15 -13 45.63 8.38 -11 -15 -13 44.22 3.75 -11 -15 -14 7.31 1.48 -11 -15 -14 10.04 1.70 -11 -15 -14 8.17 2.38 -11 -15 -14 6.68 1.35 -11 -15 -15 28.17 2.61 -11 -15 -15 26.48 3.36 -11 -15 -15 27.21 2.24 -11 -15 -15 30.23 2.70 -11 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9.54 1.56 12 -12 -12 12.55 1.33 -12 12 11 30.78 2.87 -12 12 11 26.73 2.52 12 -12 -11 33.47 2.17 -12 12 10 2.66 1.27 -12 12 10 0.27 1.02 12 -12 -10 2.74 0.93 -12 12 9 2.18 1.35 -12 12 9 2.68 1.16 12 -12 -9 3.70 1.07 -12 12 8 2.26 1.54 -12 12 8 0.20 1.21 12 -12 -7 17.78 1.66 -12 12 7 14.95 2.26 -12 12 7 17.46 2.07 12 -12 -6 14.42 1.52 -12 12 6 15.00 2.20 -12 12 6 10.33 1.56 12 -12 -5 53.48 2.65 -12 12 5 54.33 3.97 12 -12 -4 2.07 0.82 -12 12 4 2.62 1.43 12 -12 -3 26.08 1.83 -12 12 3 24.95 2.80 12 -12 -3 27.45 1.83 -12 12 2 39.77 3.43 12 -12 -2 40.43 2.26 -12 12 1 1.94 1.32 12 -12 -1 1.17 0.79 -12 12 0 4.83 1.59 12 -12 0 6.04 1.08 -12 12 -1 7.50 1.77 12 -12 1 9.45 1.29 -12 12 -2 2.30 1.32 12 -12 2 4.02 0.91 -12 12 -3 5.86 1.57 12 -12 3 5.76 1.01 -12 12 -4 2.38 1.29 12 -12 4 1.66 0.72 -12 12 -5 0.36 1.00 12 -12 5 0.17 0.56 -12 12 -6 23.50 2.15 12 -12 6 26.47 1.61 -12 11 16 3.48 1.02 -12 11 16 4.18 1.08 12 -11 -16 3.60 0.75 -12 11 15 1.69 1.13 -12 11 15 0.01 0.88 12 -11 -15 1.03 0.66 -12 11 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45.05 3.88 12 -10 1 68.14 3.44 -12 10 -1 70.46 4.78 12 -10 2 13.18 1.67 -12 10 -2 6.54 2.03 12 -10 3 30.24 2.41 -12 10 -3 30.21 3.12 12 -10 4 6.80 1.27 -12 10 -4 9.19 2.01 12 -10 5 3.76 1.12 -12 10 -5 2.23 1.56 12 -10 6 18.39 1.80 -12 10 -6 14.68 2.31 12 -10 7 26.89 1.99 -12 10 -7 22.12 2.55 12 -10 8 26.62 1.93 -12 10 -8 23.06 2.38 12 -10 9 113.13 3.58 -12 10 -9 99.20 3.85 -12 10 -9 102.56 4.46 -12 10 -10 12.09 1.67 12 -9 -18 4.14 0.77 -12 9 18 2.17 0.82 -12 9 17 2.46 1.13 12 -9 -17 1.53 0.71 -12 9 17 1.52 0.93 -12 9 16 1.64 1.24 12 -9 -16 0.86 0.71 12 -9 -15 17.94 1.73 -12 9 15 12.69 2.06 12 -9 -14 12.32 1.54 -12 9 14 13.13 2.25 12 -9 -13 38.08 2.57 -12 9 13 32.00 3.26 12 -9 -12 28.47 2.39 -12 9 12 26.02 3.03 12 -9 -11 1.52 1.09 -12 9 11 3.02 1.53 12 -9 -10 6.64 1.45 -12 9 10 7.15 2.14 12 -9 -9 83.13 4.09 -12 9 9 78.77 5.22 12 -9 -8 4.79 1.27 -12 9 8 2.39 1.64 12 -9 -7 29.02 2.59 -12 9 7 28.95 3.27 12 -9 -6 23.07 2.29 -12 9 6 19.71 2.92 12 -9 -5 30.71 2.70 -12 9 5 26.25 3.18 12 -9 -5 30.13 2.25 -12 9 4 0.41 1.57 -12 9 4 2.52 1.25 12 -9 -4 3.40 1.23 12 -9 -4 2.54 1.04 -12 9 3 13.76 2.55 12 -9 -3 15.39 1.72 -12 9 3 14.23 2.16 12 -9 -3 18.26 2.12 12 -9 -2 4.50 1.21 -12 9 2 2.45 1.67 12 -9 -2 3.49 1.10 -12 9 1 193.03 7.90 12 -9 -1 202.61 6.07 -12 9 0 17.83 2.60 12 -9 0 15.68 1.90 -12 9 -1 271.09 8.27 12 -9 1 273.66 7.13 -12 9 -1 264.84 9.13 12 -9 2 33.13 2.59 -12 9 -2 33.85 3.54 12 -9 3 170.80 5.66 -12 9 -3 173.14 7.42 12 -9 4 43.09 2.88 -12 9 -4 43.93 3.93 12 -9 5 28.66 2.39 -12 9 -5 27.11 3.10 12 -9 6 5.28 1.18 -12 9 -6 6.00 1.86 12 -9 7 24.82 2.16 -12 9 -7 21.26 2.75 12 -9 8 23.97 2.04 -12 9 -8 19.94 2.56 12 -9 9 2.10 0.86 -12 9 -9 3.24 1.39 -12 9 -9 1.08 1.29 -12 9 -10 53.84 3.21 12 -9 10 64.06 2.78 -12 9 -10 56.18 3.49 12 -9 11 20.68 1.52 -12 9 -11 18.18 1.94 -12 9 -12 148.36 4.66 12 -8 -19 6.50 0.85 -12 8 18 -0.07 0.83 -12 8 18 1.63 0.88 12 -8 -18 2.13 0.80 -12 8 18 0.64 0.87 -12 8 17 2.92 1.32 -12 8 17 1.87 1.03 -12 8 17 3.23 1.23 12 -8 -17 0.83 0.67 -12 8 16 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136.30 6.64 -12 8 -3 10.22 2.35 12 -8 3 5.48 1.36 -12 8 -4 60.37 4.62 12 -8 4 61.50 3.63 -12 8 -5 4.50 1.86 12 -8 5 6.75 1.58 -12 8 -6 104.90 5.83 12 -8 6 99.04 4.41 -12 8 -7 7.98 1.96 12 -8 7 6.04 1.33 -12 8 -8 74.45 4.79 12 -8 8 80.62 3.83 -12 8 -9 24.16 2.91 12 -8 9 30.22 2.35 -12 8 -10 22.21 2.55 -12 8 -10 19.10 2.44 12 -8 10 19.32 1.84 12 -8 11 50.26 2.58 -12 8 -11 45.84 3.33 -12 8 -11 44.17 3.18 12 -8 12 24.88 1.71 -12 8 -12 24.90 2.11 -12 8 -12 23.51 2.30 -12 8 -13 -0.13 0.93 12 -7 -19 0.52 0.61 -12 7 19 2.01 1.11 -12 7 18 0.97 1.01 12 -7 -18 3.42 0.91 -12 7 18 2.04 0.88 -12 7 18 2.70 1.08 -12 7 17 5.26 1.41 -12 7 17 7.90 1.65 -12 7 17 8.06 1.59 12 -7 -17 8.77 1.25 -12 7 16 -3.56 1.65 12 -7 -16 -0.74 0.84 -12 7 16 -3.52 1.60 12 -7 -15 85.87 3.78 -12 7 15 82.70 5.01 -12 7 15 80.18 4.59 -12 7 14 5.08 1.88 -12 7 14 4.51 1.68 12 -7 -14 5.14 1.30 -12 7 13 13.24 2.63 -12 7 13 17.10 2.55 12 -7 -13 12.93 1.67 -12 7 12 4.22 1.80 12 -7 -12 4.93 1.37 -12 7 12 2.55 1.79 -12 7 11 1.66 1.81 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3.16 -12 7 -8 44.91 3.97 12 -7 9 87.18 4.09 -12 7 -9 76.10 4.83 12 -7 10 285.58 7.02 -12 7 -10 269.08 8.87 12 -7 11 -0.31 0.78 -12 7 -11 -1.23 1.33 -12 7 -11 0.11 1.27 -12 7 -12 39.35 3.09 -12 7 -12 33.82 3.03 12 -7 12 38.40 2.30 -12 7 -13 2.85 1.16 -12 7 -13 1.43 1.18 -12 7 -14 9.09 1.46 12 -6 -20 16.10 1.23 -12 6 20 20.35 1.71 12 -6 -19 3.57 0.83 -12 6 19 3.18 0.97 12 -6 -18 0.07 0.67 -12 6 18 0.00 1.03 -12 6 18 -1.40 0.88 -12 6 18 0.64 1.11 12 -6 -17 9.85 1.30 -12 6 17 8.15 1.74 -12 6 17 7.83 1.43 -12 6 17 8.29 1.79 -12 6 16 3.03 1.47 -12 6 16 2.80 1.44 12 -6 -16 3.49 1.06 -12 6 15 59.67 4.06 -12 6 15 51.67 4.20 12 -6 -15 51.83 3.07 -12 6 14 48.54 3.84 -12 6 14 39.32 4.01 12 -6 -14 37.21 2.76 -12 6 13 94.68 5.47 -12 6 13 88.19 5.70 12 -6 -13 85.65 4.21 -12 6 12 107.36 5.70 -12 6 12 96.28 6.10 12 -6 -12 100.30 4.35 -12 6 11 1.97 1.93 -12 6 11 3.56 1.77 12 -6 -11 3.50 1.18 -12 6 10 -0.52 1.69 12 -6 -10 2.24 1.28 -12 6 9 19.65 3.14 -12 6 9 15.86 2.56 12 -6 -9 16.13 1.98 -12 6 8 -1.51 1.76 12 -6 -8 -0.54 1.04 -12 6 8 -0.38 1.54 -12 6 7 129.61 6.72 -12 6 7 137.37 6.61 12 -6 -7 125.43 5.13 -12 6 6 69.59 4.89 12 -6 -6 68.80 7.37 12 -6 -6 78.43 3.99 -12 6 6 69.30 4.86 -12 6 5 6.26 2.04 12 -6 -5 9.06 2.85 12 -6 -5 5.76 1.51 12 -6 -5 4.99 2.60 -12 6 5 5.37 1.72 12 -6 -4 17.20 3.92 12 -6 -4 14.42 1.98 12 -6 -4 6.03 2.76 -12 6 4 12.53 2.45 12 -6 -3 20.50 3.90 12 -6 -3 17.73 2.08 12 -6 -3 15.99 3.63 -12 6 3 16.95 2.70 -12 6 2 -0.11 1.41 12 -6 -2 0.01 1.23 12 -6 -2 1.87 2.78 -12 6 2 2.17 1.48 12 -6 -2 -0.36 2.00 12 -6 -1 69.44 3.95 -12 6 1 55.68 6.82 12 -6 -1 63.91 7.02 -12 6 1 58.81 4.23 12 -6 -1 63.81 3.54 -12 6 1 60.21 4.18 12 -6 0 1.68 1.28 -12 6 0 4.94 1.48 -12 6 0 3.05 2.18 -12 6 0 5.14 1.53 12 -6 0 7.43 1.62 12 -6 0 3.76 2.43 -12 6 -1 28.85 4.93 12 -6 1 29.94 5.10 12 -6 1 21.48 2.27 -12 6 -1 27.32 3.09 -12 6 -2 94.04 5.47 -12 6 -2 89.46 8.48 12 -6 2 90.83 4.39 12 -6 2 104.37 9.45 -12 6 -3 5.32 1.82 -12 6 -3 1.55 1.74 12 -6 3 2.67 1.21 -12 6 -4 157.49 6.76 -12 6 -4 162.29 7.44 12 -6 4 153.13 5.63 -12 6 -5 2.19 1.66 12 -6 5 1.45 1.04 -12 6 -6 18.60 2.91 12 -6 6 19.22 2.35 -12 6 -7 187.12 7.87 12 -6 7 186.67 6.39 -12 6 -8 39.42 3.82 12 -6 8 38.71 2.95 -12 6 -9 125.61 6.42 12 -6 9 138.80 5.27 -12 6 -10 25.38 3.11 12 -6 10 33.80 2.55 -12 6 -11 119.69 6.15 -12 6 -11 126.19 6.17 12 -6 11 131.13 4.82 12 -6 12 11.74 1.50 -12 6 -12 11.95 2.14 -12 6 -12 10.98 2.19 -12 6 -13 16.74 2.33 -12 6 -13 17.43 2.32 12 -6 13 14.77 1.55 -12 6 -14 1.50 1.14 -12 6 -14 -0.97 1.20 -12 6 -15 35.56 2.62 12 -6 15 42.28 2.04 12 -6 16 13.75 1.07 -12 5 20 22.98 1.86 12 -5 -20 24.07 1.50 12 -5 -19 10.18 1.22 -12 5 19 11.98 1.65 12 -5 -18 3.66 0.97 -12 5 18 3.41 1.44 -12 5 18 3.70 1.47 -12 5 17 6.19 1.74 12 -5 -17 7.08 1.23 -12 5 17 3.74 1.14 -12 5 17 8.84 1.70 -12 5 16 13.21 2.57 -12 5 16 13.74 2.31 12 -5 -16 13.96 1.68 -12 5 16 13.05 2.11 -12 5 15 36.59 4.13 -12 5 15 45.96 3.60 12 -5 -15 43.81 2.90 12 -5 -14 184.89 5.80 -12 5 14 194.55 7.40 -12 5 13 23.53 2.95 -12 5 13 20.97 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3.71 -12 -6 0 28.16 4.29 -12 -6 0 25.15 3.75 12 6 1 20.39 3.13 -12 -6 -1 18.91 3.28 -12 -6 -1 19.07 3.72 12 6 2 169.74 8.59 -12 -6 -2 166.52 9.69 -12 -6 -2 158.93 9.54 12 6 3 36.36 4.01 -12 -6 -3 39.78 4.86 -12 -6 -3 38.83 4.71 12 6 4 357.32 12.98 -12 -6 -4 338.80 13.38 12 6 5 420.18 14.06 -12 -6 -5 440.73 15.11 12 6 6 312.42 12.55 -12 -6 -6 268.26 11.69 12 6 7 78.73 6.49 -12 -6 -7 75.55 6.36 12 6 8 19.68 3.78 -12 -6 -8 15.35 3.10 -12 -6 -9 615.70 12.81 -12 -6 -9 639.29 18.56 -12 -6 -10 9.44 1.87 -12 -6 -10 6.41 1.83 -12 -6 -10 7.95 1.89 12 6 10 2.14 2.32 -12 -6 -10 10.95 2.98 -12 -6 -10 9.90 2.21 -12 -6 -11 148.18 6.85 12 6 11 123.02 10.87 -12 -6 -11 145.30 6.71 -12 -6 -11 144.39 5.95 -12 -6 -11 152.18 9.24 -12 -6 -11 151.67 6.85 -12 -6 -12 22.51 3.04 -12 -6 -12 21.99 2.60 12 6 12 14.67 4.05 -12 -6 -12 21.84 3.02 -12 -6 -12 17.97 2.72 -12 -6 -13 129.64 6.66 -12 -6 -13 122.71 6.35 -12 -6 -14 46.87 4.12 -12 -6 -14 46.38 4.05 12 6 14 51.19 8.39 -12 -6 -15 67.53 4.90 -12 -6 -15 65.91 4.95 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-9 151.44 8.84 -12 -7 -9 161.53 6.55 -12 -7 -10 89.67 4.97 -12 -7 -10 90.03 5.22 12 7 10 104.03 9.60 -12 -7 -10 99.83 7.28 -12 -7 -10 89.39 5.15 -12 -7 -10 91.53 4.64 -12 -7 -11 12.15 1.59 -12 -7 -11 12.34 2.25 -12 -7 -11 11.15 2.00 -12 -7 -11 11.03 1.51 12 7 11 7.60 2.92 -12 -7 -11 12.10 2.18 -12 -7 -11 12.94 2.56 -12 -7 -11 10.00 2.33 -12 -7 -12 82.79 5.03 -12 -7 -12 85.59 3.81 -12 -7 -12 87.30 5.73 -12 -7 -12 82.32 5.24 -12 -7 -12 90.69 4.87 -12 -7 -12 90.39 3.92 -12 -7 -13 6.13 1.74 -12 -7 -13 5.39 1.77 -12 -7 -13 6.70 1.91 12 7 13 8.54 3.31 -12 -7 -13 5.03 2.00 12 7 14 124.99 12.18 -12 -7 -14 121.35 6.54 -12 -7 -14 119.33 6.46 12 7 15 55.50 8.92 -12 -7 -15 58.69 4.87 -12 -7 -15 56.98 4.66 -12 -7 -16 37.74 3.95 -12 -7 -16 38.21 3.98 -12 -7 -17 150.66 7.49 -12 -7 -17 157.12 7.37 -12 -7 -18 24.07 3.23 -12 -7 -18 27.88 3.35 -12 -7 -19 19.79 2.91 -12 -7 -19 16.58 2.41 -12 -7 -20 4.50 1.86 -12 -7 -20 1.60 1.43 -12 -7 -21 50.14 3.72 -12 -7 -22 2.94 1.46 -12 -7 -23 1.20 0.93 -12 -7 -24 1.80 0.81 -12 -8 18 77.59 3.11 12 8 -18 92.17 2.96 -12 -8 17 0.78 0.76 -12 -8 17 1.94 1.00 12 8 -17 1.84 0.79 -12 -8 16 -0.46 0.83 -12 -8 16 0.34 0.92 12 8 -16 -0.92 0.87 -12 -8 15 12.67 1.93 -12 -8 15 9.98 2.00 -12 -8 15 10.18 1.51 12 8 -15 10.55 1.52 -12 -8 14 74.91 4.43 -12 -8 14 67.53 3.59 -12 -8 14 65.95 4.53 12 8 -14 69.38 3.57 -12 -8 13 9.85 1.39 -12 -8 13 10.09 2.26 12 8 -13 9.17 1.56 -12 -8 12 61.03 3.45 -12 -8 12 60.96 4.19 12 8 -12 65.80 3.63 -12 -8 11 60.33 3.50 -12 -8 11 55.58 4.03 12 8 -11 60.63 3.55 -12 -8 10 126.39 4.78 -12 -8 10 122.13 5.76 12 8 -9 19.57 4.15 12 8 -9 14.29 1.91 -12 -8 9 19.90 2.52 -12 -8 9 19.53 2.24 12 8 -8 2.02 1.98 -12 -8 8 1.22 1.38 12 8 -8 1.80 1.08 12 8 -8 -0.08 2.33 -12 -8 8 0.77 1.09 -12 -8 7 169.67 6.23 12 8 -7 167.43 10.46 -12 -8 7 160.02 5.35 12 8 -7 170.37 5.75 -12 -8 6 1.94 2.29 12 8 -6 -0.95 1.19 12 8 -6 1.31 1.56 -12 -8 6 -0.82 1.09 12 8 -6 -2.64 1.80 -12 -8 6 1.84 1.20 -12 -8 5 2.94 1.69 12 8 -5 11.53 2.93 -12 -8 5 10.17 1.91 12 8 -5 5.56 2.28 -12 -8 5 8.41 1.42 -12 -8 4 32.19 4.35 -12 -8 4 42.95 3.20 12 8 -4 30.81 4.05 12 8 -4 45.18 5.10 12 8 -3 130.28 8.27 -12 -8 3 121.65 8.43 12 8 -3 112.28 7.63 12 8 -2 101.93 7.12 -12 -8 2 88.69 7.06 12 8 -2 103.94 7.14 12 8 -1 31.61 3.98 12 8 -1 38.17 4.39 -12 -8 1 31.31 4.44 12 8 0 65.93 5.49 -12 -8 0 56.73 5.59 12 8 0 58.74 5.11 -12 -8 0 61.82 6.43 12 8 1 1.21 1.41 -12 -8 -1 3.61 1.95 -12 -8 -1 4.85 2.13 12 8 1 1.67 1.22 12 8 2 715.03 17.24 12 8 2 743.73 17.42 -12 -8 -2 737.29 20.92 -12 -8 -3 59.28 5.74 -12 -8 -3 52.75 5.77 12 8 3 67.46 5.45 -12 -8 -4 69.63 6.21 -12 -8 -4 73.45 6.47 12 8 4 74.56 5.65 -12 -8 -5 13.69 3.27 12 8 5 13.68 2.98 -12 -8 -5 7.38 2.12 -12 -8 -6 160.34 9.05 -12 -8 -6 164.86 9.77 12 8 6 179.90 9.33 12 8 7 254.01 11.30 -12 -8 -7 229.57 10.83 12 8 8 1.40 1.80 -12 -8 -8 -0.01 1.45 -12 -8 -9 7.70 2.35 -12 -8 -9 10.27 2.03 -12 -8 -10 32.76 3.28 -12 -8 -10 33.05 2.97 12 8 10 41.93 6.08 -12 -8 -10 31.46 3.33 -12 -8 -11 53.22 3.02 -12 -8 -11 52.37 4.08 -12 -8 -11 53.12 2.97 12 8 11 56.55 7.35 -12 -8 -11 49.89 3.97 -12 -8 -11 52.34 4.21 -12 -8 -11 50.04 3.66 -12 -8 -12 1.18 1.75 -12 -8 -12 2.05 1.40 -12 -8 -12 0.39 0.93 -12 -8 -12 0.13 1.37 -12 -8 -12 -0.47 0.95 12 8 12 -4.80 4.36 -12 -8 -12 -0.56 1.82 -12 -8 -13 18.88 2.03 -12 -8 -13 20.98 2.15 -12 -8 -13 18.20 2.82 -12 -8 -13 18.48 2.71 -12 -8 -13 21.24 2.75 -12 -8 -13 16.47 3.04 -12 -8 -14 120.76 6.47 -12 -8 -14 120.42 4.69 12 8 14 113.12 11.63 -12 -8 -14 123.11 4.77 -12 -8 -14 120.53 6.70 -12 -8 -14 124.03 6.52 -12 -8 -15 2.28 1.76 -12 -8 -15 4.70 1.92 -12 -8 -15 4.25 1.21 -12 -8 -15 3.72 1.33 12 8 15 3.54 2.89 -12 -8 -16 140.44 7.17 -12 -8 -16 139.20 5.02 -12 -8 -16 137.26 6.96 -12 -8 -16 141.71 5.16 -12 -8 -17 11.09 2.36 -12 -8 -17 15.51 1.74 -12 -8 -17 13.28 1.68 -12 -8 -18 3.42 1.97 -12 -8 -18 3.01 1.99 -12 -8 -19 67.43 4.77 -12 -8 -19 66.09 4.74 -12 -8 -20 3.17 1.83 -12 -8 -20 0.72 1.58 -12 -8 -21 37.26 3.17 -12 -8 -21 38.51 3.07 -12 -8 -22 14.49 2.09 -12 -8 -23 2.32 1.15 -12 -8 -24 0.92 0.77 12 9 -18 13.63 1.10 -12 -9 17 55.16 2.75 12 9 -17 65.28 2.70 -12 -9 16 -0.07 0.80 -12 -9 16 -0.78 1.04 12 9 -16 0.37 0.79 -12 -9 15 27.94 2.78 12 9 -15 27.67 2.15 -12 -9 15 25.44 2.39 -12 -9 15 25.94 1.93 -12 -9 14 33.00 3.17 12 9 -14 33.06 2.48 -12 -9 14 35.05 3.00 -12 -9 14 34.19 2.41 -12 -9 13 6.22 1.79 12 9 -13 5.37 1.21 -12 -9 13 7.90 1.79 -12 -9 13 8.09 1.44 -12 -9 12 79.83 4.70 -12 -9 12 84.00 4.84 -12 -9 12 85.68 3.94 12 9 -12 86.55 4.14 12 9 -11 0.84 1.12 -12 -9 11 0.97 1.32 -12 -9 11 3.21 1.50 -12 -9 10 18.99 2.51 12 9 -10 19.43 2.20 -12 -9 9 33.41 2.88 -12 -9 9 31.17 3.01 12 9 -8 17.35 2.05 12 9 -8 23.07 4.18 -12 -9 8 23.10 2.53 -12 -9 8 25.16 2.43 -12 -9 7 168.57 6.64 -12 -9 7 160.47 5.38 12 9 -7 181.47 11.22 -12 -9 7 171.48 6.18 12 9 -6 100.22 8.26 -12 -9 6 88.95 4.39 -12 -9 6 90.24 4.72 -12 -9 6 75.47 7.01 -12 -9 6 73.71 3.69 -12 -9 5 0.84 0.97 -12 -9 5 -0.34 1.11 12 9 -5 -0.86 1.66 -12 -9 5 -0.38 1.44 -12 -9 5 0.76 1.02 -12 -9 4 232.48 12.37 -12 -9 4 249.64 7.53 12 9 -4 259.85 11.88 12 9 -4 245.20 11.71 -12 -9 4 235.48 5.91 -12 -9 3 132.58 5.36 -12 -9 3 118.86 8.55 12 9 -3 138.92 8.55 12 9 -3 131.83 8.46 -12 -9 2 591.67 18.76 12 9 -2 614.06 17.31 -12 -9 1 88.81 7.31 12 9 -1 97.41 6.96 12 9 0 22.53 3.29 12 9 0 15.33 2.60 -12 -9 0 20.68 3.71 -12 -9 -1 245.98 11.70 -12 -9 -1 253.80 12.69 12 9 1 254.87 10.49 12 9 1 231.95 9.91 -12 -9 -2 94.91 7.30 -12 -9 -2 98.58 7.69 12 9 2 93.91 6.27 12 9 2 108.39 6.70 -12 -9 -3 479.55 16.07 -12 -9 -3 494.51 17.14 12 9 3 519.64 14.68 -12 -9 -4 288.12 12.55 -12 -9 -4 272.44 12.28 12 9 4 280.50 10.58 -12 -9 -5 67.99 6.15 12 9 5 69.26 5.60 -12 -9 -5 74.51 6.37 12 9 5 72.73 5.30 12 9 6 17.55 2.93 -12 -9 -6 20.15 3.48 -12 -9 -6 19.97 3.39 12 9 7 4.84 1.58 -12 -9 -7 13.29 2.96 -12 -9 -7 10.12 2.50 12 9 8 248.53 11.49 -12 -9 -8 214.30 10.27 12 9 9 8.68 2.56 -12 -9 -9 4.84 1.41 -12 -9 -9 6.20 2.00 -12 -9 -9 4.36 1.52 -12 -9 -10 105.33 4.11 -12 -9 -10 111.05 6.00 -12 -9 -10 103.81 5.55 -12 -9 -10 107.96 5.20 -12 -9 -10 110.62 4.24 -12 -9 -11 3.82 1.35 -12 -9 -11 2.81 1.18 -12 -9 -11 2.05 1.53 -12 -9 -11 2.09 1.52 -12 -9 -11 3.45 1.71 -12 -9 -11 4.28 1.11 -12 -9 -12 27.54 2.38 -12 -9 -12 26.57 3.12 -12 -9 -12 26.46 2.27 -12 -9 -12 26.97 3.59 -12 -9 -12 25.47 3.07 12 9 12 31.01 6.15 -12 -9 -12 28.27 2.97 -12 -9 -13 9.96 2.29 12 9 13 15.04 4.76 -12 -9 -13 7.67 1.38 -12 -9 -13 8.53 2.69 -12 -9 -13 8.76 2.36 -12 -9 -13 7.82 1.93 -12 -9 -13 7.28 1.43 -12 -9 -14 139.23 5.26 -12 -9 -14 143.97 6.97 -12 -9 -14 133.66 5.03 -12 -9 -14 131.29 7.24 -12 -9 -14 133.19 6.22 -12 -9 -14 130.87 6.84 12 9 14 130.52 12.29 12 9 15 6.68 4.71 -12 -9 -15 5.11 1.31 -12 -9 -15 7.46 2.09 -12 -9 -15 6.56 1.39 -12 -9 -15 7.04 2.22 -12 -9 -16 173.02 5.80 -12 -9 -16 167.25 5.64 -12 -9 -16 164.13 7.57 -12 -9 -16 169.72 7.86 -12 -9 -17 0.33 0.84 -12 -9 -17 -1.06 1.77 -12 -9 -17 1.66 0.94 -12 -9 -17 -0.63 1.94 -12 -9 -18 38.36 2.77 -12 -9 -18 36.80 3.84 -12 -9 -18 35.61 3.67 -12 -9 -18 43.45 2.85 -12 -9 -19 154.03 5.05 -12 -9 -19 156.72 5.08 -12 -9 -19 154.13 7.20 -12 -9 -19 156.22 7.15 -12 -9 -20 8.96 1.29 -12 -9 -20 6.92 1.82 -12 -9 -20 9.67 1.35 -12 -9 -20 8.40 1.95 -12 -9 -21 64.13 4.22 -12 -9 -21 59.08 4.01 -12 -9 -22 59.07 3.73 -12 -9 -23 0.76 1.09 -12 -9 -24 31.41 2.22 12 10 -17 3.63 0.70 -12 -10 16 3.09 1.11 12 10 -16 4.10 0.96 -12 -10 15 7.97 1.66 -12 -10 15 5.37 1.24 12 10 -15 9.61 1.30 -12 -10 14 41.60 3.27 -12 -10 14 39.42 2.97 12 10 -14 38.79 2.50 -12 -10 13 13.08 2.13 -12 -10 13 13.69 1.96 12 10 -13 13.43 1.77 -12 -10 12 57.55 4.02 12 10 -12 56.45 3.35 -12 -10 12 52.19 3.73 12 10 -11 5.69 1.49 -12 -10 11 6.99 1.77 -12 -10 11 6.70 1.82 12 10 -10 70.82 3.92 -12 -10 10 68.34 4.20 -12 -10 10 70.77 3.96 -12 -10 10 69.11 4.34 -12 -10 9 10.62 1.81 -12 -10 9 14.55 2.32 -12 -10 9 16.22 2.09 12 10 -8 41.71 5.75 -12 -10 8 41.22 2.98 12 10 -8 33.93 2.82 -12 -10 8 44.04 3.43 -12 -10 8 40.28 3.34 -12 -10 7 11.71 2.02 12 10 -7 7.84 3.31 -12 -10 7 10.15 1.96 12 10 -7 7.05 1.24 -12 -10 7 12.92 1.90 12 10 -6 553.55 19.50 -12 -10 6 534.31 11.35 -12 -10 6 538.31 10.61 -12 -10 6 538.39 9.53 -12 -10 6 538.47 18.77 12 10 -5 12.14 3.36 -12 -10 5 9.76 1.98 -12 -10 5 13.67 2.00 -12 -10 5 13.85 1.73 -12 -10 5 11.44 3.03 -12 -10 4 224.53 7.27 -12 -10 4 215.85 5.90 -12 -10 4 208.37 11.78 12 10 -4 222.35 11.76 -12 -10 3 327.62 8.45 -12 -10 3 325.04 6.94 12 10 -3 316.55 13.22 -12 -10 3 306.74 13.96 -12 -10 2 47.48 5.49 12 10 -2 43.95 4.88 -12 -10 2 45.83 3.10 -12 -10 1 65.58 6.28 -12 -10 1 74.34 3.92 12 10 -1 68.37 5.91 -12 -10 0 7.18 2.79 12 10 0 0.10 1.01 -12 -10 -1 68.97 6.42 12 10 1 77.36 6.17 -12 -10 -2 24.47 3.89 12 10 2 20.49 3.02 -12 -10 -3 3.60 2.11 -12 -10 -3 5.26 2.33 12 10 3 4.07 1.82 -12 -10 -4 77.75 6.67 12 10 4 75.60 5.69 -12 -10 -4 75.08 6.59 -12 -10 -5 48.68 5.43 12 10 5 61.44 5.01 -12 -10 -5 52.20 5.33 -12 -10 -6 40.64 4.90 -12 -10 -6 45.23 4.75 12 10 6 46.61 4.35 -12 -10 -7 3.50 1.98 -12 -10 -7 4.83 2.13 -12 -10 -8 7.38 2.49 -12 -10 -8 5.55 1.44 -12 -10 -8 9.45 2.33 -12 -10 -9 10.42 1.44 -12 -10 -9 10.64 2.30 -12 -10 -9 8.43 1.84 -12 -10 -9 9.21 1.50 -12 -10 -9 10.01 1.84 -12 -10 -10 1.11 0.86 -12 -10 -10 1.24 1.47 -12 -10 -10 2.17 1.50 -12 -10 -10 1.61 1.61 -12 -10 -10 1.90 1.00 -12 -10 -11 175.74 5.64 -12 -10 -11 175.60 6.85 -12 -10 -11 171.87 7.41 -12 -10 -11 174.12 5.52 -12 -10 -11 184.09 8.11 -12 -10 -11 184.13 6.94 -12 -10 -12 43.50 2.95 -12 -10 -12 43.25 2.90 -12 -10 -12 42.15 4.25 -12 -10 -12 43.63 3.86 -12 -10 -12 43.45 3.60 -12 -10 -12 44.74 3.73 -12 -10 -13 0.07 1.65 -12 -10 -13 2.55 1.83 -12 -10 -13 0.94 0.92 -12 -10 -13 0.17 0.88 -12 -10 -13 0.59 1.40 -12 -10 -13 2.90 1.78 12 10 14 9.70 4.43 -12 -10 -14 12.85 2.64 -12 -10 -14 13.02 1.80 -12 -10 -14 12.50 1.84 -12 -10 -14 10.49 2.13 -12 -10 -14 12.70 2.47 12 10 15 5.74 4.35 -12 -10 -15 7.42 1.39 -12 -10 -15 8.73 1.55 -12 -10 -15 8.46 2.24 -12 -10 -15 7.40 1.97 -12 -10 -16 14.16 1.83 -12 -10 -16 13.17 1.75 -12 -10 -16 12.52 2.43 -12 -10 -16 12.95 2.77 -12 -10 -17 70.15 3.87 -12 -10 -17 68.04 3.74 -12 -10 -17 68.82 5.11 -12 -10 -17 66.91 4.84 -12 -10 -18 9.34 1.54 -12 -10 -18 5.86 1.25 -12 -10 -18 10.69 2.60 -12 -10 -18 7.41 2.16 -12 -10 -19 1.38 0.90 -12 -10 -19 1.55 0.76 -12 -10 -19 3.52 2.04 -12 -10 -19 1.39 1.53 -12 -10 -20 73.58 3.54 -12 -10 -20 64.41 4.79 -12 -10 -20 73.78 3.49 -12 -10 -20 70.36 4.73 -12 -10 -21 22.65 1.93 -12 -10 -21 22.19 2.58 -12 -10 -21 22.75 1.87 -12 -10 -21 22.56 2.71 -12 -10 -22 3.63 1.35 -12 -10 -23 14.53 1.81 -12 -10 -24 24.88 2.01 12 11 -16 27.14 1.67 12 11 -15 1.85 0.86 -12 -11 15 -0.58 1.05 12 11 -14 48.59 2.60 -12 -11 14 46.94 3.26 -12 -11 14 41.51 2.76 12 11 -13 8.57 1.43 -12 -11 13 7.54 1.58 -12 -11 13 8.50 1.56 12 11 -12 98.70 4.22 -12 -11 12 94.94 4.92 -12 -11 12 92.77 4.71 -12 -11 11 4.34 1.41 -12 -11 11 2.86 1.36 12 11 -11 1.56 1.20 -12 -11 10 75.42 4.10 -12 -11 10 72.60 4.31 12 11 -10 77.89 3.98 -12 -11 10 70.69 4.30 -12 -11 9 0.53 1.27 12 11 -9 -0.15 1.27 -12 -11 9 1.03 1.25 -12 -11 9 1.18 1.27 12 11 -8 1.88 1.31 -12 -11 8 0.95 1.46 -12 -11 8 2.56 1.25 -12 -11 8 1.12 1.18 -12 -11 7 106.41 5.34 -12 -11 7 109.32 4.63 12 11 -7 110.85 9.18 -12 -11 7 108.61 5.08 12 11 -7 118.94 5.06 -12 -11 6 90.99 4.41 -12 -11 6 102.52 4.38 -12 -11 6 97.18 8.84 12 11 -6 87.70 8.13 -12 -11 6 88.74 4.72 -12 -11 5 38.37 2.69 -12 -11 5 37.58 3.22 -12 -11 5 34.17 5.30 -12 -11 5 38.75 2.99 12 11 -5 37.96 5.14 -12 -11 4 23.06 2.51 12 11 -4 20.45 3.80 -12 -11 4 26.87 2.21 -12 -11 4 26.62 4.69 -12 -11 3 36.51 5.06 -12 -11 3 34.42 2.92 12 11 -3 32.50 4.60 -12 -11 3 34.18 2.50 12 11 -2 10.13 2.67 -12 -11 2 12.19 1.90 -12 -11 2 13.81 1.70 -12 -11 2 15.77 3.59 -12 -11 1 145.32 5.60 -12 -11 1 132.76 9.31 12 11 -1 134.13 8.43 -12 -11 1 134.42 4.47 -12 -11 0 2.87 1.85 -12 -11 0 2.49 1.29 12 11 0 1.23 1.25 -12 -11 -1 43.17 5.22 -12 -11 -1 42.03 2.62 12 11 1 42.06 4.56 -12 -11 -1 39.12 2.55 -12 -11 -1 44.34 3.02 12 11 2 3.08 1.22 -12 -11 -2 3.43 1.36 12 11 3 27.38 3.52 -12 -11 -3 22.38 3.91 -12 -11 -4 277.42 12.74 12 11 4 293.47 11.35 -12 -11 -5 182.75 10.45 12 11 5 199.94 9.12 -12 -11 -6 12.46 2.95 -12 -11 -7 112.78 4.17 -12 -11 -7 123.96 5.20 -12 -11 -7 111.62 4.18 -12 -11 -7 113.67 5.70 -12 -11 -7 111.58 8.17 -12 -11 -8 108.62 5.88 -12 -11 -8 108.93 5.40 -12 -11 -8 106.80 8.16 -12 -11 -8 106.05 5.03 -12 -11 -8 103.28 4.13 -12 -11 -8 108.40 4.27 -12 -11 -9 21.03 2.03 -12 -11 -9 19.68 2.29 -12 -11 -9 21.07 5.81 -12 -11 -9 16.48 3.16 -12 -11 -9 19.15 1.89 -12 -11 -9 19.97 2.71 -12 -11 -9 18.05 2.77 -12 -11 -10 89.70 4.01 -12 -11 -10 90.98 5.31 -12 -11 -10 96.43 11.19 -12 -11 -10 92.76 4.09 -12 -11 -10 90.24 4.92 -12 -11 -10 88.68 5.70 -12 -11 -11 84.77 3.96 -12 -11 -11 92.77 5.46 -12 -11 -11 88.52 10.31 -12 -11 -11 84.19 3.98 -12 -11 -11 86.06 4.80 -12 -11 -11 87.79 5.92 -12 -11 -12 17.29 2.52 -12 -11 -12 17.37 2.71 -12 -11 -12 15.61 1.84 -12 -11 -12 17.35 5.23 -12 -11 -12 16.18 1.91 -12 -11 -12 13.81 2.99 -12 -11 -12 18.40 2.66 -12 -11 -13 5.58 2.50 -12 -11 -13 0.92 1.14 -12 -11 -13 -1.17 1.73 -12 -11 -13 -0.36 1.63 -12 -11 -13 1.33 1.64 -12 -11 -13 7.28 4.54 -12 -11 -13 -0.40 1.07 -12 -11 -14 227.36 6.82 -12 -11 -14 226.08 8.95 -12 -11 -14 226.35 8.31 -12 -11 -14 226.28 8.07 -12 -11 -14 223.72 6.67 -12 -11 -15 0.74 1.00 -12 -11 -15 0.70 1.58 -12 -11 -15 -0.80 1.79 -12 -11 -15 1.95 1.35 -12 -11 -16 9.14 1.69 -12 -11 -16 8.55 2.27 -12 -11 -16 7.92 1.63 -12 -11 -16 6.93 2.06 -12 -11 -17 26.77 2.44 -12 -11 -17 27.94 3.56 -12 -11 -17 26.47 2.48 -12 -11 -17 34.24 3.56 -12 -11 -18 94.14 4.38 -12 -11 -18 88.61 5.79 -12 -11 -18 92.08 4.28 -12 -11 -18 89.04 5.38 -12 -11 -19 26.52 2.35 -12 -11 -19 24.41 2.95 -12 -11 -19 25.06 3.28 -12 -11 -19 25.43 2.27 -12 -11 -20 -0.41 0.87 -12 -11 -20 0.57 1.30 -12 -11 -20 -0.51 1.68 -12 -11 -20 0.56 0.79 -12 -11 -21 -0.03 0.68 -12 -11 -21 1.52 1.32 -12 -11 -21 2.37 1.47 -12 -11 -21 0.88 0.69 -12 -11 -22 2.34 1.26 -12 -11 -22 2.98 0.75 -12 -11 -22 1.87 0.79 -12 -11 -23 37.88 1.91 -12 -11 -23 36.65 2.70 -12 -11 -23 38.80 1.89 -12 -11 -24 1.88 0.90 12 12 -16 20.31 1.33 12 12 -15 165.49 4.07 -12 -12 15 165.51 5.38 12 12 -14 5.52 1.04 -12 -12 14 2.65 1.23 12 12 -13 127.98 4.26 -12 -12 13 135.10 5.32 -12 -12 12 10.73 1.74 -12 -12 12 13.14 1.82 12 12 -12 15.01 1.76 -12 -12 11 174.98 6.23 12 12 -11 176.28 5.62 -12 -12 11 173.28 6.37 -12 -12 10 43.03 3.37 -12 -12 10 51.46 3.43 12 12 -10 48.46 3.11 -12 -12 10 44.27 3.34 -12 -12 9 52.97 3.59 -12 -12 9 51.18 3.54 -12 -12 9 48.36 3.36 12 12 -9 53.53 3.39 -12 -12 8 3.04 1.35 -12 -12 8 1.18 1.17 12 12 -8 1.86 1.14 -12 -12 8 3.02 1.40 -12 -12 7 3.24 1.39 12 12 -7 5.36 1.69 -12 -12 7 5.04 1.47 -12 -12 7 7.51 1.62 -12 -12 6 2.15 2.99 -12 -12 6 4.57 1.47 12 12 -6 6.24 2.76 -12 -12 6 4.24 1.25 -12 -12 6 6.08 1.64 -12 -12 5 4.35 2.93 -12 -12 5 6.80 1.65 12 12 -5 7.12 2.46 -12 -12 5 6.80 1.66 -12 -12 5 6.90 1.47 12 12 -4 42.88 5.57 -12 -12 4 46.30 3.50 -12 -12 4 43.58 5.76 -12 -12 4 49.01 3.16 -12 -12 4 45.83 2.95 -12 -12 3 1.28 1.10 -12 -12 3 2.21 2.35 -12 -12 3 2.70 1.12 12 12 -3 0.85 1.39 -12 -12 2 182.99 11.32 12 12 -2 194.45 10.98 -12 -12 2 187.97 6.60 -12 -12 2 192.57 5.62 -12 -12 1 85.88 7.83 -12 -12 1 95.75 4.04 12 12 -1 102.17 7.76 -12 -12 1 97.54 4.75 -12 -12 0 2.53 0.89 -12 -12 0 2.20 2.08 12 12 0 4.19 1.97 -12 -12 0 3.75 1.23 12 12 1 337.78 13.29 -12 -12 -1 347.69 7.41 -12 -12 -1 362.40 7.23 -12 -12 -1 346.95 15.13 -12 -12 -1 354.24 8.73 -12 -12 -1 344.47 7.26 12 12 2 137.94 8.21 -12 -12 -2 134.11 9.18 -12 -12 -2 136.53 4.55 -12 -12 -2 130.50 4.40 -12 -12 -2 135.16 4.48 -12 -12 -2 145.88 5.69 12 12 3 0.55 1.30 -12 -12 -3 1.49 0.94 -12 -12 -3 0.74 0.76 -12 -12 -3 1.06 1.16 -12 -12 -3 3.08 2.30 -12 -12 -4 8.60 2.17 -12 -12 -4 11.57 3.15 12 12 4 7.70 2.15 -12 -12 -4 9.35 1.40 -12 -12 -4 8.13 1.40 -12 -12 -4 10.36 1.43 -12 -12 -5 556.11 18.49 -12 -12 -5 551.72 12.98 -12 -12 -5 574.25 11.30 -12 -12 -5 537.73 8.93 -12 -12 -5 543.71 9.08 -12 -12 -6 50.98 5.71 -12 -12 -6 60.53 4.55 -12 -12 -6 61.64 3.18 -12 -12 -6 67.64 4.05 -12 -12 -6 57.81 3.14 -12 -12 -7 283.78 13.14 -12 -12 -7 287.13 6.95 -12 -12 -7 314.07 9.97 -12 -12 -7 311.06 8.53 -12 -12 -7 290.45 6.87 -12 -12 -8 82.66 4.54 -12 -12 -8 74.11 3.56 -12 -12 -8 82.48 10.17 -12 -12 -8 80.84 7.06 -12 -12 -8 78.50 3.79 -12 -12 -8 80.71 4.74 -12 -12 -8 80.87 5.38 -12 -12 -9 319.35 10.67 -12 -12 -9 292.27 9.37 -12 -12 -9 321.27 20.00 -12 -12 -9 319.27 14.39 -12 -12 -9 321.92 7.58 -12 -12 -9 308.28 8.95 -12 -12 -9 322.86 7.89 -12 -12 -10 1.18 1.82 -12 -12 -10 -0.57 2.10 -12 -12 -10 0.52 3.33 -12 -12 -10 1.63 1.00 -12 -12 -10 0.57 1.40 -12 -12 -10 1.62 0.84 -12 -12 -11 50.48 3.22 -12 -12 -11 47.55 4.16 -12 -12 -11 56.97 8.82 -12 -12 -11 47.48 4.56 -12 -12 -11 53.51 3.95 -12 -12 -11 50.56 3.21 -12 -12 -12 11.59 2.35 -12 -12 -12 12.06 2.58 -12 -12 -12 16.40 2.52 -12 -12 -12 17.65 4.63 -12 -12 -12 12.45 1.68 -12 -12 -12 12.21 1.59 -12 -12 -13 1.50 0.98 -12 -12 -13 0.81 1.76 -12 -12 -13 1.02 0.89 -12 -12 -13 -0.02 1.64 -12 -12 -13 0.61 1.30 -12 -12 -14 145.59 6.58 -12 -12 -14 150.05 5.69 -12 -12 -14 139.31 7.00 -12 -12 -14 145.79 5.44 -12 -12 -14 154.72 14.67 -12 -12 -14 144.48 6.57 -12 -12 -15 22.38 2.33 -12 -12 -15 24.13 2.33 -12 -12 -15 18.56 3.01 -12 -12 -15 20.52 2.99 -12 -12 -16 92.90 4.49 -12 -12 -16 86.63 5.17 -12 -12 -16 94.48 4.46 -12 -12 -16 94.11 6.07 -12 -12 -17 5.03 1.43 -12 -12 -17 1.01 1.85 -12 -12 -17 3.38 1.27 -12 -12 -17 1.67 1.52 -12 -12 -18 182.44 6.25 -12 -12 -18 176.46 7.20 -12 -12 -18 170.84 5.94 -12 -12 -18 173.82 8.14 -12 -12 -19 15.08 1.81 -12 -12 -19 12.95 2.26 -12 -12 -19 14.58 2.87 -12 -12 -19 13.84 1.84 -12 -12 -20 12.98 1.89 -12 -12 -20 7.54 1.86 -12 -12 -20 10.20 2.35 -12 -12 -20 14.35 2.07 -12 -12 -21 -0.39 0.81 -12 -12 -21 -0.34 1.31 -12 -12 -21 0.57 1.39 -12 -12 -21 0.96 0.85 -12 -12 -22 1.82 0.82 -12 -12 -22 1.83 0.77 -12 -12 -22 1.88 1.26 -12 -12 -23 1.66 0.63 -12 -12 -23 2.06 0.69 -12 -12 -23 0.21 0.94 -12 -12 -24 34.96 2.25 -12 -13 15 15.00 1.61 12 13 -15 16.36 1.22 -12 -13 14 98.04 4.13 12 13 -14 101.07 3.21 -12 -13 13 69.87 3.65 12 13 -13 78.07 3.20 -12 -13 12 69.76 3.86 12 13 -12 72.59 3.29 -12 -13 11 121.36 5.15 12 13 -11 127.46 4.55 -12 -13 10 4.31 1.27 -12 -13 10 2.90 1.19 -12 -13 10 3.34 1.30 12 13 -10 3.53 1.16 -12 -13 9 85.02 4.38 -12 -13 9 72.52 4.17 12 13 -9 80.28 4.03 -12 -13 9 83.20 4.14 -12 -13 8 15.66 2.04 12 13 -8 16.94 2.21 -12 -13 8 13.16 1.96 -12 -13 8 12.66 1.93 -12 -13 7 2.52 1.24 -12 -13 7 4.24 1.42 -12 -13 7 4.52 1.41 -12 -13 6 81.99 4.01 -12 -13 6 88.08 4.77 -12 -13 6 93.69 4.59 -12 -13 5 26.03 2.44 -12 -13 5 23.63 2.43 -12 -13 5 25.77 2.75 -12 -13 4 14.11 2.12 -12 -13 4 11.80 1.80 12 13 -4 11.52 2.95 -12 -13 4 12.75 1.71 -12 -13 4 14.45 4.13 -12 -13 3 201.01 12.45 -12 -13 3 212.43 7.10 12 13 -3 209.41 12.05 -12 -13 3 205.06 5.97 12 13 -2 17.50 3.40 -12 -13 2 17.30 4.19 -12 -13 2 16.19 1.85 -12 -13 2 16.79 2.33 12 13 -1 -0.51 1.57 -12 -13 1 2.60 2.16 -12 -13 1 1.58 1.11 -12 -13 1 0.97 1.19 -12 -13 0 47.78 5.80 12 13 0 49.18 5.52 -12 -13 0 45.16 2.86 -12 -13 0 45.82 3.41 -12 -13 -1 76.83 7.39 12 13 1 77.76 6.57 -12 -13 -1 77.45 3.60 -12 -13 -1 74.92 4.16 -12 -13 -2 5.39 1.96 -12 -13 -2 9.12 1.43 -12 -13 -2 8.12 1.65 12 13 2 7.87 2.56 -12 -13 -2 6.96 1.30 -12 -13 -2 5.57 1.32 -12 -13 -2 8.88 2.70 12 13 3 200.44 10.13 -12 -13 -3 185.62 5.36 -12 -13 -3 195.39 6.67 -12 -13 -3 191.10 7.77 -12 -13 -3 187.09 5.35 -12 -13 -3 184.46 5.44 -12 -13 -3 181.48 10.90 -12 -13 -4 15.68 3.51 -12 -13 -4 17.07 1.86 -12 -13 -4 19.00 2.86 -12 -13 -4 17.13 1.78 -12 -13 -4 16.18 2.22 -12 -13 -4 13.74 1.56 -12 -13 -5 63.97 3.91 -12 -13 -5 62.29 3.26 -12 -13 -5 67.32 4.73 -12 -13 -5 65.47 3.22 -12 -13 -5 63.67 6.39 -12 -13 -5 58.02 3.16 -12 -13 -6 19.39 1.96 -12 -13 -6 18.92 2.30 -12 -13 -6 23.11 3.14 -12 -13 -6 16.91 3.65 -12 -13 -6 15.14 1.70 -12 -13 -6 18.18 1.89 -12 -13 -7 3.25 1.08 -12 -13 -7 3.16 1.08 -12 -13 -7 1.46 1.64 -12 -13 -7 2.23 1.67 -12 -13 -7 2.04 1.23 -12 -13 -7 4.95 1.95 -12 -13 -7 4.31 1.04 -12 -13 -8 17.16 1.89 -12 -13 -8 13.59 2.72 -12 -13 -8 14.95 4.83 -12 -13 -8 15.85 3.35 -12 -13 -8 19.58 1.78 -12 -13 -8 16.02 2.48 -12 -13 -8 14.12 1.66 -12 -13 -8 14.34 2.14 -12 -13 -9 206.50 6.33 -12 -13 -9 214.26 8.86 -12 -13 -9 210.70 16.25 -12 -13 -9 188.00 10.94 -12 -13 -9 209.03 7.35 -12 -13 -9 202.26 6.13 -12 -13 -9 203.38 7.78 -12 -13 -10 18.31 2.44 -12 -13 -10 21.33 2.18 -12 -13 -10 23.06 6.11 -12 -13 -10 16.02 3.24 -12 -13 -10 21.02 3.58 -12 -13 -10 17.52 2.63 -12 -13 -10 17.65 1.94 -12 -13 -11 208.10 6.34 -12 -13 -11 200.01 8.09 -12 -13 -11 201.22 16.29 -12 -13 -11 199.03 9.03 -12 -13 -11 208.10 7.69 -12 -13 -11 209.82 6.47 -12 -13 -12 6.34 2.32 -12 -13 -12 5.64 1.98 -12 -13 -12 6.23 4.32 -12 -13 -12 6.08 1.48 -12 -13 -12 6.25 1.51 -12 -13 -13 101.68 4.63 -12 -13 -13 104.95 6.14 -12 -13 -13 101.90 4.55 -12 -13 -13 112.95 12.57 -12 -13 -13 104.63 5.60 -12 -13 -14 74.44 4.60 -12 -13 -14 72.73 3.96 -12 -13 -14 71.03 5.20 -12 -13 -14 75.66 3.98 -12 -13 -14 74.59 10.78 -12 -13 -14 73.30 4.88 -12 -13 -15 21.40 2.19 -12 -13 -15 20.17 2.70 -12 -13 -15 22.54 3.24 -12 -13 -15 20.25 2.13 -12 -13 -16 7.75 1.48 -12 -13 -16 9.62 2.50 -12 -13 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11 50.06 4.04 13 6 -10 5.50 1.39 -13 -6 10 6.59 1.58 -13 -6 10 8.57 2.31 13 6 -9 40.18 5.48 -13 -6 9 34.17 2.97 13 6 -9 24.00 4.97 -13 -6 9 36.50 3.73 13 6 -8 77.09 7.06 13 6 -8 89.84 8.14 -13 -6 8 79.96 4.15 13 6 -8 64.40 3.48 -13 -6 8 80.66 4.77 13 6 -7 6.31 3.17 13 6 -7 3.80 1.88 -13 -6 7 3.70 1.47 13 6 -7 7.17 1.66 -13 -6 7 5.21 1.57 13 6 -6 118.18 8.35 13 6 -6 118.26 8.98 -13 -6 6 121.52 5.49 -13 -6 6 116.46 4.71 -13 -6 6 121.47 4.35 13 6 -5 342.52 14.65 -13 -6 5 356.83 8.87 13 6 -5 357.50 14.42 -13 -6 4 19.61 2.21 -13 -6 4 30.78 4.75 13 6 -4 25.34 4.07 13 6 -4 21.99 3.65 -13 -6 4 26.81 2.56 13 6 -3 116.90 8.12 -13 -6 3 118.60 5.07 -13 -6 3 123.48 10.04 13 6 -3 118.26 7.76 13 6 -2 2.58 1.80 -13 -6 2 0.36 1.77 13 6 -2 1.17 1.34 -13 -6 2 1.80 1.96 13 6 -1 69.15 6.10 -13 -6 1 63.93 6.59 -13 -6 1 67.57 7.17 13 6 -1 60.02 5.47 -13 -6 0 115.64 8.41 -13 -6 0 119.95 9.44 13 6 0 121.61 7.85 -13 -6 -1 9.05 3.00 13 6 1 5.70 2.19 -13 -6 -2 20.13 4.07 13 6 2 15.88 3.24 -13 -6 -3 898.28 23.57 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3.68 13 7 -6 76.13 6.90 -13 -7 5 1.97 1.93 -13 -7 5 1.12 0.98 -13 -7 5 1.59 1.01 13 7 -5 -0.29 1.47 13 7 -4 118.98 8.35 -13 -7 4 111.13 5.15 -13 -7 4 116.52 4.99 13 7 -4 107.68 8.10 -13 -7 3 35.03 4.65 13 7 -3 42.95 4.96 -13 -7 3 45.04 3.18 -13 -7 2 124.38 8.74 13 7 -2 127.79 8.40 13 7 -2 132.76 8.18 -13 -7 2 130.28 10.20 -13 -7 1 9.93 3.34 13 7 -1 7.22 2.04 13 7 -1 6.78 2.38 -13 -7 1 4.43 1.94 -13 -7 0 6.89 2.83 13 7 0 6.23 2.08 13 7 0 6.47 2.12 -13 -7 0 3.48 2.08 13 7 1 205.47 10.03 -13 -7 -1 198.18 11.68 -13 -7 -1 197.10 11.06 -13 -7 -2 13.81 3.00 13 7 2 17.92 3.29 -13 -7 -2 18.72 3.68 -13 -7 -3 20.05 3.75 13 7 3 16.48 3.04 -13 -7 -3 10.33 3.02 13 7 4 119.32 7.63 -13 -7 -4 116.07 8.41 13 7 5 88.51 7.10 -13 -7 -5 69.18 6.46 13 7 6 455.27 15.76 -13 -7 -6 449.90 16.54 -13 -7 -7 2.82 2.09 13 7 7 3.75 1.95 -13 -7 -7 5.57 1.75 13 7 8 289.60 13.33 -13 -7 -8 268.21 12.40 -13 -7 -8 284.71 8.86 -13 -7 -8 292.80 8.93 -13 -7 -8 279.01 7.84 -13 -7 -9 14.77 2.13 13 7 9 19.64 3.92 -13 -7 -9 19.51 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9 -15 58.83 2.91 -13 -9 14 36.55 2.99 13 9 -14 41.30 2.60 -13 -9 14 37.71 3.29 -13 -9 13 128.81 5.73 13 9 -13 130.04 4.74 -13 -9 13 125.18 5.94 -13 -9 12 7.62 1.74 13 9 -12 8.98 1.51 -13 -9 12 11.88 2.11 -13 -9 11 44.05 3.70 13 9 -11 42.55 2.92 -13 -9 11 42.73 3.50 13 9 -10 21.65 2.17 -13 -9 10 23.03 2.79 -13 -9 10 21.81 2.71 -13 -9 9 59.90 4.12 -13 -9 9 61.96 3.59 -13 -9 9 54.29 3.98 -13 -9 8 74.60 4.48 13 9 -8 65.67 3.66 -13 -9 8 72.57 4.64 -13 -9 8 66.92 3.76 -13 -9 7 17.87 2.24 13 9 -7 23.96 4.46 -13 -9 7 21.84 2.64 13 9 -7 17.52 2.24 -13 -9 7 21.27 2.60 13 9 -6 154.81 10.37 -13 -9 6 158.63 5.24 -13 -9 6 163.37 6.05 -13 -9 6 148.53 6.26 13 9 -5 162.07 10.11 -13 -9 5 146.41 10.09 -13 -9 5 134.29 4.67 -13 -9 5 155.33 6.24 -13 -9 4 41.50 3.35 -13 -9 4 33.20 2.47 13 9 -4 40.43 5.00 13 9 -3 190.86 10.31 -13 -9 3 200.73 6.76 -13 -9 3 198.19 11.42 -13 -9 3 196.91 5.23 13 9 -3 207.80 10.91 -13 -9 2 43.64 3.24 -13 -9 2 35.47 4.97 13 9 -2 43.01 4.84 13 9 -2 40.02 4.83 -13 -9 1 245.34 7.22 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87.67 4.04 -13 -11 -18 83.36 5.48 -13 -11 -18 80.53 5.05 -13 -11 -19 14.10 1.65 -13 -11 -19 15.59 1.80 -13 -11 -19 14.59 2.70 -13 -11 -19 17.36 2.53 -13 -11 -20 3.03 0.94 -13 -11 -20 2.43 0.85 -13 -11 -20 2.35 1.54 -13 -11 -20 1.32 1.42 -13 -11 -21 1.41 0.73 -13 -11 -21 2.81 0.91 -13 -11 -21 2.16 1.28 -13 -11 -21 2.69 1.42 -13 -11 -22 23.00 2.33 -13 -11 -23 1.66 1.04 -13 -11 -24 16.61 1.55 13 12 -15 4.97 0.83 -13 -12 14 119.75 4.78 13 12 -14 124.39 3.69 -13 -12 13 1.79 0.96 -13 -12 13 1.56 1.05 -13 -12 12 62.51 3.63 -13 -12 12 66.56 3.84 13 12 -12 66.12 3.16 -13 -12 11 2.35 1.27 -13 -12 11 2.73 1.21 13 12 -11 2.06 1.05 -13 -12 10 62.73 3.87 -13 -12 10 63.42 3.92 13 12 -10 68.74 3.47 -13 -12 9 27.90 2.92 -13 -12 9 24.60 2.45 -13 -12 9 28.27 2.83 13 12 -9 33.53 2.71 -13 -12 8 37.68 3.19 -13 -12 8 37.38 2.89 -13 -12 8 39.87 3.31 13 12 -8 28.10 2.47 -13 -12 7 60.58 3.88 -13 -12 7 58.71 4.03 -13 -12 7 60.35 3.55 -13 -12 6 25.60 2.64 -13 -12 6 24.70 2.86 -13 -12 6 27.43 2.47 13 12 -5 247.26 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4.64 2.47 -15 -3 -7 49.16 3.79 -15 -3 -7 46.86 3.94 15 3 7 56.12 6.65 -15 -3 -7 42.17 6.07 -15 -3 -8 9.64 2.06 -15 -3 -8 11.86 2.35 15 3 8 13.66 3.88 -15 -3 -8 12.65 3.65 -15 -3 -9 67.51 4.83 15 3 9 76.08 8.47 -15 -3 -9 61.26 7.18 15 3 10 55.35 3.56 -15 -3 -10 41.24 3.90 -15 -3 -11 2.26 1.79 -15 -3 -12 30.23 3.28 -15 -3 -12 35.66 3.86 -15 -3 -13 68.95 5.06 -15 -3 -13 69.42 4.98 -15 -3 -14 32.53 3.63 -15 -3 -14 28.19 3.15 -15 -3 -15 31.44 3.54 -15 -3 -15 26.54 2.96 -15 -3 -16 12.68 2.33 -15 -3 -16 13.87 2.11 -15 -3 -17 24.44 2.90 15 3 18 1.68 0.64 -15 -3 -18 0.88 1.25 -15 -3 -19 30.85 2.71 -15 -3 -20 3.39 1.17 15 4 -18 2.14 0.57 -15 -4 18 3.40 0.85 -15 -4 18 2.01 0.84 15 4 -17 10.61 1.20 -15 -4 17 11.38 1.46 -15 -4 17 12.00 1.60 15 4 -16 2.85 0.95 -15 -4 16 1.53 0.98 -15 -4 16 1.26 0.89 15 4 -15 7.94 1.37 -15 -4 15 9.85 1.69 -15 -4 15 8.24 1.63 15 4 -14 5.68 1.25 -15 -4 14 4.19 1.31 -15 -4 14 4.22 1.32 15 4 -13 28.16 2.38 -15 -4 13 25.28 2.68 -15 -4 13 23.14 2.69 15 4 -12 2.18 1.04 -15 -4 12 2.69 1.57 -15 -4 12 2.27 1.39 -15 -4 11 50.44 3.73 15 4 -11 54.52 3.34 15 4 -10 0.37 1.12 -15 -4 10 3.78 1.64 -15 -4 9 85.83 4.70 -15 -4 9 86.03 5.12 -15 -4 9 81.27 4.77 15 4 -8 18.71 2.08 -15 -4 8 18.84 2.44 -15 -4 8 20.60 2.64 -15 -4 8 20.51 2.68 -15 -4 7 4.21 1.63 -15 -4 7 -0.32 1.36 15 4 -7 1.58 1.04 -15 -4 7 -0.20 1.33 15 4 -7 -0.09 1.67 15 4 -7 -1.12 1.97 15 4 -6 43.17 5.47 -15 -4 6 47.12 3.70 -15 -4 6 49.45 3.97 -15 -4 6 49.80 3.50 15 4 -6 49.79 6.48 -15 -4 5 10.96 2.04 -15 -4 5 10.46 2.06 -15 -4 5 9.08 1.94 15 4 -5 13.53 3.07 15 4 -5 11.63 3.75 15 4 -4 95.35 7.89 -15 -4 4 97.44 4.97 -15 -4 4 97.62 5.34 -15 -4 4 100.45 10.18 15 4 -4 91.47 8.28 -15 -4 4 94.35 4.78 -15 -4 3 27.40 2.77 -15 -4 3 29.60 2.83 -15 -4 3 32.87 3.12 15 4 -3 27.00 4.64 -15 -4 3 26.09 5.43 15 4 -3 30.78 4.59 -15 -4 2 0.85 1.15 -15 -4 2 -0.93 1.36 -15 -4 2 0.56 1.36 15 4 -2 2.61 2.08 -15 -4 2 0.27 2.36 -15 -4 1 40.30 3.44 -15 -4 1 31.93 5.64 -15 -4 1 38.52 3.23 15 4 -1 36.39 5.06 -15 -4 1 35.00 2.93 -15 -4 0 97.78 5.28 -15 -4 0 94.07 9.38 -15 -4 0 94.73 4.92 15 4 0 89.98 7.65 -15 -4 0 97.91 4.56 -15 -4 -1 1.39 1.99 -15 -4 -1 1.92 1.30 -15 -4 -1 0.88 1.23 15 4 1 -0.77 2.09 -15 -4 -1 1.22 1.15 -15 -4 -2 38.40 3.24 -15 -4 -2 31.47 4.99 15 4 2 40.01 5.36 -15 -4 -2 35.28 3.33 -15 -4 -3 53.84 3.81 -15 -4 -3 43.04 6.07 15 4 3 51.45 5.92 -15 -4 -3 49.52 3.90 -15 -4 -4 10.81 2.06 -15 -4 -4 7.40 2.93 15 4 4 7.86 2.90 -15 -4 -4 9.87 2.13 -15 -4 -5 100.21 5.11 -15 -4 -5 109.33 9.44 -15 -4 -5 99.90 5.48 15 4 5 98.69 8.22 -15 -4 -6 9.36 1.89 -15 -4 -6 11.10 3.58 15 4 6 12.06 3.71 -15 -4 -6 8.27 2.05 -15 -4 -7 33.17 3.19 -15 -4 -7 33.42 5.39 -15 -4 -7 32.07 3.51 15 4 7 32.56 4.93 -15 -4 -8 1.19 1.94 -15 -4 -8 4.72 1.74 15 4 8 5.25 2.89 -15 -4 -8 7.93 1.90 -15 -4 -9 165.95 7.04 -15 -4 -9 169.05 11.36 15 4 9 176.74 12.31 -15 -4 -9 164.08 7.29 15 4 10 26.02 5.33 -15 -4 -10 18.26 3.96 -15 -4 -10 22.94 2.94 -15 -4 -10 23.49 2.94 -15 -4 -11 21.92 3.03 -15 -4 -11 21.97 3.27 -15 -4 -12 19.62 2.82 -15 -4 -12 18.65 2.97 -15 -4 -13 5.79 1.81 -15 -4 -13 6.50 2.24 -15 -4 -14 54.04 4.31 -15 -4 -14 60.14 4.69 -15 -4 -15 47.22 4.11 -15 -4 -15 50.35 4.37 -15 -4 -16 24.41 2.88 -15 -4 -16 26.94 3.13 -15 -4 -17 1.01 1.38 -15 -4 -17 0.28 1.40 -15 -4 -18 14.97 2.32 -15 -4 -19 36.53 3.08 -15 -4 -20 1.85 1.04 -15 -4 -21 2.80 0.88 -15 -5 18 2.86 0.88 15 5 -18 1.87 0.54 -15 -5 17 14.08 1.55 -15 -5 17 13.39 1.63 15 5 -17 16.63 1.38 -15 -5 16 30.50 2.26 -15 -5 16 30.77 2.54 15 5 -16 36.57 2.20 -15 -5 15 13.89 1.71 -15 -5 15 14.60 2.05 15 5 -15 17.06 1.74 -15 -5 14 9.53 1.77 -15 -5 14 7.91 1.78 15 5 -14 9.21 1.44 -15 -5 13 1.11 1.12 -15 -5 13 1.77 1.12 15 5 -13 1.17 0.96 -15 -5 12 53.37 3.63 -15 -5 12 52.53 3.96 15 5 -12 55.79 3.30 -15 -5 11 52.83 3.71 -15 -5 11 48.12 3.85 15 5 -11 59.88 3.44 -15 -5 10 53.14 3.73 -15 -5 10 52.39 4.03 15 5 -10 55.34 3.32 -15 -5 9 2.03 1.37 -15 -5 9 0.48 1.27 15 5 -9 2.93 1.48 -15 -5 8 96.71 5.28 -15 -5 8 85.23 4.61 -15 -5 8 90.46 5.14 -15 -5 7 22.03 2.75 15 5 -7 27.30 2.40 15 5 -7 26.04 4.94 -15 -5 7 24.25 2.76 -15 -5 7 21.68 2.55 15 5 -7 18.89 3.80 -15 -5 6 30.46 3.11 15 5 -6 24.22 4.47 -15 -5 6 25.87 2.89 -15 -5 6 26.85 2.64 15 5 -6 25.69 4.34 -15 -5 5 10.50 2.10 -15 -5 5 7.51 1.99 15 5 -5 14.55 3.81 -15 -5 5 9.28 2.05 15 5 -5 11.15 2.96 -15 -5 4 104.33 5.14 -15 -5 4 106.22 5.41 15 5 -4 109.04 8.96 -15 -5 4 106.28 10.43 15 5 -4 102.19 8.03 -15 -5 4 108.09 4.88 -15 -5 3 95.77 4.91 -15 -5 3 98.27 5.18 15 5 -3 95.46 8.22 -15 -5 3 96.23 9.98 15 5 -3 107.95 8.23 -15 -5 3 96.34 4.61 -15 -5 2 159.36 6.08 -15 -5 2 164.87 6.63 15 5 -2 154.95 10.36 -15 -5 2 155.34 12.30 -15 -5 2 160.71 5.89 15 5 -2 158.61 9.84 -15 -5 1 4.21 1.41 -15 -5 1 1.29 1.23 15 5 -1 2.14 1.95 -15 -5 1 6.84 2.87 -15 -5 1 0.05 1.32 -15 -5 1 2.07 1.43 -15 -5 0 154.79 5.93 -15 -5 0 158.89 6.40 15 5 0 159.13 10.03 -15 -5 0 152.16 11.64 -15 -5 0 157.61 5.82 -15 -5 0 157.36 6.51 -15 -5 -1 116.22 5.13 15 5 1 113.24 8.54 -15 -5 -1 117.17 5.60 -15 -5 -1 112.23 5.68 -15 -5 -1 124.75 10.43 -15 -5 -2 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-15 -6 6 206.86 6.79 15 6 -6 231.17 13.12 15 6 -5 11.88 3.33 -15 -6 5 17.74 2.56 -15 -6 5 13.68 2.14 15 6 -5 13.41 3.56 -15 -6 5 18.60 2.56 15 6 -4 3.29 2.31 -15 -6 4 2.74 1.50 -15 -6 4 4.73 1.61 15 6 -4 4.37 2.08 -15 -6 4 3.00 1.26 15 6 -3 46.88 5.97 -15 -6 3 46.04 3.57 15 6 -3 44.10 5.52 -15 -6 3 45.47 3.52 -15 -6 3 39.62 6.50 -15 -6 2 13.26 4.24 15 6 -2 12.59 2.84 -15 -6 2 14.46 2.26 15 6 -2 16.52 3.66 -15 -6 2 18.03 2.34 -15 -6 2 16.08 2.09 15 6 -1 -0.34 1.75 -15 -6 1 -2.10 2.53 -15 -6 1 0.34 1.66 15 6 -1 -0.26 2.23 -15 -6 1 5.30 1.48 -15 -6 1 -2.61 1.47 -15 -6 0 19.39 4.54 -15 -6 0 18.53 2.37 15 6 0 19.15 3.83 -15 -6 0 17.32 2.32 -15 -6 0 19.14 2.26 -15 -6 -1 102.46 9.40 -15 -6 -1 93.16 4.92 15 6 1 85.09 7.33 -15 -6 -1 86.63 4.74 -15 -6 -1 95.06 4.67 -15 -6 -2 204.92 13.28 -15 -6 -2 224.75 7.59 -15 -6 -2 222.21 7.68 15 6 2 209.62 11.41 -15 -6 -2 209.94 6.94 -15 -6 -3 96.57 8.81 -15 -6 -3 99.18 5.12 -15 -6 -3 91.24 5.14 15 6 3 92.81 7.79 -15 -6 -3 92.25 4.62 -15 -6 -4 55.20 6.83 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118.14 6.20 -15 -6 -16 16.84 2.71 -15 -6 -16 14.65 2.39 -15 -6 -17 149.86 6.80 -15 -6 -17 141.64 6.45 -15 -6 -18 0.86 1.48 -15 -6 -18 2.46 1.18 -15 -6 -19 17.23 2.39 -15 -6 -19 19.00 2.21 -15 -6 -20 -0.23 1.07 -15 -6 -21 7.30 1.48 -15 -6 -22 31.88 2.12 -15 -7 17 15.19 1.54 15 7 -17 18.12 1.30 -15 -7 16 2.33 1.03 15 7 -16 0.35 0.65 -15 -7 16 -0.02 0.77 15 7 -15 35.82 2.22 -15 -7 15 34.45 2.75 -15 -7 15 32.37 2.27 -15 -7 14 10.87 1.86 -15 -7 14 10.48 1.53 15 7 -14 8.25 1.40 -15 -7 13 1.40 1.15 15 7 -13 1.97 1.02 -15 -7 13 0.48 1.04 15 7 -12 29.39 2.38 -15 -7 12 27.67 2.94 -15 -7 12 28.09 2.53 -15 -7 11 18.41 2.44 -15 -7 11 17.68 2.20 15 7 -11 19.10 2.02 -15 -7 10 10.79 2.11 -15 -7 10 9.78 1.79 15 7 -10 9.16 1.63 -15 -7 9 7.46 1.91 15 7 -9 8.02 1.88 -15 -7 9 5.50 1.52 -15 -7 8 228.71 8.11 -15 -7 8 235.33 7.23 -15 -7 7 49.84 3.44 -15 -7 7 49.57 3.88 15 7 -6 174.89 11.63 -15 -7 6 170.85 6.94 -15 -7 6 175.99 6.82 15 7 -6 169.62 10.94 15 7 -5 66.24 7.26 -15 -7 5 65.70 4.32 -15 -7 5 67.51 4.51 15 7 -5 68.46 6.85 15 7 -4 97.73 8.60 -15 -7 4 94.32 5.01 -15 -7 4 100.34 5.13 15 7 -4 103.17 8.47 15 7 -3 158.80 10.81 15 7 -3 141.12 9.51 -15 -7 3 143.34 6.00 -15 -7 3 145.37 6.27 15 7 -2 47.71 5.81 -15 -7 2 61.01 4.03 15 7 -2 59.51 6.05 -15 -7 2 56.44 7.76 -15 -7 2 56.04 3.75 15 7 -1 5.47 3.04 -15 -7 1 4.84 1.51 -15 -7 1 1.89 1.42 15 7 -1 2.28 1.70 -15 -7 1 -0.33 2.11 15 7 0 14.11 3.12 -15 -7 0 10.99 3.41 15 7 0 14.48 3.24 -15 -7 0 10.00 1.74 -15 -7 0 9.69 1.92 -15 -7 0 12.84 2.25 -15 -7 -1 0.32 2.14 15 7 1 3.74 1.78 15 7 1 2.22 1.81 -15 -7 -1 3.51 1.30 -15 -7 -1 3.05 1.51 -15 -7 -1 1.00 1.49 -15 -7 -2 7.81 2.93 15 7 2 5.66 2.59 -15 -7 -2 10.48 1.86 -15 -7 -2 7.84 2.01 -15 -7 -2 8.21 2.01 -15 -7 -3 54.93 6.96 15 7 3 63.67 6.37 -15 -7 -3 60.26 3.70 -15 -7 -3 63.16 4.18 -15 -7 -3 61.56 4.25 -15 -7 -4 27.98 4.88 15 7 4 28.42 4.41 -15 -7 -4 29.83 2.79 -15 -7 -4 27.74 1.97 -15 -7 -4 27.74 3.03 -15 -7 -4 26.41 2.04 -15 -7 -4 30.02 3.04 -15 -7 -5 142.70 6.30 -15 -7 -5 131.98 9.98 15 7 5 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7 5.57 1.47 -15 -11 7 5.52 1.76 -15 -11 6 5.15 1.59 -15 -11 6 2.97 1.29 -15 -11 5 1.69 1.14 -15 -11 5 1.49 1.18 -15 -11 4 13.70 1.71 -15 -11 4 13.37 2.24 -15 -11 3 0.92 2.15 -15 -11 3 3.43 1.58 -15 -11 3 4.14 1.33 15 11 -3 2.19 1.81 -15 -11 2 172.17 6.74 -15 -11 2 167.99 11.34 -15 -11 2 181.89 5.28 15 11 -2 163.94 10.38 -15 -11 1 5.53 2.95 15 11 -1 6.87 2.63 -15 -11 1 2.73 1.48 -15 -11 1 8.82 1.92 -15 -11 0 202.20 7.24 -15 -11 0 207.34 12.85 15 11 0 199.81 11.16 -15 -11 0 204.93 7.85 -15 -11 -1 31.25 5.24 -15 -11 -1 36.62 3.19 15 11 1 35.86 4.74 -15 -11 -1 32.38 3.42 -15 -11 -2 369.80 9.69 -15 -11 -2 357.71 16.88 -15 -11 -2 372.57 10.69 15 11 2 366.37 15.01 -15 -11 -3 45.02 2.82 -15 -11 -3 44.97 3.55 -15 -11 -3 39.91 5.74 -15 -11 -3 46.24 3.94 -15 -11 -3 42.11 2.83 15 11 3 50.10 5.59 -15 -11 -4 3.84 1.46 -15 -11 -4 3.19 1.06 -15 -11 -4 7.45 2.23 -15 -11 -4 4.95 2.67 15 11 4 3.30 2.03 -15 -11 -4 0.79 1.40 -15 -11 -4 4.85 2.56 -15 -11 -4 3.59 0.99 -15 -11 -5 10.67 2.09 -15 -11 -5 10.95 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-25 -9 -1 19.61 1.97 -25 -9 -2 10.75 1.60 -25 -9 -3 42.83 2.81 -25 -9 -4 13.25 1.88 -25 -9 -5 4.78 1.28 -25 -10 -1 27.32 2.25 -25 -10 -2 2.13 1.28 -25 -10 -3 5.71 1.45 -25 -10 -4 8.07 1.55 -25 -10 -5 26.11 2.30 -25 -10 -6 26.14 2.34 -25 -11 -2 7.14 1.31 -25 -11 -3 13.04 1.75 -25 -11 -4 1.24 1.20 -25 -11 -5 0.47 1.01 -25 -11 -6 1.52 0.98 -25 -11 -7 45.82 2.89 -25 -12 -3 0.41 0.96 -25 -12 -4 6.31 1.50 -25 -12 -5 3.75 1.30 -25 -12 -6 0.33 1.06 -25 -12 -7 20.46 2.12 -25 -13 -4 2.36 1.17 -25 -13 -5 3.48 1.22 -25 -13 -6 22.23 2.31 -25 -13 -7 0.74 1.10 0 0 0 0.00 0.00 TITL hasj240506a in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 20.469911 20.480922 21.459449 70.0843 81.7552 64.5639 ZERR 3.00 0.000553 0.000540 0.000493 0.0023 0.0021 0.0026 LATT 1 SFAC C H N O P Ca UNIT 393.00 633.00 18.00 12.00 21.00 9.00 REM CrysAlisPro recorded range (K): Min=99.8; max=100.1; aver:100.0 TEMP -173 SIZE 0.15 0.19 0.30 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; 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0.0579 22 18 13 1.4069 0.1800 22 18 14 0.0980 0.2034 22 19 0 0.4971 0.2532 22 19 1 -0.5559 -0.1021 22 19 2 -0.4541 0.2988 22 19 3 0.5638 0.1901 22 19 4 -0.0643 -0.0788 22 19 5 -0.1116 0.1755 22 19 6 -0.4405 0.1311 22 19 7 -0.3066 0.0450 22 19 8 0.0673 0.3234 22 19 9 0.8195 0.0160 22 19 10 0.1139 -0.2549 22 19 11 0.1337 0.1657 22 19 12 0.3118 0.0434 22 19 13 0.5227 0.0277 22 20 3 0.4948 -0.0019 22 20 4 -0.8250 -0.1544 22 20 5 0.0705 -0.0609 22 20 6 0.0522 -0.1704 22 20 7 0.0933 0.1366 22 20 8 0.0838 0.2530 22 20 9 -0.0213 -0.4538 22 20 10 -0.9020 -0.3405 22 20 11 0.2146 0.2333 23 1 0 0.2136 0.5189 23 1 1 0.3287 0.0045 23 1 2 0.4713 0.0626 23 1 3 -0.2045 -0.4833 23 1 4 -0.3526 -0.1954 23 2 0 -0.6744 -0.9513 23 2 1 0.0157 -0.5443 23 2 2 0.2577 -0.0974 23 2 3 -1.0309 -0.1611 23 2 4 -0.5544 0.3232 23 2 5 0.6726 0.0076 23 2 6 0.0462 0.0590 23 3 0 -0.4753 -0.2675 23 3 1 0.6588 0.7140 23 3 2 -0.0255 0.3925 23 3 3 -0.2089 0.0884 23 3 4 0.7263 0.1540 23 3 5 0.4314 -0.0151 23 3 6 -1.0204 0.0874 23 3 7 -0.8380 -0.1764 23 3 8 -0.0992 0.0863 23 4 0 0.0477 0.6034 23 4 1 0.4129 0.2089 23 4 2 -0.1839 0.0032 23 4 3 -0.1857 -0.1374 23 4 4 -0.6786 -0.0014 23 4 5 0.0980 -0.1231 23 4 6 0.4093 -0.0845 23 4 7 1.0383 -0.0803 23 4 8 1.1867 0.1617 23 4 9 0.2077 -0.1650 23 5 0 0.8962 0.3095 23 5 1 -0.3528 -0.2095 23 5 2 -0.3706 -0.2515 23 5 3 -0.4708 -0.3642 23 5 4 0.2082 -0.0651 23 5 5 0.9980 -0.1354 23 5 6 -0.6381 0.0309 23 5 7 -0.3899 -0.1120 23 5 8 -0.3748 0.0222 23 5 9 -0.6130 -0.0210 23 5 10 -0.6000 0.1705 23 6 0 1.1348 -0.6931 23 6 1 -0.8581 -0.3010 23 6 2 0.0713 -0.0135 23 6 3 0.2649 0.2443 23 6 4 0.3393 0.0895 23 6 5 -0.5342 0.1365 23 6 6 -0.3002 0.2045 23 6 7 0.7290 0.0778 23 6 8 -0.6375 0.2236 23 6 9 -0.1579 0.0368 23 6 10 -0.0807 -0.0559 23 6 11 0.9644 -0.0432 23 7 0 -1.7543 -0.0685 23 7 1 -0.9555 0.1575 23 7 2 0.4462 0.1770 23 7 3 0.3459 0.0206 23 7 4 -0.6080 -0.0656 23 7 5 0.1414 0.1888 23 7 6 1.0543 -0.1704 23 7 7 -0.5578 -0.1493 23 7 8 -0.7165 -0.0850 23 7 9 1.3085 -0.0399 23 7 10 -0.1571 -0.0597 23 7 11 0.1890 -0.0006 23 7 12 -0.9788 -0.0993 23 8 0 -0.8690 0.7108 23 8 1 0.8678 0.3910 23 8 2 0.1236 0.1546 23 8 3 -0.8229 -0.0965 23 8 4 -0.7623 0.0311 23 8 5 1.1903 -0.1067 23 8 6 0.0177 -0.0747 23 8 7 -0.9337 0.1554 23 8 8 0.9262 0.0292 23 8 9 0.8198 0.0063 23 8 10 -0.8512 -0.0866 23 8 11 0.6860 0.1317 23 8 12 -0.1663 0.1209 23 8 13 0.7268 0.1124 23 9 0 0.6532 -0.5037 23 9 1 0.0876 -0.6151 23 9 2 -0.1359 -0.3908 23 9 3 -0.0355 -0.0097 23 9 4 1.2457 0.0130 23 9 5 0.5197 -0.0969 23 9 6 -1.4222 0.0406 23 9 7 -0.5782 -0.1403 23 9 8 0.2744 -0.0428 23 9 9 -0.7332 0.0640 23 9 10 -0.6939 0.0845 23 9 11 -0.0493 0.0155 23 9 12 -0.6200 -0.1293 23 9 13 0.5042 -0.1143 23 10 0 -0.3347 -0.2009 23 10 1 -0.3869 0.3635 23 10 2 0.6868 0.1854 23 10 3 -0.1218 0.0831 23 10 4 0.3049 -0.1434 23 10 5 -1.0101 0.0457 23 10 6 0.5656 0.0779 23 10 7 1.1113 0.0881 23 10 8 0.4570 0.1216 23 10 9 0.1504 -0.0390 23 10 10 0.5380 -0.0269 23 10 11 0.1748 -0.0273 23 10 12 0.4360 0.0362 23 10 13 0.2308 -0.1220 23 10 14 -0.7414 -0.1423 23 11 0 0.5272 0.2100 23 11 1 -0.1754 -0.0738 23 11 2 -0.1971 0.1082 23 11 3 -1.2308 0.0580 23 11 4 -0.2954 0.0735 23 11 5 -0.2630 0.0529 23 11 6 0.3600 0.0134 23 11 7 -1.4908 0.0838 23 11 8 -0.4226 0.0551 23 11 9 0.8102 0.1179 23 11 10 0.1124 0.0510 23 11 11 -0.7566 -0.0227 23 11 12 0.3950 -0.1924 23 11 13 -0.0535 -0.0371 23 11 14 -0.0315 0.3360 23 12 0 0.4360 0.1686 23 12 1 -0.3841 -0.1286 23 12 2 0.4339 -0.0830 23 12 3 0.0812 -0.1777 23 12 4 0.8051 0.0467 23 12 5 0.9334 -0.0262 23 12 6 0.1771 -0.0387 23 12 7 0.3643 -0.0977 23 12 8 1.5635 -0.1830 23 12 9 0.0653 -0.2689 23 12 10 -1.8223 -0.2428 23 12 11 -0.5380 0.0194 23 12 12 1.1122 -0.0204 23 12 13 -0.5484 0.3271 23 12 14 -0.5435 0.0295 23 13 0 0.3279 -0.2990 23 13 1 -0.5804 0.0829 23 13 2 -0.3169 0.0561 23 13 3 -0.1004 0.0629 23 13 4 0.5427 -0.0952 23 13 5 0.0904 -0.1157 23 13 6 -1.0190 0.0184 23 13 7 0.0886 0.2105 23 13 8 -0.4407 0.0640 23 13 9 -0.7638 0.1161 23 13 10 -0.0709 0.2142 23 13 11 1.2127 0.1134 23 13 12 0.3620 -0.1677 23 13 13 -1.1667 -0.0342 23 13 14 0.0141 -0.3313 23 14 0 0.4939 0.0409 23 14 1 -0.6438 -0.1944 23 14 2 -0.1347 -0.1467 23 14 3 0.7746 0.0538 23 14 4 -0.4853 0.1413 23 14 5 -0.5721 0.0971 23 14 6 -0.0367 -0.0297 23 14 7 0.7600 0.0089 23 14 8 -0.4833 -0.0898 23 14 9 -0.0053 0.1513 23 14 10 0.0988 0.0145 23 14 11 -0.1106 -0.0459 23 14 12 0.2100 -0.0134 23 14 13 0.1490 0.1181 23 14 14 0.6889 0.1582 23 15 0 -0.2111 -0.2890 23 15 1 -1.1657 0.0518 23 15 2 0.3212 0.1955 23 15 3 0.7301 0.1166 23 15 4 -0.6649 0.0447 23 15 5 1.0653 -0.1129 23 15 6 0.4464 0.1563 23 15 7 -0.4657 0.1661 23 15 8 -0.2857 -0.0874 23 15 9 0.6248 -0.3363 23 15 10 0.0791 -0.3009 23 15 11 -0.5831 -0.0242 23 15 12 0.2369 0.1139 23 15 13 -1.0439 0.0504 23 15 14 -0.4650 0.1371 23 16 0 0.0192 -0.0242 23 16 1 -0.1405 0.3717 23 16 2 1.3850 0.0481 23 16 3 0.4410 0.1593 23 16 4 -0.4663 -0.1411 23 16 5 0.5096 -0.2412 23 16 6 -1.2420 -0.0432 23 16 7 -0.6794 -0.0834 23 16 8 0.5555 -0.0495 23 16 9 -0.2078 0.0881 23 16 10 -0.3026 0.4623 23 16 11 0.1228 0.0627 23 16 12 1.1190 -0.2549 23 16 13 -0.2713 -0.4703 23 17 0 -0.1685 0.5220 23 17 1 -0.6136 -0.0818 23 17 2 -0.0846 -0.2935 23 17 3 -0.9397 -0.1550 23 17 4 -0.6209 -0.2498 23 17 5 0.1689 0.1477 23 17 6 -0.4361 0.2101 23 17 7 1.0848 0.0581 23 17 8 0.8434 -0.1514 23 17 9 -0.5563 -0.1153 23 17 10 0.1344 -0.0164 23 17 11 -0.4998 -0.2009 23 17 12 -0.2424 0.2606 23 17 13 -0.5886 0.5271 23 18 1 -0.1013 -0.5411 23 18 2 0.4389 0.2973 23 18 3 0.1884 0.1036 23 18 4 0.2322 0.1420 23 18 5 0.1788 0.0682 23 18 6 -0.2674 -0.0107 23 18 7 0.5124 0.1059 23 18 8 -0.7988 0.0701 23 18 9 -0.5746 -0.0294 23 18 10 0.4278 -0.0037 23 18 11 0.0236 -0.0500 23 18 12 0.8802 -0.0602 23 19 4 0.0792 0.0979 23 19 5 0.2556 -0.0740 23 19 6 0.2274 0.0433 23 19 7 0.3242 -0.0280 23 19 8 -0.7369 -0.3478 23 19 9 0.2809 -0.2589 23 19 10 -0.1078 0.3143 24 3 0 -0.1598 0.6734 24 3 1 0.0401 -0.0202 24 3 2 -0.0000 -0.5689 24 4 0 0.2654 -0.1886 24 4 1 0.1783 -0.4971 24 4 2 -0.1177 -0.0415 24 4 3 -0.2462 0.1049 24 4 4 -0.1198 -0.1915 24 4 5 1.7061 0.2126 24 5 0 0.1544 -0.5191 24 5 1 -0.5988 0.0027 24 5 2 -0.3883 0.0367 24 5 3 -0.1869 0.1122 24 5 4 0.7109 0.1565 24 5 5 0.0533 0.1154 24 5 6 -1.6690 -0.1508 24 5 7 0.1257 0.1186 24 6 0 -0.6437 0.1511 24 6 1 -0.4020 0.4520 24 6 2 0.1320 0.2071 24 6 3 0.4914 0.1747 24 6 4 0.4353 -0.0633 24 6 5 -0.5280 0.0313 24 6 6 -0.1135 -0.0125 24 6 7 0.4984 0.0538 24 6 8 -0.4672 -0.1336 24 7 0 0.6834 0.4196 24 7 1 1.1856 -0.1461 24 7 2 0.2920 -0.1723 24 7 3 0.3691 -0.2398 24 7 4 -0.2726 -0.1543 24 7 5 0.1120 -0.1489 24 7 6 -0.2681 -0.2237 24 7 7 -0.0570 0.0089 24 7 8 0.5361 0.0447 24 7 9 0.1884 0.0384 24 8 0 1.8747 0.1087 24 8 1 -0.2124 -0.4200 24 8 2 -1.3825 -0.1144 24 8 3 0.0768 -0.0310 24 8 4 0.0815 0.1036 24 8 5 0.1745 0.1202 24 8 6 -0.9918 0.2696 24 8 7 0.9482 0.1115 24 8 8 0.4265 -0.0031 24 8 9 -0.9008 0.0442 24 8 10 -0.0435 0.1851 24 9 0 -0.3702 -1.0672 24 9 1 -0.4068 0.0833 24 9 2 -0.3173 0.3448 24 9 3 0.8993 0.2231 24 9 4 -0.4265 -0.0003 24 9 5 -0.8344 0.1068 24 9 6 0.0456 -0.0229 24 9 7 1.5007 -0.0839 24 9 8 -0.7532 0.0867 24 9 9 -0.7267 -0.0497 24 9 10 0.6714 -0.1659 24 9 11 0.4887 -0.3452 24 10 0 -0.2606 1.0085 24 10 1 1.6914 0.5139 24 10 2 -1.1090 -0.1254 24 10 3 0.0887 -0.1153 24 10 4 -0.0491 -0.0106 24 10 5 0.7851 0.0259 24 10 6 1.0472 -0.2288 24 10 7 -0.6479 -0.1216 24 10 8 -1.1922 -0.1151 24 10 9 -0.1220 -0.0576 24 10 10 0.6078 0.0933 24 10 11 -0.1014 -0.0277 24 11 0 -0.5179 0.1800 24 11 1 0.4177 -0.4156 24 11 2 -1.6237 -0.1435 24 11 3 1.5227 -0.0311 24 11 4 0.8232 -0.0774 24 11 5 -0.0617 -0.1219 24 11 6 -0.5016 0.1401 24 11 7 -0.6029 0.1904 24 11 8 1.3434 0.1453 24 11 9 0.1132 -0.0058 24 11 10 0.5001 -0.0810 24 11 11 -0.0394 -0.1926 24 12 0 -0.2525 -0.7737 24 12 1 0.6623 -0.2372 24 12 2 -0.8711 0.0578 24 12 3 -0.0768 0.0448 24 12 4 -0.5121 -0.0147 24 12 5 -0.9668 0.0545 24 12 6 -0.2852 0.0278 24 12 7 -0.4741 -0.2084 24 12 8 0.1761 -0.0536 24 12 9 -1.6677 0.0174 24 12 10 0.7446 0.3142 24 12 11 -0.0157 -0.0096 24 12 12 -0.5894 0.2591 24 13 0 -0.9344 0.3478 24 13 1 0.4657 0.4765 24 13 2 -0.0530 0.0598 24 13 3 0.9091 -0.0005 24 13 4 1.5934 0.2230 24 13 5 -0.4678 0.3262 24 13 6 0.4412 0.0508 24 13 7 0.3341 0.0570 24 13 8 1.0878 0.0338 24 13 9 -0.4191 0.0166 24 13 10 1.2176 -0.1938 24 13 11 -0.7033 -0.5240 24 13 12 -0.5443 0.1980 24 14 0 -0.8734 0.2795 24 14 1 0.6773 -0.1228 24 14 2 -0.4293 0.0695 24 14 3 -0.4708 0.0175 24 14 4 0.0219 -0.0470 24 14 5 -1.2040 -0.4650 24 14 6 0.5177 -0.3474 24 14 7 -0.3322 0.0414 24 14 8 -0.2082 -0.0851 24 14 9 -0.8333 0.0262 24 14 10 0.7074 -0.2654 24 14 11 -0.4606 0.0825 24 15 0 -0.4335 0.5339 24 15 1 1.2106 -0.1303 24 15 2 0.0443 -0.0515 24 15 3 -0.0162 -0.1811 24 15 4 0.4322 0.0527 24 15 5 -0.8344 0.1069 24 15 6 -0.1148 0.2912 24 15 7 -0.2704 0.0057 24 15 8 0.3088 -0.2500 24 15 9 -0.0741 0.2583 24 15 10 0.0396 0.1720 24 15 11 -0.4337 0.5258 24 16 1 0.8520 -0.4002 24 16 2 -1.0667 -0.0236 24 16 3 -0.7395 -0.1785 24 16 4 0.3535 -0.0249 24 16 5 -0.1226 0.0970 24 16 6 0.6328 0.0209 24 16 7 0.4937 0.0278 24 16 8 0.1151 0.0679 24 16 9 -0.0342 0.2091 24 16 10 0.2582 -0.6189 24 17 3 0.6710 0.1082 24 17 4 0.9565 0.5163 24 17 5 -0.2378 0.0972 24 17 6 -0.0280 -0.3870 24 17 7 -0.2080 -0.1941 24 17 8 -0.2364 -0.0632 24 17 9 -0.0724 0.1823 25 7 2 -0.5392 0.1232 25 7 3 -0.4143 -0.0782 25 8 0 0.3993 -0.4641 25 8 1 -1.3711 0.0469 25 8 2 0.5935 -0.1170 25 8 3 0.6830 -0.0241 25 8 4 0.8477 0.1168 25 8 5 -0.1509 -0.1455 25 9 0 0.1692 0.4754 25 9 1 -0.9026 0.5106 25 9 2 1.0649 0.0531 25 9 3 -0.2009 0.0475 25 9 4 -0.5135 -0.0230 25 9 5 -0.6556 -0.0132 25 9 6 0.4073 0.0116 25 10 0 0.5506 -0.0511 25 10 1 -1.1553 -0.5501 25 10 2 0.8719 -0.2844 25 10 3 0.5135 -0.1685 25 10 4 -0.2735 -0.1073 25 10 5 -0.0044 -0.1122 25 10 6 -0.3293 -0.0294 25 10 7 -0.4248 0.1234 25 11 0 0.3576 -0.2961 25 11 1 -0.6097 0.0278 25 11 2 1.4690 0.2531 25 11 3 -0.3449 0.1137 25 11 4 -1.6516 0.1838 25 11 5 0.3210 0.2222 25 11 6 -0.0082 0.2014 25 11 7 0.8838 -0.0892 25 11 8 0.0734 -0.2198 25 12 1 -0.8619 0.4211 25 12 2 0.2983 0.0182 25 12 3 -0.3308 0.0317 25 12 4 0.1885 -0.0283 25 12 5 1.3595 -0.0463 25 12 6 -0.3786 -0.1207 25 12 7 0.4862 -0.0717 25 12 8 -0.5060 0.1517 25 13 2 0.8097 -0.1876 25 13 3 0.0266 0.1874 25 13 4 -1.1385 -0.1163 25 13 5 -0.5523 -0.2410 25 13 6 -0.7050 -0.1113 25 13 7 0.3569 -0.1358 25 14 3 -0.1191 -0.1022 25 14 4 -0.3466 -0.3720 25 14 5 1.2251 0.1488 25 14 6 0.3990 0.5334 25 14 7 0.3278 0.0115 0 0 0 0.0 0.0 ; _shelx_fab_checksum 14664 _olex2_date_sample_data_collection 2024-05-06 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.958 _oxdiff_exptl_absorpt_empirical_full_min 0.607 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ca1 Ca 0.85535(2) 0.70967(2) 0.21828(2) 0.02455(6) Uani 1 1 d . . . . . Ca2 Ca 0.54934(2) 0.73873(2) 0.20737(2) 0.02636(6) Uani 1 1 d . . . . . Ca3 Ca 0.79341(2) 0.42985(2) 0.31784(2) 0.02563(6) Uani 1 1 d . . . . . P1 P 0.72492(2) 0.69345(2) 0.15670(2) 0.02688(8) Uani 1 1 d . . . . . P2 P 0.69832(2) 0.59070(2) 0.19067(2) 0.02745(8) Uani 1 1 d . . . . . P3 P 0.81318(2) 0.57585(2) 0.19758(2) 0.02713(8) Uani 1 1 d . . . . . P4 P 0.69218(2) 0.74008(2) 0.23818(2) 0.02618(8) Uani 1 1 d . . . . . P5 P 0.65730(2) 0.58268(2) 0.29036(2) 0.02701(8) Uani 1 1 d . . . . . P6 P 0.82710(2) 0.56711(2) 0.29843(2) 0.02646(8) Uani 1 1 d . . . . . P7 P 0.71561(2) 0.63507(2) 0.32056(2) 0.02655(8) Uani 1 1 d . . . . . O1 O 0.97339(6) 0.64437(6) 0.26708(5) 0.0325(2) Uani 1 1 d . . . . . O2 O 0.49224(6) 0.87115(6) 0.19519(6) 0.0336(2) Uani 1 1 d . . . . . O3 O 0.71974(6) 0.36143(6) 0.36680(6) 0.0342(2) Uani 1 1 d . . . . . N1 N 0.90480(7) 0.75961(7) 0.11270(6) 0.0257(2) Uani 1 1 d . . . . . N2 N 0.83464(7) 0.82941(7) 0.22834(6) 0.0269(2) Uani 1 1 d . . . . . N3 N 0.48827(7) 0.75868(7) 0.11032(6) 0.0295(3) Uani 1 1 d . . . . . N4 N 0.44547(7) 0.71713(8) 0.26030(7) 0.0319(3) Uani 1 1 d . . . . . N5 N 0.85835(7) 0.34041(7) 0.25899(6) 0.0273(3) Uani 1 1 d . . . . . N6 N 0.88860(7) 0.34188(7) 0.39677(6) 0.0283(3) Uani 1 1 d . . . . . C1 C 0.82005(9) 0.82440(9) 0.01759(7) 0.0299(3) Uani 1 1 d . . . . . H1A H 0.825616 0.776784 0.011917 0.045 Uiso 1 1 calc R U . . . H1B H 0.852315 0.844346 -0.013093 0.045 Uiso 1 1 calc R U . . . H1C H 0.769831 0.861685 0.008275 0.045 Uiso 1 1 calc R U . . . C2 C 0.83926(8) 0.80950(8) 0.08841(7) 0.0252(3) Uani 1 1 d . . . . . C3 C 0.78215(8) 0.84936(8) 0.12522(7) 0.0263(3) Uani 1 1 d . . . . . H3 H 0.7369(10) 0.8763(10) 0.1017(9) 0.034(5) Uiso 1 1 d . . . . . C4 C 0.78140(8) 0.86713(8) 0.18380(7) 0.0264(3) Uani 1 1 d . . . . . C5 C 0.71194(9) 0.93038(9) 0.19521(8) 0.0345(3) Uani 1 1 d . . . . . H5A H 0.683045 0.957456 0.154394 0.052 Uiso 1 1 calc R U . . . H5B H 0.723447 0.965969 0.207825 0.052 Uiso 1 1 calc R U . . . H5C H 0.684370 0.908637 0.230793 0.052 Uiso 1 1 calc R U . . . C6 C 0.95969(8) 0.73836(8) 0.06439(7) 0.0283(3) Uani 1 1 d . . . . . C7 C 0.99648(8) 0.78590(9) 0.03275(8) 0.0316(3) Uani 1 1 d . . . . . C8 C 1.04526(9) 0.76829(10) -0.01754(9) 0.0383(4) Uani 1 1 d . . . . . H8 H 1.069359 0.800505 -0.039572 0.046 Uiso 1 1 calc R U . . . C9 C 1.05958(10) 0.70536(10) -0.03627(9) 0.0405(4) Uani 1 1 d . . . . . H9 H 1.092146 0.695148 -0.071484 0.049 Uiso 1 1 calc R U . . . C10 C 1.02599(9) 0.65741(9) -0.00321(8) 0.0365(3) Uani 1 1 d . . . . . H10 H 1.036846 0.613299 -0.015249 0.044 Uiso 1 1 calc R U . . . C11 C 0.97648(8) 0.67221(9) 0.04746(8) 0.0297(3) Uani 1 1 d . . . . . C12 C 0.98438(9) 0.85481(9) 0.05230(8) 0.0337(3) Uani 1 1 d . . . . . H12 H 0.969732 0.844007 0.099970 0.040 Uiso 1 1 calc R U . . . C13 C 1.05439(10) 0.86737(10) 0.04762(10) 0.0436(4) Uani 1 1 d . . . . . H13A H 1.069980 0.878868 0.000752 0.052 Uiso 1 1 calc R U . . . H13B H 1.043588 0.912321 0.061581 0.052 Uiso 1 1 calc R U . . . C14 C 1.11664(10) 0.79964(12) 0.08972(11) 0.0512(5) Uani 1 1 d . . . . . H14A H 1.159187 0.811410 0.083823 0.077 Uiso 1 1 calc R U . . . H14B H 1.128261 0.754927 0.075929 0.077 Uiso 1 1 calc R U . . . H14C H 1.102513 0.789040 0.136496 0.077 Uiso 1 1 calc R U . . . C15 C 0.92306(9) 0.92873(9) 0.01345(9) 0.0368(4) Uani 1 1 d . . . . . H15A H 0.876569 0.923734 0.026025 0.044 Uiso 1 1 calc R U . . . H15B H 0.921018 0.971129 0.027096 0.044 Uiso 1 1 calc R U . . . C16 C 0.93032(10) 0.94962(10) -0.06197(9) 0.0430(4) Uani 1 1 d . . . . . H16A H 0.891893 0.999563 -0.082503 0.065 Uiso 1 1 calc R U . . . H16B H 0.926165 0.911268 -0.076780 0.065 Uiso 1 1 calc R U . . . H16C H 0.977562 0.951414 -0.074966 0.065 Uiso 1 1 calc R U . . . C17 C 0.94380(8) 0.61571(8) 0.08445(7) 0.0294(3) Uani 1 1 d . . . . . H17 H 0.896369 0.644863 0.102465 0.035 Uiso 1 1 calc R U . . . C18 C 0.99148(9) 0.55597(9) 0.14447(8) 0.0343(3) Uani 1 1 d . . . . . H18A H 0.996439 0.582865 0.172882 0.041 Uiso 1 1 calc R U . . . H18B H 0.966057 0.523777 0.170693 0.041 Uiso 1 1 calc R U . . . C19 C 1.06701(10) 0.50411(11) 0.12835(10) 0.0469(4) Uani 1 1 d . . . . . H19A H 1.093364 0.534999 0.103116 0.070 Uiso 1 1 calc R U . . . H19B H 1.063124 0.475189 0.101949 0.070 Uiso 1 1 calc R U . . . H19C H 1.093104 0.468812 0.169636 0.070 Uiso 1 1 calc R U . . . C20 C 0.92785(9) 0.57763(9) 0.04155(8) 0.0356(3) Uani 1 1 d . . . . . H20A H 0.973399 0.550869 0.020618 0.043 Uiso 1 1 calc R U . . . H20B H 0.910586 0.538979 0.070522 0.043 Uiso 1 1 calc R U . . . C21 C 0.87197(11) 0.63285(11) -0.01222(10) 0.0457(4) Uani 1 1 d . . . . . H21A H 0.864223 0.604918 -0.037489 0.069 Uiso 1 1 calc R U . . . H21B H 0.889235 0.670463 -0.042011 0.069 Uiso 1 1 calc R U . . . H21C H 0.826321 0.658889 0.008059 0.069 Uiso 1 1 calc R U . . . C22 C 0.83197(9) 0.86570(8) 0.27603(7) 0.0296(3) Uani 1 1 d . . . . . C23 C 0.80253(9) 0.84594(9) 0.33951(8) 0.0315(3) Uani 1 1 d . . . . . C24 C 0.79656(9) 0.88714(10) 0.38147(9) 0.0375(4) Uani 1 1 d . . . . . H24 H 0.777128 0.874162 0.424584 0.045 Uiso 1 1 calc R U . . . C25 C 0.81822(10) 0.94656(10) 0.36200(9) 0.0415(4) Uani 1 1 d . . . . . H25 H 0.811137 0.975781 0.390497 0.050 Uiso 1 1 calc R U . . . C26 C 0.85012(10) 0.96301(9) 0.30097(9) 0.0401(4) Uani 1 1 d . . . . . H26 H 0.865965 1.003051 0.288127 0.048 Uiso 1 1 calc R U . . . C27 C 0.85960(10) 0.92209(9) 0.25775(8) 0.0373(4) Uani 1 1 d D . . . . C28 C 0.78046(9) 0.77953(9) 0.36249(8) 0.0334(3) Uani 1 1 d . . . . . H28 H 0.763953 0.776825 0.322127 0.040 Uiso 1 1 calc R U . . . C29 C 0.84754(10) 0.70458(9) 0.38917(8) 0.0387(4) Uani 1 1 d . . . . . H29A H 0.832886 0.661648 0.401005 0.046 Uiso 1 1 calc R U . . . H29B H 0.883493 0.698802 0.353059 0.046 Uiso 1 1 calc R U . . . C30 C 0.88400(12) 0.69841(11) 0.44910(10) 0.0489(5) Uani 1 1 d . . . . . H30A H 0.900787 0.739250 0.437591 0.073 Uiso 1 1 calc R U . . . H30B H 0.925373 0.648988 0.462716 0.073 Uiso 1 1 calc R U . . . H30C H 0.849339 0.703031 0.485640 0.073 Uiso 1 1 calc R U . . . C31 C 0.71742(11) 0.78802(12) 0.41125(9) 0.0455(4) Uani 1 1 d . . . . . H31A H 0.707616 0.741852 0.424090 0.055 Uiso 1 1 calc R U . . . H31B H 0.731588 0.791592 0.451786 0.055 Uiso 1 1 calc R U . . . C32 C 0.64837(11) 0.85754(14) 0.38332(12) 0.0574(5) Uani 1 1 d . . . . . H32A H 0.632862 0.853477 0.344169 0.086 Uiso 1 1 calc R U . . . H32B H 0.657481 0.903588 0.370816 0.086 Uiso 1 1 calc R U . . . H32C H 0.610327 0.860318 0.416986 0.086 Uiso 1 1 calc R U . . . C38 C 1.02103(10) 0.68338(10) 0.24743(10) 0.0464(4) Uani 1 1 d . . . . . H38A H 1.027089 0.698328 0.284781 0.056 Uiso 1 1 calc R U . . . H38B H 0.999195 0.730259 0.209811 0.056 Uiso 1 1 calc R U . . . C39 C 1.09451(11) 0.63264(12) 0.22715(12) 0.0563(5) Uani 1 1 d . . . . . H39A H 1.126831 0.659698 0.215376 0.068 Uiso 1 1 calc R U . . . H39B H 1.088979 0.620925 0.187610 0.068 Uiso 1 1 calc R U . . . C40 C 1.12827(10) 0.55860(11) 0.28371(11) 0.0489(4) Uani 1 1 d . . . . . H40A H 1.173091 0.523489 0.268115 0.059 Uiso 1 1 calc R U . . . H40B H 1.141155 0.569463 0.320710 0.059 Uiso 1 1 calc R U . . . C41 C 1.07532(9) 0.52151(9) 0.30775(9) 0.0394(4) Uani 1 1 d . . . . . H41A H 1.069104 0.502724 0.273131 0.047 Uiso 1 1 calc R U . . . H41B H 1.095057 0.477288 0.347914 0.047 Uiso 1 1 calc R U . . . C42 C 1.00286(9) 0.57687(10) 0.32355(8) 0.0393(4) Uani 1 1 d . . . . . H42A H 0.968809 0.551854 0.336971 0.047 Uiso 1 1 calc R U . . . H42B H 1.008299 0.591655 0.361243 0.047 Uiso 1 1 calc R U . . . C43 C 0.52409(10) 0.64719(9) 0.07155(8) 0.0365(3) Uani 1 1 d . . . . . H43A H 0.572087 0.644182 0.054757 0.055 Uiso 1 1 calc R U . . . H43B H 0.488855 0.676882 0.035189 0.055 Uiso 1 1 calc R U . . . H43C H 0.525495 0.595760 0.090111 0.055 Uiso 1 1 calc R U . . . C44 C 0.50225(8) 0.68537(9) 0.12495(8) 0.0296(3) Uani 1 1 d . . . . . C45 C 0.50215(8) 0.63641(9) 0.19035(8) 0.0299(3) Uani 1 1 d . . . . . H45 H 0.5203(9) 0.5850(10) 0.1935(8) 0.026(4) Uiso 1 1 d . . . . . C46 C 0.46818(8) 0.65091(9) 0.24937(8) 0.0317(3) Uani 1 1 d . . . . . C47 C 0.46469(11) 0.58117(10) 0.30301(9) 0.0422(4) Uani 1 1 d . . . . . H47A H 0.512856 0.547500 0.322511 0.063 Uiso 1 1 calc R U . . . H47B H 0.448194 0.553952 0.283534 0.063 Uiso 1 1 calc R U . . . H47C H 0.430775 0.597130 0.337538 0.063 Uiso 1 1 calc R U . . . C48 C 0.47333(9) 0.80440(9) 0.04199(8) 0.0318(3) Uani 1 1 d . . . . . C49 C 0.52679(9) 0.82239(9) -0.00006(8) 0.0322(3) Uani 1 1 d . . . . . C50 C 0.50971(9) 0.86447(10) -0.06667(8) 0.0380(4) Uani 1 1 d . . . . . H50 H 0.545869 0.875688 -0.095565 0.046 Uiso 1 1 calc R U . . . C51 C 0.44104(10) 0.89019(10) -0.09141(9) 0.0426(4) Uani 1 1 d . . . . . H51 H 0.430463 0.918084 -0.136954 0.051 Uiso 1 1 calc R U . . . C52 C 0.38847(10) 0.87494(10) -0.04945(9) 0.0431(4) Uani 1 1 d . . . . . H52 H 0.341183 0.893833 -0.066403 0.052 Uiso 1 1 calc R U . . . C53 C 0.40248(9) 0.83242(10) 0.01750(9) 0.0383(4) Uani 1 1 d . . . . . C54 C 0.60081(9) 0.80020(9) 0.02620(7) 0.0318(3) Uani 1 1 d . . . . . H54 H 0.609234 0.755176 0.066865 0.038 Uiso 1 1 calc R U . . . C55 C 0.59983(9) 0.86444(9) 0.04898(8) 0.0341(3) Uani 1 1 d . . . . . H55A H 0.557961 0.878024 0.078774 0.041 Uiso 1 1 calc R U . . . H55B H 0.644161 0.844350 0.075319 0.041 Uiso 1 1 calc R U . . . C56 C 0.59548(10) 0.93691(10) -0.00605(9) 0.0399(4) Uani 1 1 d . . . . . H56A H 0.638066 0.925050 -0.034590 0.060 Uiso 1 1 calc R U . . . H56B H 0.593960 0.974315 0.013560 0.060 Uiso 1 1 calc R U . . . H56C H 0.551620 0.957902 -0.032455 0.060 Uiso 1 1 calc R U . . . C57 C 0.66339(9) 0.77541(10) -0.02062(8) 0.0373(4) Uani 1 1 d . . . . . H57A H 0.654972 0.817182 -0.063114 0.045 Uiso 1 1 calc R U . . . H57B H 0.708703 0.766252 -0.001069 0.045 Uiso 1 1 calc R U . . . C58 C 0.67266(11) 0.70370(12) -0.03426(10) 0.0496(4) Uani 1 1 d . . . . . H58A H 0.713975 0.689913 -0.063826 0.074 Uiso 1 1 calc R U . . . H58B H 0.628719 0.713007 -0.055329 0.074 Uiso 1 1 calc R U . . . H58C H 0.681262 0.661997 0.007579 0.074 Uiso 1 1 calc R U . . . C59 C 0.34229(10) 0.81846(11) 0.06201(10) 0.0453(4) Uani 1 1 d . . . . . H59 H 0.356440 0.808075 0.108266 0.054 Uiso 1 1 calc R U . . . C60 C 0.26999(10) 0.88895(11) 0.04792(10) 0.0465(4) Uani 1 1 d . . . . . H60A H 0.251853 0.897959 0.004082 0.056 Uiso 1 1 calc R U . . . H60B H 0.234378 0.878209 0.081583 0.056 Uiso 1 1 calc R U . . . C61 C 0.27421(11) 0.96120(12) 0.04833(11) 0.0520(5) Uani 1 1 d . . . . . H61A H 0.302316 0.977643 0.010098 0.078 Uiso 1 1 calc R U . . . H61B H 0.297764 0.951135 0.089292 0.078 Uiso 1 1 calc R U . . . H61C H 0.225268 1.001335 0.045863 0.078 Uiso 1 1 calc R U . . . C62 C 0.33322(11) 0.74786(12) 0.06151(12) 0.0589(6) Uani 1 1 d . . . . . H62A H 0.376020 0.702069 0.083420 0.071 Uiso 1 1 calc R U . . . H62B H 0.290427 0.745394 0.088623 0.071 Uiso 1 1 calc R U . . . C63 C 0.32427(17) 0.74426(14) -0.00594(15) 0.0828(9) Uani 1 1 d . . . . . H63A H 0.367557 0.743358 -0.032594 0.124 Uiso 1 1 calc R U . . . H63B H 0.281902 0.789041 -0.028344 0.124 Uiso 1 1 calc R U . . . H63C H 0.317562 0.698043 -0.000530 0.124 Uiso 1 1 calc R U . . . C64 C 0.39861(9) 0.72976(9) 0.31533(8) 0.0358(3) Uani 1 1 d D U . . . C65 C 0.3262(4) 0.7388(3) 0.3159(3) 0.0344(13) Uani 0.534(4) 1 d D U P A 1 C66 C 0.2801(5) 0.7542(4) 0.3678(4) 0.0366(16) Uani 0.534(4) 1 d D U P A 1 H66 H 0.230275 0.765733 0.364818 0.044 Uiso 0.534(4) 1 calc R U P A 1 C67 C 0.3065(6) 0.7526(7) 0.4231(5) 0.039(2) Uani 0.534(4) 1 d D U P A 1 H67 H 0.274684 0.764877 0.458234 0.047 Uiso 0.534(4) 1 calc R U P A 1 C68 C 0.3797(6) 0.7333(9) 0.4287(5) 0.043(3) Uani 0.534(4) 1 d D U P A 1 H68 H 0.399006 0.725412 0.469627 0.051 Uiso 0.534(4) 1 calc R U P A 1 C69 C 0.42498(9) 0.72541(9) 0.37412(8) 0.0349(3) Uani 1 1 d D U . . . C75 C 0.50462(9) 0.70440(10) 0.38357(8) 0.0380(4) Uani 1 1 d . . . . . H75 H 0.532097 0.677173 0.350970 0.046 Uiso 1 1 calc R U . . . C76 C 0.52063(10) 0.77523(11) 0.36689(9) 0.0440(4) Uani 1 1 d . . . . . H76A H 0.573197 0.758296 0.372379 0.053 Uiso 1 1 calc R U . . . H76B H 0.508647 0.804676 0.319627 0.053 Uiso 1 1 calc R U . . . C77 C 0.48024(12) 0.82810(12) 0.40826(10) 0.0512(5) Uani 1 1 d . . . . . H77A H 0.493405 0.871708 0.393539 0.077 Uiso 1 1 calc R U . . . H77B H 0.493307 0.800472 0.455060 0.077 Uiso 1 1 calc R U . . . H77C H 0.428011 0.846130 0.402786 0.077 Uiso 1 1 calc R U . . . C78 C 0.53415(10) 0.64943(11) 0.45279(9) 0.0442(4) Uani 1 1 d . . . . . H78A H 0.586469 0.636672 0.454331 0.053 Uiso 1 1 calc R U . . . H78B H 0.509807 0.675691 0.486159 0.053 Uiso 1 1 calc R U . . . C79 C 0.52365(12) 0.57641(11) 0.47147(10) 0.0539(5) Uani 1 1 d . . . . . H79A H 0.549243 0.548892 0.439762 0.081 Uiso 1 1 calc R U . . . H79B H 0.471948 0.588357 0.470627 0.081 Uiso 1 1 calc R U . . . H79C H 0.542959 0.544662 0.516114 0.081 Uiso 1 1 calc R U . . . C80 C 0.41617(9) 0.90801(10) 0.17792(10) 0.0423(4) Uani 1 1 d . . . . . H80A H 0.398426 0.869025 0.181008 0.051 Uiso 1 1 calc R U . . . H80B H 0.409709 0.942168 0.131581 0.051 Uiso 1 1 calc R U . . . C81 C 0.37270(11) 0.95326(11) 0.22320(12) 0.0564(5) Uani 1 1 d . . . . . H81A H 0.375799 0.918543 0.269052 0.068 Uiso 1 1 calc R U . . . H81B H 0.321280 0.979469 0.209353 0.068 Uiso 1 1 calc R U . . . C82 C 0.40064(13) 1.01195(11) 0.22148(12) 0.0599(6) Uani 1 1 d . . . . . H82A H 0.390697 1.051336 0.177439 0.072 Uiso 1 1 calc R U . . . H82B H 0.375208 1.037197 0.255264 0.072 Uiso 1 1 calc R U . . . C83 C 0.48174(12) 0.97336(11) 0.23517(10) 0.0507(5) Uani 1 1 d . . . . . H83A H 0.500408 1.012557 0.228438 0.061 Uiso 1 1 calc R U . . . H83B H 0.490811 0.940448 0.281908 0.061 Uiso 1 1 calc R U . . . C84 C 0.52124(10) 0.92610(9) 0.19024(9) 0.0389(4) Uani 1 1 d . . . . . H84A H 0.516991 0.959853 0.143869 0.047 Uiso 1 1 calc R U . . . H84B H 0.573206 0.898977 0.202270 0.047 Uiso 1 1 calc R U . . . C85 C 0.94545(9) 0.37373(9) 0.17556(7) 0.0320(3) Uani 1 1 d . . . . . H85A H 0.913151 0.422317 0.145670 0.048 Uiso 1 1 calc R U . . . H85B H 0.951169 0.332178 0.159467 0.048 Uiso 1 1 calc R U . . . H85C H 0.992785 0.374438 0.176926 0.048 Uiso 1 1 calc R U . . . C86 C 0.91332(8) 0.36175(8) 0.24464(7) 0.0271(3) Uani 1 1 d . . . . . C87 C 0.94203(8) 0.38006(8) 0.28916(7) 0.0279(3) Uani 1 1 d . . . . . H87 H 0.9741(10) 0.4006(10) 0.2694(8) 0.028(4) Uiso 1 1 d . . . . . C88 C 0.93870(8) 0.36144(8) 0.35981(7) 0.0284(3) Uani 1 1 d . . . . . C89 C 0.99631(9) 0.36981(9) 0.38997(8) 0.0351(3) Uani 1 1 d . . . . . H89A H 1.033738 0.374473 0.356907 0.053 Uiso 1 1 calc R U . . . H89B H 1.018142 0.324918 0.428364 0.053 Uiso 1 1 calc R U . . . H89C H 0.974215 0.415433 0.404105 0.053 Uiso 1 1 calc R U . . . C90 C 0.84728(8) 0.30234(8) 0.21891(7) 0.0282(3) Uani 1 1 d . . . . . C91 C 0.78979(8) 0.33935(8) 0.17292(7) 0.0285(3) Uani 1 1 d . . . . . C92 C 0.77970(9) 0.29808(9) 0.13783(8) 0.0338(3) Uani 1 1 d . . . . . H92 H 0.741332 0.322681 0.106537 0.041 Uiso 1 1 calc R U . . . C93 C 0.82432(10) 0.22244(9) 0.14775(9) 0.0382(4) Uani 1 1 d . . . . . H93 H 0.816549 0.195140 0.123646 0.046 Uiso 1 1 calc R U . . . C94 C 0.88046(10) 0.18642(9) 0.19293(9) 0.0389(4) Uani 1 1 d . . . . . H94 H 0.911181 0.134313 0.199194 0.047 Uiso 1 1 calc R U . . . C95 C 0.89330(9) 0.22439(9) 0.22962(8) 0.0338(3) Uani 1 1 d . . . . . C96 C 0.73787(8) 0.42202(8) 0.16123(8) 0.0296(3) Uani 1 1 d . . . . . H96 H 0.761840 0.444904 0.179798 0.036 Uiso 1 1 calc R U . . . C97 C 0.66696(9) 0.42968(10) 0.20022(8) 0.0359(3) Uani 1 1 d . . . . . H97A H 0.679506 0.401001 0.247515 0.043 Uiso 1 1 calc R U . . . H97B H 0.639006 0.483958 0.196966 0.043 Uiso 1 1 calc R U . . . C98 C 0.61786(11) 0.40244(12) 0.17881(10) 0.0483(4) Uani 1 1 d . . . . . H98A H 0.604873 0.430052 0.131988 0.073 Uiso 1 1 calc R U . . . H98B H 0.573868 0.411957 0.205769 0.073 Uiso 1 1 calc R U . . . H98C H 0.643273 0.347781 0.184899 0.073 Uiso 1 1 calc R U . . . C99 C 0.72224(9) 0.46974(9) 0.08786(8) 0.0342(3) Uani 1 1 d . . . . . H99A H 0.706243 0.443838 0.065718 0.041 Uiso 1 1 calc R U . . . H99B H 0.681985 0.519786 0.085077 0.041 Uiso 1 1 calc R U . . . C100 C 0.78688(10) 0.48247(10) 0.05094(9) 0.0423(4) Uani 1 1 d . . . . . H10A H 0.772985 0.514374 0.005035 0.063 Uiso 1 1 calc R U . . . H10B H 0.826154 0.433332 0.051316 0.063 Uiso 1 1 calc R U . . . H10C H 0.803261 0.507918 0.072609 0.063 Uiso 1 1 calc R U . . . C101 C 0.95474(10) 0.18072(9) 0.28030(9) 0.0390(4) Uani 1 1 d . . . . . H101 H 0.942223 0.208476 0.313634 0.047 Uiso 1 1 calc R U . . . C102 C 0.96126(11) 0.09930(9) 0.31871(9) 0.0461(4) Uani 1 1 d . . . . . H10D H 0.974705 0.069789 0.287216 0.055 Uiso 1 1 calc R U . . . H10E H 1.000949 0.074588 0.351527 0.055 Uiso 1 1 calc R U . . . C103 C 0.89312(12) 0.09565(10) 0.35448(10) 0.0498(5) Uani 1 1 d . . . . . H10F H 0.854771 0.114903 0.322031 0.075 Uiso 1 1 calc R U . . . H10G H 0.877809 0.126887 0.384131 0.075 Uiso 1 1 calc R U . . . H10H H 0.902593 0.042777 0.380472 0.075 Uiso 1 1 calc R U . . . C104 C 1.02851(11) 0.17848(11) 0.25136(10) 0.0472(4) Uani 1 1 d . . . . . H10I H 1.025844 0.230927 0.236667 0.057 Uiso 1 1 calc R U . . . H10J H 1.065018 0.147632 0.287290 0.057 Uiso 1 1 calc R U . . . C105 C 1.05499(13) 0.14679(14) 0.19385(12) 0.0615(6) Uani 1 1 d . . . . . H10K H 1.021435 0.179054 0.156418 0.092 Uiso 1 1 calc R U . . . H10L H 1.057534 0.094979 0.207309 0.092 Uiso 1 1 calc R U . . . H10M H 1.103165 0.145827 0.180569 0.092 Uiso 1 1 calc R U . . . C106 C 0.89894(9) 0.31373(8) 0.46754(7) 0.0316(3) Uani 1 1 d . . . . . C107 C 0.93797(10) 0.23511(9) 0.49828(8) 0.0370(4) Uani 1 1 d . . . . . C108 C 0.95071(11) 0.20925(9) 0.56627(9) 0.0457(4) Uani 1 1 d . . . . . H108 H 0.978147 0.156610 0.587292 0.055 Uiso 1 1 calc R U . . . C109 C 0.92463(12) 0.25792(10) 0.60380(8) 0.0467(4) Uani 1 1 d . . . . . H109 H 0.935030 0.239207 0.649884 0.056 Uiso 1 1 calc R U . . . C110 C 0.88319(11) 0.33420(9) 0.57388(8) 0.0404(4) Uani 1 1 d . . . . . H110 H 0.863459 0.367331 0.600192 0.048 Uiso 1 1 calc R U . . . C111 C 0.86969(9) 0.36365(9) 0.50574(8) 0.0331(3) Uani 1 1 d . . . . . C112 C 0.96516(10) 0.17907(9) 0.45892(8) 0.0379(4) Uani 1 1 d . . . . . H112 H 0.929885 0.200588 0.421875 0.045 Uiso 1 1 calc R U . . . C113 C 1.03904(10) 0.17069(10) 0.42669(9) 0.0426(4) Uani 1 1 d . . . . . H11A H 1.053749 0.132368 0.403312 0.051 Uiso 1 1 calc R U . . . H11B H 1.033597 0.219837 0.392957 0.051 Uiso 1 1 calc R U . . . C114 C 1.09938(12) 0.14733(13) 0.47409(12) 0.0592(5) Uani 1 1 d . . . . . H11C H 1.143822 0.145156 0.449000 0.089 Uiso 1 1 calc R U . . . H11D H 1.107646 0.097110 0.506061 0.089 Uiso 1 1 calc R U . . . H11E H 1.085580 0.184667 0.497754 0.089 Uiso 1 1 calc R U . . . C115 C 0.96623(11) 0.10035(9) 0.49941(9) 0.0461(4) Uani 1 1 d . . . . . H11F H 0.982688 0.067863 0.470195 0.055 Uiso 1 1 calc R U . . . H11G H 1.002303 0.076571 0.535487 0.055 Uiso 1 1 calc R U . . . C116 C 0.89416(13) 0.10092(11) 0.52983(10) 0.0549(5) Uani 1 1 d . . . . . H11H H 0.857170 0.126865 0.495002 0.082 Uiso 1 1 calc R U . . . H11I H 0.879920 0.127808 0.562889 0.082 Uiso 1 1 calc R U . . . H11J H 0.898986 0.048466 0.551187 0.082 Uiso 1 1 calc R U . . . C117 C 0.82064(9) 0.44683(8) 0.47462(8) 0.0334(3) Uani 1 1 d . . . . . H117 H 0.837273 0.462117 0.427867 0.040 Uiso 1 1 calc R U . . . C118 C 0.74260(10) 0.45514(9) 0.47091(8) 0.0391(4) Uani 1 1 d . . . . . H11K H 0.712889 0.508288 0.444987 0.047 Uiso 1 1 calc R U . . . H11L H 0.743249 0.421825 0.446305 0.047 Uiso 1 1 calc R U . . . C119 C 0.70605(12) 0.43586(11) 0.53718(9) 0.0484(4) Uani 1 1 d . . . . . H11M H 0.659515 0.436524 0.530041 0.073 Uiso 1 1 calc R U . . . H11N H 0.697995 0.473508 0.559166 0.073 Uiso 1 1 calc R U . . . H11O H 0.737036 0.385117 0.565130 0.073 Uiso 1 1 calc R U . . . C120 C 0.82394(11) 0.50140(9) 0.50721(8) 0.0410(4) Uani 1 1 d . . . . . H12A H 0.788733 0.553609 0.484919 0.049 Uiso 1 1 calc R U . . . H12B H 0.809374 0.486838 0.554199 0.049 Uiso 1 1 calc R U . . . C121 C 0.89862(12) 0.50152(10) 0.50409(9) 0.0474(4) Uani 1 1 d . . . . . H12C H 0.912809 0.517488 0.457670 0.071 Uiso 1 1 calc R U . . . H12D H 0.933706 0.450175 0.526684 0.071 Uiso 1 1 calc R U . . . H12E H 0.897442 0.536964 0.525917 0.071 Uiso 1 1 calc R U . . . C122 C 0.64950(10) 0.38523(10) 0.39793(9) 0.0384(4) Uani 1 1 d . . . . . H12F H 0.627250 0.441374 0.386605 0.046 Uiso 1 1 calc R U . . . H12G H 0.655435 0.363349 0.446670 0.046 Uiso 1 1 calc R U . . . C123 C 0.59987(11) 0.35974(12) 0.37545(10) 0.0469(4) Uani 1 1 d . . . . . H12H H 0.589024 0.386618 0.327651 0.056 Uiso 1 1 calc R U . . . H12I H 0.553676 0.373419 0.399990 0.056 Uiso 1 1 calc R U . . . C124 C 0.63445(12) 0.27424(12) 0.38731(11) 0.0543(5) Uani 1 1 d . . . . . H12J H 0.604277 0.260185 0.366623 0.065 Uiso 1 1 calc R U . . . H12K H 0.636959 0.247238 0.435526 0.065 Uiso 1 1 calc R U . . . C125 C 0.71043(12) 0.24981(11) 0.35811(10) 0.0489(5) Uani 1 1 d . . . . . H12L H 0.734342 0.193567 0.371152 0.059 Uiso 1 1 calc R U . . . H12M H 0.707294 0.269790 0.309133 0.059 Uiso 1 1 calc R U . . . C126 C 0.75531(10) 0.27938(9) 0.38246(9) 0.0409(4) Uani 1 1 d . . . . . H12N H 0.762295 0.255655 0.431004 0.049 Uiso 1 1 calc R U . . . H12O H 0.803533 0.265140 0.361299 0.049 Uiso 1 1 calc R U . . . C33 C 0.90813(17) 0.93122(17) 0.19516(12) 0.0318(6) Uani 0.762(4) 1 d D . P B 1 H33 H 0.900315 0.904378 0.167650 0.038 Uiso 0.762(4) 1 calc R U P B 1 C34 C 0.88750(13) 1.01411(12) 0.15143(11) 0.0357(6) Uani 0.762(4) 1 d . . P B 1 H34A H 0.891491 1.043588 0.177813 0.043 Uiso 0.762(4) 1 calc R U P B 1 H34B H 0.922000 1.015752 0.114146 0.043 Uiso 0.762(4) 1 calc R U P B 1 C35 C 0.8117(2) 1.05070(19) 0.12419(18) 0.0443(8) Uani 0.762(4) 1 d . . P B 1 H35A H 0.803955 1.099787 0.090424 0.066 Uiso 0.762(4) 1 calc R U P B 1 H35B H 0.776856 1.058690 0.160172 0.066 Uiso 0.762(4) 1 calc R U P B 1 H35C H 0.805137 1.017409 0.104259 0.066 Uiso 0.762(4) 1 calc R U P B 1 C36 C 0.99008(14) 0.89209(14) 0.21222(12) 0.0353(5) Uani 0.762(4) 1 d . . P B 1 H36A H 1.001781 0.838486 0.239346 0.042 Uiso 0.762(4) 1 calc R U P B 1 H36B H 1.017529 0.891486 0.170346 0.042 Uiso 0.762(4) 1 calc R U P B 1 C37 C 1.01688(15) 0.92721(14) 0.24871(12) 0.0373(6) Uani 0.762(4) 1 d . . P B 1 H37A H 1.006877 0.980037 0.222167 0.056 Uiso 0.762(4) 1 calc R U P B 1 H37B H 1.069111 0.898309 0.256249 0.056 Uiso 0.762(4) 1 calc R U P B 1 H37C H 0.992053 0.926078 0.291404 0.056 Uiso 0.762(4) 1 calc R U P B 1 C70 C 0.29625(17) 0.7329(2) 0.25841(18) 0.0355(9) Uani 0.534(4) 1 d D U P A 1 H70 H 0.332656 0.730568 0.221861 0.043 Uiso 0.534(4) 1 calc R U P A 1 C71 C 0.2833(2) 0.6594(2) 0.2799(2) 0.0377(9) Uani 0.534(4) 1 d . . P A 1 H71A H 0.322026 0.618677 0.311234 0.045 Uiso 0.534(4) 1 calc R U P A 1 H71B H 0.236742 0.668446 0.303843 0.045 Uiso 0.534(4) 1 calc R U P A 1 C72 C 0.2816(2) 0.6317(2) 0.22321(17) 0.0453(10) Uani 0.534(4) 1 d . . P A 1 H72A H 0.242751 0.671133 0.192218 0.068 Uiso 0.534(4) 1 calc R U P A 1 H72B H 0.272754 0.585315 0.240787 0.068 Uiso 0.534(4) 1 calc R U P A 1 H72C H 0.328062 0.620709 0.200042 0.068 Uiso 0.534(4) 1 calc R U P A 1 C73 C 0.2253(2) 0.8023(3) 0.2319(2) 0.0399(9) Uani 0.534(4) 1 d . . P A 1 H73A H 0.211664 0.799846 0.190539 0.048 Uiso 0.534(4) 1 calc R U P A 1 H73B H 0.186552 0.799175 0.264686 0.048 Uiso 0.534(4) 1 calc R U P A 1 C74 C 0.2288(2) 0.8789(3) 0.21767(19) 0.0421(9) Uani 0.534(4) 1 d . . P A 1 H74A H 0.184918 0.919678 0.193897 0.063 Uiso 0.534(4) 1 calc R U P A 1 H74B H 0.271275 0.879770 0.190418 0.063 Uiso 0.534(4) 1 calc R U P A 1 H74C H 0.232311 0.886435 0.259555 0.063 Uiso 0.534(4) 1 calc R U P A 1 C33A C 0.8745(6) 0.9602(5) 0.1882(3) 0.041(2) Uani 0.238(4) 1 d D . P B 2 H33A H 0.892221 0.920784 0.165061 0.049 Uiso 0.238(4) 1 calc R U P B 2 C34A C 0.8118(8) 1.0254(7) 0.1489(6) 0.049(3) Uani 0.238(4) 1 d . . P B 2 H34C H 0.782361 1.003993 0.136407 0.059 Uiso 0.238(4) 1 calc R U P B 2 H34D H 0.831154 1.050527 0.107335 0.059 Uiso 0.238(4) 1 calc R U P B 2 C35A C 0.7615(5) 1.0860(5) 0.1777(5) 0.054(2) Uani 0.238(4) 1 d . . P B 2 H35D H 0.727665 1.127685 0.143428 0.082 Uiso 0.238(4) 1 calc R U P B 2 H35E H 0.789443 1.105393 0.194326 0.082 Uiso 0.238(4) 1 calc R U P B 2 H35F H 0.734490 1.064831 0.214272 0.082 Uiso 0.238(4) 1 calc R U P B 2 C36A C 0.9371(4) 0.9749(4) 0.1943(4) 0.041(2) Uani 0.238(4) 1 d . . P B 2 H36C H 0.920321 1.016369 0.214343 0.049 Uiso 0.238(4) 1 calc R U P B 2 H36D H 0.954410 0.993834 0.149129 0.049 Uiso 0.238(4) 1 calc R U P B 2 C37A C 0.9998(5) 0.9098(6) 0.2338(6) 0.051(2) Uani 0.238(4) 1 d . . P B 2 H37D H 1.014912 0.866512 0.217122 0.076 Uiso 0.238(4) 1 calc R U P B 2 H37E H 0.985855 0.895268 0.280467 0.076 Uiso 0.238(4) 1 calc R U P B 2 H37F H 1.040077 0.924858 0.229901 0.076 Uiso 0.238(4) 1 calc R U P B 2 C70A C 0.2866(2) 0.7814(4) 0.2363(2) 0.0534(13) Uani 0.466(4) 1 d D U P A 2 H70A H 0.317640 0.800248 0.201029 0.064 Uiso 0.466(4) 1 calc R U P A 2 C71A C 0.2863(2) 0.7109(3) 0.2241(2) 0.0583(14) Uani 0.466(4) 1 d . . P A 2 H71C H 0.261823 0.727985 0.181285 0.070 Uiso 0.466(4) 1 calc R U P A 2 H71D H 0.336956 0.675519 0.220048 0.070 Uiso 0.466(4) 1 calc R U P A 2 C72A C 0.2494(4) 0.6675(5) 0.2776(4) 0.072(2) Uani 0.466(4) 1 d . . P A 2 H72D H 0.249579 0.625821 0.264856 0.108 Uiso 0.466(4) 1 calc R U P A 2 H72E H 0.199325 0.702094 0.282754 0.108 Uiso 0.466(4) 1 calc R U P A 2 H72F H 0.275379 0.646768 0.319634 0.108 Uiso 0.466(4) 1 calc R U P A 2 C73A C 0.2106(3) 0.8449(5) 0.2260(3) 0.0599(16) Uani 0.466(4) 1 d . . P A 2 H73C H 0.178652 0.828078 0.260657 0.072 Uiso 0.466(4) 1 calc R U P A 2 H73D H 0.192248 0.852898 0.182577 0.072 Uiso 0.466(4) 1 calc R U P A 2 C74A C 0.2053(3) 0.9208(4) 0.2279(3) 0.0724(17) Uani 0.466(4) 1 d . . P A 2 H74D H 0.238095 0.937230 0.194926 0.109 Uiso 0.466(4) 1 calc R U P A 2 H74E H 0.218934 0.914800 0.272154 0.109 Uiso 0.466(4) 1 calc R U P A 2 H74F H 0.155559 0.959035 0.217970 0.109 Uiso 0.466(4) 1 calc R U P A 2 O4A O 0.4319(6) 0.3015(7) 0.3892(8) 0.112(4) Uani 0.263(4) 1 d D U P C 2 C132 C 0.3780(7) 0.3844(8) 0.3794(8) 0.124(4) Uani 0.263(4) 1 d D U P C 2 H13C H 0.373168 0.396212 0.421308 0.149 Uiso 0.263(4) 1 calc R U P C 2 H13D H 0.396364 0.418906 0.345045 0.149 Uiso 0.263(4) 1 calc R U P C 2 C133 C 0.3073(7) 0.3969(9) 0.3593(10) 0.109(4) Uani 0.263(4) 1 d D U P C 2 H13E H 0.272795 0.448888 0.358873 0.131 Uiso 0.263(4) 1 calc R U P C 2 H13F H 0.311154 0.395502 0.313239 0.131 Uiso 0.263(4) 1 calc R U P C 2 C134 C 0.2767(6) 0.3444(8) 0.3993(7) 0.126(4) Uani 0.263(4) 1 d D U P C 2 H13G H 0.232183 0.354376 0.377761 0.151 Uiso 0.263(4) 1 calc R U P C 2 H13H H 0.263365 0.351956 0.443294 0.151 Uiso 0.263(4) 1 calc R U P C 2 C135 C 0.3282(7) 0.2669(8) 0.4072(7) 0.121(4) Uani 0.263(4) 1 d D U P C 2 H13I H 0.335067 0.257536 0.363950 0.146 Uiso 0.263(4) 1 calc R U P C 2 H13J H 0.308131 0.231772 0.438398 0.146 Uiso 0.263(4) 1 calc R U P C 2 C136 C 0.3990(7) 0.2497(10) 0.4322(9) 0.118(4) Uani 0.263(4) 1 d D U P C 2 H13K H 0.432078 0.196505 0.435133 0.142 Uiso 0.263(4) 1 calc R U P C 2 H13L H 0.393020 0.253981 0.477454 0.142 Uiso 0.263(4) 1 calc R U P C 2 O4 O 0.44338(17) 0.3423(2) 0.33036(16) 0.0985(10) Uani 0.737(4) 1 d D U P C 1 C127 C 0.3898(2) 0.4179(2) 0.3343(2) 0.0768(10) Uani 0.737(4) 1 d D U P C 1 H12P H 0.407351 0.432892 0.365584 0.092 Uiso 0.737(4) 1 calc R U P C 1 H12Q H 0.384268 0.456582 0.290107 0.092 Uiso 0.737(4) 1 calc R U P C 1 C128 C 0.3186(3) 0.4154(3) 0.3568(3) 0.0719(12) Uani 0.737(4) 1 d D U P C 1 H12R H 0.298563 0.405844 0.323096 0.086 Uiso 0.737(4) 1 calc R U P C 1 H12S H 0.284450 0.465022 0.362012 0.086 Uiso 0.737(4) 1 calc R U P C 1 C129 C 0.3266(2) 0.3534(2) 0.42182(19) 0.0817(11) Uani 0.737(4) 1 d D U P C 1 H12T H 0.340267 0.366499 0.456940 0.098 Uiso 0.737(4) 1 calc R U P C 1 H12U H 0.279803 0.349079 0.434155 0.098 Uiso 0.737(4) 1 calc R U P C 1 C130 C 0.3827(3) 0.2798(3) 0.4167(3) 0.1005(17) Uani 0.737(4) 1 d D U P C 1 H13M H 0.366047 0.264000 0.385406 0.121 Uiso 0.737(4) 1 calc R U P C 1 H13N H 0.389568 0.240472 0.460629 0.121 Uiso 0.737(4) 1 calc R U P C 1 C131 C 0.4545(2) 0.2848(3) 0.3930(4) 0.0703(12) Uani 0.737(4) 1 d D U P C 1 H13O H 0.473146 0.297559 0.425343 0.084 Uiso 0.737(4) 1 calc R U P C 1 H13P H 0.490451 0.235232 0.388918 0.084 Uiso 0.737(4) 1 calc R U P C 1 C68A C 0.3737(6) 0.7485(10) 0.4221(5) 0.030(2) Uani 0.466(4) 1 d D U P A 2 H68A H 0.390044 0.750187 0.460562 0.036 Uiso 0.466(4) 1 calc R U P A 2 C67A C 0.3007(6) 0.7687(9) 0.4160(6) 0.037(2) Uani 0.466(4) 1 d D U P A 2 H67A H 0.268380 0.778070 0.451560 0.044 Uiso 0.466(4) 1 calc R U P A 2 C66A C 0.2766(6) 0.7749(5) 0.3573(5) 0.041(2) Uani 0.466(4) 1 d D U P A 2 H66A H 0.226356 0.788898 0.353028 0.049 Uiso 0.466(4) 1 calc R U P A 2 C65A C 0.3209(4) 0.7619(4) 0.3030(3) 0.0425(19) Uani 0.466(4) 1 d D U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ca1 0.02631(14) 0.01890(13) 0.02791(13) -0.00211(10) -0.00560(11) -0.01100(11) Ca2 0.02493(14) 0.02283(14) 0.02967(14) -0.00138(11) -0.00441(11) -0.01210(11) Ca3 0.02841(14) 0.01848(13) 0.02817(14) -0.00211(10) -0.00537(11) -0.01021(11) P1 0.02849(18) 0.02314(17) 0.02665(17) 0.00020(13) -0.00659(14) -0.01248(14) P2 0.02975(19) 0.02323(17) 0.03050(18) -0.00470(14) -0.00612(15) -0.01277(15) P3 0.02787(18) 0.02199(17) 0.02989(18) -0.00396(14) -0.00211(14) -0.01119(14) P4 0.02661(18) 0.01893(16) 0.03155(18) -0.00246(13) -0.00613(14) -0.01022(14) P5 0.02658(18) 0.02118(17) 0.03143(18) -0.00191(14) -0.00325(14) -0.01189(14) P6 0.02702(18) 0.01974(16) 0.03010(18) -0.00027(13) -0.00787(14) -0.01058(14) P7 0.02986(19) 0.02171(17) 0.02640(17) -0.00267(13) -0.00441(14) -0.01136(14) O1 0.0306(6) 0.0263(5) 0.0375(6) -0.0020(4) -0.0116(5) -0.0113(4) O2 0.0303(6) 0.0226(5) 0.0432(6) -0.0018(4) -0.0070(5) -0.0108(4) O3 0.0382(6) 0.0254(5) 0.0395(6) -0.0048(4) 0.0024(5) -0.0183(5) N1 0.0274(6) 0.0220(6) 0.0298(6) -0.0044(5) -0.0032(5) -0.0139(5) N2 0.0331(7) 0.0221(6) 0.0278(6) -0.0036(5) -0.0067(5) -0.0144(5) N3 0.0279(6) 0.0266(6) 0.0317(6) -0.0001(5) -0.0070(5) -0.0139(5) N4 0.0269(6) 0.0339(7) 0.0367(7) -0.0075(5) 0.0009(5) -0.0168(5) N5 0.0328(7) 0.0201(6) 0.0292(6) -0.0039(5) -0.0058(5) -0.0121(5) N6 0.0349(7) 0.0176(5) 0.0279(6) -0.0022(5) -0.0074(5) -0.0082(5) C1 0.0313(8) 0.0301(7) 0.0291(7) -0.0059(6) -0.0046(6) -0.0144(6) C2 0.0306(7) 0.0200(6) 0.0279(7) -0.0019(5) -0.0051(6) -0.0156(6) C3 0.0280(7) 0.0211(7) 0.0300(7) -0.0024(5) -0.0066(6) -0.0124(6) C4 0.0306(7) 0.0187(6) 0.0308(7) -0.0025(5) -0.0045(6) -0.0135(6) C5 0.0383(9) 0.0253(7) 0.0364(8) -0.0098(6) -0.0082(7) -0.0073(6) C6 0.0263(7) 0.0266(7) 0.0309(7) -0.0045(6) -0.0036(6) -0.0121(6) C7 0.0282(8) 0.0283(7) 0.0379(8) -0.0046(6) -0.0022(6) -0.0149(6) C8 0.0347(9) 0.0336(8) 0.0454(9) -0.0061(7) 0.0045(7) -0.0191(7) C9 0.0379(9) 0.0386(9) 0.0425(9) -0.0113(7) 0.0100(7) -0.0175(7) C10 0.0371(9) 0.0314(8) 0.0408(9) -0.0118(7) 0.0044(7) -0.0147(7) C11 0.0288(7) 0.0269(7) 0.0329(7) -0.0055(6) -0.0009(6) -0.0137(6) C12 0.0333(8) 0.0279(8) 0.0424(8) -0.0054(6) -0.0031(7) -0.0180(7) C13 0.0398(9) 0.0380(9) 0.0592(11) -0.0090(8) -0.0041(8) -0.0249(8) C14 0.0359(10) 0.0486(11) 0.0732(13) -0.0125(10) -0.0105(9) -0.0227(8) C15 0.0352(9) 0.0277(8) 0.0478(9) -0.0056(7) -0.0022(7) -0.0172(7) C16 0.0413(10) 0.0337(9) 0.0477(10) -0.0009(7) 0.0012(8) -0.0191(8) C17 0.0313(8) 0.0258(7) 0.0340(7) -0.0095(6) 0.0023(6) -0.0146(6) C18 0.0358(8) 0.0285(8) 0.0390(8) -0.0081(6) -0.0016(7) -0.0149(7) C19 0.0392(10) 0.0398(10) 0.0511(10) -0.0108(8) -0.0048(8) -0.0077(8) C20 0.0385(9) 0.0329(8) 0.0425(9) -0.0163(7) 0.0028(7) -0.0185(7) C21 0.0516(11) 0.0463(10) 0.0483(10) -0.0220(8) -0.0069(8) -0.0204(9) C22 0.0355(8) 0.0218(7) 0.0319(7) -0.0052(6) -0.0103(6) -0.0113(6) C23 0.0312(8) 0.0282(7) 0.0354(8) -0.0092(6) -0.0069(6) -0.0109(6) C24 0.0403(9) 0.0386(9) 0.0379(8) -0.0160(7) -0.0023(7) -0.0163(7) C25 0.0462(10) 0.0366(9) 0.0504(10) -0.0220(8) -0.0072(8) -0.0161(8) C26 0.0530(10) 0.0296(8) 0.0442(9) -0.0094(7) -0.0117(8) -0.0208(8) C27 0.0548(10) 0.0278(8) 0.0332(8) -0.0031(6) -0.0116(7) -0.0219(7) C28 0.0395(9) 0.0365(8) 0.0316(7) -0.0115(6) -0.0017(7) -0.0209(7) C29 0.0503(10) 0.0313(8) 0.0384(8) -0.0080(7) -0.0057(8) -0.0207(8) C30 0.0596(12) 0.0374(9) 0.0507(10) -0.0088(8) -0.0192(9) -0.0187(9) C31 0.0518(11) 0.0575(11) 0.0412(9) -0.0192(8) 0.0073(8) -0.0342(9) C32 0.0412(11) 0.0744(15) 0.0671(13) -0.0322(12) 0.0096(10) -0.0282(10) C38 0.0454(10) 0.0302(8) 0.0646(12) 0.0006(8) -0.0252(9) -0.0203(8) C39 0.0391(10) 0.0528(12) 0.0709(13) 0.0049(10) -0.0137(10) -0.0276(9) C40 0.0350(9) 0.0440(10) 0.0613(12) -0.0069(9) -0.0156(9) -0.0126(8) C41 0.0377(9) 0.0300(8) 0.0443(9) -0.0045(7) -0.0153(7) -0.0090(7) C42 0.0362(9) 0.0337(8) 0.0369(8) 0.0012(7) -0.0117(7) -0.0101(7) C43 0.0409(9) 0.0317(8) 0.0362(8) -0.0050(6) -0.0068(7) -0.0163(7) C44 0.0237(7) 0.0283(7) 0.0350(8) -0.0030(6) -0.0084(6) -0.0116(6) C45 0.0291(7) 0.0236(7) 0.0364(8) -0.0026(6) -0.0068(6) -0.0135(6) C46 0.0277(7) 0.0320(8) 0.0365(8) -0.0020(6) -0.0042(6) -0.0184(6) C47 0.0525(11) 0.0402(9) 0.0403(9) -0.0050(7) 0.0033(8) -0.0315(8) C48 0.0330(8) 0.0270(7) 0.0323(8) 0.0003(6) -0.0101(6) -0.0136(6) C49 0.0318(8) 0.0291(8) 0.0336(8) -0.0018(6) -0.0093(6) -0.0139(6) C50 0.0367(9) 0.0392(9) 0.0340(8) 0.0015(7) -0.0094(7) -0.0190(7) C51 0.0436(10) 0.0426(9) 0.0352(8) 0.0061(7) -0.0171(7) -0.0205(8) C52 0.0369(9) 0.0422(9) 0.0439(9) 0.0055(7) -0.0193(8) -0.0189(8) C53 0.0350(9) 0.0335(8) 0.0419(9) 0.0046(7) -0.0142(7) -0.0179(7) C54 0.0318(8) 0.0309(8) 0.0294(7) 0.0024(6) -0.0094(6) -0.0159(6) C55 0.0322(8) 0.0323(8) 0.0355(8) -0.0010(6) -0.0090(6) -0.0158(7) C56 0.0369(9) 0.0321(8) 0.0454(9) 0.0005(7) -0.0093(7) -0.0158(7) C57 0.0345(8) 0.0377(9) 0.0350(8) -0.0023(7) -0.0074(7) -0.0149(7) C58 0.0448(10) 0.0509(11) 0.0545(11) -0.0188(9) -0.0019(9) -0.0184(9) C59 0.0344(9) 0.0446(10) 0.0478(10) 0.0098(8) -0.0156(8) -0.0217(8) C60 0.0351(9) 0.0490(10) 0.0490(10) 0.0043(8) -0.0123(8) -0.0225(8) C61 0.0390(10) 0.0527(11) 0.0592(12) -0.0033(9) -0.0096(9) -0.0219(9) C62 0.0405(10) 0.0426(10) 0.0811(15) 0.0132(10) -0.0213(10) -0.0239(9) C63 0.094(2) 0.0518(13) 0.106(2) 0.0063(13) -0.0549(17) -0.0390(14) C64 0.0324(8) 0.0357(8) 0.0393(8) -0.0080(7) 0.0038(7) -0.0181(7) C65 0.033(2) 0.031(3) 0.037(2) -0.001(2) -0.0004(18) -0.018(2) C66 0.034(2) 0.028(4) 0.043(3) 0.000(3) 0.006(2) -0.018(3) C67 0.038(3) 0.024(5) 0.039(3) 0.003(3) 0.004(2) -0.009(3) C68 0.043(4) 0.027(6) 0.042(4) 0.004(3) -0.003(2) -0.010(3) C69 0.0327(8) 0.0283(8) 0.0354(8) -0.0014(6) 0.0020(7) -0.0123(6) C75 0.0321(8) 0.0414(9) 0.0315(8) -0.0054(7) 0.0002(7) -0.0114(7) C76 0.0394(9) 0.0507(11) 0.0385(9) -0.0062(8) 0.0014(7) -0.0217(8) C77 0.0540(12) 0.0569(12) 0.0480(10) -0.0139(9) 0.0053(9) -0.0309(10) C78 0.0389(9) 0.0477(10) 0.0342(8) -0.0053(7) -0.0033(7) -0.0116(8) C79 0.0587(13) 0.0400(10) 0.0415(10) -0.0020(8) -0.0041(9) -0.0076(9) C80 0.0313(8) 0.0299(8) 0.0534(10) 0.0021(7) -0.0104(8) -0.0099(7) C81 0.0417(11) 0.0370(10) 0.0736(14) -0.0079(9) 0.0096(10) -0.0110(8) C82 0.0666(14) 0.0339(10) 0.0692(14) -0.0171(9) 0.0193(11) -0.0166(9) C83 0.0741(14) 0.0334(9) 0.0480(10) -0.0074(8) -0.0015(10) -0.0285(9) C84 0.0398(9) 0.0248(7) 0.0492(9) -0.0024(7) -0.0081(8) -0.0151(7) C85 0.0377(8) 0.0300(8) 0.0313(7) -0.0087(6) -0.0006(6) -0.0169(7) C86 0.0306(7) 0.0172(6) 0.0304(7) -0.0027(5) -0.0050(6) -0.0089(6) C87 0.0284(7) 0.0216(7) 0.0325(7) -0.0038(6) -0.0037(6) -0.0117(6) C88 0.0309(8) 0.0166(6) 0.0333(7) -0.0043(5) -0.0092(6) -0.0058(6) C89 0.0375(9) 0.0311(8) 0.0369(8) -0.0069(6) -0.0108(7) -0.0139(7) C90 0.0347(8) 0.0224(7) 0.0296(7) -0.0054(6) -0.0008(6) -0.0154(6) C91 0.0329(8) 0.0247(7) 0.0304(7) -0.0056(6) -0.0008(6) -0.0160(6) C92 0.0377(9) 0.0311(8) 0.0370(8) -0.0085(6) -0.0040(7) -0.0183(7) C93 0.0486(10) 0.0309(8) 0.0440(9) -0.0140(7) -0.0021(8) -0.0218(7) C94 0.0473(10) 0.0240(7) 0.0451(9) -0.0099(7) -0.0064(8) -0.0130(7) C95 0.0411(9) 0.0240(7) 0.0362(8) -0.0060(6) -0.0045(7) -0.0144(7) C96 0.0311(8) 0.0251(7) 0.0348(8) -0.0071(6) -0.0062(6) -0.0132(6) C97 0.0334(8) 0.0358(8) 0.0405(8) -0.0111(7) -0.0015(7) -0.0161(7) C98 0.0392(10) 0.0574(12) 0.0576(11) -0.0197(9) 0.0015(8) -0.0272(9) C99 0.0379(9) 0.0282(8) 0.0362(8) -0.0065(6) -0.0083(7) -0.0134(7) C100 0.0460(10) 0.0331(9) 0.0396(9) -0.0017(7) -0.0024(8) -0.0155(8) C101 0.0476(10) 0.0222(7) 0.0431(9) -0.0063(7) -0.0128(8) -0.0097(7) C102 0.0633(12) 0.0231(8) 0.0459(10) -0.0059(7) -0.0173(9) -0.0108(8) C103 0.0725(14) 0.0305(9) 0.0473(10) -0.0032(7) -0.0144(9) -0.0243(9) C104 0.0469(10) 0.0338(9) 0.0530(11) -0.0108(8) -0.0125(9) -0.0077(8) C105 0.0530(12) 0.0616(13) 0.0636(13) -0.0259(11) -0.0042(10) -0.0116(10) C106 0.0386(8) 0.0242(7) 0.0281(7) -0.0020(6) -0.0079(6) -0.0117(6) C107 0.0462(10) 0.0231(7) 0.0338(8) -0.0026(6) -0.0105(7) -0.0086(7) C108 0.0646(12) 0.0227(8) 0.0352(9) 0.0009(6) -0.0165(8) -0.0072(8) C109 0.0701(13) 0.0303(8) 0.0292(8) 0.0005(7) -0.0156(8) -0.0138(8) C110 0.0583(11) 0.0284(8) 0.0290(8) -0.0047(6) -0.0074(7) -0.0139(8) C111 0.0423(9) 0.0230(7) 0.0294(7) -0.0022(6) -0.0068(7) -0.0116(7) C112 0.0480(10) 0.0213(7) 0.0352(8) -0.0028(6) -0.0127(7) -0.0067(7) C113 0.0472(10) 0.0293(8) 0.0449(9) -0.0103(7) -0.0141(8) -0.0064(7) C114 0.0522(12) 0.0552(12) 0.0636(13) -0.0219(10) -0.0206(10) -0.0071(10) C115 0.0623(12) 0.0209(8) 0.0435(9) -0.0019(7) -0.0140(9) -0.0085(8) C116 0.0756(15) 0.0279(9) 0.0506(11) -0.0034(8) -0.0013(10) -0.0180(9) C117 0.0447(9) 0.0218(7) 0.0271(7) -0.0019(6) -0.0072(6) -0.0098(7) C118 0.0451(10) 0.0300(8) 0.0341(8) -0.0044(6) -0.0061(7) -0.0104(7) C119 0.0545(12) 0.0450(10) 0.0410(9) -0.0082(8) 0.0003(8) -0.0202(9) C120 0.0612(11) 0.0229(7) 0.0326(8) -0.0045(6) -0.0078(8) -0.0124(7) C121 0.0693(13) 0.0335(9) 0.0423(9) -0.0074(7) -0.0150(9) -0.0224(9) C122 0.0428(9) 0.0358(9) 0.0396(9) -0.0114(7) 0.0082(7) -0.0215(7) C123 0.0462(10) 0.0565(11) 0.0500(10) -0.0207(9) 0.0134(8) -0.0326(9) C124 0.0695(14) 0.0602(12) 0.0579(12) -0.0279(10) 0.0226(10) -0.0484(11) C125 0.0654(13) 0.0414(10) 0.0525(11) -0.0185(8) 0.0150(9) -0.0349(10) C126 0.0503(10) 0.0258(8) 0.0432(9) -0.0048(7) 0.0042(8) -0.0184(7) C33 0.0515(16) 0.0220(14) 0.0273(11) -0.0004(10) -0.0079(11) -0.0231(12) C34 0.0493(14) 0.0291(11) 0.0341(11) -0.0047(9) -0.0077(9) -0.0224(10) C35 0.0550(17) 0.0336(18) 0.046(2) -0.0070(14) -0.0180(17) -0.0183(15) C36 0.0428(14) 0.0282(11) 0.0377(12) -0.0104(9) -0.0010(10) -0.0166(10) C37 0.0396(14) 0.0320(12) 0.0412(13) -0.0095(10) -0.0065(10) -0.0148(10) C70 0.0256(16) 0.0324(19) 0.0403(19) 0.0001(15) -0.0005(13) -0.0130(14) C71 0.034(2) 0.0371(18) 0.0368(18) -0.0022(13) -0.0032(18) -0.0161(18) C72 0.047(2) 0.047(2) 0.0434(18) 0.0000(15) -0.0077(15) -0.0296(16) C73 0.030(2) 0.037(2) 0.0457(19) -0.0012(19) -0.0036(15) -0.0146(19) C74 0.038(2) 0.035(2) 0.0421(19) -0.0014(17) -0.0025(16) -0.012(2) C33A 0.065(7) 0.016(4) 0.037(4) 0.002(3) -0.023(4) -0.013(4) C34A 0.060(6) 0.041(7) 0.044(6) -0.006(5) 0.000(6) -0.025(6) C35A 0.047(5) 0.037(4) 0.065(5) 0.001(4) -0.020(4) -0.011(4) C36A 0.035(4) 0.035(4) 0.055(5) -0.009(3) -0.001(3) -0.019(3) C37A 0.044(5) 0.056(6) 0.075(7) -0.034(5) -0.006(5) -0.029(4) C70A 0.029(2) 0.071(4) 0.047(2) -0.003(2) -0.0091(18) -0.017(2) C71A 0.041(2) 0.089(4) 0.048(3) -0.019(3) -0.0076(19) -0.029(2) C72A 0.061(4) 0.106(5) 0.068(4) -0.026(3) 0.002(4) -0.054(4) C73A 0.037(3) 0.071(5) 0.060(3) 0.000(4) -0.011(2) -0.024(4) C74A 0.049(3) 0.066(4) 0.079(4) 0.002(3) -0.014(3) -0.018(3) O4A 0.102(7) 0.113(6) 0.060(5) -0.014(5) -0.010(6) 0.004(5) C132 0.128(7) 0.115(6) 0.091(7) -0.029(6) -0.026(6) -0.009(6) C133 0.104(7) 0.103(7) 0.068(6) -0.037(6) -0.014(6) 0.016(6) C134 0.113(7) 0.128(7) 0.084(7) -0.037(6) -0.015(6) 0.007(6) C135 0.115(7) 0.125(7) 0.080(6) -0.030(6) -0.014(6) -0.007(6) C136 0.108(7) 0.118(8) 0.085(8) -0.026(7) -0.019(6) -0.006(6) O4 0.096(2) 0.126(3) 0.097(2) -0.0540(19) 0.0164(17) -0.0570(19) C127 0.096(3) 0.075(2) 0.070(2) -0.0193(19) -0.005(2) -0.046(2) C128 0.077(3) 0.058(2) 0.074(3) -0.0270(19) -0.027(2) -0.0083(19) C129 0.072(2) 0.091(3) 0.074(2) -0.028(2) 0.0083(19) -0.027(2) C130 0.119(4) 0.073(3) 0.077(3) 0.003(2) -0.001(3) -0.029(3) C131 0.052(2) 0.061(2) 0.071(3) -0.017(2) -0.009(2) 0.0010(18) C68A 0.030(3) 0.022(5) 0.020(2) 0.004(3) 0.002(2) -0.004(2) C67A 0.033(3) 0.020(5) 0.036(3) 0.004(3) 0.008(2) -0.003(3) C66A 0.035(3) 0.035(5) 0.045(4) 0.002(3) 0.004(2) -0.019(3) C65A 0.032(3) 0.049(5) 0.043(3) -0.001(3) 0.004(2) -0.024(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ca Ca 0.3641 1.2855 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 8 13 3 0.1153 -1 -2 0 0.1353 -7 3 11 0.0792 1 0 -1 0.0657 -11 -3 6 0.0765 -10 -11 -8 0.0940 11 11 8 0.0846 0 11 10 0.0777 -12 0 -1 0.1164 2 1 -13 0.1004 -3 -5 11 0.1051 1 0 13 0.1146 1 1 0 0.0975 11 0 -4 0.0947 1 -2 -2 0.1031 2 -2 -1 0.1141 1 -2 0 0.1223 9 -4 3 0.1373 1 6 14 0.0827 -7 -2 10 0.0672 -12 -9 1 0.0751 -8 4 -6 0.1280 -6 -10 -12 0.0997 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag P1 Ca1 P3 39.400(10) . . ? P4 Ca1 P1 39.033(10) . . ? P4 Ca1 P3 65.582(11) . . ? P6 Ca1 P1 65.634(11) . . ? P6 Ca1 P3 38.671(10) . . ? P6 Ca1 P4 65.719(11) . . ? O1 Ca1 P1 145.80(3) . . ? O1 Ca1 P3 106.48(3) . . ? O1 Ca1 P4 146.53(3) . . ? O1 Ca1 P6 87.71(3) . . ? O1 Ca1 N1 90.50(4) . . ? O1 Ca1 C2 118.07(4) . . ? O1 Ca1 C3 135.02(4) . . ? O1 Ca1 C4 121.99(4) . . ? N1 Ca1 P1 96.38(3) . . ? N1 Ca1 P3 104.63(3) . . ? N1 Ca1 P4 122.87(3) . . ? N1 Ca1 P6 139.64(3) . . ? N1 Ca1 C2 28.37(4) . . ? N1 Ca1 C3 55.41(4) . . ? N1 Ca1 C4 74.34(4) . . ? N2 Ca1 P1 119.06(3) . . ? N2 Ca1 P3 157.31(3) . . ? N2 Ca1 P4 92.49(3) . . ? N2 Ca1 P6 138.52(3) . . ? N2 Ca1 O1 95.05(4) . . ? N2 Ca1 N1 81.81(4) . . ? N2 Ca1 C2 74.24(4) . . ? N2 Ca1 C3 55.59(4) . . ? N2 Ca1 C4 28.54(4) . . ? C2 Ca1 P1 76.92(3) . . ? C2 Ca1 P3 100.91(3) . . ? C2 Ca1 P4 95.37(3) . . ? C2 Ca1 P6 139.06(3) . . ? C3 Ca1 P1 73.58(3) . . ? C3 Ca1 P3 109.84(3) . . ? C3 Ca1 P4 74.68(3) . . ? C3 Ca1 P6 137.19(3) . . ? C3 Ca1 C2 29.45(4) . . ? C3 Ca1 C4 29.59(4) . . ? C4 Ca1 P1 92.06(3) . . ? C4 Ca1 P3 131.45(3) . . ? C4 Ca1 P4 74.68(3) . . ? C4 Ca1 P6 138.09(3) . . ? C4 Ca1 C2 55.37(4) . . ? P2 Ca2 P1 39.011(9) . . ? P4 Ca2 P1 38.350(10) . . ? P4 Ca2 P2 65.555(11) . . ? P5 Ca2 P1 65.521(11) . . ? P5 Ca2 P2 39.172(10) . . ? P5 Ca2 P4 66.411(11) . . ? O2 Ca2 P1 109.05(3) . . ? O2 Ca2 P2 148.06(3) . . ? O2 Ca2 P4 87.95(3) . . ? O2 Ca2 P5 144.88(3) . . ? O2 Ca2 N3 91.12(4) . . ? O2 Ca2 N4 92.89(4) . . ? O2 Ca2 C44 117.98(4) . . ? O2 Ca2 C45 133.52(4) . . ? O2 Ca2 C46 119.66(4) . . ? N3 Ca2 P1 103.01(3) . . ? N3 Ca2 P2 96.35(3) . . ? N3 Ca2 P4 136.78(3) . . ? N3 Ca2 P5 123.99(3) . . ? N3 Ca2 C44 28.07(4) . . ? N3 Ca2 C45 55.04(4) . . ? N3 Ca2 C46 73.85(4) . . ? N4 Ca2 P1 157.41(3) . . ? N4 Ca2 P2 118.91(3) . . ? N4 Ca2 P4 141.95(3) . . ? N4 Ca2 P5 93.50(3) . . ? N4 Ca2 N3 81.26(4) . . ? N4 Ca2 C44 73.46(5) . . ? N4 Ca2 C45 54.94(5) . . ? N4 Ca2 C46 28.19(5) . . ? C44 Ca2 P1 99.73(3) . . ? C44 Ca2 P2 77.30(3) . . ? C44 Ca2 P4 137.92(3) . . ? C44 Ca2 P5 96.92(3) . . ? C45 Ca2 P1 109.12(3) . . ? C45 Ca2 P2 73.96(3) . . ? C45 Ca2 P4 138.40(3) . . ? C45 Ca2 P5 76.46(3) . . ? C45 Ca2 C44 29.28(4) . . ? C45 Ca2 C46 29.29(5) . . ? C46 Ca2 P1 131.15(4) . . ? C46 Ca2 P2 92.21(3) . . ? C46 Ca2 P4 141.16(3) . . ? C46 Ca2 P5 76.26(3) . . ? C46 Ca2 C44 54.91(5) . . ? P3 Ca3 P2 38.658(10) . . ? P5 Ca3 P2 37.959(10) . . ? P5 Ca3 P3 65.208(11) . . ? P6 Ca3 P2 65.141(10) . . ? P6 Ca3 P3 39.042(10) . . ? P6 Ca3 P5 66.470(11) . . ? O3 Ca3 P2 109.31(3) . . ? O3 Ca3 P3 147.75(3) . . ? O3 Ca3 P5 90.35(3) . . ? O3 Ca3 P6 149.01(3) . . ? O3 Ca3 N5 89.57(4) . . ? O3 Ca3 N6 91.65(4) . . ? O3 Ca3 C86 116.69(4) . . ? O3 Ca3 C87 131.61(4) . . ? O3 Ca3 C88 117.77(4) . . ? N5 Ca3 P2 101.47(3) . . ? N5 Ca3 P3 93.81(3) . . ? N5 Ca3 P5 135.57(3) . . ? N5 Ca3 P6 121.31(3) . . ? N5 Ca3 N6 81.20(4) . . ? N5 Ca3 C86 28.35(4) . . ? N5 Ca3 C87 54.87(4) . . ? N5 Ca3 C88 73.49(4) . . ? N6 Ca3 P2 158.80(3) . . ? N6 Ca3 P3 120.57(3) . . ? N6 Ca3 P5 143.20(3) . . ? N6 Ca3 P6 95.31(3) . . ? N6 Ca3 C86 73.76(4) . . ? N6 Ca3 C87 54.99(4) . . ? N6 Ca3 C88 27.86(4) . . ? C86 Ca3 P2 98.49(3) . . ? C86 Ca3 P3 75.15(3) . . ? C86 Ca3 P5 136.15(3) . . ? C86 Ca3 P6 94.22(3) . . ? C86 Ca3 C87 29.10(4) . . ? C86 Ca3 C88 54.92(4) . . ? C87 Ca3 P2 109.25(3) . . ? C87 Ca3 P3 73.94(3) . . ? C87 Ca3 P5 137.77(3) . . ? C87 Ca3 P6 75.35(3) . . ? C87 Ca3 C88 29.45(4) . . ? C88 Ca3 P2 132.45(3) . . ? C88 Ca3 P3 93.84(3) . . ? C88 Ca3 P5 142.03(3) . . ? C88 Ca3 P6 77.35(3) . . ? Ca1 P1 Ca2 128.214(14) . . ? P2 P1 Ca1 125.655(17) . . ? P2 P1 Ca2 68.510(15) . . ? P2 P1 P3 60.006(16) . . ? P3 P1 Ca1 71.610(14) . . ? P3 P1 Ca2 122.255(17) . . ? P4 P1 Ca1 65.258(14) . . ? P4 P1 Ca2 62.961(14) . . ? P4 P1 P2 104.39(2) . . ? P4 P1 P3 105.71(2) . . ? Ca2 P2 Ca3 125.966(14) . . ? P1 P2 Ca2 72.479(15) . . ? P1 P2 Ca3 121.607(17) . . ? P1 P2 P3 60.140(16) . . ? P3 P2 Ca2 125.855(17) . . ? P3 P2 Ca3 68.102(14) . . ? P5 P2 Ca2 63.965(15) . . ? P5 P2 Ca3 62.017(14) . . ? P5 P2 P1 105.84(2) . . ? P5 P2 P3 104.11(2) . . ? Ca3 P3 Ca1 126.440(13) . . ? P1 P3 Ca1 68.990(14) . . ? P1 P3 Ca3 125.841(18) . . ? P2 P3 Ca1 123.189(17) . . ? P2 P3 Ca3 73.240(15) . . ? P2 P3 P1 59.854(16) . . ? P6 P3 Ca1 63.440(14) . . ? P6 P3 Ca3 63.007(14) . . ? P6 P3 P1 103.96(2) . . ? P6 P3 P2 105.82(2) . . ? Ca2 P4 Ca1 154.386(15) . . ? P1 P4 Ca1 75.708(16) . . ? P1 P4 Ca2 78.689(15) . . ? P1 P4 P7 99.487(19) . . ? P7 P4 Ca1 92.296(17) . . ? P7 P4 Ca2 91.151(16) . . ? Ca2 P5 Ca3 156.847(16) . . ? P2 P5 Ca2 76.862(16) . . ? P2 P5 Ca3 80.024(16) . . ? P2 P5 P7 99.37(2) . . ? P7 P5 Ca2 91.687(16) . . ? P7 P5 Ca3 90.737(16) . . ? Ca3 P6 Ca1 155.824(15) . . ? P3 P6 Ca1 77.889(15) . . ? P3 P6 Ca3 77.951(15) . . ? P3 P6 P7 99.53(2) . . ? P7 P6 Ca1 92.793(16) . . ? P7 P6 Ca3 92.045(16) . . ? P4 P7 P5 101.52(2) . . ? P4 P7 P6 101.01(2) . . ? P6 P7 P5 100.97(2) . . ? C38 O1 Ca1 117.43(9) . . ? C38 O1 C42 110.65(12) . . ? C42 O1 Ca1 130.75(10) . . ? C80 O2 Ca2 115.46(9) . . ? C80 O2 C84 111.59(12) . . ? C84 O2 Ca2 131.95(9) . . ? C122 O3 Ca3 130.21(9) . . ? C122 O3 C126 111.75(12) . . ? C126 O3 Ca3 116.34(10) . . ? C2 N1 Ca1 92.01(9) . . ? C2 N1 C6 115.78(12) . . ? C6 N1 Ca1 143.47(9) . . ? C4 N2 Ca1 92.62(8) . . ? C4 N2 C22 115.87(12) . . ? C22 N2 Ca1 142.47(9) . . ? C44 N3 Ca2 93.55(9) . . ? C44 N3 C48 116.90(13) . . ? C48 N3 Ca2 142.55(10) . . ? C46 N4 Ca2 92.76(9) . . ? C46 N4 C64 118.96(13) . . ? C64 N4 Ca2 139.50(10) . . ? C86 N5 Ca3 93.40(9) . . ? C86 N5 C90 118.85(13) . . ? C90 N5 Ca3 141.68(10) . . ? C88 N6 Ca3 93.98(9) . . ? C88 N6 C106 117.33(13) . . ? C106 N6 Ca3 138.47(10) . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? N1 C2 Ca1 59.63(7) . . ? N1 C2 C1 120.30(13) . . ? N1 C2 C3 124.57(13) . . ? C1 C2 Ca1 144.79(9) . . ? C3 C2 Ca1 74.18(8) . . ? C3 C2 C1 115.06(13) . . ? Ca1 C3 H3 138.2(11) . . ? C2 C3 Ca1 76.37(8) . . ? C2 C3 H3 112.4(11) . . ? C2 C3 C4 132.31(14) . . ? C4 C3 Ca1 75.48(8) . . ? C4 C3 H3 114.3(11) . . ? N2 C4 Ca1 58.85(7) . . ? N2 C4 C3 124.17(14) . . ? N2 C4 C5 121.00(13) . . ? C3 C4 Ca1 74.92(8) . . ? C3 C4 C5 114.71(13) . . ? C5 C4 Ca1 143.27(10) . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5B 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C7 C6 N1 118.99(13) . . ? C11 C6 N1 121.35(13) . . ? C11 C6 C7 119.65(14) . . ? C6 C7 C12 121.94(14) . . ? C8 C7 C6 118.65(14) . . ? C8 C7 C12 119.41(14) . . ? C7 C8 H8 119.1 . . ? C9 C8 C7 121.85(15) . . ? C9 C8 H8 119.1 . . ? C8 C9 H9 120.4 . . ? C8 C9 C10 119.17(16) . . ? C10 C9 H9 120.4 . . ? C9 C10 H10 119.2 . . ? C9 C10 C11 121.56(15) . . ? C11 C10 H10 119.2 . . ? C6 C11 C17 121.54(13) . . ? C10 C11 C6 118.99(14) . . ? C10 C11 C17 119.44(14) . . ? C7 C12 H12 106.8 . . ? C7 C12 C13 112.19(14) . . ? C7 C12 C15 113.87(13) . . ? C13 C12 H12 106.8 . . ? C15 C12 H12 106.8 . . ? C15 C12 C13 109.92(13) . . ? C12 C13 H13A 108.7 . . ? C12 C13 H13B 108.7 . . ? H13A C13 H13B 107.6 . . ? C14 C13 C12 114.05(15) . . ? C14 C13 H13A 108.7 . . ? C14 C13 H13B 108.7 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C12 C15 H15A 108.5 . . ? C12 C15 H15B 108.5 . . ? H15A C15 H15B 107.5 . . ? C16 C15 C12 114.97(15) . . ? C16 C15 H15A 108.5 . . ? C16 C15 H15B 108.5 . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C11 C17 H17 106.8 . . ? C11 C17 C18 110.04(13) . . ? C11 C17 C20 114.86(13) . . ? C18 C17 H17 106.8 . . ? C20 C17 H17 106.8 . . ? C20 C17 C18 111.16(13) . . ? C17 C18 H18A 108.3 . . ? C17 C18 H18B 108.3 . . ? H18A C18 H18B 107.4 . . ? C19 C18 C17 115.78(14) . . ? C19 C18 H18A 108.3 . . ? C19 C18 H18B 108.3 . . ? C18 C19 H19A 109.5 . . ? C18 C19 H19B 109.5 . . ? C18 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C17 C20 H20A 108.8 . . ? C17 C20 H20B 108.8 . . ? H20A C20 H20B 107.7 . . ? C21 C20 C17 113.70(14) . . ? C21 C20 H20A 108.8 . . ? C21 C20 H20B 108.8 . . ? C20 C21 H21A 109.5 . . ? C20 C21 H21B 109.5 . . ? C20 C21 H21C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C23 C22 N2 121.17(13) . . ? C23 C22 C27 120.36(14) . . ? C27 C22 N2 118.47(14) . . ? C22 C23 C28 120.82(13) . . ? C24 C23 C22 118.27(15) . . ? C24 C23 C28 120.87(15) . . ? C23 C24 H24 119.2 . . ? C25 C24 C23 121.67(16) . . ? C25 C24 H24 119.2 . . ? C24 C25 H25 120.3 . . ? C26 C25 C24 119.49(15) . . ? C26 C25 H25 120.3 . . ? C25 C26 H26 119.4 . . ? C25 C26 C27 121.29(16) . . ? C27 C26 H26 119.4 . . ? C22 C27 C33 120.68(16) . . ? C22 C27 C33A 123.9(4) . . ? C26 C27 C22 118.58(16) . . ? C26 C27 C33 120.28(16) . . ? C26 C27 C33A 114.0(4) . . ? C23 C28 H28 106.6 . . ? C23 C28 C29 109.49(13) . . ? C23 C28 C31 114.66(14) . . ? C29 C28 H28 106.6 . . ? C31 C28 H28 106.6 . . ? C31 C28 C29 112.41(14) . . ? C28 C29 H29A 108.4 . . ? C28 C29 H29B 108.4 . . ? H29A C29 H29B 107.5 . . ? C30 C29 C28 115.36(14) . . ? C30 C29 H29A 108.4 . . ? C30 C29 H29B 108.4 . . ? C29 C30 H30A 109.5 . . ? C29 C30 H30B 109.5 . . ? C29 C30 H30C 109.5 . . ? H30A C30 H30B 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C28 C31 H31A 108.9 . . ? C28 C31 H31B 108.9 . . ? H31A C31 H31B 107.7 . . ? C32 C31 C28 113.32(16) . . ? C32 C31 H31A 108.9 . . ? C32 C31 H31B 108.9 . . ? C31 C32 H32A 109.5 . . ? C31 C32 H32B 109.5 . . ? C31 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? O1 C38 H38A 109.5 . . ? O1 C38 H38B 109.5 . . ? O1 C38 C39 110.81(14) . . ? H38A C38 H38B 108.1 . . ? C39 C38 H38A 109.5 . . ? C39 C38 H38B 109.5 . . ? C38 C39 H39A 109.6 . . ? C38 C39 H39B 109.6 . . ? C38 C39 C40 110.48(18) . . ? H39A C39 H39B 108.1 . . ? C40 C39 H39A 109.6 . . ? C40 C39 H39B 109.6 . . ? C39 C40 H40A 109.7 . . ? C39 C40 H40B 109.7 . . ? H40A C40 H40B 108.2 . . ? C41 C40 C39 109.97(15) . . ? C41 C40 H40A 109.7 . . ? C41 C40 H40B 109.7 . . ? C40 C41 H41A 109.4 . . ? C40 C41 H41B 109.4 . . ? H41A C41 H41B 108.0 . . ? C42 C41 C40 111.19(15) . . ? C42 C41 H41A 109.4 . . ? C42 C41 H41B 109.4 . . ? O1 C42 C41 111.42(14) . . ? O1 C42 H42A 109.3 . . ? O1 C42 H42B 109.3 . . ? C41 C42 H42A 109.3 . . ? C41 C42 H42B 109.3 . . ? H42A C42 H42B 108.0 . . ? H43A C43 H43B 109.5 . . ? H43A C43 H43C 109.5 . . ? H43B C43 H43C 109.5 . . ? C44 C43 H43A 109.5 . . ? C44 C43 H43B 109.5 . . ? C44 C43 H43C 109.5 . . ? N3 C44 Ca2 58.38(8) . . ? N3 C44 C43 120.90(14) . . ? N3 C44 C45 123.98(14) . . ? C43 C44 Ca2 145.25(11) . . ? C45 C44 Ca2 74.37(9) . . ? C45 C44 C43 115.03(13) . . ? Ca2 C45 H45 139.3(10) . . ? C44 C45 Ca2 76.35(9) . . ? C44 C45 H45 114.0(10) . . ? C46 C45 Ca2 75.49(9) . . ? C46 C45 C44 132.17(15) . . ? C46 C45 H45 112.7(10) . . ? N4 C46 Ca2 59.05(8) . . ? N4 C46 C45 124.44(14) . . ? N4 C46 C47 121.47(15) . . ? C45 C46 Ca2 75.22(8) . . ? C45 C46 C47 113.93(14) . . ? C47 C46 Ca2 142.35(11) . . ? C46 C47 H47A 109.5 . . ? C46 C47 H47B 109.5 . . ? C46 C47 H47C 109.5 . . ? H47A C47 H47B 109.5 . . ? H47A C47 H47C 109.5 . . ? H47B C47 H47C 109.5 . . ? C49 C48 N3 121.65(13) . . ? C49 C48 C53 120.02(14) . . ? C53 C48 N3 118.33(14) . . ? C48 C49 C54 121.35(14) . . ? C50 C49 C48 118.89(14) . . ? C50 C49 C54 119.69(14) . . ? C49 C50 H50 119.3 . . ? C51 C50 C49 121.31(16) . . ? C51 C50 H50 119.3 . . ? C50 C51 H51 120.3 . . ? C52 C51 C50 119.36(16) . . ? C52 C51 H51 120.3 . . ? C51 C52 H52 119.0 . . ? C51 C52 C53 121.96(16) . . ? C53 C52 H52 119.0 . . ? C48 C53 C59 121.71(15) . . ? C52 C53 C48 118.36(16) . . ? C52 C53 C59 119.92(15) . . ? C49 C54 H54 106.5 . . ? C49 C54 C55 109.70(13) . . ? C49 C54 C57 114.75(13) . . ? C55 C54 H54 106.5 . . ? C57 C54 H54 106.5 . . ? C57 C54 C55 112.43(13) . . ? C54 C55 H55A 108.3 . . ? C54 C55 H55B 108.3 . . ? H55A C55 H55B 107.4 . . ? C56 C55 C54 115.91(14) . . ? C56 C55 H55A 108.3 . . ? C56 C55 H55B 108.3 . . ? C55 C56 H56A 109.5 . . ? C55 C56 H56B 109.5 . . ? C55 C56 H56C 109.5 . . ? H56A C56 H56B 109.5 . . ? H56A C56 H56C 109.5 . . ? H56B C56 H56C 109.5 . . ? C54 C57 H57A 109.0 . . ? C54 C57 H57B 109.0 . . ? H57A C57 H57B 107.8 . . ? C58 C57 C54 112.95(15) . . ? C58 C57 H57A 109.0 . . ? C58 C57 H57B 109.0 . . ? C57 C58 H58A 109.5 . . ? C57 C58 H58B 109.5 . . ? C57 C58 H58C 109.5 . . ? H58A C58 H58B 109.5 . . ? H58A C58 H58C 109.5 . . ? H58B C58 H58C 109.5 . . ? C53 C59 H59 106.4 . . ? C53 C59 C60 112.48(14) . . ? C53 C59 C62 113.45(18) . . ? C60 C59 H59 106.4 . . ? C60 C59 C62 111.11(15) . . ? C62 C59 H59 106.4 . . ? C59 C60 H60A 108.7 . . ? C59 C60 H60B 108.7 . . ? H60A C60 H60B 107.6 . . ? C61 C60 C59 114.37(15) . . ? C61 C60 H60A 108.7 . . ? C61 C60 H60B 108.7 . . ? C60 C61 H61A 109.5 . . ? C60 C61 H61B 109.5 . . ? C60 C61 H61C 109.5 . . ? H61A C61 H61B 109.5 . . ? H61A C61 H61C 109.5 . . ? H61B C61 H61C 109.5 . . ? C59 C62 H62A 108.2 . . ? C59 C62 H62B 108.2 . . ? H62A C62 H62B 107.4 . . ? C63 C62 C59 116.17(18) . . ? C63 C62 H62A 108.2 . . ? C63 C62 H62B 108.2 . . ? C62 C63 H63A 109.5 . . ? C62 C63 H63B 109.5 . . ? C62 C63 H63C 109.5 . . ? H63A C63 H63B 109.5 . . ? H63A C63 H63C 109.5 . . ? H63B C63 H63C 109.5 . . ? N4 C64 C65A 116.8(3) . . ? C65 C64 N4 121.9(3) . . ? C69 C64 N4 121.12(14) . . ? C69 C64 C65 116.7(3) . . ? C69 C64 C65A 121.0(3) . . ? C64 C65 C70 120.4(5) . . ? C66 C65 C64 121.8(5) . . ? C66 C65 C70 117.8(6) . . ? C65 C66 H66 120.2 . . ? C67 C66 C65 119.7(7) . . ? C67 C66 H66 120.2 . . ? C66 C67 H67 119.8 . . ? C66 C67 C68 120.4(8) . . ? C68 C67 H67 119.8 . . ? C67 C68 H68 120.0 . . ? C67 C68 C69 120.0(7) . . ? C69 C68 H68 120.0 . . ? C64 C69 C75 122.00(14) . . ? C64 C69 C68A 117.2(4) . . ? C68 C69 C64 120.5(4) . . ? C68 C69 C75 117.3(4) . . ? C68A C69 C75 120.6(4) . . ? C69 C75 H75 106.7 . . ? C69 C75 C76 111.87(14) . . ? C69 C75 C78 113.65(14) . . ? C76 C75 H75 106.7 . . ? C76 C75 C78 110.74(15) . . ? C78 C75 H75 106.7 . . ? C75 C76 H76A 108.4 . . ? C75 C76 H76B 108.4 . . ? H76A C76 H76B 107.4 . . ? C77 C76 C75 115.58(15) . . ? C77 C76 H76A 108.4 . . ? C77 C76 H76B 108.4 . . ? C76 C77 H77A 109.5 . . ? C76 C77 H77B 109.5 . . ? C76 C77 H77C 109.5 . . ? H77A C77 H77B 109.5 . . ? H77A C77 H77C 109.5 . . ? H77B C77 H77C 109.5 . . ? C75 C78 H78A 108.8 . . ? C75 C78 H78B 108.8 . . ? H78A C78 H78B 107.7 . . ? C79 C78 C75 113.88(16) . . ? C79 C78 H78A 108.8 . . ? C79 C78 H78B 108.8 . . ? C78 C79 H79A 109.5 . . ? C78 C79 H79B 109.5 . . ? C78 C79 H79C 109.5 . . ? H79A C79 H79B 109.5 . . ? H79A C79 H79C 109.5 . . ? H79B C79 H79C 109.5 . . ? O2 C80 H80A 109.4 . . ? O2 C80 H80B 109.4 . . ? O2 C80 C81 111.03(16) . . ? H80A C80 H80B 108.0 . . ? C81 C80 H80A 109.4 . . ? C81 C80 H80B 109.4 . . ? C80 C81 H81A 109.5 . . ? C80 C81 H81B 109.5 . . ? C80 C81 C82 110.66(17) . . ? H81A C81 H81B 108.1 . . ? C82 C81 H81A 109.5 . . ? C82 C81 H81B 109.5 . . ? C81 C82 H82A 109.6 . . ? C81 C82 H82B 109.6 . . ? H82A C82 H82B 108.2 . . ? C83 C82 C81 110.06(16) . . ? C83 C82 H82A 109.6 . . ? C83 C82 H82B 109.6 . . ? C82 C83 H83A 109.4 . . ? C82 C83 H83B 109.4 . . ? H83A C83 H83B 108.0 . . ? C84 C83 C82 111.15(17) . . ? C84 C83 H83A 109.4 . . ? C84 C83 H83B 109.4 . . ? O2 C84 C83 111.28(15) . . ? O2 C84 H84A 109.4 . . ? O2 C84 H84B 109.4 . . ? C83 C84 H84A 109.4 . . ? C83 C84 H84B 109.4 . . ? H84A C84 H84B 108.0 . . ? H85A C85 H85B 109.5 . . ? H85A C85 H85C 109.5 . . ? H85B C85 H85C 109.5 . . ? C86 C85 H85A 109.5 . . ? C86 C85 H85B 109.5 . . ? C86 C85 H85C 109.5 . . ? N5 C86 Ca3 58.25(8) . . ? N5 C86 C85 120.59(13) . . ? N5 C86 C87 123.98(14) . . ? C85 C86 Ca3 142.26(10) . . ? C87 C86 Ca3 75.56(9) . . ? C87 C86 C85 115.27(13) . . ? Ca3 C87 H87 138.4(11) . . ? C86 C87 Ca3 75.34(9) . . ? C86 C87 H87 112.4(11) . . ? C86 C87 C88 131.79(14) . . ? C88 C87 Ca3 75.61(9) . . ? C88 C87 H87 114.9(11) . . ? N6 C88 Ca3 58.16(8) . . ? N6 C88 C87 124.27(14) . . ? N6 C88 C89 121.43(14) . . ? C87 C88 Ca3 74.94(9) . . ? C87 C88 C89 114.23(14) . . ? C89 C88 Ca3 145.55(10) . . ? C88 C89 H89A 109.5 . . ? C88 C89 H89B 109.5 . . ? C88 C89 H89C 109.5 . . ? H89A C89 H89B 109.5 . . ? H89A C89 H89C 109.5 . . ? H89B C89 H89C 109.5 . . ? C91 C90 N5 121.61(13) . . ? C91 C90 C95 120.26(13) . . ? C95 C90 N5 118.02(14) . . ? C90 C91 C96 122.14(13) . . ? C92 C91 C90 118.87(14) . . ? C92 C91 C96 118.98(14) . . ? C91 C92 H92 119.4 . . ? C93 C92 C91 121.24(16) . . ? C93 C92 H92 119.4 . . ? C92 C93 H93 120.2 . . ? C92 C93 C94 119.68(15) . . ? C94 C93 H93 120.2 . . ? C93 C94 H94 119.1 . . ? C93 C94 C95 121.87(15) . . ? C95 C94 H94 119.1 . . ? C90 C95 C101 122.60(14) . . ? C94 C95 C90 118.09(15) . . ? C94 C95 C101 119.31(14) . . ? C91 C96 H96 106.3 . . ? C91 C96 C97 111.72(13) . . ? C91 C96 C99 114.60(13) . . ? C97 C96 H96 106.3 . . ? C99 C96 H96 106.3 . . ? C99 C96 C97 110.93(13) . . ? C96 C97 H97A 108.1 . . ? C96 C97 H97B 108.1 . . ? H97A C97 H97B 107.3 . . ? C98 C97 C96 116.78(14) . . ? C98 C97 H97A 108.1 . . ? C98 C97 H97B 108.1 . . ? C97 C98 H98A 109.5 . . ? C97 C98 H98B 109.5 . . ? C97 C98 H98C 109.5 . . ? H98A C98 H98B 109.5 . . ? H98A C98 H98C 109.5 . . ? H98B C98 H98C 109.5 . . ? C96 C99 H99A 108.9 . . ? C96 C99 H99B 108.9 . . ? H99A C99 H99B 107.7 . . ? C100 C99 C96 113.57(14) . . ? C100 C99 H99A 108.9 . . ? C100 C99 H99B 108.9 . . ? C99 C100 H10A 109.5 . . ? C99 C100 H10B 109.5 . . ? C99 C100 H10C 109.5 . . ? H10A C100 H10B 109.5 . . ? H10A C100 H10C 109.5 . . ? H10B C100 H10C 109.5 . . ? C95 C101 H101 106.5 . . ? C95 C101 C102 112.58(14) . . ? C95 C101 C104 114.07(15) . . ? C102 C101 H101 106.5 . . ? C104 C101 H101 106.5 . . ? C104 C101 C102 110.02(15) . . ? C101 C102 H10D 108.7 . . ? C101 C102 H10E 108.7 . . ? H10D C102 H10E 107.6 . . ? C103 C102 C101 114.28(15) . . ? C103 C102 H10D 108.7 . . ? C103 C102 H10E 108.7 . . ? C102 C103 H10F 109.5 . . ? C102 C103 H10G 109.5 . . ? C102 C103 H10H 109.5 . . ? H10F C103 H10G 109.5 . . ? H10F C103 H10H 109.5 . . ? H10G C103 H10H 109.5 . . ? C101 C104 H10I 108.2 . . ? C101 C104 H10J 108.2 . . ? H10I C104 H10J 107.4 . . ? C105 C104 C101 116.15(17) . . ? C105 C104 H10I 108.2 . . ? C105 C104 H10J 108.2 . . ? C104 C105 H10K 109.5 . . ? C104 C105 H10L 109.5 . . ? C104 C105 H10M 109.5 . . ? H10K C105 H10L 109.5 . . ? H10K C105 H10M 109.5 . . ? H10L C105 H10M 109.5 . . ? C107 C106 N6 119.05(14) . . ? C111 C106 N6 120.63(13) . . ? C111 C106 C107 120.31(14) . . ? C106 C107 C112 121.39(14) . . ? C108 C107 C106 118.38(15) . . ? C108 C107 C112 120.23(14) . . ? C107 C108 H108 119.1 . . ? C109 C108 C107 121.77(15) . . ? C109 C108 H108 119.1 . . ? C108 C109 H109 120.3 . . ? C108 C109 C110 119.43(16) . . ? C110 C109 H109 120.3 . . ? C109 C110 H110 119.3 . . ? C109 C110 C111 121.36(16) . . ? C111 C110 H110 119.3 . . ? C106 C111 C117 120.95(13) . . ? C110 C111 C106 118.61(14) . . ? C110 C111 C117 120.34(14) . . ? C107 C112 H112 106.5 . . ? C107 C112 C113 113.14(15) . . ? C107 C112 C115 113.18(14) . . ? C113 C112 H112 106.5 . . ? C113 C112 C115 110.41(14) . . ? C115 C112 H112 106.5 . . ? C112 C113 H11A 108.5 . . ? C112 C113 H11B 108.5 . . ? H11A C113 H11B 107.5 . . ? C114 C113 C112 115.29(17) . . ? C114 C113 H11A 108.5 . . ? C114 C113 H11B 108.5 . . ? C113 C114 H11C 109.5 . . ? C113 C114 H11D 109.5 . . ? C113 C114 H11E 109.5 . . ? H11C C114 H11D 109.5 . . ? H11C C114 H11E 109.5 . . ? H11D C114 H11E 109.5 . . ? C112 C115 H11F 108.5 . . ? C112 C115 H11G 108.5 . . ? H11F C115 H11G 107.5 . . ? C116 C115 C112 115.25(15) . . ? C116 C115 H11F 108.5 . . ? C116 C115 H11G 108.5 . . ? C115 C116 H11H 109.5 . . ? C115 C116 H11I 109.5 . . ? C115 C116 H11J 109.5 . . ? H11H C116 H11I 109.5 . . ? H11H C116 H11J 109.5 . . ? H11I C116 H11J 109.5 . . ? C111 C117 H117 106.6 . . ? C111 C117 C118 109.57(13) . . ? C111 C117 C120 114.90(13) . . ? C118 C117 H117 106.6 . . ? C120 C117 H117 106.6 . . ? C120 C117 C118 111.98(14) . . ? C117 C118 H11K 108.4 . . ? C117 C118 H11L 108.4 . . ? H11K C118 H11L 107.5 . . ? C119 C118 C117 115.46(15) . . ? C119 C118 H11K 108.4 . . ? C119 C118 H11L 108.4 . . ? C118 C119 H11M 109.5 . . ? C118 C119 H11N 109.5 . . ? C118 C119 H11O 109.5 . . ? H11M C119 H11N 109.5 . . ? H11M C119 H11O 109.5 . . ? H11N C119 H11O 109.5 . . ? C117 C120 H12A 108.9 . . ? C117 C120 H12B 108.9 . . ? H12A C120 H12B 107.7 . . ? C121 C120 C117 113.24(15) . . ? C121 C120 H12A 108.9 . . ? C121 C120 H12B 108.9 . . ? C120 C121 H12C 109.5 . . ? C120 C121 H12D 109.5 . . ? C120 C121 H12E 109.5 . . ? H12C C121 H12D 109.5 . . ? H12C C121 H12E 109.5 . . ? H12D C121 H12E 109.5 . . ? O3 C122 H12F 109.4 . . ? O3 C122 H12G 109.4 . . ? O3 C122 C123 111.26(14) . . ? H12F C122 H12G 108.0 . . ? C123 C122 H12F 109.4 . . ? C123 C122 H12G 109.4 . . ? C122 C123 H12H 109.4 . . ? C122 C123 H12I 109.4 . . ? C122 C123 C124 111.16(17) . . ? H12H C123 H12I 108.0 . . ? C124 C123 H12H 109.4 . . ? C124 C123 H12I 109.4 . . ? C123 C124 H12J 109.5 . . ? C123 C124 H12K 109.5 . . ? C123 C124 C125 110.67(15) . . ? H12J C124 H12K 108.1 . . ? C125 C124 H12J 109.5 . . ? C125 C124 H12K 109.5 . . ? C124 C125 H12L 109.5 . . ? C124 C125 H12M 109.5 . . ? H12L C125 H12M 108.1 . . ? C126 C125 C124 110.71(15) . . ? C126 C125 H12L 109.5 . . ? C126 C125 H12M 109.5 . . ? O3 C126 C125 110.66(16) . . ? O3 C126 H12N 109.5 . . ? O3 C126 H12O 109.5 . . ? C125 C126 H12N 109.5 . . ? C125 C126 H12O 109.5 . . ? H12N C126 H12O 108.1 . . ? C27 C33 H33 106.6 . . ? C34 C33 C27 113.7(2) . . ? C34 C33 H33 106.6 . . ? C34 C33 C36 110.2(2) . . ? C36 C33 C27 112.7(2) . . ? C36 C33 H33 106.6 . . ? C33 C34 H34A 109.2 . . ? C33 C34 H34B 109.2 . . ? H34A C34 H34B 107.9 . . ? C35 C34 C33 112.2(2) . . ? C35 C34 H34A 109.2 . . ? C35 C34 H34B 109.2 . . ? C34 C35 H35A 109.5 . . ? C34 C35 H35B 109.5 . . ? C34 C35 H35C 109.5 . . ? H35A C35 H35B 109.5 . . ? H35A C35 H35C 109.5 . . ? H35B C35 H35C 109.5 . . ? C33 C36 H36A 108.1 . . ? C33 C36 H36B 108.1 . . ? H36A C36 H36B 107.3 . . ? C37 C36 C33 116.7(2) . . ? C37 C36 H36A 108.1 . . ? C37 C36 H36B 108.1 . . ? C36 C37 H37A 109.5 . . ? C36 C37 H37B 109.5 . . ? C36 C37 H37C 109.5 . . ? H37A C37 H37B 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C65 C70 H70 108.5 . . ? C65 C70 C71 110.2(4) . . ? C65 C70 C73 111.6(4) . . ? C71 C70 H70 108.5 . . ? C73 C70 H70 108.5 . . ? C73 C70 C71 109.6(3) . . ? C70 C71 H71A 108.6 . . ? C70 C71 H71B 108.6 . . ? H71A C71 H71B 107.6 . . ? C72 C71 C70 114.5(3) . . ? C72 C71 H71A 108.6 . . ? C72 C71 H71B 108.6 . . ? C71 C72 H72A 109.5 . . ? C71 C72 H72B 109.5 . . ? C71 C72 H72C 109.5 . . ? H72A C72 H72B 109.5 . . ? H72A C72 H72C 109.5 . . ? H72B C72 H72C 109.5 . . ? C70 C73 H73A 108.7 . . ? C70 C73 H73B 108.7 . . ? H73A C73 H73B 107.6 . . ? C74 C73 C70 114.4(3) . . ? C74 C73 H73A 108.7 . . ? C74 C73 H73B 108.7 . . ? C73 C74 H74A 109.5 . . ? C73 C74 H74B 109.5 . . ? C73 C74 H74C 109.5 . . ? H74A C74 H74B 109.5 . . ? H74A C74 H74C 109.5 . . ? H74B C74 H74C 109.5 . . ? C27 C33A H33A 106.3 . . ? C27 C33A C34A 116.5(8) . . ? C34A C33A H33A 106.3 . . ? C36A C33A C27 103.6(6) . . ? C36A C33A H33A 106.3 . . ? C36A C33A C34A 117.0(8) . . ? C33A C34A H34C 107.3 . . ? C33A C34A H34D 107.3 . . ? C33A C34A C35A 120.3(10) . . ? H34C C34A H34D 106.9 . . ? C35A C34A H34C 107.3 . . ? C35A C34A H34D 107.3 . . ? C34A C35A H35D 109.5 . . ? C34A C35A H35E 109.5 . . ? C34A C35A H35F 109.5 . . ? H35D C35A H35E 109.5 . . ? H35D C35A H35F 109.5 . . ? H35E C35A H35F 109.5 . . ? C33A C36A H36C 108.0 . . ? C33A C36A H36D 108.0 . . ? C33A C36A C37A 117.1(7) . . ? H36C C36A H36D 107.3 . . ? C37A C36A H36C 108.0 . . ? C37A C36A H36D 108.0 . . ? C36A C37A H37D 109.5 . . ? C36A C37A H37E 109.5 . . ? C36A C37A H37F 109.5 . . ? H37D C37A H37E 109.5 . . ? H37D C37A H37F 109.5 . . ? H37E C37A H37F 109.5 . . ? C71A C70A H70A 106.6 . . ? C73A C70A H70A 106.6 . . ? C73A C70A C71A 109.6(5) . . ? C73A C70A C65A 113.9(5) . . ? C65A C70A H70A 106.6 . . ? C65A C70A C71A 113.0(5) . . ? C70A C71A H71C 108.5 . . ? C70A C71A H71D 108.5 . . ? H71C C71A H71D 107.5 . . ? C72A C71A C70A 115.0(5) . . ? C72A C71A H71C 108.5 . . ? C72A C71A H71D 108.5 . . ? C71A C72A H72D 109.5 . . ? C71A C72A H72E 109.5 . . ? C71A C72A H72F 109.5 . . ? H72D C72A H72E 109.5 . . ? H72D C72A H72F 109.5 . . ? H72E C72A H72F 109.5 . . ? C70A C73A H73C 108.5 . . ? C70A C73A H73D 108.5 . . ? C70A C73A C74A 114.9(5) . . ? H73C C73A H73D 107.5 . . ? C74A C73A H73C 108.5 . . ? C74A C73A H73D 108.6 . . ? C73A C74A H74D 109.5 . . ? C73A C74A H74E 109.5 . . ? C73A C74A H74F 109.5 . . ? H74D C74A H74E 109.5 . . ? H74D C74A H74F 109.5 . . ? H74E C74A H74F 109.5 . . ? C136 O4A C132 109.4(12) . . ? O4A C132 H13C 109.5 . . ? O4A C132 H13D 109.5 . . ? H13C C132 H13D 108.1 . . ? C133 C132 O4A 110.7(10) . . ? C133 C132 H13C 109.5 . . ? C133 C132 H13D 109.5 . . ? C132 C133 H13E 108.1 . . ? C132 C133 H13F 108.1 . . ? H13E C133 H13F 107.3 . . ? C134 C133 C132 116.9(12) . . ? C134 C133 H13E 108.1 . . ? C134 C133 H13F 108.1 . . ? C133 C134 H13G 109.6 . . ? C133 C134 H13H 109.6 . . ? C133 C134 C135 110.2(11) . . ? H13G C134 H13H 108.1 . . ? C135 C134 H13G 109.6 . . ? C135 C134 H13H 109.6 . . ? C134 C135 H13I 108.9 . . ? C134 C135 H13J 108.9 . . ? C134 C135 C136 113.2(12) . . ? H13I C135 H13J 107.8 . . ? C136 C135 H13I 108.9 . . ? C136 C135 H13J 108.9 . . ? O4A C136 H13K 109.1 . . ? O4A C136 H13L 109.1 . . ? C135 C136 O4A 112.4(11) . . ? C135 C136 H13K 109.1 . . ? C135 C136 H13L 109.1 . . ? H13K C136 H13L 107.9 . . ? C131 O4 C127 111.8(4) . . ? O4 C127 H12P 109.6 . . ? O4 C127 H12Q 109.6 . . ? H12P C127 H12Q 108.1 . . ? C128 C127 O4 110.5(3) . . ? C128 C127 H12P 109.6 . . ? C128 C127 H12Q 109.6 . . ? C127 C128 H12R 109.6 . . ? C127 C128 H12S 109.6 . . ? C127 C128 C129 110.4(4) . . ? H12R C128 H12S 108.1 . . ? C129 C128 H12R 109.6 . . ? C129 C128 H12S 109.6 . . ? C128 C129 H12T 109.6 . . ? C128 C129 H12U 109.6 . . ? H12T C129 H12U 108.1 . . ? C130 C129 C128 110.3(4) . . ? C130 C129 H12T 109.6 . . ? C130 C129 H12U 109.6 . . ? C129 C130 H13M 109.2 . . ? C129 C130 H13N 109.2 . . ? C129 C130 C131 111.9(4) . . ? H13M C130 H13N 107.9 . . ? C131 C130 H13M 109.2 . . ? C131 C130 H13N 109.2 . . ? O4 C131 C130 108.5(4) . . ? O4 C131 H13O 110.0 . . ? O4 C131 H13P 110.0 . . ? C130 C131 H13O 110.0 . . ? C130 C131 H13P 110.0 . . ? H13O C131 H13P 108.4 . . ? C69 C68A H68A 118.4 . . ? C67A C68A C69 123.1(6) . . ? C67A C68A H68A 118.4 . . ? C68A C67A H67A 121.1 . . ? C66A C67A C68A 117.9(8) . . ? C66A C67A H67A 121.1 . . ? C67A C66A H66A 117.9 . . ? C67A C66A C65A 124.2(8) . . ? C65A C66A H66A 117.9 . . ? C64 C65A C70A 124.9(6) . . ? C66A C65A C64 115.5(6) . . ? C66A C65A C70A 119.6(7) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ca1 P1 3.3252(5) . ? Ca1 P3 3.3801(5) . ? Ca1 P4 3.1164(5) . ? Ca1 P6 3.0922(4) . ? Ca1 O1 2.3915(11) . ? Ca1 N1 2.4201(12) . ? Ca1 N2 2.3836(12) . ? Ca1 C2 2.8033(14) . ? Ca1 C3 2.7752(15) . ? Ca1 C4 2.7824(14) . ? Ca2 P1 3.4152(5) . ? Ca2 P2 3.3324(5) . ? Ca2 P4 3.1022(5) . ? Ca2 P5 3.0747(5) . ? Ca2 O2 2.3815(11) . ? Ca2 N3 2.4074(13) . ? Ca2 N4 2.4040(13) . ? Ca2 C44 2.8217(15) . ? Ca2 C45 2.7964(15) . ? Ca2 C46 2.7999(15) . ? Ca3 P2 3.4610(5) . ? Ca3 P3 3.3537(5) . ? Ca3 P5 3.1032(5) . ? Ca3 P6 3.0557(4) . ? Ca3 O3 2.3874(11) . ? Ca3 N5 2.3919(12) . ? Ca3 N6 2.4008(12) . ? Ca3 C86 2.8078(15) . ? Ca3 C87 2.8106(16) . ? Ca3 C88 2.8193(15) . ? P1 P2 2.2544(5) . ? P1 P3 2.2609(5) . ? P1 P4 2.1610(5) . ? P2 P3 2.2579(5) . ? P2 P5 2.1615(5) . ? P3 P6 2.1601(5) . ? P4 P7 2.1787(5) . ? P5 P7 2.1890(5) . ? P6 P7 2.1868(5) . ? O1 C38 1.445(2) . ? O1 C42 1.4474(19) . ? O2 C80 1.448(2) . ? O2 C84 1.4507(19) . ? O3 C122 1.447(2) . ? O3 C126 1.4496(19) . ? N1 C2 1.3327(19) . ? N1 C6 1.4422(19) . ? N2 C4 1.3306(19) . ? N2 C22 1.4388(18) . ? N3 C44 1.330(2) . ? N3 C48 1.4379(19) . ? N4 C46 1.324(2) . ? N4 C64 1.432(2) . ? N5 C86 1.336(2) . ? N5 C90 1.4363(18) . ? N6 C88 1.321(2) . ? N6 C106 1.4403(19) . ? C1 H1A 0.9800 . ? C1 H1B 0.9800 . ? C1 H1C 0.9800 . ? C1 C2 1.5198(19) . ? C2 C3 1.418(2) . ? C3 H3 0.960(19) . ? C3 C4 1.419(2) . ? C4 C5 1.514(2) . ? C5 H5A 0.9800 . ? C5 H5B 0.9800 . ? C5 H5C 0.9800 . ? C6 C7 1.417(2) . ? C6 C11 1.409(2) . ? C7 C8 1.392(2) . ? C7 C12 1.517(2) . ? C8 H8 0.9500 . ? C8 C9 1.380(2) . ? C9 H9 0.9500 . ? C9 C10 1.381(2) . ? C10 H10 0.9500 . ? C10 C11 1.395(2) . ? C11 C17 1.518(2) . ? C12 H12 1.0000 . ? C12 C13 1.545(2) . ? C12 C15 1.540(2) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C13 C14 1.524(3) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C15 C16 1.529(2) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17 1.0000 . ? C17 C18 1.539(2) . ? C17 C20 1.535(2) . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C18 C19 1.525(2) . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9900 . ? C20 H20B 0.9900 . ? C20 C21 1.516(3) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 C23 1.408(2) . ? C22 C27 1.413(2) . ? C23 C24 1.391(2) . ? C23 C28 1.518(2) . ? C24 H24 0.9500 . ? C24 C25 1.384(2) . ? C25 H25 0.9500 . ? C25 C26 1.378(3) . ? C26 H26 0.9500 . ? C26 C27 1.392(2) . ? C27 C33 1.559(3) . ? C27 C33A 1.486(6) . ? C28 H28 1.0000 . ? C28 C29 1.545(2) . ? C28 C31 1.528(2) . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C29 C30 1.520(2) . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? C31 H31A 0.9900 . ? C31 H31B 0.9900 . ? C31 C32 1.522(3) . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C38 H38A 0.9900 . ? C38 H38B 0.9900 . ? C38 C39 1.520(3) . ? C39 H39A 0.9900 . ? C39 H39B 0.9900 . ? C39 C40 1.529(3) . ? C40 H40A 0.9900 . ? C40 H40B 0.9900 . ? C40 C41 1.516(3) . ? C41 H41A 0.9900 . ? C41 H41B 0.9900 . ? C41 C42 1.508(2) . ? C42 H42A 0.9900 . ? C42 H42B 0.9900 . ? C43 H43A 0.9800 . ? C43 H43B 0.9800 . ? C43 H43C 0.9800 . ? C43 C44 1.513(2) . ? C44 C45 1.420(2) . ? C45 H45 0.936(18) . ? C45 C46 1.415(2) . ? C46 C47 1.521(2) . ? C47 H47A 0.9800 . ? C47 H47B 0.9800 . ? C47 H47C 0.9800 . ? C48 C49 1.409(2) . ? C48 C53 1.417(2) . ? C49 C50 1.398(2) . ? C49 C54 1.516(2) . ? C50 H50 0.9500 . ? C50 C51 1.387(2) . ? C51 H51 0.9500 . ? C51 C52 1.373(3) . ? C52 H52 0.9500 . ? C52 C53 1.399(2) . ? C53 C59 1.514(3) . ? C54 H54 1.0000 . ? C54 C55 1.544(2) . ? C54 C57 1.526(2) . ? C55 H55A 0.9900 . ? C55 H55B 0.9900 . ? C55 C56 1.526(2) . ? C56 H56A 0.9800 . ? C56 H56B 0.9800 . ? C56 H56C 0.9800 . ? C57 H57A 0.9900 . ? C57 H57B 0.9900 . ? C57 C58 1.522(3) . ? C58 H58A 0.9800 . ? C58 H58B 0.9800 . ? C58 H58C 0.9800 . ? C59 H59 1.0000 . ? C59 C60 1.537(3) . ? C59 C62 1.539(3) . ? C60 H60A 0.9900 . ? C60 H60B 0.9900 . ? C60 C61 1.522(3) . ? C61 H61A 0.9800 . ? C61 H61B 0.9800 . ? C61 H61C 0.9800 . ? C62 H62A 0.9900 . ? C62 H62B 0.9900 . ? C62 C63 1.515(4) . ? C63 H63A 0.9800 . ? C63 H63B 0.9800 . ? C63 H63C 0.9800 . ? C64 C65 1.411(7) . ? C64 C69 1.403(2) . ? C64 C65A 1.461(8) . ? C65 C66 1.382(9) . ? C65 C70 1.515(5) . ? C66 H66 0.9500 . ? C66 C67 1.359(9) . ? C67 H67 0.9500 . ? C67 C68 1.387(9) . ? C68 H68 0.9500 . ? C68 C69 1.394(9) . ? C69 C75 1.522(2) . ? C69 C68A 1.408(8) . ? C75 H75 1.0000 . ? C75 C76 1.537(3) . ? C75 C78 1.541(2) . ? C76 H76A 0.9900 . ? C76 H76B 0.9900 . ? C76 C77 1.523(3) . ? C77 H77A 0.9800 . ? C77 H77B 0.9800 . ? C77 H77C 0.9800 . ? C78 H78A 0.9900 . ? C78 H78B 0.9900 . ? C78 C79 1.512(3) . ? C79 H79A 0.9800 . ? C79 H79B 0.9800 . ? C79 H79C 0.9800 . ? C80 H80A 0.9900 . ? C80 H80B 0.9900 . ? C80 C81 1.501(3) . ? C81 H81A 0.9900 . ? C81 H81B 0.9900 . ? C81 C82 1.526(3) . ? C82 H82A 0.9900 . ? C82 H82B 0.9900 . ? C82 C83 1.524(3) . ? C83 H83A 0.9900 . ? C83 H83B 0.9900 . ? C83 C84 1.503(3) . ? C84 H84A 0.9900 . ? C84 H84B 0.9900 . ? C85 H85A 0.9800 . ? C85 H85B 0.9800 . ? C85 H85C 0.9800 . ? C85 C86 1.517(2) . ? C86 C87 1.412(2) . ? C87 H87 0.908(18) . ? C87 C88 1.431(2) . ? C88 C89 1.519(2) . ? C89 H89A 0.9800 . ? C89 H89B 0.9800 . ? C89 H89C 0.9800 . ? C90 C91 1.411(2) . ? C90 C95 1.418(2) . ? C91 C92 1.397(2) . ? C91 C96 1.517(2) . ? C92 H92 0.9500 . ? C92 C93 1.377(2) . ? C93 H93 0.9500 . ? C93 C94 1.382(3) . ? C94 H94 0.9500 . ? C94 C95 1.395(2) . ? C95 C101 1.526(2) . ? C96 H96 1.0000 . ? C96 C97 1.542(2) . ? C96 C99 1.538(2) . ? C97 H97A 0.9900 . ? C97 H97B 0.9900 . ? C97 C98 1.524(2) . ? C98 H98A 0.9800 . ? C98 H98B 0.9800 . ? C98 H98C 0.9800 . ? C99 H99A 0.9900 . ? C99 H99B 0.9900 . ? C99 C100 1.517(2) . ? C100 H10A 0.9800 . ? C100 H10B 0.9800 . ? C100 H10C 0.9800 . ? C101 H101 1.0000 . ? C101 C102 1.543(2) . ? C101 C104 1.536(3) . ? C102 H10D 0.9900 . ? C102 H10E 0.9900 . ? C102 C103 1.511(3) . ? C103 H10F 0.9800 . ? C103 H10G 0.9800 . ? C103 H10H 0.9800 . ? C104 H10I 0.9900 . ? C104 H10J 0.9900 . ? C104 C105 1.513(3) . ? C105 H10K 0.9800 . ? C105 H10L 0.9800 . ? C105 H10M 0.9800 . ? C106 C107 1.410(2) . ? C106 C111 1.407(2) . ? C107 C108 1.393(2) . ? C107 C112 1.522(2) . ? C108 H108 0.9500 . ? C108 C109 1.376(3) . ? C109 H109 0.9500 . ? C109 C110 1.381(2) . ? C110 H110 0.9500 . ? C110 C111 1.396(2) . ? C111 C117 1.518(2) . ? C112 H112 1.0000 . ? C112 C113 1.534(3) . ? C112 C115 1.541(2) . ? C113 H11A 0.9900 . ? C113 H11B 0.9900 . ? C113 C114 1.520(3) . ? C114 H11C 0.9800 . ? C114 H11D 0.9800 . ? C114 H11E 0.9800 . ? C115 H11F 0.9900 . ? C115 H11G 0.9900 . ? C115 C116 1.522(3) . ? C116 H11H 0.9800 . ? C116 H11I 0.9800 . ? C116 H11J 0.9800 . ? C117 H117 1.0000 . ? C117 C118 1.543(3) . ? C117 C120 1.534(2) . ? C118 H11K 0.9900 . ? C118 H11L 0.9900 . ? C118 C119 1.518(2) . ? C119 H11M 0.9800 . ? C119 H11N 0.9800 . ? C119 H11O 0.9800 . ? C120 H12A 0.9900 . ? C120 H12B 0.9900 . ? C120 C121 1.521(3) . ? C121 H12C 0.9800 . ? C121 H12D 0.9800 . ? C121 H12E 0.9800 . ? C122 H12F 0.9900 . ? C122 H12G 0.9900 . ? C122 C123 1.518(3) . ? C123 H12H 0.9900 . ? C123 H12I 0.9900 . ? C123 C124 1.522(3) . ? C124 H12J 0.9900 . ? C124 H12K 0.9900 . ? C124 C125 1.526(3) . ? C125 H12L 0.9900 . ? C125 H12M 0.9900 . ? C125 C126 1.521(3) . ? C126 H12N 0.9900 . ? C126 H12O 0.9900 . ? C33 H33 1.0000 . ? C33 C34 1.534(3) . ? C33 C36 1.553(4) . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C34 C35 1.507(4) . ? C35 H35A 0.9800 . ? C35 H35B 0.9800 . ? C35 H35C 0.9800 . ? C36 H36A 0.9900 . ? C36 H36B 0.9900 . ? C36 C37 1.509(4) . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C70 H70 1.0000 . ? C70 C71 1.544(6) . ? C70 C73 1.539(5) . ? C71 H71A 0.9900 . ? C71 H71B 0.9900 . ? C71 C72 1.517(6) . ? C72 H72A 0.9800 . ? C72 H72B 0.9800 . ? C72 H72C 0.9800 . ? C73 H73A 0.9900 . ? C73 H73B 0.9900 . ? C73 C74 1.524(6) . ? C74 H74A 0.9800 . ? C74 H74B 0.9800 . ? C74 H74C 0.9800 . ? C33A H33A 1.0000 . ? C33A C34A 1.488(17) . ? C33A C36A 1.468(13) . ? C34A H34C 0.9900 . ? C34A H34D 0.9900 . ? C34A C35A 1.491(16) . ? C35A H35D 0.9800 . ? C35A H35E 0.9800 . ? C35A H35F 0.9800 . ? C36A H36C 0.9900 . ? C36A H36D 0.9900 . ? C36A C37A 1.489(12) . ? C37A H37D 0.9800 . ? C37A H37E 0.9800 . ? C37A H37F 0.9800 . ? C70A H70A 1.0000 . ? C70A C71A 1.555(8) . ? C70A C73A 1.525(8) . ? C70A C65A 1.535(6) . ? C71A H71C 0.9900 . ? C71A H71D 0.9900 . ? C71A C72A 1.520(8) . ? C72A H72D 0.9800 . ? C72A H72E 0.9800 . ? C72A H72F 0.9800 . ? C73A H73C 0.9900 . ? C73A H73D 0.9900 . ? C73A C74A 1.525(9) . ? C74A H74D 0.9800 . ? C74A H74E 0.9800 . ? C74A H74F 0.9800 . ? O4A C132 1.536(13) . ? O4A C136 1.483(14) . ? C132 H13C 0.9900 . ? C132 H13D 0.9900 . ? C132 C133 1.459(12) . ? C133 H13E 0.9900 . ? C133 H13F 0.9900 . ? C133 C134 1.442(13) . ? C134 H13G 0.9900 . ? C134 H13H 0.9900 . ? C134 C135 1.446(12) . ? C135 H13I 0.9900 . ? C135 H13J 0.9900 . ? C135 C136 1.472(13) . ? C136 H13K 0.9900 . ? C136 H13L 0.9900 . ? O4 C127 1.488(5) . ? O4 C131 1.423(7) . ? C127 H12P 0.9900 . ? C127 H12Q 0.9900 . ? C127 C128 1.485(6) . ? C128 H12R 0.9900 . ? C128 H12S 0.9900 . ? C128 C129 1.504(6) . ? C129 H12T 0.9900 . ? C129 H12U 0.9900 . ? C129 C130 1.481(6) . ? C130 H13M 0.9900 . ? C130 H13N 0.9900 . ? C130 C131 1.520(7) . ? C131 H13O 0.9900 . ? C131 H13P 0.9900 . ? C68A H68A 0.9500 . ? C68A C67A 1.380(10) . ? C67A H67A 0.9500 . ? C67A C66A 1.367(10) . ? C66A H66A 0.9500 . ? C66A C65A 1.397(10) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ca1 O1 C38 C39 -129.90(13) . . . . ? Ca1 O1 C42 C41 132.32(12) . . . . ? Ca1 N1 C2 C1 -138.98(11) . . . . ? Ca1 N1 C2 C3 38.02(14) . . . . ? Ca1 N1 C6 C7 -140.78(13) . . . . ? Ca1 N1 C6 C11 40.2(2) . . . . ? Ca1 N2 C4 C3 -38.94(14) . . . . ? Ca1 N2 C4 C5 136.84(12) . . . . ? Ca1 N2 C22 C23 -38.2(2) . . . . ? Ca1 N2 C22 C27 141.87(14) . . . . ? Ca1 C2 C3 C4 55.29(15) . . . . ? Ca1 C3 C4 N2 33.85(13) . . . . ? Ca1 C3 C4 C5 -142.17(12) . . . . ? Ca2 O2 C80 C81 129.90(12) . . . . ? Ca2 O2 C84 C83 -133.09(13) . . . . ? Ca2 N3 C44 C43 -139.12(13) . . . . ? Ca2 N3 C44 C45 37.19(15) . . . . ? Ca2 N3 C48 C49 41.8(3) . . . . ? Ca2 N3 C48 C53 -137.31(15) . . . . ? Ca2 N4 C46 C45 -39.46(16) . . . . ? Ca2 N4 C46 C47 135.67(14) . . . . ? Ca2 N4 C64 C65 152.5(3) . . . . ? Ca2 N4 C64 C69 -34.6(2) . . . . ? Ca2 N4 C64 C65A 133.5(4) . . . . ? Ca2 C44 C45 C46 55.40(16) . . . . ? Ca2 C45 C46 N4 34.31(14) . . . . ? Ca2 C45 C46 C47 -141.15(13) . . . . ? Ca3 O3 C122 C123 135.90(13) . . . . ? Ca3 O3 C126 C125 -132.79(12) . . . . ? Ca3 N5 C86 C85 -135.60(12) . . . . ? Ca3 N5 C86 C87 39.58(15) . . . . ? Ca3 N5 C90 C91 37.1(2) . . . . ? Ca3 N5 C90 C95 -139.02(14) . . . . ? Ca3 N6 C88 C87 -37.51(15) . . . . ? Ca3 N6 C88 C89 139.30(12) . . . . ? Ca3 N6 C106 C107 136.48(14) . . . . ? Ca3 N6 C106 C111 -42.6(2) . . . . ? Ca3 C86 C87 C88 54.67(16) . . . . ? Ca3 C87 C88 N6 32.39(13) . . . . ? Ca3 C87 C88 C89 -144.62(12) . . . . ? O1 C38 C39 C40 -57.3(2) . . . . ? O2 C80 C81 C82 57.0(2) . . . . ? O3 C122 C123 C124 54.9(2) . . . . ? N1 C2 C3 Ca1 -33.53(12) . . . . ? N1 C2 C3 C4 21.8(2) . . . . ? N1 C6 C7 C8 -174.99(14) . . . . ? N1 C6 C7 C12 5.2(2) . . . . ? N1 C6 C11 C10 175.09(14) . . . . ? N1 C6 C11 C17 -6.9(2) . . . . ? N2 C22 C23 C24 -175.21(14) . . . . ? N2 C22 C23 C28 7.0(2) . . . . ? N2 C22 C27 C26 173.20(15) . . . . ? N2 C22 C27 C33 -14.6(3) . . . . ? N2 C22 C27 C33A 15.8(6) . . . . ? N3 C44 C45 Ca2 -32.31(13) . . . . ? N3 C44 C45 C46 23.1(3) . . . . ? N3 C48 C49 C50 177.43(15) . . . . ? N3 C48 C49 C54 -5.4(2) . . . . ? N3 C48 C53 C52 -178.08(16) . . . . ? N3 C48 C53 C59 2.9(2) . . . . ? N4 C64 C65 C66 -177.2(4) . . . . ? N4 C64 C65 C70 1.9(6) . . . . ? N4 C64 C69 C68 -176.1(8) . . . . ? N4 C64 C69 C75 -2.3(2) . . . . ? N4 C64 C69 C68A 171.8(8) . . . . ? N4 C64 C65A C70A 1.2(8) . . . . ? N4 C64 C65A C66A -178.8(5) . . . . ? N5 C86 C87 Ca3 -34.02(13) . . . . ? N5 C86 C87 C88 20.6(3) . . . . ? N5 C90 C91 C92 -176.78(14) . . . . ? N5 C90 C91 C96 2.1(2) . . . . ? N5 C90 C95 C94 177.04(15) . . . . ? N5 C90 C95 C101 -1.7(2) . . . . ? N6 C106 C107 C108 176.77(17) . . . . ? N6 C106 C107 C112 -3.9(3) . . . . ? N6 C106 C111 C110 -177.85(16) . . . . ? N6 C106 C111 C117 5.9(2) . . . . ? C1 C2 C3 Ca1 143.61(11) . . . . ? C1 C2 C3 C4 -161.10(14) . . . . ? C2 N1 C6 C7 83.39(17) . . . . ? C2 N1 C6 C11 -95.61(16) . . . . ? C2 C3 C4 Ca1 -55.61(15) . . . . ? C2 C3 C4 N2 -21.8(2) . . . . ? C2 C3 C4 C5 162.22(15) . . . . ? C4 N2 C22 C23 97.38(17) . . . . ? C4 N2 C22 C27 -82.53(18) . . . . ? C6 N1 C2 Ca1 155.47(12) . . . . ? C6 N1 C2 C1 16.50(18) . . . . ? C6 N1 C2 C3 -166.51(13) . . . . ? C6 C7 C8 C9 -1.3(3) . . . . ? C6 C7 C12 C13 144.41(16) . . . . ? C6 C7 C12 C15 -89.94(18) . . . . ? C6 C11 C17 C18 -88.60(17) . . . . ? C6 C11 C17 C20 145.07(15) . . . . ? C7 C6 C11 C10 -3.9(2) . . . . ? C7 C6 C11 C17 174.14(14) . . . . ? C7 C8 C9 C10 -1.6(3) . . . . ? C7 C12 C13 C14 -57.5(2) . . . . ? C7 C12 C15 C16 -54.60(19) . . . . ? C8 C7 C12 C13 -35.3(2) . . . . ? C8 C7 C12 C15 90.30(18) . . . . ? C8 C9 C10 C11 1.7(3) . . . . ? C9 C10 C11 C6 1.0(3) . . . . ? C9 C10 C11 C17 -177.08(16) . . . . ? C10 C11 C17 C18 89.45(17) . . . . ? C10 C11 C17 C20 -36.9(2) . . . . ? C11 C6 C7 C8 4.0(2) . . . . ? C11 C6 C7 C12 -175.73(14) . . . . ? C11 C17 C18 C19 -64.92(18) . . . . ? C11 C17 C20 C21 -63.14(19) . . . . ? C12 C7 C8 C9 178.49(16) . . . . ? C13 C12 C15 C16 72.25(18) . . . . ? C15 C12 C13 C14 174.68(16) . . . . ? C18 C17 C20 C21 171.10(14) . . . . ? C20 C17 C18 C19 63.48(18) . . . . ? C22 N2 C4 Ca1 -154.74(14) . . . . ? C22 N2 C4 C3 166.31(13) . . . . ? C22 N2 C4 C5 -17.9(2) . . . . ? C22 C23 C24 C25 0.5(3) . . . . ? C22 C23 C28 C29 83.08(18) . . . . ? C22 C23 C28 C31 -149.51(15) . . . . ? C22 C27 C33 C34 134.68(19) . . . . ? C22 C27 C33 C36 -98.9(2) . . . . ? C22 C27 C33A C34A 82.8(9) . . . . ? C22 C27 C33A C36A -147.2(4) . . . . ? C23 C22 C27 C26 -6.7(2) . . . . ? C23 C22 C27 C33 165.52(19) . . . . ? C23 C22 C27 C33A -164.1(6) . . . . ? C23 C24 C25 C26 -3.6(3) . . . . ? C23 C28 C29 C30 62.08(19) . . . . ? C23 C28 C31 C32 59.8(2) . . . . ? C24 C23 C28 C29 -94.63(18) . . . . ? C24 C23 C28 C31 32.8(2) . . . . ? C24 C25 C26 C27 1.4(3) . . . . ? C25 C26 C27 C22 3.6(3) . . . . ? C25 C26 C27 C33 -168.6(2) . . . . ? C25 C26 C27 C33A 163.2(5) . . . . ? C26 C27 C33 C34 -53.2(3) . . . . ? C26 C27 C33 C36 73.2(3) . . . . ? C26 C27 C33A C34A -75.5(9) . . . . ? C26 C27 C33A C36A 54.4(8) . . . . ? C27 C22 C23 C24 4.7(2) . . . . ? C27 C22 C23 C28 -173.07(15) . . . . ? C27 C33 C34 C35 -61.8(3) . . . . ? C27 C33 C36 C37 -68.7(3) . . . . ? C27 C33A C34A C35A 47.0(14) . . . . ? C27 C33A C36A C37A 50.1(10) . . . . ? C28 C23 C24 C25 178.25(16) . . . . ? C29 C28 C31 C32 -174.29(15) . . . . ? C31 C28 C29 C30 -66.6(2) . . . . ? C38 O1 C42 C41 -60.60(18) . . . . ? C38 C39 C40 C41 52.4(2) . . . . ? C39 C40 C41 C42 -51.9(2) . . . . ? C40 C41 C42 O1 56.27(19) . . . . ? C42 O1 C38 C39 61.11(19) . . . . ? C43 C44 C45 Ca2 144.20(13) . . . . ? C43 C44 C45 C46 -160.41(16) . . . . ? C44 N3 C48 C49 -99.12(18) . . . . ? C44 N3 C48 C53 81.77(19) . . . . ? C44 C45 C46 Ca2 -55.71(16) . . . . ? C44 C45 C46 N4 -21.4(3) . . . . ? C44 C45 C46 C47 163.14(16) . . . . ? C46 N4 C64 C65 -70.4(3) . . . . ? C46 N4 C64 C69 102.49(18) . . . . ? C46 N4 C64 C65A -89.4(4) . . . . ? C48 N3 C44 Ca2 157.41(14) . . . . ? C48 N3 C44 C43 18.3(2) . . . . ? C48 N3 C44 C45 -165.40(14) . . . . ? C48 C49 C50 C51 1.6(3) . . . . ? C48 C49 C54 C55 -89.73(17) . . . . ? C48 C49 C54 C57 142.59(15) . . . . ? C48 C53 C59 C60 138.87(17) . . . . ? C48 C53 C59 C62 -94.0(2) . . . . ? C49 C48 C53 C52 2.8(3) . . . . ? C49 C48 C53 C59 -176.23(16) . . . . ? C49 C50 C51 C52 0.9(3) . . . . ? C49 C54 C55 C56 -71.29(18) . . . . ? C49 C54 C57 C58 -63.38(18) . . . . ? C50 C49 C54 C55 87.40(18) . . . . ? C50 C49 C54 C57 -40.3(2) . . . . ? C50 C51 C52 C53 -1.6(3) . . . . ? C51 C52 C53 C48 -0.2(3) . . . . ? C51 C52 C53 C59 178.82(18) . . . . ? C52 C53 C59 C60 -40.1(2) . . . . ? C52 C53 C59 C62 87.0(2) . . . . ? C53 C48 C49 C50 -3.5(2) . . . . ? C53 C48 C49 C54 173.68(15) . . . . ? C53 C59 C60 C61 -52.2(2) . . . . ? C53 C59 C62 C63 -53.3(2) . . . . ? C54 C49 C50 C51 -175.59(16) . . . . ? C55 C54 C57 C58 170.33(14) . . . . ? C57 C54 C55 C56 57.67(18) . . . . ? C60 C59 C62 C63 74.6(3) . . . . ? C62 C59 C60 C61 179.34(18) . . . . ? C64 N4 C46 Ca2 -153.72(15) . . . . ? C64 N4 C46 C45 166.81(15) . . . . ? C64 N4 C46 C47 -18.1(2) . . . . ? C64 C65 C66 C67 -7.2(9) . . . . ? C64 C65 C70 C71 110.0(4) . . . . ? C64 C65 C70 C73 -128.1(4) . . . . ? C64 C69 C75 C76 95.43(19) . . . . ? C64 C69 C75 C78 -138.25(16) . . . . ? C64 C69 C68A C67A 5.4(17) . . . . ? C65 C64 C69 C68 -2.8(8) . . . . ? C65 C64 C69 C75 171.0(3) . . . . ? C65 C66 C67 C68 -2.1(13) . . . . ? C65 C70 C71 C72 -157.6(4) . . . . ? C65 C70 C73 C74 50.0(5) . . . . ? C66 C65 C70 C71 -70.9(6) . . . . ? C66 C65 C70 C73 51.1(6) . . . . ? C66 C67 C68 C69 8.7(18) . . . . ? C67 C68 C69 C64 -6.1(15) . . . . ? C67 C68 C69 C75 179.8(9) . . . . ? C68 C69 C75 C76 -90.5(7) . . . . ? C68 C69 C75 C78 35.8(8) . . . . ? C69 C64 C65 C66 9.5(6) . . . . ? C69 C64 C65 C70 -171.4(3) . . . . ? C69 C64 C65A C70A 169.3(5) . . . . ? C69 C64 C65A C66A -10.7(7) . . . . ? C69 C75 C76 C77 60.1(2) . . . . ? C69 C75 C78 C79 55.9(2) . . . . ? C69 C68A C67A C66A -8(2) . . . . ? C75 C69 C68A C67A 179.5(11) . . . . ? C76 C75 C78 C79 -177.21(16) . . . . ? C78 C75 C76 C77 -67.8(2) . . . . ? C80 O2 C84 C83 59.15(19) . . . . ? C80 C81 C82 C83 -52.9(2) . . . . ? C81 C82 C83 C84 52.1(2) . . . . ? C82 C83 C84 O2 -55.19(19) . . . . ? C84 O2 C80 C81 -60.16(18) . . . . ? C85 C86 C87 Ca3 141.39(12) . . . . ? C85 C86 C87 C88 -163.94(15) . . . . ? C86 N5 C90 C91 -106.57(17) . . . . ? C86 N5 C90 C95 77.27(18) . . . . ? C86 C87 C88 Ca3 -54.56(16) . . . . ? C86 C87 C88 N6 -22.2(3) . . . . ? C86 C87 C88 C89 160.81(16) . . . . ? C88 N6 C106 C107 -88.99(18) . . . . ? C88 N6 C106 C111 91.95(19) . . . . ? C90 N5 C86 Ca3 158.43(14) . . . . ? C90 N5 C86 C85 22.8(2) . . . . ? C90 N5 C86 C87 -161.99(13) . . . . ? C90 C91 C92 C93 0.5(2) . . . . ? C90 C91 C96 C97 -98.36(17) . . . . ? C90 C91 C96 C99 134.40(15) . . . . ? C90 C95 C101 C102 139.58(16) . . . . ? C90 C95 C101 C104 -94.13(19) . . . . ? C91 C90 C95 C94 0.8(2) . . . . ? C91 C90 C95 C101 -177.95(15) . . . . ? C91 C92 C93 C94 -0.3(3) . . . . ? C91 C96 C97 C98 -67.48(19) . . . . ? C91 C96 C99 C100 -68.20(17) . . . . ? C92 C91 C96 C97 80.56(18) . . . . ? C92 C91 C96 C99 -46.7(2) . . . . ? C92 C93 C94 C95 0.5(3) . . . . ? C93 C94 C95 C90 -0.7(3) . . . . ? C93 C94 C95 C101 178.10(17) . . . . ? C94 C95 C101 C102 -39.2(2) . . . . ? C94 C95 C101 C104 87.11(19) . . . . ? C95 C90 C91 C92 -0.7(2) . . . . ? C95 C90 C91 C96 178.22(14) . . . . ? C95 C101 C102 C103 -56.8(2) . . . . ? C95 C101 C104 C105 -56.1(2) . . . . ? C96 C91 C92 C93 -178.50(15) . . . . ? C97 C96 C99 C100 164.15(13) . . . . ? C99 C96 C97 C98 61.72(19) . . . . ? C102 C101 C104 C105 71.6(2) . . . . ? C104 C101 C102 C103 174.74(15) . . . . ? C106 N6 C88 Ca3 -151.72(13) . . . . ? C106 N6 C88 C87 170.78(13) . . . . ? C106 N6 C88 C89 -12.4(2) . . . . ? C106 C107 C108 C109 1.8(3) . . . . ? C106 C107 C112 C113 86.1(2) . . . . ? C106 C107 C112 C115 -147.32(17) . . . . ? C106 C111 C117 C118 82.96(19) . . . . ? C106 C111 C117 C120 -149.96(16) . . . . ? C107 C106 C111 C110 3.1(3) . . . . ? C107 C106 C111 C117 -173.16(16) . . . . ? C107 C108 C109 C110 1.6(3) . . . . ? C107 C112 C113 C114 56.5(2) . . . . ? C107 C112 C115 C116 56.2(2) . . . . ? C108 C107 C112 C113 -94.5(2) . . . . ? C108 C107 C112 C115 32.0(3) . . . . ? C108 C109 C110 C111 -2.7(3) . . . . ? C109 C110 C111 C106 0.4(3) . . . . ? C109 C110 C111 C117 176.67(18) . . . . ? C110 C111 C117 C118 -93.23(19) . . . . ? C110 C111 C117 C120 33.9(2) . . . . ? C111 C106 C107 C108 -4.2(3) . . . . ? C111 C106 C107 C112 175.20(16) . . . . ? C111 C117 C118 C119 65.97(18) . . . . ? C111 C117 C120 C121 61.16(19) . . . . ? C112 C107 C108 C109 -177.55(19) . . . . ? C113 C112 C115 C116 -175.85(16) . . . . ? C115 C112 C113 C114 -71.5(2) . . . . ? C118 C117 C120 C121 -173.00(13) . . . . ? C120 C117 C118 C119 -62.74(18) . . . . ? C122 O3 C126 C125 60.55(18) . . . . ? C122 C123 C124 C125 -51.3(2) . . . . ? C123 C124 C125 C126 52.1(2) . . . . ? C124 C125 C126 O3 -56.4(2) . . . . ? C126 O3 C122 C123 -59.80(19) . . . . ? C34 C33 C36 C37 59.5(3) . . . . ? C36 C33 C34 C35 170.5(2) . . . . ? C70 C65 C66 C67 173.7(7) . . . . ? C71 C70 C73 C74 172.3(3) . . . . ? C73 C70 C71 C72 79.3(4) . . . . ? C34A C33A C36A C37A 179.8(9) . . . . ? C36A C33A C34A C35A -76.2(12) . . . . ? C71A C70A C73A C74A -172.7(5) . . . . ? C71A C70A C65A C64 81.2(7) . . . . ? C71A C70A C65A C66A -98.7(7) . . . . ? C73A C70A C71A C72A -72.1(6) . . . . ? C73A C70A C65A C64 -152.8(6) . . . . ? C73A C70A C65A C66A 27.2(9) . . . . ? O4A C132 C133 C134 51(2) . . . . ? C132 O4A C136 C135 54(2) . . . . ? C132 C133 C134 C135 -52(2) . . . . ? C133 C134 C135 C136 53.0(18) . . . . ? C134 C135 C136 O4A -57(2) . . . . ? C136 O4A C132 C133 -49.9(19) . . . . ? O4 C127 C128 C129 55.5(5) . . . . ? C127 O4 C131 C130 59.8(6) . . . . ? C127 C128 C129 C130 -53.9(6) . . . . ? C128 C129 C130 C131 55.1(7) . . . . ? C129 C130 C131 O4 -58.1(7) . . . . ? C131 O4 C127 C128 -60.5(5) . . . . ? C68A C69 C75 C76 -78.4(8) . . . . ? C68A C69 C75 C78 47.9(8) . . . . ? C68A C67A C66A C65A 0.1(17) . . . . ? C67A C66A C65A C64 8.7(12) . . . . ? C67A C66A C65A C70A -171.4(9) . . . . ? C65A C64 C69 C75 -169.9(4) . . . . ? C65A C64 C69 C68A 4.1(9) . . . . ? C65A C70A C71A C72A 56.1(7) . . . . ? C65A C70A C73A C74A 59.6(7) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 8.3648 12.8585 3.3858 0.2029 0.4247 -0.8823 -0.9995 -1.9982 0.0010 -0.0415 -0.1057 0.1131 -6.5874 2.8212 10.5936 0.8524 -0.5215 -0.0376 0.9992 -0.0011 -1.0002 -0.0923 0.0610 -0.0220 -11.2231 -2.8773 5.6922 0.7551 -0.4625 0.4647 -10.3175 -10.9364 -8.0999 -0.0581 0.0345 0.9977 10.7527 10.8187 7.5106 0.0080 -0.0039 -1.0000 0.0762 10.5430 10.1091 0.8040 -0.1047 -0.5853 -11.9809 0.0041 -0.6419 0.8345 0.1546 0.5289 2.0228 0.6742 -12.7079 -0.3784 0.9124 0.1557 -2.9254 -4.5151 10.6630 0.1826 -0.9813 0.0608 1.4264 -0.0949 12.9585 0.1722 -0.9282 -0.3297 0.9995 0.9991 -0.0004 -0.0146 0.0483 -0.0781 11.3921 -0.4698 -3.5550 -0.9091 0.1186 -0.3993 0.9990 -2.0005 -1.9995 -0.2260 0.0163 0.0691 1.9989 -1.9997 -0.9990 -0.2753 -0.0630 0.0051 0.9996 -1.9985 0.0012 -0.1830 -0.1240 0.0271 8.7814 -4.1416 3.1782 -0.7859 -0.5412 -0.2992 0.8859 5.6996 13.7487 0.5529 -0.6459 -0.5264 -7.4410 -1.8520 10.1143 0.6400 -0.7486 0.1732 -12.0862 -8.7780 0.6825 0.3771 -0.4419 0.8139 -7.8943 3.7987 -5.6399 0.6509 0.6862 0.3247 -5.9800 -10.1403 -11.8944 -0.4019 0.3071 0.8627 loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.500 -0.669 0.169 1714.5 340.0 ?