#------------------------------------------------------------------------------ #$Date: 2025-02-07 03:14:43 +0200 (Fri, 07 Feb 2025) $ #$Revision: 297626 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/38/1573856.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573856 loop_ _publ_author_name 'Meher, Niranjan' 'Khatun, Mst Nasima' 'Parui, Retwik' 'Iyer, Parameswar K.' _publ_section_title ; Non-Conjugated Alkyl Chains Engineering to Tune Condensed State Photophysical and Supramolecular Assembly Properties ; _journal_name_full Nanoscale _journal_paper_doi 10.1039/D5NR00163C _journal_year 2025 _chemical_formula_sum 'C17 H17 N O2' _chemical_formula_weight 267.31 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _audit_update_record ; 2024-07-30 deposited with the CCDC. 2025-02-06 downloaded from the CCDC. ; _cell_angle_alpha 89.903(9) _cell_angle_beta 89.916(9) _cell_angle_gamma 81.105(9) _cell_formula_units_Z 4 _cell_length_a 9.639(3) _cell_length_b 9.806(3) _cell_length_c 14.785(4) _cell_measurement_reflns_used 6979 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 21.67 _cell_measurement_theta_min 2.51 _cell_volume 1380.7(7) _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0689 _diffrn_reflns_av_unetI/netI 0.0302 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 56551 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.000 _diffrn_reflns_theta_max 25.000 _diffrn_reflns_theta_min 1.377 _exptl_absorpt_coefficient_mu 0.084 _exptl_crystal_colour Colourless _exptl_crystal_density_diffrn 1.286 _exptl_crystal_description block _exptl_crystal_F_000 568 _refine_diff_density_max 0.385 _refine_diff_density_min -0.274 _refine_diff_density_rms 0.050 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.141 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 363 _refine_ls_number_reflns 4856 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.141 _refine_ls_R_factor_all 0.0897 _refine_ls_R_factor_gt 0.0595 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.2751P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1643 _refine_ls_wR_factor_ref 0.1966 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3189 _reflns_number_total 4856 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d5nr00163c2.cif _cod_data_source_block CN-5_0m_a _cod_original_cell_volume 1380.6(7) _cod_database_code 1573856 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL CN-5_0m_a.res in P-1 CN-5_0m_a.res created by SHELXL-2016/6 at 12:53:41 on 09-Aug-2019 CELL 0.71073 9.6391 9.8056 14.7851 89.903 89.916 81.105 ZERR 4.000 0.0028 0.0029 0.0044 0.009 0.009 0.009 LATT 1 SFAC C H N O UNIT 68 68 4 8 OMIT -3 50 REM Old TITL CN-5_0m in P-1 REM SHELXT solution in P-1 REM R1 0.189, Rweak 0.008, Alpha 0.036, Orientation as input REM Formula found by SHELXT: C34 N2 O4 L.S. 40 ACTA BOND $H FMAP 2 PLAN 4 TEMP 23.000 WGHT 0.100000 0.275050 FVAR 0.62001 O001 4 0.275334 0.192866 0.142017 11.00000 0.06921 0.08265 = 0.04733 -0.00672 -0.01460 -0.01481 O002 4 0.775018 0.192966 0.357905 11.00000 0.06945 0.08263 = 0.04682 0.01015 0.01362 -0.01391 O003 4 0.363503 0.406716 0.474182 11.00000 0.07211 0.06112 = 0.06307 0.00532 -0.01001 0.01282 O004 4 -0.136424 0.406856 0.025688 11.00000 0.07197 0.05998 = 0.06541 -0.00231 0.00837 0.01371 N005 3 0.570922 0.301105 0.417239 11.00000 0.05883 0.04217 = 0.03766 0.00762 -0.00447 -0.01105 N006 3 0.070840 0.301263 0.082758 11.00000 0.05915 0.04241 = 0.03756 -0.00432 0.00262 -0.01079 C007 1 0.595680 0.111620 0.561087 11.00000 0.04463 0.03789 = 0.03243 -0.00194 -0.00549 -0.01255 C008 1 0.095394 0.111749 -0.061064 11.00000 0.04481 0.03885 = 0.03145 0.00289 0.00350 -0.01275 C009 1 0.477395 0.214683 0.556021 11.00000 0.04681 0.04104 = 0.03670 -0.00214 -0.00235 -0.00948 C00A 1 -0.022424 0.214469 -0.056051 11.00000 0.04496 0.04136 = 0.03675 0.00448 0.00079 -0.00983 C00B 1 0.699570 0.099154 0.493453 11.00000 0.04565 0.04239 = 0.03497 -0.00159 -0.00515 -0.01053 C00C 1 0.199925 0.099508 0.006615 11.00000 0.04474 0.04296 = 0.03550 0.00244 0.00337 -0.00966 C00D 1 0.111077 0.017610 -0.134947 11.00000 0.05565 0.04223 = 0.03597 0.00048 0.00618 -0.01508 C00E 1 0.611400 0.017337 0.635002 11.00000 0.05649 0.04455 = 0.03554 0.00283 -0.00744 -0.01709 C00F 1 0.462985 0.314686 0.480931 11.00000 0.05270 0.04280 = 0.04208 0.00152 -0.01011 -0.00481 C00G 1 -0.037070 0.314745 0.018984 11.00000 0.05376 0.04200 = 0.04306 0.00194 0.00753 -0.00577 C00H 1 0.186769 0.198699 0.082211 11.00000 0.05179 0.05016 = 0.03506 0.00213 -0.00100 -0.01562 C00I 1 0.686664 0.198643 0.417562 11.00000 0.05195 0.04948 = 0.03629 0.00103 -0.00198 -0.01469 C00J 1 0.313360 -0.003188 0.001614 11.00000 0.04920 0.05640 = 0.04566 0.00567 -0.00097 -0.00458 AFIX 43 H00J 2 0.380409 -0.012218 0.047286 11.00000 -1.20000 AFIX 0 C00K 1 0.813231 -0.003062 0.498370 11.00000 0.04957 0.05696 = 0.04660 -0.00293 0.00129 -0.00401 AFIX 43 H00K 2 0.880390 -0.011823 0.452660 11.00000 -1.20000 AFIX 0 C00L 1 0.505907 0.031135 0.701771 11.00000 0.07322 0.05738 = 0.04095 0.00789 0.00242 -0.01977 AFIX 43 H00L 2 0.514505 -0.028706 0.751012 11.00000 -1.20000 AFIX 0 C00M 1 0.730813 -0.084594 0.638378 11.00000 0.06810 0.04627 = 0.04735 0.00824 -0.01728 -0.00845 AFIX 43 H00M 2 0.742662 -0.145938 0.686797 11.00000 -1.20000 AFIX 0 C00N 1 0.231017 -0.084672 -0.138063 11.00000 0.06957 0.04609 = 0.04668 -0.00585 0.01517 -0.00747 AFIX 43 H00N 2 0.242997 -0.146143 -0.186297 11.00000 -1.20000 AFIX 0 C00O 1 0.005322 0.031382 -0.201638 11.00000 0.07357 0.05831 = 0.04156 -0.00592 -0.00297 -0.02085 AFIX 43 H00O 2 0.013863 -0.028534 -0.250721 11.00000 -1.20000 AFIX 0 C00P 1 -0.018359 0.375762 0.236073 11.00000 0.06009 0.05288 = 0.04422 -0.00562 0.00158 -0.01151 AFIX 23 H00A 2 0.032150 0.294895 0.265944 11.00000 -1.20000 H00B 2 -0.108850 0.354152 0.217291 11.00000 -1.20000 AFIX 0 C00Q 1 0.481453 0.375990 0.263960 11.00000 0.05993 0.05267 = 0.04568 0.00782 -0.00302 -0.01208 AFIX 23 H00C 2 0.390941 0.354314 0.282864 11.00000 -1.20000 H00D 2 0.532050 0.295195 0.234144 11.00000 -1.20000 AFIX 0 C00R 1 0.375914 0.223814 0.621927 11.00000 0.05241 0.05745 = 0.05484 -0.00268 0.00514 -0.00717 AFIX 43 H00R 2 0.296925 0.291306 0.618195 11.00000 -1.20000 AFIX 0 C00S 1 -0.124258 0.223546 -0.121876 11.00000 0.05159 0.05719 = 0.05653 0.00432 -0.00863 -0.00581 AFIX 43 H00S 2 -0.203334 0.290903 -0.117948 11.00000 -1.20000 AFIX 0 C00T 1 0.829245 -0.094872 0.571944 11.00000 0.05793 0.05152 = 0.05973 0.00233 -0.01239 0.00394 AFIX 43 H00T 2 0.907690 -0.163075 0.575181 11.00000 -1.20000 AFIX 0 C00U 1 0.329466 -0.094858 -0.071647 11.00000 0.06080 0.05204 = 0.05896 0.00036 0.00983 0.00230 AFIX 43 H00U 2 0.407946 -0.163027 -0.074830 11.00000 -1.20000 AFIX 0 C00V 1 0.562321 0.408368 0.345942 11.00000 0.07650 0.04635 = 0.04874 0.01262 -0.00746 -0.01901 AFIX 23 H00E 2 0.656713 0.418987 0.327575 11.00000 -1.20000 H00F 2 0.517980 0.495713 0.371001 11.00000 -1.20000 AFIX 0 C00W 1 0.062583 0.408156 0.154039 11.00000 0.07812 0.04556 = 0.04756 -0.01083 0.00747 -0.01827 AFIX 23 H00G 2 0.018527 0.495715 0.129023 11.00000 -1.20000 H00H 2 0.157058 0.418374 0.172256 11.00000 -1.20000 AFIX 0 C00X 1 -0.108816 0.131122 -0.194993 11.00000 0.06486 0.07239 = 0.05187 0.00175 -0.01994 -0.01987 AFIX 43 H00X 2 -0.177714 0.138344 -0.239461 11.00000 -1.20000 AFIX 0 C00Y 1 0.391646 0.130918 0.695080 11.00000 0.06778 0.07345 = 0.05064 0.00069 0.01798 -0.02064 AFIX 43 H00Y 2 0.322710 0.137873 0.739630 11.00000 -1.20000 AFIX 0 C00Z 1 0.458799 0.496238 0.196808 11.00000 0.06561 0.07798 = 0.05509 0.01846 -0.00919 -0.01058 AFIX 23 H00I 2 0.398832 0.472768 0.148463 11.00000 -1.20000 H00P 2 0.408824 0.576455 0.227562 11.00000 -1.20000 AFIX 0 C010 1 -0.041192 0.496235 0.303328 11.00000 0.06732 0.08206 = 0.05456 -0.01624 0.00934 -0.01075 AFIX 23 H01A 2 -0.091048 0.576514 0.272493 11.00000 -1.20000 H01B 2 -0.101378 0.472673 0.351691 11.00000 -1.20000 AFIX 0 C011 1 0.086201 0.534503 0.343861 11.00000 0.07246 0.09030 = 0.07137 -0.02609 0.00070 -0.01361 AFIX 23 H01C 2 0.144643 0.563021 0.296108 11.00000 -1.20000 H01D 2 0.138547 0.453731 0.372804 11.00000 -1.20000 AFIX 0 C012 1 0.585777 0.534249 0.156525 11.00000 0.07590 0.09353 = 0.07313 0.03072 -0.00298 -0.01604 AFIX 23 H01E 2 0.638208 0.453450 0.127743 11.00000 -1.20000 H01F 2 0.643966 0.562592 0.204304 11.00000 -1.20000 AFIX 0 C013 1 0.558084 0.649468 0.087238 11.00000 0.11707 0.09453 = 0.08284 0.04520 0.00100 -0.02876 AFIX 137 H01G 2 0.499836 0.622821 0.039848 11.00000 -1.50000 H01H 2 0.645602 0.666786 0.062118 11.00000 -1.50000 H01I 2 0.511288 0.731720 0.115898 11.00000 -1.50000 AFIX 0 C014 1 0.057736 0.649365 0.412804 11.00000 0.11676 0.09612 = 0.08314 -0.04449 -0.00086 -0.02768 AFIX 137 H01J 2 0.012263 0.731947 0.383781 11.00000 -1.50000 H01K 2 0.144860 0.665921 0.438708 11.00000 -1.50000 H01L 2 -0.001972 0.623087 0.459659 11.00000 -1.50000 AFIX 0 HKLF 4 REM CN-5_0m_a.res in P-1 REM R1 = 0.0595 for 3189 Fo > 4sig(Fo) and 0.0897 for all 4856 data REM 363 parameters refined using 0 restraints END WGHT 0.0878 0.7262 REM Highest difference peak 0.385, deepest hole -0.274, 1-sigma level 0.050 Q1 1 0.0444 0.4182 0.3271 11.00000 0.05 0.39 Q2 1 0.0006 0.6037 0.3113 11.00000 0.05 0.39 Q3 1 0.5374 0.4232 0.1655 11.00000 0.05 0.37 Q4 1 0.4978 0.6050 0.1892 11.00000 0.05 0.34 ; _shelx_res_checksum 98197 _shelx_hkl_file ; -1 0 0 0.30 0.20 -1 0 0 2.10 0.30 -1 0 0 0.90 0.30 1 0 0 1.40 0.20 1 0 0 1.80 0.60 1 0 0 0.50 0.30 -2 0 0 1312.97 61.69 -2 0 0 1401.06 61.39 -2 0 0 1422.36 61.99 -2 0 0 1434.66 61.99 -2 0 0 1403.66 62.09 2 0 0 1321.17 62.19 2 0 0 1314.17 61.49 2 0 0 1363.66 62.19 2 0 0 1397.16 62.19 2 0 0 1260.67 61.49 2 0 0 1317.47 61.99 2 0 0 1317.77 62.69 2 0 0 1384.96 62.19 2 0 0 1350.56 63.19 2 0 0 1304.87 62.29 -3 0 0 -0.20 0.50 -3 0 0 0.10 0.40 -3 0 0 0.40 0.70 -3 0 0 0.20 0.60 -3 0 0 -0.80 0.60 3 0 0 0.30 0.60 3 0 0 0.50 0.80 3 0 0 -1.10 1.00 3 0 0 -0.30 0.50 3 0 0 -0.20 0.40 3 0 0 1.00 0.90 3 0 0 0.30 0.60 3 0 0 -0.50 0.50 3 0 0 -0.40 0.40 -4 0 0 1.70 0.60 -4 0 0 2.20 0.80 -4 0 0 2.40 1.10 -4 0 0 0.20 1.00 -4 0 0 0.60 1.10 -4 0 0 2.90 1.20 4 0 0 3.30 1.30 4 0 0 0.50 0.80 4 0 0 1.60 0.80 4 0 0 1.90 1.20 4 0 0 2.20 1.00 4 0 0 0.60 0.70 4 0 0 0.90 0.90 4 0 0 0.20 0.90 4 0 0 2.60 2.10 -5 0 0 0.50 1.00 -5 0 0 -0.30 1.30 -5 0 0 0.40 1.40 -5 0 0 -0.50 1.20 -5 0 0 -0.30 0.90 -5 0 0 -0.40 0.60 -5 0 0 -1.50 0.80 5 0 0 0.30 1.00 5 0 0 -1.50 1.10 5 0 0 2.40 1.40 5 0 0 -1.10 0.60 5 0 0 0.20 0.80 5 0 0 -0.20 1.00 5 0 0 0.00 1.00 5 0 0 1.70 1.40 5 0 0 -0.70 1.10 -6 0 0 -0.80 1.50 -6 0 0 2.20 1.90 -6 0 0 -0.40 1.10 -6 0 0 -0.10 0.90 -6 0 0 2.80 1.80 -6 0 0 2.30 1.30 -6 0 0 -1.40 1.30 6 0 0 3.50 2.00 6 0 0 1.40 1.20 6 0 0 1.20 1.60 6 0 0 1.50 1.60 6 0 0 1.70 1.80 6 0 0 1.60 1.60 6 0 0 0.40 2.10 6 0 0 3.20 1.80 6 0 0 0.90 1.80 -7 0 0 1.00 1.70 -7 0 0 0.20 1.80 -7 0 0 0.00 1.30 -7 0 0 -1.90 1.50 -7 0 0 -0.40 1.70 7 0 0 1.40 2.10 7 0 0 0.50 1.20 7 0 0 -0.70 3.00 7 0 0 -1.00 1.30 7 0 0 0.20 1.60 7 0 0 1.60 1.90 7 0 0 -1.20 1.40 -8 0 0 1.80 1.90 -8 0 0 -0.10 1.70 -8 0 0 0.30 2.50 -8 0 0 1.10 1.90 -8 0 0 -2.50 2.10 8 0 0 -0.70 1.60 8 0 0 1.30 2.60 8 0 0 2.70 2.70 8 0 0 -1.20 1.70 8 0 0 -1.60 1.80 8 0 0 2.20 4.50 8 0 0 1.30 1.70 -9 0 0 4.20 3.10 -9 0 0 2.70 2.60 -9 0 0 7.50 3.40 -9 0 0 2.40 2.10 -9 0 0 0.80 3.10 9 0 0 1.70 2.40 9 0 0 -1.40 5.10 9 0 0 4.80 2.70 9 0 0 2.70 3.50 9 0 0 0.50 2.40 9 0 0 4.40 3.10 -10 0 0 10.90 4.30 -10 0 0 24.30 5.20 -10 0 0 12.00 4.40 -10 0 0 12.70 4.00 10 0 0 13.80 4.60 10 0 0 18.50 5.00 10 0 0 16.10 7.30 10 0 0 15.40 5.30 10 0 0 20.30 5.80 10 0 0 28.00 5.70 -11 0 0 2.70 3.80 -11 0 0 0.30 3.10 -11 0 0 -3.00 2.20 -11 0 0 -3.00 3.50 11 0 0 0.30 2.80 11 0 0 7.90 4.60 11 0 0 1.80 7.30 11 0 0 4.10 2.80 11 0 0 -2.40 2.70 11 0 0 0.50 3.20 -12 0 0 -1.90 2.50 -12 0 0 3.00 4.40 -12 0 0 3.30 3.40 12 0 0 -1.40 3.10 12 0 0 -1.50 4.80 12 0 0 7.60 4.40 12 0 0 3.70 4.60 12 0 0 2.90 3.20 11 -1 0 -0.60 3.40 11 -1 0 -3.80 2.70 11 -1 0 0.90 7.20 11 -1 0 -0.20 2.80 11 -1 0 -0.90 2.70 11 -1 0 3.30 3.60 -11 1 0 -0.70 3.60 -11 1 0 -4.30 2.80 -11 1 0 -7.50 1.80 -11 1 0 -0.80 2.50 10 -1 0 2.00 3.10 10 -1 0 13.40 5.20 10 -1 0 2.80 6.80 10 -1 0 7.00 4.10 10 -1 0 12.20 4.00 10 -1 0 6.20 3.40 -10 1 0 7.20 3.60 -10 1 0 11.60 4.00 -10 1 0 7.80 4.10 -10 1 0 6.30 3.50 -10 1 0 7.90 3.60 9 -1 0 3.30 4.30 9 -1 0 -2.50 2.40 9 -1 0 1.10 3.20 9 -1 0 4.40 2.90 9 -1 0 -1.20 1.80 9 -1 0 -1.00 2.90 -9 1 0 1.10 3.00 -9 1 0 0.40 2.80 -9 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332.67 21.80 10 1 0 383.96 28.50 10 1 0 335.47 22.80 10 1 0 373.76 22.10 -11 -1 0 -2.70 3.10 -11 -1 0 2.80 3.80 -11 -1 0 -0.70 2.20 -11 -1 0 -6.80 2.70 11 1 0 1.50 2.60 11 1 0 5.00 8.40 11 1 0 -4.30 3.80 11 1 0 5.40 3.20 11 1 0 6.40 4.20 11 1 0 1.60 2.50 -12 -1 0 -0.20 3.90 -12 -1 0 2.80 4.40 -12 -1 0 5.20 4.50 -12 -1 0 1.50 3.10 -12 -1 0 -0.20 2.90 12 1 0 -6.10 4.50 12 1 0 -2.50 2.50 12 1 0 -1.40 3.50 12 1 0 0.40 2.70 12 1 0 -2.60 2.30 11 -2 0 -0.60 3.20 11 -2 0 -0.20 11.90 11 -2 0 0.30 2.90 11 -2 0 2.50 3.60 11 -2 0 -4.30 3.30 -11 2 0 0.20 3.50 -11 2 0 0.90 2.40 -11 2 0 -4.90 2.90 10 -2 0 -2.90 4.00 10 -2 0 -0.40 2.50 10 -2 0 -4.10 3.20 10 -2 0 0.80 3.40 10 -2 0 -0.10 2.30 -10 2 0 1.50 3.10 -10 2 0 3.70 2.90 -10 2 0 -5.00 2.60 -10 2 0 0.70 2.60 -10 2 0 -0.60 2.40 9 -2 0 1.90 2.40 9 -2 0 0.70 5.20 9 -2 0 -1.00 2.30 9 -2 0 -2.20 2.10 9 -2 0 2.10 2.50 9 -2 0 -3.20 2.50 9 -2 0 2.10 2.30 -9 2 0 -1.60 2.00 -9 2 0 0.40 2.00 -9 2 0 1.60 2.50 -9 2 0 -0.50 3.10 8 -2 0 18.00 4.80 8 -2 0 15.70 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0 287.17 16.50 4 -2 0 289.67 15.60 4 -2 0 281.97 16.00 4 -2 0 297.17 16.20 4 -2 0 296.97 16.00 -4 2 0 308.07 16.00 -4 2 0 325.87 16.10 -4 2 0 307.17 15.40 -4 2 0 307.17 16.20 -4 2 0 302.57 15.30 -4 2 0 298.27 14.90 3 -2 0 0.20 0.70 3 -2 0 -0.10 0.90 3 -2 0 0.30 0.60 3 -2 0 0.50 1.30 3 -2 0 0.20 0.60 3 -2 0 0.40 0.90 3 -2 0 1.30 0.90 3 -2 0 2.10 1.30 3 -2 0 0.30 1.10 -3 2 0 1.20 1.00 -3 2 0 1.40 1.00 -3 2 0 0.90 0.90 -3 2 0 1.90 1.00 -3 2 0 -0.10 0.90 -3 2 0 0.00 1.00 2 -2 0 870.51 40.30 2 -2 0 804.42 39.80 2 -2 0 860.71 40.40 2 -2 0 848.12 40.00 2 -2 0 850.31 40.10 2 -2 0 855.31 39.70 2 -2 0 873.31 40.40 2 -2 0 855.51 40.00 -2 2 0 818.72 39.80 -2 2 0 799.22 39.90 -2 2 0 821.12 39.60 -2 2 0 862.81 39.90 -2 2 0 892.31 39.70 -2 2 0 863.61 39.50 1 -2 0 0.80 0.60 1 -2 0 0.50 0.60 1 -2 0 0.60 0.60 1 -2 0 0.70 0.90 1 -2 0 -1.20 0.70 1 -2 0 -0.40 0.70 1 -2 0 0.30 0.50 -1 2 0 -0.30 0.60 -1 2 0 -0.60 0.50 -1 2 0 0.70 0.60 -1 2 0 0.30 0.80 -1 2 0 1.50 0.70 0 -2 0 341.97 15.80 0 -2 0 329.87 16.00 0 -2 0 326.97 16.10 0 -2 0 314.57 16.10 0 2 0 332.67 15.80 0 2 0 314.77 15.90 0 2 0 322.57 15.60 0 2 0 335.77 15.80 -1 -2 0 0.30 0.50 -1 -2 0 0.50 0.50 -1 -2 0 0.20 0.70 -1 -2 0 -0.90 0.30 1 2 0 1.20 0.70 1 2 0 -0.70 0.60 1 2 0 -0.70 0.40 1 2 0 -0.30 0.50 1 2 0 -1.10 0.90 -2 -2 0 575.74 26.30 -2 -2 0 577.54 27.10 -2 -2 0 557.94 26.80 -2 -2 0 529.65 27.30 2 2 0 546.95 26.20 2 2 0 549.25 27.10 2 2 0 567.34 27.10 2 2 0 581.04 27.30 2 2 0 565.24 27.00 2 2 0 556.84 26.40 2 2 0 594.74 27.30 2 2 0 559.94 28.50 -3 -2 0 1.30 1.10 -3 -2 0 0.00 0.60 -3 -2 0 -0.90 0.80 -3 -2 0 -0.70 0.50 -3 -2 0 -1.20 0.40 3 2 0 0.10 0.40 3 2 0 -0.20 0.60 3 2 0 -0.10 0.50 3 2 0 1.40 0.90 3 2 0 0.10 0.70 3 2 0 0.20 0.80 3 2 0 -1.00 0.80 3 2 0 -1.10 0.60 3 2 0 -1.20 0.70 -4 -2 0 15.50 2.20 -4 -2 0 16.30 3.10 -4 -2 0 17.60 2.70 -4 -2 0 16.10 2.70 -4 -2 0 21.10 2.30 4 2 0 19.00 3.00 4 2 0 19.20 2.10 4 2 0 22.80 3.00 4 2 0 19.00 1.50 4 2 0 15.40 2.70 4 2 0 17.70 3.00 4 2 0 18.90 2.70 4 2 0 15.30 2.90 -5 -2 0 2.00 1.10 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-0.20 0.60 -1 3 0 1.50 0.80 -1 3 0 0.20 0.80 -1 3 0 0.20 0.70 -1 3 0 0.50 0.80 -1 3 0 -0.20 0.60 -1 3 0 1.60 1.20 0 -3 0 6.10 1.40 0 -3 0 4.70 1.40 0 -3 0 4.50 1.20 0 -3 0 5.00 1.50 0 -3 0 2.20 1.00 0 -3 0 7.30 1.50 0 -3 0 4.30 1.20 0 -3 0 7.90 1.50 0 3 0 8.60 1.40 0 3 0 3.90 0.90 0 3 0 6.50 1.30 0 3 0 5.50 1.50 0 3 0 4.50 1.40 0 3 0 5.00 1.50 -1 -3 0 -0.10 1.10 -1 -3 0 0.00 0.60 -1 -3 0 -0.20 0.70 -1 -3 0 -1.60 0.80 -1 -3 0 0.00 0.50 -1 -3 0 -1.30 0.60 1 3 0 -0.10 0.60 1 3 0 0.30 0.80 1 3 0 -0.10 0.60 1 3 0 -0.60 0.80 1 3 0 0.30 0.70 1 3 0 0.40 0.60 1 3 0 1.70 0.80 1 3 0 -0.30 0.90 -2 -3 0 576.24 26.20 -2 -3 0 549.25 26.40 -2 -3 0 491.35 26.30 -2 -3 0 496.45 26.50 -2 -3 0 520.95 25.30 2 3 0 541.85 26.40 2 3 0 526.45 25.40 2 3 0 577.34 26.50 2 3 0 501.45 26.10 2 3 0 540.35 25.70 2 3 0 565.24 26.40 2 3 0 538.65 26.20 2 3 0 539.75 25.10 -3 -3 0 0.10 0.70 -3 -3 0 0.80 0.70 -3 -3 0 -0.20 0.60 -3 -3 0 0.90 0.90 -3 -3 0 -1.10 1.20 3 3 0 1.20 1.00 3 3 0 -0.70 0.60 3 3 0 0.30 0.60 3 3 0 -0.20 0.80 3 3 0 1.10 0.80 3 3 0 -1.70 1.40 3 3 0 -0.70 1.10 3 3 0 0.30 0.80 -4 -3 0 32.20 4.10 -4 -3 0 36.60 4.00 -4 -3 0 37.60 3.00 -4 -3 0 32.50 2.80 -4 -3 0 33.00 4.60 4 3 0 34.40 2.90 4 3 0 28.70 4.00 4 3 0 29.00 3.90 4 3 0 28.20 4.10 4 3 0 33.80 2.60 4 3 0 30.90 4.10 4 3 0 35.70 4.00 4 3 0 34.30 4.20 -5 -3 0 -2.00 1.10 -5 -3 0 0.00 1.00 -5 -3 0 -0.40 1.20 -5 -3 0 -1.80 0.80 -5 -3 0 -0.80 0.80 5 3 0 0.50 0.60 5 3 0 1.90 1.10 5 3 0 0.40 1.10 5 3 0 0.00 1.20 5 3 0 1.80 2.80 5 3 0 -1.00 0.70 5 3 0 1.20 1.80 5 3 0 0.00 0.90 5 3 0 -2.70 1.20 -6 -3 0 3.10 1.70 -6 -3 0 -0.10 1.30 -6 -3 0 1.50 1.50 -6 -3 0 4.30 2.60 -6 -3 0 0.20 1.20 6 3 0 0.40 1.20 6 3 0 -0.60 1.10 6 3 0 0.50 2.20 6 3 0 -0.20 1.40 6 3 0 0.10 2.00 6 3 0 2.90 3.40 6 3 0 0.80 1.00 6 3 0 0.30 1.90 -7 -3 0 -1.50 1.30 -7 -3 0 -0.70 1.30 -7 -3 0 0.80 1.70 -7 -3 0 1.60 2.10 -7 -3 0 0.20 1.50 7 3 0 -1.20 1.40 7 3 0 1.50 1.60 7 3 0 0.30 1.80 7 3 0 -0.20 1.70 7 3 0 -0.10 1.40 7 3 0 -1.70 1.20 7 3 0 0.50 3.20 -8 -3 0 1.10 1.80 -8 -3 0 -1.40 1.50 -8 -3 0 0.10 2.90 -8 -3 0 -3.30 2.00 -8 -3 0 3.10 2.10 8 3 0 -1.80 2.20 8 3 0 1.50 1.90 8 3 0 0.90 1.80 8 3 0 4.10 5.60 8 3 0 2.80 2.20 8 3 0 0.50 2.00 8 3 0 0.40 2.00 -9 -3 0 -0.70 2.20 -9 -3 0 -0.60 2.80 -9 -3 0 1.10 3.20 -9 -3 0 -0.70 2.00 -9 -3 0 -1.60 1.70 9 3 0 0.30 2.30 9 3 0 -0.90 1.50 9 3 0 -1.30 3.90 9 3 0 4.60 3.10 9 3 0 0.50 2.80 9 3 0 2.90 3.60 -10 -3 0 3.30 3.10 -10 -3 0 6.60 3.00 -10 -3 0 5.20 3.10 10 3 0 3.50 4.60 10 3 0 13.50 8.20 10 3 0 -0.10 3.30 10 3 0 3.10 2.80 10 3 0 4.70 3.00 10 3 0 1.80 2.80 -11 -3 0 0.70 3.40 -11 -3 0 0.90 3.80 -11 -3 0 0.10 2.80 11 3 0 1.50 4.70 11 3 0 -2.40 2.90 11 3 0 -1.30 3.90 11 3 0 0.90 3.50 11 3 0 15.00 9.80 11 3 0 3.50 3.00 -12 -3 0 1.00 3.40 -12 -3 0 4.90 3.50 -12 -3 0 4.10 5.20 12 3 0 -0.70 2.70 12 3 0 -0.40 4.10 12 3 0 -1.10 5.00 12 3 0 -3.60 4.30 10 -4 0 2.80 3.10 10 -4 0 2.10 3.50 10 -4 0 -0.90 2.20 10 -4 0 2.20 4.10 10 -4 0 -0.60 4.10 -10 4 0 -2.30 3.70 -10 4 0 1.80 3.40 -10 4 0 5.90 3.60 9 -4 0 0.40 3.50 9 -4 0 0.20 2.20 9 -4 0 -1.40 2.70 9 -4 0 -0.70 3.10 9 -4 0 0.60 2.50 -9 4 0 -2.10 3.00 -9 4 0 -0.70 2.30 -9 4 0 -2.20 1.80 -9 4 0 2.50 3.80 8 -4 0 5.10 3.10 8 -4 0 5.30 3.50 8 -4 0 3.10 3.30 8 -4 0 4.50 2.80 8 -4 0 7.20 4.20 -8 4 0 2.60 3.40 -8 4 0 11.50 3.90 -8 4 0 8.70 4.00 -8 4 0 12.60 3.80 -8 4 0 6.60 3.30 7 -4 0 -0.10 2.30 7 -4 0 -3.00 1.70 7 -4 0 -1.00 2.90 7 -4 0 -3.70 2.50 7 -4 0 0.20 1.80 7 -4 0 0.00 3.50 7 -4 0 1.10 2.40 -7 4 0 -0.50 2.40 -7 4 0 -0.20 2.50 -7 4 0 -6.20 1.80 -7 4 0 1.90 2.00 -7 4 0 -4.60 2.30 6 -4 0 18.50 4.50 6 -4 0 9.20 2.80 6 -4 0 11.40 4.50 6 -4 0 15.00 3.70 6 -4 0 10.30 3.20 6 -4 0 16.30 3.60 6 -4 0 16.10 4.10 -6 4 0 7.40 3.40 -6 4 0 5.40 2.30 -6 4 0 12.30 3.30 -6 4 0 10.50 3.30 -6 4 0 14.40 3.20 5 -4 0 -0.50 1.40 5 -4 0 0.40 1.60 5 -4 0 -1.40 1.00 5 -4 0 1.20 1.30 5 -4 0 0.40 1.80 5 -4 0 1.70 1.90 5 -4 0 -1.80 1.10 5 -4 0 2.00 1.90 -5 4 0 0.20 1.60 -5 4 0 1.00 1.70 -5 4 0 -0.10 1.70 -5 4 0 0.40 1.90 -5 4 0 0.70 1.50 -5 4 0 1.30 1.30 4 -4 0 13.70 3.00 4 -4 0 15.00 2.90 4 -4 0 11.10 3.20 4 -4 0 10.60 3.20 4 -4 0 9.80 2.50 4 -4 0 11.30 2.80 4 -4 0 14.00 3.40 4 -4 0 11.70 2.80 4 -4 0 11.70 2.10 -4 4 0 9.30 2.30 -4 4 0 17.10 3.50 -4 4 0 15.30 2.90 -4 4 0 15.40 2.80 -4 4 0 12.50 2.90 -4 4 0 9.80 2.40 3 -4 0 -2.40 0.80 3 -4 0 0.10 1.10 3 -4 0 0.40 0.90 3 -4 0 -0.70 1.20 3 -4 0 1.20 1.20 3 -4 0 2.10 1.60 3 -4 0 0.00 0.70 3 -4 0 -0.80 1.80 3 -4 0 0.40 1.30 -3 4 0 -0.80 0.90 -3 4 0 0.10 1.60 -3 4 0 0.00 0.90 -3 4 0 -0.50 1.40 -3 4 0 -0.10 1.00 -3 4 0 -0.70 1.00 -3 4 0 1.50 1.70 2 -4 0 795.22 38.60 2 -4 0 785.72 39.20 2 -4 0 831.82 39.60 2 -4 0 812.82 39.60 2 -4 0 805.22 39.70 2 -4 0 839.42 38.70 2 -4 0 840.42 39.40 2 -4 0 822.22 39.70 -2 4 0 800.62 38.90 -2 4 0 823.92 38.80 -2 4 0 814.92 38.20 -2 4 0 787.02 38.80 -2 4 0 772.82 39.00 -2 4 0 799.72 38.80 1 -4 0 -1.00 0.60 1 -4 0 -0.70 1.00 1 -4 0 -1.90 0.60 1 -4 0 -0.30 0.80 1 -4 0 -0.20 1.10 1 -4 0 0.60 1.30 1 -4 0 1.10 1.30 1 -4 0 0.70 0.90 -1 4 0 0.00 0.90 -1 4 0 -0.20 0.70 -1 4 0 -0.30 0.80 -1 4 0 -0.60 0.80 -1 4 0 0.40 0.90 -1 4 0 1.30 0.90 0 -4 0 93.89 5.90 0 -4 0 77.99 6.00 0 -4 0 96.39 6.10 0 -4 0 89.49 5.90 0 -4 0 89.79 6.20 0 -4 0 91.59 6.30 0 -4 0 93.79 5.90 0 -4 0 82.99 5.80 0 4 0 81.39 5.50 0 4 0 83.89 5.40 0 4 0 91.79 5.90 0 4 0 82.09 5.40 0 4 0 88.99 5.80 0 4 0 84.29 5.70 -1 -4 0 -0.20 0.70 -1 -4 0 0.90 1.00 -1 -4 0 -1.50 1.20 -1 -4 0 -0.60 0.60 -1 -4 0 -1.40 0.90 -1 -4 0 -0.80 0.60 -1 -4 0 0.70 0.80 -1 -4 0 2.20 1.10 1 4 0 -0.70 0.50 1 4 0 -0.10 1.30 1 4 0 0.00 0.80 1 4 0 -0.90 0.50 1 4 0 -0.30 1.00 1 4 0 -1.30 0.90 1 4 0 1.90 1.10 1 4 0 -0.50 0.60 1 4 0 0.30 0.80 -2 -4 0 184.58 11.40 -2 -4 0 191.28 13.20 -2 -4 0 201.18 10.50 -2 -4 0 202.08 11.90 -2 -4 0 213.68 11.40 -2 -4 0 199.18 10.40 -2 -4 0 206.38 11.70 2 4 0 210.58 11.60 2 4 0 207.18 10.40 2 4 0 194.58 11.00 2 4 0 199.78 11.50 2 4 0 179.78 10.60 2 4 0 211.08 11.60 2 4 0 201.98 12.90 2 4 0 190.38 11.20 -3 -4 0 0.50 1.50 -3 -4 0 0.60 1.40 -3 -4 0 0.30 0.80 -3 -4 0 -0.90 0.90 -3 -4 0 0.90 0.90 -3 -4 0 0.00 0.60 3 4 0 -0.50 0.70 3 4 0 -0.90 1.10 3 4 0 -1.10 1.70 3 4 0 -0.60 0.90 3 4 0 0.10 0.70 3 4 0 -0.20 0.50 3 4 0 -1.00 0.60 3 4 0 0.30 1.30 3 4 0 -1.20 1.10 -4 -4 0 30.80 3.90 -4 -4 0 26.20 3.90 -4 -4 0 32.60 3.20 -4 -4 0 31.10 3.00 -4 -4 0 32.60 4.70 -4 -4 0 29.70 4.50 4 4 0 31.70 4.20 4 4 0 30.50 3.10 4 4 0 32.00 4.50 4 4 0 32.40 4.50 4 4 0 32.90 2.60 4 4 0 28.90 5.80 4 4 0 30.30 4.50 4 4 0 36.10 4.40 4 4 0 25.20 3.30 -5 -4 0 0.00 1.10 -5 -4 0 1.00 1.20 -5 -4 0 0.80 1.50 -5 -4 0 -0.40 1.40 -5 -4 0 -0.40 1.60 5 4 0 -1.50 0.90 5 4 0 0.20 0.80 5 4 0 0.00 1.70 5 4 0 -2.00 0.80 5 4 0 0.90 1.00 5 4 0 3.00 2.60 5 4 0 -1.40 1.60 5 4 0 -0.80 1.20 -6 -4 0 100.79 8.10 -6 -4 0 114.39 7.10 -6 -4 0 94.19 8.30 -6 -4 0 115.69 7.30 -6 -4 0 121.09 9.60 6 4 0 108.69 8.90 6 4 0 113.29 8.50 6 4 0 105.39 7.00 6 4 0 109.29 11.50 6 4 0 99.09 9.00 6 4 0 106.69 8.70 6 4 0 119.29 8.90 -7 -4 0 -1.60 1.70 -7 -4 0 0.20 1.70 -7 -4 0 1.00 1.40 -7 -4 0 -0.40 1.50 -7 -4 0 1.40 1.50 7 4 0 -0.70 1.20 7 4 0 -1.30 2.10 7 4 0 -2.20 1.20 7 4 0 1.10 1.40 7 4 0 1.00 1.30 7 4 0 -0.20 1.80 7 4 0 5.30 4.80 -8 -4 0 31.30 5.20 -8 -4 0 28.00 6.10 -8 -4 0 34.70 5.80 8 4 0 18.70 6.30 8 4 0 28.20 6.00 8 4 0 24.90 4.80 8 4 0 21.40 5.00 8 4 0 10.40 3.50 8 4 0 19.60 4.50 8 4 0 22.20 4.70 -9 -4 0 -0.10 1.90 -9 -4 0 -0.60 3.70 -9 -4 0 -2.30 1.50 9 4 0 0.40 2.10 9 4 0 2.20 2.20 9 4 0 -1.70 2.70 9 4 0 -1.70 2.80 9 4 0 -1.30 1.80 9 4 0 0.60 6.00 9 4 0 0.30 2.00 -10 -4 0 4.40 3.00 -10 -4 0 1.00 2.50 -10 -4 0 3.70 5.10 10 4 0 0.40 3.40 10 4 0 0.40 2.40 10 4 0 3.50 4.20 10 4 0 2.50 5.40 10 4 0 -1.10 3.10 10 4 0 2.30 2.80 -11 -4 0 -4.60 2.20 -11 -4 0 -3.80 4.00 -11 -4 0 -1.60 2.60 11 4 0 -1.80 3.60 11 4 0 -1.30 3.70 11 4 0 -1.40 2.60 11 4 0 -3.30 2.30 11 4 0 -3.20 4.20 11 4 0 7.40 8.60 -12 -4 0 0.10 3.80 -12 -4 0 1.90 4.00 -12 -4 0 2.30 3.90 12 4 0 3.90 4.00 12 4 0 -2.20 3.60 12 4 0 4.70 5.10 12 4 0 0.20 3.40 12 4 0 3.00 3.60 10 -5 0 7.10 4.10 10 -5 0 3.90 3.40 10 -5 0 0.50 4.10 10 -5 0 0.50 3.30 10 -5 0 1.30 4.20 -10 5 0 2.70 4.20 -10 5 0 6.30 3.20 -10 5 0 9.40 4.30 9 -5 0 8.80 4.70 9 -5 0 2.90 3.70 9 -5 0 3.40 3.10 9 -5 0 -2.20 2.90 9 -5 0 7.90 4.60 -9 5 0 -1.30 3.30 -9 5 0 5.90 3.70 -9 5 0 -4.10 3.40 -9 5 0 -0.40 3.70 8 -5 0 34.10 6.30 8 -5 0 36.90 6.90 8 -5 0 34.70 6.90 8 -5 0 47.10 8.00 8 -5 0 48.00 7.60 -8 5 0 42.40 6.90 -8 5 0 42.20 7.10 -8 5 0 53.39 6.50 -8 5 0 45.00 7.20 -8 5 0 41.50 6.60 7 -5 0 -3.00 2.70 7 -5 0 -0.10 1.90 7 -5 0 0.60 2.50 7 -5 0 2.30 2.80 7 -5 0 -0.40 2.40 7 -5 0 0.80 2.10 -7 5 0 0.30 2.70 -7 5 0 3.50 3.10 -7 5 0 1.10 2.30 -7 5 0 0.20 2.60 -7 5 0 0.70 2.20 6 -5 0 92.59 8.40 6 -5 0 110.29 11.50 6 -5 0 92.49 9.80 6 -5 0 93.39 10.10 6 -5 0 130.89 10.70 6 -5 0 104.69 10.70 -6 5 0 111.19 8.40 -6 5 0 89.39 9.20 -6 5 0 112.39 8.60 -6 5 0 111.79 9.40 -6 5 0 84.99 9.40 5 -5 0 -0.90 2.00 5 -5 0 0.90 2.10 5 -5 0 -0.60 2.20 5 -5 0 1.10 1.70 5 -5 0 -1.60 2.40 5 -5 0 0.70 2.60 5 -5 0 0.10 1.70 -5 5 0 0.50 2.20 -5 5 0 -0.20 1.70 -5 5 0 -0.30 1.30 -5 5 0 1.50 1.60 -5 5 0 -1.40 1.80 -5 5 0 0.70 2.70 4 -5 0 0.80 1.60 4 -5 0 1.50 1.70 4 -5 0 0.90 1.50 4 -5 0 -0.30 2.10 4 -5 0 -0.10 0.90 4 -5 0 0.80 1.70 4 -5 0 0.90 1.30 4 -5 0 0.90 2.10 -4 5 0 0.20 1.30 -4 5 0 1.40 1.80 -4 5 0 0.80 1.30 -4 5 0 0.90 1.90 -4 5 0 0.50 1.40 -4 5 0 1.20 2.10 3 -5 0 -0.40 1.40 3 -5 0 -0.40 1.30 3 -5 0 -1.40 1.60 3 -5 0 -0.30 1.30 3 -5 0 -0.50 1.20 3 -5 0 0.80 1.80 3 -5 0 -0.80 1.20 3 -5 0 0.20 1.60 -3 5 0 -1.50 1.50 -3 5 0 -0.40 1.10 -3 5 0 -0.60 1.10 -3 5 0 -1.00 1.00 -3 5 0 -1.20 1.00 -3 5 0 1.30 1.20 -3 5 0 0.10 1.20 2 -5 0 -0.60 1.10 2 -5 0 -1.60 1.40 2 -5 0 1.30 1.50 2 -5 0 -0.20 1.90 2 -5 0 0.40 1.20 2 -5 0 -1.10 1.00 2 -5 0 1.00 1.40 2 -5 0 0.20 1.30 -2 5 0 -0.80 0.90 -2 5 0 -0.30 1.00 -2 5 0 -0.40 0.80 -2 5 0 -1.40 0.90 -2 5 0 0.10 1.50 -2 5 0 -1.00 1.00 -2 5 0 0.00 1.20 1 -5 0 -0.90 0.90 1 -5 0 0.10 1.20 1 -5 0 -0.20 1.00 1 -5 0 0.10 1.30 1 -5 0 0.30 1.50 1 -5 0 -1.60 1.10 1 -5 0 1.30 1.70 1 -5 0 -2.60 1.20 -1 5 0 0.70 1.10 -1 5 0 -0.30 0.90 -1 5 0 -1.40 1.20 -1 5 0 -0.40 1.00 -1 5 0 1.50 1.60 -1 5 0 -0.20 1.00 -1 5 0 1.20 1.50 0 -5 0 92.19 6.10 0 -5 0 105.89 6.80 0 -5 0 108.49 6.90 0 -5 0 86.79 6.90 0 -5 0 91.89 6.90 0 -5 0 110.59 7.50 0 -5 0 86.99 7.00 0 -5 0 97.39 6.80 0 -5 0 98.09 6.80 0 5 0 91.09 6.60 0 5 0 95.89 6.60 0 5 0 97.89 6.40 0 5 0 88.99 6.10 0 5 0 112.89 7.00 0 5 0 91.29 5.90 0 5 0 100.89 6.30 -1 -5 0 -0.50 1.20 -1 -5 0 1.70 1.20 -1 -5 0 0.90 1.50 -1 -5 0 0.10 1.10 -1 -5 0 -1.20 1.70 -1 -5 0 0.30 1.10 -1 -5 0 -1.00 1.00 -1 -5 0 -1.40 1.00 1 5 0 -0.50 0.80 1 5 0 -0.40 1.20 1 5 0 -1.20 0.90 1 5 0 -0.30 1.30 1 5 0 -0.20 0.80 1 5 0 -0.60 1.50 1 5 0 -0.70 1.00 1 5 0 -0.70 1.10 -2 -5 0 52.29 3.90 -2 -5 0 44.30 4.90 -2 -5 0 41.80 3.60 -2 -5 0 53.69 7.40 -2 -5 0 40.30 4.90 -2 -5 0 42.80 3.40 -2 -5 0 39.20 4.90 -2 -5 0 39.80 5.20 2 5 0 45.10 5.00 2 5 0 44.20 4.60 2 5 0 42.70 3.10 2 5 0 48.50 4.70 2 5 0 41.50 5.90 2 5 0 43.10 3.50 2 5 0 53.99 5.50 2 5 0 45.50 4.90 2 5 0 51.29 5.10 -3 -5 0 -0.80 0.80 -3 -5 0 -0.90 0.90 -3 -5 0 -0.60 1.00 -3 -5 0 -0.40 1.60 -3 -5 0 0.60 1.10 -3 -5 0 -1.70 0.70 3 5 0 0.40 1.10 3 5 0 -1.20 1.90 3 5 0 -1.10 1.50 3 5 0 -1.40 0.90 3 5 0 0.10 1.10 3 5 0 -1.30 0.70 3 5 0 -0.90 1.00 3 5 0 0.20 1.40 -4 -5 0 8.50 2.60 -4 -5 0 6.40 1.70 -4 -5 0 7.00 1.80 -4 -5 0 4.30 2.50 -4 -5 0 6.80 2.30 -4 -5 0 9.10 2.60 4 5 0 4.10 2.20 4 5 0 9.60 2.60 4 5 0 6.10 2.20 4 5 0 6.20 3.90 4 5 0 5.90 2.40 4 5 0 5.50 1.70 4 5 0 9.90 1.90 4 5 0 8.50 1.50 4 5 0 1.00 2.00 -5 -5 0 0.30 1.80 -5 -5 0 0.40 1.50 -5 -5 0 -0.40 1.10 -5 -5 0 3.30 1.70 -5 -5 0 0.60 1.10 -5 -5 0 -1.00 1.00 5 5 0 -0.10 2.90 5 5 0 0.00 1.00 5 5 0 -0.60 1.10 5 5 0 0.80 1.50 5 5 0 0.50 1.20 5 5 0 -0.20 2.00 5 5 0 -3.30 1.50 5 5 0 0.40 1.80 -6 -5 0 68.49 7.50 -6 -5 0 59.79 7.50 -6 -5 0 75.59 7.40 -6 -5 0 54.59 7.50 -6 -5 0 67.19 5.80 6 5 0 69.99 5.40 6 5 0 57.69 7.30 6 5 0 71.39 8.30 6 5 0 66.79 7.70 6 5 0 78.79 6.80 6 5 0 61.49 7.80 6 5 0 39.40 8.00 -7 -5 0 -0.70 1.50 -7 -5 0 -1.60 2.90 -7 -5 0 -2.00 1.30 7 5 0 -4.90 2.00 7 5 0 3.20 5.10 7 5 0 -1.60 1.30 7 5 0 -2.20 2.10 7 5 0 0.60 2.50 7 5 0 -0.20 1.90 -8 -5 0 23.60 6.10 -8 -5 0 25.60 4.80 -8 -5 0 20.30 4.70 8 5 0 4.70 6.00 8 5 0 15.90 5.00 8 5 0 16.80 5.00 8 5 0 16.20 4.60 8 5 0 19.20 5.40 8 5 0 21.30 4.60 -9 -5 0 -0.10 2.00 -9 -5 0 1.30 2.40 -9 -5 0 1.50 2.70 9 5 0 0.50 2.40 9 5 0 -0.80 3.10 9 5 0 -0.90 2.00 9 5 0 0.90 2.70 9 5 0 -1.70 4.60 9 5 0 3.20 3.50 -10 -5 0 -2.30 1.80 -10 -5 0 -3.00 4.30 -10 -5 0 -1.20 2.40 10 5 0 -2.90 6.30 10 5 0 -2.00 3.50 10 5 0 -3.10 2.80 10 5 0 0.70 2.70 10 5 0 1.70 3.80 -11 -5 0 1.10 2.80 -11 -5 0 -2.00 3.40 -11 -5 0 1.70 5.00 11 5 0 1.10 4.10 11 5 0 -4.50 3.40 11 5 0 -3.10 3.20 11 5 0 -3.30 2.70 9 -6 0 3.80 3.60 9 -6 0 2.40 4.20 9 -6 0 1.10 2.50 9 -6 0 -0.60 4.00 -9 6 0 -3.80 3.20 -9 6 0 3.60 3.00 -9 6 0 -2.40 2.50 -9 6 0 -1.00 3.40 8 -6 0 24.40 5.90 8 -6 0 12.10 4.80 8 -6 0 15.30 4.80 8 -6 0 6.40 4.40 8 -6 0 17.60 5.00 -8 6 0 7.60 4.50 -8 6 0 11.60 4.20 -8 6 0 17.30 4.60 -8 6 0 9.10 4.00 -8 6 0 15.60 5.30 7 -6 0 0.00 2.80 7 -6 0 1.60 2.60 7 -6 0 -0.70 2.30 7 -6 0 2.60 2.40 7 -6 0 4.50 2.70 7 -6 0 4.50 3.20 -7 6 0 -2.70 1.90 -7 6 0 -0.60 2.20 -7 6 0 1.60 2.50 -7 6 0 2.60 3.20 -7 6 0 -0.50 2.10 6 -6 0 4.60 2.80 6 -6 0 8.80 3.40 6 -6 0 5.60 3.20 6 -6 0 3.80 3.00 6 -6 0 10.50 3.90 6 -6 0 11.60 3.80 -6 6 0 8.80 3.60 -6 6 0 6.30 2.90 -6 6 0 9.50 3.50 -6 6 0 6.60 2.80 -6 6 0 4.20 2.70 5 -6 0 -0.80 2.00 5 -6 0 1.20 2.90 5 -6 0 -1.80 1.70 5 -6 0 -1.60 2.80 5 -6 0 -0.40 2.30 5 -6 0 0.60 2.10 -5 6 0 -0.10 2.20 -5 6 0 1.50 2.30 -5 6 0 -1.80 2.10 -5 6 0 0.30 2.40 -5 6 0 -0.80 1.70 -5 6 0 -1.90 2.20 4 -6 0 13.00 4.00 4 -6 0 12.50 2.90 4 -6 0 8.20 2.80 4 -6 0 9.40 3.30 4 -6 0 4.50 3.30 4 -6 0 19.00 4.00 4 -6 0 24.50 4.60 -4 6 0 10.80 3.10 -4 6 0 10.40 3.20 -4 6 0 5.80 2.30 -4 6 0 12.90 3.50 -4 6 0 18.50 3.70 -4 6 0 8.50 3.00 3 -6 0 -2.50 1.30 3 -6 0 1.60 1.90 3 -6 0 -2.00 2.00 3 -6 0 -1.20 1.20 3 -6 0 0.80 1.50 3 -6 0 -2.20 1.50 3 -6 0 0.00 1.50 -3 6 0 -1.10 1.40 -3 6 0 -1.40 1.20 -3 6 0 -0.40 1.30 -3 6 0 -2.00 1.10 -3 6 0 -3.20 1.70 -3 6 0 0.10 1.20 2 -6 0 3.20 2.00 2 -6 0 3.60 2.20 2 -6 0 6.20 2.40 2 -6 0 5.80 2.80 2 -6 0 5.10 1.80 2 -6 0 3.50 2.10 2 -6 0 2.40 2.30 -2 6 0 4.60 2.00 -2 6 0 2.40 1.60 -2 6 0 6.40 2.10 -2 6 0 4.90 2.10 -2 6 0 1.90 1.70 -2 6 0 8.60 2.40 -2 6 0 3.70 2.00 1 -6 0 0.20 1.80 1 -6 0 -1.20 1.70 1 -6 0 -0.80 1.70 1 -6 0 -0.40 1.40 1 -6 0 -1.10 1.60 1 -6 0 0.30 1.90 1 -6 0 -2.10 1.10 1 -6 0 0.30 1.20 -1 6 0 -0.50 1.20 -1 6 0 2.70 1.80 -1 6 0 0.10 1.40 -1 6 0 0.90 1.60 -1 6 0 0.00 0.90 -1 6 0 0.10 1.50 0 -6 0 -0.40 1.00 0 -6 0 1.70 1.80 0 -6 0 0.60 1.70 0 -6 0 1.40 1.70 0 -6 0 -1.10 1.40 0 -6 0 -1.10 1.60 0 -6 0 -0.90 1.40 0 -6 0 0.30 1.00 0 -6 0 0.80 1.70 0 6 0 -0.80 1.50 0 6 0 0.40 1.50 0 6 0 0.60 0.70 0 6 0 -1.00 1.10 0 6 0 -0.90 0.90 0 6 0 0.70 1.20 0 6 0 0.70 1.20 0 6 0 -0.30 1.10 -1 -6 0 -0.60 1.10 -1 -6 0 0.20 1.10 -1 -6 0 -2.40 1.10 -1 -6 0 -0.80 1.90 -1 -6 0 -0.70 1.20 -1 -6 0 -0.30 1.70 -1 -6 0 -1.50 1.30 -1 -6 0 0.60 1.40 -1 -6 0 -2.20 1.10 1 6 0 1.10 1.00 1 6 0 -0.10 0.90 1 6 0 0.20 2.00 1 6 0 -0.10 1.20 1 6 0 -0.20 1.00 1 6 0 -0.50 1.40 1 6 0 -0.50 1.20 1 6 0 1.20 1.50 -2 -6 0 255.27 13.40 -2 -6 0 223.28 16.00 -2 -6 0 246.88 12.90 -2 -6 0 241.28 14.40 -2 -6 0 243.58 14.70 -2 -6 0 245.68 13.20 -2 -6 0 232.88 14.00 -2 -6 0 236.48 14.70 2 6 0 235.98 14.20 2 6 0 225.88 13.70 2 6 0 239.28 12.30 2 6 0 232.68 13.00 2 6 0 230.78 14.00 2 6 0 219.78 13.40 2 6 0 260.87 14.10 2 6 0 261.97 16.00 2 6 0 241.18 14.30 -3 -6 0 -1.50 1.90 -3 -6 0 1.60 3.30 -3 -6 0 0.10 1.30 -3 -6 0 1.20 1.50 -3 -6 0 -0.60 1.20 -3 -6 0 5.80 1.80 -3 -6 0 0.80 1.30 3 6 0 0.20 1.30 3 6 0 -0.30 2.50 3 6 0 -0.10 1.40 3 6 0 1.50 1.70 3 6 0 -1.00 1.40 3 6 0 0.20 1.80 3 6 0 -1.40 0.90 3 6 0 1.80 1.60 -4 -6 0 65.99 10.50 -4 -6 0 56.49 6.70 -4 -6 0 61.89 4.70 -4 -6 0 55.49 6.30 -4 -6 0 45.30 6.20 -4 -6 0 53.99 6.90 4 6 0 60.09 6.70 4 6 0 64.09 5.00 4 6 0 60.59 6.00 4 6 0 59.09 4.20 4 6 0 45.80 6.30 4 6 0 61.39 6.60 4 6 0 58.99 7.00 4 6 0 43.70 7.70 -5 -6 0 -0.60 1.20 -5 -6 0 -0.10 1.50 -5 -6 0 1.70 1.70 -5 -6 0 -2.90 1.70 5 6 0 4.50 2.30 5 6 0 -1.80 1.30 5 6 0 3.60 4.20 5 6 0 -0.80 1.50 5 6 0 -3.10 2.00 5 6 0 -2.10 1.60 5 6 0 -0.30 1.20 5 6 0 0.50 1.40 -6 -6 0 15.80 4.00 -6 -6 0 9.30 3.30 -6 -6 0 9.90 3.80 -6 -6 0 15.80 4.00 6 6 0 10.70 5.60 6 6 0 17.50 4.10 6 6 0 11.20 3.40 6 6 0 21.90 4.60 6 6 0 8.20 3.30 6 6 0 7.80 3.10 6 6 0 16.30 3.30 -7 -6 0 0.80 2.20 -7 -6 0 8.30 3.60 -7 -6 0 -1.80 1.30 -7 -6 0 -0.50 2.10 7 6 0 -0.50 2.40 7 6 0 0.00 2.20 7 6 0 -0.10 2.10 7 6 0 3.10 5.20 7 6 0 -0.40 1.70 7 6 0 -1.20 1.60 -8 -6 0 -1.80 3.10 -8 -6 0 -2.70 1.40 -8 -6 0 3.00 3.50 -8 -6 0 6.50 3.10 8 6 0 1.60 2.80 8 6 0 -0.70 2.20 8 6 0 0.90 3.30 8 6 0 4.00 3.30 8 6 0 6.60 3.20 8 6 0 2.70 6.50 -9 -6 0 -0.30 3.10 -9 -6 0 -0.90 2.80 -9 -6 0 -2.00 2.10 -9 -6 0 -0.10 2.70 9 6 0 2.50 2.60 9 6 0 2.50 3.00 9 6 0 -1.20 2.10 9 6 0 0.80 2.70 9 6 0 3.20 2.70 9 6 0 0.70 6.80 -10 -6 0 8.30 5.00 -10 -6 0 0.30 2.50 -10 -6 0 4.00 4.00 -10 -6 0 1.50 2.60 10 6 0 6.60 3.40 10 6 0 13.70 5.10 10 6 0 3.30 4.10 10 6 0 -4.60 6.40 10 6 0 5.10 3.60 10 6 0 -0.10 3.60 -11 -6 0 4.20 4.80 -11 -6 0 -3.10 3.20 -11 -6 0 -3.00 3.30 -11 -6 0 -2.70 3.40 11 6 0 -0.70 3.60 11 6 0 5.80 3.80 11 6 0 1.90 3.60 11 6 0 -2.60 3.80 8 -7 0 -0.10 2.60 8 -7 0 4.00 4.50 8 -7 0 -1.80 3.90 8 -7 0 1.40 4.20 -8 7 0 1.70 4.00 -8 7 0 2.60 3.30 -8 7 0 -2.40 2.40 7 -7 0 0.80 2.60 7 -7 0 -1.10 2.90 7 -7 0 2.80 3.00 7 -7 0 0.00 3.00 7 -7 0 -3.60 1.60 -7 7 0 -1.70 2.40 -7 7 0 -4.10 2.80 -7 7 0 1.40 3.00 -7 7 0 1.20 2.70 -7 7 0 -1.90 2.00 6 -7 0 49.20 8.10 6 -7 0 48.20 7.50 6 -7 0 30.40 6.40 6 -7 0 41.90 7.70 6 -7 0 46.60 7.60 -6 7 0 27.80 6.40 -6 7 0 49.30 7.00 -6 7 0 40.90 6.80 -6 7 0 42.20 6.40 -6 7 0 35.30 6.00 5 -7 0 -3.40 3.00 5 -7 0 -2.20 2.00 5 -7 0 -0.80 2.40 5 -7 0 3.80 3.50 5 -7 0 -1.70 2.60 5 -7 0 0.80 3.40 -5 7 0 2.40 2.90 -5 7 0 -0.70 2.70 -5 7 0 2.00 2.20 -5 7 0 2.00 3.00 -5 7 0 0.20 3.20 -5 7 0 4.70 3.50 4 -7 0 74.39 8.70 4 -7 0 104.59 10.40 4 -7 0 89.69 9.50 4 -7 0 73.59 7.90 4 -7 0 75.39 9.50 4 -7 0 75.99 8.90 -4 7 0 77.89 8.30 -4 7 0 77.59 8.60 -4 7 0 77.79 8.60 -4 7 0 74.19 8.10 -4 7 0 68.49 8.00 -4 7 0 76.89 8.20 3 -7 0 -1.70 1.70 3 -7 0 4.10 3.20 3 -7 0 -3.90 2.60 3 -7 0 0.30 2.30 3 -7 0 -0.60 1.80 3 -7 0 2.40 1.90 3 -7 0 0.50 2.40 -3 7 0 -0.60 2.20 -3 7 0 -0.80 1.90 -3 7 0 1.90 2.00 -3 7 0 -1.50 1.60 -3 7 0 -1.40 2.10 -3 7 0 -0.60 1.70 2 -7 0 2.00 2.50 2 -7 0 3.20 2.00 2 -7 0 4.50 2.50 2 -7 0 3.80 2.50 2 -7 0 2.70 1.90 2 -7 0 1.70 2.70 2 -7 0 -1.40 1.60 -2 7 0 5.70 2.30 -2 7 0 4.10 2.10 -2 7 0 3.00 1.80 -2 7 0 -0.20 2.30 -2 7 0 3.80 2.30 -2 7 0 1.70 2.60 -2 7 0 1.50 1.60 1 -7 0 0.20 1.50 1 -7 0 2.30 1.80 1 -7 0 -1.40 1.30 1 -7 0 -2.00 1.80 1 -7 0 1.50 2.10 1 -7 0 -2.60 1.90 1 -7 0 -1.40 1.80 -1 7 0 -2.80 1.00 -1 7 0 0.30 1.50 -1 7 0 0.50 1.80 -1 7 0 1.30 1.50 -1 7 0 0.80 1.70 -1 7 0 -2.60 1.20 -1 7 0 -0.60 1.50 0 -7 0 13.90 3.40 0 -7 0 8.40 2.60 0 -7 0 12.20 3.10 0 -7 0 11.40 3.00 0 -7 0 15.40 3.90 0 -7 0 11.60 3.50 0 -7 0 15.30 3.40 0 7 0 11.70 3.00 0 7 0 10.00 2.40 0 7 0 10.30 2.50 0 7 0 12.90 2.90 0 7 0 12.80 2.70 0 7 0 10.60 2.90 0 7 0 12.20 2.80 -1 -7 0 0.00 2.20 -1 -7 0 -0.60 1.40 -1 -7 0 -1.10 1.80 -1 -7 0 1.90 1.40 -1 -7 0 0.50 1.70 -1 -7 0 1.10 2.30 -1 -7 0 0.80 1.50 -1 -7 0 -0.70 1.50 -1 -7 0 -0.20 1.40 1 7 0 0.40 1.60 1 7 0 -0.60 1.50 1 7 0 1.10 1.20 1 7 0 0.80 1.10 1 7 0 2.00 1.40 1 7 0 -1.60 1.00 -2 -7 0 13.90 2.90 -2 -7 0 15.40 3.50 -2 -7 0 17.90 3.70 -2 -7 0 16.90 3.80 -2 -7 0 17.70 3.60 -2 -7 0 12.40 4.40 2 7 0 19.20 5.10 2 7 0 15.50 3.50 2 7 0 12.40 3.10 2 7 0 12.10 2.50 2 7 0 20.40 3.60 2 7 0 7.00 2.10 2 7 0 18.70 2.80 2 7 0 12.80 3.20 -3 -7 0 1.40 1.90 -3 -7 0 -1.10 3.30 -3 -7 0 -0.40 2.20 -3 -7 0 1.50 1.90 -3 -7 0 1.50 1.80 3 7 0 -0.40 2.10 3 7 0 -1.00 1.70 3 7 0 1.30 2.80 3 7 0 0.60 2.10 3 7 0 -0.30 1.20 3 7 0 0.10 1.30 3 7 0 -1.90 1.10 3 7 0 -1.90 1.40 -4 -7 0 115.49 8.80 -4 -7 0 116.29 9.40 -4 -7 0 101.19 10.70 -4 -7 0 101.39 9.10 -4 -7 0 115.79 12.30 4 7 0 113.59 9.40 4 7 0 115.09 8.00 4 7 0 103.09 11.10 4 7 0 117.59 9.40 4 7 0 122.69 9.40 4 7 0 105.99 8.20 4 7 0 113.79 7.20 4 7 0 108.49 8.90 -5 -7 0 -2.10 2.10 -5 -7 0 -1.60 2.10 -5 -7 0 -0.70 1.60 -5 -7 0 -0.10 1.40 -5 -7 0 -0.50 5.30 5 7 0 1.10 2.50 5 7 0 -2.70 1.30 5 7 0 -2.40 1.20 5 7 0 0.60 1.50 5 7 0 -1.30 2.00 5 7 0 -1.40 4.30 5 7 0 -1.70 2.10 -6 -7 0 -0.40 1.80 -6 -7 0 3.80 3.00 -6 -7 0 -0.50 2.70 -6 -7 0 2.60 2.50 6 7 0 0.70 1.90 6 7 0 4.90 3.40 6 7 0 2.10 2.00 6 7 0 1.40 2.10 6 7 0 3.80 4.70 6 7 0 4.00 2.50 -7 -7 0 3.60 3.50 -7 -7 0 1.20 2.10 -7 -7 0 2.90 3.30 -7 -7 0 -2.00 2.20 7 7 0 0.70 3.00 7 7 0 -0.50 4.20 7 7 0 -5.30 2.10 7 7 0 0.70 2.10 7 7 0 -1.80 1.60 7 7 0 0.80 2.30 -8 -7 0 8.00 3.10 -8 -7 0 4.70 3.20 -8 -7 0 11.00 4.60 -8 -7 0 9.30 5.00 8 7 0 12.50 5.10 8 7 0 7.90 4.00 8 7 0 7.40 4.10 8 7 0 14.50 4.90 8 7 0 10.60 3.80 8 7 0 -0.40 6.40 -9 -7 0 -1.50 2.40 -9 -7 0 0.00 3.20 -9 -7 0 0.60 3.10 -9 -7 0 0.00 3.80 9 7 0 0.60 3.70 9 7 0 -1.50 2.70 9 7 0 1.60 2.80 9 7 0 -3.90 6.70 9 7 0 1.40 3.50 9 7 0 3.50 3.90 -10 -7 0 1.70 3.40 -10 -7 0 1.00 2.50 -10 -7 0 0.60 3.10 -10 -7 0 4.10 3.70 10 7 0 -1.50 2.20 10 7 0 2.10 8.00 10 7 0 -0.90 3.80 10 7 0 0.10 2.80 10 7 0 -1.50 2.60 10 7 0 3.80 4.20 -11 -7 0 -0.60 2.90 -11 -7 0 -1.50 3.10 -11 -7 0 1.90 5.00 -11 -7 0 3.00 3.90 11 7 0 -7.40 3.90 11 7 0 -0.20 2.90 11 7 0 1.80 4.40 11 7 0 -0.30 4.30 8 -8 0 -0.30 2.40 8 -8 0 2.60 3.50 8 -8 0 5.20 5.40 8 -8 0 -1.90 4.10 -8 8 0 -2.10 4.00 -8 8 0 -1.20 4.10 -8 8 0 2.60 3.70 7 -8 0 3.40 4.80 7 -8 0 -0.80 3.70 7 -8 0 2.50 4.30 7 -8 0 -4.40 2.40 7 -8 0 -0.90 2.40 -7 8 0 1.10 4.20 -7 8 0 -5.30 3.10 -7 8 0 -1.00 2.60 -7 8 0 -1.30 3.40 -7 8 0 -0.10 2.60 6 -8 0 11.00 4.80 6 -8 0 4.70 4.30 6 -8 0 6.10 3.30 6 -8 0 10.10 5.30 6 -8 0 6.30 3.50 -6 8 0 2.50 3.90 -6 8 0 4.30 2.90 -6 8 0 9.80 4.00 -6 8 0 4.60 4.20 -6 8 0 2.90 3.70 5 -8 0 -0.20 2.90 5 -8 0 -1.80 1.70 5 -8 0 -1.30 3.50 5 -8 0 0.50 3.60 5 -8 0 0.40 3.30 -5 8 0 -3.10 1.80 -5 8 0 0.70 3.80 -5 8 0 6.30 2.90 -5 8 0 -0.90 1.70 -5 8 0 -1.60 1.60 -5 8 0 -0.70 2.00 4 -8 0 27.20 5.60 4 -8 0 25.10 5.70 4 -8 0 9.80 3.60 4 -8 0 10.90 4.20 4 -8 0 19.80 5.60 -4 8 0 24.60 5.20 -4 8 0 16.60 4.10 -4 8 0 16.90 4.80 -4 8 0 23.30 4.30 -4 8 0 24.30 4.60 -4 8 0 18.70 4.30 3 -8 0 -2.30 2.50 3 -8 0 -0.40 2.30 3 -8 0 -1.30 2.90 3 -8 0 2.10 2.60 3 -8 0 -0.10 2.10 -3 8 0 0.10 1.80 -3 8 0 -1.70 2.50 -3 8 0 -0.40 1.90 -3 8 0 -1.30 2.80 -3 8 0 3.00 2.90 -3 8 0 0.90 2.10 2 -8 0 8.20 3.00 2 -8 0 10.70 3.50 2 -8 0 2.00 3.20 2 -8 0 14.30 4.70 2 -8 0 12.80 3.80 -2 8 0 18.10 4.50 -2 8 0 12.20 3.50 -2 8 0 8.50 2.80 -2 8 0 12.70 3.20 -2 8 0 10.70 3.40 -2 8 0 8.30 3.20 1 -8 0 0.70 2.10 1 -8 0 0.10 2.00 1 -8 0 -3.70 2.00 1 -8 0 -0.30 1.80 1 -8 0 1.90 2.90 1 -8 0 -2.60 2.10 -1 8 0 -0.30 1.10 -1 8 0 -1.30 1.90 -1 8 0 0.20 1.30 -1 8 0 -0.50 1.50 -1 8 0 -0.20 1.50 -1 8 0 0.20 1.70 -1 8 0 2.90 2.10 0 -8 0 2.50 2.00 0 -8 0 5.70 2.70 0 -8 0 6.10 2.60 0 -8 0 8.80 3.60 0 -8 0 -0.40 2.40 0 -8 0 5.40 2.70 0 -8 0 5.30 2.40 0 8 0 3.20 1.80 0 8 0 3.50 2.30 0 8 0 5.70 2.50 0 8 0 3.70 2.10 0 8 0 3.80 2.60 0 8 0 4.30 2.20 -1 -8 0 2.30 2.00 -1 -8 0 -2.30 1.40 -1 -8 0 -2.40 2.40 -1 -8 0 1.40 2.50 1 8 0 2.00 1.60 1 8 0 0.30 1.40 1 8 0 0.10 1.40 1 8 0 -0.50 1.40 1 8 0 -0.20 1.40 1 8 0 -1.90 1.60 1 8 0 -1.90 1.30 -2 -8 0 1.50 1.60 -2 -8 0 0.50 2.20 -2 -8 0 3.00 2.70 -2 -8 0 0.30 1.90 2 8 0 -0.20 1.60 2 8 0 1.50 2.20 2 8 0 2.10 1.80 2 8 0 -0.90 1.40 2 8 0 1.70 2.40 -3 -8 0 2.90 4.50 -3 -8 0 -1.60 1.40 -3 -8 0 -0.50 2.30 -3 -8 0 -2.20 1.50 -3 -8 0 3.00 2.20 3 8 0 0.30 1.50 3 8 0 -1.90 1.40 3 8 0 -3.60 1.60 3 8 0 0.30 3.00 3 8 0 1.10 2.40 3 8 0 2.10 2.90 3 8 0 0.10 1.90 -4 -8 0 330.67 24.10 -4 -8 0 313.37 20.30 -4 -8 0 342.17 21.30 -4 -8 0 343.47 20.10 -4 -8 0 323.57 20.50 4 8 0 361.66 21.00 4 8 0 332.97 19.90 4 8 0 354.06 20.90 4 8 0 313.17 22.70 4 8 0 348.87 19.60 4 8 0 332.57 20.50 4 8 0 357.56 19.10 -5 -8 0 -1.10 4.60 -5 -8 0 0.90 2.20 -5 -8 0 0.60 2.80 -5 -8 0 0.40 2.40 -5 -8 0 0.00 2.40 5 8 0 0.60 2.70 5 8 0 -1.40 2.30 5 8 0 -1.30 2.00 5 8 0 0.00 1.50 5 8 0 0.90 4.70 5 8 0 1.30 1.50 5 8 0 4.40 3.10 -6 -8 0 1.10 3.60 -6 -8 0 3.30 3.70 -6 -8 0 -4.80 6.60 -6 -8 0 5.50 3.10 -6 -8 0 5.80 2.50 6 8 0 4.20 2.60 6 8 0 1.70 2.40 6 8 0 2.50 2.80 6 8 0 1.90 2.20 6 8 0 -0.90 2.50 6 8 0 -0.20 5.30 -7 -8 0 2.90 3.70 -7 -8 0 5.10 4.00 -7 -8 0 -4.90 2.50 -7 -8 0 0.40 2.30 -7 -8 0 -1.00 6.70 7 8 0 1.90 2.60 7 8 0 -2.30 2.30 7 8 0 -1.00 2.80 7 8 0 -1.00 2.80 7 8 0 -1.50 6.10 7 8 0 2.50 3.20 -8 -8 0 8.50 4.00 -8 -8 0 9.50 8.40 -8 -8 0 8.40 4.30 -8 -8 0 6.50 3.60 -8 -8 0 2.90 3.30 8 8 0 7.50 3.40 8 8 0 -5.20 6.00 8 8 0 0.70 2.60 8 8 0 10.00 4.50 8 8 0 -0.20 3.20 -9 -8 0 2.80 4.60 -9 -8 0 -0.30 3.00 -9 -8 0 -0.40 2.60 -9 -8 0 4.60 9.50 -9 -8 0 -2.90 3.30 9 8 0 4.30 4.10 9 8 0 -1.80 2.30 9 8 0 -0.60 2.40 9 8 0 1.20 3.50 9 8 0 -0.70 2.50 9 8 0 -6.50 6.80 -10 -8 0 -6.10 3.00 -10 -8 0 1.70 4.70 -10 -8 0 1.60 3.20 -10 -8 0 2.60 3.90 10 8 0 3.40 3.40 10 8 0 5.70 5.00 10 8 0 -1.40 3.70 10 8 0 0.20 3.70 10 8 0 -1.00 2.60 7 -9 0 -2.30 3.20 6 -9 0 3.00 4.50 6 -9 0 1.30 3.10 6 -9 0 -0.20 3.60 6 -9 0 15.30 6.00 6 -9 0 2.30 3.70 -6 9 0 0.10 3.50 -6 9 0 0.00 2.70 -6 9 0 -1.90 3.70 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41.70 9.80 4 8 -4 30.20 4.30 4 8 -4 23.60 5.50 4 8 -4 31.60 5.20 4 8 -4 26.10 6.00 4 8 -4 26.80 5.30 4 8 -4 27.10 5.80 -4 -8 4 28.10 6.20 -4 -8 4 28.90 5.30 -4 -8 4 29.30 9.70 -4 -8 4 17.00 4.80 -4 -8 4 29.90 6.00 3 8 -4 33.80 8.80 3 8 -4 31.50 5.90 3 8 -4 37.20 5.20 3 8 -4 44.30 6.50 3 8 -4 45.20 6.00 3 8 -4 47.30 6.40 3 8 -4 27.10 5.80 -3 -8 4 33.70 8.80 -3 -8 4 29.80 6.30 -3 -8 4 34.40 5.60 -3 -8 4 25.80 5.70 -3 -8 4 39.60 7.00 2 8 -4 37.50 6.10 2 8 -4 27.10 5.00 2 8 -4 38.40 5.00 2 8 -4 28.50 4.90 2 8 -4 20.90 5.10 2 8 -4 38.10 6.10 -2 -8 4 27.60 5.80 -2 -8 4 29.40 5.30 -2 -8 4 34.00 8.80 -2 -8 4 24.80 5.60 -2 -8 4 23.10 5.10 1 8 -4 7.90 2.80 1 8 -4 -2.20 2.40 1 8 -4 11.90 3.80 1 8 -4 2.50 1.90 1 8 -4 6.40 2.80 -1 -8 4 -0.20 3.00 -1 -8 4 3.50 3.40 -1 -8 4 1.90 2.40 -1 -8 4 6.00 3.20 -1 -8 4 11.00 5.00 0 8 -4 52.99 6.90 0 8 -4 45.80 6.30 0 8 -4 44.70 6.30 0 8 -4 47.40 6.10 0 8 -4 42.40 5.40 0 -8 4 31.80 6.10 0 -8 4 35.60 6.40 0 -8 4 32.20 5.50 0 -8 4 42.30 6.80 0 -8 4 50.29 9.10 -1 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4.40 4.30 -7 -6 8 5.10 3.90 -7 -6 8 1.30 6.10 -7 -6 8 3.30 3.20 6 6 -8 2.10 2.90 6 6 -8 -2.20 3.50 6 6 -8 1.10 2.80 6 6 -8 7.90 7.80 6 6 -8 -1.10 3.60 6 6 -8 0.80 2.60 6 6 -8 2.90 4.30 -6 -6 8 1.10 3.10 -6 -6 8 2.70 4.40 -6 -6 8 4.90 3.40 -6 -6 8 1.70 7.60 -6 -6 8 5.80 4.30 5 6 -8 38.20 7.60 5 6 -8 48.50 11.40 5 6 -8 37.20 7.30 5 6 -8 32.40 5.30 5 6 -8 32.00 6.80 5 6 -8 48.60 7.30 5 6 -8 38.20 6.10 5 6 -8 29.00 6.90 -5 -6 8 53.69 13.20 -5 -6 8 36.00 7.70 -5 -6 8 35.80 7.40 -5 -6 8 44.50 6.30 -5 -6 8 39.20 7.20 4 6 -8 108.79 12.60 4 6 -8 118.49 13.00 4 6 -8 132.89 11.10 4 6 -8 148.09 19.20 4 6 -8 111.79 9.70 4 6 -8 111.39 8.90 4 6 -8 105.49 9.50 -4 -6 8 109.79 8.80 -4 -6 8 129.89 18.70 -4 -6 8 117.79 12.10 -4 -6 8 115.69 13.20 -4 -6 8 130.39 13.20 3 6 -8 13.60 3.40 3 6 -8 8.40 3.20 3 6 -8 6.80 3.20 3 6 -8 12.80 4.10 3 6 -8 8.40 3.80 3 6 -8 8.40 3.40 -3 -6 8 4.90 4.00 -3 -6 8 4.30 3.10 -3 -6 8 10.10 4.50 -3 -6 8 9.30 3.10 -3 -6 8 8.50 6.60 2 6 -8 -1.20 2.40 2 6 -8 -1.70 1.20 2 6 -8 -1.90 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49.10 7.60 6 -4 8 48.40 10.00 6 -4 8 51.19 7.70 -7 4 -8 6.60 3.50 -7 4 -8 4.60 3.10 -7 4 -8 0.30 3.10 -7 4 -8 4.60 3.80 -7 4 -8 6.60 3.20 7 -4 8 3.30 2.90 7 -4 8 0.80 2.40 7 -4 8 2.70 3.60 7 -4 8 0.20 4.30 7 -4 8 6.00 3.40 7 -4 8 2.60 3.10 -8 4 -8 4.20 3.40 -8 4 -8 3.20 3.50 -8 4 -8 -1.90 1.80 -8 4 -8 9.00 3.90 8 -4 8 4.40 4.10 8 -4 8 2.90 3.50 8 -4 8 3.60 5.60 8 -4 8 6.40 4.60 8 -4 8 0.60 3.10 8 -4 8 -2.30 1.90 -9 4 -8 -3.80 2.90 -9 4 -8 6.00 3.00 -9 4 -8 -2.20 2.20 9 -4 8 6.00 5.30 9 -4 8 0.20 7.90 9 -4 8 0.20 3.70 9 -4 8 3.00 3.40 9 -4 8 -2.70 2.60 9 -4 8 -1.70 2.80 -11 -3 8 -5.70 4.50 10 3 -8 -3.20 2.90 10 3 -8 -2.80 3.40 10 3 -8 1.20 3.10 10 3 -8 -1.60 3.70 10 3 -8 -2.50 3.60 10 3 -8 -2.50 7.50 10 3 -8 2.60 3.40 -10 -3 8 -2.30 6.30 -10 -3 8 -5.60 3.60 -10 -3 8 4.20 4.70 -10 -3 8 2.90 3.70 -10 -3 8 0.60 3.00 9 3 -8 2.80 2.80 9 3 -8 2.40 2.70 9 3 -8 2.30 4.50 9 3 -8 -8.50 8.00 9 3 -8 3.40 2.90 9 3 -8 0.80 2.90 9 3 -8 -0.80 3.70 -9 -3 8 2.00 3.20 -9 -3 8 -2.60 4.00 -9 -3 8 0.60 3.00 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25.90 5.10 -1 4 -9 27.40 4.60 -1 4 -9 33.20 4.90 -1 4 -9 35.30 4.40 -1 4 -9 24.10 4.50 1 -4 9 30.50 5.40 1 -4 9 35.60 8.50 1 -4 9 33.00 5.90 1 -4 9 20.10 4.60 1 -4 9 37.10 5.20 -2 4 -9 6.50 2.80 -2 4 -9 12.20 3.20 -2 4 -9 11.20 2.70 -2 4 -9 11.40 2.90 -2 4 -9 8.10 2.90 -2 4 -9 8.90 3.30 -2 4 -9 9.80 3.30 -2 4 -9 9.10 2.70 2 -4 9 12.10 3.60 2 -4 9 10.30 3.40 2 -4 9 7.40 3.50 2 -4 9 11.80 3.40 2 -4 9 5.90 4.90 -3 4 -9 -2.00 1.10 -3 4 -9 0.80 1.60 -3 4 -9 0.30 1.70 -3 4 -9 -2.80 1.70 -3 4 -9 0.10 2.30 -3 4 -9 -1.90 1.80 3 -4 9 0.10 2.10 3 -4 9 0.10 2.10 3 -4 9 -0.60 1.80 3 -4 9 -1.20 3.20 3 -4 9 -2.30 2.10 -4 4 -9 9.20 3.30 -4 4 -9 8.30 3.20 -4 4 -9 7.00 2.60 -4 4 -9 16.00 3.50 -4 4 -9 9.20 3.50 4 -4 9 14.60 4.20 4 -4 9 2.80 3.70 4 -4 9 3.00 3.10 4 -4 9 2.70 3.20 -5 4 -9 144.59 10.50 -5 4 -9 143.09 10.60 -5 4 -9 130.49 11.10 -5 4 -9 132.99 10.20 -5 4 -9 139.19 11.00 5 -4 9 169.08 12.90 5 -4 9 160.08 12.30 5 -4 9 148.29 11.70 5 -4 9 167.28 16.10 -6 4 -9 4.00 2.60 -6 4 -9 -0.70 2.80 -6 4 -9 6.40 2.70 -6 4 -9 6.10 3.40 6 -4 9 4.30 3.30 6 -4 9 2.80 3.30 6 -4 9 2.90 4.40 6 -4 9 8.10 3.40 -7 4 -9 2.60 3.70 -7 4 -9 4.60 2.40 -7 4 -9 2.40 3.20 -7 4 -9 1.60 2.90 7 -4 9 1.70 3.60 7 -4 9 5.10 3.80 7 -4 9 -3.70 2.90 7 -4 9 5.00 6.60 -8 4 -9 5.10 4.50 -8 4 -9 5.00 4.30 -8 4 -9 9.50 4.30 8 -4 9 3.70 5.60 8 -4 9 6.90 4.80 8 -4 9 7.00 3.70 8 -4 9 7.70 3.90 -9 4 -9 -2.00 2.50 -9 4 -9 1.00 3.60 9 -4 9 -2.40 3.90 9 -4 9 1.30 3.40 9 -4 9 -1.50 4.30 10 3 -9 2.60 4.30 10 3 -9 0.30 2.50 10 3 -9 -1.70 4.90 10 3 -9 -1.80 4.70 10 3 -9 5.90 5.00 10 3 -9 -0.10 2.90 -10 -3 9 1.50 7.80 -10 -3 9 -2.30 4.30 -10 -3 9 3.70 4.70 -10 -3 9 2.60 3.50 9 3 -9 -1.00 3.80 9 3 -9 0.70 3.90 9 3 -9 0.90 2.90 9 3 -9 -2.40 3.40 9 3 -9 1.00 6.60 9 3 -9 0.50 3.60 9 3 -9 -0.50 2.20 -9 -3 9 7.00 6.60 -9 -3 9 1.70 3.00 -9 -3 9 4.20 4.20 -9 -3 9 -1.00 2.70 8 3 -9 3.60 3.90 8 3 -9 9.10 8.40 8 3 -9 8.40 3.90 8 3 -9 -2.20 3.60 8 3 -9 -2.50 4.00 8 3 -9 -1.30 2.30 8 3 -9 1.50 2.40 8 3 -9 2.20 3.60 -8 -3 9 2.40 3.60 -8 -3 9 2.50 6.40 -8 -3 9 1.10 2.50 -8 -3 9 -3.60 3.20 7 3 -9 0.90 2.00 7 3 -9 2.10 2.50 7 3 -9 5.90 3.00 7 3 -9 2.50 3.10 7 3 -9 -1.60 3.50 7 3 -9 1.50 3.00 7 3 -9 -4.40 6.30 7 3 -9 7.90 3.40 7 3 -9 5.40 2.60 7 3 -9 7.90 3.60 -7 -3 9 3.40 4.10 -7 -3 9 4.70 4.10 -7 -3 9 13.20 4.30 -7 -3 9 9.70 6.90 6 3 -9 -2.20 2.40 6 3 -9 0.90 5.00 6 3 -9 0.80 3.50 6 3 -9 5.50 3.00 6 3 -9 3.20 2.30 6 3 -9 2.50 2.20 6 3 -9 11.10 3.60 6 3 -9 -0.10 2.90 6 3 -9 6.80 3.40 -6 -3 9 7.60 3.30 -6 -3 9 2.00 4.10 -6 -3 9 -2.80 3.00 -6 -3 9 3.10 3.00 5 3 -9 26.60 5.30 5 3 -9 42.50 5.70 5 3 -9 39.10 7.00 5 3 -9 22.00 5.40 5 3 -9 30.90 6.20 5 3 -9 42.20 6.00 5 3 -9 50.89 10.80 5 3 -9 41.20 6.80 -5 -3 9 25.50 8.00 -5 -3 9 28.50 6.30 -5 -3 9 25.40 5.60 -5 -3 9 35.30 6.20 -5 -3 9 25.50 6.20 4 3 -9 245.18 16.00 4 3 -9 272.87 15.60 4 3 -9 255.77 15.40 4 3 -9 242.38 15.80 4 3 -9 265.47 21.00 4 3 -9 271.07 17.10 4 3 -9 255.87 17.60 4 3 -9 262.47 17.60 4 3 -9 241.98 16.60 -4 -3 9 259.87 18.00 -4 -3 9 262.87 16.50 -4 -3 9 262.37 17.50 -4 -3 9 211.18 16.70 -4 -3 9 265.67 21.40 3 3 -9 312.17 19.20 3 3 -9 307.17 19.00 3 3 -9 276.47 17.20 3 3 -9 298.87 16.90 3 3 -9 274.87 18.00 3 3 -9 298.17 17.30 3 3 -9 280.67 16.60 -3 -3 9 273.87 21.70 -3 -3 9 262.57 18.00 -3 -3 9 285.87 17.30 -3 -3 9 284.17 19.00 -3 -3 9 282.87 18.60 2 3 -9 21.00 3.90 2 3 -9 12.50 3.00 2 3 -9 17.20 4.50 2 3 -9 22.20 3.80 2 3 -9 16.30 3.80 2 3 -9 12.60 3.20 2 3 -9 18.50 4.60 2 3 -9 14.80 2.60 -2 -3 9 10.60 3.70 -2 -3 9 14.70 3.60 -2 -3 9 22.00 4.80 -2 -3 9 16.50 4.30 -2 -3 9 17.80 6.50 1 3 -9 8.00 3.10 1 3 -9 3.00 1.90 1 3 -9 6.70 3.20 1 3 -9 7.20 2.00 1 3 -9 5.10 1.80 1 3 -9 2.60 1.90 1 3 -9 2.20 1.70 1 3 -9 3.00 2.10 -1 -3 9 0.70 2.70 -1 -3 9 3.90 2.80 -1 -3 9 3.10 2.90 -1 -3 9 6.10 4.50 -1 -3 9 4.80 2.40 0 3 -9 351.76 19.50 0 3 -9 379.26 20.50 0 3 -9 358.36 20.70 0 3 -9 366.06 20.80 0 3 -9 379.96 21.90 0 3 -9 390.26 21.50 0 3 -9 370.86 20.80 0 3 -9 354.36 19.40 0 -3 9 389.36 21.90 0 -3 9 382.86 22.50 0 -3 9 403.36 20.70 0 -3 9 369.86 21.70 0 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7 -10 10.60 3.70 2 7 -10 6.10 4.40 2 7 -10 8.00 4.40 2 7 -10 9.00 4.00 -2 -7 10 18.40 8.10 -2 -7 10 9.70 4.20 -2 -7 10 8.10 5.50 -2 -7 10 8.40 3.80 -2 -7 10 12.40 5.20 1 7 -10 31.40 6.00 1 7 -10 39.80 7.30 1 7 -10 38.80 6.70 1 7 -10 38.60 7.10 1 7 -10 42.10 6.60 1 7 -10 42.40 6.20 -1 -7 10 44.50 8.00 -1 -7 10 26.80 8.80 -1 -7 10 34.20 6.80 -1 -7 10 34.20 7.30 -1 -7 10 44.50 8.30 0 7 -10 15.70 5.10 0 7 -10 10.00 4.00 0 7 -10 14.50 4.70 0 7 -10 10.90 3.80 0 7 -10 7.40 3.50 0 7 -10 13.90 4.00 0 -7 10 7.10 6.10 0 -7 10 10.30 4.80 0 -7 10 6.60 4.30 0 -7 10 8.60 4.40 0 -7 10 9.00 4.30 -1 7 -10 1.50 2.30 -1 7 -10 3.10 3.40 -1 7 -10 1.00 1.80 -1 7 -10 -1.50 2.60 1 -7 10 0.00 2.40 1 -7 10 1.10 3.80 1 -7 10 -2.60 7.10 1 -7 10 -0.50 2.90 -2 7 -10 3.00 3.30 -2 7 -10 0.10 2.00 -2 7 -10 3.40 2.80 -2 7 -10 3.20 2.50 2 -7 10 0.30 4.10 2 -7 10 -0.60 3.90 2 -7 10 3.50 3.00 2 -7 10 1.20 2.70 -3 7 -10 73.69 9.10 -3 7 -10 99.39 10.70 -3 7 -10 89.69 10.20 -3 7 -10 82.09 9.70 3 -7 10 78.19 10.10 3 -7 10 90.19 11.60 -4 7 -10 15.00 4.10 -4 7 -10 19.20 5.10 -4 7 -10 9.70 4.20 4 -7 10 9.30 4.30 4 -7 10 6.80 5.40 4 -7 10 9.80 4.50 4 -7 10 14.50 5.70 -5 7 -10 6.10 4.00 -5 7 -10 -1.10 2.20 -5 7 -10 3.10 2.30 5 -7 10 -0.40 4.20 5 -7 10 -2.10 2.50 5 -7 10 -0.70 7.70 -6 7 -10 4.10 2.80 -6 7 -10 -3.60 2.80 -6 7 -10 -3.50 3.70 6 -7 10 0.80 8.90 6 -7 10 -4.30 2.30 6 -7 10 -9.20 3.80 9 6 -10 2.10 5.80 9 6 -10 -0.10 4.60 9 6 -10 -4.00 4.20 9 6 -10 -2.00 3.90 -9 -6 10 1.10 5.10 -9 -6 10 -1.20 3.10 -9 -6 10 -0.70 3.70 8 6 -10 11.10 5.20 8 6 -10 5.30 6.10 8 6 -10 13.70 6.10 8 6 -10 15.50 6.30 8 6 -10 24.30 6.60 -8 -6 10 7.00 5.20 -8 -6 10 9.80 5.90 -8 -6 10 9.10 5.90 7 6 -10 -1.40 4.20 7 6 -10 1.80 2.80 7 6 -10 -2.40 4.20 7 6 -10 2.70 3.40 7 6 -10 1.90 3.70 7 6 -10 2.90 8.80 7 6 -10 1.50 3.40 -7 -6 10 -1.30 2.40 -7 -6 10 -4.10 6.80 -7 -6 10 -2.80 4.50 -7 -6 10 -3.80 2.70 6 6 -10 9.90 5.50 6 6 -10 8.70 4.70 6 6 -10 2.90 3.60 6 6 -10 0.60 3.40 6 6 -10 4.30 2.90 6 6 -10 14.30 7.50 6 6 -10 1.80 4.00 6 6 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5.50 -6 -2 10 1.60 2.80 -6 -2 10 2.10 3.90 -6 -2 10 5.30 3.10 -6 -2 10 2.20 2.50 5 2 -10 1.70 2.20 5 2 -10 0.00 1.60 5 2 -10 -1.40 2.00 5 2 -10 0.70 2.70 5 2 -10 -1.90 3.90 5 2 -10 -0.80 2.30 5 2 -10 -1.60 1.90 5 2 -10 -0.40 2.00 5 2 -10 -1.30 2.30 5 2 -10 -3.30 2.20 -5 -2 10 4.70 3.30 -5 -2 10 -4.30 2.70 -5 -2 10 3.90 4.60 -5 -2 10 -0.40 1.90 -5 -2 10 0.60 2.30 4 2 -10 256.87 18.70 4 2 -10 291.97 17.60 4 2 -10 263.37 17.40 4 2 -10 285.27 18.50 4 2 -10 295.87 17.40 4 2 -10 269.77 18.70 4 2 -10 307.87 18.30 4 2 -10 281.27 17.30 -4 -2 10 299.47 17.50 -4 -2 10 314.77 19.00 -4 -2 10 286.57 19.50 -4 -2 10 252.87 18.30 -4 -2 10 287.87 22.60 3 2 -10 2.10 1.90 3 2 -10 -0.50 1.80 3 2 -10 1.60 1.90 3 2 -10 1.60 1.60 3 2 -10 -0.10 1.50 3 2 -10 0.30 1.70 3 2 -10 1.90 1.80 3 2 -10 -0.40 2.00 3 2 -10 0.40 1.80 -3 -2 10 -2.20 1.30 -3 -2 10 -3.70 1.70 -3 -2 10 -0.30 2.50 -3 -2 10 1.40 3.30 -3 -2 10 1.80 2.20 2 2 -10 0.70 1.40 2 2 -10 -0.60 1.30 2 2 -10 -0.80 1.20 2 2 -10 1.00 1.70 2 2 -10 1.70 1.90 2 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-1.30 4.80 4 -2 -17 4.40 3.70 4 -2 -17 -0.60 4.10 4 -2 -17 5.00 5.00 -4 2 17 12.80 5.30 -4 2 17 9.40 5.10 -4 2 17 10.60 4.20 3 -2 -17 1.10 4.00 3 -2 -17 3.40 4.00 3 -2 -17 2.50 3.30 3 -2 -17 -1.00 3.50 3 -2 -17 0.20 4.10 3 -2 -17 3.80 3.70 -3 2 17 3.80 4.00 -3 2 17 7.90 4.10 -3 2 17 3.10 4.40 2 -2 -17 2.90 3.90 2 -2 -17 2.50 3.70 2 -2 -17 -0.30 3.30 2 -2 -17 -4.50 3.30 2 -2 -17 8.80 4.60 2 -2 -17 -0.60 2.30 -2 2 17 0.80 3.70 -2 2 17 -0.40 3.20 -2 2 17 3.30 2.80 1 -2 -17 0.00 2.20 1 -2 -17 4.50 4.20 1 -2 -17 1.60 3.70 1 -2 -17 -2.30 3.60 1 -2 -17 1.10 2.90 1 -2 -17 0.10 3.50 1 -2 -17 3.90 3.90 -1 2 17 0.70 3.30 -1 2 17 4.30 4.30 -1 2 17 2.20 2.50 -1 2 17 2.40 2.90 -1 2 17 -7.10 3.30 0 -2 -17 -2.80 3.80 0 -2 -17 0.00 3.20 0 -2 -17 5.70 4.50 0 -2 -17 0.10 2.70 0 -2 -17 3.50 3.50 0 -2 -17 4.90 4.10 0 -2 -17 -0.30 2.80 0 2 17 -0.40 2.80 0 2 17 2.30 3.40 0 2 17 0.20 2.50 0 2 17 -1.50 2.90 0 2 17 -1.10 3.00 -1 -2 -17 10.10 4.50 -1 -2 -17 15.70 5.10 -1 -2 -17 6.60 4.20 -1 -2 -17 2.70 4.90 -1 -2 -17 10.30 5.30 -1 -2 -17 7.10 4.60 1 2 17 2.30 3.30 1 2 17 6.80 4.00 1 2 17 5.30 3.90 1 2 17 14.80 4.80 1 2 17 5.10 3.40 -2 -2 -17 57.59 8.10 -2 -2 -17 30.10 7.30 -2 -2 -17 54.59 8.90 -2 -2 -17 54.39 8.50 -2 -2 -17 50.29 8.00 -2 -2 -17 44.40 8.40 2 2 17 49.50 7.70 2 2 17 46.30 8.20 2 2 17 48.40 7.80 2 2 17 35.80 8.30 2 2 17 28.00 6.70 -3 -2 -17 6.00 4.90 -3 -2 -17 14.50 4.70 -3 -2 -17 22.10 8.40 -3 -2 -17 6.60 4.10 3 2 17 13.50 5.10 3 2 17 6.30 4.80 3 2 17 17.40 5.70 3 2 17 2.50 5.80 -4 -2 -17 -0.20 4.10 -4 -2 -17 0.90 4.30 4 2 17 4.10 6.60 4 2 17 -1.40 3.60 4 2 17 -1.50 2.40 4 2 17 2.10 3.20 -5 -2 -17 18.60 6.50 -5 -2 -17 13.70 4.90 5 2 17 10.60 5.90 5 2 17 5.80 4.30 3 -3 -17 6.30 5.10 3 -3 -17 2.40 4.70 3 -3 -17 6.00 5.10 3 -3 -17 -1.80 2.60 3 -3 -17 -2.60 3.70 -3 3 17 0.60 3.60 -3 3 17 -0.50 4.30 -3 3 17 3.10 3.20 2 -3 -17 3.60 3.70 2 -3 -17 -0.70 3.90 2 -3 -17 -0.10 3.50 2 -3 -17 0.80 2.60 2 -3 -17 1.20 5.30 2 -3 -17 1.60 4.30 -2 3 17 5.90 3.40 -2 3 17 2.30 3.60 -2 3 17 -0.40 2.40 1 -3 -17 1.80 4.20 1 -3 -17 -2.30 3.70 1 -3 -17 0.50 2.80 1 -3 -17 1.40 4.50 1 -3 -17 -0.20 2.30 -1 3 17 5.70 3.80 -1 3 17 3.40 3.00 -1 3 17 -0.20 3.70 0 -3 -17 -1.70 5.50 0 -3 -17 4.40 4.30 0 -3 -17 0.10 2.40 0 -3 -17 -5.60 2.80 0 -3 -17 0.00 2.80 0 -3 -17 -1.20 3.10 0 3 17 4.20 2.80 0 3 17 0.80 3.50 0 3 17 2.80 2.90 0 3 17 3.10 3.20 -1 -3 -17 89.39 10.70 -1 -3 -17 87.99 11.00 -1 -3 -17 67.09 10.70 -1 -3 -17 65.09 9.60 -1 -3 -17 48.70 9.30 -1 -3 -17 83.69 11.80 1 3 17 67.79 10.50 1 3 17 70.69 9.30 1 3 17 46.60 8.50 1 3 17 80.79 11.10 1 3 17 86.99 10.40 -2 -3 -17 23.50 6.10 -2 -3 -17 19.60 5.00 -2 -3 -17 24.60 5.90 -2 -3 -17 16.10 5.40 -2 -3 -17 17.10 5.50 2 3 17 30.00 6.50 2 3 17 31.80 6.60 2 3 17 5.90 4.10 2 3 17 30.50 7.00 2 3 17 44.30 7.30 -3 -3 -17 2.50 3.10 -3 -3 -17 4.00 3.50 -3 -3 -17 -2.60 3.20 3 3 17 -1.80 2.20 3 3 17 0.90 4.30 3 3 17 -0.80 2.70 -4 -3 -17 -2.00 2.90 -4 -3 -17 3.60 3.30 4 3 17 0.60 4.30 4 3 17 3.50 3.50 4 3 17 0.10 2.60 2 -4 -17 9.90 6.00 2 -4 -17 3.30 4.10 2 -4 -17 9.80 4.30 2 -4 -17 0.60 5.00 -2 4 17 3.50 4.50 -2 4 17 4.90 3.60 -2 4 17 11.00 4.10 -2 4 17 6.40 4.60 1 -4 -17 10.70 5.40 1 -4 -17 1.90 3.10 1 -4 -17 4.70 4.00 1 -4 -17 1.30 3.30 -1 4 17 11.00 4.40 -1 4 17 7.20 5.10 -1 4 17 -1.00 2.70 -1 4 17 1.80 2.40 0 -4 -17 3.70 4.50 0 -4 -17 4.30 4.20 0 -4 -17 2.80 2.80 0 -4 -17 -1.70 2.50 0 4 17 -0.70 2.20 0 4 17 3.40 3.10 0 4 17 7.80 4.60 -1 -4 -17 3.00 3.70 -1 -4 -17 17.20 5.60 -1 -4 -17 15.40 5.10 -1 -4 -17 20.50 5.70 -1 -4 -17 27.50 6.80 1 4 17 4.70 3.90 1 4 17 28.80 6.20 1 4 17 21.00 6.40 1 4 17 16.60 4.50 -2 -4 -17 1.30 2.60 -2 -4 -17 1.80 2.80 -2 -4 -17 0.70 3.20 -2 -4 -17 -0.10 3.40 -2 -4 -17 9.70 5.60 2 4 17 5.90 4.20 2 4 17 -0.60 2.80 2 4 17 2.20 2.30 2 4 17 4.10 3.00 -3 -4 -17 4.80 4.60 -3 -4 -17 4.20 4.40 3 4 17 12.40 4.70 3 4 17 0.50 2.10 3 4 17 6.90 5.20 4 4 17 2.50 3.80 4 4 17 -1.40 2.80 1 -5 -17 -1.00 4.00 1 -5 -17 0.60 2.80 -1 5 17 2.60 3.00 -1 5 17 5.60 3.90 0 -5 -17 1.00 3.20 0 -5 -17 -2.10 3.00 0 -5 -17 1.70 3.60 0 -5 -17 1.80 2.70 0 5 17 -0.50 3.60 0 5 17 -2.30 1.90 0 5 17 9.40 5.40 0 5 17 -1.30 2.10 -1 -5 -17 -2.20 2.00 -1 -5 -17 -1.70 3.80 -1 -5 -17 1.20 4.70 -1 -5 -17 3.40 3.50 1 5 17 2.30 3.00 1 5 17 6.90 4.30 1 5 17 3.50 3.50 1 5 17 -1.50 4.00 -2 -5 -17 5.70 4.40 -2 -5 -17 8.10 6.00 -2 -5 -17 17.50 6.50 -2 -5 -17 14.60 4.80 2 5 17 3.00 2.80 2 5 17 13.50 5.80 2 5 17 10.50 4.80 2 5 17 8.10 4.30 2 5 17 9.40 5.00 2 3 -18 65.59 10.40 2 3 -18 84.99 11.60 2 3 -18 93.89 13.40 2 3 -18 94.49 14.40 2 3 -18 71.39 11.20 -2 -3 18 75.39 12.60 -2 -3 18 97.19 13.00 -2 -3 18 83.99 13.20 1 3 -18 10.20 5.50 1 3 -18 3.00 5.00 1 3 -18 -1.90 3.80 1 3 -18 12.60 5.10 -1 -3 18 1.40 4.00 -1 -3 18 -1.80 4.90 -1 -3 18 2.90 4.20 0 3 -18 6.10 4.30 0 3 -18 1.40 3.20 0 3 -18 2.20 4.90 0 3 -18 3.80 4.00 0 -3 18 12.60 5.80 0 -3 18 0.30 3.70 0 -3 18 4.10 3.20 0 -3 18 -3.10 4.40 -1 3 -18 6.00 5.30 -1 3 -18 -1.90 3.70 -1 3 -18 -2.90 2.60 -1 3 -18 1.90 4.20 1 -3 18 -1.00 3.90 1 -3 18 -2.40 3.70 1 -3 18 0.40 3.20 1 -3 18 -1.20 2.90 3 2 -18 4.50 4.90 3 2 -18 -1.50 4.80 3 2 -18 0.80 3.80 3 2 -18 5.80 4.30 3 2 -18 -0.20 4.00 -3 -2 18 -2.40 4.80 -3 -2 18 5.80 4.90 -3 -2 18 1.30 3.60 2 2 -18 22.10 7.80 2 2 -18 13.20 5.70 2 2 -18 27.00 6.60 2 2 -18 13.80 5.20 -2 -2 18 20.00 6.40 -2 -2 18 21.00 7.00 -2 -2 18 23.50 7.50 1 2 -18 1.90 2.90 1 2 -18 4.70 4.70 1 2 -18 6.80 4.40 1 2 -18 8.50 4.60 -1 -2 18 0.60 3.80 -1 -2 18 7.20 4.80 -1 -2 18 6.40 5.20 0 2 -18 0.50 2.50 0 2 -18 2.80 4.00 0 2 -18 1.90 3.90 0 2 -18 4.90 5.10 0 -2 18 -2.00 3.00 0 -2 18 5.30 4.10 0 -2 18 0.60 4.90 -1 2 -18 -0.70 2.50 -1 2 -18 7.80 3.80 -1 2 -18 4.80 4.80 -1 2 -18 -2.20 3.00 1 -2 18 1.50 3.80 1 -2 18 7.30 4.40 1 -2 18 0.80 4.10 -2 2 -18 2.10 3.80 -2 2 -18 1.20 3.10 -2 2 -18 6.20 4.90 2 -2 18 -1.40 3.00 2 -2 18 7.60 3.90 2 -2 18 2.50 4.40 3 1 -18 0.30 4.30 3 1 -18 -0.80 4.50 3 1 -18 4.00 4.70 3 1 -18 2.20 4.50 -3 -1 18 -1.70 4.10 -3 -1 18 6.20 5.40 -3 -1 18 7.30 5.00 2 1 -18 2.10 5.00 2 1 -18 3.80 3.60 2 1 -18 -5.60 3.20 2 1 -18 0.80 3.00 -2 -1 18 3.00 3.50 -2 -1 18 5.80 4.50 -2 -1 18 4.30 8.10 -2 -1 18 -2.40 2.70 1 1 -18 10.00 5.80 1 1 -18 -1.30 2.80 1 1 -18 -0.60 2.50 1 1 -18 1.90 3.10 -1 -1 18 0.40 2.50 -1 -1 18 0.10 6.50 -1 -1 18 -1.80 4.80 -1 -1 18 -0.90 3.00 0 1 -18 0.30 3.90 0 1 -18 -2.30 3.40 0 1 -18 4.30 4.60 0 1 -18 -1.10 4.20 0 -1 18 4.40 4.20 0 -1 18 6.10 4.50 0 -1 18 3.90 6.30 0 -1 18 -0.50 3.90 -1 1 -18 -1.70 3.30 -1 1 -18 -1.80 4.20 -1 1 -18 -0.40 4.00 -1 1 -18 0.00 3.20 1 -1 18 0.80 3.50 1 -1 18 2.00 4.00 1 -1 18 4.60 3.50 -2 1 -18 0.70 4.60 -2 1 -18 4.20 3.90 -2 1 -18 -0.80 2.60 -2 1 -18 4.20 4.40 -2 1 -18 1.50 4.30 -2 1 -18 -0.40 2.60 2 -1 18 0.20 3.50 2 -1 18 -6.00 3.40 2 -1 18 0.20 3.40 2 -1 18 11.30 3.80 -3 1 -18 1.40 3.80 -3 1 -18 1.70 3.90 -3 1 -18 2.50 3.30 3 -1 18 11.00 6.10 3 -1 18 -0.10 3.30 3 0 -18 3.50 3.80 3 0 -18 10.60 5.90 3 0 -18 6.00 5.60 3 0 -18 -3.00 3.30 -3 0 18 5.60 5.20 -3 0 18 10.40 4.10 -3 0 18 6.80 4.40 -3 0 18 -0.90 3.50 2 0 -18 5.90 3.80 2 0 -18 -0.90 3.80 2 0 -18 1.70 3.20 2 0 -18 -0.60 4.70 -2 0 18 -2.60 6.40 -2 0 18 1.80 2.70 -2 0 18 8.50 4.20 -2 0 18 0.20 3.20 -2 0 18 -1.10 4.30 1 0 -18 8.40 4.50 1 0 -18 -3.70 2.40 1 0 -18 0.00 2.40 1 0 -18 2.20 3.40 -1 0 18 -3.50 3.10 -1 0 18 6.00 3.50 -1 0 18 8.30 4.40 -1 0 18 2.00 4.00 -1 0 18 0.60 5.50 0 0 -18 27.40 6.10 0 0 -18 30.90 7.00 0 0 -18 32.20 8.20 0 0 -18 34.00 7.10 0 0 -18 35.30 7.50 0 0 18 39.40 8.60 0 0 18 5.40 4.70 0 0 18 25.50 6.10 0 0 18 42.90 9.00 -1 0 -18 3.50 4.40 -1 0 -18 3.40 4.30 -1 0 -18 -3.90 2.40 -1 0 -18 3.20 3.90 -1 0 -18 0.50 2.90 -1 0 -18 0.10 2.80 -1 0 -18 0.30 4.30 1 0 18 2.60 3.60 1 0 18 7.50 4.70 1 0 18 1.90 5.30 1 0 18 3.50 2.60 1 0 18 2.50 5.30 1 0 18 0.80 3.00 -2 0 -18 -1.20 3.70 -2 0 -18 7.50 5.30 -2 0 -18 -4.00 3.90 -2 0 -18 6.80 4.10 -2 0 -18 6.00 4.10 -2 0 -18 -1.60 3.70 -2 0 -18 -3.10 2.60 2 0 18 4.90 4.00 2 0 18 -1.40 4.40 2 0 18 3.70 3.70 2 0 18 4.70 4.10 2 0 18 2.60 4.00 -3 0 -18 2.50 3.70 -3 0 -18 11.40 4.70 -3 0 -18 4.00 5.00 3 0 18 7.40 5.40 3 0 18 2.50 4.10 3 0 18 0.10 2.80 3 -1 -18 5.20 5.10 3 -1 -18 4.30 5.20 3 -1 -18 -1.90 4.20 3 -1 -18 0.60 2.70 -3 1 18 10.70 4.70 -3 1 18 2.60 4.40 -3 1 18 -0.80 4.40 2 -1 -18 0.90 4.30 2 -1 -18 1.80 3.10 2 -1 -18 4.70 4.20 2 -1 -18 -3.30 2.50 2 -1 -18 -0.90 3.00 -2 1 18 -4.20 3.00 -2 1 18 0.10 2.00 -2 1 18 -3.20 3.90 -2 1 18 -0.20 2.50 1 -1 -18 -3.00 4.80 1 -1 -18 2.80 3.60 1 -1 -18 -2.60 2.90 1 -1 -18 4.50 4.10 1 -1 -18 3.00 3.50 1 -1 -18 -3.70 2.40 -1 1 18 1.60 3.80 -1 1 18 -0.20 2.50 -1 1 18 -0.80 2.80 -1 1 18 0.90 4.60 0 -1 -18 8.70 5.10 0 -1 -18 -1.90 3.60 0 -1 -18 -1.80 3.00 0 -1 -18 0.30 3.70 0 -1 -18 -0.20 3.70 0 -1 -18 1.10 3.40 0 1 18 1.90 3.60 0 1 18 -3.10 2.80 0 1 18 -0.30 3.80 0 1 18 2.20 3.60 -1 -1 -18 4.70 4.10 -1 -1 -18 -1.20 3.20 -1 -1 -18 -3.80 3.60 -1 -1 -18 -0.70 4.30 -1 -1 -18 1.60 3.70 -1 -1 -18 3.60 3.00 -1 -1 -18 1.40 4.30 1 1 18 2.20 5.50 1 1 18 0.20 3.50 1 1 18 3.10 5.20 1 1 18 2.60 3.60 1 1 18 0.80 2.70 1 1 18 1.70 3.50 -2 -1 -18 -1.60 2.40 -2 -1 -18 6.00 4.90 -2 -1 -18 2.40 4.90 -2 -1 -18 0.40 3.60 -2 -1 -18 0.80 3.70 2 1 18 1.70 3.00 2 1 18 -3.60 2.80 2 1 18 0.90 4.80 2 1 18 1.50 2.60 2 1 18 0.90 5.20 2 1 18 -5.10 3.30 -3 -1 -18 2.60 3.60 -3 -1 -18 4.80 4.60 -3 -1 -18 3.90 4.00 3 1 18 6.20 4.80 3 1 18 0.60 3.20 3 1 18 3.20 4.40 2 -2 -18 -0.40 3.90 2 -2 -18 6.40 4.50 2 -2 -18 2.70 3.50 2 -2 -18 7.00 5.00 2 -2 -18 3.10 4.10 -2 2 18 3.10 4.10 -2 2 18 11.00 5.40 -2 2 18 1.80 4.50 1 -2 -18 0.40 2.50 1 -2 -18 0.50 4.10 1 -2 -18 0.90 3.00 1 -2 -18 6.30 3.70 1 -2 -18 0.70 3.10 1 -2 -18 -2.20 7.00 -1 2 18 1.60 2.90 -1 2 18 0.70 3.40 -1 2 18 2.70 3.70 0 -2 -18 -1.90 3.90 0 -2 -18 -3.40 2.20 0 -2 -18 -0.10 3.50 0 -2 -18 -1.60 2.40 0 -2 -18 5.80 6.30 0 2 18 -0.40 3.30 0 2 18 -1.50 2.20 0 2 18 3.90 4.80 0 2 18 -1.90 3.90 -1 -2 -18 6.50 4.00 -1 -2 -18 4.60 3.80 -1 -2 -18 4.50 3.20 -1 -2 -18 4.50 3.50 1 2 18 -3.90 3.50 1 2 18 0.00 3.80 1 2 18 4.00 3.70 1 2 18 8.50 4.20 -2 -2 -18 7.60 5.50 -2 -2 -18 13.90 4.70 -2 -2 -18 29.60 7.50 -2 -2 -18 19.80 5.10 -2 -2 -18 31.20 6.90 2 2 18 22.20 6.80 2 2 18 20.80 4.90 2 2 18 14.70 6.00 2 2 18 7.80 4.60 2 2 18 23.90 5.60 -3 -2 -18 4.90 4.00 -3 -2 -18 -3.60 3.70 -3 -2 -18 6.30 3.20 3 2 18 -1.10 4.30 3 2 18 1.50 3.10 3 2 18 1.20 3.40 1 -3 -18 0.00 4.60 1 -3 -18 -1.10 3.00 1 -3 -18 1.20 3.20 1 -3 -18 -1.50 4.20 -1 3 18 1.40 2.80 -1 3 18 -0.80 2.70 -1 3 18 -2.80 3.60 0 -3 -18 5.90 4.20 0 -3 -18 8.70 4.70 0 -3 -18 -0.50 4.50 0 -3 -18 2.50 3.60 0 3 18 7.20 4.50 0 3 18 3.40 4.50 0 3 18 0.20 4.50 -1 -3 -18 2.40 2.70 -1 -3 -18 1.80 3.90 -1 -3 -18 1.60 2.70 -1 -3 -18 -2.90 2.40 1 3 18 1.20 4.00 1 3 18 0.20 2.80 1 3 18 2.90 3.40 -2 -3 -18 70.99 11.30 -2 -3 -18 69.09 9.80 -2 -3 -18 79.79 10.50 -2 -3 -18 48.20 9.90 -2 -3 -18 75.79 14.40 2 3 18 83.69 11.40 2 3 18 88.89 10.80 2 3 18 65.79 10.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 87738 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 0.2753(2) 0.1929(2) 0.14202(12) 0.0660(6) Uani 1 1 d . . . . . O002 O 0.7750(2) 0.1930(2) 0.35790(12) 0.0661(6) Uani 1 1 d . . . . . O003 O 0.3635(2) 0.4067(2) 0.47418(13) 0.0679(6) Uani 1 1 d . . . . . O004 O -0.1364(2) 0.4069(2) 0.02569(13) 0.0683(6) Uani 1 1 d . . . . . N005 N 0.5709(2) 0.3011(2) 0.41724(12) 0.0459(5) Uani 1 1 d . . . . . N006 N 0.0708(2) 0.3013(2) 0.08276(12) 0.0461(5) Uani 1 1 d . . . . . C007 C 0.5957(2) 0.1116(2) 0.56109(14) 0.0377(5) Uani 1 1 d . . . . . C008 C 0.0954(2) 0.1117(2) -0.06106(14) 0.0377(5) Uani 1 1 d . . . . . C009 C 0.4774(2) 0.2147(2) 0.55602(15) 0.0412(6) Uani 1 1 d . . . . . C00A C -0.0224(2) 0.2145(2) -0.05605(15) 0.0407(5) Uani 1 1 d . . . . . C00B C 0.6996(2) 0.0992(2) 0.49345(14) 0.0406(5) Uani 1 1 d . . . . . C00C C 0.1999(2) 0.0995(2) 0.00662(15) 0.0408(6) Uani 1 1 d . . . . . C00D C 0.1111(3) 0.0176(2) -0.13495(15) 0.0438(6) Uani 1 1 d . . . . . C00E C 0.6114(3) 0.0173(3) 0.63500(15) 0.0445(6) Uani 1 1 d . . . . . C00F C 0.4630(3) 0.3147(3) 0.48093(16) 0.0461(6) Uani 1 1 d . . . . . C00G C -0.0371(3) 0.3147(3) 0.01898(16) 0.0465(6) Uani 1 1 d . . . . . C00H C 0.1868(3) 0.1987(3) 0.08221(15) 0.0449(6) Uani 1 1 d . . . . . C00I C 0.6867(3) 0.1986(3) 0.41756(15) 0.0452(6) Uani 1 1 d . . . . . C00J C 0.3134(3) -0.0032(3) 0.00161(17) 0.0508(6) Uani 1 1 d . . . . . H00J H 0.380409 -0.012218 0.047286 0.061 Uiso 1 1 calc R U . . . C00K C 0.8132(3) -0.0031(3) 0.49837(17) 0.0515(6) Uani 1 1 d . . . . . H00K H 0.880390 -0.011823 0.452660 0.062 Uiso 1 1 calc R U . . . C00L C 0.5059(3) 0.0311(3) 0.70177(17) 0.0562(7) Uani 1 1 d . . . . . H00L H 0.514505 -0.028706 0.751012 0.067 Uiso 1 1 calc R U . . . C00M C 0.7308(3) -0.0846(3) 0.63838(17) 0.0539(7) Uani 1 1 d . . . . . H00M H 0.742662 -0.145938 0.686797 0.065 Uiso 1 1 calc R U . . . C00N C 0.2310(3) -0.0847(3) -0.13806(18) 0.0543(7) Uani 1 1 d . . . . . H00N H 0.242997 -0.146143 -0.186297 0.065 Uiso 1 1 calc R U . . . C00O C 0.0053(3) 0.0314(3) -0.20164(17) 0.0567(7) Uani 1 1 d . . . . . H00O H 0.013863 -0.028534 -0.250721 0.068 Uiso 1 1 calc R U . . . C00P C -0.0184(3) 0.3758(3) 0.23607(16) 0.0521(7) Uani 1 1 d . . . . . H00A H 0.032150 0.294895 0.265944 0.063 Uiso 1 1 calc R U . . . H00B H -0.108850 0.354152 0.217291 0.063 Uiso 1 1 calc R U . . . C00Q C 0.4815(3) 0.3760(3) 0.26396(16) 0.0524(7) Uani 1 1 d . . . . . H00C H 0.390941 0.354314 0.282864 0.063 Uiso 1 1 calc R U . . . H00D H 0.532050 0.295195 0.234144 0.063 Uiso 1 1 calc R U . . . C00R C 0.3759(3) 0.2238(3) 0.62193(18) 0.0550(7) Uani 1 1 d . . . . . H00R H 0.296925 0.291306 0.618195 0.066 Uiso 1 1 calc R U . . . C00S C -0.1243(3) 0.2235(3) -0.12188(18) 0.0554(7) Uani 1 1 d . . . . . H00S H -0.203334 0.290903 -0.117948 0.066 Uiso 1 1 calc R U . . . C00T C 0.8292(3) -0.0949(3) 0.57194(19) 0.0577(7) Uani 1 1 d . . . . . H00T H 0.907690 -0.163075 0.575181 0.069 Uiso 1 1 calc R U . . . C00U C 0.3295(3) -0.0949(3) -0.07165(19) 0.0584(7) Uani 1 1 d . . . . . H00U H 0.407946 -0.163027 -0.074830 0.070 Uiso 1 1 calc R U . . . C00V C 0.5623(3) 0.4084(3) 0.34594(17) 0.0562(7) Uani 1 1 d . . . . . H00E H 0.656713 0.418987 0.327575 0.067 Uiso 1 1 calc R U . . . H00F H 0.517980 0.495713 0.371001 0.067 Uiso 1 1 calc R U . . . C00W C 0.0626(3) 0.4082(3) 0.15404(17) 0.0562(7) Uani 1 1 d . . . . . H00G H 0.018527 0.495715 0.129023 0.067 Uiso 1 1 calc R U . . . H00H H 0.157058 0.418374 0.172256 0.067 Uiso 1 1 calc R U . . . C00X C -0.1088(3) 0.1311(3) -0.19499(19) 0.0620(8) Uani 1 1 d . . . . . H00X H -0.177714 0.138344 -0.239461 0.074 Uiso 1 1 calc R U . . . C00Y C 0.3916(3) 0.1309(3) 0.69508(18) 0.0630(8) Uani 1 1 d . . . . . H00Y H 0.322710 0.137873 0.739630 0.076 Uiso 1 1 calc R U . . . C00Z C 0.4588(3) 0.4962(3) 0.1968(2) 0.0663(8) Uani 1 1 d . . . . . H00I H 0.398832 0.472768 0.148463 0.080 Uiso 1 1 calc R U . . . H00P H 0.408824 0.576455 0.227562 0.080 Uiso 1 1 calc R U . . . C010 C -0.0412(3) 0.4962(3) 0.3033(2) 0.0681(8) Uani 1 1 d . . . . . H01A H -0.091048 0.576514 0.272493 0.082 Uiso 1 1 calc R U . . . H01B H -0.101378 0.472673 0.351691 0.082 Uiso 1 1 calc R U . . . C011 C 0.0862(4) 0.5345(4) 0.3439(2) 0.0779(9) Uani 1 1 d . . . . . H01C H 0.144643 0.563021 0.296108 0.093 Uiso 1 1 calc R U . . . H01D H 0.138547 0.453731 0.372804 0.093 Uiso 1 1 calc R U . . . C012 C 0.5858(4) 0.5342(4) 0.1565(2) 0.0806(10) Uani 1 1 d . . . . . H01E H 0.638208 0.453450 0.127743 0.097 Uiso 1 1 calc R U . . . H01F H 0.643966 0.562592 0.204304 0.097 Uiso 1 1 calc R U . . . C013 C 0.5581(5) 0.6495(4) 0.0872(3) 0.0969(12) Uani 1 1 d . . . . . H01G H 0.499836 0.622821 0.039848 0.145 Uiso 1 1 calc R U . . . H01H H 0.645602 0.666786 0.062118 0.145 Uiso 1 1 calc R U . . . H01I H 0.511288 0.731720 0.115898 0.145 Uiso 1 1 calc R U . . . C014 C 0.0577(5) 0.6494(4) 0.4128(3) 0.0974(12) Uani 1 1 d . . . . . H01J H 0.012263 0.731947 0.383781 0.146 Uiso 1 1 calc R U . . . H01K H 0.144860 0.665921 0.438708 0.146 Uiso 1 1 calc R U . . . H01L H -0.001972 0.623087 0.459659 0.146 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0692(13) 0.0826(15) 0.0473(11) -0.0067(10) -0.0146(9) -0.0148(11) O002 0.0695(13) 0.0826(15) 0.0468(10) 0.0101(10) 0.0136(9) -0.0139(11) O003 0.0721(13) 0.0611(13) 0.0631(12) 0.0053(10) -0.0100(10) 0.0128(11) O004 0.0720(13) 0.0600(13) 0.0654(12) -0.0023(10) 0.0084(10) 0.0137(11) N005 0.0588(13) 0.0422(12) 0.0377(11) 0.0076(9) -0.0045(9) -0.0110(10) N006 0.0591(13) 0.0424(12) 0.0376(11) -0.0043(9) 0.0026(9) -0.0108(10) C007 0.0446(13) 0.0379(13) 0.0324(11) -0.0019(9) -0.0055(9) -0.0125(10) C008 0.0448(13) 0.0389(13) 0.0315(11) 0.0029(9) 0.0035(9) -0.0127(10) C009 0.0468(13) 0.0410(13) 0.0367(12) -0.0021(10) -0.0023(10) -0.0095(11) C00A 0.0450(13) 0.0414(13) 0.0367(12) 0.0045(10) 0.0008(10) -0.0098(11) C00B 0.0457(13) 0.0424(14) 0.0350(12) -0.0016(10) -0.0052(10) -0.0105(11) C00C 0.0447(13) 0.0430(14) 0.0355(12) 0.0024(10) 0.0034(10) -0.0097(11) C00D 0.0556(15) 0.0422(14) 0.0360(12) 0.0005(10) 0.0062(10) -0.0151(11) C00E 0.0565(15) 0.0445(14) 0.0355(12) 0.0028(10) -0.0074(10) -0.0171(12) C00F 0.0527(15) 0.0428(14) 0.0421(13) 0.0015(11) -0.0101(11) -0.0048(12) C00G 0.0538(15) 0.0420(14) 0.0431(13) 0.0019(11) 0.0075(11) -0.0058(12) C00H 0.0518(14) 0.0502(15) 0.0351(12) 0.0021(11) -0.0010(11) -0.0156(12) C00I 0.0520(14) 0.0495(15) 0.0363(13) 0.0010(11) -0.0020(11) -0.0147(12) C00J 0.0492(14) 0.0564(16) 0.0457(14) 0.0057(12) -0.0010(11) -0.0046(12) C00K 0.0496(15) 0.0570(16) 0.0466(14) -0.0029(12) 0.0013(11) -0.0040(13) C00L 0.0732(19) 0.0574(17) 0.0410(14) 0.0079(12) 0.0024(12) -0.0198(15) C00M 0.0681(17) 0.0463(15) 0.0474(15) 0.0082(12) -0.0173(13) -0.0085(13) C00N 0.0696(18) 0.0461(15) 0.0467(15) -0.0059(12) 0.0152(13) -0.0075(13) C00O 0.0736(19) 0.0583(17) 0.0416(14) -0.0059(12) -0.0030(13) -0.0208(15) C00P 0.0601(16) 0.0529(16) 0.0442(14) -0.0056(11) 0.0016(11) -0.0115(13) C00Q 0.0599(16) 0.0527(16) 0.0457(14) 0.0078(11) -0.0030(12) -0.0121(13) C00R 0.0524(15) 0.0575(17) 0.0548(16) -0.0027(13) 0.0051(12) -0.0072(13) C00S 0.0516(15) 0.0572(17) 0.0565(16) 0.0043(13) -0.0086(12) -0.0058(13) C00T 0.0579(17) 0.0515(16) 0.0597(17) 0.0023(13) -0.0124(13) 0.0039(13) C00U 0.0608(17) 0.0520(17) 0.0590(17) 0.0004(13) 0.0098(13) 0.0023(13) C00V 0.0765(19) 0.0464(15) 0.0487(15) 0.0126(12) -0.0075(13) -0.0190(14) C00W 0.0781(19) 0.0456(15) 0.0476(15) -0.0108(12) 0.0075(13) -0.0183(14) C00X 0.0649(18) 0.072(2) 0.0519(16) 0.0017(14) -0.0199(13) -0.0199(16) C00Y 0.0678(18) 0.073(2) 0.0506(16) 0.0007(14) 0.0180(13) -0.0206(16) C00Z 0.0656(18) 0.078(2) 0.0551(16) 0.0185(15) -0.0092(13) -0.0106(15) C010 0.0673(18) 0.082(2) 0.0546(16) -0.0162(15) 0.0093(14) -0.0107(16) C011 0.072(2) 0.090(2) 0.071(2) -0.0261(18) 0.0007(16) -0.0136(18) C012 0.076(2) 0.094(3) 0.073(2) 0.0307(18) -0.0030(16) -0.0160(19) C013 0.117(3) 0.095(3) 0.083(2) 0.045(2) 0.001(2) -0.029(2) C014 0.117(3) 0.096(3) 0.083(2) -0.044(2) -0.001(2) -0.028(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00I N005 C00F 125.1(2) . . ? C00I N005 C00V 118.0(2) . . ? C00F N005 C00V 116.9(2) . . ? C00H N006 C00G 124.8(2) . . ? C00H N006 C00W 117.9(2) . . ? C00G N006 C00W 117.2(2) . . ? C009 C007 C00B 120.9(2) . . ? C009 C007 C00E 120.1(2) . . ? C00B C007 C00E 119.0(2) . . ? C00A C008 C00C 120.8(2) . . ? C00A C008 C00D 120.0(2) . . ? C00C C008 C00D 119.1(2) . . ? C00R C009 C007 120.0(2) . . ? C00R C009 C00F 119.8(2) . . ? C007 C009 C00F 120.1(2) . . ? C00S C00A C008 120.0(2) . . ? C00S C00A C00G 119.7(2) . . ? C008 C00A C00G 120.2(2) . . ? C00K C00B C007 120.3(2) . . ? C00K C00B C00I 120.0(2) . . ? C007 C00B C00I 119.7(2) . . ? C00J C00C C008 120.1(2) . . ? C00J C00C C00H 120.2(2) . . ? C008 C00C C00H 119.6(2) . . ? C00N C00D C00O 123.1(2) . . ? C00N C00D C008 118.7(2) . . ? C00O C00D C008 118.2(2) . . ? C00M C00E C00L 123.0(2) . . ? C00M C00E C007 118.9(2) . . ? C00L C00E C007 118.2(2) . . ? O003 C00F N005 120.5(2) . . ? O003 C00F C009 122.6(2) . . ? N005 C00F C009 116.9(2) . . ? O004 C00G N006 120.4(2) . . ? O004 C00G C00A 122.7(2) . . ? N006 C00G C00A 116.9(2) . . ? O001 C00H N006 120.6(2) . . ? O001 C00H C00C 122.0(2) . . ? N006 C00H C00C 117.5(2) . . ? O002 C00I N005 120.7(2) . . ? O002 C00I C00B 122.0(2) . . ? N005 C00I C00B 117.3(2) . . ? C00C C00J C00U 120.7(2) . . ? C00C C00J H00J 119.7 . . ? C00U C00J H00J 119.7 . . ? C00B C00K C00T 120.5(2) . . ? C00B C00K H00K 119.8 . . ? C00T C00K H00K 119.8 . . ? C00Y C00L C00E 120.7(2) . . ? C00Y C00L H00L 119.6 . . ? C00E C00L H00L 119.6 . . ? C00T C00M C00E 120.9(2) . . ? C00T C00M H00M 119.5 . . ? C00E C00M H00M 119.5 . . ? C00U C00N C00D 121.0(2) . . ? C00U C00N H00N 119.5 . . ? C00D C00N H00N 119.5 . . ? C00X C00O C00D 120.8(2) . . ? C00X C00O H00O 119.6 . . ? C00D C00O H00O 119.6 . . ? C00W C00P C010 112.2(2) . . ? C00W C00P H00A 109.2 . . ? C010 C00P H00A 109.2 . . ? C00W C00P H00B 109.2 . . ? C010 C00P H00B 109.2 . . ? H00A C00P H00B 107.9 . . ? C00V C00Q C00Z 112.2(2) . . ? C00V C00Q H00C 109.2 . . ? C00Z C00Q H00C 109.2 . . ? C00V C00Q H00D 109.2 . . ? C00Z C00Q H00D 109.2 . . ? H00C C00Q H00D 107.9 . . ? C009 C00R C00Y 119.9(3) . . ? C009 C00R H00R 120.1 . . ? C00Y C00R H00R 120.1 . . ? C00A C00S C00X 120.0(3) . . ? C00A C00S H00S 120.0 . . ? C00X C00S H00S 120.0 . . ? C00M C00T C00K 120.3(2) . . ? C00M C00T H00T 119.8 . . ? C00K C00T H00T 119.8 . . ? C00N C00U C00J 120.4(3) . . ? C00N C00U H00U 119.8 . . ? C00J C00U H00U 119.8 . . ? N005 C00V C00Q 113.4(2) . . ? N005 C00V H00E 108.9 . . ? C00Q C00V H00E 108.9 . . ? N005 C00V H00F 108.9 . . ? C00Q C00V H00F 108.9 . . ? H00E C00V H00F 107.7 . . ? N006 C00W C00P 113.5(2) . . ? N006 C00W H00G 108.9 . . ? C00P C00W H00G 108.9 . . ? N006 C00W H00H 108.9 . . ? C00P C00W H00H 108.9 . . ? H00G C00W H00H 107.7 . . ? C00O C00X C00S 120.9(2) . . ? C00O C00X H00X 119.5 . . ? C00S C00X H00X 119.5 . . ? C00L C00Y C00R 121.1(2) . . ? C00L C00Y H00Y 119.4 . . ? C00R C00Y H00Y 119.4 . . ? C012 C00Z C00Q 115.8(3) . . ? C012 C00Z H00I 108.3 . . ? C00Q C00Z H00I 108.3 . . ? C012 C00Z H00P 108.3 . . ? C00Q C00Z H00P 108.3 . . ? H00I C00Z H00P 107.4 . . ? C011 C010 C00P 115.9(3) . . ? C011 C010 H01A 108.3 . . ? C00P C010 H01A 108.3 . . ? C011 C010 H01B 108.3 . . ? C00P C010 H01B 108.3 . . ? H01A C010 H01B 107.4 . . ? C010 C011 C014 113.8(3) . . ? C010 C011 H01C 108.8 . . ? C014 C011 H01C 108.8 . . ? C010 C011 H01D 108.8 . . ? C014 C011 H01D 108.8 . . ? H01C C011 H01D 107.7 . . ? C00Z C012 C013 114.0(3) . . ? C00Z C012 H01E 108.8 . . ? C013 C012 H01E 108.8 . . ? C00Z C012 H01F 108.8 . . ? C013 C012 H01F 108.8 . . ? H01E C012 H01F 107.7 . . ? C012 C013 H01G 109.5 . . ? C012 C013 H01H 109.5 . . ? H01G C013 H01H 109.5 . . ? C012 C013 H01I 109.5 . . ? H01G C013 H01I 109.5 . . ? H01H C013 H01I 109.5 . . ? C011 C014 H01J 109.5 . . ? C011 C014 H01K 109.5 . . ? H01J C014 H01K 109.5 . . ? C011 C014 H01L 109.5 . . ? H01J C014 H01L 109.5 . . ? H01K C014 H01L 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 C00H 1.225(3) . ? O002 C00I 1.221(3) . ? O003 C00F 1.215(3) . ? O004 C00G 1.215(3) . ? N005 C00I 1.381(3) . ? N005 C00F 1.393(3) . ? N005 C00V 1.481(3) . ? N006 C00H 1.383(3) . ? N006 C00G 1.396(3) . ? N006 C00W 1.481(3) . ? C007 C009 1.404(3) . ? C007 C00B 1.406(3) . ? C007 C00E 1.423(3) . ? C008 C00A 1.399(3) . ? C008 C00C 1.413(3) . ? C008 C00D 1.424(3) . ? C009 C00R 1.373(3) . ? C009 C00F 1.472(3) . ? C00A C00S 1.376(3) . ? C00A C00G 1.476(3) . ? C00B C00K 1.368(3) . ? C00B C00I 1.478(3) . ? C00C C00J 1.369(3) . ? C00C C00H 1.475(3) . ? C00D C00N 1.409(4) . ? C00D C00O 1.411(4) . ? C00E C00M 1.404(4) . ? C00E C00L 1.408(4) . ? C00J C00U 1.402(4) . ? C00J H00J 0.9300 . ? C00K C00T 1.404(4) . ? C00K H00K 0.9300 . ? C00L C00Y 1.359(4) . ? C00L H00L 0.9300 . ? C00M C00T 1.358(4) . ? C00M H00M 0.9300 . ? C00N C00U 1.359(4) . ? C00N H00N 0.9300 . ? C00O C00X 1.358(4) . ? C00O H00O 0.9300 . ? C00P C00W 1.501(4) . ? C00P C010 1.535(4) . ? C00P H00A 0.9700 . ? C00P H00B 0.9700 . ? C00Q C00V 1.503(4) . ? C00Q C00Z 1.530(4) . ? C00Q H00C 0.9700 . ? C00Q H00D 0.9700 . ? C00R C00Y 1.406(4) . ? C00R H00R 0.9300 . ? C00S C00X 1.405(4) . ? C00S H00S 0.9300 . ? C00T H00T 0.9300 . ? C00U H00U 0.9300 . ? C00V H00E 0.9700 . ? C00V H00F 0.9700 . ? C00W H00G 0.9700 . ? C00W H00H 0.9700 . ? C00X H00X 0.9300 . ? C00Y H00Y 0.9300 . ? C00Z C012 1.459(4) . ? C00Z H00I 0.9700 . ? C00Z H00P 0.9700 . ? C010 C011 1.467(4) . ? C010 H01A 0.9700 . ? C010 H01B 0.9700 . ? C011 C014 1.513(4) . ? C011 H01C 0.9700 . ? C011 H01D 0.9700 . ? C012 C013 1.517(4) . ? C012 H01E 0.9700 . ? C012 H01F 0.9700 . ? C013 H01G 0.9600 . ? C013 H01H 0.9600 . ? C013 H01I 0.9600 . ? C014 H01J 0.9600 . ? C014 H01K 0.9600 . ? C014 H01L 0.9600 . ?