#------------------------------------------------------------------------------ #$Date: 2025-02-14 01:11:31 +0200 (Fri, 14 Feb 2025) $ #$Revision: 297730 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/57/39/1573924.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1573924 loop_ _publ_author_name 'Xu, Ziwei' 'Ying, Xin-Wen' 'Li, Yi' 'Dong, Xiaoyan' 'Liu, Jiyong' 'Wang, Shu-Ping' 'Little, Marc' 'Zhang, Dahao' 'Xie, Yongshu' 'Zhang, Zibin' 'Yu, Ling' 'Huang, Feihe' 'Li, Shijun' _publ_section_title ; Template-directed self-assembly of porphyrin nanorings through imine condensation reaction ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D4SC08569H _journal_year 2025 _chemical_formula_moiety 'C270 H210 N30 O18 Zn3' _chemical_formula_sum 'C270 H210 N30 O18 Zn3' _chemical_formula_weight 4358.78 _space_group_crystal_system hexagonal _space_group_IT_number 176 _space_group_name_Hall '-P 6c' _space_group_name_H-M_alt 'P 63/m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-11-14 _audit_creation_method ; Olex2 1.5 (compiled 2022.04.07 svn.rca3783a0 for OlexSys, GUI svn.r6498) ; _audit_update_record ; 2024-11-18 deposited with the CCDC. 2025-02-13 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 2 _cell_length_a 26.4305(13) _cell_length_b 26.4305(13) _cell_length_c 28.419(2) _cell_measurement_reflns_used 9481 _cell_measurement_temperature 170.00 _cell_measurement_theta_max 37.850 _cell_measurement_theta_min 2.705 _cell_volume 17192.9(17) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/2 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 170.00 _diffrn_detector CPAD _diffrn_detector_area_resol_mean 7.41 _diffrn_detector_type 'Bruker PHOTON III M28' _diffrn_measured_fraction_theta_full 0.986 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'ZJU Bruker D8 VENTURE Metaljet PHOTON III' _diffrn_measurement_method '\w and \f scans' _diffrn_measurement_specimen_support 'MiTeGen micromount' _diffrn_radiation_monochromator 'mirror optics' _diffrn_radiation_probe x-ray _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.1431 _diffrn_reflns_av_unetI/netI 0.1069 _diffrn_reflns_Laue_measured_fraction_full 0.986 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 69027 _diffrn_reflns_point_group_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 42.170 _diffrn_reflns_theta_max 42.170 _diffrn_reflns_theta_min 2.909 _diffrn_source 'liquid Metal X-ray source' _diffrn_source_current 3.57 _diffrn_source_power 0.24954300000000001 _diffrn_source_type 'Bruker Excillum Metaljet D2+' _diffrn_source_voltage 69.9 _exptl_absorpt_coefficient_mu 0.406 _exptl_absorpt_correction_T_max 0.7483 _exptl_absorpt_correction_T_min 0.4172 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1083 before and 0.0832 after correction. The Ratio of minimum to maximum transmission is 0.5575. The \l/2 correction factor is Not present. ; _exptl_crystal_colour red _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 0.842 _exptl_crystal_description block _exptl_crystal_F_000 4548 _exptl_crystal_size_max 0.06 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.04 _refine_diff_density_max 0.800 _refine_diff_density_min -0.427 _refine_diff_density_rms 0.090 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.202 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 475 _refine_ls_number_reflns 6096 _refine_ls_number_restraints 91 _refine_ls_restrained_S_all 1.213 _refine_ls_R_factor_all 0.2082 _refine_ls_R_factor_gt 0.1363 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.2000P)^2^+6.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.3491 _refine_ls_wR_factor_ref 0.4048 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2699 _reflns_number_total 6096 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL 241031_XZW3Por_Ben_a.res in P6(3)/m 241031_xzw3por_ben.res created by SHELXL-2019/2 at 17:16:33 on 14-Nov-2024 REM Old TITL 241031_XZW3Por_Ben in P6(3)/m REM SHELXT solution in P6(3)/m: R1 0.372, Rweak 0.023, Alpha 0.088 REM 0.547 for 13 systematic absences, Orientation as input REM Formula found by SHELXT: C245 N78 O45 Zn3 CELL 1.34139 26.4305 26.4305 28.4188 90 90 120 ZERR 2 0.0013 0.0013 0.0021 0 0 0 LATT 1 SYMM -Y,+X-Y,+Z SYMM +Y-X,-X,+Z SYMM -X,-Y,0.5+Z SYMM +Y,-X+Y,0.5+Z SYMM -Y+X,+X,0.5+Z SFAC C H N O Zn DISP C 0.0137 0.0067 57.1 DISP H -0 0 0.6481 DISP N 0.0241 0.0134 109.9 DISP O 0.0389 0.0241 193.4 DISP Zn -2.7473 0.5279 4188.7 UNIT 540 420 60 36 6 SIMU 0.02 0.04 2 C5 C11 C21 C23 C41 C43 C45 SIMU 0.02 0.04 2 N7 C9 C17 C19 C28 C35 C37 C39 DFIX 1.43 C18 C24 L.S. 20 PLAN 38 SIZE 0.04 0.05 0.06 TEMP -103.15 CONF BOND LIST 4 MORE -1 HTAB ABIN BOND $H fmap 2 acta OMIT 0 9 3 OMIT -1 6 4 OMIT -8 9 1 OMIT -6 7 7 OMIT -4 10 2 OMIT -1 3 7 OMIT -6 7 1 OMIT -2 4 0 OMIT -1 4 1 OMIT -3 12 3 OMIT 0 9 5 OMIT -4 11 5 OMIT -1 8 11 OMIT -4 8 8 OMIT -9 13 4 OMIT -1 4 6 OMIT 0 1 3 OMIT -3 14 6 OMIT -10 13 3 OMIT -1 13 8 OMIT 0 3 0 OMIT -2 7 3 OMIT -8 12 2 OMIT -2 3 8 OMIT -1 8 3 OMIT -2 11 3 OMIT -2 4 7 OMIT 0 1 1 OMIT -1 9 3 OMIT -6 11 3 OMIT 0 0 2 OMIT 0 3 1 OMIT -5 7 3 OMIT -5 6 0 OMIT 0 3 5 OMIT -4 11 3 OMIT -5 10 11 OMIT -1 3 2 OMIT -3 5 13 OMIT 0 9 8 OMIT -5 13 4 OMIT -4 5 3 OMIT -3 6 4 OMIT -3 4 4 OMIT -8 9 4 OMIT 0 1 5 OMIT -2 3 13 OMIT -7 11 4 OMIT -2 3 7 OMIT -4 5 0 OMIT -1 5 8 OMIT -1 3 0 OMIT -5 15 5 OMIT -5 9 5 OMIT -5 12 0 OMIT -1 11 9 OMIT 0 8 1 OMIT -6 16 2 OMIT -1 5 16 OMIT -3 6 0 OMIT -6 13 7 OMIT -6 8 4 OMIT -2 5 3 OMIT -1 2 8 OMIT -3 7 0 OMIT -4 5 6 OMIT -5 6 3 OMIT -4 5 4 OMIT -4 10 7 OMIT -4 14 5 OMIT -1 2 1 OMIT -2 13 2 OMIT -4 14 9 OMIT -4 12 2 OMIT -12 14 6 OMIT -6 9 5 OMIT -5 12 6 REM REM REM WGHT 0.200000 6.000000 FVAR 0.21204 ZN1 5 0.383005 0.348443 0.750000 10.50000 0.11547 0.11689 = 0.06835 0.00000 0.00000 0.05364 O1 4 0.562492 0.764535 0.503601 11.00000 0.35463 0.13865 = 0.35453 -0.04336 -0.12312 0.09124 O2 4 0.209886 0.129894 0.445280 11.00000 0.17754 0.14650 = 0.13607 0.00565 -0.01123 0.05871 O3 4 0.299425 -0.018492 0.515115 11.00000 0.25792 0.22642 = 0.10186 -0.02091 -0.02725 0.18190 N1 3 0.324426 0.261745 0.750000 10.50000 0.10633 0.15470 = 0.07628 0.00000 0.00000 0.07338 N2 3 0.374848 0.350174 0.677570 11.00000 0.10159 0.09043 = 0.07320 -0.01306 -0.00175 0.02962 N3 3 0.421492 0.441937 0.750000 10.50000 0.11560 0.12331 = 0.07666 0.00000 0.00000 0.06403 N4 3 0.463168 0.345183 0.750000 10.50000 0.14008 0.13388 = 0.06021 0.00000 0.00000 0.06036 N5 3 0.670224 0.388119 0.750000 10.50000 0.08628 0.12701 = 0.10848 0.00000 0.00000 0.03194 N6 3 0.563528 0.678468 0.520630 11.00000 0.13555 0.14920 = 0.10029 0.00795 0.00200 0.06740 N7 3 0.226745 0.064277 0.482087 11.00000 0.16169 0.14151 = 0.09257 -0.01202 -0.00293 0.07249 C1 1 0.305838 0.224435 0.712053 11.00000 0.11097 0.11706 = 0.07212 -0.01335 -0.00910 0.05307 C2 1 0.290974 -0.100849 0.557523 11.00000 0.19738 0.21920 = 0.09561 0.01211 0.00249 0.14719 AFIX 23 H2A 2 0.261180 -0.137632 0.572469 11.00000 -1.20000 H2B 2 0.319541 -0.076863 0.582074 11.00000 -1.20000 AFIX 0 C3 1 0.194073 0.118586 0.595227 11.00000 0.12779 0.13378 = 0.08921 -0.00997 0.00306 0.05139 AFIX 43 H3 2 0.152586 0.096824 0.595117 11.00000 -1.20000 AFIX 0 C4 1 0.569899 0.339496 0.750000 10.50000 0.09990 0.10606 = 0.09040 0.00000 0.00000 0.04778 C5 1 0.546728 0.714632 0.495787 11.00000 0.22814 0.28498 = 0.12927 -0.02935 -0.03335 0.19934 C6 1 0.618030 0.334968 0.750000 10.50000 0.11307 0.18935 = 0.06888 0.00000 0.00000 0.11379 C7 1 0.453305 0.544232 0.620232 11.00000 0.18026 0.15394 = 0.11265 0.01044 0.02826 0.09524 AFIX 43 H7 2 0.425710 0.546665 0.640122 11.00000 -1.20000 AFIX 0 C8 1 0.435197 0.456078 0.665997 11.00000 0.12048 0.09245 = 0.09079 0.01842 -0.00065 0.03239 C10 1 0.400184 0.398240 0.649719 11.00000 0.12552 0.11705 = 0.06805 0.03297 0.00663 0.06190 C12 1 0.444679 0.473966 0.712387 11.00000 0.12303 0.09804 = 0.09630 -0.01027 -0.01707 0.05391 C13 1 0.482145 0.587596 0.583667 11.00000 0.14758 0.15082 = 0.11632 0.04142 0.03420 0.07417 AFIX 43 H13 2 0.476821 0.620468 0.581030 11.00000 -1.20000 AFIX 0 C14 1 0.227158 0.110178 0.559032 11.00000 0.13615 0.09874 = 0.09277 -0.00509 -0.01227 0.03266 C15 1 0.262445 -0.069358 0.539820 11.00000 0.22898 0.14889 = 0.15692 0.02702 0.02844 0.09058 AFIX 23 H15A 2 0.229831 -0.095716 0.518937 11.00000 -1.20000 H15B 2 0.245537 -0.059124 0.566765 11.00000 -1.20000 AFIX 0 C16 1 0.223626 0.158563 0.629777 11.00000 0.08519 0.12396 = 0.10165 -0.01107 -0.00248 0.03342 AFIX 43 H16 2 0.202457 0.160834 0.655926 11.00000 -1.20000 AFIX 66 C17 1 0.265551 0.102378 0.403915 11.00000 0.22642 0.16008 = 0.09560 0.00643 0.01508 0.07864 C35 1 0.324395 0.119019 0.406087 11.00000 0.22537 0.16714 = 0.12757 0.02873 0.03196 0.11209 AFIX 43 H35 2 0.344590 0.130634 0.435257 11.00000 -1.20000 AFIX 65 C9 1 0.353689 0.118665 0.365579 11.00000 0.24781 0.19932 = 0.15463 0.02293 0.05579 0.08428 AFIX 43 H9 2 0.393907 0.130038 0.367063 11.00000 -1.20000 AFIX 65 C37 1 0.324140 0.101670 0.322898 11.00000 0.28786 0.22801 = 0.15211 0.01128 0.06670 0.09127 AFIX 43 H37 2 0.344162 0.101428 0.295213 11.00000 -1.20000 AFIX 65 C19 1 0.265297 0.085029 0.320726 11.00000 0.31041 0.26480 = 0.15373 0.01397 0.05629 0.07313 AFIX 43 H19 2 0.245101 0.073414 0.291556 11.00000 -1.20000 AFIX 65 C39 1 0.236001 0.085383 0.361234 11.00000 0.28356 0.23887 = 0.09592 0.00157 0.02275 0.04104 AFIX 43 H39 2 0.195784 0.074010 0.359749 11.00000 -1.20000 AFIX 0 C18 1 0.314074 0.244063 0.664558 11.00000 0.11315 0.10401 = 0.07467 -0.00787 -0.00696 0.03607 C20 1 0.344069 0.301675 0.650279 11.00000 0.08314 0.12128 = 0.07632 0.00966 -0.00079 0.03969 C22 1 0.511424 0.289758 0.750000 10.50000 0.09194 0.15688 = 0.15098 0.00000 0.00000 0.09702 AFIX 43 H22 2 0.506742 0.251703 0.750000 10.50000 -1.20000 AFIX 0 C24 1 0.282075 0.195020 0.627941 11.00000 0.16070 0.14449 = 0.07202 -0.00109 -0.00073 0.08297 C25 1 0.503319 0.492043 0.593642 11.00000 0.13087 0.14795 = 0.10754 -0.01228 0.02209 0.07963 AFIX 43 H25 2 0.510895 0.460581 0.595982 11.00000 -1.20000 AFIX 0 C26 1 0.465318 0.499091 0.626725 11.00000 0.13528 0.10378 = 0.14510 -0.00961 -0.04410 0.06005 C27 1 0.190712 0.062827 0.522353 11.00000 0.15204 0.14912 = 0.09547 -0.02074 0.00672 0.06460 AFIX 23 H27A 2 0.172812 0.023905 0.537473 11.00000 -1.20000 H27B 2 0.158770 0.068859 0.510823 11.00000 -1.20000 AFIX 0 C28 1 0.231813 0.098184 0.444417 11.00000 0.18776 0.12297 = 0.10263 -0.01357 -0.02566 0.05960 C29 1 0.518641 0.397644 0.750000 10.50000 0.10570 0.10805 = 0.13966 0.00000 0.00000 0.02192 AFIX 43 H29 2 0.521551 0.434954 0.750000 10.50000 -1.20000 AFIX 0 C30 1 0.278303 0.163628 0.726096 11.00000 0.12259 0.09507 = 0.07925 -0.00258 -0.01141 0.03310 AFIX 43 H30 2 0.263317 0.130534 0.705974 11.00000 -1.20000 AFIX 0 C31 1 0.238373 0.017926 0.478802 11.00000 0.13220 0.15696 = 0.13613 -0.02551 -0.02549 0.08547 AFIX 23 H31A 2 0.249770 0.014889 0.446194 11.00000 -1.20000 H31B 2 0.202897 -0.019352 0.486978 11.00000 -1.20000 AFIX 0 C32 1 0.286174 0.148757 0.557653 11.00000 0.12675 0.13352 = 0.09356 0.00670 -0.00242 0.05705 AFIX 43 H32 2 0.307318 0.146687 0.531401 11.00000 -1.20000 AFIX 0 C33 1 0.290834 0.030052 0.514683 11.00000 0.17273 0.19581 = 0.11781 -0.04524 -0.03789 0.11962 AFIX 43 H33 2 0.312542 0.064624 0.532716 11.00000 -1.20000 AFIX 0 C34 1 0.350592 0.321223 0.601185 11.00000 0.12245 0.14496 = 0.07189 0.00679 -0.01211 0.04601 AFIX 43 H34 2 0.334430 0.297502 0.574048 11.00000 -1.20000 AFIX 0 C36 1 0.486354 0.531650 0.725479 11.00000 0.16436 0.12453 = 0.13031 0.01644 -0.02723 0.05753 AFIX 43 H36 2 0.509436 0.563598 0.705190 11.00000 -1.20000 AFIX 0 C38 1 0.466620 0.294521 0.750000 10.50000 0.16998 0.09650 = 0.13619 0.00000 0.00000 0.07601 AFIX 43 H38 2 0.430367 0.258895 0.750000 10.50000 -1.20000 AFIX 0 C40 1 0.527815 0.533737 0.558571 11.00000 0.12706 0.13793 = 0.09252 0.01810 0.00573 0.04515 AFIX 43 H40 2 0.553460 0.530180 0.537152 11.00000 -1.20000 AFIX 66 C41 1 0.506402 0.685575 0.456731 11.00000 0.22685 0.32549 = 0.17134 -0.04560 -0.04909 0.17928 C21 1 0.519964 0.671446 0.413202 11.00000 0.25880 0.32536 = 0.18212 -0.02714 -0.04103 0.15362 AFIX 43 H21 2 0.555892 0.672018 0.408909 11.00000 -1.20000 AFIX 65 C43 1 0.480958 0.656481 0.375953 11.00000 0.27789 0.31716 = 0.15468 0.02024 -0.04017 0.14974 AFIX 43 H43 2 0.490227 0.646824 0.346203 11.00000 -1.20000 AFIX 65 C11 1 0.428390 0.655645 0.382233 11.00000 0.29646 0.36620 = 0.15746 0.00279 -0.00446 0.16214 AFIX 43 H11 2 0.401731 0.645417 0.356775 11.00000 -1.20000 AFIX 65 C45 1 0.414827 0.669774 0.425763 11.00000 0.30975 0.38664 = 0.18499 -0.00386 -0.02440 0.16880 AFIX 43 H45 2 0.378899 0.669202 0.430055 11.00000 -1.20000 AFIX 65 C23 1 0.453833 0.684739 0.463012 11.00000 0.27827 0.37539 = 0.19304 -0.06957 -0.01385 0.13190 AFIX 43 H23 2 0.444563 0.694395 0.492762 11.00000 -1.20000 AFIX 0 C42 1 0.569430 0.391924 0.750000 10.50000 0.09822 0.16634 = 0.11154 0.00000 0.00000 0.06646 AFIX 43 H42 2 0.606217 0.426960 0.750000 10.50000 -1.20000 AFIX 0 C44 1 0.317147 0.190381 0.591578 11.00000 0.15816 0.11209 = 0.07516 -0.01955 -0.01793 0.06055 AFIX 43 H44 2 0.358492 0.214095 0.590864 11.00000 -1.20000 AFIX 0 C46 1 0.518507 0.579027 0.552088 11.00000 0.12722 0.10237 = 0.10914 0.01536 0.01447 0.03974 C47 1 0.545508 0.618771 0.511128 11.00000 0.16892 0.11805 = 0.11458 0.01683 0.02110 0.06158 AFIX 23 H47A 2 0.579901 0.616268 0.500615 11.00000 -1.20000 H47B 2 0.517037 0.605002 0.484908 11.00000 -1.20000 AFIX 0 C48 1 0.383503 0.378470 0.602610 11.00000 0.14723 0.12511 = 0.07810 0.02444 0.02000 0.06684 AFIX 43 H48 2 0.394638 0.403273 0.575833 11.00000 -1.20000 AFIX 0 HKLF 4 REM 241031_XZW3Por_Ben_a.res in P6(3)/m REM wR2 = 0.4048, GooF = S = 1.202, Restrained GooF = 1.213 for all data REM R1 = 0.1363 for 2699 Fo > 4sig(Fo) and 0.2082 for all 6096 data REM 475 parameters refined using 91 restraints END WGHT 0.2000 0.0000 REM Instructions for potential hydrogen bonds EQIV $4 y, -x+y, -z+1 HTAB C27 O2_$4 HTAB C31 O2_$4 EQIV $5 x-y, x, -z+1 HTAB C34 O3_$5 EQIV $3 -x+y+1, -x+1, z HTAB C47 O3_$3 REM Highest difference peak 0.800, deepest hole -0.427, 1-sigma level 0.090 Q1 1 0.0273 0.0690 0.5766 11.00000 0.05 0.50 Q2 1 0.4614 0.6327 0.4744 11.00000 0.05 0.42 Q3 1 0.6791 0.4432 0.7500 10.50000 0.05 0.37 Q4 1 0.4093 0.6884 0.3667 11.00000 0.05 0.36 Q5 1 0.3993 0.2332 0.7500 10.50000 0.05 0.36 Q6 1 0.3999 0.6110 0.3706 11.00000 0.05 0.34 Q7 1 0.5569 0.7962 0.4689 11.00000 0.05 0.32 Q8 1 0.5492 0.7813 0.4613 11.00000 0.05 0.31 Q9 1 0.2186 0.2025 0.7500 10.50000 0.05 0.30 Q10 1 0.3548 0.6614 0.4810 11.00000 0.05 0.28 Q11 1 0.4085 0.5924 0.4307 11.00000 0.05 0.28 Q12 1 0.5515 0.3110 0.7500 10.50000 0.05 0.27 Q13 1 0.1926 0.1484 0.5540 11.00000 0.05 0.25 Q14 1 0.3701 0.6276 0.5700 11.00000 0.05 0.25 Q15 1 0.1684 0.1577 0.6610 11.00000 0.05 0.25 Q16 1 0.1616 0.0907 0.4212 11.00000 0.05 0.25 Q17 1 0.3824 0.5549 0.4632 11.00000 0.05 0.25 Q18 1 0.3483 0.1676 0.3327 11.00000 0.05 0.25 Q19 1 0.4909 0.3741 0.7500 10.50000 0.05 0.24 Q20 1 0.2588 0.0191 0.4860 11.00000 0.05 0.24 Q21 1 0.3333 0.6667 0.6493 10.33333 0.05 0.24 Q22 1 0.2132 0.0148 0.3070 11.00000 0.05 0.23 Q23 1 0.1546 0.0022 0.2500 10.50000 0.05 0.23 Q24 1 0.2148 0.0663 0.5110 11.00000 0.05 0.23 Q25 1 0.5232 0.5246 0.5906 11.00000 0.05 0.22 Q26 1 0.3333 0.6667 0.5488 10.33333 0.05 0.22 Q27 1 0.3333 0.6667 0.7078 10.33333 0.05 0.22 Q28 1 0.3546 0.6096 0.4902 11.00000 0.05 0.22 Q29 1 0.3359 0.3548 0.5866 11.00000 0.05 0.22 Q30 1 0.0000 0.0000 0.6113 10.33333 0.05 0.22 Q31 1 0.6827 0.4132 0.6785 11.00000 0.05 0.21 Q32 1 0.2286 0.0113 0.3169 11.00000 0.05 0.21 Q33 1 0.3770 0.6306 0.5326 11.00000 0.05 0.21 Q34 1 0.3077 0.5973 0.6877 11.00000 0.05 0.21 Q35 1 0.3374 0.3320 0.5871 11.00000 0.05 0.21 Q36 1 0.3333 0.6667 0.6156 10.33333 0.05 0.20 Q37 1 0.3794 0.6794 0.6719 11.00000 0.05 0.20 Q38 1 0.5036 0.6868 0.4123 11.00000 0.05 0.20 REM The information below was added by Olex2. REM REM R1 = 0.1363 for 2699 Fo > 4sig(Fo) and 0.2082 for all 70516 data REM 475 parameters refined using n/a restraints REM Highest difference peak 0.80, deepest hole -0.43 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.2082 REM R1_gt = 0.1363 REM wR_ref = 0.4048 REM GOOF = 1.202 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 70516 REM Reflections_gt = 2699 REM Parameters = 475 REM Hole = -0.43 REM Peak = 0.80 REM Flack = n/a ; _cod_data_source_file d4sc08569h2.cif _cod_data_source_block 241031_xzw3por_ben _cod_original_cell_volume 17193(2) _cod_database_code 1573924 _shelx_shelxl_version_number 2019/2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.984 _shelx_estimated_absorpt_t_min 0.976 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2. Restrained distances C18-C24 1.43 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints C5 \\sim C11 \\sim C21 \\sim C23 \\sim C41 \\sim C43 \\sim C45: within 2A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 2A N7 \\sim C9 \\sim C17 \\sim C19 \\sim C28 \\sim C35 \\sim C37 \\sim C39: within 2A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 2A 4.a Secondary CH2 refined with riding coordinates: C2(H2A,H2B), C15(H15A,H15B), C27(H27A,H27B), C31(H31A,H31B), C47(H47A,H47B) 4.b Aromatic/amide H refined with riding coordinates: C3(H3), C7(H7), C13(H13), C16(H16), C35(H35), C9(H9), C37(H37), C19(H19), C39(H39), C22(H22), C25(H25), C29(H29), C30(H30), C32(H32), C33(H33), C34(H34), C36(H36), C38(H38), C40(H40), C21(H21), C43(H43), C11(H11), C45(H45), C23(H23), C42(H42), C44(H44), C48(H48) 4.c Fitted hexagon refined as free rotating group: C17(C35,C9,C37,C19,C39), C41(C21,C43,C11,C45,C23) ; _smtbx_masks_special_details ; A solvent mask was calculated and 2507 electrons were found in a volume of 8156\%A^3^ in 1 void per unit cell. This is consistent with the presence of 21[CHCl3] per Asymmetric Unit which account for 2436 electrons per unit cell. ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_fab_file ; 0 0 2 -378.7928 -0.8448 0 0 4 147.3840 0.1139 0 0 6 88.3326 0.1948 0 0 8 -252.8138 0.0385 0 0 10 3.1829 -0.0593 0 0 12 44.8530 -0.0034 0 0 14 47.3482 0.0215 0 0 16 2.4585 0.0156 0 0 18 -24.2875 -0.0039 0 0 20 -8.8126 -0.0074 0 0 22 0.2245 -0.0038 0 0 24 -14.1035 0.0019 0 0 26 -10.0374 -0.0150 0 0 28 13.0217 -0.1325 0 1 1 -173.0161 0.0547 0 1 2 -92.4060 -0.0912 0 1 3 68.9014 0.2494 0 1 4 -18.9309 -0.0255 0 1 5 -102.7224 -0.0115 0 1 6 -116.5724 -0.0467 0 1 7 44.2866 -0.1064 0 1 8 -72.0986 0.0444 0 1 9 30.1860 -0.0711 0 1 10 27.3336 0.0501 0 1 11 -24.4787 0.0207 0 1 12 46.2545 0.0005 0 1 13 -13.1664 0.0555 0 1 14 45.9968 -0.0284 0 1 15 4.1542 -0.0014 0 1 16 -9.4372 -0.0208 0 1 17 -0.0148 -0.0356 0 1 18 -12.8644 -0.0005 0 1 19 -0.3156 -0.0036 0 1 20 -5.0526 0.0237 0 1 21 5.7849 0.0181 0 1 22 0.0096 -0.0004 0 1 23 4.3883 0.0123 0 1 24 3.8481 -0.0143 0 1 25 0.9686 -0.0249 0 1 26 0.0221 0.0052 0 1 27 0.1427 -0.0346 0 1 28 3.2618 0.0168 0 2 0 -6.6501 -0.4592 0 2 1 69.8682 0.3594 0 2 2 56.2204 -0.0136 0 2 3 61.1301 0.1074 0 2 4 10.2181 0.0872 0 2 5 -40.4386 0.0288 0 2 6 -84.1887 0.0024 0 2 7 -21.5008 -0.0614 0 2 8 -58.8172 0.0180 0 2 9 -13.4451 -0.0649 0 2 10 45.2244 -0.0115 0 2 11 10.9541 -0.0136 0 2 12 14.2794 -0.0313 0 2 13 -27.8536 0.0245 0 2 14 25.9461 -0.0122 0 2 15 -0.5437 0.0038 0 2 16 -0.7170 0.0030 0 2 17 7.7477 -0.0076 0 2 18 -15.1663 0.0159 0 2 19 -8.5590 -0.0078 0 2 20 -11.0950 0.0037 0 2 21 7.8795 0.0059 0 2 22 -4.3086 -0.0032 0 2 23 2.0148 0.0204 0 2 24 10.7657 -0.0076 0 2 25 -3.8801 -0.0069 0 2 26 -1.6124 0.0016 0 2 27 3.8108 -0.0249 0 2 28 -3.1325 -0.0286 0 3 0 -46.9612 -0.6268 0 3 1 65.7088 0.0169 0 3 2 -5.1019 0.0609 0 3 3 -31.8822 -0.0065 0 3 4 -85.6513 0.0833 0 3 5 1.7970 0.0342 0 3 6 -43.1144 -0.0187 0 3 7 8.5461 -0.0251 0 3 8 -61.0959 -0.0455 0 3 9 6.3902 -0.0097 0 3 10 1.2151 0.0086 0 3 11 4.1220 0.0078 0 3 12 27.1660 0.0053 0 3 13 -7.4462 0.0033 0 3 14 11.3216 -0.0004 0 3 15 -5.7905 0.0070 0 3 16 -2.6335 -0.0170 0 3 17 3.5378 -0.0024 0 3 18 -3.9548 0.0097 0 3 19 3.9486 -0.0042 0 3 20 -3.1486 0.0151 0 3 21 -3.6864 -0.0045 0 3 22 2.3627 -0.0030 0 3 23 1.5219 0.0088 0 3 24 -2.0941 0.0000 0 3 25 0.5625 0.0012 0 3 26 5.4157 -0.0193 0 3 27 -2.2388 0.0064 0 3 28 -2.0416 -0.1694 0 4 0 96.4518 0.2821 0 4 1 73.4052 0.4633 0 4 2 -52.6768 -0.2419 0 4 3 -66.8805 0.1294 0 4 4 -39.8721 -0.2330 0 4 5 -65.0275 -0.0665 0 4 6 -21.1696 -0.0090 0 4 7 -8.2030 -0.1022 0 4 8 -53.8692 0.0544 0 4 9 -46.8335 -0.0491 0 4 10 -25.7482 0.0487 0 4 11 -13.3558 0.0210 0 4 12 31.6536 -0.0048 0 4 13 -21.3934 0.0278 0 4 14 34.6316 -0.0279 0 4 15 -13.1292 -0.0072 0 4 16 -3.3204 -0.0021 0 4 17 -0.2580 -0.0104 0 4 18 -8.7236 0.0099 0 4 19 -4.3119 0.0008 0 4 20 5.0142 -0.0082 0 4 21 1.0340 0.0057 0 4 22 -2.7151 -0.0122 0 4 23 -3.8908 -0.0123 0 4 24 -13.9811 -0.0092 0 4 25 -0.0600 0.0004 0 4 26 7.4522 0.0243 0 4 27 -0.6606 0.0546 0 4 28 1.8630 0.1386 0 5 0 -127.9225 -0.2961 0 5 1 -79.3086 0.1463 0 5 2 -7.5750 -0.0772 0 5 3 -73.5828 0.0552 0 5 4 25.0589 0.0098 0 5 5 39.9468 0.0593 0 5 6 -9.1743 0.0485 0 5 7 -15.9480 0.0019 0 5 8 18.6441 0.0314 0 5 9 89.0900 -0.0421 0 5 10 -27.9574 0.0088 0 5 11 58.9827 -0.0167 0 5 12 2.3155 -0.0153 0 5 13 -25.4550 0.0104 0 5 14 18.4496 -0.0315 0 5 15 8.0301 0.0225 0 5 16 -14.4884 -0.0068 0 5 17 -3.8093 0.0164 0 5 18 -3.4647 0.0165 0 5 19 -5.5721 -0.0112 0 5 20 14.5408 0.0172 0 5 21 3.9093 -0.0142 0 5 22 0.4993 -0.0145 0 5 23 1.1313 -0.0038 0 5 24 -1.1577 -0.0083 0 5 25 -2.0814 0.0010 0 5 26 -2.9435 -0.0470 0 5 27 -6.3534 0.0396 0 6 0 81.4734 -0.1919 0 6 1 13.9372 0.0774 0 6 2 -1.9656 0.0716 0 6 3 -26.4661 -0.0140 0 6 4 60.1019 0.0234 0 6 5 -37.0468 -0.0223 0 6 6 7.7615 -0.0259 0 6 7 15.9981 -0.0062 0 6 8 18.1269 -0.0071 0 6 9 44.2455 -0.0108 0 6 10 -14.6430 0.0134 0 6 11 16.7434 -0.0129 0 6 12 -29.2353 0.0201 0 6 13 -21.5235 0.0005 0 6 14 -7.0531 -0.0114 0 6 15 -3.0361 -0.0002 0 6 16 -0.3984 -0.0150 0 6 17 -2.9768 -0.0056 0 6 18 3.6473 -0.0093 0 6 19 -5.0657 -0.0165 0 6 20 3.4192 0.0208 0 6 21 3.5449 -0.0081 0 6 22 -6.7330 0.0076 0 6 23 3.0497 -0.0120 0 6 24 2.1208 -0.0010 0 6 25 -9.1367 -0.0085 0 6 26 -7.8242 -0.0342 0 6 27 -1.8865 0.0312 0 7 0 17.8261 0.3518 0 7 1 -50.4848 0.4709 0 7 2 7.5674 -0.1259 0 7 3 -40.9189 0.0611 0 7 4 49.8702 -0.0716 0 7 5 -0.0289 -0.0660 0 7 6 -8.6680 -0.0139 0 7 7 23.4424 -0.0370 0 7 8 24.6061 0.0314 0 7 9 56.1532 0.0100 0 7 10 -7.8894 -0.0096 0 7 11 34.0515 0.0131 0 7 12 -4.2603 -0.0182 0 7 13 10.3995 0.0070 0 7 14 -7.1231 -0.0316 0 7 15 -9.5859 -0.0027 0 7 16 2.5506 -0.0069 0 7 17 -17.0774 0.0177 0 7 18 -3.3886 0.0239 0 7 19 -5.1578 0.0037 0 7 20 -2.1376 -0.0018 0 7 21 10.2861 -0.0233 0 7 22 1.5352 0.0008 0 7 23 1.6948 -0.0089 0 7 24 -2.3741 0.0263 0 7 25 0.9540 -0.0192 0 7 26 3.7010 0.0122 0 7 27 3.1914 0.0914 0 8 0 -16.9247 -0.1964 0 8 1 -32.8394 -0.1107 0 8 2 -61.4396 0.0701 0 8 3 -50.4583 0.0275 0 8 4 -17.1293 -0.0080 0 8 5 -33.6088 0.0267 0 8 6 29.3709 -0.0495 0 8 7 31.8802 0.0213 0 8 8 34.7138 -0.0035 0 8 9 66.2337 -0.0255 0 8 10 -16.5482 0.0211 0 8 11 37.6601 -0.0564 0 8 12 -17.9741 0.0035 0 8 13 8.6542 -0.0137 0 8 14 -14.2940 -0.0139 0 8 15 -16.7048 0.0287 0 8 16 -1.4851 -0.0117 0 8 17 6.3844 -0.0038 0 8 18 2.3629 0.0123 0 8 19 -7.3679 -0.0016 0 8 20 9.8071 0.0222 0 8 21 3.0703 -0.0186 0 8 22 4.1573 0.0179 0 8 23 6.8357 -0.0036 0 8 24 -3.4767 -0.0149 0 8 25 -2.5550 0.0304 0 8 26 -0.1702 0.0416 0 9 0 -41.1704 0.0104 0 9 1 -12.7904 0.2320 0 9 2 -9.0093 -0.1040 0 9 3 -3.2187 0.0548 0 9 4 75.8120 -0.0630 0 9 5 -55.0102 -0.0598 0 9 6 48.4925 -0.0144 0 9 7 24.0835 -0.0529 0 9 8 34.0917 0.0283 0 9 9 30.5985 0.0110 0 9 10 -4.1787 0.0320 0 9 11 3.2125 0.0168 0 9 12 -11.8482 0.0029 0 9 13 -8.9062 0.0154 0 9 14 -7.1266 -0.0052 0 9 15 -12.2178 0.0102 0 9 16 -4.5255 -0.0112 0 9 17 -10.1371 -0.0000 0 9 18 -0.8315 -0.0024 0 9 19 -4.3966 -0.0025 0 9 20 5.0365 0.0156 0 9 21 3.1691 -0.0292 0 9 22 -2.6981 0.0227 0 9 23 -1.3329 0.0010 0 9 24 -5.5164 -0.0065 0 9 25 4.7628 -0.0046 0 9 26 3.7565 -0.0150 0 10 0 -13.9032 0.2007 0 10 1 -20.0948 0.2377 0 10 2 -33.5681 -0.0479 0 10 3 -55.9896 0.0597 0 10 4 -40.8808 -0.0379 0 10 5 -60.1144 -0.0073 0 10 6 9.9089 -0.0042 0 10 7 -10.4595 -0.0216 0 10 8 -2.9393 0.0474 0 10 9 22.2926 0.0100 0 10 10 0.9434 0.0090 0 10 11 11.8175 0.0215 0 10 12 -1.1486 -0.0300 0 10 13 -4.7040 -0.0177 0 10 14 -3.1769 -0.0143 0 10 15 -7.9771 0.0052 0 10 16 0.2219 -0.0079 0 10 17 -15.4678 0.0169 0 10 18 3.4085 -0.0070 0 10 19 -1.1386 0.0052 0 10 20 2.4839 0.0109 0 10 21 2.8401 0.0048 0 10 22 1.8410 0.0175 0 10 23 0.7211 -0.0123 0 10 24 1.4041 0.0300 0 10 25 1.0245 -0.0554 0 11 0 -18.9128 0.0138 0 11 1 -16.6080 -0.1763 0 11 2 1.1068 -0.0407 0 11 3 -29.6396 -0.0112 0 11 4 11.1701 -0.0167 0 11 5 -24.5033 0.0392 0 11 6 18.5167 -0.0034 0 11 7 15.2076 -0.0117 0 11 8 21.4089 -0.0007 0 11 9 26.5829 -0.0297 0 11 10 -0.2514 -0.0067 0 11 11 -0.3254 -0.0078 0 11 12 1.3877 -0.0080 0 11 13 -7.0004 -0.0133 0 11 14 -11.3554 -0.0093 0 11 15 -6.1912 0.0127 0 11 16 -4.8057 -0.0029 0 11 17 -9.7940 0.0078 0 11 18 -5.1587 -0.0112 0 11 19 3.6011 -0.0140 0 11 20 6.8109 -0.0066 0 11 21 -5.0598 -0.0142 0 11 22 4.9799 0.0308 0 11 23 3.0629 0.0097 0 11 24 5.5471 0.0274 0 12 0 -14.6370 0.2401 0 12 1 0.2597 0.2686 0 12 2 -7.4857 -0.0595 0 12 3 -17.1143 0.0385 0 12 4 -14.5275 -0.0454 0 12 5 -16.7026 -0.0238 0 12 6 12.4247 -0.0122 0 12 7 -1.3662 -0.0318 0 12 8 8.0184 0.0084 0 12 9 11.0627 -0.0040 0 12 10 -1.3802 -0.0021 0 12 11 3.4555 0.0291 0 12 12 -5.9514 -0.0137 0 12 13 1.2123 0.0003 0 12 14 -8.2221 -0.0031 0 12 15 -3.8605 -0.0039 0 12 16 4.7143 -0.0030 0 12 17 -5.0220 -0.0021 0 12 18 3.6284 0.0020 0 12 19 -4.4499 0.0151 0 12 20 2.0400 -0.0114 0 12 21 0.0406 0.0236 0 12 22 5.1855 -0.0247 0 12 23 0.8317 -0.0162 0 12 24 -2.6856 0.0304 0 13 0 0.5590 0.0521 0 13 1 -1.4470 0.0195 0 13 2 -15.5145 -0.0610 0 13 3 -14.8816 0.0186 0 13 4 1.5501 -0.0164 0 13 5 -4.3851 -0.0086 0 13 6 14.9638 0.0086 0 13 7 -10.6339 -0.0023 0 13 8 -0.4795 0.0088 0 13 9 -8.2211 -0.0202 0 13 10 7.7191 0.0158 0 13 11 6.9582 -0.0214 0 13 12 -4.3465 0.0032 0 13 13 0.0751 0.0019 0 13 14 -9.0569 -0.0083 0 13 15 -2.5015 0.0174 0 13 16 -0.0517 -0.0072 0 13 17 2.5697 0.0097 0 13 18 2.8609 -0.0040 0 13 19 -2.1506 0.0092 0 13 20 4.2678 -0.0019 0 13 21 -1.5643 -0.0001 0 13 22 -5.9767 0.0170 0 13 23 -3.8997 -0.0442 0 14 0 -21.7178 0.1213 0 14 1 4.1967 -0.1201 0 14 2 -1.9227 -0.0351 0 14 3 1.8044 0.0077 0 14 4 -6.4489 -0.0385 0 14 5 4.4147 0.0477 0 14 6 4.0049 0.0209 0 14 7 17.0311 0.0248 0 14 8 7.2166 0.0156 0 14 9 -2.8792 -0.0223 0 14 10 -9.5567 0.0117 0 14 11 6.7002 -0.0090 0 14 12 -3.5266 -0.0101 0 14 13 13.2365 0.0200 0 14 14 -0.7596 -0.0144 0 14 15 4.8590 0.0092 0 14 16 -0.8733 -0.0105 0 14 17 3.3743 0.0007 0 14 18 0.5610 -0.0005 0 14 19 -2.2513 0.0057 0 14 20 -0.7715 -0.0076 0 14 21 -4.2415 -0.0192 0 14 22 5.4851 -0.0966 0 15 0 1.2808 0.1102 0 15 1 0.1607 0.1474 0 15 2 -0.8489 -0.0051 0 15 3 5.5237 0.0545 0 15 4 0.9129 -0.0311 0 15 5 -5.2238 -0.0245 0 15 6 2.3846 -0.0278 0 15 7 -9.6331 -0.0289 0 15 8 2.9898 0.0007 0 15 9 -0.0717 -0.0202 0 15 10 -6.7128 0.0140 0 15 11 2.1890 -0.0100 0 15 12 7.9936 -0.0010 0 15 13 -9.1420 0.0122 0 15 14 -5.5484 -0.0179 0 15 15 7.8354 0.0106 0 15 16 -8.7227 -0.0276 0 15 17 7.1794 0.0172 0 15 18 1.6855 -0.0118 0 15 19 -5.4259 0.0332 0 15 20 -2.0834 0.0111 0 15 21 7.8659 -0.0486 0 16 0 -0.5010 0.0923 0 16 1 0.2965 -0.1153 0 16 2 -3.6155 -0.0507 0 16 3 8.2281 -0.0055 0 16 4 -5.0429 -0.0329 0 16 5 10.5390 0.0266 0 16 6 13.0537 0.0241 0 16 7 -3.4330 0.0061 0 16 8 -6.4433 0.0228 0 16 9 -9.5794 -0.0119 0 16 10 6.2278 0.0088 0 16 11 -8.1883 -0.0219 0 16 12 -2.9330 0.0014 0 16 13 15.0083 0.0215 0 16 14 -0.1641 -0.0114 0 16 15 1.9143 0.0043 0 16 16 -1.7845 -0.0330 0 16 17 4.0216 -0.0020 0 16 18 -5.6057 -0.0076 0 16 19 1.0782 0.0159 0 16 20 9.9033 0.0541 0 17 0 4.0800 0.1063 0 17 1 10.0821 -0.0431 0 17 2 -7.1304 -0.0188 0 17 3 19.5030 0.0114 0 17 4 5.8435 -0.0195 0 17 5 5.6324 0.0340 0 17 6 -1.2376 0.0018 0 17 7 -4.6531 -0.0018 0 17 8 1.6228 -0.0032 0 17 9 -12.4419 -0.0215 0 17 10 1.4552 0.0126 0 17 11 -8.9740 -0.0071 0 17 12 0.3329 0.0093 0 17 13 6.4482 0.0008 0 17 14 -2.4066 0.0071 0 17 15 0.4556 0.0060 0 17 16 -4.6089 0.0114 0 17 17 1.9668 0.0204 0 17 18 4.4270 -0.0728 0 17 19 6.2045 -0.0145 0 18 0 -7.1334 -0.0181 0 18 1 -0.2617 0.0619 0 18 2 -1.0014 0.0231 0 18 3 8.8309 0.0382 0 18 4 4.8160 -0.0147 0 18 5 -0.3357 -0.0031 0 18 6 10.7920 0.0025 0 18 7 1.0546 -0.0179 0 18 8 11.9549 -0.0083 0 18 9 -5.9068 -0.0168 0 18 10 8.6277 0.0116 0 18 11 -11.5132 -0.0116 0 18 12 -5.9962 0.0203 0 18 13 -0.7362 0.0036 0 18 14 -2.8987 -0.0185 0 18 15 -9.2259 0.0009 0 18 16 -4.3295 -0.0320 0 18 17 2.7380 0.0016 0 19 0 -3.1461 0.1204 0 19 1 -4.5426 -0.1061 0 19 2 -2.0811 -0.0335 0 19 3 1.4029 -0.0155 0 19 4 -0.2106 -0.0392 0 19 5 11.1598 0.0361 0 19 6 3.5080 0.0193 0 19 7 -2.3840 0.0124 0 19 8 10.8503 0.0035 0 19 9 -7.3647 -0.0376 0 19 10 -3.1661 0.0292 0 19 11 -1.7172 0.0055 0 19 12 -3.9733 0.0087 0 19 13 -4.1330 0.0341 0 19 14 -2.0519 -0.0408 0 19 15 5.5873 -0.0455 0 20 0 3.4061 0.0402 0 20 1 7.6354 -0.0171 0 20 2 -5.1355 -0.0102 0 20 3 2.9102 0.0249 0 20 4 4.1707 0.0121 0 20 5 6.0438 0.0119 0 20 6 5.3535 -0.0405 0 20 7 -1.7471 -0.0127 0 20 8 -4.8776 0.0314 0 20 9 -8.0087 -0.0104 0 20 10 1.7345 -0.0019 0 20 11 -1.2464 -0.0338 0 20 12 7.7063 0.0011 0 20 13 -0.1371 0.0009 0 21 0 -4.3363 0.0012 0 21 1 -8.3353 -0.0023 0 21 2 -5.4564 0.0185 0 21 3 -2.9455 -0.0068 0 21 4 -5.2518 0.0046 0 21 5 2.8242 0.0310 0 21 6 7.2845 -0.0085 0 21 7 1.8966 -0.0306 0 21 8 -4.1934 -0.0062 0 21 9 -4.8722 0.0073 0 21 10 -1.5316 0.0250 0 21 11 0.9026 -0.0028 0 22 0 7.8263 0.0660 0 22 1 -2.0114 -0.0346 0 22 2 -1.2462 -0.0478 0 22 3 6.6132 -0.0572 0 22 4 -1.9316 0.0318 0 22 5 -5.3600 0.0660 0 22 6 -0.9596 -0.0414 0 22 7 1.2786 -0.0134 1 1 0 225.8352 0.8932 1 1 1 210.6813 -0.2963 1 1 2 -30.8742 -0.1393 1 1 3 -55.5305 -0.2286 1 1 4 0.9512 -0.1053 1 1 5 -132.8456 0.0368 1 1 6 -217.2147 -0.0329 1 1 7 102.2616 0.1016 1 1 8 -62.2662 -0.0268 1 1 9 -21.6108 0.0051 1 1 10 53.2781 -0.0106 1 1 11 -61.0452 -0.0116 1 1 12 1.0716 -0.0021 1 1 13 1.6325 0.0060 1 1 14 39.1359 0.0062 1 1 15 -4.2629 0.0094 1 1 16 -1.4851 0.0074 1 1 17 -3.9743 0.0010 1 1 18 -16.9895 -0.0014 1 1 19 0.3802 -0.0228 1 1 20 -1.0894 -0.0099 1 1 21 1.6755 -0.0191 1 1 22 -2.8819 -0.0003 1 1 23 9.3564 -0.0015 1 1 24 9.5022 -0.0015 1 1 25 -5.5390 0.0129 1 1 26 0.5352 0.0109 1 1 27 -2.5728 0.0875 1 1 28 -2.3457 0.0977 1 2 0 8.3223 -0.4598 1 2 1 -44.0615 -0.0543 1 2 2 -94.1906 -0.0571 1 2 3 -62.5032 -0.1205 1 2 4 12.9809 0.2121 1 2 5 43.0248 -0.0406 1 2 6 -124.0396 0.1285 1 2 7 26.8288 0.0180 1 2 8 -92.2226 -0.0298 1 2 9 59.2511 0.0343 1 2 10 73.3033 -0.0818 1 2 11 4.3517 0.0142 1 2 12 41.8548 -0.0139 1 2 13 -5.4431 -0.0111 1 2 14 3.7433 0.0204 1 2 15 21.3601 -0.0056 1 2 16 9.9247 0.0139 1 2 17 -3.2730 0.0037 1 2 18 -11.5446 -0.0193 1 2 19 -6.5921 0.0106 1 2 20 -10.9566 -0.0207 1 2 21 1.9897 0.0092 1 2 22 -0.0378 0.0113 1 2 23 4.5830 0.0016 1 2 24 9.5675 0.0405 1 2 25 -5.5987 -0.0147 1 2 26 -3.1019 0.0387 1 2 27 -8.2096 -0.0409 1 2 28 2.2476 -0.0379 1 3 0 102.9890 0.3647 1 3 1 -184.2371 -0.3517 1 3 2 108.3181 0.1347 1 3 3 18.1844 -0.1124 1 3 4 66.2575 0.0975 1 3 5 20.1782 0.0576 1 3 6 36.0638 0.0372 1 3 7 -0.0498 0.0963 1 3 8 -87.1657 -0.0274 1 3 9 28.8126 0.0463 1 3 10 -4.9608 -0.0463 1 3 11 18.7043 0.0294 1 3 12 14.6007 -0.0242 1 3 13 -4.5429 0.0036 1 3 14 -3.7704 -0.0094 1 3 15 9.8853 -0.0241 1 3 16 5.4318 0.0105 1 3 17 -2.1720 -0.0281 1 3 18 -3.6195 0.0114 1 3 19 -6.7387 -0.0040 1 3 20 -7.7910 -0.0083 1 3 21 -1.6835 0.0159 1 3 22 1.3955 0.0022 1 3 23 -0.7143 -0.0053 1 3 24 -1.4597 0.0142 1 3 25 1.9390 -0.0104 1 3 26 -3.2501 0.0376 1 3 27 0.6893 -0.0289 1 3 28 -1.6058 0.0662 1 4 0 91.3593 0.3765 1 4 1 35.7557 -0.3631 1 4 2 71.9177 0.0339 1 4 3 -23.1369 -0.0276 1 4 4 -23.5398 0.0041 1 4 5 13.2577 0.0047 1 4 6 -4.8736 -0.0207 1 4 7 29.4358 -0.0040 1 4 8 -35.3423 -0.0120 1 4 9 16.6037 -0.0191 1 4 10 6.1338 -0.0249 1 4 11 27.2139 -0.0042 1 4 12 4.0547 -0.0171 1 4 13 3.8595 0.0213 1 4 14 8.3485 0.0152 1 4 15 2.8133 0.0162 1 4 16 -5.8397 0.0172 1 4 17 -3.4457 -0.0115 1 4 18 0.9285 0.0025 1 4 19 6.5491 -0.0166 1 4 20 -7.8812 -0.0133 1 4 21 6.8197 -0.0027 1 4 22 -2.6346 0.0033 1 4 23 -3.4937 -0.0030 1 4 24 -5.0227 0.0003 1 4 25 1.8736 0.0122 1 4 26 3.9468 0.0027 1 4 27 0.6514 0.0128 1 5 0 -27.3720 -0.6297 1 5 1 26.3016 0.0342 1 5 2 -7.7770 0.1964 1 5 3 -73.1601 0.0107 1 5 4 -69.2193 0.1285 1 5 5 -37.2745 -0.0783 1 5 6 12.0412 0.0154 1 5 7 -0.1633 -0.0142 1 5 8 5.7011 -0.0626 1 5 9 31.9195 0.0348 1 5 10 4.0334 -0.0372 1 5 11 10.8089 0.0433 1 5 12 -2.5199 0.0151 1 5 13 -10.2904 -0.0019 1 5 14 -11.5081 0.0215 1 5 15 5.3321 -0.0153 1 5 16 -5.7301 -0.0090 1 5 17 -6.4194 -0.0052 1 5 18 -0.2790 -0.0065 1 5 19 -5.4622 0.0150 1 5 20 -3.6885 0.0084 1 5 21 7.1797 0.0188 1 5 22 3.1292 0.0398 1 5 23 4.8211 -0.0091 1 5 24 -1.2481 0.0040 1 5 25 3.5684 0.0025 1 5 26 4.2210 -0.0533 1 5 27 -0.9387 -0.0512 1 6 0 14.9658 0.2470 1 6 1 4.8001 -0.2206 1 6 2 25.4349 -0.0693 1 6 3 -44.1049 -0.0298 1 6 4 23.6962 -0.0326 1 6 5 -23.0733 -0.0244 1 6 6 40.0617 0.0539 1 6 7 30.2210 -0.0020 1 6 8 8.3853 0.0611 1 6 9 32.0721 0.0385 1 6 10 18.5298 -0.0052 1 6 11 -6.1488 0.0394 1 6 12 -5.1914 -0.0451 1 6 13 -20.3100 0.0110 1 6 14 -18.4654 -0.0101 1 6 15 1.9824 -0.0050 1 6 16 -0.1650 0.0150 1 6 17 -2.7550 -0.0207 1 6 18 3.8484 0.0109 1 6 19 -3.0425 0.0084 1 6 20 -4.0355 -0.0018 1 6 21 10.1283 0.0079 1 6 22 0.1522 -0.0130 1 6 23 2.2561 0.0172 1 6 24 3.5264 -0.0116 1 6 25 3.8123 -0.0186 1 6 26 -2.1299 0.0114 1 6 27 -7.8659 -0.1195 1 7 0 -106.0076 -0.2157 1 7 1 -19.8230 -0.1467 1 7 2 5.3674 0.1077 1 7 3 -89.2140 -0.0348 1 7 4 15.4080 0.0968 1 7 5 -70.0230 -0.0346 1 7 6 -17.5360 0.0407 1 7 7 -10.9471 0.0117 1 7 8 -3.6742 -0.0092 1 7 9 1.9473 0.0248 1 7 10 11.8681 -0.0224 1 7 11 -1.9745 0.0147 1 7 12 8.0166 -0.0160 1 7 13 -10.3351 0.0071 1 7 14 -19.4451 -0.0046 1 7 15 -19.2730 -0.0039 1 7 16 3.4140 0.0089 1 7 17 -3.9441 -0.0122 1 7 18 2.2023 0.0036 1 7 19 -8.2579 -0.0017 1 7 20 2.2804 0.0104 1 7 21 0.6095 0.0061 1 7 22 -0.7976 -0.0110 1 7 23 4.2632 0.0120 1 7 24 -1.1913 -0.0237 1 7 25 -1.1697 -0.0006 1 7 26 3.0947 0.0189 1 8 0 -6.9882 -0.4711 1 8 1 -22.3024 0.0389 1 8 2 -13.5006 0.2096 1 8 3 -46.0617 -0.0250 1 8 4 -10.3466 0.1181 1 8 5 5.5230 -0.0316 1 8 6 37.1166 0.0126 1 8 7 -28.1612 0.0145 1 8 8 16.8837 -0.0388 1 8 9 19.0264 0.0262 1 8 10 3.5572 -0.0317 1 8 11 15.8267 0.0149 1 8 12 -6.6935 -0.0049 1 8 13 -11.6403 0.0122 1 8 14 -14.1277 -0.0067 1 8 15 -18.8648 -0.0045 1 8 16 2.5307 0.0037 1 8 17 0.8835 -0.0067 1 8 18 -0.6472 0.0033 1 8 19 1.6672 0.0006 1 8 20 7.6892 -0.0052 1 8 21 0.6906 0.0075 1 8 22 -0.6922 0.0010 1 8 23 1.5900 0.0195 1 8 24 0.7822 0.0053 1 8 25 6.1934 -0.0332 1 8 26 -1.5625 0.0666 1 9 0 3.3643 0.2207 1 9 1 -13.8506 -0.0705 1 9 2 -24.2057 -0.0357 1 9 3 -25.2921 -0.0357 1 9 4 -0.2537 -0.0278 1 9 5 -24.8370 -0.0373 1 9 6 2.2956 -0.0118 1 9 7 13.8149 -0.0178 1 9 8 21.9917 0.0303 1 9 9 42.2084 -0.0105 1 9 10 -3.5405 0.0105 1 9 11 12.4202 0.0056 1 9 12 2.9034 -0.0261 1 9 13 1.5225 0.0236 1 9 14 -19.2895 -0.0072 1 9 15 -8.5593 -0.0049 1 9 16 -6.9312 0.0070 1 9 17 0.9962 -0.0024 1 9 18 10.6391 0.0283 1 9 19 -8.7650 -0.0132 1 9 20 9.1073 0.0024 1 9 21 0.3810 0.0014 1 9 22 -3.9683 -0.0321 1 9 23 5.3850 -0.0068 1 9 24 1.4248 -0.0297 1 9 25 -4.6927 0.0346 1 10 0 -37.9774 -0.3931 1 10 1 -22.2059 -0.0406 1 10 2 -30.3365 0.1679 1 10 3 -1.2974 -0.0109 1 10 4 18.0605 0.1027 1 10 5 -35.9046 -0.0021 1 10 6 11.6652 0.0076 1 10 7 17.3035 -0.0018 1 10 8 9.3237 -0.0298 1 10 9 9.0428 -0.0007 1 10 10 19.2265 -0.0126 1 10 11 15.6976 -0.0025 1 10 12 -7.5164 0.0241 1 10 13 -3.9182 0.0127 1 10 14 -6.8362 0.0057 1 10 15 -6.0830 0.0030 1 10 16 -1.2427 -0.0195 1 10 17 -10.6123 -0.0004 1 10 18 2.9688 0.0146 1 10 19 -6.0866 -0.0016 1 10 20 0.2034 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-0.0138 1 12 14 -10.8363 -0.0048 1 12 15 -0.1412 -0.0078 1 12 16 -3.5067 0.0125 1 12 17 -3.7737 -0.0151 1 12 18 -1.5336 0.0010 1 12 19 -1.4072 -0.0224 1 12 20 -0.0276 -0.0047 1 12 21 -2.0612 0.0106 1 12 22 -1.3097 0.0219 1 12 23 5.5791 0.0423 1 13 0 0.1470 -0.4224 1 13 1 -9.6832 0.0127 1 13 2 11.0489 0.1037 1 13 3 -10.3232 -0.0096 1 13 4 -14.8685 0.0873 1 13 5 -12.7837 0.0032 1 13 6 -1.5966 0.0224 1 13 7 -5.5632 -0.0159 1 13 8 -8.9968 -0.0336 1 13 9 0.8883 -0.0173 1 13 10 2.5527 -0.0168 1 13 11 -5.5385 -0.0021 1 13 12 0.9479 0.0022 1 13 13 -1.0696 0.0072 1 13 14 5.6337 -0.0016 1 13 15 4.0857 0.0090 1 13 16 9.1078 0.0044 1 13 17 2.0423 0.0171 1 13 18 -3.2132 -0.0108 1 13 19 0.9282 -0.0035 1 13 20 2.9973 0.0209 1 13 21 -0.7658 -0.0268 1 13 22 9.7315 0.0626 1 14 0 4.8110 0.0313 1 14 1 -4.0276 0.0954 1 14 2 10.0460 0.0208 1 14 3 2.1919 -0.0078 1 14 4 -6.6828 0.0071 1 14 5 6.1691 -0.0474 1 14 6 4.0898 0.0045 1 14 7 5.1340 -0.0065 1 14 8 6.9136 0.0028 1 14 9 -3.2760 0.0230 1 14 10 -3.0423 0.0073 1 14 11 3.6486 0.0123 1 14 12 -1.0020 0.0166 1 14 13 3.6149 0.0108 1 14 14 5.4489 0.0053 1 14 15 -6.1085 -0.0060 1 14 16 -4.0631 -0.0051 1 14 17 4.0724 -0.0160 1 14 18 -1.4178 0.0044 1 14 19 1.9042 -0.0355 1 14 20 -4.6523 -0.0207 1 14 21 7.0015 -0.0124 1 15 0 0.0902 -0.0254 1 15 1 2.9982 0.1000 1 15 2 3.8685 0.0095 1 15 3 7.2421 0.0149 1 15 4 1.2798 0.0118 1 15 5 3.9539 -0.0507 1 15 6 0.7882 0.0249 1 15 7 -3.4168 -0.0005 1 15 8 10.3669 0.0168 1 15 9 -1.1010 0.0155 1 15 10 0.3107 -0.0041 1 15 11 -10.8801 -0.0153 1 15 12 0.3985 0.0010 1 15 13 -1.2824 0.0063 1 15 14 -3.3951 -0.0010 1 15 15 3.1150 -0.0180 1 15 16 0.1313 0.0047 1 15 17 -3.4225 0.0011 1 15 18 -0.4668 0.0125 1 15 19 0.0917 0.0271 1 15 20 -2.2309 -0.0460 1 16 0 21.4493 -0.2358 1 16 1 -1.4894 -0.0284 1 16 2 -8.2568 -0.0008 1 16 3 -0.1341 -0.0027 1 16 4 3.4182 0.0523 1 16 5 5.7439 0.0125 1 16 6 3.5837 0.0104 1 16 7 -3.1702 -0.0049 1 16 8 3.5511 0.0090 1 16 9 -2.7332 -0.0027 1 16 10 1.3723 -0.0134 1 16 11 -8.9721 -0.0014 1 16 12 5.5401 -0.0190 1 16 13 4.8565 0.0256 1 16 14 5.8113 -0.0006 1 16 15 -1.2316 0.0159 1 16 16 -3.9748 -0.0138 1 16 17 -6.4616 -0.0360 1 16 18 0.2014 -0.0115 1 16 19 -4.4838 -0.0386 1 17 0 -1.8698 0.1319 1 17 1 12.4705 0.1405 1 17 2 -7.9791 -0.0176 1 17 3 9.8193 0.0198 1 17 4 1.5546 -0.0189 1 17 5 5.7059 -0.0534 1 17 6 6.0351 0.0003 1 17 7 -1.0575 -0.0104 1 17 8 0.4155 0.0295 1 17 9 -4.7682 0.0162 1 17 10 -2.6083 -0.0136 1 17 11 -1.8147 0.0209 1 17 12 -5.0251 0.0002 1 17 13 8.3781 0.0113 1 17 14 -1.2293 0.0139 1 17 15 -0.2610 0.0052 1 17 16 -6.3427 0.0162 1 17 17 -0.8445 -0.0506 1 17 18 -1.0961 -0.0256 1 18 0 -16.3624 -0.0270 1 18 1 7.4639 0.0345 1 18 2 -6.1068 -0.0137 1 18 3 2.3804 -0.0205 1 18 4 -0.5383 0.0218 1 18 5 8.5011 0.0150 1 18 6 2.3316 0.0158 1 18 7 -2.8248 -0.0288 1 18 8 -3.4691 0.0117 1 18 9 -8.6732 0.0033 1 18 10 -1.5683 -0.0098 1 18 11 -4.1545 0.0266 1 18 12 7.2662 -0.0039 1 18 13 0.5438 -0.0265 1 18 14 2.4785 0.0020 1 18 15 4.8316 0.0139 1 18 16 -5.2788 -0.0022 1 19 0 2.8810 -0.0729 1 19 1 5.9109 0.0084 1 19 2 -9.3113 -0.0133 1 19 3 1.9443 0.0023 1 19 4 -1.4779 0.0144 1 19 5 -0.9330 0.0073 1 19 6 1.4412 0.0323 1 19 7 6.4901 -0.0037 1 19 8 9.1915 -0.0039 1 19 9 3.5918 -0.0212 1 19 10 1.9358 -0.0044 1 19 11 -4.9351 0.0181 1 19 12 0.3255 -0.0010 1 19 13 -2.1531 -0.0117 1 19 14 -3.4248 0.0108 1 20 0 1.2017 0.0948 1 20 1 5.2023 0.1225 1 20 2 1.9461 -0.0288 1 20 3 0.3250 -0.0295 1 20 4 -1.5351 -0.0325 1 20 5 4.9237 -0.0121 1 20 6 3.1148 0.0182 1 20 7 -3.9066 0.0023 1 20 8 2.2041 0.0214 1 20 9 -0.5090 -0.0645 1 20 10 -2.8679 -0.0259 1 20 11 -1.3715 0.0400 1 20 12 -2.6448 -0.0013 1 21 0 1.0518 -0.0032 1 21 1 3.0239 -0.0042 1 21 2 5.0177 -0.0433 1 21 3 -0.5812 0.0132 1 21 4 -7.2697 0.0094 1 21 5 3.6625 0.0158 1 21 6 7.9705 0.0126 1 21 7 4.7287 -0.0022 1 21 8 -3.7182 0.0113 1 21 9 0.5906 0.0087 1 22 0 -3.4939 0.0151 1 22 1 -1.9340 -0.0112 1 22 2 2.7302 -0.0255 1 22 3 -2.4031 0.0215 1 22 4 0.8110 -0.0047 1 22 5 -0.8883 -0.0430 2 1 0 418.9075 0.8955 2 1 1 47.4998 0.3903 2 1 2 72.3383 -0.0841 2 1 3 37.2443 0.0625 2 1 4 28.5292 -0.1338 2 1 5 -28.4338 -0.0331 2 1 6 -4.4368 -0.0448 2 1 7 20.5741 -0.0357 2 1 8 -107.9350 -0.0086 2 1 9 18.6525 0.0215 2 1 10 32.2477 0.0507 2 1 11 -24.3326 0.0180 2 1 12 10.6340 0.0429 2 1 13 -5.0344 -0.0112 2 1 14 33.5961 0.0193 2 1 15 10.6818 -0.0107 2 1 16 11.5513 -0.0099 2 1 17 -2.6328 -0.0061 2 1 18 -14.9327 -0.0151 2 1 19 -0.7085 0.0033 2 1 20 -15.4679 -0.0034 2 1 21 2.4057 0.0061 2 1 22 -8.8216 -0.0101 2 1 23 8.4814 0.0122 2 1 24 0.1567 -0.0113 2 1 25 -8.4900 0.0109 2 1 26 -4.1571 -0.0309 2 1 27 5.1926 -0.0120 2 1 28 6.8854 0.0407 2 2 0 -232.9235 0.1635 2 2 1 104.5140 0.5013 2 2 2 65.2289 -0.0007 2 2 3 23.6327 0.0313 2 2 4 -104.8296 -0.1371 2 2 5 -101.8751 -0.1149 2 2 6 -113.6100 0.0213 2 2 7 -8.7610 -0.0199 2 2 8 -42.0884 0.0371 2 2 9 -11.5633 0.0041 2 2 10 43.4501 0.0006 2 2 11 -3.4015 -0.0260 2 2 12 7.7035 -0.0045 2 2 13 -10.0321 -0.0429 2 2 14 0.2493 -0.0088 2 2 15 17.1844 -0.0074 2 2 16 3.7384 0.0139 2 2 17 -1.1920 0.0315 2 2 18 -9.1307 -0.0027 2 2 19 -2.3768 0.0270 2 2 20 0.0986 -0.0007 2 2 21 6.4798 0.0127 2 2 22 3.0650 -0.0086 2 2 23 4.1122 0.0020 2 2 24 3.0119 0.0009 2 2 25 2.6191 -0.0326 2 2 26 5.0629 -0.0024 2 2 27 2.1138 -0.0260 2 2 28 -1.7854 0.0568 2 3 0 40.8199 -0.0710 2 3 1 46.0562 -0.2674 2 3 2 1.5629 0.0643 2 3 3 0.9190 -0.1108 2 3 4 -48.2511 -0.0572 2 3 5 2.8623 0.0773 2 3 6 9.4112 -0.0347 2 3 7 19.2375 0.0954 2 3 8 -21.3383 0.0017 2 3 9 -82.2495 -0.0095 2 3 10 47.4041 0.0269 2 3 11 19.2543 -0.0527 2 3 12 5.1015 0.0223 2 3 13 -3.0501 -0.0243 2 3 14 1.2385 0.0224 2 3 15 -14.0081 0.0167 2 3 16 -7.1210 0.0046 2 3 17 4.0762 0.0180 2 3 18 -5.0484 -0.0066 2 3 19 1.6332 -0.0063 2 3 20 -10.4034 0.0014 2 3 21 -4.4905 -0.0086 2 3 22 -2.6975 -0.0167 2 3 23 -9.3712 0.0088 2 3 24 -0.0490 -0.0311 2 3 25 9.9770 0.0182 2 3 26 3.0083 -0.0386 2 3 27 0.5208 -0.0130 2 4 0 -29.5794 0.3198 2 4 1 -22.6104 0.3543 2 4 2 38.6625 0.0530 2 4 3 -29.1245 0.0620 2 4 4 26.7021 -0.0690 2 4 5 -23.3225 -0.0997 2 4 6 -56.1057 -0.0509 2 4 7 15.6082 0.0034 2 4 8 16.5891 0.0082 2 4 9 -64.0216 0.0226 2 4 10 8.3803 -0.0056 2 4 11 7.3431 -0.0041 2 4 12 -24.8503 0.0278 2 4 13 -9.3220 -0.0031 2 4 14 6.9916 0.0268 2 4 15 -25.5940 -0.0124 2 4 16 -1.8268 -0.0011 2 4 17 5.8482 0.0077 2 4 18 10.2456 -0.0108 2 4 19 7.4036 0.0163 2 4 20 3.3532 -0.0283 2 4 21 -5.6788 -0.0038 2 4 22 1.5504 -0.0152 2 4 23 -6.5179 -0.0096 2 4 24 -0.4940 0.0170 2 4 25 2.0203 -0.0166 2 4 26 1.2845 0.0549 2 4 27 3.3482 0.0649 2 5 0 -51.4438 0.2601 2 5 1 3.0840 0.0603 2 5 2 28.3788 -0.1121 2 5 3 -12.5380 0.0345 2 5 4 -18.9489 -0.0710 2 5 5 -6.8888 0.0198 2 5 6 -16.4729 -0.0265 2 5 7 -18.7014 -0.0034 2 5 8 10.5967 0.0229 2 5 9 -15.7200 -0.0166 2 5 10 -6.5581 0.0237 2 5 11 5.7729 -0.0318 2 5 12 -6.5883 -0.0037 2 5 13 -5.0782 -0.0242 2 5 14 2.3726 0.0110 2 5 15 -3.2732 -0.0250 2 5 16 -4.1144 0.0043 2 5 17 3.1031 -0.0016 2 5 18 1.5033 -0.0016 2 5 19 1.0849 0.0103 2 5 20 5.0020 -0.0028 2 5 21 2.1922 -0.0018 2 5 22 -5.4510 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12 2 1 -13.6079 -0.0715 12 2 2 -14.9895 0.0502 12 2 3 15.7195 -0.0037 12 2 4 7.0760 0.0500 12 2 5 13.1551 0.0135 12 2 6 3.5435 0.0335 12 2 7 -11.5854 0.0167 12 2 8 7.6517 -0.0227 12 2 9 1.9615 -0.0001 12 2 10 5.2535 -0.0084 12 2 11 -10.1388 -0.0052 12 2 12 -10.1266 -0.0159 12 2 13 1.9778 -0.0112 12 2 14 -5.8298 0.0031 12 2 15 3.5426 -0.0015 12 2 16 -7.4315 0.0088 12 2 17 -0.8043 -0.0011 12 2 18 0.8500 0.0111 12 2 19 -4.0527 0.0114 12 2 20 -0.1591 0.0184 12 2 21 -0.4205 0.0128 12 2 22 -4.6130 0.0016 12 2 23 0.7904 -0.0293 12 3 0 -5.4206 0.1196 12 3 1 2.5253 -0.0951 12 3 2 -10.4818 -0.0186 12 3 3 -2.2531 -0.0445 12 3 4 2.0936 -0.0690 12 3 5 7.2312 -0.0185 12 3 6 11.3193 -0.0053 12 3 7 4.0519 0.0157 12 3 8 5.2897 0.0264 12 3 9 -1.1615 0.0021 12 3 10 7.5166 0.0277 12 3 11 4.5902 0.0092 12 3 12 0.6733 0.0083 12 3 13 -0.1521 0.0038 12 3 14 -10.5759 -0.0052 12 3 15 0.6379 -0.0034 12 3 16 4.9377 -0.0206 12 3 17 5.7196 0.0062 12 3 18 7.3515 0.0006 12 3 19 1.7107 0.0063 12 3 20 -0.4451 0.0157 12 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6.2152 0.0816 12 8 1 0.7350 0.0495 12 8 2 8.3685 -0.0419 12 8 3 -3.7843 -0.0201 12 8 4 -4.4718 -0.0153 12 8 5 -5.5297 -0.0228 12 8 6 -8.9696 0.0054 12 8 7 -3.3239 -0.0020 12 8 8 1.9482 0.0206 12 8 9 -5.9451 0.0135 12 8 10 -1.1972 0.0064 12 8 11 -4.8921 -0.0049 12 8 12 4.9829 -0.0154 12 8 13 -3.2611 -0.0066 12 8 14 -0.2694 -0.0001 12 8 15 -1.4886 0.0285 12 8 16 -0.7225 -0.0003 12 8 17 -0.7819 -0.0173 12 8 18 1.3067 -0.0386 12 9 0 6.6224 -0.0686 12 9 1 3.7867 0.0257 12 9 2 3.4544 0.0198 12 9 3 0.5911 0.0067 12 9 4 -3.9968 0.0308 12 9 5 -4.0412 -0.0236 12 9 6 -8.2244 -0.0160 12 9 7 7.4741 -0.0057 12 9 8 0.2520 -0.0148 12 9 9 9.7430 0.0064 12 9 10 0.4555 -0.0077 12 9 11 7.2849 -0.0100 12 9 12 2.1055 0.0103 12 9 13 4.5892 0.0186 12 9 14 -10.8055 -0.0009 12 9 15 0.8805 0.0013 12 9 16 5.5609 -0.0170 12 9 17 4.5147 -0.0396 12 10 0 9.0035 -0.1340 12 10 1 -0.7567 0.0310 12 10 2 -0.2973 0.0005 12 10 3 1.5713 -0.0149 12 10 4 0.4272 0.0280 12 10 5 -0.6123 0.0029 12 10 6 1.4885 0.0299 12 10 7 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0.0392 12 13 8 -5.2595 0.0259 12 13 9 0.1115 0.0008 12 14 0 -2.0073 0.0418 12 14 1 -0.4344 -0.0041 12 14 2 -3.1225 -0.0715 12 14 3 -6.1191 0.0698 12 14 4 1.2695 0.0252 13 1 0 -18.8470 0.0961 13 1 1 -1.0381 0.1794 13 1 2 3.3859 -0.0356 13 1 3 -0.3326 0.0602 13 1 4 -3.7983 -0.0126 13 1 5 4.9721 -0.0285 13 1 6 11.7643 -0.0041 13 1 7 1.5961 -0.0472 13 1 8 12.0193 0.0023 13 1 9 -2.4553 -0.0206 13 1 10 -9.0404 -0.0087 13 1 11 2.8815 0.0076 13 1 12 -0.2819 0.0066 13 1 13 5.3668 0.0095 13 1 14 -4.6294 0.0044 13 1 15 -0.2958 0.0011 13 1 16 -4.0648 0.0133 13 1 17 -1.9320 0.0164 13 1 18 -2.8560 -0.0138 13 1 19 5.0906 -0.0108 13 1 20 8.6795 -0.0292 13 1 21 -4.0915 -0.0166 13 1 22 4.0304 -0.0046 13 2 0 5.8438 0.1371 13 2 1 -1.8497 -0.2045 13 2 2 -1.5957 -0.0526 13 2 3 5.2429 -0.0024 13 2 4 1.0962 -0.0417 13 2 5 2.8281 0.0589 13 2 6 -5.8369 0.0214 13 2 7 11.8406 0.0393 13 2 8 11.5710 0.0108 13 2 9 -1.4478 -0.0238 13 2 10 -2.7324 -0.0168 13 2 11 -1.8542 -0.0241 13 2 12 -3.1572 -0.0020 13 2 13 -0.6112 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-8.5355 0.0164 16 1 19 5.7826 -0.0112 16 2 0 0.6139 0.0652 16 2 1 0.0473 -0.1074 16 2 2 -6.0981 -0.0438 16 2 3 -7.1595 -0.0109 16 2 4 11.0612 -0.0153 16 2 5 -10.6469 0.0449 16 2 6 4.5844 0.0193 16 2 7 4.9467 0.0194 16 2 8 4.5041 0.0186 16 2 9 6.6908 -0.0168 16 2 10 -4.4425 -0.0057 16 2 11 7.9445 -0.0207 16 2 12 -2.4872 -0.0207 16 2 13 5.9925 -0.0168 16 2 14 2.8025 0.0026 16 2 15 -0.6427 0.0269 16 2 16 1.1350 0.0001 16 2 17 -0.7430 0.0107 16 2 18 -2.6996 -0.0012 16 3 0 -1.2320 0.0511 16 3 1 -17.2866 0.0894 16 3 2 -0.1925 -0.0165 16 3 3 -12.4654 0.0193 16 3 4 -0.2756 -0.0205 16 3 5 -12.3802 -0.0322 16 3 6 5.5020 -0.0223 16 3 7 2.2672 -0.0145 16 3 8 2.6370 -0.0059 16 3 9 16.7009 0.0072 16 3 10 11.5605 0.0265 16 3 11 4.6237 0.0171 16 3 12 -6.9550 -0.0003 16 3 13 3.7176 0.0231 16 3 14 -5.0954 0.0065 16 3 15 -2.3221 0.0153 16 3 16 4.6483 -0.0190 16 3 17 -6.4474 -0.0336 16 3 18 0.1558 -0.0372 16 4 0 -9.0646 0.0838 16 4 1 -6.3089 -0.0319 16 4 2 -9.1967 -0.0268 16 4 3 -21.3558 0.0323 16 4 4 -0.1989 -0.0236 16 4 5 -1.2690 0.0584 16 4 6 16.7607 0.0092 16 4 7 6.0587 -0.0091 16 4 8 2.8378 0.0073 16 4 9 4.2972 -0.0293 16 4 10 -6.3195 -0.0097 16 4 11 7.4701 0.0021 16 4 12 -3.8849 -0.0262 16 4 13 -8.5241 -0.0096 16 4 14 0.7480 0.0039 16 4 15 -0.1389 -0.0097 16 4 16 -0.9698 0.0105 16 4 17 4.7675 0.0560 16 5 0 2.0522 0.0687 16 5 1 -5.6925 -0.0653 16 5 2 -3.5768 -0.0225 16 5 3 -0.8175 -0.0004 16 5 4 2.9485 -0.0112 16 5 5 0.0075 -0.0062 16 5 6 15.2696 -0.0149 16 5 7 2.3193 0.0252 16 5 8 -5.3709 -0.0071 16 5 9 9.1517 0.0049 16 5 10 2.2640 -0.0078 16 5 11 7.6560 0.0068 16 5 12 -1.7475 0.0079 16 5 13 -2.5659 0.0156 16 5 14 -2.7158 0.0072 16 5 15 -1.2192 -0.0347 16 6 0 4.9603 -0.0078 16 6 1 0.7089 0.0581 16 6 2 -2.7680 0.0246 16 6 3 -6.6298 0.0046 16 6 4 -6.5184 -0.0158 16 6 5 5.4708 0.0073 16 6 6 2.9983 -0.0118 16 6 7 0.7236 -0.0155 16 6 8 0.0770 -0.0188 16 6 9 0.1223 -0.0028 16 6 10 5.4642 0.0252 16 6 11 -4.9408 0.0163 16 6 12 -4.2738 0.0315 16 6 13 -2.5503 -0.0030 16 6 14 -2.5427 -0.0156 16 7 0 -9.7139 0.0786 16 7 1 -2.4065 -0.0989 16 7 2 -6.0086 -0.0231 16 7 3 0.2868 0.0296 16 7 4 1.1316 -0.0091 16 7 5 -8.4346 0.0153 16 7 6 9.4840 -0.0024 16 7 7 -0.1729 0.0237 16 7 8 0.4369 0.0063 16 7 9 7.2554 0.0466 16 7 10 -9.3900 -0.0416 16 7 11 -6.5567 -0.0694 16 7 12 8.2133 0.0107 16 8 0 -5.3342 0.0335 16 8 1 2.1247 -0.0253 16 8 2 3.9646 0.0289 16 8 3 8.1376 -0.0089 16 8 4 4.9198 -0.0288 16 8 5 2.3000 -0.0056 16 8 6 -3.8975 -0.0049 16 8 7 4.0359 -0.0113 16 8 8 2.7636 -0.0082 16 8 9 2.0364 0.0334 16 8 10 -2.2321 0.0095 16 9 0 10.1050 -0.0195 16 9 1 8.6454 0.0059 16 9 2 -9.2507 0.0163 16 9 3 -5.1850 0.0047 16 9 4 -1.9292 0.0175 16 9 5 2.4218 0.0051 16 9 6 1.0089 0.0267 16 9 7 -0.8096 -0.0043 16 9 8 5.1550 -0.0223 16 10 0 -2.1740 0.0738 16 10 1 -0.5588 0.0246 16 10 2 2.3921 -0.0182 16 10 3 -1.6393 -0.0630 17 1 0 -8.9929 -0.1660 17 1 1 -1.3224 -0.0013 17 1 2 -10.5404 0.0633 17 1 3 -12.0914 -0.0097 17 1 4 8.1443 0.0427 17 1 5 -11.7078 -0.0006 17 1 6 7.5061 -0.0009 17 1 7 9.3870 -0.0094 17 1 8 8.9251 -0.0401 17 1 9 5.4193 -0.0067 17 1 10 2.9305 0.0017 17 1 11 5.6627 -0.0196 17 1 12 -5.7175 0.0111 17 1 13 -3.9082 0.0323 17 1 14 -1.3439 -0.0046 17 1 15 -1.1910 0.0046 17 1 16 -4.7945 -0.0327 17 1 17 0.0851 -0.0095 17 1 18 -4.7475 0.0810 17 2 0 -6.3697 -0.0742 17 2 1 -15.6228 0.0486 17 2 2 -8.0950 -0.0148 17 2 3 -11.1220 0.0015 17 2 4 6.3785 0.0201 17 2 5 4.2877 -0.0341 17 2 6 13.3467 0.0190 17 2 7 -0.3372 0.0230 17 2 8 -0.9649 0.0180 17 2 9 10.8796 0.0213 17 2 10 1.6594 -0.0085 17 2 11 4.5059 -0.0072 17 2 12 -2.7849 -0.0219 17 2 13 2.3850 0.0192 17 2 14 3.2818 0.0078 17 2 15 -1.8316 -0.0153 17 2 16 -9.6253 0.0221 17 2 17 5.6397 -0.0407 17 3 0 -9.8386 0.0752 17 3 1 -9.2689 0.0676 17 3 2 1.8913 0.0289 17 3 3 -2.3544 -0.0136 17 3 4 4.5395 -0.0295 17 3 5 -1.8558 -0.0260 17 3 6 2.9012 0.0038 17 3 7 -3.8800 -0.0174 17 3 8 5.5901 -0.0075 17 3 9 10.9623 0.0035 17 3 10 11.8771 -0.0015 17 3 11 5.7686 0.0096 17 3 12 -13.3823 -0.0042 17 3 13 -0.9343 -0.0136 17 3 14 -4.5597 -0.0252 17 3 15 -3.8968 0.0012 17 3 16 -4.1057 0.0060 17 4 0 -5.3149 -0.1280 17 4 1 -3.0139 -0.0238 17 4 2 2.2978 0.0093 17 4 3 -7.8661 0.0051 17 4 4 -7.9096 0.0570 17 4 5 -3.7630 0.0089 17 4 6 8.3712 -0.0037 17 4 7 1.1954 0.0049 17 4 8 1.8912 0.0136 17 4 9 7.4013 0.0091 17 4 10 1.5727 -0.0171 17 4 11 7.6210 -0.0154 17 4 12 -2.2493 -0.0122 17 4 13 -1.6968 -0.0046 17 4 14 -2.0279 0.0358 17 4 15 -7.6429 0.0029 17 5 0 4.2229 0.0278 17 5 1 -6.9060 0.0930 17 5 2 -1.9601 -0.0248 17 5 3 -5.7599 -0.0189 17 5 4 -1.6142 -0.0083 17 5 5 -1.8149 -0.0217 17 5 6 5.5595 0.0336 17 5 7 2.7273 -0.0158 17 5 8 5.3814 0.0033 17 5 9 2.5042 0.0174 17 5 10 -2.9549 -0.0340 17 5 11 -0.2865 0.0567 17 5 12 0.2326 0.0199 17 5 13 8.0712 -0.0420 17 6 0 0.5341 0.0050 17 6 1 -2.9591 0.0183 17 6 2 -0.8407 0.0088 17 6 3 -0.7503 0.0053 17 6 4 -4.7652 0.0232 17 6 5 5.0194 -0.0123 17 6 6 10.5910 0.0067 17 6 7 7.9124 -0.0144 17 6 8 4.9551 -0.0041 17 6 9 7.7981 -0.0211 17 6 10 -2.8243 -0.0190 17 6 11 0.3385 0.0460 17 6 12 0.0537 -0.0102 17 7 0 8.4092 -0.0439 17 7 1 2.9998 0.0081 17 7 2 0.9591 -0.0082 17 7 3 2.2088 -0.0093 17 7 4 -8.2065 -0.0030 17 7 5 -2.3916 -0.0159 17 7 6 5.2873 0.0358 17 7 7 -9.4793 0.0085 17 7 8 5.0195 -0.0018 17 7 9 -5.2450 -0.0191 17 7 10 -3.4973 0.0135 17 8 0 2.7055 0.0547 17 8 1 -4.6998 0.0073 17 8 2 -10.3879 -0.0459 17 8 3 -7.9533 0.0659 17 8 4 15.3477 0.0374 17 8 5 2.3704 -0.0896 17 8 6 -4.8641 -0.0548 17 8 7 2.2808 0.0301 17 9 0 -1.2111 0.0109 18 1 0 -2.0691 -0.0705 18 1 1 -1.6354 0.0276 18 1 2 -1.0147 0.0298 18 1 3 -11.4785 0.0047 18 1 4 -3.4354 0.0316 18 1 5 -5.6647 0.0139 18 1 6 1.0736 -0.0154 18 1 7 -2.7017 -0.0196 18 1 8 -0.8216 -0.0119 18 1 9 5.2177 -0.0177 18 1 10 1.3020 -0.0168 18 1 11 10.5131 0.0031 18 1 12 3.2723 -0.0071 18 1 13 -0.4362 -0.0037 18 1 14 -7.2650 0.0357 18 1 15 -11.2752 0.0255 18 1 16 -5.2446 -0.0271 18 2 0 -6.2535 0.0863 18 2 1 -4.8904 -0.1045 18 2 2 -1.1460 -0.0142 18 2 3 -10.0443 -0.0158 18 2 4 -2.6800 -0.0132 18 2 5 -5.9526 0.0131 18 2 6 10.3908 0.0004 18 2 7 3.5506 0.0351 18 2 8 6.4166 0.0072 18 2 9 5.6372 -0.0183 18 2 10 -3.3911 -0.0075 18 2 11 6.4187 0.0074 18 2 12 2.6613 0.0098 18 2 13 3.8829 0.0153 18 2 14 -4.6134 -0.0103 18 2 15 0.6100 -0.0626 18 3 0 2.7398 -0.0589 18 3 1 -5.8704 -0.0135 18 3 2 -3.3093 0.0391 18 3 3 -11.2682 -0.0178 18 3 4 -0.8928 0.0115 18 3 5 -1.3421 -0.0145 18 3 6 16.8053 -0.0468 18 3 7 4.9015 0.0071 18 3 8 3.1540 -0.0044 18 3 9 12.8902 0.0174 18 3 10 -3.8007 0.0043 18 3 11 1.4895 0.0319 18 3 12 -9.1715 -0.0191 18 3 13 3.4863 0.0003 18 3 14 4.1806 0.0481 18 4 0 2.6291 -0.0552 18 4 1 -8.0984 -0.0227 18 4 2 -3.1706 0.0066 18 4 3 3.8169 -0.0032 18 4 4 -9.0161 0.0054 18 4 5 -3.5410 0.0211 18 4 6 4.7276 0.0026 18 4 7 -2.8937 0.0004 18 4 8 6.6007 -0.0154 18 4 9 -0.3163 -0.0100 18 4 10 0.9208 0.0109 18 4 11 -2.4652 -0.0186 18 4 12 -2.3368 -0.0167 18 4 13 3.0845 0.0281 18 5 0 -5.2027 0.0441 18 5 1 -2.9707 -0.0657 18 5 2 1.1353 -0.0204 18 5 3 -4.3788 0.0040 18 5 4 0.4839 -0.0099 18 5 5 -3.3018 -0.0008 18 5 6 7.1603 -0.0321 18 5 7 -1.7466 0.0063 18 5 8 -3.6596 0.0058 18 5 9 9.2928 0.0628 18 5 10 -11.9724 0.0198 18 5 11 1.5831 -0.0351 18 6 0 0.2234 -0.1267 18 6 1 3.3857 -0.0033 18 6 2 -2.0312 0.1090 18 6 3 -2.7197 0.0079 18 6 4 -13.3442 -0.0411 18 6 5 3.7696 -0.0126 18 6 6 9.1680 0.0347 18 6 7 -10.5058 0.0135 18 6 8 3.7329 -0.0573 18 6 9 -0.2206 -0.0174 18 7 0 -4.7944 -0.0101 18 7 1 8.3759 0.0113 18 7 2 -4.2143 -0.0156 18 7 3 1.7789 -0.0215 18 7 4 -4.5947 0.0063 18 7 5 5.8724 0.0145 18 7 6 -1.2894 0.0148 19 1 0 -7.7901 0.0357 19 1 1 -6.8558 -0.0009 19 1 2 0.7362 -0.0227 19 1 3 -2.9894 0.0256 19 1 4 2.4855 -0.0049 19 1 5 -10.3841 0.0128 19 1 6 5.1137 -0.0010 19 1 7 0.6953 -0.0152 19 1 8 -0.0178 -0.0286 19 1 9 10.1365 -0.0453 19 1 10 3.3228 0.0147 19 1 11 2.0343 -0.0135 19 1 12 -1.8272 -0.0041 19 1 13 3.2570 0.0494 19 1 14 -9.2638 0.0191 19 2 0 -8.2258 0.0340 19 2 1 -1.1051 -0.0177 19 2 2 -0.8092 0.0008 19 2 3 -1.3048 -0.0096 19 2 4 -6.7570 -0.0235 19 2 5 -7.0962 0.0072 19 2 6 -4.4513 0.0002 19 2 7 -2.0513 0.0075 19 2 8 8.8126 0.0132 19 2 9 2.4901 0.0173 19 2 10 -2.8763 -0.0013 19 2 11 -1.4460 -0.0029 19 2 12 -1.6070 -0.0212 19 2 13 0.0529 -0.0069 19 3 0 -8.5844 0.0377 19 3 1 -4.4224 0.0625 19 3 2 1.2277 0.0209 19 3 3 -7.0043 0.0045 19 3 4 4.2738 -0.0387 19 3 5 -1.1342 -0.0043 19 3 6 11.4684 0.0258 19 3 7 3.2941 -0.0015 19 3 8 -5.5675 0.0093 19 3 9 11.6014 -0.0487 19 3 10 -0.2054 -0.0658 19 3 11 -2.2431 0.0107 19 3 12 -4.3217 0.0455 19 4 0 3.2762 0.0331 19 4 1 -0.6919 -0.0380 19 4 2 -5.2592 -0.0247 19 4 3 2.7553 0.0080 19 4 4 -4.4031 0.0063 19 4 5 0.0217 0.0585 19 4 6 2.1872 -0.0180 19 4 7 -0.8400 -0.0463 19 4 8 3.7368 0.0020 19 4 9 5.9566 0.0193 19 4 10 2.5635 -0.0190 19 5 0 -7.6805 0.0377 19 5 1 -3.3848 0.0099 19 5 2 1.2989 -0.0257 19 5 3 2.9558 -0.0108 19 5 4 -5.2732 0.0106 19 5 5 1.7992 -0.0063 19 5 6 4.1300 -0.0303 19 5 7 2.3344 0.0008 19 5 8 2.6967 0.0344 19 6 0 -1.4309 0.0421 19 6 1 -3.9037 -0.0009 19 6 2 5.4754 -0.0028 19 6 3 -1.8453 0.0102 19 6 4 3.4812 0.0043 20 1 0 -9.6567 -0.1427 20 1 1 -3.1381 0.0228 20 1 2 4.3755 0.0366 20 1 3 -6.6617 -0.0248 20 1 4 2.7763 0.0635 20 1 5 2.3456 -0.0001 20 1 6 4.0862 -0.0096 20 1 7 5.1008 -0.0117 20 1 8 1.9864 -0.0344 20 1 9 -0.6582 -0.0068 20 1 10 8.8418 0.0296 20 1 11 10.6035 0.0254 20 1 12 -7.3773 -0.0596 20 2 0 -3.7712 0.0048 20 2 1 1.8154 0.0497 20 2 2 0.5236 -0.0395 20 2 3 -1.3462 -0.0326 20 2 4 3.8216 0.0021 20 2 5 3.5644 -0.0069 20 2 6 2.1817 -0.0016 20 2 7 -4.4573 0.0241 20 2 8 4.7431 0.0585 20 2 9 4.4523 0.0061 20 2 10 -1.9103 -0.0202 20 2 11 2.9447 0.0099 20 3 0 3.9135 -0.0229 20 3 1 -4.3283 0.0136 20 3 2 -1.9507 0.0344 20 3 3 1.7445 0.0094 20 3 4 -0.8766 0.0113 20 3 5 -2.8447 -0.0175 20 3 6 -7.9268 0.0086 20 3 7 6.3069 0.0078 20 3 8 5.1035 -0.0291 20 3 9 -4.1032 -0.0051 20 4 0 0.9162 -0.1072 20 4 1 -9.9642 -0.0212 20 4 2 4.4010 0.0457 20 4 3 -7.2647 0.0192 20 4 4 -0.9604 -0.0405 20 4 5 0.5296 -0.0130 20 4 6 9.4129 0.0710 21 1 0 11.6974 -0.0050 21 1 1 -1.4030 -0.0004 21 1 2 4.5426 -0.0131 21 1 3 -8.4282 -0.0100 21 1 4 -6.9181 0.0054 21 1 5 -1.2068 0.0368 21 1 6 -0.2589 0.0117 21 1 7 2.9505 -0.0154 21 1 8 1.0348 -0.0096 21 1 9 -3.7000 -0.0075 21 2 0 4.9257 0.0368 21 2 1 -4.8308 0.0042 21 2 2 -0.3159 -0.0069 21 2 3 -3.4381 -0.0651 21 2 4 -4.2046 -0.0046 21 2 5 -5.6361 0.0640 21 2 6 1.6553 -0.0088 21 2 7 7.2332 -0.0530 21 3 0 0.2267 -0.0539 21 3 1 -0.0388 -0.0246 21 3 2 -2.8452 0.1011 21 3 3 2.8677 0.0221 21 3 4 -2.9891 -0.0381 22 1 0 -6.3679 -0.0350 22 1 1 3.9219 -0.0330 22 1 2 -3.9890 0.0042 22 1 3 6.0276 0.0187 22 1 4 4.0014 -0.0059 22 1 5 2.3220 0.0297 0 0 0 0.0 0.0 ; _olex2_diffrn_ambient_temperature_device 'Oxford Cryostream 800' _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-x, -y, z+1/2' 'y, -x+y, z+1/2' 'x-y, x, z+1/2' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' 'x, y, -z-1/2' '-y, x-y, -z-1/2' '-x+y, -x, -z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.38300(9) 0.34844(9) 0.750000 0.1022(8) Uani 1 2 d S T P . . O1 O 0.5625(8) 0.7645(6) 0.5036(7) 0.297(10) Uani 1 1 d . . . . . O2 O 0.2099(5) 0.1299(5) 0.4453(3) 0.163(4) Uani 1 1 d . . . . . O3 O 0.2994(5) -0.0185(6) 0.5151(3) 0.168(4) Uani 1 1 d . . . . . N1 N 0.3244(5) 0.2617(6) 0.750000 0.109(4) Uani 1 2 d S T P . . N2 N 0.3748(4) 0.3502(4) 0.6776(3) 0.097(2) Uani 1 1 d . . . . . N3 N 0.4215(5) 0.4419(6) 0.750000 0.103(4) Uani 1 2 d S T P . . N4 N 0.4632(7) 0.3452(8) 0.750000 0.115(4) Uani 1 2 d S T P . . N5 N 0.6702(14) 0.3881(8) 0.750000 0.117(5) Uani 1 2 d S T P . . N6 N 0.5635(5) 0.6785(6) 0.5206(4) 0.130(3) Uani 1 1 d . . . . . N7 N 0.2267(5) 0.0643(5) 0.4821(4) 0.133(3) Uani 1 1 d . U . . . C1 C 0.3058(5) 0.2244(5) 0.7121(4) 0.102(3) Uani 1 1 d . . . . . C2 C 0.2910(7) -0.1008(7) 0.5575(4) 0.152(5) Uani 1 1 d . . . . . H2A H 0.261180 -0.137632 0.572469 0.182 Uiso 1 1 calc R U . . . H2B H 0.319541 -0.076863 0.582074 0.182 Uiso 1 1 calc R U . . . C3 C 0.1941(6) 0.1186(5) 0.5952(4) 0.123(4) Uani 1 1 d . . . . . H3 H 0.152586 0.096824 0.595117 0.148 Uiso 1 1 calc R U . . . C4 C 0.5699(10) 0.3395(10) 0.750000 0.100(4) Uani 1 2 d S T P . . C5 C 0.5467(9) 0.7146(12) 0.4958(6) 0.183(6) Uani 1 1 d . U . . . C6 C 0.6180(12) 0.3350(19) 0.750000 0.107(6) Uani 1 2 d S T P . . C7 C 0.4533(6) 0.5442(7) 0.6202(4) 0.144(4) Uani 1 1 d . . . . . H7 H 0.425710 0.546665 0.640122 0.173 Uiso 1 1 calc R U . . . C8 C 0.4352(5) 0.4561(6) 0.6660(4) 0.111(3) Uani 1 1 d . . . . . C10 C 0.4002(5) 0.3982(7) 0.6497(4) 0.103(3) Uani 1 1 d . . . . . C12 C 0.4447(5) 0.4740(6) 0.7124(4) 0.106(3) Uani 1 1 d . . . . . C13 C 0.4821(6) 0.5876(6) 0.5837(5) 0.138(4) Uani 1 1 d . . . . . H13 H 0.476821 0.620468 0.581030 0.166 Uiso 1 1 calc R U . . . C14 C 0.2272(7) 0.1102(5) 0.5590(4) 0.121(4) Uani 1 1 d . . . . . C15 C 0.2624(8) -0.0694(8) 0.5398(6) 0.180(7) Uani 1 1 d . . . . . H15A H 0.229831 -0.095716 0.518937 0.216 Uiso 1 1 calc R U . . . H15B H 0.245537 -0.059124 0.566765 0.216 Uiso 1 1 calc R U . . . C16 C 0.2236(6) 0.1586(6) 0.6298(4) 0.112(4) Uani 1 1 d . . . . . H16 H 0.202457 0.160834 0.655926 0.134 Uiso 1 1 calc R U . . . C17 C 0.2656(6) 0.1024(5) 0.4039(3) 0.169(5) Uani 1 1 d G U . . . C35 C 0.3244(6) 0.1190(4) 0.4061(3) 0.167(5) Uani 1 1 d G U . . . H35 H 0.344590 0.130634 0.435257 0.201 Uiso 1 1 calc R U . . . C9 C 0.3537(5) 0.1187(5) 0.3656(5) 0.213(6) Uani 1 1 d G U . . . H9 H 0.393907 0.130038 0.367063 0.255 Uiso 1 1 calc R U . . . C37 C 0.3241(7) 0.1017(5) 0.3229(4) 0.239(8) Uani 1 1 d G U . . . H37 H 0.344162 0.101428 0.295213 0.287 Uiso 1 1 calc R U . . . C19 C 0.2653(7) 0.0850(5) 0.3207(3) 0.274(9) Uani 1 1 d G U . . . H19 H 0.245101 0.073414 0.291556 0.329 Uiso 1 1 calc R U . . . C39 C 0.2360(5) 0.0854(5) 0.3612(4) 0.246(8) Uani 1 1 d G U . . . H39 H 0.195784 0.074010 0.359749 0.295 Uiso 1 1 calc R U . . . C18 C 0.3141(5) 0.2441(5) 0.6646(4) 0.105(3) Uani 1 1 d D . . . . C20 C 0.3441(5) 0.3017(6) 0.6503(4) 0.099(3) Uani 1 1 d . . . . . C22 C 0.5114(9) 0.2898(9) 0.750000 0.118(6) Uani 1 2 d S T P . . H22 H 0.506742 0.251703 0.750000 0.141 Uiso 1 2 calc R U P . . C24 C 0.2821(7) 0.1950(6) 0.6279(4) 0.123(4) Uani 1 1 d D . . . . C25 C 0.5033(6) 0.4920(6) 0.5936(5) 0.124(4) Uani 1 1 d . . . . . H25 H 0.510895 0.460581 0.595982 0.149 Uiso 1 1 calc R U . . . C26 C 0.4653(6) 0.4991(6) 0.6267(5) 0.128(4) Uani 1 1 d . . . . . C27 C 0.1907(6) 0.0628(6) 0.5224(4) 0.137(4) Uani 1 1 d . . . . . H27A H 0.172812 0.023905 0.537473 0.164 Uiso 1 1 calc R U . . . H27B H 0.158770 0.068859 0.510823 0.164 Uiso 1 1 calc R U . . . C28 C 0.2318(8) 0.0982(7) 0.4444(6) 0.146(5) Uani 1 1 d . U . . . C29 C 0.5186(10) 0.3976(8) 0.750000 0.132(6) Uani 1 2 d S T P . . H29 H 0.521551 0.434954 0.750000 0.158 Uiso 1 2 calc R U P . . C30 C 0.2783(5) 0.1636(5) 0.7261(3) 0.108(3) Uani 1 1 d . . . . . H30 H 0.263317 0.130534 0.705974 0.130 Uiso 1 1 calc R U . . . C31 C 0.2384(5) 0.0179(7) 0.4788(5) 0.136(4) Uani 1 1 d . . . . . H31A H 0.249770 0.014889 0.446194 0.163 Uiso 1 1 calc R U . . . H31B H 0.202897 -0.019352 0.486978 0.163 Uiso 1 1 calc R U . . . C32 C 0.2862(7) 0.1488(7) 0.5577(4) 0.122(4) Uani 1 1 d . . . . . H32 H 0.307318 0.146687 0.531401 0.146 Uiso 1 1 calc R U . . . C33 C 0.2908(6) 0.0301(8) 0.5147(4) 0.150(5) Uani 1 1 d . . . . . H33 H 0.312542 0.064624 0.532716 0.180 Uiso 1 1 calc R U . . . C34 C 0.3506(5) 0.3212(7) 0.6012(4) 0.122(4) Uani 1 1 d . . . . . H34 H 0.334430 0.297502 0.574048 0.147 Uiso 1 1 calc R U . . . C36 C 0.4864(6) 0.5316(6) 0.7255(4) 0.146(4) Uani 1 1 d . . . . . H36 H 0.509436 0.563598 0.705190 0.176 Uiso 1 1 calc R U . . . C38 C 0.4666(10) 0.2945(8) 0.750000 0.130(6) Uani 1 2 d S T P . . H38 H 0.430367 0.258895 0.750000 0.156 Uiso 1 2 calc R U P . . C40 C 0.5278(5) 0.5337(7) 0.5586(4) 0.129(4) Uani 1 1 d . . . . . H40 H 0.553460 0.530180 0.537152 0.154 Uiso 1 1 calc R U . . . C41 C 0.5064(7) 0.6856(7) 0.4567(5) 0.223(6) Uani 1 1 d G U . . . C21 C 0.5200(6) 0.6714(7) 0.4132(6) 0.252(7) Uani 1 1 d G U . . . H21 H 0.555892 0.672018 0.408909 0.302 Uiso 1 1 calc R U . . . C43 C 0.4810(8) 0.6565(7) 0.3760(4) 0.249(8) Uani 1 1 d G U . . . H43 H 0.490227 0.646824 0.346203 0.299 Uiso 1 1 calc R U . . . C11 C 0.4284(7) 0.6556(7) 0.3822(5) 0.275(9) Uani 1 1 d G U . . . H11 H 0.401731 0.645417 0.356775 0.330 Uiso 1 1 calc R U . . . C45 C 0.4148(6) 0.6698(8) 0.4258(7) 0.296(9) Uani 1 1 d G U . . . H45 H 0.378899 0.669202 0.430055 0.355 Uiso 1 1 calc R U . . . C23 C 0.4538(8) 0.6847(8) 0.4630(5) 0.296(9) Uani 1 1 d G U . . . H23 H 0.444563 0.694395 0.492762 0.355 Uiso 1 1 calc R U . . . C42 C 0.5694(9) 0.3919(11) 0.750000 0.125(6) Uani 1 2 d S T P . . H42 H 0.606217 0.426960 0.750000 0.150 Uiso 1 2 calc R U P . . C44 C 0.3171(6) 0.1904(5) 0.5916(4) 0.118(4) Uani 1 1 d . . . . . H44 H 0.358492 0.214095 0.590864 0.142 Uiso 1 1 calc R U . . . C46 C 0.5185(6) 0.5790(6) 0.5521(4) 0.121(4) Uani 1 1 d . . . . . C47 C 0.5455(6) 0.6188(6) 0.5111(4) 0.138(4) Uani 1 1 d . . . . . H47A H 0.579901 0.616268 0.500615 0.166 Uiso 1 1 calc R U . . . H47B H 0.517037 0.605002 0.484908 0.166 Uiso 1 1 calc R U . . . C48 C 0.3835(6) 0.3785(7) 0.6026(4) 0.117(4) Uani 1 1 d . . . . . H48 H 0.394638 0.403273 0.575833 0.141 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.1155(17) 0.1169(17) 0.0683(12) 0.000 0.000 0.0536(14) O1 0.35(2) 0.139(9) 0.35(2) -0.043(11) -0.123(16) 0.091(12) O2 0.178(9) 0.147(8) 0.136(7) 0.006(6) -0.011(6) 0.059(7) O3 0.258(12) 0.226(11) 0.102(6) -0.021(7) -0.027(6) 0.182(11) N1 0.106(9) 0.155(12) 0.076(8) 0.000 0.000 0.073(9) N2 0.102(6) 0.090(6) 0.073(5) -0.013(6) -0.002(5) 0.030(5) N3 0.116(10) 0.123(11) 0.077(9) 0.000 0.000 0.064(9) N4 0.140(13) 0.134(12) 0.060(7) 0.000 0.000 0.060(12) N5 0.086(13) 0.127(17) 0.108(10) 0.000 0.000 0.032(17) N6 0.136(8) 0.149(10) 0.100(7) 0.008(7) 0.002(6) 0.067(8) N7 0.162(8) 0.142(9) 0.093(7) -0.012(6) -0.003(6) 0.072(7) C1 0.111(8) 0.117(10) 0.072(8) -0.013(7) -0.009(6) 0.053(7) C2 0.197(14) 0.219(15) 0.096(9) 0.012(9) 0.002(9) 0.147(13) C3 0.128(10) 0.134(10) 0.089(8) -0.010(8) 0.003(8) 0.051(9) C4 0.100(18) 0.106(14) 0.090(10) 0.000 0.000 0.048(16) C5 0.228(15) 0.285(17) 0.129(10) -0.029(13) -0.033(10) 0.199(14) C6 0.11(3) 0.19(3) 0.069(9) 0.000 0.000 0.11(3) C7 0.180(13) 0.154(12) 0.113(10) 0.010(9) 0.028(9) 0.095(11) C8 0.120(9) 0.092(10) 0.091(9) 0.018(8) -0.001(7) 0.032(8) C10 0.126(9) 0.117(11) 0.068(7) 0.033(8) 0.007(7) 0.062(8) C12 0.123(10) 0.098(10) 0.096(10) -0.010(8) -0.017(7) 0.054(8) C13 0.148(11) 0.151(12) 0.116(9) 0.041(9) 0.034(9) 0.074(10) C14 0.136(12) 0.099(9) 0.093(9) -0.005(7) -0.012(8) 0.033(9) C15 0.229(19) 0.149(13) 0.157(14) 0.027(11) 0.028(13) 0.091(13) C16 0.085(9) 0.124(9) 0.102(9) -0.011(7) -0.002(7) 0.033(8) C17 0.226(11) 0.160(9) 0.096(8) 0.006(7) 0.015(9) 0.079(9) C35 0.225(12) 0.167(10) 0.128(9) 0.029(8) 0.032(9) 0.112(10) C9 0.248(13) 0.199(11) 0.155(11) 0.023(10) 0.056(11) 0.084(11) C37 0.288(16) 0.228(13) 0.152(11) 0.011(11) 0.067(12) 0.091(13) C19 0.310(16) 0.265(13) 0.154(11) 0.014(11) 0.056(13) 0.073(14) C39 0.284(14) 0.239(12) 0.096(8) 0.002(10) 0.023(10) 0.041(12) C18 0.113(9) 0.104(9) 0.075(8) -0.008(7) -0.007(6) 0.036(7) C20 0.083(7) 0.121(10) 0.076(7) 0.010(8) -0.001(6) 0.040(7) C22 0.092(15) 0.157(19) 0.151(14) 0.000 0.000 0.097(17) C24 0.161(14) 0.144(11) 0.072(8) -0.001(7) -0.001(8) 0.083(11) C25 0.131(10) 0.148(11) 0.108(9) -0.012(9) 0.022(8) 0.080(9) C26 0.135(11) 0.104(10) 0.145(12) -0.010(9) -0.044(10) 0.060(9) C27 0.152(10) 0.149(11) 0.095(8) -0.021(8) 0.007(8) 0.065(9) C28 0.188(11) 0.123(10) 0.103(9) -0.014(8) -0.026(8) 0.060(9) C29 0.106(15) 0.108(15) 0.140(15) 0.000 0.000 0.022(15) C30 0.123(8) 0.095(8) 0.079(6) -0.003(5) -0.011(5) 0.033(7) C31 0.132(10) 0.157(12) 0.136(10) -0.026(9) -0.025(8) 0.085(9) C32 0.127(11) 0.134(11) 0.094(9) 0.007(8) -0.002(8) 0.057(10) C33 0.173(12) 0.196(14) 0.118(9) -0.045(9) -0.038(9) 0.120(11) C34 0.122(9) 0.145(12) 0.072(8) 0.007(7) -0.012(6) 0.046(9) C36 0.164(11) 0.125(11) 0.130(9) 0.016(7) -0.027(8) 0.058(9) C38 0.17(2) 0.097(15) 0.136(14) 0.000 0.000 0.076(14) C40 0.127(10) 0.138(12) 0.093(9) 0.018(9) 0.006(7) 0.045(10) C41 0.227(13) 0.325(13) 0.171(11) -0.046(11) -0.049(10) 0.179(12) C21 0.259(14) 0.325(15) 0.182(13) -0.027(13) -0.041(12) 0.154(13) C43 0.278(17) 0.317(14) 0.155(11) 0.020(11) -0.040(12) 0.150(14) C11 0.296(17) 0.366(16) 0.157(12) 0.003(13) -0.004(13) 0.162(15) C45 0.310(17) 0.387(17) 0.185(14) -0.004(15) -0.024(13) 0.169(15) C23 0.278(17) 0.375(16) 0.193(13) -0.070(13) -0.014(13) 0.132(15) C42 0.098(16) 0.17(2) 0.112(12) 0.000 0.000 0.066(15) C44 0.158(10) 0.112(9) 0.075(7) -0.020(7) -0.018(8) 0.061(8) C46 0.127(10) 0.102(10) 0.109(10) 0.015(8) 0.014(8) 0.040(9) C47 0.169(12) 0.118(11) 0.115(10) 0.017(9) 0.021(8) 0.062(9) C48 0.147(11) 0.125(11) 0.078(9) 0.024(7) 0.020(7) 0.067(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn -2.7473 0.5279 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 1 1 0 2389.86 330.67 -2 1 0 1343.47 325.87 -1 -1 0 1527.95 344.77 2 -1 0 1890.51 303.07 0 -2 0 351.36 216.48 2 0 0 468.95 133.69 -2 2 0 -426.16 155.48 0 2 0 393.56 158.08 2 -2 0 329.17 127.79 -2 0 0 220.28 222.28 1 2 0 387.86 198.98 -3 1 0 -278.77 313.17 3 -1 0 492.55 159.08 -2 3 0 617.84 215.38 -1 -2 0 472.45 341.07 1 -3 0 22.6 372.76 2 1 0 2587.84 358.16 -2 -1 0 2235.68 454.05 -1 3 0 1756.02 359.46 3 -2 0 2182.48 330.37 3 0 0 2589.14 424.26 -3 3 0 2563.64 461.95 0 -3 0 1773.22 519.15 -3 0 0 1381.26 557.74 0 3 0 2384.76 465.35 3 -3 0 2563.64 417.26 3 -4 0 516.15 78.99 2 -4 0 77.99 16.7 2 2 0 108.39 16.6 2 -4 0 104.09 17.4 -4 2 0 99.19 16.3 -4 2 0 101.89 17.3 2 2 0 85.89 17 -2 -2 0 154.58 16.7 4 -2 0 71.59 16.2 -2 4 0 98.79 17.4 -2 4 0 128.79 16.4 4 -2 0 116.69 16.6 3 1 0 71.19 11.8 1 -4 0 83.59 12.3 3 1 0 84.69 12.5 3 1 0 89.39 13.3 -4 3 0 83.39 11.9 -4 3 0 76.29 12.4 1 -4 0 56.59 12.1 -3 -1 0 71.29 12 -1 4 0 64.29 12.2 -3 -1 0 58.59 11.6 -3 -1 0 71.59 12.5 4 0 0 2084.79 351.46 0 -4 0 785.82 617.04 -4 4 0 1811.52 475.25 -4 0 0 608.14 799.42 4 -4 0 1509.65 345.07 0 4 0 1505.35 404.66 -5 1 0 677.43 114.99 -5 1 0 724.03 115.19 -5 1 0 718.93 115.09 4 -5 0 670.93 115.09 4 -5 0 740.33 114.89 1 4 0 817.02 115.39 -1 -4 0 925.01 115.49 5 -1 0 797.32 114.99 -4 5 0 768.02 114.89 5 -1 0 670.13 114.99 5 -1 0 751.02 115.19 -1 -4 0 797.82 115.39 2 3 0 5859.41 865.21 5 -2 0 4820.82 808.42 -3 5 0 5544.45 881.41 -2 -3 0 1503.25 1119.79 2 -5 0 -213.98 675.73 3 2 0 3977.3 622.34 5 -3 0 3605.34 573.54 -2 5 0 4070.19 662.83 -3 -2 0 2431.06 1017.6 5 -3 0 4224.68 597.14 -5 4 0 35.4 8.7 4 1 0 40.5 7.5 4 1 0 17.3 7.7 1 -5 0 52.89 8.5 1 -5 0 49.2 8.7 -1 5 0 23.3 8.3 -4 -1 0 38.6 8 0 -5 0 2545.65 896.31 -5 5 0 2563.14 721.03 5 0 0 3478.55 529.75 5 -5 0 2982.3 528.45 0 5 0 1854.31 572.14 5 -6 0 387.66 55.59 1 5 0 380.86 56.59 -6 1 0 318.27 55.79 -6 1 0 304.17 55.49 -5 6 0 359.36 55.79 6 -1 0 357.66 55.89 6 -1 0 374.16 55.39 6 -1 0 358.16 55.49 -5 6 0 392.46 55.19 4 -6 0 6.4 5.8 4 -6 0 5.4 4.1 -6 2 0 16 6.1 -6 2 0 12.1 4.1 6 -2 0 15.5 6.3 -4 6 0 2.7 6.1 6 -2 0 17.9 4.2 3 -6 0 356.36 56.29 3 3 0 340.97 56.29 -6 3 0 403.96 56.39 -6 3 0 319.67 55.69 3 3 0 385.46 56.49 -3 -3 0 405.26 56.59 -3 6 0 347.17 56.29 4 2 0 9304.47 1457.65 2 -6 0 8639.94 1575.14 -2 6 0 8939.51 1511.35 6 -4 0 9322.87 1450.75 6 -4 0 9134.69 1433.16 -6 5 0 3291.77 929.81 5 1 0 4184.08 685.43 1 -6 0 915.01 993.9 6 -5 0 4112.29 659.63 -1 6 0 3838.72 762.62 -6 6 0 1737.03 263.27 6 0 0 1666.13 263.27 6 0 0 1693.83 263.37 0 -6 0 1888.01 263.67 0 -6 0 1752.12 263.67 6 0 0 1662.33 263.37 0 6 0 1718.63 263.57 -6 0 0 1716.43 263.27 -6 0 0 1764.62 263.37 -6 0 0 1632.34 263.37 -7 1 0 30.9 8.1 -7 1 0 42.8 6.9 7 -1 0 28.3 7.3 -6 7 0 33.4 7.7 7 -1 0 25.3 8.2 7 -1 0 33.9 6.5 5 -7 0 268.17 42.3 -7 2 0 230.08 41.8 5 -7 0 302.77 41.6 -7 2 0 269.37 42.5 7 -2 0 247.58 41.7 7 -2 0 273.27 42.6 -5 7 0 299.87 42.4 4 -7 0 550.84 94.49 -7 3 0 552.44 94.49 3 4 0 746.13 94.59 4 -7 0 613.84 94.09 -7 3 0 528.85 93.99 -3 -4 0 697.13 94.89 -4 7 0 533.85 94.39 -3 -4 0 783.72 95.29 4 3 0 48.4 9.9 3 -7 0 34.4 9.5 3 -7 0 64.69 10.4 -7 4 0 73.29 10.5 4 3 0 48.2 10.1 -7 4 0 33.9 8.3 4 3 0 31.3 9.4 -4 -3 0 53.49 10.4 -3 7 0 63.59 10.2 -4 -3 0 68.49 12.2 2 -7 0 174.48 31.3 2 -7 0 186.88 31.9 -7 5 0 185.78 30.2 -7 5 0 217.58 31.9 5 2 0 203.08 30.7 5 2 0 183.08 31.2 5 2 0 182.58 31.1 -5 -2 0 162.98 31.1 -2 7 0 200.88 31.7 -5 -2 0 181.48 31.5 -5 -2 0 232.68 30.8 6 1 0 3765.82 580.34 1 -7 0 3818.52 580.44 1 -7 0 3985.2 580.44 6 1 0 3797.32 580.24 -6 -1 0 3768.02 580.34 -6 -1 0 3643.74 580.24 7 0 0 478.65 79.59 0 -7 0 560.64 80.19 0 -7 0 540.85 80.19 7 0 0 517.45 79.39 7 0 0 457.75 79.49 -7 7 0 517.65 79.49 -7 0 0 530.25 79.59 -7 0 0 534.35 79.39 0 7 0 527.85 80.09 -7 0 0 518.95 79.59 7 -8 0 1018.4 146.39 1 7 0 978.9 146.89 -8 1 0 901.81 146.59 -8 1 0 900.11 146.39 -1 -7 0 944.61 146.99 -1 -7 0 1025 147.09 8 -1 0 955 146.39 8 -1 0 962.4 146.39 -7 8 0 951.2 146.59 8 -1 0 933.31 146.69 -8 2 0 -9.7 6.5 6 -8 0 -2.5 6 6 -8 0 6.4 3.6 2 6 0 14.5 5.6 2 6 0 6.3 7.7 -8 2 0 3.6 4.5 -2 -6 0 -1.4 9.6 -2 -6 0 8.7 7.8 -6 8 0 4.1 6.4 8 -2 0 -4.2 6.6 8 -2 0 5.1 4.6 3 5 0 2095.39 328.17 5 -8 0 2172.18 328.07 5 -8 0 2201.88 327.97 -8 3 0 2099.69 327.97 -8 3 0 2249.77 328.17 3 5 0 2242.58 328.07 -3 -5 0 2208.28 328.37 -3 -5 0 2078.99 328.27 8 -3 0 1897.61 327.87 -5 8 0 2215.58 328.17 -8 4 0 1719.03 255.37 4 -8 0 1674.73 255.27 4 4 0 1660.33 255.27 4 4 0 1679.73 255.27 4 4 0 1720.93 255.27 -8 4 0 1645.14 255.07 4 -8 0 1714.13 255.17 -4 8 0 1671.73 255.27 -4 -4 0 1592.04 255.37 -4 -4 0 1594.44 255.47 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-7 62.89 9.2 -4 -2 -7 27.7 10.4 -2 6 -7 45.5 9.7 -2 6 -7 37.4 10.6 4 2 7 35.5 10.3 -6 4 7 58.99 7.8 -6 4 7 32.4 9.7 4 2 7 15 11 4 2 7 44.6 9.7 2 -6 7 42.5 10.5 -4 -1 -7 33.9 8.1 -1 5 -7 6.3 7.2 -1 5 -7 25.8 8.2 -4 -1 -7 30.1 6.5 -4 -1 -7 32.6 8.6 1 -5 7 26.5 7.9 -5 4 7 18.1 5.2 4 1 7 26.5 8.9 4 1 7 22.5 8 -5 4 7 50.49 7.8 4 1 7 0.5 6.8 0 4 -7 1974 289.87 0 4 -7 1862.21 289.87 -4 0 -7 1910.71 289.87 -4 0 -7 1932.71 289.97 -4 0 -7 1857.71 290.07 0 -4 7 1919.01 289.87 -4 4 7 1953.4 289.87 4 0 7 1876.31 289.97 4 0 7 1881.01 290.17 -4 4 7 1872.01 289.77 0 -4 7 1777.42 289.97 4 0 7 1918.51 289.87 -4 1 -7 66.09 17.3 1 3 -7 155.88 18.5 1 3 -7 141.79 18.8 -4 1 -7 97.89 17.2 4 -1 7 179.48 19.5 4 -1 7 84.59 17.3 4 -1 7 188.78 21.2 -3 4 7 69.99 17.4 -3 4 7 84.09 16.7 -1 -3 7 144.59 19 -4 2 -7 139.99 24.2 2 2 -7 114.89 23.4 2 -4 -7 138.09 22.9 2 -4 -7 138.29 23.3 2 2 -7 188.58 23.7 -2 4 7 106.09 23 -2 -2 7 212.98 24.1 -2 -2 7 193.28 23.5 4 -2 7 115.29 22.9 -2 4 7 137.79 23.8 1 -4 -7 110.89 22 -4 3 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-7 -3 26 5.3 18.2 -10 8 -26 -1 10 -2 10 26 10 14.7 -8 -2 26 2.3 17.9 0 0 27 -21.4 14.8 -1 0 -27 -2.1 8.1 0 1 -27 8.5 12.3 -1 1 27 2.1 13.4 0 -1 27 -6.7 13.4 1 0 27 6.3 12.4 -1 1 -27 1.3 8.6 -1 0 27 -6.6 14 0 1 27 18.8 15.8 1 -1 27 0.6 13 -1 2 -27 114.89 17.7 -1 -1 -27 113.29 17.3 -2 1 27 74.09 21.2 1 1 27 70.09 20.8 1 -2 27 62.29 20.4 -2 -1 -27 -5.9 8.3 -1 3 -27 -1.8 8.6 2 1 27 17.1 12.5 1 -3 27 -25.4 14.1 -3 2 27 -1.1 13 -2 0 -27 11.5 8.9 0 -2 27 1.7 13.7 2 0 27 18.6 13.1 -2 2 27 18.7 15.3 -2 1 -27 117.19 17.3 2 -1 27 104.89 20.7 -1 -1 27 23.8 20.3 -1 2 27 93.79 20.9 -2 2 -27 7.5 9.1 0 2 27 13 15 -2 0 27 -7.4 13.1 2 -2 27 -0.3 13.1 -1 -2 -27 10.5 8.8 -2 3 -27 -0.6 9 -3 1 27 -11.3 13.6 2 -3 27 -8.3 12.8 1 2 27 -0.1 14.3 -2 4 -27 29.1 10.6 -2 -2 -27 40.7 10.1 -4 2 27 21.9 14.8 2 2 27 24.9 13.9 2 -4 27 24.3 15.6 -3 -2 -27 13.5 9 -2 5 -27 9.7 9.4 -5 3 27 -0.1 13.3 2 -5 27 10.4 15.2 3 2 27 1 11.7 -3 -1 -27 6.7 8.7 -1 4 -27 -9.7 8.6 -4 3 27 -7.3 13.4 1 -4 27 11.8 14.3 3 1 27 2.1 12 -3 0 -27 -9.2 8.7 0 -3 27 -2.7 14.8 -3 3 27 -6.2 15 3 0 27 -2.8 13.6 -3 1 -27 0.1 9.4 -2 3 27 -1.1 12.9 -1 -2 27 24.9 15.2 3 -1 27 12.1 14.7 -3 2 -27 8.6 9.3 -1 3 27 -0.2 15.2 3 -2 27 -0.4 12.9 -2 -1 27 9.3 14.4 -3 3 -27 10.1 9.5 0 3 27 4.7 12.1 3 -3 27 0 13 -3 0 27 5.6 14.4 -3 4 -27 17.9 10.1 -4 1 27 21 15.1 1 3 27 0.8 15.1 3 -4 27 30.3 16.1 -3 5 -27 -3.7 9.5 -2 -3 -27 0.6 8.5 -5 2 27 13.6 14.2 3 -5 27 -7 15.3 2 3 27 6 14.6 -3 6 -27 8.6 9.7 -3 -3 -27 -0.1 8.8 -6 3 27 -12.9 14.2 3 3 27 -20.5 13.2 3 -6 27 4.3 15.7 -3 7 -27 34.3 10.8 -4 -3 -27 32.6 10.2 3 -7 27 1 16.9 4 3 27 1.9 14.3 -7 4 27 15.6 15.3 -4 -2 -27 -13.9 8.8 -2 6 -27 1.9 9.4 -6 4 27 16.8 14.8 2 -6 27 -10.2 15 4 2 27 7.5 11.9 -4 -1 -27 7.1 9.3 -1 5 -27 18.3 9.4 4 1 27 2.9 12 -5 4 27 27.1 15.1 1 -5 27 45.5 16.5 -4 0 -27 24.9 9.9 0 -4 27 -9.4 15.1 4 0 27 10.9 12.2 -4 4 27 1.4 14.1 -4 1 -27 28.3 10.6 -3 4 27 22.6 14.7 -1 -3 27 -1.1 15.2 4 -1 27 38.8 13.8 -4 2 -27 23.8 9.9 4 -2 27 12.1 13 -2 4 27 4.8 15.4 -2 -2 27 4.4 15 -4 3 -27 -7.2 9.4 4 -3 27 11.1 12.8 -3 -1 27 -11.2 14.4 -1 4 27 14.7 13.2 -4 4 -27 21.3 10.8 -4 0 27 16.1 15.5 4 -4 27 35.6 16.3 0 4 27 23.2 15.6 -4 5 -27 -9.2 9.7 1 4 27 -0.4 11.5 -5 1 27 7 14.6 4 -5 27 -1.9 14.2 -4 6 -27 -1.3 9.7 -6 2 27 4.8 14.4 2 4 27 6.8 11.7 4 -6 27 12.3 16.2 -4 7 -27 2.7 9.8 3 4 27 8 13 -7 3 27 -5.6 14.5 4 -7 27 -0.4 15.2 -4 8 -27 5.9 10.6 -8 4 27 7.3 15 4 4 27 17.3 13.6 -5 -3 -27 -4.2 9.4 -3 8 -27 -8.8 9.9 5 3 27 -22.7 13.9 -8 5 27 -24.7 14 -2 7 -27 1.5 9.6 -5 -2 -27 18.3 9.9 2 -7 27 9.2 16.8 5 2 27 10.1 13.5 -7 5 27 -12 13.8 -5 -1 -27 21.2 9.9 -1 6 -27 28.5 10.2 -6 5 27 21.2 14.1 1 -6 27 13 16.5 5 1 27 16.5 12.7 -5 0 -27 1 9.3 0 -5 27 25.8 16 5 0 27 4.5 11.6 -5 5 27 1.6 16 -5 1 -27 1.8 10.2 -4 5 27 19.4 15.8 5 -1 27 9.8 12.2 -1 -4 27 2.7 15.4 -5 2 -27 -3.2 9.8 -3 5 27 6.6 15.4 5 -2 27 8.5 12.8 -2 -3 27 17.8 14.8 -5 3 -27 -4.1 9.9 -2 5 27 -2.7 12.4 -3 -2 27 -15.2 14.6 5 -3 27 -11.8 14.6 -5 4 -27 -4.2 9.7 -1 5 27 -3 14.7 5 -4 27 0.5 14.8 -4 -1 27 11.5 15.3 -5 5 -27 1.6 10 5 -5 27 18.8 14.1 -5 0 27 6.2 14.9 0 5 27 7.3 12.3 -5 6 -27 -8.8 10.4 5 -6 27 12.1 16.3 -6 1 27 14.1 15 1 5 27 -2.9 14.6 -5 7 -27 3 9.8 -7 2 27 -9 13.8 2 5 27 -4.7 12.9 -5 8 -27 1.3 10 -8 3 27 -1.6 14.9 3 5 27 -3.4 15.8 3 5 27 6.2 12.4 6 2 27 26.6 15 -6 -1 -27 7.6 10 -1 7 -27 6.2 9.5 -7 6 27 15 15.4 1 -7 27 -1.2 17 6 1 27 -16.4 13.9 -6 0 -27 -8.5 9.3 -6 6 27 1.7 14.4 0 -6 27 -15.9 15.7 6 0 27 14.5 14 -6 1 -27 7.3 9.6 -5 6 27 1.6 13.6 -1 -5 27 -0.7 15.7 6 -1 27 -8.2 13.8 -6 2 -27 4.8 9.7 -2 -4 27 -14.8 14.9 6 -2 27 -0.6 14.6 -4 6 27 3 13.1 -6 3 -27 -9 9.7 -3 -3 27 20.5 15.3 6 -3 27 3.9 13.7 -3 6 27 9.5 13.2 -6 4 -27 2.9 10.1 -2 6 27 -9.3 15.2 6 -4 27 -8.5 13.2 -4 -2 27 -3.8 14.9 -6 5 -27 17.2 11.1 -5 -1 27 4.4 15.6 6 -5 27 31.1 16.3 -1 6 27 1.8 12.2 -6 6 -27 7.5 10.2 0 6 27 5.9 14.9 6 -6 27 12.4 26.7 -6 0 27 -1.1 15.2 -6 7 -27 -5.2 10.4 -7 1 27 -13.1 14.8 1 6 27 -0.6 11.2 2 6 27 4 11.8 -7 0 -27 7.3 9.6 -7 7 27 2.2 15.6 0 -7 27 -5.8 16.5 7 0 27 1.8 12.9 -7 1 -27 3.2 10.1 7 -1 27 -6.8 12.6 -6 7 27 5.9 16.2 -1 -6 27 20.2 16.3 -7 2 -27 -4.2 10.2 -2 -5 27 26.5 15.9 7 -2 27 4.5 12.7 -5 7 27 -3.5 15.6 -7 3 -27 13.2 10.4 -4 7 27 0.9 15.9 7 -3 27 -5 14.3 -3 -4 27 20.1 16.3 -7 4 -27 33.1 11.2 7 -4 27 18.6 15.7 -4 -3 27 14.9 16.3 -3 7 27 13.2 15.4 -7 5 -27 11.9 10.2 -2 7 27 1.9 12.6 -5 -2 27 -7.9 15.4 -7 6 -27 3.5 10.2 -6 -1 27 -1.6 15.4 -1 7 27 13.1 15.1 -7 7 -27 1.3 10.3 0 7 27 -7 10.9 -7 0 27 10 16 8 -2 27 15.5 15.1 -8 3 -27 1 10.5 -5 8 27 5.2 14.7 8 -3 27 -21 24 -3 -5 27 1.6 16.7 -8 4 -27 -11.1 10.4 -4 8 27 -3.6 14.8 -4 -4 27 -4.6 16.6 -8 5 -27 0.6 9.7 -3 8 27 -3.2 15.5 -5 -3 27 -23.1 16.3 -2 8 27 -1 13.2 0 0 28 19.4 14.7 0 -1 28 -3.6 15.3 -1 1 28 11.5 14.5 1 0 28 24.5 14 0 1 28 -2.9 14.3 1 -1 28 6 13.1 -1 0 28 19.6 15.1 -2 1 28 6.2 16.4 1 -2 28 0 13.2 1 1 28 15.1 13.5 -3 2 28 7 16.3 2 1 28 9.2 15.6 1 -3 28 20.7 16.5 2 0 28 -10.3 15.1 0 -2 28 -14.9 14.1 -2 2 28 -15.6 16.2 -2 1 -28 17.2 14.8 -1 2 28 -8.1 12.3 2 -1 28 3.5 15.4 -1 -1 28 -10.2 15 -2 2 -28 10.8 12.9 2 -2 28 23.5 15.3 -2 0 28 -1.6 13.7 0 2 28 -8.8 14.7 -2 3 -28 3.6 11.6 2 -3 28 -2 13.3 1 2 28 5.8 12.1 -3 1 28 11.3 14.5 -2 4 -28 19.8 11 2 -4 28 -4.7 17 -4 2 28 5.5 14.5 2 2 28 20.9 15 -3 -1 -28 -1.3 10.6 3 1 28 -7.1 14.5 -4 3 28 10 16.9 1 -4 28 1.6 15.9 -3 0 -28 84.39 15.2 0 -3 28 64.99 20 -3 3 28 72.49 21.5 3 0 28 56.59 20 -3 1 -28 28.3 9.5 -2 3 28 -8 13.9 3 -1 28 1.8 15.4 -1 -2 28 28.4 16.2 -3 2 -28 15.4 9.4 -2 -1 28 -14.7 13.9 -1 3 28 13.2 12.5 3 -2 28 7.6 15.6 -3 3 -28 81.99 15.1 -3 0 28 70.69 19.7 0 3 28 67.99 20.3 3 -3 28 57.19 18.6 -3 4 -28 15.3 9.7 3 -4 28 8.7 15.8 1 3 28 -10.2 12.9 -4 1 28 -20.1 14.5 4 0 28 6.2 14.7 -4 1 -28 6.2 9.2 -3 4 28 -3.2 13 -1 -3 28 5.1 15.4 4 -1 28 18.2 15.5 -4 2 -28 27.4 10.3 -2 4 28 7.1 12.3 -2 -2 28 15.4 16 4 -2 28 22.8 16.6 -4 3 -28 3.8 9.5 4 -3 28 -1.1 13.7 -3 -1 28 3.8 15 -1 4 28 2.9 15.2 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Zn1 N2 89.8(3) . . ? N1 Zn1 N2 89.8(3) . 10_557 ? N1 Zn1 N3 162.7(5) . . ? N1 Zn1 N4 99.5(6) . . ? N2 Zn1 N2 166.6(4) . 10_557 ? N2 Zn1 N3 88.2(3) . . ? N2 Zn1 N3 88.2(3) 10_557 . ? N2 Zn1 N4 96.6(2) 10_557 . ? N2 Zn1 N4 96.6(2) . . ? N3 Zn1 N4 97.8(6) . . ? C15 O3 C33 121.9(13) . . ? C1 N1 Zn1 127.5(7) . . ? C1 N1 Zn1 127.5(7) 10_557 . ? C1 N1 C1 103.2(13) . 10_557 ? C10 N2 Zn1 126.3(8) . . ? C10 N2 C20 109.4(9) . . ? C20 N2 Zn1 124.3(7) . . ? C12 N3 Zn1 122.8(7) . . ? C12 N3 Zn1 122.8(7) 10_557 . ? C12 N3 C12 109.4(14) 10_557 . ? C29 N4 Zn1 120.8(15) . . ? C38 N4 Zn1 125.2(15) . . ? C38 N4 C29 114.0(16) . . ? C6 N5 C6 113.0(19) 3_665 . ? C5 N6 C2 114.5(14) . 3_665 ? C47 N6 C2 118.1(12) . 3_665 ? C47 N6 C5 127.1(14) . . ? C28 N7 C27 118.5(14) . . ? C28 N7 C31 122.0(13) . . ? C31 N7 C27 116.6(11) . . ? N1 C1 C18 123.2(10) . . ? N1 C1 C30 112.3(10) . . ? C18 C1 C30 124.4(9) . . ? N6 C2 H2A 108.8 2_655 . ? N6 C2 H2B 108.8 2_655 . ? H2A C2 H2B 107.7 . . ? C15 C2 N6 113.6(11) . 2_655 ? C15 C2 H2A 108.8 . . ? C15 C2 H2B 108.8 . . ? C14 C3 H3 120.7 . . ? C16 C3 H3 120.7 . . ? C16 C3 C14 118.5(12) . . ? C6 C4 C22 124(3) . . ? C6 C4 C42 125(3) . . ? C42 C4 C22 111.6(19) . . ? O1 C5 N6 126.7(19) . . ? O1 C5 C41 118.9(18) . . ? N6 C5 C41 114.4(19) . . ? N5 C6 N5 127.0(19) 2_655 . ? N5 C6 C4 118(4) 2_655 . ? C4 C6 N5 115(4) . . ? C13 C7 H7 119.4 . . ? C26 C7 H7 119.4 . . ? C26 C7 C13 121.2(13) . . ? C10 C8 C26 112.8(11) . . ? C12 C8 C10 126.3(10) . . ? C12 C8 C26 120.8(12) . . ? N2 C10 C8 124.9(10) . . ? N2 C10 C48 106.7(11) . . ? C8 C10 C48 128.3(11) . . ? N3 C12 C8 127.7(12) . . ? N3 C12 C36 110.0(11) . . ? C8 C12 C36 122.1(12) . . ? C7 C13 H13 121.3 . . ? C46 C13 C7 117.3(13) . . ? C46 C13 H13 121.3 . . ? C3 C14 C27 115.3(13) . . ? C32 C14 C3 117.3(11) . . ? C32 C14 C27 126.9(13) . . ? O3 C15 C2 114.2(15) . . ? O3 C15 H15A 108.7 . . ? O3 C15 H15B 108.7 . . ? C2 C15 H15A 108.7 . . ? C2 C15 H15B 108.7 . . ? H15A C15 H15B 107.6 . . ? C3 C16 H16 119.0 . . ? C24 C16 C3 122.1(11) . . ? C24 C16 H16 119.0 . . ? C35 C17 C39 120.0 . . ? C35 C17 C28 123.1(11) . . ? C39 C17 C28 116.8(11) . . ? C17 C35 H35 120.0 . . ? C9 C35 C17 120.0 . . ? C9 C35 H35 120.0 . . ? C35 C9 H9 120.0 . . ? C37 C9 C35 120.0 . . ? C37 C9 H9 120.0 . . ? C9 C37 H37 120.0 . . ? C19 C37 C9 120.0 . . ? C19 C37 H37 120.0 . . ? C37 C19 H19 120.0 . . ? C37 C19 C39 120.0 . . ? C39 C19 H19 120.0 . . ? C17 C39 H39 120.0 . . ? C19 C39 C17 120.0 . . ? C19 C39 H39 120.0 . . ? C1 C18 C24 114.4(10) . . ? C20 C18 C1 125.4(9) . . ? C20 C18 C24 120.0(10) . . ? N2 C20 C18 127.8(10) . . ? N2 C20 C34 107.4(11) . . ? C18 C20 C34 124.7(12) . . ? C4 C22 H22 118.5 . . ? C38 C22 C4 123(2) . . ? C38 C22 H22 118.5 . . ? C16 C24 C18 121.6(12) . . ? C16 C24 C44 121.6(11) . . ? C44 C24 C18 116.8(13) . . ? C26 C25 H25 121.9 . . ? C40 C25 H25 121.9 . . ? C40 C25 C26 116.2(12) . . ? C7 C26 C8 119.0(14) . . ? C7 C26 C25 119.5(13) . . ? C25 C26 C8 121.4(13) . . ? N7 C27 C14 111.7(11) . . ? N7 C27 H27A 109.3 . . ? N7 C27 H27B 109.3 . . ? C14 C27 H27A 109.3 . . ? C14 C27 H27B 109.3 . . ? H27A C27 H27B 107.9 . . ? O2 C28 N7 120.5(16) . . ? O2 C28 C17 116.8(16) . . ? N7 C28 C17 122.6(16) . . ? N4 C29 H29 121.3 . . ? C42 C29 N4 117.5(18) . . ? C42 C29 H29 121.3 . . ? C1 C30 H30 127.0 . . ? C30 C30 C1 106.0(5) 10_557 . ? C30 C30 H30 127.0 10_557 . ? N7 C31 H31A 109.9 . . ? N7 C31 H31B 109.9 . . ? N7 C31 C33 108.9(11) . . ? H31A C31 H31B 108.3 . . ? C33 C31 H31A 109.9 . . ? C33 C31 H31B 109.9 . . ? C14 C32 H32 117.5 . . ? C14 C32 C44 124.9(12) . . ? C44 C32 H32 117.5 . . ? O3 C33 C31 109.7(11) . . ? O3 C33 H33 125.2 . . ? C31 C33 H33 125.2 . . ? C20 C34 H34 127.2 . . ? C48 C34 C20 105.6(11) . . ? C48 C34 H34 127.2 . . ? C12 C36 H36 127.4 . . ? C36 C36 C12 105.3(7) 10_557 . ? C36 C36 H36 127.4 10_557 . ? N4 C38 H38 115.9 . . ? C22 C38 N4 128.3(19) . . ? C22 C38 H38 115.9 . . ? C25 C40 H40 117.1 . . ? C46 C40 C25 125.8(13) . . ? C46 C40 H40 117.1 . . ? C21 C41 C5 126.8(14) . . ? C21 C41 C23 120.0 . . ? C23 C41 C5 111.8(14) . . ? C41 C21 H21 120.0 . . ? C41 C21 C43 120.0 . . ? C43 C21 H21 120.0 . . ? C21 C43 H43 120.0 . . ? C21 C43 C11 120.0 . . ? C11 C43 H43 120.0 . . ? C43 C11 H11 120.0 . . ? C45 C11 C43 120.0 . . ? C45 C11 H11 120.0 . . ? C11 C45 H45 120.0 . . ? C23 C45 C11 120.0 . . ? C23 C45 H45 120.0 . . ? C41 C23 H23 120.0 . . ? C45 C23 C41 120.0 . . ? C45 C23 H23 120.0 . . ? C4 C42 C29 125.7(19) . . ? C4 C42 H42 117.1 . . ? C29 C42 H42 117.1 . . ? C24 C44 H44 122.6 . . ? C32 C44 C24 114.8(12) . . ? C32 C44 H44 122.6 . . ? C13 C46 C47 120.5(14) . . ? C40 C46 C13 119.7(12) . . ? C40 C46 C47 119.8(14) . . ? N6 C47 C46 114.2(11) . . ? N6 C47 H47A 108.7 . . ? N6 C47 H47B 108.7 . . ? C46 C47 H47A 108.7 . . ? C46 C47 H47B 108.7 . . ? H47A C47 H47B 107.6 . . ? C10 C48 H48 124.6 . . ? C34 C48 C10 110.9(11) . . ? C34 C48 H48 124.6 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 N1 2.025(14) . ? Zn1 N2 2.073(8) . ? Zn1 N2 2.073(8) 10_557 ? Zn1 N3 2.151(13) . ? Zn1 N4 2.163(15) . ? O1 C5 1.19(2) . ? O2 C28 1.235(16) . ? O3 C15 1.393(16) . ? O3 C33 1.410(15) . ? N1 C1 1.376(12) . ? N1 C1 1.376(12) 10_557 ? N2 C10 1.356(12) . ? N2 C20 1.365(12) . ? N3 C12 1.310(13) 10_557 ? N3 C12 1.310(13) . ? N4 C29 1.428(19) . ? N4 C38 1.387(19) . ? N5 C6 1.39(2) . ? N5 C6 1.32(2) 3_665 ? N6 C2 1.480(15) 3_665 ? N6 C5 1.426(18) . ? N6 C47 1.428(14) . ? N7 C27 1.477(14) . ? N7 C28 1.359(17) . ? N7 C31 1.407(13) . ? C1 C18 1.423(14) . ? C1 C30 1.450(13) . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C2 C15 1.464(19) . ? C3 H3 0.9500 . ? C3 C14 1.437(16) . ? C3 C16 1.366(14) . ? C4 C6 1.34(2) . ? C4 C22 1.44(2) . ? C4 C42 1.39(2) . ? C5 C41 1.46(2) . ? C7 H7 0.9500 . ? C7 C13 1.449(16) . ? C7 C26 1.392(15) . ? C8 C10 1.412(14) . ? C8 C12 1.381(14) . ? C8 C26 1.506(16) . ? C10 C48 1.425(15) . ? C12 C36 1.413(15) . ? C13 H13 0.9500 . ? C13 C46 1.414(16) . ? C14 C27 1.541(16) . ? C14 C32 1.373(15) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C16 H16 0.9500 . ? C16 C24 1.352(14) . ? C17 C35 1.3900 . ? C17 C39 1.3900 . ? C17 C28 1.426(18) . ? C35 H35 0.9500 . ? C35 C9 1.3900 . ? C9 H9 0.9500 . ? C9 C37 1.3900 . ? C37 H37 0.9500 . ? C37 C19 1.3900 . ? C19 H19 0.9500 . ? C19 C39 1.3900 . ? C39 H39 0.9500 . ? C18 C20 1.380(13) . ? C18 C24 1.543(12) . ? C20 C34 1.468(14) . ? C22 H22 0.9500 . ? C22 C38 1.25(2) . ? C24 C44 1.434(15) . ? C25 H25 0.9500 . ? C25 C26 1.454(16) . ? C25 C40 1.383(15) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C29 H29 0.9500 . ? C29 C42 1.42(2) . ? C30 C30 1.359(17) 10_557 ? C30 H30 0.9500 . ? C31 H31A 0.9900 . ? C31 H31B 0.9900 . ? C31 C33 1.619(16) . ? C32 H32 0.9500 . ? C32 C44 1.382(15) . ? C33 H33 0.9500 . ? C34 H34 0.9500 . ? C34 C48 1.316(14) . ? C36 C36 1.39(2) 10_557 ? C36 H36 0.9500 . ? C38 H38 0.9500 . ? C40 H40 0.9500 . ? C40 C46 1.350(16) . ? C41 C21 1.3900 . ? C41 C23 1.3900 . ? C21 H21 0.9500 . ? C21 C43 1.3900 . ? C43 H43 0.9500 . ? C43 C11 1.3900 . ? C11 H11 0.9500 . ? C11 C45 1.3900 . ? C45 H45 0.9500 . ? C45 C23 1.3900 . ? C23 H23 0.9500 . ? C42 H42 0.9500 . ? C44 H44 0.9500 . ? C46 C47 1.489(16) . ? C47 H47A 0.9900 . ? C47 H47B 0.9900 . ? C48 H48 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Zn1 N1 C1 C18 -16.6(16) . . . . ? Zn1 N1 C1 C30 162.2(8) . . . . ? Zn1 N2 C10 C8 -2.3(15) . . . . ? Zn1 N2 C10 C48 178.7(7) . . . . ? Zn1 N2 C20 C18 -0.9(14) . . . . ? Zn1 N2 C20 C34 -178.2(7) . . . . ? Zn1 N3 C12 C8 19.7(17) . . . . ? Zn1 N3 C12 C36 -155.7(8) . . . . ? Zn1 N4 C29 C42 180.0 . . . . ? Zn1 N4 C38 C22 180.0 . . . . ? O1 C5 C41 C21 105(2) . . . . ? O1 C5 C41 C23 -61(3) . . . . ? N1 C1 C18 C20 4.0(17) . . . . ? N1 C1 C18 C24 -171.5(11) . . . . ? N1 C1 C30 C30 2.0(9) . . . 10_557 ? N2 C10 C48 C34 -1.2(13) . . . . ? N2 C20 C34 C48 -0.5(12) . . . . ? N3 C12 C36 C36 0.1(10) . . . 10_557 ? N4 C29 C42 C4 0.0 . . . . ? N6 C2 C15 O3 -54.5(19) 2_655 . . . ? N6 C5 C41 C21 -74(2) . . . . ? N6 C5 C41 C23 119.5(12) . . . . ? N7 C31 C33 O3 174.6(11) . . . . ? C1 N1 C1 C18 178.0(6) 10_557 . . . ? C1 N1 C1 C30 -3.1(15) 10_557 . . . ? C1 C18 C20 N2 5.2(18) . . . . ? C1 C18 C20 C34 -178.0(10) . . . . ? C1 C18 C24 C16 56.8(14) . . . . ? C1 C18 C24 C44 -123.9(11) . . . . ? C2 N6 C5 O1 -4(3) 3_665 . . . ? C2 N6 C5 C41 175.0(13) 3_665 . . . ? C2 N6 C47 C46 60.9(15) 3_665 . . . ? C3 C14 C27 N7 169.7(11) . . . . ? C3 C14 C32 C44 8.3(17) . . . . ? C3 C16 C24 C18 173.8(11) . . . . ? C3 C16 C24 C44 -5.5(18) . . . . ? C4 C22 C38 N4 0.0 . . . . ? C5 N6 C47 C46 -124.6(15) . . . . ? C5 C41 C21 C43 -165.0(19) . . . . ? C5 C41 C23 C45 167.1(17) . . . . ? C6 N5 C6 N5 0.0 3_665 . . 2_655 ? C6 N5 C6 C4 180.0 3_665 . . . ? C6 C4 C22 C38 180.0 . . . . ? C6 C4 C42 C29 180.0 . . . . ? C7 C13 C46 C40 -3.9(19) . . . . ? C7 C13 C46 C47 174.7(12) . . . . ? C8 C10 C48 C34 179.9(11) . . . . ? C8 C12 C36 C36 -175.7(9) . . . 10_557 ? C10 N2 C20 C18 177.0(10) . . . . ? C10 N2 C20 C34 -0.2(11) . . . . ? C10 C8 C12 N3 -3(2) . . . . ? C10 C8 C12 C36 171.6(11) . . . . ? C10 C8 C26 C7 118.9(12) . . . . ? C10 C8 C26 C25 -56.7(14) . . . . ? C12 N3 C12 C8 175.3(7) 10_557 . . . ? C12 N3 C12 C36 -0.1(17) 10_557 . . . ? C12 C8 C10 N2 -6.9(18) . . . . ? C12 C8 C10 C48 171.8(11) . . . . ? C12 C8 C26 C7 -63.5(15) . . . . ? C12 C8 C26 C25 120.8(13) . . . . ? C13 C7 C26 C8 178.5(11) . . . . ? C13 C7 C26 C25 -5.7(18) . . . . ? C13 C46 C47 N6 37.1(17) . . . . ? C14 C3 C16 C24 8.0(17) . . . . ? C14 C32 C44 C24 -5.6(16) . . . . ? C15 O3 C33 C31 -77.8(15) . . . . ? C16 C3 C14 C27 178.0(11) . . . . ? C16 C3 C14 C32 -9.1(16) . . . . ? C16 C24 C44 C32 3.9(16) . . . . ? C17 C35 C9 C37 0.0 . . . . ? C35 C17 C39 C19 0.0 . . . . ? C35 C17 C28 O2 119.6(14) . . . . ? C35 C17 C28 N7 -56.0(17) . . . . ? C35 C9 C37 C19 0.0 . . . . ? C9 C37 C19 C39 0.0 . . . . ? C37 C19 C39 C17 0.0 . . . . ? C39 C17 C35 C9 0.0 . . . . ? C39 C17 C28 O2 -64.3(15) . . . . ? C39 C17 C28 N7 120.1(12) . . . . ? C18 C1 C30 C30 -179.2(9) . . . 10_557 ? C18 C20 C34 C48 -177.8(11) . . . . ? C18 C24 C44 C32 -175.4(10) . . . . ? C20 N2 C10 C8 179.8(10) . . . . ? C20 N2 C10 C48 0.8(11) . . . . ? C20 C18 C24 C16 -119.0(12) . . . . ? C20 C18 C24 C44 60.3(14) . . . . ? C20 C34 C48 C10 1.0(14) . . . . ? C22 C4 C6 N5 0.0 . . . 2_655 ? C22 C4 C6 N5 180.0 . . . . ? C22 C4 C42 C29 0.0 . . . . ? C24 C18 C20 N2 -179.6(11) . . . . ? C24 C18 C20 C34 -2.8(16) . . . . ? C25 C40 C46 C13 2(2) . . . . ? C25 C40 C46 C47 -176.7(12) . . . . ? C26 C7 C13 C46 6.0(18) . . . . ? C26 C8 C10 N2 170.5(10) . . . . ? C26 C8 C10 C48 -10.8(17) . . . . ? C26 C8 C12 N3 179.5(12) . . . . ? C26 C8 C12 C36 -5.6(18) . . . . ? C26 C25 C40 C46 -1.4(18) . . . . ? C27 N7 C28 O2 5(2) . . . . ? C27 N7 C28 C17 -179.9(11) . . . . ? C27 N7 C31 C33 -79.8(13) . . . . ? C27 C14 C32 C44 -179.6(11) . . . . ? C28 N7 C27 C14 -90.4(14) . . . . ? C28 N7 C31 C33 120.0(13) . . . . ? C28 C17 C35 C9 176.0(13) . . . . ? C28 C17 C39 C19 -176.2(12) . . . . ? C29 N4 C38 C22 0.0 . . . . ? C30 C1 C18 C20 -174.7(10) . . . . ? C30 C1 C18 C24 9.8(16) . . . . ? C31 N7 C27 C14 108.7(12) . . . . ? C31 N7 C28 O2 164.5(13) . . . . ? C31 N7 C28 C17 -20(2) . . . . ? C32 C14 C27 N7 -2.5(18) . . . . ? C33 O3 C15 C2 -149.4(12) . . . . ? C38 N4 C29 C42 0.0 . . . . ? C40 C25 C26 C7 3.3(16) . . . . ? C40 C25 C26 C8 179.0(11) . . . . ? C40 C46 C47 N6 -144.3(12) . . . . ? C41 C21 C43 C11 0.0 . . . . ? C21 C41 C23 C45 0.0 . . . . ? C21 C43 C11 C45 0.0 . . . . ? C43 C11 C45 C23 0.0 . . . . ? C11 C45 C23 C41 0.0 . . . . ? C23 C41 C21 C43 0.0 . . . . ? C42 C4 C6 N5 180.0 . . . 2_655 ? C42 C4 C6 N5 0.0 . . . . ? C42 C4 C22 C38 0.0 . . . . ? C47 N6 C5 O1 -179(2) . . . . ? C47 N6 C5 C41 0(2) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.012 -0.337 -0.433 8156.5 2507.2 '42 CHCl3'