#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2003063.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2003063_Fobs loop_ _publ_author_name 'Iwasaki, Fujiko' 'Yoshikawa, Joseph H.' 'Yamamoto, Hajime' 'Kan-nari, Eiji' 'Takada, Kiwamu' 'Yasui, Masanori' 'Ishida, Takayuki' 'Nogami, Takashi' _publ_section_title ; TEMPO radicals showing magnetic interactions. I. 4-(4-Halobenzylideneamino)TEMPO and related compounds ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 231 _journal_page_last 245 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _exptl_crystal_F_000 700.00 _reflns_d_resolution_high 0.7686 _[local]_cod_data_source_file oa00193sup6.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title 4-Br-Ph-TEMPO _shelx_refln_list_code 4 _shelx_f_calc_maximum 187.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 780.09 556.39 10.13 o 2 0 0 5572.05 5072.03 39.28 o 3 0 0 9663.72 9091.55 64.06 o 4 0 0 3228.32 3437.69 47.01 o 5 0 0 4.59 6.30 16.63 o 6 0 0 181.73 179.87 22.10 o 7 0 0 125.62 88.38 25.41 o 8 0 0 25.75 30.78 42.80 o 9 0 0 8.38 -2.87 47.50 o 1 1 0 1540.52 1488.00 13.95 o 2 1 0 171.61 149.21 12.35 o 3 1 0 914.14 927.18 23.75 o 4 1 0 895.69 960.96 29.31 o 5 1 0 36.64 20.75 23.75 o 6 1 0 0.63 22.06 20.23 o 7 1 0 25.76 38.08 24.35 o 8 1 0 7.36 -42.06 42.06 o 9 1 0 0.05 -10.88 48.59 o 1 2 0 20340.25 18704.43 102.57 o 2 2 0 11851.66 11557.83 57.07 o 3 2 0 444.60 419.06 18.99 o 4 2 0 2032.59 1993.69 37.27 o 5 2 0 332.90 297.95 28.31 o 6 2 0 32.10 23.83 20.89 o 7 2 0 1.24 11.01 34.74 o 8 2 0 34.86 55.24 29.23 o 9 2 0 7.14 -3.62 48.53 o 1 3 0 13193.16 12536.97 53.65 o 2 3 0 4.52 4.72 10.51 o 3 3 0 17.85 26.93 10.04 o 4 3 0 167.31 172.24 14.50 o 5 3 0 217.90 217.96 18.32 o 6 3 0 4.57 -21.97 28.04 o 7 3 0 36.29 33.60 24.47 o 8 3 0 0.79 21.26 40.64 o 9 3 0 3.19 -47.48 47.48 o 0 4 0 540.63 532.82 12.89 o 1 4 0 27881.95 25584.67 149.10 o 2 4 0 1094.52 1087.78 20.98 o 3 4 0 5053.53 5002.17 45.00 o 4 4 0 577.25 498.25 23.75 o 5 4 0 171.19 187.66 17.54 o 6 4 0 2.72 -28.09 28.09 o 7 4 0 11.84 16.92 24.47 o 8 4 0 5.92 -6.88 40.25 o 9 4 0 24.97 37.24 47.95 o 1 5 0 86.00 83.10 8.85 o 2 5 0 81.94 95.94 9.84 o 3 5 0 1069.10 1108.80 25.50 o 4 5 0 45.82 51.37 12.94 o 5 5 0 134.15 138.39 16.80 o 6 5 0 8.16 -11.48 28.35 o 7 5 0 4.23 21.03 23.43 o 8 5 0 10.01 74.58 28.06 o 9 5 0 0.77 19.82 47.59 o 0 6 0 18869.15 17989.57 80.22 o 1 6 0 8630.25 8545.96 54.73 o 2 6 0 241.74 227.85 16.51 o 3 6 0 4853.84 4856.11 48.69 o 4 6 0 825.62 840.43 27.13 o 5 6 0 24.65 -22.68 22.68 o 6 6 0 22.26 6.36 27.93 o 7 6 0 62.97 81.30 24.27 o 8 6 0 0.53 2.66 40.30 o 9 6 0 23.13 35.29 46.76 o 1 7 0 2955.98 3040.47 35.49 o 2 7 0 2.22 -12.01 15.38 o 3 7 0 4.18 6.36 17.57 o 4 7 0 87.23 104.70 14.82 o 5 7 0 473.25 479.93 29.56 o 6 7 0 146.77 151.56 21.19 o 7 7 0 45.63 13.62 34.32 o 8 7 0 0.54 28.23 39.02 o 9 7 0 1.54 -14.78 46.23 o 0 8 0 5946.08 6124.34 51.31 o 1 8 0 5717.39 5480.88 49.47 o 2 8 0 6999.40 7323.61 60.63 o 3 8 0 488.45 373.12 24.11 o 4 8 0 967.06 1029.94 32.97 o 5 8 0 36.39 53.84 18.05 o 6 8 0 1.34 46.62 20.53 o 7 8 0 1.03 9.47 33.59 o 8 8 0 13.89 28.26 27.79 o 9 8 0 15.72 -15.11 46.75 o 1 9 0 1129.27 1148.43 28.34 o 2 9 0 8.10 -16.31 17.80 o 3 9 0 362.39 368.11 23.88 o 4 9 0 1.60 22.39 22.82 o 5 9 0 31.82 15.27 26.60 o 6 9 0 524.80 512.14 36.74 o 7 9 0 113.04 117.78 25.64 o 8 9 0 0.35 -34.22 40.74 o 9 9 0 3.27 35.29 45.61 o 0 10 0 12134.00 12457.02 81.73 o 1 10 0 5108.05 5207.02 53.94 o 2 10 0 1798.44 1746.60 35.80 o 3 10 0 1103.19 1034.92 33.22 o 4 10 0 983.10 964.44 35.50 o 5 10 0 508.84 414.72 34.52 o 6 10 0 136.24 157.30 23.55 o 7 10 0 35.67 -19.67 36.69 o 8 10 0 21.01 20.77 39.82 o 9 10 0 10.49 -8.49 48.48 o 1 11 0 292.42 71.69 21.32 o 2 11 0 507.39 561.90 27.33 o 3 11 0 4.58 9.24 23.34 o 4 11 0 83.52 49.22 19.13 o 5 11 0 126.46 133.74 22.20 o 6 11 0 80.07 69.04 24.09 o 7 11 0 22.05 -6.13 26.95 o 8 11 0 5.49 -13.44 43.25 o 0 12 0 2530.62 2568.30 43.07 o 1 12 0 1188.64 1179.04 33.77 o 2 12 0 1077.29 1068.43 33.99 o 3 12 0 1038.60 1079.35 36.79 o 4 12 0 218.34 214.59 21.86 o 5 12 0 910.31 795.86 40.89 o 6 12 0 91.59 129.94 25.58 o 7 12 0 102.24 106.02 28.33 o 8 12 0 27.48 70.05 31.36 o 1 13 0 12.23 -43.21 43.21 o 2 13 0 26.84 -24.52 24.52 o 3 13 0 1.02 24.08 26.03 o 4 13 0 131.15 185.70 22.16 o 5 13 0 5.85 47.61 22.73 o 6 13 0 2.58 6.94 36.66 o 7 13 0 28.44 -6.05 42.01 o 8 13 0 0.21 -10.24 45.19 o 0 14 0 388.24 372.38 27.94 o 1 14 0 1070.89 1059.71 36.18 o 2 14 0 1352.53 1428.36 41.39 o 3 14 0 98.77 94.18 20.53 o 4 14 0 522.47 474.63 37.74 o 5 14 0 4.61 -3.25 34.53 o 6 14 0 22.00 -28.42 37.98 o 7 14 0 1.82 -30.21 42.40 o 8 14 0 9.57 5.77 48.17 o 1 15 0 10.99 -48.92 48.92 o 2 15 0 0.77 -26.04 27.17 o 3 15 0 406.52 466.01 34.74 o 4 15 0 198.20 200.68 25.22 o 5 15 0 0.75 22.86 35.90 o 6 15 0 0.55 6.47 40.28 o 7 15 0 0.19 32.19 43.30 o 8 15 0 16.62 -48.52 48.97 o 0 16 0 357.86 407.24 32.24 o 1 16 0 659.17 649.01 36.76 o 2 16 0 226.29 219.85 22.52 o 3 16 0 71.71 70.91 22.86 o 4 16 0 187.41 179.64 26.04 o 5 16 0 25.38 63.63 27.19 o 6 16 0 2.66 -8.97 40.86 o 7 16 0 8.47 -45.51 45.51 o 1 17 0 10.86 -41.47 41.47 o 2 17 0 83.58 74.32 22.44 o 3 17 0 124.58 159.05 25.14 o 4 17 0 13.17 -9.98 35.45 o 5 17 0 257.31 247.41 30.58 o 6 17 0 12.20 -0.68 43.87 o 7 17 0 4.61 38.97 46.96 o 0 18 0 334.14 364.76 35.15 o 1 18 0 176.91 90.21 26.25 o 2 18 0 101.92 57.58 24.66 o 3 18 0 426.08 434.43 41.14 o 4 18 0 29.35 24.49 37.13 o 5 18 0 83.99 79.61 29.64 o 6 18 0 13.25 6.90 45.23 o 7 18 0 11.40 -5.64 50.36 o 1 19 0 70.36 -44.90 44.90 o 2 19 0 5.31 -34.62 34.62 o 3 19 0 82.36 3.15 38.63 o 4 19 0 3.39 34.88 39.73 o 5 19 0 6.68 -4.26 43.48 o 6 19 0 7.85 -32.83 47.93 o 7 19 0 54.20 -28.65 52.56 o 0 20 0 76.41 101.80 26.05 o 1 20 0 206.11 131.30 28.29 o 2 20 0 150.90 140.59 27.85 o 3 20 0 7.01 4.50 40.81 o 4 20 0 99.51 99.39 31.09 o 5 20 0 46.97 2.34 46.01 o 6 20 0 9.51 71.28 34.10 o 1 21 0 32.61 -42.48 42.48 o 2 21 0 90.08 77.35 29.31 o 3 21 0 0.49 31.79 42.41 o 4 21 0 148.47 191.04 32.50 o 5 21 0 8.44 -48.06 48.06 o 6 21 0 0.58 -50.79 50.79 o 0 22 0 193.11 223.85 30.03 o 1 22 0 21.41 15.37 40.91 o 2 22 0 43.10 -30.93 41.69 o 3 22 0 0.84 -6.47 43.02 o 4 22 0 49.67 40.15 47.36 o 5 22 0 28.04 80.60 35.00 o 1 23 0 0.28 -45.15 45.15 o 2 23 0 67.35 -5.38 44.28 o 3 23 0 0.49 -46.43 46.43 o 4 23 0 34.94 30.32 49.72 o 5 23 0 0.85 3.30 36.90 o 0 24 0 139.65 120.08 32.79 o 1 24 0 57.61 -31.86 45.89 o 2 24 0 1.69 31.87 46.23 o 3 24 0 23.01 36.26 48.66 o 4 24 0 8.12 11.45 35.79 o 1 25 0 1.26 -48.16 48.16 o 2 25 0 1.72 -21.15 48.32 o 3 25 0 22.47 19.20 35.78 o 0 26 0 5.21 -25.21 51.32 o 1 26 0 25.57 -46.97 52.46 o 2 26 0 0.20 -51.33 51.33 o -9 1 1 12.69 47.86 33.05 o -8 1 1 21.13 6.33 39.57 o -7 1 1 191.67 197.25 25.84 o -6 1 1 2152.20 2111.23 50.14 o -5 1 1 994.31 1010.06 33.88 o -4 1 1 6737.06 6914.08 62.54 o -3 1 1 6210.37 6141.31 50.13 o -2 1 1 35124.65 32607.98 177.95 o -1 1 1 170.33 174.58 7.59 o 1 1 1 1459.37 1406.57 15.16 o 2 1 1 18.03 -0.52 10.01 o 3 1 1 1032.60 1019.87 24.24 o 4 1 1 3700.82 3804.99 50.54 o 5 1 1 691.03 733.44 34.29 o 6 1 1 656.01 742.70 39.56 o 7 1 1 332.84 396.21 29.58 o 8 1 1 258.42 302.19 33.49 o 9 1 1 100.15 178.47 36.73 o -9 2 1 0.36 31.11 45.90 o -8 2 1 0.93 14.49 38.60 o -7 2 1 43.33 59.33 24.11 o -6 2 1 43.12 48.56 20.40 o -5 2 1 48.86 42.27 16.46 o -4 2 1 1023.33 1137.25 29.05 o -3 2 1 678.76 697.72 20.82 o -2 2 1 2312.94 2304.81 25.75 o -1 2 1 11272.74 11068.29 46.16 o 0 2 1 14.73 12.83 2.42 o 1 2 1 3118.55 2953.35 23.55 o 2 2 1 620.23 624.50 15.69 o 3 2 1 16.88 14.68 10.11 o 4 2 1 558.96 577.07 26.98 o 5 2 1 279.26 278.31 20.81 o 6 2 1 6.77 28.71 31.45 o 7 2 1 13.84 20.75 26.29 o 8 2 1 7.99 -44.32 44.32 o 9 2 1 13.28 52.73 36.24 o -9 3 1 5.39 19.46 45.98 o -8 3 1 11.56 29.20 38.79 o -7 3 1 296.35 296.28 26.49 o -6 3 1 408.66 428.36 32.48 o -5 3 1 4647.52 4734.63 59.42 o -4 3 1 902.44 806.67 26.75 o -3 3 1 1988.36 1942.99 29.59 o -2 3 1 16323.58 16048.69 71.18 o -1 3 1 23919.90 22884.21 126.18 o 0 3 1 5259.92 5065.03 202.41 o 1 3 1 957.68 904.73 16.27 o 2 3 1 133.60 151.58 13.01 o 3 3 1 234.67 257.44 16.05 o 4 3 1 906.76 928.24 29.42 o 5 3 1 1763.17 1736.04 44.67 o 6 3 1 391.97 387.86 37.35 o 7 3 1 350.83 323.81 29.37 o 8 3 1 151.75 192.40 31.62 o 9 3 1 60.05 82.14 36.39 o -9 4 1 5.33 78.34 32.43 o -8 4 1 0.07 21.03 27.47 o -7 4 1 0.18 13.01 33.47 o -6 4 1 37.66 41.33 19.34 o -5 4 1 144.40 167.29 17.40 o -4 4 1 376.36 369.08 22.11 o -3 4 1 16.72 10.65 14.50 o -2 4 1 863.92 857.56 18.95 o -1 4 1 4.38 9.49 6.67 o 0 4 1 2.64 1.29 6.35 o 1 4 1 106.54 93.10 8.49 o 2 4 1 1397.38 1453.11 25.43 o 3 4 1 281.35 271.57 18.41 o 4 4 1 1.55 2.05 18.69 o 5 4 1 79.45 142.63 19.58 o 6 4 1 20.06 4.14 31.86 o 7 4 1 22.21 97.00 26.71 o 8 4 1 2.78 -43.76 43.76 o 9 4 1 0.05 -27.82 50.00 o -9 5 1 0.30 11.38 43.68 o -8 5 1 29.23 7.43 38.91 o -7 5 1 40.82 47.40 23.58 o -6 5 1 215.36 236.00 21.75 o -5 5 1 1880.73 1822.65 40.19 o -4 5 1 1455.69 1374.58 31.10 o -3 5 1 14551.53 14502.03 80.35 o -2 5 1 414.21 365.52 15.62 o -1 5 1 27643.63 26297.88 95.96 o 0 5 1 7934.93 7754.93 133.64 o 1 5 1 2189.40 2120.72 27.91 o 2 5 1 142.25 134.98 11.40 o 3 5 1 499.56 487.94 22.67 o 4 5 1 385.36 402.12 25.68 o 5 5 1 981.11 1037.51 38.61 o 6 5 1 861.63 795.68 42.86 o 7 5 1 412.19 409.09 30.46 o 8 5 1 165.26 89.43 33.16 o 9 5 1 87.50 153.52 36.90 o -9 6 1 10.10 37.34 32.08 o -8 6 1 27.48 13.36 27.98 o -7 6 1 21.65 -9.66 33.84 o -6 6 1 198.40 195.23 21.79 o -5 6 1 352.45 334.82 27.05 o -4 6 1 31.87 41.43 13.61 o -3 6 1 174.49 181.99 12.50 o -2 6 1 329.04 360.58 17.10 o -1 6 1 849.41 846.60 19.61 o 0 6 1 1132.82 1142.55 16.08 o 1 6 1 2774.50 2649.70 33.37 o 2 6 1 1126.60 1099.91 26.73 o 3 6 1 37.87 30.25 13.38 o 4 6 1 112.77 167.30 17.08 o 5 6 1 145.82 133.65 19.26 o 6 6 1 2.35 23.91 30.81 o 7 6 1 32.45 33.45 37.01 o 8 6 1 0.93 18.61 30.77 o 9 6 1 15.57 76.11 35.51 o -9 7 1 11.83 25.20 45.68 o -8 7 1 9.46 -9.53 39.44 o -7 7 1 35.13 17.98 24.37 o -6 7 1 1654.57 1585.94 44.90 o -5 7 1 1091.80 1118.32 35.19 o -4 7 1 1356.77 1438.79 33.71 o -3 7 1 3279.24 3159.62 40.90 o -2 7 1 5152.51 5240.15 47.07 o -1 7 1 1181.52 1220.22 23.53 o 0 7 1 905.28 925.34 26.54 o 1 7 1 115.11 140.78 11.77 o 2 7 1 151.54 146.72 13.31 o 3 7 1 56.00 60.26 14.77 o 4 7 1 351.30 369.19 27.84 o 5 7 1 330.27 351.49 32.37 o 6 7 1 208.87 212.52 21.96 o 7 7 1 308.78 398.36 38.53 o 8 7 1 91.75 72.32 31.11 o 9 7 1 36.65 70.45 35.59 o -9 8 1 7.33 -6.78 46.45 o -8 8 1 10.37 24.51 28.41 o -7 8 1 20.74 -26.81 35.02 o -6 8 1 147.45 127.45 21.94 o -5 8 1 115.56 118.59 18.37 o -4 8 1 0.09 14.94 20.95 o -3 8 1 141.50 161.59 13.95 o -2 8 1 2714.37 2917.35 38.23 o -1 8 1 133.87 159.61 11.59 o 0 8 1 106.70 97.34 7.97 o 1 8 1 886.87 933.04 25.99 o 2 8 1 2.37 -3.99 18.20 o 3 8 1 203.94 197.60 16.96 o 4 8 1 692.16 688.61 33.15 o 5 8 1 40.25 -2.95 29.31 o 6 8 1 8.18 -8.95 21.95 o 7 8 1 6.03 7.24 34.49 o 8 8 1 11.45 21.67 40.78 o 9 8 1 2.24 43.72 34.93 o -9 9 1 1.91 -39.76 47.53 o -8 9 1 10.83 -10.65 41.22 o -7 9 1 463.83 425.28 40.72 o -6 9 1 272.69 299.26 23.88 o -5 9 1 918.87 914.75 36.40 o -4 9 1 2388.68 2418.32 43.96 o -3 9 1 206.56 208.94 15.08 o -2 9 1 10296.85 10825.76 74.78 o -1 9 1 2482.80 2354.03 34.74 o 0 9 1 271.42 302.27 14.14 o 1 9 1 907.07 930.00 27.21 o 2 9 1 0.06 17.48 18.92 o 3 9 1 175.30 183.81 17.19 o 4 9 1 256.23 272.72 20.50 o 5 9 1 1150.88 1117.60 42.94 o 6 9 1 465.75 419.97 39.84 o 7 9 1 127.29 163.18 27.00 o 8 9 1 75.32 91.31 29.42 o 9 9 1 62.26 81.79 33.85 o -9 10 1 8.34 61.46 33.31 o -8 10 1 48.51 24.09 41.00 o -7 10 1 88.44 84.90 26.15 o -6 10 1 0.22 10.34 31.03 o -5 10 1 1.29 14.30 26.81 o -4 10 1 50.92 16.86 16.98 o -3 10 1 21.26 30.97 14.59 o -2 10 1 284.80 290.11 22.25 o -1 10 1 32.54 2.80 17.39 o 0 10 1 1679.57 1657.81 38.09 o 1 10 1 5.33 -8.07 19.46 o 2 10 1 473.43 570.21 27.40 o 3 10 1 555.40 505.16 30.08 o 4 10 1 530.46 504.60 33.63 o 5 10 1 158.13 183.19 23.77 o 6 10 1 136.18 95.61 26.17 o 7 10 1 6.47 -3.34 38.25 o 8 10 1 1.62 -42.02 42.02 o 9 10 1 3.08 24.46 33.47 o -8 11 1 39.40 -20.05 42.67 o -7 11 1 277.09 239.88 28.46 o -6 11 1 298.04 284.77 25.91 o -5 11 1 183.94 204.89 21.42 o -4 11 1 640.22 649.34 32.41 o -3 11 1 3352.87 3489.91 51.11 o -2 11 1 449.95 466.53 25.21 o -1 11 1 437.89 440.00 24.15 o 0 11 1 2296.86 2270.47 59.82 o 1 11 1 36.47 17.78 14.66 o 2 11 1 6.29 7.59 15.25 o 3 11 1 33.67 44.30 17.83 o 4 11 1 1347.49 1330.49 43.75 o 5 11 1 656.10 773.59 40.98 o 6 11 1 357.30 364.31 28.98 o 7 11 1 116.35 145.37 29.70 o 8 11 1 107.79 171.91 32.12 o -8 12 1 6.56 9.48 43.01 o -7 12 1 2.34 -29.82 38.64 o -6 12 1 20.48 -12.31 34.36 o -5 12 1 11.97 22.42 30.56 o -4 12 1 147.44 141.49 19.92 o -3 12 1 275.38 306.03 28.10 o -2 12 1 80.63 63.68 15.69 o -1 12 1 536.45 707.91 27.85 o 0 12 1 101.07 83.28 11.09 o 1 12 1 683.69 793.44 31.09 o 2 12 1 469.65 469.24 29.58 o 3 12 1 36.53 25.92 19.11 o 4 12 1 69.17 25.97 21.66 o 5 12 1 123.39 149.32 24.82 o 6 12 1 25.30 51.51 26.29 o 7 12 1 0.22 35.02 29.04 o 8 12 1 5.72 13.28 45.98 o -8 13 1 22.06 29.81 31.60 o -7 13 1 93.00 75.53 28.98 o -6 13 1 319.16 297.94 28.07 o -5 13 1 128.77 106.68 23.43 o -4 13 1 324.94 376.47 32.73 o -3 13 1 375.02 387.94 29.75 o -2 13 1 1132.04 1098.47 35.73 o -1 13 1 1292.34 1388.69 36.15 o 0 13 1 357.35 362.48 19.29 o 1 13 1 43.49 56.37 16.77 o 2 13 1 99.97 87.07 18.69 o 3 13 1 43.69 42.69 20.17 o 4 13 1 262.01 229.72 24.19 o 5 13 1 660.65 566.56 42.20 o 6 13 1 296.32 296.94 30.58 o 7 13 1 5.20 -26.94 44.41 o 8 13 1 106.51 113.86 35.06 o -8 14 1 0.09 -17.73 46.19 o -7 14 1 55.10 -15.95 42.33 o -6 14 1 56.58 31.32 26.54 o -5 14 1 40.56 2.62 33.35 o -4 14 1 0.64 -4.65 30.07 o -3 14 1 14.43 -9.79 27.51 o -2 14 1 93.70 99.84 19.12 o -1 14 1 117.39 97.15 18.26 o 0 14 1 80.24 62.82 15.26 o 1 14 1 48.24 63.87 18.56 o 2 14 1 213.84 220.57 20.78 o 3 14 1 16.36 10.47 29.65 o 4 14 1 5.06 13.04 22.85 o 5 14 1 17.07 17.07 36.15 o 6 14 1 75.29 86.69 28.62 o 7 14 1 3.72 34.70 44.70 o 8 14 1 2.23 -50.25 50.25 o -8 15 1 17.90 -9.89 49.11 o -7 15 1 24.85 -8.93 43.86 o -6 15 1 67.81 28.62 40.21 o -5 15 1 85.27 67.27 25.64 o -4 15 1 463.28 453.32 37.29 o -3 15 1 222.91 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