#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/30/2003064.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2003064_Fobs loop_ _publ_author_name 'Iwasaki, Fujiko' 'Yoshikawa, Joseph H.' 'Yamamoto, Hajime' 'Kan-nari, Eiji' 'Takada, Kiwamu' 'Yasui, Masanori' 'Ishida, Takayuki' 'Nogami, Takashi' _publ_section_title ; TEMPO radicals showing magnetic interactions. I. 4-(4-Halobenzylideneamino)TEMPO and related compounds ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section B' _journal_page_first 231 _journal_page_last 245 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _exptl_crystal_F_000 772.00 _reflns_d_resolution_high 0.7697 _[local]_cod_data_source_file oa00194asup7.hkl _[local]_cod_data_source_block 4a #BEGIN Tags that were not found in dictionaries: _shelx_title 4-I-Ph-TEMPO(a) _shelx_refln_list_code 4 _shelx_f_calc_maximum 262.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 8507.41 8352.64 91.21 o 2 0 0 6073.48 6064.42 107.01 o 3 0 0 4337.97 4113.88 108.57 o 4 0 0 105.45 111.82 11.12 o 5 0 0 143.78 185.03 17.62 o 6 0 0 1.99 9.36 24.97 o 7 0 0 12.07 13.39 23.53 o 1 1 0 394.57 374.48 19.05 o 2 1 0 0.02 3.12 8.58 o 3 1 0 2.43 -9.69 13.07 o 4 1 0 19.11 21.71 16.64 o 5 1 0 111.80 89.20 12.29 o 6 1 0 32.07 -1.76 16.51 o 7 1 0 8.88 4.55 25.16 o 1 2 0 68759.92 59849.46 326.89 o 2 2 0 13307.18 13214.89 164.16 o 3 2 0 2725.46 2661.34 87.64 o 4 2 0 73.42 52.01 9.30 o 5 2 0 22.01 22.69 22.75 o 6 2 0 31.52 15.86 25.94 o 7 2 0 0.02 -11.44 22.56 o 1 3 0 9206.76 9514.44 109.68 o 2 3 0 45.29 50.26 6.05 o 3 3 0 66.64 59.42 7.87 o 4 3 0 34.98 47.07 8.00 o 5 3 0 9.71 14.43 10.53 o 6 3 0 102.09 94.46 13.46 o 7 3 0 0.13 23.34 18.40 o 0 4 0 15452.73 15171.42 134.19 o 1 4 0 21761.99 21280.50 183.34 o 2 4 0 6473.39 6446.31 117.54 o 3 4 0 2178.46 2281.98 84.52 o 4 4 0 857.44 870.47 61.44 o 5 4 0 7.44 -18.07 18.07 o 6 4 0 84.24 98.50 14.37 o 7 4 0 0.68 14.43 20.67 o 1 5 0 910.24 1005.57 39.92 o 2 5 0 95.52 110.46 10.08 o 3 5 0 53.52 38.10 7.41 o 4 5 0 299.31 280.86 25.75 o 5 5 0 0.64 3.71 16.38 o 6 5 0 14.47 4.75 18.27 o 7 5 0 9.29 -20.09 21.58 o 0 6 0 13910.46 13416.24 148.56 o 1 6 0 13911.19 14061.76 163.05 o 2 6 0 8091.86 8337.24 142.90 o 3 6 0 1837.97 1853.22 77.76 o 4 6 0 460.49 430.59 31.66 o 5 6 0 4.48 28.41 27.05 o 6 6 0 1.79 -4.42 26.33 o 7 6 0 13.25 13.26 18.33 o 1 7 0 1982.96 1949.11 62.48 o 2 7 0 442.50 447.03 34.78 o 3 7 0 3.45 8.58 15.47 o 4 7 0 333.06 328.06 29.19 o 5 7 0 357.63 332.03 32.83 o 6 7 0 13.44 2.28 27.63 o 7 7 0 0.84 11.44 13.33 o 0 8 0 42792.62 38471.96 306.67 o 1 8 0 15565.37 15303.78 190.10 o 2 8 0 6886.51 6883.01 138.87 o 3 8 0 1505.24 1524.57 74.96 o 4 8 0 35.59 29.19 20.87 o 5 8 0 27.77 29.00 8.65 o 6 8 0 6.75 24.51 26.92 o 7 8 0 0.13 5.59 23.60 o 1 9 0 3785.07 4009.33 99.93 o 2 9 0 99.01 120.02 11.38 o 3 9 0 468.15 463.03 42.84 o 4 9 0 262.74 272.93 27.11 o 5 9 0 40.20 20.80 22.10 o 6 9 0 11.95 26.98 20.61 o 7 9 0 0.63 32.44 25.16 o 0 10 0 20722.65 20177.80 232.62 o 1 10 0 13708.18 13985.37 199.40 o 2 10 0 9134.93 9433.89 175.28 o 3 10 0 1179.00 1137.22 68.65 o 4 10 0 0.38 -13.26 13.26 o 5 10 0 29.11 38.49 26.46 o 6 10 0 7.86 11.64 23.86 o 7 10 0 2.37 -11.83 21.00 o 1 11 0 265.65 334.50 25.29 o 2 11 0 1445.16 1674.82 76.91 o 3 11 0 323.69 345.55 28.93 o 4 11 0 3.52 -11.64 14.69 o 5 11 0 23.03 28.48 22.56 o 6 11 0 4.56 -20.22 27.24 o 0 12 0 4315.82 4241.24 112.08 o 1 12 0 16963.94 18019.87 245.82 o 2 12 0 4657.95 4815.24 133.86 o 3 12 0 599.40 537.99 52.01 o 4 12 0 124.49 143.75 14.04 o 5 12 0 1.19 -2.67 20.80 o 6 12 0 10.23 -3.12 22.62 o 1 13 0 140.08 36.34 26.33 o 2 13 0 181.86 164.22 14.56 o 3 13 0 2.54 -14.11 14.11 o 4 13 0 47.00 7.35 25.03 o 5 13 0 9.22 -10.40 24.64 o 6 13 0 1.83 -12.22 12.22 o 0 14 0 9722.84 9807.72 185.87 o 1 14 0 4662.56 4530.61 128.60 o 2 14 0 3174.60 3270.45 118.06 o 3 14 0 743.60 681.47 59.29 o 4 14 0 225.44 214.74 19.50 o 5 14 0 14.29 18.46 20.87 o 6 14 0 0.75 15.28 16.51 o 1 15 0 17.02 -17.62 17.62 o 2 15 0 7.80 11.05 11.38 o 3 15 0 193.01 172.03 17.16 o 4 15 0 17.85 3.12 22.10 o 5 15 0 1.87 -2.54 20.74 o 6 15 0 46.15 63.97 14.04 o 0 16 0 5727.58 5700.47 150.44 o 1 16 0 4408.80 4366.65 134.64 o 2 16 0 3123.46 3254.98 123.98 o 3 16 0 538.97 526.09 40.05 o 4 16 0 1.28 -8.13 17.10 o 5 16 0 27.53 3.84 25.23 o 6 16 0 0.57 -34.00 34.00 o 1 17 0 14.75 -23.80 23.80 o 2 17 0 88.23 90.63 13.46 o 3 17 0 13.41 14.82 20.74 o 4 17 0 60.93 27.37 11.05 o 5 17 0 45.02 19.83 25.94 o 6 17 0 2.83 -22.75 26.85 o 0 18 0 6758.51 6608.19 173.91 o 1 18 0 3685.36 3768.13 133.86 o 2 18 0 859.51 806.11 70.02 o 3 18 0 834.04 818.26 73.14 o 4 18 0 29.34 19.11 18.40 o 5 18 0 0.49 29.97 22.82 o 6 18 0 7.53 26.53 20.93 o 1 19 0 39.57 -29.26 29.26 o 2 19 0 14.86 18.59 22.95 o 3 19 0 228.42 232.88 21.97 o 4 19 0 15.81 5.20 19.44 o 5 19 0 7.87 19.18 13.91 o 6 19 0 32.27 -3.32 24.64 o 0 20 0 3431.50 3529.60 134.77 o 1 20 0 2464.33 2441.59 113.90 o 2 20 0 1892.92 1894.57 106.43 o 3 20 0 129.53 152.07 16.25 o 4 20 0 19.16 14.17 11.90 o 5 20 0 19.98 10.60 15.93 o 1 21 0 27.49 -32.70 32.70 o 2 21 0 111.77 101.68 13.98 o 3 21 0 18.99 -25.81 25.81 o 4 21 0 79.39 49.02 34.20 o 5 21 0 75.55 37.64 40.05 o 0 22 0 1714.51 1621.83 97.13 o 1 22 0 2441.68 2475.85 121.12 o 2 22 0 717.38 767.62 73.92 o 3 22 0 70.39 75.81 14.56 o 4 22 0 0.13 -2.34 20.15 o 5 22 0 7.90 19.44 20.80 o 1 23 0 1.98 -73.14 73.14 o 2 23 0 161.42 136.46 17.03 o 3 23 0 169.10 185.74 18.07 o 4 23 0 107.81 91.41 15.41 o 5 23 0 1.31 17.75 19.37 o 0 24 0 1392.52 1475.55 97.72 o 1 24 0 1452.24 1437.00 100.38 o 2 24 0 303.69 305.50 29.39 o 3 24 0 58.30 81.40 13.65 o 4 24 0 1.00 6.63 19.37 o 5 24 0 1.78 18.07 19.83 o 1 25 0 89.41 -48.89 48.89 o 2 25 0 127.45 101.62 16.58 o 3 25 0 190.77 197.25 20.09 o 4 25 0 20.99 -29.19 29.19 o 0 26 0 1998.85 1712.85 111.11 o 1 26 0 153.01 111.69 20.54 o 2 26 0 400.02 430.59 34.39 o 3 26 0 93.16 85.75 16.64 o 4 26 0 0.07 28.15 20.02 o 1 27 0 67.22 -73.99 73.99 o 2 27 0 52.55 48.83 13.65 o 3 27 0 52.78 45.51 31.40 o 4 27 0 71.36 47.53 42.52 o 0 28 0 62.00 64.56 14.04 o 1 28 0 604.72 564.97 51.62 o 2 28 0 138.06 154.28 17.75 o 3 28 0 26.88 47.07 32.57 o 4 28 0 11.74 5.01 29.71 o 1 29 0 1.05 -68.07 68.07 o 2 29 0 25.21 37.77 27.57 o 3 29 0 105.06 139.78 19.50 o 0 30 0 285.12 263.89 22.75 o 1 30 0 154.35 139.19 17.94 o 2 30 0 50.33 42.97 14.76 o 3 30 0 2.69 33.09 29.58 o 1 31 0 1.25 -47.07 47.07 o 2 31 0 70.95 37.64 26.46 o 0 32 0 141.07 136.14 19.37 o 1 32 0 111.40 84.45 20.35 o 2 32 0 0.38 17.03 18.66 o 1 33 0 41.98 -19.57 41.80 o -7 1 1 4.54 -12.87 27.44 o -6 1 1 78.29 75.48 12.94 o -5 1 1 354.80 439.10 34.72 o -4 1 1 815.33 815.01 56.69 o -3 1 1 901.53 874.44 49.28 o -2 1 1 190.45 185.87 14.43 o -1 1 1 776.56 773.27 27.89 o 0 1 1 2935.76 2776.07 41.41 o 1 1 1 1280.26 1212.51 37.97 o 2 1 1 15303.90 15476.07 184.51 o 3 1 1 3569.28 3563.34 104.02 o 4 1 1 1841.26 1741.52 87.12 o 5 1 1 842.31 856.17 70.86 o 6 1 1 30.97 48.89 11.05 o 7 1 1 8.18 3.58 28.80 o -7 2 1 7.08 -16.90 16.90 o -6 2 1 44.46 51.10 11.05 o -5 2 1 338.91 339.50 32.12 o -4 2 1 91.95 97.33 10.27 o -3 2 1 56.31 61.11 7.48 o -2 2 1 551.96 632.13 35.82 o -1 2 1 457.12 455.36 23.27 o 0 2 1 1545.65 1538.09 22.14 o 1 2 1 11004.21 10620.58 118.59 o 2 2 1 1008.43 998.09 46.22 o 3 2 1 1.42 -10.27 10.27 o 4 2 1 123.08 121.64 11.83 o 5 2 1 192.50 174.69 16.84 o 6 2 1 92.66 97.98 14.50 o 7 2 1 7.09 11.05 12.87 o -7 3 1 41.06 28.09 28.28 o -6 3 1 14.17 17.88 17.23 o -5 3 1 179.77 200.70 18.40 o -4 3 1 2517.23 2621.68 102.66 o -3 3 1 1795.91 1809.14 73.34 o -2 3 1 14.91 24.58 4.88 o -1 3 1 2219.40 2074.33 51.17 o 0 3 1 84.71 96.13 5.66 o 1 3 1 50484.39 46605.90 295.94 o 2 3 1 13554.39 13436.26 174.76 o 3 3 1 4737.72 5210.14 128.21 o 4 3 1 1322.06 1503.96 80.23 o 5 3 1 186.48 169.17 15.02 o 6 3 1 60.39 62.15 12.74 o 7 3 1 12.61 30.36 27.18 o -7 4 1 10.89 15.02 16.32 o -6 4 1 66.39 65.99 12.16 o -5 4 1 16.90 2.34 20.41 o -4 4 1 25.81 35.63 7.09 o -3 4 1 752.12 741.35 48.11 o -2 4 1 745.84 846.48 44.66 o -1 4 1 165.99 148.62 11.83 o 0 4 1 6841.35 6906.56 60.20 o 1 4 1 332.74 344.05 23.27 o 2 4 1 2536.19 2725.57 78.47 o 3 4 1 159.95 169.56 15.54 o 4 4 1 1.64 2.54 15.47 o 5 4 1 42.66 34.72 25.36 o 6 4 1 20.81 21.52 8.91 o 7 4 1 4.63 24.12 19.18 o -7 5 1 7.01 30.30 23.27 o -6 5 1 99.01 93.03 13.52 o -5 5 1 523.41 640.06 61.18 o -4 5 1 1390.35 1404.23 78.86 o -3 5 1 3047.60 3263.69 102.33 o -2 5 1 6.31 -12.61 12.61 o -1 5 1 916.83 960.19 39.66 o 0 5 1 22538.52 21480.90 124.63 o 1 5 1 40062.75 37846.07 277.41 o 2 5 1 6647.49 6581.73 125.15 o 3 5 1 7499.77 7481.65 157.79 o 4 5 1 1155.00 1143.40 72.88 o 5 5 1 111.16 108.12 12.29 o 6 5 1 7.07 19.89 15.60 o 7 5 1 8.76 10.73 14.56 o -7 6 1 3.49 23.47 18.59 o -6 6 1 11.39 -15.60 17.16 o -5 6 1 220.44 245.95 24.38 o -4 6 1 27.00 43.95 8.71 o -3 6 1 601.42 583.11 45.64 o -2 6 1 326.99 428.38 34.39 o -1 6 1 3.33 12.16 10.47 o 0 6 1 8614.70 8602.85 80.66 o 1 6 1 7004.82 6942.17 112.02 o 2 6 1 2428.46 2812.76 83.41 o 3 6 1 355.50 414.14 39.14 o 4 6 1 9.74 13.26 8.84 o 5 6 1 100.45 102.20 13.33 o 6 6 1 2.30 -1.37 14.56 o 7 6 1 0.41 15.02 21.65 o -7 7 1 6.01 -20.02 21.65 o -6 7 1 96.72 80.94 13.85 o -5 7 1 1055.14 1067.72 78.73 o -4 7 1 619.18 577.52 55.91 o -3 7 1 466.02 496.51 44.14 o -2 7 1 1242.36 1175.25 58.90 o -1 7 1 2202.66 2383.40 70.34 o 0 7 1 12327.63 12598.51 106.33 o 1 7 1 6976.74 6780.29 116.11 o 2 7 1 16818.74 17452.16 220.46 o 3 7 1 1737.50 1709.80 77.95 o 4 7 1 1216.60 1173.95 76.46 o 5 7 1 228.20 186.65 17.42 o 6 7 1 36.12 18.33 24.12 o 7 7 1 9.82 26.98 11.05 o -7 8 1 4.97 24.64 10.66 o -6 8 1 33.05 47.53 11.38 o -5 8 1 16.63 -20.35 20.35 o -4 8 1 45.59 41.35 8.32 o -3 8 1 5.03 10.79 8.19 o -2 8 1 110.53 110.59 10.34 o -1 8 1 3748.93 3877.03 94.73 o 0 8 1 1364.42 1478.73 74.80 o 1 8 1 930.95 971.37 46.16 o 2 8 1 2789.48 2913.33 90.04 o 3 8 1 44.89 58.38 8.91 o 4 8 1 158.24 139.97 13.26 o 5 8 1 4.09 10.14 16.77 o 6 8 1 0.00 -2.08 18.33 o 7 8 1 4.70 -0.98 13.00 o -7 9 1 2.44 -26.14 26.14 o -6 9 1 171.83 174.11 18.72 o -5 9 1 266.75 343.01 34.20 o -4 9 1 490.92 514.39 37.19 o -3 9 1 545.76 609.96 49.80 o -2 9 1 79.20 59.94 8.32 o -1 9 1 607.66 631.87 41.02 o 0 9 1 5230.85 5276.85 192.25 o 1 9 1 1262.69 1159.46 52.60 o 2 9 1 4085.87 4132.40 111.11 o 3 9 1 5196.19 5190.76 140.82 o 4 9 1 1006.55 1052.90 72.17 o 5 9 1 103.07 103.57 14.11 o 6 9 1 4.26 3.51 25.23 o -7 10 1 0.41 14.43 25.68 o -6 10 1 2.56 -2.80 21.39 o -5 10 1 78.44 92.19 13.00 o -4 10 1 33.77 38.68 9.43 o -3 10 1 938.97 881.00 61.57 o -2 10 1 484.49 455.03 40.37 o -1 10 1 33.85 29.26 5.92 o 0 10 1 305.53 353.00 34.49 o 1 10 1 5901.01 6519.71 131.78 o 2 10 1 216.51 250.56 21.52 o 3 10 1 52.90 32.38 8.78 o 4 10 1 139.03 128.27 13.72 o 5 10 1 2.10 -8.45 18.92 o 6 10 1 2.54 5.14 20.48 o -7 11 1 17.73 24.38 11.18 o -6 11 1 74.96 76.33 13.72 o -5 11 1 38.92 2.15 26.40 o -4 11 1 687.99 688.24 62.67 o -3 11 1 25.65 20.61 14.37 o -2 11 1 251.89 279.69 23.34 o -1 11 1 86.99 93.94 8.45 o 0 11 1 3449.33 3316.59 67.32 o 1 11 1 7263.56 7567.67 148.30 o 2 11 1 2401.38 2247.20 87.31 o 3 11 1 2774.34 2944.73 111.50 o 4 11 1 421.03 403.74 33.81 o 5 11 1 125.49 111.43 15.02 o 6 11 1 31.48 27.83 11.25 o -7 12 1 21.58 25.10 24.90 o -6 12 1 2.94 13.20 9.75 o -5 12 1 99.99 85.69 13.91 o -4 12 1 410.37 449.18 37.25 o -3 12 1 437.89 438.97 33.09 o -2 12 1 958.47 944.65 60.46 o -1 12 1 1340.69 1404.75 66.83 o 0 12 1 568.84 592.69 43.79 o 1 12 1 673.42 719.51 48.18 o 2 12 1 509.62 623.74 49.22 o 3 12 1 145.84 174.63 15.60 o 4 12 1 53.30 1.82 23.53 o 5 12 1 19.80 17.55 19.76 o 6 12 1 0.06 -19.63 23.34 o -6 13 1 8.48 -22.69 22.69 o -5 13 1 481.55 571.99 47.66 o -4 13 1 1.87 7.93 24.38 o -3 13 1 1388.89 1644.91 90.37 o -2 13 1 11.08 -0.59 9.69 o -1 13 1 1219.99 1346.24 68.52 o 0 13 1 3771.01 3855.63 79.80 o 1 13 1 5146.33 5133.42 132.30 o 2 13 1 2861.76 2910.28 106.56 o 3 13 1 1771.09 1650.18 88.87 o 4 13 1 889.05 980.99 75.35 o 5 13 1 10.99 -15.54 17.03 o 6 13 1 6.12 -8.78 8.78 o -6 14 1 43.42 34.85 12.16 o -5 14 1 34.02 30.23 30.95 o -4 14 1 478.78 394.89 35.30 o -3 14 1 236.33 235.35 20.61 o -2 14 1 376.03 408.55 30.17 o -1 14 1 2142.88 2149.75 89.33 o 0 14 1 3799.33 3884.09 83.42 o 1 14 1 1.59 -15.67 15.67 o 2 14 1 169.29 176.58 15.80 o 3 14 1 18.74 12.94 16.06 o 4 14 1 1.16 3.45 19.44 o 5 14 1 0.37 -19.11 19.11 o 6 14 1 6.72 -9.88 15.15 o -6 15 1 139.16 153.95 20.09 o -5 15 1 86.43 89.78 13.72 o -4 15 1 632.22 716.84 67.35 o -3 15 1 253.20 243.87 22.10 o -2 15 1 43.24 43.17 8.71 o -1 15 1 605.54 603.72 52.21 o 0 15 1 3081.10 3182.69 78.17 o 1 15 1 2973.44 3050.77 110.72 o 2 15 1 4050.64 4303.46 139.97 o 3 15 1 1306.05 1324.98 83.41 o 4 15 1 240.71 271.82 24.97 o 5 15 1 74.30 71.58 14.17 o 6 15 1 16.87 46.61 32.38 o -6 16 1 8.22 5.92 24.06 o -5 16 1 34.47 28.35 21.45 o -4 16 1 177.65 161.36 17.29 o -3 16 1 605.16 629.98 60.79 o -2 16 1 971.34 1015.51 70.73 o -1 16 1 1735.23 1934.16 90.63 o 0 16 1 411.95 423.52 26.19 o 1 16 1 383.94 389.69 31.47 o 2 16 1 432.52 405.04 33.68 o 3 16 1 0.98 2.60 21.06 o 4 16 1 8.70 16.45 21.06 o 5 16 1 10.78 13.85 14.89 o 6 16 1 0.53 5.72 23.99 o -6 17 1 64.80 94.86 15.93 o -5 17 1 92.64 131.39 17.29 o -4 17 1 619.02 737.39 72.30 o -3 17 1 913.41 841.15 70.41 o -2 17 1 20.04 2.21 21.06 o -1 17 1 679.84 672.31 56.56 o 0 17 1 690.69 692.41 39.72 o 1 17 1 2379.45 2643.46 110.00 o 2 17 1 2608.97 2600.81 115.66 o 3 17 1 1067.84 1227.52 84.58 o 4 17 1 326.14 351.33 30.49 o 5 17 1 80.60 66.70 14.24 o 6 17 1 0.37 -10.86 16.58 o -6 18 1 14.22 8.26 16.71 o -5 18 1 49.12 12.09 28.93 o -4 18 1 155.06 185.55 17.81 o -3 18 1 538.95 532.98 41.02 o -2 18 1 1214.85 1282.14 82.44 o -1 18 1 877.74 841.93 64.17 o 0 18 1 598.46 547.47 32.31 o 1 18 1 505.75 558.47 55.07 o 2 18 1 9.09 8.97 16.77 o 3 18 1 47.99 37.71 27.44 o 4 18 1 19.31 18.46 20.80 o 5 18 1 0.32 4.62 24.71 o 6 18 1 5.32 -23.73 27.96 o -6 19 1 17.00 14.89 31.73 o -5 19 1 123.70 139.13 18.72 o -4 19 1 176.22 177.62 18.72 o -3 19 1 182.15 175.86 17.42 o -2 19 1 928.41 939.71 73.14 o -1 19 1 4.80 -17.23 17.23 o 0 19 1 1622.23 1548.66 61.97 o 1 19 1 1537.52 1552.79 90.63 o 2 19 1 1288.14 1138.91 80.81 o 3 19 1 868.64 992.37 80.23 o 4 19 1 284.35 242.83 24.12 o 5 19 1 47.81 -3.38 24.32 o -6 20 1 1.42 -2.28 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