#------------------------------------------------------------------------------ #$Date: 2016-10-07 04:53:24 +0300 (Fri, 07 Oct 2016) $ #$Revision: 186994 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/06/2020608.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020608 _cell_angle_alpha 90.000 _cell_angle_beta 95.975 _cell_angle_gamma 90.000 _cell_length_a 8.4544 _cell_length_b 15.0084 _cell_length_c 10.6904 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.6000 _cod_data_source_file yp3115Isup2.hkl _cod_data_source_block I _shelx_title ' jonyj35 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 150.79 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 -23 0 246.47 429.57 136.42 o 4 -23 0 413.43 444.75 133.15 o 5 -23 0 357.21 230.47 87.38 o 1 -22 0 591.27 402.94 104.65 o 2 -22 0 214.21 115.16 87.83 o 3 -22 0 37.12 32.00 77.78 o 4 -22 0 23.52 32.03 56.90 o 5 -22 0 136.12 129.21 68.62 o 6 -22 0 0.71 31.08 62.94 o 1 -21 0 172.44 256.01 96.00 o 2 -21 0 158.40 109.09 79.65 o 3 -21 0 307.71 526.74 126.60 o 4 -21 0 380.40 328.89 111.42 o 5 -21 0 352.71 189.01 71.24 o 6 -21 0 213.97 113.85 62.84 o 7 -21 0 343.01 213.77 105.11 o 0 -20 0 498.85 529.08 104.41 o 1 -20 0 566.30 459.70 103.95 o 2 -20 0 295.90 368.13 99.27 o 3 -20 0 242.28 178.46 87.83 o 4 -20 0 104.91 267.69 106.05 o 5 -20 0 41.35 57.89 52.16 o 6 -20 0 6.04 52.15 61.99 o 7 -20 0 50.66 24.24 55.68 o 8 -20 0 58.42 56.97 63.33 o 1 -19 0 186.62 142.02 78.72 o 2 -19 0 464.73 372.11 93.90 o 3 -19 0 453.63 608.26 122.63 o 4 -19 0 342.96 325.86 104.41 o 5 -19 0 449.14 337.04 92.73 o 6 -19 0 508.16 551.74 109.32 o 7 -19 0 171.99 144.83 66.60 o 8 -19 0 130.09 6.15 56.86 o 9 -19 0 305.20 238.98 119.95 o 1 -18 0 1267.07 1381.67 131.51 o 2 -18 0 435.98 547.06 104.18 o 3 -18 0 144.26 129.88 72.41 o 4 -18 0 50.85 -20.79 63.30 o 5 -18 0 0.24 -16.92 40.90 o 6 -18 0 33.93 45.02 53.07 o 7 -18 0 27.34 -13.56 43.68 o 8 -18 0 18.91 28.82 59.93 o 9 -18 0 193.23 243.63 79.12 o 1 -17 0 276.17 334.25 57.12 o 2 -17 0 236.25 282.41 83.62 o 3 -17 0 1169.82 997.89 116.09 o 4 -17 0 1000.55 919.17 127.77 o 5 -17 0 188.47 99.41 49.34 o 6 -17 0 441.12 422.35 78.79 o 7 -17 0 442.42 228.69 110.84 o 8 -17 0 380.79 321.26 78.46 o 9 -17 0 397.64 472.18 94.04 o 10 -17 0 260.02 343.51 220.97 o 1 -16 0 1200.42 1268.38 102.08 o 2 -16 0 961.16 1147.15 117.96 o 3 -16 0 48.53 81.99 65.40 o 4 -16 0 67.76 21.26 54.19 o 5 -16 0 1.84 -22.60 36.20 o 6 -16 0 94.21 14.65 92.85 o 7 -16 0 12.22 -21.16 36.25 o 8 -16 0 47.43 21.32 51.97 o 9 -16 0 255.57 263.95 77.00 o 10 -16 0 227.29 325.73 83.23 o 1 -15 0 498.59 531.65 83.16 o 2 -15 0 860.08 757.59 63.55 o 3 -15 0 826.99 620.64 88.76 o 4 -15 0 726.70 702.27 62.80 o 5 -15 0 491.41 468.12 82.69 o 6 -15 0 429.97 514.69 80.88 o 7 -15 0 509.96 389.74 74.15 o 8 -15 0 280.29 174.17 64.08 o 9 -15 0 465.70 396.93 85.44 o 10 -15 0 592.61 650.82 225.65 o 11 -15 0 39.52 96.00 68.98 o 2 -14 0 1325.35 1428.52 77.96 o 3 -14 0 716.32 671.84 57.42 o 4 -14 0 27.19 -11.44 49.17 o 5 -14 0 1.78 29.63 48.12 o 6 -14 0 8.36 -12.01 35.75 o 7 -14 0 38.98 61.77 83.51 o 8 -14 0 114.62 173.55 58.38 o 9 -14 0 372.60 540.08 111.89 o 10 -14 0 335.03 330.32 82.52 o 11 -14 0 142.15 40.20 68.26 o 2 -13 0 1828.82 1703.32 120.02 o 3 -13 0 647.07 711.61 55.84 o 4 -13 0 1384.99 1418.36 60.50 o 5 -13 0 1325.18 1202.79 85.74 o 6 -13 0 842.78 847.73 128.12 o 7 -13 0 345.40 367.99 68.62 o 8 -13 0 732.69 929.54 109.17 o 9 -13 0 562.48 577.07 164.80 o 10 -13 0 319.70 332.86 149.38 o 11 -13 0 214.83 120.59 72.68 o 2 -12 0 1004.98 1070.09 62.98 o 3 -12 0 467.59 468.80 104.06 o 4 -12 0 19.36 13.52 20.08 o 5 -12 0 11.15 30.26 40.11 o 6 -12 0 37.13 -19.03 35.33 o 7 -12 0 131.27 155.78 52.32 o 8 -12 0 93.16 106.02 55.62 o 9 -12 0 99.18 87.47 112.24 o 10 -12 0 422.58 444.85 88.90 o 11 -12 0 552.30 493.91 119.95 o 12 -12 0 631.37 575.33 106.20 o 2 -11 0 2160.07 2182.55 116.91 o 3 -11 0 1005.07 999.79 59.45 o 4 -11 0 686.48 786.29 51.65 o 5 -11 0 863.25 757.18 99.35 o 6 -11 0 980.15 907.25 89.47 o 7 -11 0 565.25 729.48 86.95 o 8 -11 0 905.72 857.63 86.03 o 9 -11 0 529.65 505.66 86.93 o 10 -11 0 198.65 125.86 58.11 o 11 -11 0 75.59 44.20 54.72 o 12 -11 0 2.24 -13.19 57.63 o 2 -10 0 1504.85 1540.42 83.39 o 3 -10 0 152.66 170.89 33.61 o 4 -10 0 25.56 27.18 20.20 o 5 -10 0 54.51 107.88 30.44 o 6 -10 0 3.17 -19.80 23.80 o 7 -10 0 25.34 42.97 29.63 o 8 -10 0 72.14 88.40 44.68 o 9 -10 0 299.98 378.70 77.88 o 10 -10 0 450.03 456.74 82.78 o 11 -10 0 688.78 903.08 116.20 o 12 -10 0 597.67 509.79 98.59 o 2 -9 0 1996.41 1913.98 54.72 o 3 -9 0 2195.14 2113.93 55.63 o 4 -9 0 873.70 893.92 45.10 o 5 -9 0 677.08 754.73 34.91 o 6 -9 0 1030.57 963.91 56.20 o 7 -9 0 840.13 874.91 58.71 o 8 -9 0 745.20 766.75 64.06 o 9 -9 0 1140.76 1172.34 97.30 o 10 -9 0 582.87 533.67 86.91 o 11 -9 0 166.94 92.33 58.95 o 12 -9 0 2.97 -49.02 49.02 o 13 -9 0 92.73 15.75 64.76 o 2 -8 0 5522.55 5381.65 108.53 o 3 -8 0 650.94 597.71 25.42 o 4 -8 0 108.68 132.70 23.23 o 5 -8 0 241.61 216.49 28.22 o 6 -8 0 12.03 30.14 23.24 o 7 -8 0 116.62 146.54 34.92 o 8 -8 0 69.95 48.69 33.79 o 9 -8 0 294.16 324.82 68.29 o 10 -8 0 620.07 467.32 81.90 o 11 -8 0 698.52 579.57 92.82 o 12 -8 0 382.05 331.71 85.06 o 13 -8 0 374.13 230.49 137.23 o 2 -7 0 3176.34 3205.61 70.94 o 3 -7 0 1093.97 979.88 32.94 o 4 -7 0 1095.97 1114.22 36.95 o 5 -7 0 1995.71 2064.88 71.67 o 6 -7 0 103.51 80.06 30.32 o 7 -7 0 771.02 716.90 54.09 o 8 -7 0 2053.09 2022.03 111.31 o 9 -7 0 998.80 1037.43 71.60 o 10 -7 0 243.91 198.27 71.24 o 11 -7 0 45.75 13.79 45.71 o 12 -7 0 64.42 163.29 68.98 o 13 -7 0 203.76 407.93 95.88 o 2 -6 0 2832.46 2768.47 61.00 o 3 -6 0 1464.28 1436.73 31.92 o 4 -6 0 271.54 323.16 21.56 o 5 -6 0 175.21 205.54 23.43 o 6 -6 0 108.32 116.06 29.47 o 7 -6 0 241.34 272.88 42.74 o 8 -6 0 75.91 79.61 36.66 o 9 -6 0 151.81 190.36 45.15 o 10 -6 0 880.26 863.69 167.95 o 11 -6 0 1166.39 1368.03 114.21 o 12 -6 0 422.38 351.66 149.73 o 13 -6 0 354.05 433.68 93.44 o 2 -5 0 839.68 802.54 26.36 o 3 -5 0 6464.02 6518.11 93.62 o 4 -5 0 3121.64 3144.04 54.47 o 5 -5 0 443.88 436.67 31.08 o 6 -5 0 407.39 459.14 31.81 o 7 -5 0 865.24 852.12 71.96 o 8 -5 0 1326.47 1336.75 119.35 o 9 -5 0 1147.74 1125.54 73.10 o 10 -5 0 354.24 296.47 66.82 o 11 -5 0 249.88 272.70 71.11 o 12 -5 0 8.37 138.18 59.93 o 13 -5 0 151.02 114.28 64.38 o 1 -4 0 17843.13 18228.52 511.32 o 2 -4 0 6336.21 6283.92 112.98 o 3 -4 0 1684.77 1711.30 32.90 o 4 -4 0 990.27 1035.80 26.51 o 5 -4 0 115.09 137.24 13.85 o 6 -4 0 10.55 2.30 10.92 o 7 -4 0 18.16 26.31 19.60 o 8 -4 0 36.05 -8.63 35.51 o 9 -4 0 295.46 308.85 48.73 o 10 -4 0 780.20 789.28 210.11 o 11 -4 0 883.84 1165.34 105.49 o 12 -4 0 365.42 220.42 68.35 o 13 -4 0 270.42 142.89 72.25 o 1 -3 0 7032.44 6983.20 148.24 o 2 -3 0 5701.88 5845.40 88.87 o 3 -3 0 2030.67 1971.98 36.35 o 4 -3 0 2532.16 2452.49 46.02 o 5 -3 0 242.65 234.97 16.44 o 6 -3 0 1144.58 1123.07 33.69 o 7 -3 0 782.70 797.49 43.39 o 8 -3 0 916.04 849.79 57.38 o 9 -3 0 996.60 1060.90 101.02 o 10 -3 0 552.99 497.62 120.88 o 11 -3 0 160.79 163.82 61.84 o 12 -3 0 34.53 19.36 52.96 o 13 -3 0 61.69 5.97 51.89 o 1 -2 0 14539.49 14702.96 291.02 o 2 -2 0 7540.46 7791.18 103.16 o 3 -2 0 1155.80 1113.04 25.60 o 4 -2 0 314.15 381.44 17.61 o 5 -2 0 51.82 58.92 12.91 o 6 -2 0 93.86 114.14 16.34 o 7 -2 0 120.29 145.86 19.83 o 8 -2 0 267.72 235.78 40.66 o 9 -2 0 183.91 182.90 39.25 o 10 -2 0 687.01 713.09 92.01 o 11 -2 0 1106.51 1249.31 102.93 o 12 -2 0 731.61 665.09 99.18 o 13 -2 0 346.55 285.82 83.62 o 1 -1 0 1748.89 1879.02 32.13 o 2 -1 0 7043.16 7320.55 97.92 o 3 -1 0 3704.15 3623.31 58.65 o 4 -1 0 460.42 390.75 24.34 o 5 -1 0 1337.95 1374.90 37.33 o 6 -1 0 1489.36 1548.98 43.80 o 7 -1 0 1109.03 1126.09 46.79 o 8 -1 0 1144.32 1144.26 54.37 o 9 -1 0 506.39 552.92 53.44 o 10 -1 0 463.36 429.53 70.92 o 11 -1 0 198.07 242.32 61.35 o 12 -1 0 10.29 88.31 58.09 o 13 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284.88 340.48 22.69 o 5 2 0 50.18 66.01 17.34 o 6 2 0 93.61 136.85 28.58 o 7 2 0 110.73 123.82 27.17 o 8 2 0 260.25 236.13 34.26 o 9 2 0 177.69 209.69 41.62 o 10 2 0 667.08 772.43 66.41 o 11 2 0 1115.63 1158.22 80.91 o 12 2 0 740.99 698.32 100.20 o 13 2 0 355.29 304.58 75.33 o 1 3 0 7054.57 7302.51 89.39 o 2 3 0 5470.04 5667.44 93.93 o 3 3 0 2081.32 2036.26 50.71 o 4 3 0 2627.49 2605.90 61.41 o 5 3 0 266.44 255.64 25.32 o 6 3 0 1100.75 1107.94 45.05 o 7 3 0 811.72 803.76 41.89 o 8 3 0 885.43 914.02 91.44 o 9 3 0 985.72 1088.45 82.03 o 10 3 0 550.19 503.75 62.12 o 11 3 0 156.29 123.69 51.07 o 12 3 0 34.56 8.47 40.38 o 13 3 0 64.97 65.07 59.62 o 0 4 0 11630.71 11965.26 173.36 o 1 4 0 17798.38 18325.47 210.82 o 2 4 0 6373.86 6450.09 121.57 o 3 4 0 1767.62 1855.48 47.47 o 4 4 0 985.22 1005.55 42.68 o 5 4 0 110.99 117.66 24.71 o 6 4 0 10.34 15.21 19.99 o 7 4 0 19.91 28.37 19.46 o 8 4 0 25.53 24.56 26.94 o 9 4 0 301.11 343.87 40.37 o 10 4 0 769.10 744.41 66.13 o 11 4 0 894.43 836.58 77.65 o 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174.76 27.00 o 7 7 0 770.42 884.75 48.63 o 8 7 0 2023.07 2092.18 76.25 o 9 7 0 1008.30 921.11 54.92 o 10 7 0 255.58 309.87 44.40 o 11 7 0 42.94 -15.89 32.69 o 12 7 0 63.77 -7.65 41.63 o 13 7 0 201.05 173.31 72.02 o 0 8 0 2924.80 2571.15 59.78 o 1 8 0 4839.34 4604.90 66.80 o 2 8 0 5498.34 5378.01 92.85 o 3 8 0 623.26 646.61 32.92 o 4 8 0 85.54 97.00 20.44 o 5 8 0 255.92 254.48 33.24 o 6 8 0 12.39 -10.16 16.68 o 7 8 0 124.23 90.70 26.15 o 8 8 0 77.74 67.88 27.21 o 9 8 0 289.26 335.32 43.35 o 10 8 0 620.01 603.31 58.53 o 11 8 0 673.04 752.39 80.26 o 12 8 0 388.72 245.59 76.17 o 13 8 0 382.83 404.51 150.55 o 1 9 0 2248.59 2319.43 57.99 o 2 9 0 2056.54 1882.88 49.25 o 3 9 0 2163.47 2087.40 93.74 o 4 9 0 875.02 919.59 42.82 o 5 9 0 728.07 856.42 43.55 o 6 9 0 1014.40 904.18 75.02 o 7 9 0 863.42 907.00 51.01 o 8 9 0 748.67 704.34 49.74 o 9 9 0 1120.25 1192.19 78.52 o 10 9 0 601.43 595.84 58.84 o 11 9 0 168.26 166.98 59.51 o 12 9 0 2.98 62.88 56.62 o 13 9 0 92.59 38.20 64.98 o 0 10 0 4245.16 4090.33 100.67 o 1 10 0 4773.67 4906.09 82.15 o 2 10 0 1576.62 1545.79 63.85 o 3 10 0 195.68 198.11 26.17 o 4 10 0 28.36 8.71 18.61 o 5 10 0 62.63 62.20 23.29 o 6 10 0 2.98 9.37 18.75 o 7 10 0 27.96 30.61 23.92 o 8 10 0 79.31 59.28 31.32 o 9 10 0 283.21 275.71 41.57 o 10 10 0 436.64 501.07 56.21 o 11 10 0 669.23 781.76 107.75 o 12 10 0 605.74 608.54 103.34 o 1 11 0 161.49 197.15 24.58 o 2 11 0 2162.06 2133.55 57.07 o 3 11 0 984.91 940.18 44.02 o 4 11 0 729.54 756.29 42.21 o 5 11 0 906.65 834.00 45.38 o 6 11 0 1013.69 970.73 54.86 o 7 11 0 566.40 533.40 49.41 o 8 11 0 893.85 900.61 55.87 o 9 11 0 519.23 532.88 55.99 o 10 11 0 205.56 240.65 53.34 o 11 11 0 77.63 81.28 49.66 o 12 11 0 2.14 -42.81 52.96 o 0 12 0 3242.26 3115.25 90.64 o 1 12 0 2038.17 2029.76 51.30 o 2 12 0 974.90 1000.58 42.18 o 3 12 0 422.67 438.75 47.57 o 4 12 0 13.15 19.76 19.82 o 5 12 0 8.06 3.83 19.32 o 6 12 0 36.68 39.21 23.77 o 7 12 0 127.51 130.86 43.29 o 8 12 0 83.60 61.78 31.89 o 9 12 0 116.39 52.58 36.43 o 10 12 0 436.73 637.61 184.92 o 11 12 0 536.54 521.02 98.19 o 12 12 0 635.93 729.84 270.03 o 1 13 0 436.35 487.30 29.60 o 2 13 0 1752.89 1789.91 56.16 o 3 13 0 641.75 573.25 42.04 o 4 13 0 1486.70 1368.22 91.00 o 5 13 0 1349.71 1289.09 70.17 o 6 13 0 879.39 907.34 52.92 o 7 13 0 335.58 288.45 40.31 o 8 13 0 717.61 782.24 59.79 o 9 13 0 548.80 567.57 102.47 o 10 13 0 309.58 274.64 59.06 o 11 13 0 219.13 270.22 82.69 o 0 14 0 2569.52 2537.03 85.81 o 1 14 0 1104.60 1145.11 60.66 o 2 14 0 1357.91 1275.44 49.26 o 3 14 0 666.62 621.34 42.43 o 4 14 0 26.47 -10.10 21.19 o 5 14 0 2.63 -20.33 20.33 o 6 14 0 8.08 -4.49 22.84 o 7 14 0 35.94 54.58 29.18 o 8 14 0 104.16 55.07 39.03 o 9 14 0 370.13 376.32 63.03 o 10 14 0 338.80 372.27 67.58 o 11 14 0 153.18 153.62 58.19 o 1 15 0 493.42 479.38 36.22 o 2 15 0 869.07 968.24 45.87 o 3 15 0 851.35 938.83 51.23 o 4 15 0 728.36 800.20 61.90 o 5 15 0 504.90 605.97 53.41 o 6 15 0 451.84 430.81 58.69 o 7 15 0 532.27 602.78 69.02 o 8 15 0 266.55 241.31 53.58 o 9 15 0 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