#------------------------------------------------------------------------------ #$Date: 2016-10-07 04:54:14 +0300 (Fri, 07 Oct 2016) $ #$Revision: 186996 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/06/2020614.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020614 _cell_angle_alpha 90.000 _cell_angle_beta 94.066 _cell_angle_gamma 90.000 _cell_length_a 8.9560 _cell_length_b 15.7745 _cell_length_c 28.4548 _exptl_crystal_F_000 1720.00 _reflns_d_resolution_high 0.7697 _cod_data_source_file yp3112I100Ksup3.hkl _cod_data_source_block I100K _shelx_title ' LS-Ph4P[Fe(py3CMe)(NCS)3]' _shelx_refln_list_code 4 _shelx_f_calc_maximum 274.34 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 40410.60 39719.15 1271.41 o 3 0 0 11291.25 10181.08 235.80 o 4 0 0 318.86 575.09 977.98 o 5 0 0 799.55 1207.00 45.79 o 6 0 0 3642.23 3716.55 146.76 o 7 0 0 2264.50 2244.91 83.38 o 8 0 0 7022.38 7702.97 272.32 o 9 0 0 241.07 242.72 33.96 o 10 0 0 65.62 8.92 25.73 o 11 0 0 199.92 332.03 130.07 o 1 1 0 9533.34 8203.03 136.15 o 2 1 0 69.16 90.19 6.85 o 3 1 0 4276.59 3693.48 80.82 o 4 1 0 3887.61 4153.56 87.11 o 5 1 0 57.52 127.67 16.54 o 6 1 0 1417.13 1633.10 39.39 o 7 1 0 281.62 290.49 19.49 o 8 1 0 754.76 697.58 56.14 o 9 1 0 14.63 11.48 8.63 o 10 1 0 292.41 336.02 49.70 o 11 1 0 78.56 153.44 69.94 o 1 2 0 32428.42 33370.76 522.61 o 2 2 0 34816.01 34905.55 389.00 o 3 2 0 297.56 228.27 184.98 o 4 2 0 1690.56 1396.82 53.46 o 5 2 0 3891.63 3431.17 61.81 o 6 2 0 2260.61 2277.11 94.03 o 7 2 0 2768.59 2910.42 56.01 o 8 2 0 3131.12 3421.47 158.91 o 9 2 0 411.23 413.70 42.38 o 10 2 0 1867.32 2566.84 336.40 o 11 2 0 380.38 547.17 313.38 o 1 3 0 84.96 117.44 11.93 o 2 3 0 38.75 50.00 8.54 o 3 3 0 1111.55 1091.62 77.81 o 4 3 0 1610.92 1555.91 40.92 o 5 3 0 1438.56 1333.74 63.03 o 6 3 0 62.89 52.84 10.48 o 7 3 0 0.50 11.49 6.46 o 8 3 0 227.72 232.59 27.68 o 9 3 0 457.16 330.39 41.41 o 10 3 0 24.80 29.55 22.28 o 11 3 0 273.89 282.95 66.81 o 0 4 0 3633.53 3708.77 92.65 o 1 4 0 5696.47 4981.14 111.79 o 2 4 0 12851.17 12017.75 129.57 o 3 4 0 6943.04 6164.39 120.32 o 4 4 0 9167.83 9014.62 160.01 o 5 4 0 2672.48 2776.82 107.04 o 6 4 0 17099.44 18243.12 444.01 o 7 4 0 2203.98 2430.15 92.47 o 8 4 0 29.06 42.52 11.77 o 9 4 0 3349.43 3767.02 328.49 o 10 4 0 453.98 564.99 105.58 o 11 4 0 44.12 39.24 48.00 o 1 5 0 6297.35 5964.69 92.93 o 2 5 0 2923.92 2642.66 62.85 o 3 5 0 26.02 28.37 5.39 o 4 5 0 2343.87 2304.23 53.08 o 5 5 0 447.01 395.01 38.78 o 6 5 0 722.51 605.93 45.79 o 7 5 0 1171.43 1143.35 105.98 o 8 5 0 91.45 96.37 17.05 o 9 5 0 62.61 117.82 53.99 o 10 5 0 239.44 209.01 36.85 o 11 5 0 23.62 66.95 40.39 o 0 6 0 1060.03 1238.27 65.25 o 1 6 0 15530.99 14621.09 202.93 o 2 6 0 7575.72 7413.83 126.44 o 3 6 0 2860.21 2813.44 111.09 o 4 6 0 48767.83 51949.46 191.39 o 5 6 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15.24 24.17 o 9 9 0 32.73 107.95 41.20 o 10 9 0 46.78 87.54 47.95 o 0 10 0 50.21 43.23 21.50 o 1 10 0 349.59 304.70 24.46 o 2 10 0 13899.67 14354.84 223.07 o 3 10 0 4693.82 4706.12 98.50 o 4 10 0 1941.19 1870.82 45.17 o 5 10 0 6319.81 6825.17 182.49 o 6 10 0 671.94 607.30 87.17 o 7 10 0 366.99 300.06 44.95 o 8 10 0 1530.17 1734.16 185.94 o 9 10 0 174.73 257.62 56.81 o 10 10 0 112.97 146.57 47.66 o 1 11 0 831.17 875.67 61.29 o 2 11 0 196.26 193.05 22.26 o 3 11 0 1478.98 1626.99 97.29 o 4 11 0 638.08 581.51 42.01 o 5 11 0 438.07 427.89 47.81 o 6 11 0 9.07 13.90 9.38 o 7 11 0 0.07 32.13 56.57 o 8 11 0 53.12 37.85 35.69 o 9 11 0 4.40 22.45 33.98 o 0 12 0 20080.06 21051.57 348.97 o 1 12 0 680.73 660.60 51.48 o 2 12 0 1917.31 1942.11 76.63 o 3 12 0 9896.35 10875.11 111.07 o 4 12 0 1162.66 1116.38 88.52 o 5 12 0 257.33 276.01 37.18 o 6 12 0 2.71 10.60 15.87 o 7 12 0 138.59 161.16 69.66 o 8 12 0 761.13 488.08 103.05 o 9 12 0 395.36 497.74 128.37 o 1 13 0 475.49 479.75 34.20 o 2 13 0 1313.28 1481.09 104.13 o 3 13 0 5.56 46.27 11.64 o 4 13 0 208.45 209.61 30.42 o 5 13 0 137.25 91.33 21.04 o 6 13 0 935.40 833.03 132.04 o 7 13 0 3.68 -22.45 57.84 o 8 13 0 383.40 428.51 80.90 o 0 14 0 969.82 849.81 100.78 o 1 14 0 2665.53 2759.89 166.23 o 2 14 0 2492.97 2718.06 79.41 o 3 14 0 363.79 238.44 42.61 o 4 14 0 920.55 848.09 68.85 o 5 14 0 33.17 10.44 16.27 o 6 14 0 15.05 33.99 20.12 o 7 14 0 995.69 881.49 178.25 o 8 14 0 305.11 361.48 79.20 o 1 15 0 3459.46 3686.09 137.79 o 2 15 0 9.57 37.21 15.36 o 3 15 0 324.76 323.09 43.76 o 4 15 0 90.11 63.70 14.55 o 5 15 0 8.85 33.68 21.87 o 6 15 0 0.63 32.87 47.44 o 7 15 0 59.68 81.00 36.02 o 0 16 0 234.61 211.97 38.05 o 1 16 0 1189.69 1084.75 117.61 o 2 16 0 216.66 255.17 37.67 o 3 16 0 525.26 293.23 79.89 o 4 16 0 1705.98 1764.66 173.25 o 5 16 0 198.01 113.25 31.45 o 6 16 0 82.40 95.51 47.58 o 7 16 0 599.93 541.34 123.55 o 1 17 0 128.09 120.78 27.73 o 2 17 0 315.67 267.97 38.40 o 3 17 0 840.66 748.70 99.64 o 4 17 0 51.18 92.10 23.60 o 5 17 0 8.84 40.39 32.08 o 6 17 0 61.57 97.99 39.29 o 0 18 0 875.92 1039.53 964.65 o 1 18 0 1853.40 2298.25 231.40 o 2 18 0 338.06 446.33 57.04 o 3 18 0 69.64 110.60 22.19 o 4 18 0 683.67 633.85 114.84 o 5 18 0 1.34 37.84 43.53 o 1 19 0 64.01 94.23 28.63 o 2 19 0 479.57 379.75 51.60 o 3 19 0 455.21 399.10 78.95 o 4 19 0 509.12 327.01 93.77 o 0 20 0 1099.41 855.32 277.49 o 1 20 0 0.37 -13.04 32.11 o 2 20 0 3.84 31.80 23.96 o -11 1 1 76.35 83.46 58.01 o -10 1 1 31.09 51.40 14.99 o -9 1 1 1167.17 1153.33 54.33 o -8 1 1 81.59 87.24 10.17 o -7 1 1 548.43 568.05 29.91 o -6 1 1 765.97 826.53 36.34 o -5 1 1 377.48 373.10 23.38 o -4 1 1 154.95 133.46 8.83 o -3 1 1 71.17 58.96 6.98 o -2 1 1 5634.06 5126.88 75.94 o -1 1 1 25.60 36.39 7.04 o 0 1 1 336.73 271.85 9.95 o 1 1 1 2.45 13.75 3.50 o 2 1 1 980.74 851.64 30.90 o 3 1 1 6485.78 6123.09 98.90 o 4 1 1 312.79 297.76 17.44 o 5 1 1 4055.95 3950.83 76.56 o 6 1 1 482.09 504.80 27.64 o 7 1 1 1051.81 1125.11 55.40 o 8 1 1 629.32 660.63 37.85 o 9 1 1 14.61 6.00 11.81 o 10 1 1 0.11 4.69 19.95 o 11 1 1 169.05 216.58 55.58 o -11 2 1 134.82 93.85 30.16 o -10 2 1 998.01 1014.10 139.84 o -9 2 1 26.89 46.61 13.08 o -8 2 1 7.08 11.14 10.35 o -7 2 1 26.78 45.84 12.51 o -6 2 1 82.23 81.24 7.73 o -5 2 1 122.99 115.19 8.71 o -4 2 1 1760.21 1698.41 39.29 o -3 2 1 697.77 558.25 16.93 o -2 2 1 7761.45 7365.94 114.40 o -1 2 1 1221.84 1010.38 34.55 o 0 2 1 803.70 618.59 21.44 o 1 2 1 3560.11 3129.25 66.47 o 2 2 1 5507.10 5109.37 86.46 o 3 2 1 3436.85 3196.06 72.39 o 4 2 1 539.79 512.01 30.93 o 5 2 1 3115.41 3308.30 44.56 o 6 2 1 1888.15 1690.43 73.25 o 7 2 1 468.30 484.37 35.73 o 8 2 1 161.01 155.08 15.99 o 9 2 1 358.08 323.58 38.47 o 10 2 1 58.96 52.09 18.45 o 11 2 1 27.01 68.86 38.04 o -11 3 1 20.57 34.85 45.23 o -10 3 1 271.71 283.60 54.71 o -9 3 1 164.19 125.85 21.64 o -8 3 1 2240.77 2248.91 87.15 o -7 3 1 3322.80 3605.54 132.84 o -6 3 1 65.92 50.80 8.02 o -5 3 1 2831.79 2928.89 39.20 o -4 3 1 9593.35 9628.23 155.08 o -3 3 1 1294.80 1316.63 53.85 o 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657.43 562.39 90.01 o 10 4 1 51.27 47.72 23.27 o 11 4 1 33.68 43.85 30.61 o -11 5 1 766.06 1040.08 271.22 o -10 5 1 57.89 31.85 29.45 o -9 5 1 381.88 288.53 54.62 o -8 5 1 5.07 34.12 15.71 o -7 5 1 2078.57 2048.07 116.21 o -6 5 1 251.76 232.34 23.75 o -5 5 1 485.37 505.19 39.80 o -4 5 1 672.35 655.89 40.29 o -3 5 1 10746.46 11562.48 206.76 o -2 5 1 4354.52 4033.55 82.05 o -1 5 1 15423.69 14577.82 188.07 o 0 5 1 819.79 745.40 33.33 o 1 5 1 3246.61 2787.00 63.56 o 2 5 1 4220.67 4020.31 73.02 o 3 5 1 559.50 515.04 38.98 o 4 5 1 374.28 347.59 30.62 o 5 5 1 11.15 31.83 12.04 o 6 5 1 1458.81 1511.25 115.55 o 7 5 1 405.70 387.43 48.72 o 8 5 1 32.45 43.64 20.19 o 9 5 1 215.35 252.92 47.69 o 10 5 1 113.83 149.16 28.64 o 11 5 1 22.23 69.61 36.60 o -11 6 1 111.02 126.42 47.22 o -10 6 1 0.50 2.08 40.22 o -9 6 1 1.12 52.20 21.75 o -8 6 1 120.43 115.10 23.33 o -7 6 1 670.46 615.95 84.16 o -6 6 1 1623.71 1828.19 1623.72 o -5 6 1 1211.79 1157.68 88.64 o -4 6 1 5041.78 4990.36 69.33 o -3 6 1 2198.36 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97.35 32.57 o -10 8 1 10.39 54.14 36.80 o -9 8 1 120.84 69.40 36.75 o -8 8 1 235.04 225.14 60.13 o -7 8 1 1465.85 1331.23 190.34 o -6 8 1 11661.12 13045.16 276.52 o -5 8 1 1473.18 1483.50 45.05 o -4 8 1 894.81 1021.46 56.17 o -3 8 1 2429.89 2331.55 84.12 o -2 8 1 2141.50 2514.39 284.68 o -1 8 1 1582.50 1777.39 65.28 o 0 8 1 990.94 1075.63 46.01 o 1 8 1 2960.35 3077.32 124.26 o 2 8 1 4771.89 4593.80 74.86 o 3 8 1 968.99 989.55 36.06 o 4 8 1 1752.05 1695.09 71.63 o 5 8 1 0.68 23.63 18.20 o 6 8 1 5598.21 5740.24 157.12 o 7 8 1 294.69 295.43 39.95 o 8 8 1 6.23 47.66 19.82 o 9 8 1 10.97 -0.05 41.34 o 10 8 1 1144.27 1112.89 275.48 o -10 9 1 451.32 481.06 94.98 o -9 9 1 165.86 88.42 43.58 o -8 9 1 1324.40 1333.70 275.69 o -7 9 1 0.31 -26.46 27.41 o -6 9 1 929.93 934.73 108.70 o -5 9 1 306.68 302.50 27.70 o -4 9 1 136.61 143.28 9.96 o -3 9 1 4560.80 4567.70 104.49 o -2 9 1 15.99 37.49 8.82 o -1 9 1 344.10 319.59 24.29 o 0 9 1 5228.44 5059.50 119.45 o 1 9 1 64.60 77.87 9.85 o 2 9 1 56.72 57.72 10.30 o 3 9 1 3167.42 3270.07 107.77 o 4 9 1 640.14 662.69 41.53 o 5 9 1 119.53 120.90 15.58 o 6 9 1 1111.97 1226.96 153.45 o 7 9 1 25.10 58.80 30.73 o 8 9 1 35.30 43.74 29.97 o 9 9 1 121.77 109.25 34.87 o 10 9 1 25.72 50.61 37.68 o -10 10 1 4.36 56.46 29.04 o -9 10 1 967.06 1140.90 204.02 o -8 10 1 540.74 476.54 143.64 o -7 10 1 17.16 27.61 24.96 o -6 10 1 67.18 51.16 9.13 o -5 10 1 457.78 516.93 55.36 o -4 10 1 2584.20 2581.57 79.39 o -3 10 1 1521.76 1424.88 63.85 o -2 10 1 21.08 29.25 8.60 o -1 10 1 1965.86 1806.28 125.93 o 0 10 1 3644.53 3549.72 108.27 o 1 10 1 226.97 255.45 21.24 o 2 10 1 1484.17 1516.10 51.28 o 3 10 1 1172.12 1234.33 54.30 o 4 10 1 2868.48 2844.49 69.14 o 5 10 1 3118.15 3164.52 107.87 o 6 10 1 28.78 33.32 26.55 o 7 10 1 147.21 111.89 41.52 o 8 10 1 21.76 24.42 28.39 o 9 10 1 101.84 65.83 46.18 o 10 10 1 362.47 209.58 94.09 o -9 11 1 17.50 -0.09 46.25 o -8 11 1 377.39 354.56 65.12 o -7 11 1 286.29 213.53 47.71 o -6 11 1 4.43 10.62 10.53 o -5 11 1 194.32 210.53 35.73 o -4 11 1 3899.24 4414.88 59.87 o -3 11 1 1166.31 1234.27 73.08 o -2 11 1 1.59 19.16 7.73 o -1 11 1 1069.86 1001.59 64.21 o 0 11 1 354.07 374.44 52.32 o 1 11 1 350.48 361.57 29.19 o 2 11 1 5547.46 5689.35 107.76 o 3 11 1 0.90 25.80 11.51 o 4 11 1 127.47 111.89 13.31 o 5 11 1 446.98 513.88 49.84 o 6 11 1 3.63 21.49 19.94 o 7 11 1 30.56 31.83 32.18 o 8 11 1 698.64 662.41 114.01 o 9 11 1 68.16 104.65 42.88 o -9 12 1 217.12 161.76 49.45 o -8 12 1 1467.14 1469.28 232.17 o -7 12 1 261.11 241.10 73.13 o -6 12 1 101.47 61.24 26.16 o -5 12 1 5719.17 6529.15 95.80 o -4 12 1 478.07 713.19 147.34 o -3 12 1 55.69 77.55 10.85 o -2 12 1 7221.54 7971.98 147.38 o -1 12 1 786.21 846.13 62.98 o 0 12 1 290.01 317.73 26.07 o 1 12 1 1146.07 1209.61 96.39 o 2 12 1 315.12 384.16 35.17 o 3 12 1 2376.70 2557.43 176.81 o 4 12 1 161.31 129.01 15.30 o 5 12 1 99.86 100.46 14.88 o 6 12 1 3570.54 221.44 1441.52 o 7 12 1 294.84 183.82 63.67 o 8 12 1 254.04 160.37 45.15 o 9 12 1 12.39 40.00 31.63 o -8 13 1 57.73 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