#------------------------------------------------------------------------------ #$Date: 2016-10-07 04:54:14 +0300 (Fri, 07 Oct 2016) $ #$Revision: 186996 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/06/2020615.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2020615 _cell_angle_alpha 90.000 _cell_angle_beta 93.316 _cell_angle_gamma 90.000 _cell_length_a 9.0689 _cell_length_b 15.9837 _cell_length_c 28.8204 _exptl_crystal_F_000 1720.00 _reflns_d_resolution_high 0.8201 _cod_data_source_file yp3112I296Ksup4.hkl _cod_data_source_block I296K _shelx_title ' yama_red_EtOH' _shelx_refln_list_code 4 _shelx_f_calc_maximum 381.48 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 44302.05 43998.20 1297.97 o 3 0 0 8127.37 8046.65 198.95 o 4 0 0 587.40 728.42 75.12 o 5 0 0 427.68 649.38 84.46 o 6 0 0 1990.77 2047.18 162.33 o 7 0 0 877.35 974.73 119.06 o 9 0 0 6.65 -87.63 215.09 o 10 0 0 7.65 -64.35 242.54 o 1 1 0 8579.50 7961.27 171.38 o 2 1 0 481.60 509.99 43.65 o 3 1 0 2815.51 2743.08 77.47 o 4 1 0 1919.34 2112.28 65.75 o 5 1 0 1279.54 1637.22 98.82 o 6 1 0 2553.37 2633.08 104.19 o 7 1 0 214.20 115.90 92.00 o 8 1 0 3.33 82.48 108.92 o 9 1 0 5.61 10.46 220.83 o 10 1 0 2.25 139.49 245.58 o 11 1 0 36.83 139.52 197.46 o 1 2 0 30883.33 29959.53 549.78 o 2 2 0 28669.54 29478.35 545.53 o 3 2 0 257.75 220.69 50.48 o 4 2 0 1620.81 1730.27 73.90 o 5 2 0 1667.02 1589.96 83.52 o 6 2 0 1287.88 1294.15 89.84 o 7 2 0 1643.46 1699.68 109.18 o 8 2 0 721.75 768.34 113.18 o 9 2 0 11.41 9.00 211.27 o 10 2 0 161.54 447.39 258.51 o 1 3 0 1.64 40.43 55.63 o 2 3 0 266.23 313.17 59.91 o 3 3 0 2212.21 2402.31 97.51 o 4 3 0 308.46 344.12 62.00 o 5 3 0 141.64 158.81 68.98 o 6 3 0 518.35 522.07 86.53 o 7 3 0 232.82 291.64 95.27 o 8 3 0 4.39 46.49 111.50 o 9 3 0 2.91 -43.73 124.72 o 10 3 0 1.01 20.92 242.31 o 1 4 0 4525.18 4359.29 168.85 o 2 4 0 12021.65 11625.52 244.88 o 3 4 0 4306.93 4289.92 129.50 o 4 4 0 7649.34 7643.93 233.37 o 5 4 0 1834.86 2077.84 92.14 o 6 4 0 7533.82 7394.52 165.22 o 7 4 0 859.49 737.91 105.33 o 8 4 0 20.32 102.85 109.87 o 9 4 0 516.28 428.80 132.90 o 10 4 0 4.48 87.41 170.56 o 1 5 0 5150.47 5020.44 105.15 o 2 5 0 4679.40 4532.76 183.82 o 3 5 0 643.97 580.14 81.39 o 4 5 0 176.38 253.49 89.90 o 5 5 0 846.31 824.29 80.80 o 6 5 0 1.73 35.51 104.85 o 7 5 0 429.43 421.07 102.00 o 8 5 0 2.70 -38.59 205.98 o 9 5 0 277.39 269.64 135.12 o 10 5 0 78.65 154.72 147.89 o 0 6 0 558.18 631.21 91.01 o 1 6 0 12078.94 11516.46 321.28 o 2 6 0 5235.73 5398.99 149.78 o 3 6 0 2058.34 2036.45 104.74 o 4 6 0 28657.83 29200.77 559.44 o 5 6 0 4902.68 4773.94 165.99 o 6 6 0 1134.89 1204.61 102.42 o 7 6 0 79.16 168.99 135.27 o 8 6 0 17.97 63.14 119.17 o 9 6 0 14.01 46.07 133.07 o 10 6 0 0.11 60.17 186.14 o 1 7 0 450.31 329.72 106.08 o 2 7 0 613.07 621.37 85.61 o 3 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269.49 157.71 o 7 10 0 43.19 131.87 126.86 o 8 10 0 264.95 321.75 147.81 o 9 10 0 0.38 35.90 160.01 o 1 11 0 401.38 387.73 57.25 o 2 11 0 304.50 410.61 163.79 o 3 11 0 418.82 456.30 60.11 o 4 11 0 4.36 -15.77 140.63 o 5 11 0 5.22 -61.76 224.54 o 6 11 0 5.00 62.83 178.01 o 7 11 0 53.66 -66.83 190.89 o 8 11 0 32.23 -26.55 184.68 o 9 11 0 4.40 64.87 170.55 o 0 12 0 7214.25 7753.49 302.16 o 1 12 0 246.44 301.26 57.90 o 2 12 0 492.60 578.90 179.20 o 3 12 0 3185.34 3115.21 238.49 o 4 12 0 348.78 436.10 152.45 o 5 12 0 0.92 -14.44 174.07 o 6 12 0 33.62 64.23 268.08 o 7 12 0 0.20 -4.13 203.13 o 8 12 0 135.50 92.32 230.21 o 1 13 0 774.15 723.51 62.86 o 2 13 0 360.88 231.29 177.97 o 3 13 0 63.07 63.90 205.87 o 4 13 0 233.76 259.66 67.09 o 5 13 0 207.48 209.05 92.42 o 6 13 0 184.39 176.84 201.17 o 7 13 0 0.44 -142.08 311.84 o 8 13 0 43.62 168.10 176.02 o 0 14 0 487.65 262.34 179.20 o 1 14 0 1129.65 1149.17 141.28 o 2 14 0 616.46 587.38 80.50 o 3 14 0 17.29 106.20 219.70 o 4 14 0 102.53 168.40 246.36 o 5 14 0 83.03 100.38 82.54 o 6 14 0 62.86 59.44 209.15 o 7 14 0 234.81 238.58 234.39 o 1 15 0 675.78 807.11 151.61 o 2 15 0 49.62 221.95 204.18 o 3 15 0 161.22 224.65 218.35 o 4 15 0 8.77 -219.03 264.25 o 5 15 0 31.48 121.72 291.92 o 6 15 0 1.04 108.00 318.92 o 7 15 0 64.68 141.86 244.37 o 0 16 0 24.31 -14.74 209.47 o 1 16 0 60.32 99.56 231.40 o 2 16 0 0.93 -1.19 64.41 o 3 16 0 127.45 87.97 165.38 o 4 16 0 250.94 357.28 294.74 o 5 16 0 58.79 292.94 312.62 o 6 16 0 25.60 -22.84 340.18 o 1 17 0 4.48 -8.74 163.96 o 2 17 0 76.31 264.25 249.51 o 3 17 0 63.81 68.46 102.62 o 4 17 0 18.15 164.81 282.59 o 5 17 0 7.08 36.34 327.59 o 0 18 0 11.67 108.45 258.85 o 1 18 0 96.63 155.04 181.46 o 2 18 0 5.93 71.26 191.84 o 3 18 0 6.21 87.98 196.95 o 4 18 0 72.50 58.38 202.89 o 1 19 0 91.00 -7.22 195.79 o 2 19 0 39.47 46.31 212.36 o -10 1 1 42.19 34.64 177.41 o -9 1 1 115.27 155.58 219.48 o -8 1 1 0.51 13.34 108.05 o -7 1 1 139.96 152.25 113.26 o -6 1 1 169.29 256.96 83.55 o -5 1 1 319.80 317.85 70.13 o -4 1 1 85.04 66.69 55.61 o -3 1 1 45.13 151.49 52.39 o -2 1 1 5471.66 5491.60 110.26 o -1 1 1 0.31 23.82 37.22 o 1 1 1 3.63 7.46 36.03 o 2 1 1 1133.38 1128.92 43.08 o 3 1 1 5448.79 5437.55 138.71 o 4 1 1 40.86 34.64 51.24 o 5 1 1 2173.75 2239.20 74.68 o 6 1 1 425.36 453.22 79.15 o 7 1 1 152.02 172.72 90.60 o 8 1 1 101.70 149.33 106.76 o 9 1 1 2.71 50.24 119.86 o 10 1 1 6.53 23.62 244.34 o 11 1 1 37.74 -21.71 266.95 o -10 2 1 134.75 193.91 180.45 o -9 2 1 30.29 120.19 158.97 o -8 2 1 26.11 52.09 110.15 o -7 2 1 21.05 -10.05 97.57 o -6 2 1 87.80 149.34 81.71 o -5 2 1 244.98 317.16 87.76 o -4 2 1 406.01 499.61 62.82 o -3 2 1 555.90 496.06 54.38 o -2 2 1 9988.88 10406.97 220.54 o -1 2 1 1311.48 1163.08 58.98 o 0 2 1 1314.13 1160.35 105.30 o 1 2 1 4459.64 4521.88 114.82 o 2 2 1 5476.21 5568.84 138.13 o 3 2 1 1988.37 1983.26 86.60 o 4 2 1 472.94 468.89 58.59 o 5 2 1 3304.66 3401.89 127.79 o 6 2 1 256.49 242.39 78.48 o 7 2 1 179.65 202.90 94.21 o 8 2 1 4.13 -38.80 124.96 o 9 2 1 11.64 74.57 151.21 o 10 2 1 6.96 125.43 230.16 o -10 3 1 2.50 -128.36 257.73 o -9 3 1 71.94 91.32 129.50 o -8 3 1 747.25 811.64 120.09 o -7 3 1 1073.79 961.01 104.69 o -6 3 1 100.75 120.03 102.91 o -5 3 1 1739.97 1753.49 87.26 o -4 3 1 5512.35 5617.12 126.79 o -3 3 1 687.62 699.50 74.41 o -2 3 1 2614.12 2663.36 94.54 o -1 3 1 2835.10 3012.40 92.83 o 0 3 1 334.96 270.47 32.57 o 1 3 1 194.71 274.00 77.28 o 2 3 1 768.58 779.73 71.15 o 3 3 1 2.04 14.68 64.06 o 4 3 1 1292.77 1185.61 107.60 o 5 3 1 143.23 154.31 67.36 o 6 3 1 41.15 62.17 82.20 o 7 3 1 41.95 163.44 93.11 o 8 3 1 3.01 50.00 140.80 o 9 3 1 130.24 187.38 159.10 o 10 3 1 45.87 44.24 170.91 o -10 4 1 20.47 15.94 147.34 o -9 4 1 2.94 40.98 132.91 o -8 4 1 385.97 503.02 142.25 o -7 4 1 338.44 445.46 104.43 o -6 4 1 22.70 -6.09 87.41 o -5 4 1 37.57 66.11 75.30 o -4 4 1 2031.84 1905.22 103.77 o -3 4 1 5612.02 5789.78 153.68 o -2 4 1 9471.54 9388.91 207.34 o -1 4 1 9577.75 9794.18 306.61 o 0 4 1 149.19 204.21 30.17 o 1 4 1 29547.15 29749.67 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247.82 59.59 o 2 9 1 139.09 131.48 53.43 o 3 9 1 2525.25 2471.49 135.33 o 4 9 1 278.85 216.48 124.92 o 5 9 1 129.46 154.98 138.88 o 6 9 1 354.54 355.30 151.46 o 7 9 1 12.89 89.26 119.41 o 8 9 1 0.75 80.09 163.68 o 9 9 1 35.48 53.23 155.27 o -9 10 1 261.45 237.28 165.34 o -8 10 1 599.88 611.76 152.79 o -7 10 1 35.79 116.97 127.45 o -6 10 1 408.55 381.57 163.01 o -5 10 1 1238.15 1347.98 160.30 o -4 10 1 1402.07 1484.30 145.47 o -3 10 1 1840.99 1843.14 80.21 o -2 10 1 736.63 728.65 88.05 o -1 10 1 1262.05 1267.82 149.62 o 0 10 1 1616.97 1740.54 109.37 o 1 10 1 0.74 14.18 50.41 o 2 10 1 677.40 755.97 156.14 o 3 10 1 426.11 539.93 67.03 o 4 10 1 1332.28 1375.22 144.14 o 5 10 1 677.98 720.27 156.87 o 6 10 1 70.30 151.52 162.25 o 7 10 1 237.24 236.88 126.52 o 8 10 1 242.21 189.24 146.30 o 9 10 1 192.78 211.95 157.03 o -9 11 1 12.74 48.75 172.97 o -8 11 1 44.37 56.46 157.42 o -7 11 1 4.30 81.64 177.77 o -6 11 1 0.01 1.01 179.87 o -5 11 1 0.31 85.56 158.73 o -4 11 1 1325.47 1604.52 198.33 o -3 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