#------------------------------------------------------------------------------ #$Date: 2019-05-24 05:18:40 +0300 (Fri, 24 May 2019) $ #$Revision: 215469 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/16/2021648.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021648 loop_ _publ_author_name 'Kiran Kumar, Haruvegowda' 'Yathirajan, Hemmige S.' 'Manju, Nagaraj' 'Kalluraya, Balakrishna' 'Rathore, Ravindranath S.' 'Glidewell, Christopher' _publ_section_title ; Conversion of substituted 5-aryloxypyrazolecarbaldehydes into reduced 3,4'-bipyrazoles: synthesis and characterization, and the structures of four precursors and two products, and their supramolecular assembly in zero, one and two dimensions ; _journal_coeditor_code KY3177 _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229619006752 _journal_volume 75 _journal_year 2019 _chemical_formula_iupac 'C21 H16 N2 O2' _chemical_formula_moiety 'C21 H16 N2 O2' _chemical_formula_sum 'C21 H16 N2 O2' _chemical_formula_weight 328.36 _chemical_name_systematic ; 3-Methyl-5-(naphthalen-2-yloxy)-1-phenyl-1H-pyrazole-4-carbaldehyde ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014 _cell_angle_alpha 90 _cell_angle_beta 106.079(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.7302(6) _cell_length_b 17.2550(16) _cell_length_c 13.1989(11) _cell_measurement_reflns_used 4456 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 28.962 _cell_measurement_theta_min 1.993 _cell_volume 1691.7(2) _computing_cell_refinement ; SAINT (Bruker, 2015) ; _computing_data_collection ; APEX2 (Bruker, 2015) ; _computing_data_reduction ; SAINT (Bruker, 2015) ; _computing_molecular_graphics ; PLATON (Spek, 2009) ; _computing_publication_material ; SHELXL2014 (Sheldrick, 2015b) and PLATON (Spek, 2009) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296(2) _diffrn_detector_area_resol_mean 0.3333 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0485 _diffrn_reflns_av_unetI/netI 0.0336 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 34394 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.547 _diffrn_reflns_theta_min 2.361 _diffrn_source 'fine focus sealed tube' _diffrn_standards_decay_% 0 _diffrn_standards_interval_count 0 _diffrn_standards_interval_time 0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.084 _exptl_absorpt_correction_T_max 0.988 _exptl_absorpt_correction_T_min 0.954 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Bruker, 2015) ; _exptl_crystal_colour brown _exptl_crystal_density_diffrn 1.289 _exptl_crystal_description block _exptl_crystal_F_000 688 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.160 _exptl_crystal_size_min 0.140 _refine_diff_density_max 0.168 _refine_diff_density_min -0.246 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.031 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 227 _refine_ls_number_reflns 4311 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.031 _refine_ls_R_factor_all 0.0905 _refine_ls_R_factor_gt 0.0474 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0511P)^2^+0.4490P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1043 _refine_ls_wR_factor_ref 0.1297 _reflns_number_gt 2711 _reflns_number_total 4311 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ky3177sup1.cif _cod_data_source_block V _cod_database_code 2021648 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.983 _shelx_estimated_absorpt_t_max 0.988 _shelx_hkl_file ; 1 0 0 -0.80 0.20 1 0 0 -1.30 0.50 -2 0 0 1535.75 33.80 2 0 0 1487.05 33.10 2 0 0 1527.65 33.60 2 0 0 1537.65 33.70 3 0 0 -0.50 0.30 -3 0 0 0.20 0.20 3 0 0 -0.40 0.40 3 0 0 -0.50 0.60 -3 0 0 0.40 0.50 3 0 0 -0.40 0.60 4 0 0 415.06 12.60 4 0 0 408.46 9.50 4 0 0 419.76 9.60 4 0 0 403.96 12.10 -4 0 0 388.06 9.80 -4 0 0 418.16 10.00 5 0 0 -0.80 1.30 5 0 0 -0.50 0.40 -5 0 0 -0.20 0.70 5 0 0 -0.30 1.10 -6 0 0 29.60 1.80 -6 0 0 35.40 2.10 6 0 0 33.90 3.30 6 0 0 32.00 3.70 7 0 0 0.40 1.40 7 0 0 1.70 1.40 7 0 0 0.00 1.50 -7 0 0 -1.40 0.80 8 0 0 9.80 2.40 8 0 0 11.30 2.80 9 0 0 1.80 2.60 10 0 0 6.50 3.30 0 -1 0 -0.30 0.10 0 -1 0 -0.30 0.10 0 -1 0 -0.20 0.10 0 -1 0 -0.40 0.10 0 -1 0 -0.20 0.10 0 -1 0 -0.40 0.10 0 1 0 -0.30 0.10 0 1 0 -0.50 0.10 0 1 0 -0.40 0.10 0 1 0 -0.30 0.10 0 1 0 -0.40 0.10 0 1 0 -0.30 0.10 -1 -1 0 3.50 0.50 1 -1 0 4.40 0.40 1 -1 0 3.60 0.30 1 -1 0 2.40 0.40 -1 -1 0 3.00 0.50 -1 -1 0 4.60 0.50 -1 -1 0 3.50 0.50 -1 -1 0 2.80 0.50 1 1 0 4.20 0.50 1 1 0 3.10 0.50 1 1 0 4.20 0.50 1 1 0 6.70 0.60 -1 1 0 3.70 0.50 1 1 0 3.50 0.40 -1 1 0 3.70 0.50 -2 -1 0 77.99 2.90 2 -1 0 79.99 2.20 2 -1 0 78.39 3.00 -2 -1 0 78.69 2.40 2 -1 0 82.89 2.20 2 1 0 82.59 2.30 2 1 0 81.69 2.80 2 1 0 81.19 2.80 2 1 0 80.79 2.30 2 1 0 79.09 3.20 -2 1 0 79.69 2.30 3 -1 0 79.29 2.20 3 -1 0 78.99 3.40 3 -1 0 78.39 3.20 -3 -1 0 77.99 2.60 3 -1 0 77.39 2.30 -3 -1 0 74.89 3.30 3 1 0 77.69 3.30 -3 1 0 77.39 2.50 3 1 0 79.99 3.60 3 1 0 79.39 2.40 3 1 0 80.79 2.40 4 -1 0 57.29 1.80 4 -1 0 54.29 1.70 -4 -1 0 57.69 2.30 4 -1 0 55.69 3.20 4 1 0 55.09 3.40 -4 1 0 54.69 2.20 4 1 0 55.69 1.90 -4 1 0 55.59 2.00 4 1 0 56.09 2.80 4 1 0 57.09 2.10 -5 -1 0 17.90 1.40 5 -1 0 18.40 2.30 -5 -1 0 15.50 1.60 5 -1 0 14.50 2.30 5 -1 0 15.90 0.80 5 1 0 18.60 1.10 -5 1 0 17.90 1.50 5 1 0 20.50 2.50 -5 1 0 15.70 1.30 5 1 0 17.80 2.10 5 1 0 18.40 2.40 6 -1 0 30.80 3.60 -6 -1 0 33.30 2.00 6 -1 0 34.10 3.20 -6 1 0 31.90 1.70 6 1 0 38.80 3.60 6 1 0 32.70 2.90 6 1 0 29.90 3.20 -6 1 0 28.40 1.90 -7 -1 0 8.20 1.30 7 -1 0 8.80 2.60 7 -1 0 8.50 2.00 7 1 0 9.20 2.50 -7 1 0 9.00 1.20 7 1 0 6.50 1.70 7 1 0 6.40 2.00 8 -1 0 2.00 1.80 8 1 0 6.20 2.20 8 1 0 3.10 2.60 9 -1 0 7.80 3.00 9 1 0 13.00 3.70 10 -1 0 -0.20 2.50 10 -1 0 -2.40 2.40 10 1 0 1.90 3.00 0 -2 0 193.58 5.50 0 -2 0 173.98 5.70 0 -2 0 192.18 5.00 0 2 0 207.48 4.90 0 2 0 186.68 4.50 0 2 0 209.48 4.80 1 -2 0 483.75 11.00 -1 -2 0 469.25 11.10 1 -2 0 482.15 11.00 -1 -2 0 467.45 11.20 1 -2 0 497.85 11.20 1 -2 0 470.85 11.60 -1 -2 0 475.25 12.10 -1 -2 0 474.05 13.10 -1 -2 0 471.95 10.60 -1 2 0 485.05 11.00 1 2 0 479.45 10.60 -1 2 0 481.55 11.60 1 2 0 482.95 11.10 1 2 0 486.95 12.20 -1 2 0 494.05 11.20 1 2 0 471.35 13.10 1 2 0 473.55 11.20 -1 2 0 486.95 11.00 -2 -2 0 174.88 5.00 -2 -2 0 177.18 4.80 2 -2 0 175.48 5.20 -2 -2 0 172.98 4.70 -2 -2 0 173.58 5.80 2 -2 0 176.58 4.50 2 -2 0 174.08 4.40 2 -2 0 168.98 4.90 -2 -2 0 173.58 5.10 2 2 0 178.08 4.70 2 2 0 173.18 5.90 2 2 0 177.48 5.20 -2 2 0 177.58 4.60 2 2 0 180.58 4.60 3 -2 0 37.90 1.50 -3 -2 0 38.40 2.50 3 -2 0 40.40 2.30 -3 -2 0 39.80 1.80 -3 -2 0 37.90 1.80 3 -2 0 40.00 1.40 3 2 0 39.90 2.30 -3 2 0 39.80 1.70 3 2 0 37.50 2.10 3 2 0 41.00 2.70 3 2 0 39.40 1.60 3 2 0 36.80 1.60 -4 -2 0 30.10 2.40 4 -2 0 31.40 1.30 4 -2 0 30.80 1.20 -4 -2 0 30.20 1.80 4 -2 0 33.20 2.70 -4 2 0 29.00 1.40 4 2 0 30.70 1.50 -4 2 0 30.20 1.70 4 2 0 34.80 2.80 4 2 0 30.80 2.20 -5 -2 0 234.78 6.50 5 -2 0 219.78 8.10 5 -2 0 224.68 5.50 -5 2 0 225.08 6.00 5 2 0 221.58 8.50 5 2 0 237.98 8.90 -5 2 0 226.08 6.20 5 2 0 224.68 6.00 5 2 0 231.68 7.70 -6 -2 0 46.10 2.60 6 -2 0 46.70 4.00 6 -2 0 47.30 3.60 -6 -2 0 47.90 2.50 6 2 0 47.50 3.20 -6 2 0 47.20 2.10 6 2 0 45.00 3.90 -6 2 0 42.90 2.20 6 2 0 49.99 4.10 7 -2 0 4.60 1.70 7 -2 0 3.30 2.30 7 2 0 4.80 1.80 7 2 0 2.30 1.50 -7 2 0 3.50 1.00 7 2 0 3.40 1.90 -8 -2 0 2.60 1.10 8 -2 0 0.90 1.80 8 2 0 4.90 2.30 8 2 0 1.70 2.10 9 -2 0 2.00 2.50 9 -2 0 -1.00 1.40 9 2 0 2.10 2.70 10 -2 0 4.70 2.90 10 -2 0 -0.90 2.80 10 2 0 4.60 3.50 0 -3 0 0.30 0.50 0 -3 0 -0.40 0.30 0 -3 0 -0.30 0.40 0 -3 0 -0.30 0.40 0 -3 0 0.00 0.30 0 -3 0 1.00 0.60 0 3 0 -0.30 0.60 0 3 0 -0.10 0.50 0 3 0 0.20 0.30 0 3 0 -0.30 0.30 0 3 0 0.10 0.70 0 3 0 0.10 0.40 1 -3 0 3.60 0.70 -1 -3 0 4.70 0.80 1 -3 0 4.50 0.50 1 -3 0 4.30 0.70 -1 -3 0 5.50 0.90 1 -3 0 5.20 0.70 -1 -3 0 6.30 0.70 -1 -3 0 4.00 0.60 -1 -3 0 3.70 0.70 1 -3 0 6.40 0.90 1 -3 0 4.90 1.00 1 3 0 4.20 0.80 1 3 0 4.70 0.80 -1 3 0 4.30 0.90 -1 3 0 3.80 0.70 -1 3 0 4.70 0.80 -1 3 0 4.40 0.60 -1 3 0 5.20 0.60 1 3 0 4.00 0.70 1 3 0 4.90 0.80 -2 -3 0 721.73 18.00 2 -3 0 733.03 16.60 2 -3 0 691.53 16.50 -2 -3 0 704.23 16.20 -2 -3 0 706.23 16.80 -2 -3 0 702.83 16.60 -2 -3 0 719.03 19.60 2 -3 0 721.73 17.60 2 -3 0 701.53 16.30 2 3 0 718.53 19.70 2 3 0 719.23 16.50 2 3 0 710.53 16.00 -2 3 0 720.13 16.60 -2 3 0 704.63 16.30 2 3 0 708.03 18.10 2 3 0 689.33 16.60 -2 3 0 711.83 17.50 -3 -3 0 143.99 4.50 3 -3 0 140.39 4.90 -3 -3 0 139.49 4.80 3 -3 0 141.49 3.90 -3 -3 0 144.49 5.70 -3 -3 0 143.59 4.40 3 -3 0 141.29 4.80 3 3 0 141.39 5.70 3 3 0 147.59 5.00 -3 3 0 143.49 4.30 3 3 0 145.19 4.30 4 -3 0 37.00 2.50 -4 -3 0 39.80 3.00 -4 -3 0 36.90 2.20 -4 -3 0 36.50 2.10 4 -3 0 41.20 1.60 4 -3 0 36.90 2.50 4 3 0 39.50 3.10 4 3 0 39.80 2.50 -4 3 0 39.00 2.00 4 3 0 40.90 2.00 -5 -3 0 9.70 1.50 5 -3 0 6.60 0.80 5 -3 0 8.10 1.90 -5 -3 0 9.00 1.40 5 3 0 9.10 1.10 -5 3 0 8.80 1.10 -5 3 0 7.40 1.20 5 3 0 8.30 1.60 5 3 0 8.70 1.90 -6 -3 0 13.20 1.80 6 -3 0 7.90 1.90 -6 3 0 10.90 1.40 6 3 0 7.90 2.20 6 3 0 11.40 1.90 -6 3 0 10.20 1.20 6 3 0 9.20 2.20 -7 -3 0 0.10 1.20 7 -3 0 0.10 1.90 7 -3 0 1.30 1.30 7 -3 0 -0.50 1.80 7 3 0 -0.70 1.60 7 3 0 1.90 1.40 7 3 0 1.40 1.70 -7 3 0 -0.50 0.90 8 -3 0 7.30 2.70 8 -3 0 9.00 2.70 8 3 0 0.00 1.90 8 3 0 9.80 2.80 9 -3 0 1.00 2.40 9 -3 0 -2.00 1.40 9 3 0 -1.70 1.70 10 -3 0 1.00 2.70 10 -3 0 6.00 3.10 10 3 0 -0.10 2.30 0 -4 0 3521.05 80.69 0 -4 0 3655.43 80.49 0 -4 0 3586.84 76.99 0 -4 0 3737.23 80.79 0 -4 0 3640.24 87.19 0 -4 0 3643.34 92.09 0 4 0 3529.05 79.09 0 4 0 3707.93 79.09 0 4 0 3621.84 87.19 0 4 0 3578.14 92.09 0 4 0 3789.82 80.89 1 -4 0 3529.85 87.89 1 -4 0 3596.64 80.19 -1 -4 0 3799.02 82.59 -1 -4 0 3689.83 82.29 -1 -4 0 3580.64 81.49 1 -4 0 3700.43 89.19 1 -4 0 3595.74 93.89 -1 -4 0 3673.33 79.19 1 -4 0 3665.93 82.49 -1 -4 0 4037.30 89.09 1 -4 0 3603.64 82.19 -1 -4 0 3928.31 94.39 1 4 0 3921.31 80.39 -1 4 0 3455.45 93.89 -1 4 0 3646.34 82.19 1 4 0 3829.22 82.59 1 4 0 3812.62 88.99 -1 4 0 3378.76 88.09 -1 4 0 3619.14 80.19 1 4 0 3836.72 94.39 1 4 0 3957.70 82.39 -1 4 0 3645.74 82.49 1 4 0 3954.90 80.09 -2 -4 0 438.66 11.30 -2 -4 0 458.05 12.10 2 -4 0 446.16 11.10 2 -4 0 447.86 10.90 2 -4 0 453.55 12.90 2 -4 0 452.05 11.50 2 -4 0 437.16 11.10 -2 -4 0 445.36 11.10 -2 -4 0 452.85 13.30 2 4 0 448.56 13.50 -2 4 0 451.85 10.90 2 4 0 457.05 10.50 2 4 0 443.96 11.20 2 4 0 463.45 12.30 -2 4 0 442.16 11.40 -2 4 0 434.86 11.00 2 4 0 449.66 11.00 -2 4 0 458.95 11.20 -3 -4 0 1.60 0.80 3 -4 0 0.70 1.00 -3 -4 0 1.20 0.90 -3 -4 0 2.20 1.00 3 -4 0 2.70 0.90 -3 -4 0 1.80 0.90 3 -4 0 2.00 0.70 3 -4 0 1.90 0.80 3 4 0 1.50 1.20 3 4 0 2.30 0.80 -3 4 0 1.90 0.70 3 4 0 0.90 0.80 3 4 0 1.70 0.90 -3 4 0 1.30 0.90 -4 -4 0 58.29 3.30 4 -4 0 60.49 3.20 -4 -4 0 57.99 2.80 4 -4 0 61.79 2.20 4 -4 0 64.79 3.40 -4 -4 0 63.29 3.00 4 4 0 63.89 4.00 4 4 0 56.39 3.20 -4 4 0 60.39 2.70 4 4 0 60.79 2.60 -5 -4 0 -1.90 1.60 5 -4 0 -0.10 1.30 -5 -4 0 1.10 1.10 5 -4 0 0.00 0.50 5 -4 0 0.20 1.10 -5 -4 0 0.90 1.10 5 4 0 0.60 0.80 -5 4 0 1.00 0.60 -5 4 0 0.40 0.90 5 4 0 0.10 1.10 5 4 0 0.70 1.10 -6 -4 0 3.10 1.40 -6 -4 0 1.70 1.40 6 -4 0 2.60 1.40 6 -4 0 1.30 1.30 6 4 0 1.20 1.60 -6 4 0 1.20 0.90 -6 4 0 0.00 1.10 6 4 0 1.80 1.80 6 4 0 1.20 1.30 7 -4 0 27.30 3.30 7 -4 0 18.20 3.10 -7 -4 0 24.80 2.60 7 4 0 23.80 2.90 7 4 0 23.40 3.50 7 4 0 19.00 3.10 -7 4 0 23.30 1.80 -8 -4 0 5.40 1.60 8 -4 0 7.80 2.40 8 -4 0 8.10 2.30 8 4 0 7.00 2.90 8 4 0 2.20 2.20 9 -4 0 -0.10 1.70 9 -4 0 1.10 2.50 9 4 0 3.30 3.00 0 -5 0 1.00 0.80 0 -5 0 1.00 0.90 0 -5 0 0.00 0.60 0 -5 0 -0.40 1.00 0 -5 0 -0.30 0.60 0 5 0 1.70 0.70 0 5 0 -0.40 0.80 0 5 0 0.20 0.40 0 5 0 -0.10 0.60 0 5 0 -0.50 0.80 1 -5 0 530.15 13.40 -1 -5 0 547.35 14.80 1 -5 0 546.75 15.10 -1 -5 0 555.74 12.50 1 -5 0 529.35 13.30 1 -5 0 560.84 13.10 1 -5 0 542.35 12.80 -1 -5 0 586.14 13.90 1 -5 0 544.45 15.70 -1 -5 0 611.84 13.70 -1 -5 0 547.45 13.30 -1 -5 0 556.94 16.00 1 -5 0 547.15 13.70 1 5 0 538.15 14.90 -1 5 0 544.95 13.10 -1 5 0 531.15 15.60 1 5 0 541.75 16.00 1 5 0 535.15 13.70 1 5 0 552.84 12.40 1 5 0 541.75 13.40 -1 5 0 532.95 13.70 -1 5 0 530.65 13.30 -1 5 0 553.34 13.40 1 5 0 646.74 13.40 2 -5 0 152.88 4.60 -2 -5 0 148.99 5.30 -2 -5 0 153.18 4.90 2 -5 0 156.28 4.90 2 -5 0 151.68 4.80 -2 -5 0 151.48 4.40 2 -5 0 155.58 5.70 -2 -5 0 150.28 5.00 2 -5 0 152.98 4.60 2 5 0 151.48 6.10 2 5 0 160.28 5.50 -2 5 0 156.98 4.60 -2 5 0 153.68 4.60 -2 5 0 154.38 5.00 2 5 0 150.68 5.00 2 5 0 155.48 4.30 -3 -5 0 94.29 3.80 -3 -5 0 88.39 3.50 3 -5 0 94.09 4.30 -3 -5 0 90.29 3.90 3 -5 0 89.89 3.60 3 -5 0 91.09 3.70 -3 -5 0 89.39 3.80 3 -5 0 85.79 3.10 3 5 0 97.99 4.80 3 5 0 93.69 3.30 -3 5 0 88.79 3.60 3 5 0 96.09 4.10 -3 5 0 93.99 3.30 3 5 0 89.79 3.60 4 -5 0 26.60 2.20 -4 -5 0 22.30 2.20 -4 -5 0 26.60 2.20 4 -5 0 25.60 2.40 4 -5 0 25.00 1.60 -4 -5 0 25.50 2.20 -4 5 0 27.30 2.10 -4 5 0 27.60 1.80 4 5 0 23.00 1.90 4 5 0 27.60 2.30 4 5 0 28.00 3.20 -5 -5 0 111.99 4.50 5 -5 0 106.19 3.40 5 -5 0 106.19 4.80 -5 -5 0 109.09 4.40 -5 -5 0 103.69 5.00 5 -5 0 103.49 5.00 5 5 0 109.19 4.00 -5 5 0 110.39 4.10 5 5 0 109.59 6.30 5 5 0 114.09 5.10 -6 -5 0 -2.50 1.40 6 -5 0 -1.70 1.70 -6 -5 0 4.60 1.60 6 -5 0 -1.90 1.40 -6 5 0 1.50 1.00 6 5 0 2.80 1.80 -6 5 0 1.40 1.20 -7 -5 0 -1.10 1.50 7 -5 0 -1.40 1.70 7 -5 0 1.00 2.10 7 5 0 -1.40 1.30 7 5 0 2.30 2.40 7 5 0 -0.70 1.80 -7 5 0 -1.20 0.90 -8 -5 0 13.10 2.10 8 -5 0 10.20 2.50 8 -5 0 12.10 2.90 8 5 0 14.50 3.60 8 5 0 11.20 2.90 9 -5 0 23.10 3.90 9 -5 0 17.70 3.70 9 5 0 17.40 4.30 0 -6 0 306.27 10.10 0 -6 0 285.27 8.20 0 -6 0 310.07 8.60 0 -6 0 318.67 7.60 0 -6 0 312.17 9.60 0 -6 0 310.07 8.10 0 6 0 309.77 8.70 0 6 0 307.37 10.20 0 6 0 313.47 7.50 0 6 0 311.57 9.60 0 6 0 314.87 8.10 0 6 0 310.57 8.30 1 -6 0 200.08 5.60 -1 -6 0 210.58 6.40 -1 -6 0 204.08 6.10 1 -6 0 201.88 6.00 1 -6 0 203.98 5.90 1 -6 0 202.08 7.20 1 -6 0 206.98 5.50 -1 -6 0 204.78 6.80 -1 -6 0 209.78 6.10 -1 -6 0 206.38 5.30 -1 6 0 205.38 7.20 1 6 0 206.38 7.70 1 6 0 211.18 7.00 -1 6 0 208.68 5.50 -1 6 0 206.38 6.40 1 6 0 209.38 5.30 -1 6 0 206.28 7.40 -1 6 0 199.68 5.90 1 6 0 175.38 6.20 2 -6 0 49.10 2.40 2 -6 0 51.29 2.50 2 -6 0 49.20 2.20 2 -6 0 49.00 3.20 -2 -6 0 52.29 3.00 -2 -6 0 52.29 2.20 -2 -6 0 49.80 2.80 -2 -6 0 47.00 2.50 -2 6 0 49.90 2.10 2 6 0 54.09 3.80 -2 6 0 53.69 2.50 -2 6 0 53.89 2.90 2 6 0 55.49 2.10 2 6 0 49.70 3.10 2 6 0 48.40 2.60 3 -6 0 161.68 5.50 -3 -6 0 150.18 5.30 3 -6 0 161.28 5.20 3 -6 0 157.88 4.90 -3 -6 0 162.78 5.60 -3 -6 0 156.88 5.40 3 6 0 160.08 6.00 -3 6 0 150.18 5.30 3 6 0 159.78 4.80 -3 6 0 153.98 4.90 3 6 0 165.28 7.20 3 6 0 162.68 5.50 -3 6 0 161.58 5.30 -4 -6 0 110.49 4.50 4 -6 0 101.99 4.60 4 -6 0 113.69 4.60 -4 -6 0 109.79 4.50 -4 -6 0 105.39 4.60 4 -6 0 104.09 3.70 4 6 0 112.49 5.90 4 6 0 118.79 4.40 4 6 0 110.69 4.90 -4 6 0 105.69 4.30 -4 6 0 108.59 3.90 -5 -6 0 66.69 3.50 5 -6 0 65.59 2.70 5 -6 0 72.19 4.20 -5 -6 0 68.89 4.10 -5 -6 0 67.29 3.60 5 -6 0 65.89 3.90 -5 6 0 66.09 2.90 5 6 0 64.49 3.20 -5 6 0 68.49 3.40 5 6 0 73.29 4.20 5 6 0 70.59 5.30 6 -6 0 0.20 1.40 6 -6 0 -1.50 1.40 -6 -6 0 -1.90 2.10 -6 -6 0 0.80 1.50 -6 6 0 0.30 1.30 6 6 0 -0.20 1.10 6 6 0 0.50 1.90 -7 -6 0 12.20 2.20 7 -6 0 11.90 2.50 7 -6 0 11.90 2.90 7 6 0 10.20 2.70 7 6 0 8.60 2.70 7 6 0 11.40 2.30 -7 6 0 9.20 1.60 8 -6 0 7.80 2.60 -8 -6 0 5.90 2.00 8 -6 0 7.50 2.40 8 6 0 6.10 2.60 8 6 0 5.00 2.30 9 -6 0 -2.50 2.00 9 -6 0 4.10 2.70 9 6 0 1.00 2.20 0 -7 0 -0.90 0.80 0 -7 0 1.00 1.00 0 7 0 -0.10 1.00 0 7 0 1.20 0.60 0 7 0 -0.60 0.50 0 7 0 0.10 1.20 0 7 0 -0.90 1.30 1 -7 0 75.09 3.30 1 -7 0 80.89 3.40 1 -7 0 78.19 3.10 -1 -7 0 76.49 3.70 -1 -7 0 79.09 3.40 -1 -7 0 80.89 2.90 -1 -7 0 81.19 3.50 1 7 0 86.79 2.80 1 7 0 82.39 3.80 -1 7 0 81.89 4.50 -1 7 0 87.59 4.40 1 7 0 80.59 4.50 -1 7 0 76.09 3.60 1 7 0 81.79 4.30 -1 7 0 85.39 2.80 -1 7 0 82.79 3.30 2 -7 0 1.00 0.70 2 -7 0 0.50 0.80 -2 -7 0 -0.80 0.80 2 -7 0 -0.10 0.80 -2 -7 0 0.80 0.70 -2 -7 0 -0.60 1.10 2 7 0 0.30 1.10 2 7 0 1.20 0.60 -2 7 0 -0.90 1.10 2 7 0 -2.10 1.00 -2 7 0 0.10 0.60 2 7 0 1.40 1.50 -2 7 0 -0.40 0.90 -3 -7 0 201.18 6.80 3 -7 0 203.48 6.10 3 -7 0 198.58 6.50 -3 -7 0 193.08 6.40 3 -7 0 190.58 5.90 3 7 0 193.78 5.70 -3 7 0 202.48 6.10 -3 7 0 202.38 6.10 3 7 0 195.38 8.30 3 7 0 198.68 6.60 3 7 0 198.18 7.20 -3 7 0 191.08 6.50 -4 -7 0 31.60 2.70 -4 -7 0 33.20 2.60 4 -7 0 34.20 2.50 4 -7 0 34.80 2.60 -4 -7 0 29.50 2.60 4 -7 0 33.10 2.10 4 7 0 30.20 3.40 4 7 0 36.60 3.00 4 7 0 31.50 2.40 -4 7 0 30.80 2.10 -4 7 0 34.80 2.70 5 -7 0 13.60 1.50 -5 -7 0 12.90 2.20 5 -7 0 13.50 2.20 5 -7 0 15.50 2.10 -5 -7 0 10.50 2.00 -5 -7 0 14.90 2.60 -5 7 0 14.00 2.00 5 7 0 14.00 2.00 5 7 0 8.10 2.40 -5 7 0 15.40 1.70 5 7 0 13.60 2.10 6 -7 0 28.00 3.00 -6 -7 0 29.40 3.80 6 -7 0 30.70 3.20 -6 -7 0 29.20 3.10 -6 7 0 29.10 2.70 6 7 0 25.60 3.10 6 7 0 34.80 4.50 -7 -7 0 7.80 2.10 7 -7 0 6.50 2.20 7 -7 0 8.10 2.70 7 7 0 4.00 2.40 7 7 0 6.30 2.90 -7 7 0 5.90 1.60 -8 -7 0 3.90 2.00 8 -7 0 0.70 2.50 8 -7 0 1.00 2.00 8 7 0 10.60 3.50 8 7 0 3.30 2.10 9 -7 0 8.00 2.80 9 -7 0 3.40 2.30 9 7 0 8.40 3.10 0 -8 0 256.27 7.50 0 -8 0 252.07 6.90 0 -8 0 260.27 7.80 0 8 0 262.67 9.10 0 8 0 269.07 7.30 0 8 0 263.47 8.20 0 8 0 256.87 9.50 0 8 0 268.67 6.90 -1 -8 0 82.09 3.00 1 -8 0 79.39 3.20 1 -8 0 84.79 3.70 -1 -8 0 105.59 4.00 -1 -8 0 81.09 3.60 1 -8 0 78.49 3.60 1 8 0 75.29 4.00 1 8 0 81.69 5.10 -1 8 0 79.89 4.80 1 8 0 83.59 2.90 -1 8 0 84.09 2.90 -1 8 0 81.19 3.90 -1 8 0 88.69 4.70 1 8 0 83.49 4.40 2 -8 0 45.30 2.80 -2 -8 0 45.90 2.30 2 -8 0 45.70 2.70 2 -8 0 45.70 2.10 2 -8 0 47.40 2.80 2 8 0 51.39 3.00 -2 8 0 37.80 2.60 -2 8 0 47.90 3.80 2 8 0 51.89 2.20 2 8 0 60.49 4.50 -2 8 0 37.90 3.10 -2 8 0 43.50 2.10 -3 -8 0 -0.60 1.20 -3 -8 0 -1.00 0.90 3 -8 0 0.60 0.80 3 -8 0 -1.10 0.90 3 -8 0 0.80 1.10 3 8 0 0.00 1.20 3 8 0 0.70 1.60 -3 8 0 -0.30 1.40 -3 8 0 0.70 0.80 3 8 0 0.00 0.90 -3 8 0 -0.50 1.00 3 8 0 0.90 1.20 4 -8 0 56.59 3.70 -4 -8 0 59.69 3.70 4 -8 0 59.39 3.20 4 -8 0 50.89 2.80 -4 -8 0 58.99 3.50 -4 -8 0 51.49 3.40 4 8 0 49.90 4.40 -4 8 0 54.59 3.50 4 8 0 50.09 3.20 -4 8 0 51.69 2.80 4 8 0 54.99 4.00 -5 -8 0 24.20 2.70 5 -8 0 22.90 2.80 -5 -8 0 30.10 3.40 5 -8 0 24.50 3.10 -5 -8 0 26.30 2.80 5 -8 0 23.30 2.00 5 8 0 26.50 3.00 -5 8 0 24.80 2.10 -5 8 0 23.90 2.60 5 8 0 21.60 3.20 5 8 0 27.40 2.50 -6 -8 0 27.10 3.10 6 -8 0 24.40 3.10 -6 -8 0 26.70 3.70 6 -8 0 24.20 2.90 6 8 0 20.40 2.70 6 8 0 19.70 3.30 -6 8 0 24.30 2.70 -7 -8 0 0.60 1.80 7 -8 0 -3.80 1.30 7 -8 0 1.60 2.30 -7 -8 0 1.20 2.50 7 8 0 3.00 2.10 7 8 0 -2.10 2.00 -7 8 0 0.10 1.40 -8 -8 0 5.80 2.30 8 -8 0 2.80 2.30 8 -8 0 -0.30 2.30 8 8 0 4.00 2.50 8 8 0 0.00 2.20 9 -8 0 -0.60 2.70 9 8 0 1.80 3.10 0 -9 0 0.00 0.80 0 -9 0 1.10 0.90 0 -9 0 -1.00 0.80 0 9 0 0.10 0.70 0 9 0 1.80 1.90 0 9 0 0.50 1.20 0 9 0 -1.40 1.40 1 -9 0 19.70 2.30 -1 -9 0 22.80 1.70 1 -9 0 21.30 1.90 -1 -9 0 19.80 2.40 1 -9 0 19.80 1.90 -1 -9 0 20.80 2.00 1 9 0 22.40 2.30 -1 9 0 16.90 2.40 1 9 0 18.80 2.70 -1 9 0 21.00 1.60 1 9 0 24.60 1.50 -1 9 0 22.70 3.00 1 9 0 19.10 2.70 -1 9 0 18.20 2.30 -2 -9 0 41.00 3.10 -2 -9 0 40.00 2.80 2 -9 0 38.70 2.70 2 -9 0 41.50 2.00 2 -9 0 37.00 2.80 2 -9 0 38.70 2.70 -2 -9 0 42.90 2.30 -2 9 0 39.90 2.10 2 9 0 46.00 3.80 2 9 0 41.60 2.00 -2 9 0 36.40 3.10 2 9 0 38.10 3.70 -2 9 0 38.40 3.80 2 9 0 45.00 3.30 3 -9 0 87.29 4.40 -3 -9 0 94.49 3.70 3 -9 0 94.79 3.70 3 -9 0 95.89 4.00 -3 -9 0 91.99 4.30 -3 9 0 93.59 4.00 -3 9 0 92.49 4.60 3 9 0 92.79 4.90 3 9 0 96.49 6.20 3 9 0 84.19 4.20 -3 9 0 94.19 3.60 -4 -9 0 22.80 2.70 4 -9 0 21.00 2.30 4 -9 0 19.90 2.10 -4 -9 0 24.20 2.70 4 -9 0 20.90 2.50 4 9 0 17.50 2.60 4 9 0 23.90 2.60 -4 9 0 23.00 2.70 4 9 0 18.60 3.30 -4 9 0 21.60 2.10 -5 -9 0 2.90 1.90 5 -9 0 2.50 1.40 5 -9 0 2.60 1.90 5 -9 0 0.70 1.20 -5 -9 0 1.30 1.50 -5 9 0 1.90 1.90 5 9 0 2.00 1.70 5 9 0 2.90 1.80 5 9 0 0.80 2.30 -6 -9 0 2.60 1.80 -6 -9 0 1.50 1.70 6 -9 0 -1.20 1.30 6 -9 0 0.00 1.50 6 9 0 0.60 1.70 -6 9 0 2.70 1.90 6 9 0 -1.20 2.30 -7 -9 0 4.30 2.80 7 -9 0 6.60 2.20 7 -9 0 7.70 2.70 -7 -9 0 6.10 2.40 -7 9 0 4.60 1.80 7 9 0 3.00 2.50 7 9 0 9.00 2.70 8 -9 0 3.90 2.20 -8 -9 0 0.30 2.00 8 -9 0 -0.80 1.90 8 9 0 2.80 2.10 8 9 0 -1.50 2.20 9 -9 0 2.80 3.00 9 9 0 3.40 2.70 0 -10 0 11.40 1.90 0 -10 0 12.40 2.10 0 -10 0 17.20 1.50 0 10 0 12.30 1.40 0 10 0 10.00 2.30 0 10 0 8.40 2.10 0 10 0 8.50 2.40 1 -10 0 -0.20 1.00 1 -10 0 -1.70 0.80 -1 -10 0 0.80 0.90 -1 -10 0 -0.60 1.00 -1 -10 0 -0.90 1.20 1 -10 0 -0.60 1.20 1 10 0 -0.30 1.30 -1 10 0 -1.20 1.10 -1 10 0 0.50 1.40 -1 10 0 1.00 1.40 1 10 0 1.20 1.60 1 10 0 -1.40 1.60 -1 10 0 -0.50 0.70 2 -10 0 60.89 3.20 -2 -10 0 60.79 3.90 2 -10 0 72.19 3.80 2 -10 0 66.69 3.60 -2 -10 0 66.69 3.90 -2 -10 0 67.39 3.00 2 -10 0 68.49 2.80 -2 10 0 67.09 2.70 2 10 0 62.99 4.10 2 10 0 66.99 4.40 -2 10 0 65.19 4.60 -2 10 0 65.79 4.20 2 10 0 60.09 5.30 3 -10 0 120.29 4.30 -3 -10 0 113.59 4.30 3 -10 0 114.29 4.80 3 -10 0 111.69 5.00 3 -10 0 112.59 5.00 -3 -10 0 119.39 5.40 3 10 0 123.29 5.50 -3 10 0 122.49 5.60 3 10 0 108.89 6.70 3 10 0 117.99 5.90 -3 10 0 118.19 4.20 -4 -10 0 158.38 6.50 4 -10 0 148.49 6.20 4 -10 0 153.68 5.70 -4 -10 0 160.08 6.20 4 -10 0 149.99 5.40 4 10 0 146.89 8.20 4 10 0 141.19 6.00 -4 10 0 154.78 5.70 -4 10 0 146.59 6.40 4 10 0 157.58 7.30 5 -10 0 66.69 3.90 5 -10 0 65.59 4.20 -5 -10 0 62.59 4.10 -5 -10 0 66.09 4.50 5 10 0 66.79 4.80 5 10 0 57.69 6.20 5 10 0 59.59 4.00 -5 10 0 63.19 4.20 -6 -10 0 3.00 2.30 6 -10 0 0.30 1.40 -6 -10 0 2.20 2.10 6 -10 0 5.40 2.10 -6 10 0 0.20 1.80 6 10 0 -0.10 1.60 6 10 0 -0.70 1.70 7 -10 0 18.60 2.90 -7 -10 0 19.70 3.10 -7 -10 0 19.20 3.70 7 -10 0 21.00 3.70 -7 10 0 20.60 2.70 7 10 0 22.30 4.20 -8 -10 0 2.40 2.30 8 -10 0 -0.30 1.90 8 10 0 1.80 2.90 8 10 0 2.40 2.70 -9 -10 0 4.20 2.40 9 -10 0 2.30 2.40 9 10 0 9.30 3.20 0 -11 0 -2.30 1.40 0 -11 0 -0.10 1.00 0 -11 0 -0.30 1.00 0 11 0 -2.00 1.30 0 11 0 0.00 0.80 0 11 0 -0.90 1.30 0 11 0 -0.60 1.50 -1 -11 0 49.60 3.60 1 -11 0 47.70 3.00 -1 -11 0 48.90 2.70 1 -11 0 48.90 3.10 -1 -11 0 58.19 3.60 1 -11 0 44.20 3.10 -1 11 0 49.60 4.30 1 11 0 43.40 3.80 1 11 0 48.50 4.60 1 11 0 49.00 4.50 -1 11 0 50.39 3.70 -1 11 0 42.60 4.10 -1 11 0 51.79 2.60 -2 -11 0 1.80 1.30 -2 -11 0 2.90 1.10 -2 -11 0 2.90 1.40 2 -11 0 0.20 1.10 2 -11 0 1.30 1.30 2 -11 0 -0.50 1.40 2 11 0 1.80 1.90 -2 11 0 3.20 2.20 -2 11 0 2.00 0.90 2 11 0 1.50 1.40 -2 11 0 -0.60 1.80 2 11 0 3.50 2.40 3 -11 0 1.50 0.90 3 -11 0 1.90 1.60 -3 -11 0 2.40 1.90 3 -11 0 -1.30 1.20 -3 -11 0 -0.40 1.20 3 -11 0 -0.60 1.60 3 11 0 2.40 1.80 3 11 0 2.90 1.80 -3 11 0 1.30 0.80 -3 11 0 0.60 1.90 3 11 0 -1.00 1.80 -4 -11 0 1.70 1.60 4 -11 0 0.70 1.20 4 -11 0 0.20 1.40 4 -11 0 1.50 1.50 4 -11 0 2.50 2.00 4 11 0 0.70 1.90 4 11 0 1.20 1.80 -4 11 0 1.20 2.00 4 11 0 -0.60 2.40 5 -11 0 33.30 3.40 -5 -11 0 36.00 3.60 -5 -11 0 29.30 3.70 5 -11 0 26.20 2.80 -5 11 0 30.70 3.50 5 11 0 26.10 3.50 5 11 0 27.60 3.20 5 11 0 20.90 4.10 -6 -11 0 1.80 2.20 -6 -11 0 -2.00 2.00 6 -11 0 1.80 1.80 6 -11 0 -1.30 1.50 6 11 0 -0.30 2.00 -6 11 0 0.40 2.00 6 11 0 -3.60 2.30 -7 -11 0 -1.60 2.00 7 -11 0 3.10 2.10 -7 -11 0 1.90 1.90 -7 11 0 2.70 2.10 7 11 0 -2.80 2.30 -8 -11 0 3.00 2.50 8 -11 0 1.30 2.70 8 11 0 1.20 2.80 8 11 0 6.00 3.20 0 -12 0 210.48 6.60 0 -12 0 213.88 7.60 0 -12 0 206.28 7.30 0 12 0 216.48 9.80 0 12 0 208.78 8.30 0 12 0 213.08 9.20 1 -12 0 48.70 3.30 -1 -12 0 57.69 3.60 1 -12 0 49.80 3.40 1 -12 0 60.79 3.20 -1 -12 0 56.39 3.00 -1 -12 0 53.39 3.60 1 12 0 57.39 5.10 1 12 0 58.59 4.10 -1 12 0 56.89 2.70 -1 12 0 65.39 5.60 -1 12 0 54.59 4.30 1 12 0 60.39 5.20 -2 -12 0 45.30 2.80 2 -12 0 42.40 2.90 -2 -12 0 44.80 3.50 2 -12 0 45.90 3.30 -2 -12 0 45.00 3.40 2 -12 0 42.20 3.40 -2 12 0 50.79 5.10 -2 12 0 41.50 4.10 -2 12 0 44.00 2.40 2 12 0 48.20 4.80 2 12 0 42.10 3.60 2 12 0 40.40 4.60 3 -12 0 31.80 2.20 3 -12 0 26.70 2.70 3 -12 0 31.70 3.00 -3 -12 0 31.90 3.60 3 -12 0 23.20 3.00 -3 -12 0 34.90 2.70 -3 12 0 31.20 2.10 -3 12 0 27.00 3.60 3 12 0 24.70 4.10 3 12 0 33.30 3.70 3 12 0 24.30 3.60 4 -12 0 20.80 2.70 4 -12 0 20.70 2.20 -4 -12 0 23.80 3.20 4 -12 0 21.40 2.80 4 -12 0 17.50 2.90 4 12 0 22.30 3.30 -4 12 0 17.10 3.10 4 12 0 18.30 3.50 4 12 0 24.30 3.60 5 -12 0 17.30 3.20 5 -12 0 18.90 2.90 5 -12 0 16.50 2.20 -5 -12 0 17.40 3.20 -5 -12 0 17.00 2.90 5 12 0 15.90 2.90 5 12 0 17.00 3.10 -5 12 0 17.00 3.20 5 12 0 14.70 3.40 -6 -12 0 13.40 3.10 6 -12 0 7.40 2.30 -6 -12 0 13.70 3.10 6 -12 0 8.40 2.40 6 12 0 10.90 3.00 6 12 0 4.90 3.20 -6 12 0 14.40 2.90 -7 -12 0 3.80 2.80 7 -12 0 2.00 2.20 -7 -12 0 -3.00 2.10 7 12 0 2.00 2.90 -7 12 0 0.10 2.10 -8 -12 0 -0.60 2.90 8 -12 0 1.10 2.40 -8 -12 0 0.80 2.70 8 -12 0 -3.40 2.80 8 12 0 5.30 3.30 8 12 0 -1.70 2.90 0 -13 0 3.60 1.90 0 -13 0 2.90 1.30 0 -13 0 2.20 1.60 0 13 0 0.90 2.40 0 13 0 1.20 2.60 0 13 0 4.30 2.40 1 -13 0 4.60 2.10 -1 -13 0 8.70 1.70 -1 -13 0 5.80 2.30 -1 -13 0 5.60 1.70 1 -13 0 8.30 1.70 1 -13 0 6.20 1.70 -1 13 0 5.50 2.50 -1 13 0 6.90 1.30 1 13 0 5.80 2.60 -1 13 0 8.10 2.90 1 13 0 8.00 2.60 1 13 0 5.90 2.30 -2 -13 0 -1.50 2.10 -2 -13 0 5.10 2.20 2 -13 0 -0.60 1.30 2 -13 0 1.70 1.60 2 -13 0 -0.80 1.20 -2 -13 0 2.60 1.20 -2 13 0 0.90 2.40 -2 13 0 0.60 0.90 2 13 0 0.50 2.10 2 13 0 3.20 2.00 2 13 0 0.10 2.10 -2 13 0 -2.60 2.20 3 -13 0 51.89 3.90 3 -13 0 46.20 3.40 -3 -13 0 43.60 3.80 3 -13 0 47.10 3.60 -3 -13 0 50.89 3.00 3 13 0 49.10 5.40 -3 13 0 39.40 4.50 3 13 0 44.00 4.40 3 13 0 52.19 5.20 4 -13 0 57.29 4.10 4 -13 0 63.19 3.30 -4 -13 0 61.79 4.90 4 -13 0 60.19 4.20 4 -13 0 63.19 4.10 4 13 0 64.29 6.90 -4 13 0 59.39 5.00 4 13 0 55.09 5.40 4 13 0 56.19 4.50 5 -13 0 9.90 2.50 5 -13 0 14.70 3.10 -5 -13 0 9.60 2.60 -5 -13 0 10.70 3.10 5 13 0 9.60 2.90 -5 13 0 9.10 3.00 5 13 0 11.70 2.80 5 13 0 8.00 3.60 -6 -13 0 2.40 1.80 -6 -13 0 3.40 2.60 6 -13 0 -2.50 1.60 6 -13 0 -1.70 1.70 6 13 0 -0.20 2.30 6 13 0 5.20 2.80 -6 13 0 1.10 2.30 -7 -13 0 15.40 3.50 7 -13 0 7.40 3.30 -7 -13 0 19.70 3.70 7 -13 0 11.60 3.00 7 13 0 10.80 3.40 -7 13 0 14.30 3.20 -8 -13 0 -1.10 2.80 8 -13 0 -3.10 2.00 -8 -13 0 -1.90 2.60 8 -13 0 -3.20 2.10 8 13 0 3.70 3.70 8 13 0 3.70 3.20 0 -14 0 1.40 1.30 0 -14 0 1.60 2.20 0 -14 0 -0.20 1.30 0 14 0 0.20 1.90 0 14 0 -1.60 1.70 0 14 0 -2.70 1.50 -1 -14 0 43.70 2.90 1 -14 0 40.00 3.40 -1 -14 0 43.00 3.70 -1 -14 0 39.30 3.90 1 -14 0 35.70 3.90 1 -14 0 44.70 3.30 -1 14 0 45.10 5.00 1 14 0 45.80 5.30 -1 14 0 40.10 4.60 1 14 0 51.29 5.70 1 14 0 41.20 3.90 2 -14 0 16.50 2.60 -2 -14 0 16.10 2.90 -2 -14 0 17.20 2.10 2 -14 0 14.70 2.30 -2 -14 0 19.50 3.10 2 -14 0 22.40 3.20 2 14 0 20.80 3.50 2 14 0 17.30 3.60 -2 14 0 15.80 3.40 2 14 0 15.70 3.10 -2 14 0 18.10 3.70 3 -14 0 28.50 3.20 -3 -14 0 29.70 2.80 -3 -14 0 26.50 3.80 3 -14 0 30.30 3.40 3 -14 0 21.80 2.70 3 14 0 25.40 3.70 3 14 0 24.20 3.90 -3 14 0 22.40 4.00 3 14 0 24.20 4.20 4 -14 0 2.20 1.90 4 -14 0 1.20 2.20 -4 -14 0 0.80 1.90 4 -14 0 1.50 2.10 -4 14 0 2.10 2.60 4 14 0 2.70 2.10 4 14 0 -0.70 2.90 4 14 0 2.70 2.50 -5 -14 0 0.70 2.00 5 -14 0 1.10 2.40 5 -14 0 -2.10 1.70 -5 -14 0 -1.10 1.70 -5 14 0 -0.40 2.60 5 14 0 -1.70 2.80 5 14 0 -1.40 2.10 6 -14 0 4.80 3.10 -6 -14 0 3.30 2.50 -6 -14 0 4.10 3.00 6 -14 0 5.60 3.10 6 14 0 5.90 2.80 -6 14 0 8.70 3.00 6 14 0 2.20 2.60 7 -14 0 5.50 2.60 7 -14 0 11.90 3.60 -7 -14 0 8.80 3.20 -7 -14 0 2.70 3.00 -7 14 0 6.00 2.80 7 14 0 6.90 3.90 8 -14 0 1.80 3.40 8 -14 0 0.70 2.40 -8 -14 0 -5.20 2.50 8 14 0 1.90 3.20 8 14 0 -4.10 3.30 0 -15 0 -0.80 1.40 0 -15 0 0.40 1.30 0 -15 0 -1.90 1.40 0 15 0 -4.90 2.20 0 15 0 -0.20 2.10 0 15 0 0.00 2.20 -1 -15 0 5.70 1.80 1 -15 0 3.50 1.40 -1 -15 0 7.10 2.50 1 -15 0 5.40 1.90 -1 -15 0 -0.80 2.30 1 -15 0 4.40 2.50 -1 15 0 1.70 3.00 -1 15 0 3.50 2.80 1 15 0 2.80 3.20 1 15 0 2.80 3.00 1 15 0 0.80 2.60 -2 -15 0 29.80 2.80 -2 -15 0 30.20 4.10 2 -15 0 25.00 3.60 2 -15 0 25.60 3.10 -2 -15 0 26.70 3.70 2 -15 0 25.00 3.10 -2 15 0 23.00 4.10 2 15 0 26.60 4.30 -2 15 0 35.10 4.70 2 15 0 25.90 3.80 2 15 0 27.10 4.40 3 -15 0 8.10 2.70 -3 -15 0 15.30 3.50 -3 -15 0 10.60 1.90 3 -15 0 11.50 2.80 3 -15 0 8.70 2.40 3 15 0 13.90 3.30 3 15 0 11.50 3.40 -3 15 0 16.40 3.60 3 15 0 10.40 3.30 -4 -15 0 -0.90 1.90 4 -15 0 -3.70 2.00 4 -15 0 0.00 1.60 -4 15 0 -0.40 2.60 4 15 0 2.70 2.60 4 15 0 -0.40 2.60 4 15 0 2.30 2.30 -5 -15 0 0.70 2.10 5 -15 0 5.50 2.30 -5 -15 0 4.20 2.50 5 -15 0 -0.60 2.40 -5 15 0 4.60 3.00 5 15 0 3.40 2.70 5 15 0 3.60 2.80 -6 -15 0 4.70 2.10 6 -15 0 3.90 3.10 6 -15 0 5.50 2.50 -6 -15 0 0.60 3.00 6 15 0 3.30 3.70 -6 15 0 0.90 2.90 -7 -15 0 0.70 2.80 7 -15 0 -0.70 2.00 7 -15 0 0.90 2.20 -7 -15 0 -2.90 2.40 7 15 0 -3.30 3.00 -7 15 0 -0.50 2.50 0 -16 0 9.40 1.90 0 -16 0 5.60 2.20 0 -16 0 5.10 2.50 0 16 0 -1.90 3.10 0 16 0 6.20 3.40 0 16 0 4.90 3.10 -1 -16 0 47.50 4.00 -1 -16 0 49.90 3.40 -1 -16 0 50.99 4.50 1 -16 0 49.60 3.70 1 -16 0 44.60 3.90 1 -16 0 47.60 4.20 1 16 0 48.60 5.20 1 16 0 38.70 5.60 1 16 0 39.30 5.40 -1 16 0 52.39 5.80 -1 16 0 49.30 4.80 -2 -16 0 32.30 4.10 2 -16 0 28.10 3.90 -2 -16 0 31.00 4.00 -2 -16 0 29.80 2.80 2 -16 0 30.60 3.40 2 -16 0 30.20 3.40 -2 16 0 25.30 4.10 -2 16 0 30.10 4.20 2 16 0 24.60 4.20 2 16 0 27.10 4.60 2 16 0 22.60 4.40 3 -16 0 56.99 4.60 -3 -16 0 58.69 3.70 -3 -16 0 61.29 5.00 3 -16 0 60.99 4.80 3 -16 0 63.39 5.10 -3 16 0 63.69 6.00 3 16 0 60.49 5.00 3 16 0 40.10 5.40 3 16 0 50.19 6.40 4 -16 0 0.10 1.80 4 -16 0 1.00 2.40 -4 -16 0 3.50 3.10 4 16 0 3.90 2.20 4 16 0 -3.70 2.50 -4 16 0 1.60 2.90 4 16 0 0.90 2.60 -5 -16 0 23.00 4.20 5 -16 0 16.80 3.10 -5 -16 0 14.00 3.10 5 -16 0 12.30 3.40 -5 16 0 16.50 4.00 5 16 0 6.80 3.30 5 16 0 14.40 4.10 6 -16 0 0.00 1.90 -6 -16 0 0.50 2.30 6 -16 0 -0.50 3.00 -6 -16 0 0.70 2.90 -6 16 0 1.80 3.00 6 16 0 0.50 3.70 7 -16 0 4.00 3.50 -7 -16 0 14.70 3.80 -7 -16 0 10.70 3.90 7 -16 0 6.30 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4.90 1 -10 3 98.99 4.70 1 -10 3 90.39 4.20 -1 10 -3 90.79 5.20 1 10 3 84.29 5.70 -1 10 -3 96.49 5.30 -1 10 -3 91.09 5.60 1 10 3 93.09 4.00 1 10 3 86.69 4.90 -2 -10 -3 68.29 3.90 2 -10 3 69.39 3.80 2 -10 3 75.19 3.90 2 -10 3 67.69 3.90 -2 -10 -3 64.49 4.30 2 10 3 66.09 3.90 -2 10 -3 68.49 5.00 -2 10 -3 66.19 4.50 2 10 3 66.29 4.30 -2 10 -3 63.29 4.50 2 10 3 59.19 4.90 3 -10 3 17.00 2.30 -3 -10 -3 12.10 2.00 3 -10 3 17.00 2.40 -3 -10 -3 16.40 2.00 -3 -10 -3 16.30 2.50 3 -10 3 16.10 2.30 3 10 3 12.80 2.30 3 10 3 17.80 2.80 3 10 3 15.60 3.20 -3 10 -3 15.90 2.90 3 10 3 17.50 2.40 4 -10 3 9.50 2.10 -4 -10 -3 5.10 2.40 -4 -10 -3 9.40 2.00 4 -10 3 11.30 2.30 4 -10 3 7.50 2.10 4 10 3 8.60 2.50 4 10 3 8.50 2.90 4 10 3 6.60 1.90 -4 10 -3 5.50 2.50 4 10 3 8.70 2.10 -5 -10 -3 -1.30 1.60 5 -10 3 1.10 1.90 -5 -10 -3 2.40 2.20 5 -10 3 4.30 2.40 5 10 3 4.00 2.00 5 10 3 -0.90 1.60 -5 10 -3 2.20 2.40 5 10 3 -0.40 2.30 -6 -10 -3 35.20 4.40 6 -10 3 32.80 4.30 6 -10 3 38.50 4.20 6 10 3 29.20 4.50 6 10 3 35.10 4.70 -6 10 -3 37.00 4.20 -7 -10 -3 37.30 4.50 7 -10 3 26.90 3.90 7 -10 3 29.80 4.00 7 10 3 27.50 4.60 7 10 3 38.70 5.40 -7 10 -3 29.60 3.80 8 -10 3 7.40 3.30 8 -10 3 11.60 3.90 -8 -10 -3 11.30 3.30 -8 10 -3 12.30 2.90 8 10 3 10.90 3.90 9 -11 -3 5.40 2.50 9 -11 -3 -0.20 2.20 9 11 -3 3.00 3.30 8 -11 -3 9.20 2.90 -8 -11 3 5.70 2.90 8 -11 -3 10.40 3.10 -8 -11 3 8.50 2.60 8 11 -3 7.70 3.60 8 11 -3 2.20 2.50 -7 -11 3 -1.50 2.00 7 -11 -3 2.50 2.00 7 -11 -3 2.20 2.30 -7 -11 3 3.80 2.60 7 11 -3 -2.90 2.40 7 11 -3 2.80 2.30 -7 11 3 -0.40 1.60 6 -11 -3 23.70 3.30 -6 -11 3 24.50 3.70 -6 -11 3 29.70 3.60 6 -11 -3 21.30 3.00 -6 11 3 27.60 3.10 6 11 -3 16.80 3.50 6 11 -3 25.80 4.60 -5 -11 3 4.40 2.10 5 -11 -3 0.00 1.90 5 -11 -3 4.10 1.90 5 11 -3 0.40 1.80 -5 11 3 1.80 1.80 5 11 -3 0.70 1.80 5 11 -3 -1.60 2.00 4 -11 -3 8.40 1.90 4 -11 -3 5.70 2.10 4 -11 -3 8.40 2.00 -4 -11 3 10.30 2.40 4 11 -3 11.60 2.90 4 11 -3 5.00 2.10 -4 11 3 9.50 2.00 4 11 -3 3.90 2.80 -4 11 3 8.80 2.40 3 -11 -3 0.90 1.30 3 -11 -3 1.20 1.20 -3 -11 3 1.50 1.80 3 -11 -3 1.90 1.40 3 11 -3 -0.20 1.80 -3 11 3 2.70 1.80 3 11 -3 -0.20 1.60 3 11 -3 2.30 1.70 2 -11 -3 139.59 5.80 -2 -11 3 142.49 6.10 -2 -11 3 134.49 5.60 -2 -11 3 138.59 3.90 2 -11 -3 127.59 5.40 2 -11 -3 141.49 5.70 -2 11 3 139.39 6.20 2 11 -3 136.89 7.90 2 11 -3 143.49 6.30 2 11 -3 134.19 7.60 -1 -11 3 0.00 0.80 1 -11 -3 -0.90 1.50 1 -11 -3 1.70 1.50 -1 -11 3 -2.70 1.50 1 -11 -3 2.20 1.50 -1 -11 3 -1.40 1.40 -1 11 3 0.30 0.40 1 11 -3 -0.40 1.50 -1 11 3 -1.30 1.10 -1 11 3 0.40 0.40 1 11 -3 -1.00 1.90 -1 11 3 2.30 1.80 1 11 -3 0.40 1.90 0 -11 3 1.20 0.90 0 -11 3 0.10 1.10 0 -11 -3 0.30 1.30 0 -11 -3 0.90 1.40 0 -11 -3 -1.90 1.50 0 -11 3 -0.40 1.70 0 11 3 0.90 1.40 0 11 -3 1.40 1.90 0 11 3 1.00 0.80 0 11 -3 1.90 2.30 0 11 -3 2.10 1.60 0 11 3 0.40 1.60 -1 -11 -3 79.79 4.50 1 -11 3 82.09 4.40 -1 -11 -3 78.99 4.40 -1 -11 -3 73.09 4.00 1 -11 3 79.69 4.00 1 -11 3 74.89 4.40 -1 11 -3 87.69 5.70 -1 11 -3 82.59 5.60 1 11 3 75.19 4.50 1 11 3 88.69 4.00 -1 11 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11 3 5.30 3.40 8 -11 3 -2.40 1.90 -8 -11 -3 0.90 2.80 -8 11 -3 2.30 2.50 8 11 3 -0.90 2.30 -9 -12 3 -2.60 2.10 9 12 -3 3.30 3.50 -8 -12 3 4.40 3.20 -8 -12 3 1.60 2.50 8 -12 -3 3.90 2.60 8 -12 -3 2.20 2.80 8 12 -3 1.30 3.20 -7 -12 3 8.10 2.60 7 -12 -3 8.40 2.90 7 -12 -3 12.20 2.80 -7 -12 3 13.40 3.10 -7 12 3 12.20 2.40 7 12 -3 12.40 3.20 7 12 -3 9.00 3.30 6 -12 -3 0.30 1.40 6 -12 -3 1.80 1.80 -6 -12 3 -0.40 1.50 -6 -12 3 2.00 2.00 -6 12 3 -2.20 1.70 6 12 -3 -3.20 1.80 6 12 -3 -1.00 2.10 5 -12 -3 28.30 3.40 -5 -12 3 19.60 3.30 5 -12 -3 23.10 3.20 -5 12 3 20.10 3.00 5 12 -3 21.80 3.20 5 12 -3 20.10 3.80 5 12 -3 18.20 4.30 -4 -12 3 128.49 6.20 4 -12 -3 133.59 6.10 4 -12 -3 145.19 5.70 4 -12 -3 128.19 6.00 4 12 -3 129.99 7.90 4 12 -3 124.19 8.20 4 12 -3 131.99 6.50 -4 12 3 131.59 6.40 -3 -12 3 228.78 8.50 3 -12 -3 223.28 7.90 3 -12 -3 230.18 8.00 -3 -12 3 231.78 8.30 3 -12 -3 225.88 8.00 3 12 -3 233.68 9.00 -3 12 3 215.58 8.30 3 12 -3 230.08 10.50 3 12 -3 221.38 10.80 -2 -12 3 41.90 3.20 2 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61.09 5.30 -2 12 -3 61.19 4.60 2 12 3 58.49 4.60 -2 12 -3 58.89 4.80 2 12 3 65.49 4.00 -3 -12 -3 21.70 2.90 -3 -12 -3 26.90 3.80 -3 -12 -3 28.40 2.50 3 -12 3 27.20 3.20 3 -12 3 25.70 2.80 3 -12 3 27.10 3.00 -3 12 -3 26.80 3.80 3 12 3 21.10 3.00 3 12 3 17.30 3.20 3 12 3 26.70 4.00 3 12 3 24.80 3.20 -4 -12 -3 78.19 4.80 4 -12 3 92.09 5.20 -4 -12 -3 76.79 4.30 4 -12 3 75.39 4.80 4 -12 3 78.89 4.60 -4 -12 -3 83.69 5.80 4 12 3 80.89 5.70 4 12 3 88.89 5.40 4 12 3 81.99 7.30 4 12 3 80.79 5.30 -4 12 -3 83.29 5.80 5 -12 3 8.70 2.60 5 -12 3 1.50 1.90 -5 -12 -3 6.20 2.80 -5 -12 -3 6.20 2.30 5 12 3 9.30 2.60 -5 12 -3 3.10 2.60 5 12 3 9.00 3.00 5 12 3 -0.30 2.70 6 -12 3 1.70 2.10 -6 -12 -3 0.50 2.80 6 -12 3 1.30 2.10 6 12 3 0.40 2.00 -6 12 -3 1.40 2.70 6 12 3 1.30 2.00 -7 -12 -3 0.50 3.00 7 -12 3 2.80 2.50 -7 12 -3 -0.80 2.50 7 12 3 -3.90 2.70 7 12 3 0.70 2.80 -8 -12 -3 -2.90 3.00 8 -12 3 3.10 2.70 8 12 3 2.70 2.70 -8 12 -3 5.30 2.70 8 -13 -3 0.40 2.00 -8 -13 3 7.10 3.00 8 -13 -3 -3.30 2.90 -8 -13 3 -0.10 2.50 8 13 -3 1.50 2.40 -7 -13 3 3.90 3.00 7 -13 -3 2.20 2.00 -7 -13 3 -1.70 2.20 7 -13 -3 -0.90 1.90 7 13 -3 1.80 3.30 7 13 -3 6.90 2.90 -7 13 3 0.70 2.00 -6 -13 3 2.00 2.60 6 -13 -3 2.50 2.00 -6 -13 3 4.70 2.50 6 -13 -3 1.90 2.30 6 13 -3 0.40 3.10 -6 13 3 4.90 2.40 6 13 -3 1.40 2.60 5 -13 -3 41.60 3.70 5 -13 -3 37.60 3.80 -5 -13 3 45.50 4.40 5 13 -3 48.50 5.70 5 13 -3 45.50 5.80 -5 13 3 41.50 4.10 5 13 -3 39.80 4.00 4 -13 -3 108.69 5.40 4 -13 -3 125.49 5.60 -4 -13 3 121.69 6.40 4 -13 -3 135.19 6.50 -4 13 3 117.29 6.20 4 13 -3 110.09 8.00 4 13 -3 112.59 6.30 4 13 -3 117.19 7.90 3 -13 -3 204.48 7.60 3 -13 -3 213.38 7.90 -3 -13 3 219.08 8.50 -3 -13 3 198.68 5.50 -3 -13 3 222.98 8.60 3 -13 -3 224.68 8.10 -3 13 3 211.68 8.60 3 13 -3 236.68 11.70 3 13 -3 197.48 8.50 3 13 -3 223.88 10.70 -2 -13 3 0.90 0.80 2 -13 -3 0.30 1.30 -2 -13 3 2.00 1.70 2 -13 -3 0.30 1.90 -2 -13 3 1.70 1.50 2 -13 -3 1.50 1.40 2 13 -3 3.40 1.80 -2 13 3 -1.80 2.10 2 13 -3 -0.70 1.80 2 13 -3 2.70 2.60 -1 -13 3 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6.00 6 10 4 51.89 5.20 7 -10 4 31.10 4.40 -7 -10 -4 30.10 4.40 7 -10 4 33.30 4.40 7 10 4 32.40 4.80 -7 10 -4 34.10 4.40 -8 -10 -4 6.00 2.90 8 -10 4 6.00 3.50 8 -10 4 -0.80 2.80 8 10 4 9.20 4.00 -8 10 -4 0.50 2.40 9 -11 -4 -1.40 3.20 9 -11 -4 -1.70 1.80 9 11 -4 -1.00 3.00 -8 -11 4 9.70 2.70 8 -11 -4 17.40 3.80 8 -11 -4 9.10 2.80 -8 -11 4 12.90 4.00 8 11 -4 9.10 3.10 8 11 -4 7.20 3.90 7 -11 -4 10.90 2.70 7 -11 -4 8.30 2.60 -7 -11 4 2.10 2.00 -7 -11 4 6.10 2.40 7 11 -4 1.80 2.50 7 11 -4 6.40 2.90 -7 11 4 6.10 1.90 -6 -11 4 1.80 2.00 -6 -11 4 8.10 2.50 6 -11 -4 4.50 2.20 6 -11 -4 3.60 1.90 6 11 -4 4.50 2.60 6 11 -4 0.20 2.30 -6 11 4 1.90 1.80 5 -11 -4 0.30 1.30 -5 -11 4 0.80 1.90 5 -11 -4 2.70 2.30 5 11 -4 -2.40 1.70 5 11 -4 1.20 2.00 5 11 -4 1.10 1.80 -5 11 4 0.60 1.80 4 -11 -4 102.19 4.90 4 -11 -4 96.49 5.10 4 -11 -4 94.89 4.60 -4 -11 4 89.79 5.10 -4 11 4 98.69 5.10 4 11 -4 91.29 5.20 4 11 -4 89.99 6.70 4 11 -4 87.79 6.70 3 -11 -4 157.88 6.40 -3 -11 4 163.48 6.70 3 -11 -4 160.18 6.10 3 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3.30 -8 -12 4 14.90 3.10 8 -12 -4 11.40 3.80 8 -12 -4 13.70 3.30 8 12 -4 12.70 3.70 8 12 -4 15.00 3.80 7 -12 -4 -0.60 1.70 -7 -12 4 -0.90 2.00 7 -12 -4 -1.50 2.00 -7 -12 4 -0.60 2.60 7 12 -4 2.00 3.40 7 12 -4 -2.80 2.10 -7 12 4 1.40 1.70 -6 -12 4 -0.90 1.90 6 -12 -4 0.40 2.00 6 -12 -4 -0.20 1.60 -6 -12 4 0.00 2.30 -6 12 4 1.90 1.90 6 12 -4 4.40 3.20 6 12 -4 -1.90 2.40 -5 -12 4 49.90 4.40 5 -12 -4 48.20 3.60 5 -12 -4 62.29 4.90 5 12 -4 51.09 5.90 5 12 -4 42.10 4.80 -5 12 4 55.89 4.10 5 12 -4 51.49 4.20 4 -12 -4 2.10 1.60 4 -12 -4 0.80 1.80 -4 -12 4 2.50 2.10 4 -12 -4 -0.40 1.50 4 12 -4 1.00 2.40 4 12 -4 -1.50 1.30 4 12 -4 -0.20 1.90 -4 12 4 0.00 2.10 -3 -12 4 10.80 2.20 3 -12 -4 11.50 2.00 3 -12 -4 10.80 2.30 -3 -12 4 13.00 2.70 3 -12 -4 7.80 2.10 -3 12 4 10.60 2.60 3 12 -4 8.40 2.70 3 12 -4 10.10 2.70 3 12 -4 10.90 2.90 2 -12 -4 37.60 3.50 -2 -12 4 33.70 3.00 2 -12 -4 43.60 3.30 -2 -12 4 37.50 3.30 -2 -12 4 36.00 1.70 2 -12 -4 38.00 3.10 -2 12 4 45.00 4.20 2 12 -4 31.30 4.40 2 12 -4 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4.50 5 -13 -4 72.39 5.40 -5 -13 4 51.79 4.50 5 13 -4 49.50 4.30 5 13 -4 54.09 7.10 -5 13 4 49.99 4.40 5 13 -4 52.49 5.40 4 -13 -4 17.60 2.60 -4 -13 4 14.30 3.20 4 -13 -4 15.30 2.70 4 -13 -4 13.10 2.40 -4 13 4 19.30 3.30 4 13 -4 15.90 4.00 4 13 -4 22.60 3.50 4 13 -4 19.20 3.60 -3 -13 4 43.70 4.10 3 -13 -4 41.10 3.70 3 -13 -4 41.30 3.70 -3 -13 4 43.20 4.30 3 -13 -4 41.90 3.60 3 13 -4 43.00 5.10 -3 13 4 35.90 4.30 3 13 -4 44.20 4.50 3 13 -4 42.40 4.90 -2 -13 4 101.19 5.70 2 -13 -4 102.69 4.80 2 -13 -4 94.19 5.10 2 -13 -4 106.49 5.50 -2 -13 4 97.59 5.10 -2 -13 4 105.59 3.30 2 13 -4 108.39 6.00 2 13 -4 98.49 7.50 2 13 -4 99.19 7.10 -2 13 4 104.39 6.00 -1 -13 4 -1.00 1.80 1 -13 -4 -6.10 1.70 1 -13 -4 1.00 1.80 1 -13 -4 0.00 1.70 -1 -13 4 1.00 2.00 -1 -13 4 -0.90 0.80 1 13 -4 -4.20 2.00 -1 13 4 -0.80 2.60 -1 13 4 0.30 0.30 1 13 -4 -1.40 1.90 -1 13 4 -1.20 2.10 1 13 -4 -0.40 1.70 -1 13 4 -0.30 0.30 0 -13 4 0.60 1.00 0 -13 -4 0.90 2.10 0 -13 -4 -0.70 1.20 0 -13 4 -1.30 1.40 0 -13 4 0.10 1.30 0 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3 -4 -5 214.38 5.70 3 -4 -5 220.88 6.30 3 -4 -5 220.88 6.70 3 -4 -5 210.48 6.10 -3 -4 5 216.68 6.50 -3 -4 5 219.68 6.90 3 4 -5 215.78 5.10 -3 4 5 216.38 6.30 3 4 -5 223.48 8.40 -3 4 5 214.28 6.40 3 4 -5 211.58 8.80 3 4 -5 217.68 6.80 3 4 -5 226.18 6.10 2 -4 -5 67.49 2.60 2 -4 -5 58.59 2.90 2 -4 -5 63.29 3.00 -2 -4 5 66.49 3.10 -2 -4 5 64.69 2.50 -2 -4 5 64.39 3.20 2 -4 -5 65.39 2.20 -2 -4 5 65.19 1.90 2 4 -5 68.29 4.00 2 4 -5 64.99 2.00 -2 4 5 66.69 3.10 2 4 -5 70.69 4.20 2 4 -5 68.99 2.50 -2 4 5 65.89 2.20 -2 4 5 61.29 2.90 2 4 -5 68.89 3.40 -1 -4 5 72.79 3.60 -1 -4 5 67.19 3.10 1 -4 -5 68.59 3.10 -1 -4 5 68.09 2.60 -1 -4 5 70.89 2.40 1 -4 -5 74.89 3.40 -1 -4 5 70.19 3.40 1 -4 -5 69.19 2.70 -1 4 5 71.09 2.30 -1 4 5 70.49 2.90 1 4 -5 68.59 3.40 1 4 -5 66.69 3.80 1 4 -5 70.79 2.50 -1 4 5 71.99 3.30 1 4 -5 66.89 4.00 -1 4 5 71.29 3.20 0 -4 -5 87.49 4.10 0 -4 5 90.49 3.30 0 -4 5 96.09 3.40 0 -4 5 92.09 3.80 0 -4 -5 87.09 3.90 0 -4 -5 95.19 3.60 0 -4 5 94.99 4.10 0 4 -5 94.39 3.20 0 4 5 89.99 3.10 0 4 -5 99.39 4.30 0 4 5 94.79 4.00 0 4 -5 91.59 4.00 0 4 -5 95.29 4.40 0 4 5 93.59 3.70 -1 -4 -5 137.79 5.70 1 -4 5 138.49 5.00 1 -4 5 138.69 5.40 -1 -4 -5 136.79 5.20 1 -4 5 134.29 4.60 1 -4 5 134.89 5.30 -1 -4 -5 136.29 5.40 1 4 5 127.19 5.00 -1 4 -5 135.39 4.70 1 4 5 142.79 5.30 -1 4 -5 137.09 5.60 -1 4 -5 134.39 5.60 1 4 5 136.39 3.60 2 -4 5 59.39 3.30 -2 -4 -5 62.99 3.80 -2 -4 -5 64.39 3.60 -2 -4 -5 64.49 3.60 -2 -4 -5 61.19 2.00 2 -4 5 62.49 3.30 2 -4 5 59.89 3.20 2 -4 5 60.09 3.60 -2 4 -5 67.59 4.00 2 4 5 66.49 2.70 2 4 5 65.99 3.60 2 4 5 65.19 3.50 -2 4 -5 60.99 3.70 2 4 5 63.39 3.80 -3 -4 -5 80.69 4.40 3 -4 5 74.49 3.80 3 -4 5 74.59 3.80 3 -4 5 78.69 4.70 3 -4 5 78.99 3.70 3 4 5 74.69 3.80 3 4 5 77.69 4.50 3 4 5 84.99 4.30 3 4 5 76.49 3.40 -3 4 -5 85.19 4.70 4 -4 5 11.00 1.90 4 -4 5 12.00 2.30 -4 -4 -5 11.90 2.50 4 -4 5 7.00 1.80 4 4 5 7.40 2.10 4 4 5 8.70 1.80 4 4 5 8.90 1.80 -4 4 -5 9.50 2.40 -5 -4 -5 36.20 4.20 5 -4 5 29.60 3.60 5 -4 5 36.70 3.80 5 -4 5 36.10 2.80 5 4 5 28.80 3.80 -5 4 -5 33.20 3.70 5 4 5 30.80 3.40 5 4 5 32.00 3.00 -6 -4 -5 4.90 2.60 6 -4 5 8.00 2.80 6 -4 5 7.70 2.50 6 4 5 15.70 3.70 -6 4 -5 11.80 2.80 7 -4 5 -1.90 1.50 -7 -4 -5 3.40 2.40 7 -4 5 -1.10 1.80 7 4 5 -0.80 2.00 -7 4 -5 1.30 2.30 8 -4 5 4.60 3.50 8 -4 5 1.20 2.60 -8 4 -5 1.10 2.30 8 4 5 -0.10 2.10 10 -5 -5 -0.50 1.80 10 -5 -5 3.70 2.40 10 -5 -5 0.10 2.20 10 5 -5 -0.40 2.60 9 -5 -5 -1.40 2.10 9 -5 -5 3.50 2.10 9 -5 -5 7.10 2.10 9 5 -5 2.50 2.50 9 5 -5 1.80 2.40 8 -5 -5 3.60 2.00 8 -5 -5 5.50 1.80 8 -5 -5 4.40 2.20 -8 -5 5 3.30 3.10 8 5 -5 -0.50 1.60 8 5 -5 1.80 2.60 7 -5 -5 0.10 1.30 -7 -5 5 2.10 2.00 7 -5 -5 2.60 1.60 7 -5 -5 1.40 1.60 -7 -5 5 0.10 1.10 7 5 -5 -1.20 2.00 7 5 -5 0.00 1.80 -6 -5 5 43.70 4.30 6 -5 -5 43.60 3.20 6 -5 -5 51.39 3.20 -6 -5 5 44.50 2.70 -6 5 5 46.60 1.80 6 5 -5 52.69 4.40 6 5 -5 46.10 2.30 6 5 -5 39.90 4.60 -6 5 5 45.10 1.70 -5 -5 5 0.20 1.30 5 -5 -5 0.50 1.00 5 -5 -5 1.50 0.60 5 -5 -5 -0.80 1.00 -5 -5 5 -0.90 1.10 -5 -5 5 0.00 1.00 5 5 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1.50 0.80 1 5 -5 1.20 0.90 1 5 -5 -0.80 1.30 1 5 -5 2.00 0.70 -1 5 5 2.10 0.60 -1 5 5 2.20 1.20 0 -5 5 -0.40 0.70 0 -5 -5 0.20 0.80 0 -5 5 1.20 0.90 0 -5 -5 0.30 0.60 0 -5 -5 -3.50 1.10 0 -5 5 0.00 0.90 0 -5 5 -0.30 1.10 0 5 -5 0.10 0.90 0 5 -5 -1.30 1.20 0 5 -5 -0.70 1.30 0 5 5 -0.10 0.60 0 5 5 1.80 0.90 0 5 5 -1.10 1.20 1 -5 5 90.99 4.10 -1 -5 -5 90.99 4.40 -1 -5 -5 95.29 4.20 1 -5 5 88.29 4.20 -1 -5 -5 90.39 3.70 1 -5 5 95.89 3.80 -1 5 -5 92.89 4.60 1 5 5 89.39 4.10 1 5 5 96.99 4.30 -1 5 -5 90.49 4.70 -1 5 -5 90.39 3.80 1 5 5 90.19 4.70 -2 -5 -5 12.10 1.30 2 -5 5 10.90 1.80 2 -5 5 13.80 2.00 -2 -5 -5 10.30 2.10 -2 -5 -5 13.20 2.20 2 -5 5 11.30 2.10 2 5 5 11.90 2.10 2 5 5 11.30 1.90 -2 5 -5 11.30 2.00 -2 5 -5 12.70 1.30 -2 5 -5 14.70 2.40 2 5 5 13.00 2.00 3 -5 5 3.30 1.30 -3 -5 -5 1.80 1.80 3 -5 5 1.90 1.30 3 -5 5 3.10 1.80 3 5 5 0.50 1.20 3 5 5 0.80 1.30 3 5 5 0.00 1.40 -3 5 -5 0.60 1.80 4 -5 5 41.90 3.60 4 -5 5 36.90 2.90 -4 -5 -5 36.10 3.60 4 -5 5 35.00 3.00 4 5 5 39.20 3.10 4 5 5 34.20 3.30 -4 5 -5 41.30 3.80 4 5 5 34.40 3.60 5 -5 5 22.90 2.50 5 -5 5 22.20 3.30 5 -5 5 27.90 3.80 -5 -5 -5 25.60 3.50 -5 5 -5 26.90 3.50 5 5 5 23.20 3.00 5 5 5 25.60 3.40 5 5 5 18.00 3.10 6 -5 5 62.19 5.80 6 -5 5 63.99 5.20 -6 -5 -5 62.99 5.00 6 5 5 63.59 6.10 -6 5 -5 64.09 5.00 7 -5 5 1.60 2.70 7 -5 5 -2.80 2.60 -7 -5 -5 -3.10 1.90 7 5 5 0.70 2.80 -7 5 -5 -2.60 2.10 8 -5 5 -3.30 2.90 8 -5 5 6.20 3.00 8 5 5 -0.90 3.20 -8 5 -5 -2.70 2.10 10 -6 -5 1.80 2.70 10 -6 -5 0.00 2.00 10 6 -5 0.10 3.00 9 -6 -5 0.10 1.60 9 -6 -5 0.20 1.90 -9 -6 5 2.30 3.40 9 6 -5 0.00 2.20 9 6 -5 2.20 2.60 8 -6 -5 53.59 4.20 8 -6 -5 63.69 4.60 8 -6 -5 60.19 4.40 -8 -6 5 52.89 2.80 -8 -6 5 56.89 5.70 8 6 -5 52.89 5.70 8 6 -5 59.89 6.80 -7 -6 5 9.30 1.70 7 -6 -5 9.90 2.00 -7 -6 5 6.10 2.50 7 -6 -5 8.70 2.40 7 -6 -5 7.10 2.00 7 6 -5 10.60 2.90 7 6 -5 9.90 3.10 6 -6 -5 19.50 2.40 -6 -6 5 21.80 3.20 6 -6 -5 17.60 2.70 -6 -6 5 20.20 2.20 6 -6 -5 24.00 2.50 6 6 -5 17.30 3.20 -6 6 5 21.00 1.60 -6 6 5 21.90 1.50 6 6 -5 20.00 1.60 6 6 -5 14.70 3.10 5 -6 -5 5.10 1.80 -5 -6 5 6.50 1.60 5 -6 -5 6.90 1.10 -5 -6 5 7.30 1.70 5 -6 -5 5.80 1.40 5 6 -5 6.60 0.80 -5 6 5 6.10 1.20 5 6 -5 2.70 2.20 5 6 -5 6.70 1.50 5 6 -5 4.80 1.90 4 -6 -5 8.70 1.40 4 -6 -5 5.00 1.60 -4 -6 5 10.30 1.90 4 -6 -5 11.30 1.40 4 -6 -5 8.50 1.60 -4 -6 5 9.40 1.60 4 6 -5 8.90 1.60 4 6 -5 6.90 2.00 4 6 -5 10.50 2.20 4 6 -5 9.20 0.40 4 6 -5 10.10 0.50 -4 6 5 9.30 1.50 -4 6 5 8.90 1.40 3 -6 -5 0.70 0.80 3 -6 -5 0.70 0.50 3 -6 -5 0.80 0.90 -3 -6 5 1.20 1.10 3 -6 -5 -0.40 0.70 3 -6 -5 0.60 0.90 -3 -6 5 -0.50 1.30 -3 6 5 0.90 1.00 -3 6 5 0.30 1.10 3 6 -5 -0.80 1.10 3 6 -5 -0.50 1.10 -3 6 5 1.40 0.80 3 6 -5 -0.80 1.00 2 -6 -5 491.35 13.00 2 -6 -5 501.85 11.70 -2 -6 5 500.25 12.60 -2 -6 5 500.95 13.30 2 -6 -5 503.05 13.30 2 -6 -5 518.15 12.40 2 -6 -5 541.75 12.20 2 6 -5 489.15 16.10 -2 6 5 490.45 13.40 -2 6 5 499.75 12.00 -2 6 5 505.45 13.20 2 6 -5 495.35 13.90 2 6 -5 509.25 15.60 1 -6 -5 11.80 1.40 1 -6 -5 12.80 1.10 -1 -6 5 13.10 1.80 1 -6 -5 9.80 1.50 1 -6 -5 13.00 2.00 -1 -6 5 10.00 1.60 -1 -6 5 11.90 1.10 -1 -6 5 12.40 1.50 -1 6 5 12.40 2.00 1 6 -5 8.50 2.10 -1 6 5 12.40 1.30 -1 6 5 12.10 1.20 1 6 -5 10.70 2.10 1 6 -5 9.40 1.90 0 -6 -5 31.10 2.70 0 -6 -5 36.80 2.10 0 -6 -5 30.60 2.40 0 -6 5 34.90 2.10 0 -6 5 32.60 2.50 0 -6 5 33.30 2.50 0 -6 5 31.40 2.30 0 6 -5 30.90 2.70 0 6 -5 30.40 2.70 0 6 5 33.20 2.20 0 6 5 34.30 2.60 0 6 -5 33.60 3.00 1 -6 5 -1.50 0.80 -1 -6 -5 0.80 1.50 1 -6 5 1.30 1.10 -1 -6 -5 -0.50 1.00 -1 -6 -5 -0.50 1.00 1 -6 5 0.00 1.00 1 -6 5 -0.90 0.60 1 6 5 0.60 1.00 -1 6 -5 -3.00 1.30 1 6 5 -0.10 1.10 -1 6 -5 -1.00 1.00 1 6 5 0.50 1.00 -1 6 -5 1.50 1.00 -2 -6 -5 37.10 3.00 2 -6 5 41.90 3.00 -2 -6 -5 35.50 2.90 2 -6 5 39.20 2.10 2 -6 5 43.90 3.00 -2 -6 -5 40.80 2.30 2 -6 5 38.70 3.40 2 6 5 40.30 3.60 -2 6 -5 41.50 2.40 2 6 5 43.30 3.40 2 6 5 38.00 3.10 -2 6 -5 39.70 3.60 -2 6 -5 42.80 3.20 3 -6 5 4.00 1.70 -3 -6 -5 4.10 1.60 -3 -6 -5 4.00 0.50 3 -6 5 4.30 1.90 -3 -6 -5 6.30 2.20 3 -6 5 4.50 1.50 -3 6 -5 4.80 2.10 3 6 5 3.70 1.70 3 6 5 3.30 1.40 3 6 5 6.60 1.80 4 -6 5 2.00 1.40 4 -6 5 2.00 1.80 -4 -6 -5 -2.20 1.80 4 -6 5 -0.60 1.40 4 6 5 -2.60 1.30 -4 6 -5 0.60 1.90 4 6 5 -3.10 1.80 4 6 5 0.90 1.50 -5 -6 -5 207.68 8.60 5 -6 5 214.38 8.40 5 -6 5 198.58 8.70 -5 6 -5 211.48 8.40 5 6 5 206.48 8.90 5 6 5 197.98 7.60 5 6 5 215.28 9.70 6 -6 5 22.70 3.70 -6 -6 -5 20.00 3.40 6 -6 5 17.80 3.60 -6 6 -5 20.60 3.50 6 6 5 18.60 3.50 7 -6 5 1.00 2.60 -7 -6 -5 1.30 2.30 7 -6 5 -1.10 1.80 -7 6 -5 2.80 2.50 7 6 5 1.90 2.30 8 -6 5 -2.20 2.10 8 -6 5 1.50 2.10 -8 -6 -5 -0.20 2.50 8 6 5 -0.50 2.30 -8 6 -5 0.90 2.40 10 -7 -5 1.80 2.00 10 -7 -5 2.50 1.80 10 7 -5 1.70 2.30 9 -7 -5 1.10 2.10 -9 -7 5 2.60 3.60 9 -7 -5 1.10 2.50 9 7 -5 -0.20 2.70 9 7 -5 0.40 2.10 8 -7 -5 2.10 2.20 -8 -7 5 -0.20 1.30 -8 -7 5 3.00 3.10 8 -7 -5 3.70 2.00 8 7 -5 1.40 2.20 8 7 -5 0.80 2.20 -7 -7 5 0.10 1.90 -7 -7 5 0.20 1.50 7 -7 -5 0.80 2.00 7 -7 -5 3.60 1.40 7 -7 -5 2.20 1.80 7 7 -5 2.60 1.90 -7 7 5 1.40 0.60 7 7 -5 1.00 2.00 -6 -7 5 4.70 2.10 6 -7 -5 10.10 1.70 6 -7 -5 10.10 2.50 -6 -7 5 8.60 1.80 6 -7 -5 11.60 2.10 6 7 -5 7.50 2.40 6 7 -5 11.50 2.80 6 7 -5 10.00 1.10 -6 7 5 11.60 1.50 5 -7 -5 16.50 2.10 -5 -7 5 18.50 2.30 5 -7 -5 18.80 1.70 -5 -7 5 18.70 2.50 5 -7 -5 18.90 1.60 5 -7 -5 18.50 2.40 -5 7 5 15.90 1.70 5 7 -5 15.00 2.80 5 7 -5 18.60 1.10 -5 7 5 20.90 2.10 5 7 -5 13.60 2.90 5 7 -5 19.50 2.20 5 7 -5 16.80 0.90 -4 -7 5 4.30 1.60 -4 -7 5 2.30 1.40 4 -7 -5 3.50 0.70 4 -7 -5 3.60 1.20 4 -7 -5 2.50 1.10 4 -7 -5 2.90 1.30 -4 7 5 4.50 1.50 4 7 -5 0.30 1.30 4 7 -5 4.30 1.40 -4 7 5 3.10 1.10 4 7 -5 3.70 2.00 3 -7 -5 40.80 2.30 3 -7 -5 43.50 1.60 -3 -7 5 45.20 3.20 3 -7 -5 43.10 2.80 -3 -7 5 39.00 2.90 3 -7 -5 43.50 2.60 3 -7 -5 43.20 2.40 3 7 -5 41.90 3.70 -3 7 5 39.10 2.50 3 7 -5 38.30 3.00 -3 7 5 40.70 2.80 3 7 -5 45.00 4.00 2 -7 -5 1.90 0.40 2 -7 -5 2.20 0.90 -2 -7 5 2.50 0.90 2 -7 -5 1.10 1.00 2 -7 -5 3.90 1.40 -2 -7 5 -0.40 1.40 2 -7 -5 2.40 0.80 2 7 -5 1.40 1.50 2 7 -5 3.20 1.80 2 7 -5 2.90 1.50 -2 7 5 1.80 1.40 -2 7 5 1.80 1.00 1 -7 -5 153.38 4.50 1 -7 -5 144.39 3.70 -1 -7 5 150.08 4.20 1 -7 -5 153.38 4.90 -1 -7 5 149.69 5.60 -1 -7 5 147.39 4.90 1 -7 -5 139.99 5.30 1 -7 -5 145.89 5.70 1 7 -5 146.39 6.70 1 7 -5 156.78 6.30 -1 7 5 147.29 5.80 1 7 -5 154.58 6.70 -1 7 5 153.48 4.50 0 -7 5 2.60 1.20 0 -7 -5 0.90 1.50 0 -7 5 3.40 1.00 0 -7 -5 2.50 1.20 0 -7 5 3.40 1.20 0 7 5 2.80 1.30 0 7 5 3.90 1.10 0 7 -5 1.40 1.20 0 7 -5 3.70 1.90 0 7 -5 4.00 1.90 -1 -7 -5 0.30 1.10 1 -7 5 0.80 0.90 1 -7 5 0.60 1.30 -1 -7 -5 1.50 1.20 -1 -7 -5 2.20 1.70 1 -7 5 2.00 1.10 1 -7 5 1.00 1.00 1 7 5 1.00 1.10 -1 7 -5 2.00 1.20 1 7 5 1.40 1.30 -1 7 -5 3.20 1.50 -1 7 -5 0.90 1.80 1 7 5 3.00 1.30 2 -7 5 163.58 6.20 -2 -7 -5 156.58 6.20 2 -7 5 166.88 6.70 -2 -7 -5 166.78 5.70 2 -7 5 161.68 5.90 2 -7 5 162.58 5.70 -2 -7 -5 153.98 6.60 2 7 5 165.08 6.60 -2 7 -5 167.88 5.90 -2 7 -5 164.68 7.30 2 7 5 162.98 6.50 -2 7 -5 160.88 6.90 2 7 5 162.18 7.40 -3 -7 -5 23.70 3.20 -3 -7 -5 29.80 2.90 -3 -7 -5 30.30 1.70 3 -7 5 30.10 1.80 3 -7 5 32.80 3.50 3 -7 5 24.90 2.60 3 -7 5 26.20 2.60 3 7 5 27.70 2.90 -3 7 -5 29.30 3.50 3 7 5 27.60 2.90 3 7 5 29.40 3.70 4 -7 5 29.60 3.20 -4 -7 -5 31.90 3.30 4 -7 5 33.20 3.00 4 -7 5 32.60 2.90 4 7 5 30.90 3.30 4 7 5 33.80 4.20 -4 7 -5 32.10 3.80 4 7 5 28.90 3.80 -5 -7 -5 2.10 2.40 5 -7 5 1.40 2.10 5 -7 5 2.60 1.70 5 7 5 1.00 1.60 5 7 5 0.30 1.80 -5 7 -5 2.10 2.30 5 7 5 2.00 2.00 6 -7 5 20.90 3.30 -6 -7 -5 31.00 4.10 6 -7 5 18.10 3.30 -6 7 -5 23.30 3.60 6 7 5 25.60 4.30 -7 -7 -5 6.70 2.90 7 -7 5 -0.10 2.00 7 -7 5 -2.50 2.80 -7 7 -5 6.40 2.80 7 7 5 -0.30 2.90 8 -7 5 3.20 3.50 8 -7 5 8.80 3.60 -8 -7 -5 3.60 2.80 8 7 5 9.00 4.00 -8 7 -5 6.40 2.80 9 -8 -5 4.80 2.90 9 -8 -5 -2.50 1.90 9 8 -5 0.20 2.20 9 8 -5 0.30 2.10 -8 -8 5 20.80 4.30 8 -8 -5 14.70 2.90 -8 -8 5 14.60 2.30 8 -8 -5 17.40 3.40 8 8 -5 13.10 3.50 8 8 -5 14.70 4.10 -7 -8 5 2.20 2.00 -7 -8 5 1.20 1.60 7 -8 -5 0.80 1.70 7 -8 -5 -1.90 1.60 7 8 -5 -3.10 2.10 -7 8 5 0.80 0.90 7 8 -5 1.00 2.80 -6 -8 5 0.10 1.60 6 -8 -5 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2.50 2 5 -7 15.90 2.60 -2 5 7 16.90 2.30 2 5 -7 17.00 1.50 2 5 -7 16.50 2.70 -2 5 7 16.80 1.10 -2 5 7 16.60 1.90 -1 -5 7 26.20 2.70 -1 -5 7 26.20 2.90 1 -5 -7 27.40 2.40 1 -5 -7 26.50 2.50 -1 -5 7 28.40 1.80 -1 -5 7 27.30 1.90 -1 5 7 28.00 2.50 1 5 -7 29.80 3.20 1 5 -7 24.00 3.10 -1 5 7 30.50 1.70 -1 5 7 29.80 2.30 1 5 -7 27.50 2.70 0 -5 -7 2.80 1.40 0 -5 7 0.50 1.10 0 -5 -7 -1.40 1.40 0 -5 7 1.70 1.60 0 -5 7 -0.90 1.40 0 5 -7 2.10 1.90 0 5 -7 0.00 1.10 0 5 7 -0.30 1.20 0 5 7 -2.00 1.40 0 5 -7 -0.40 1.10 1 -5 7 32.50 2.70 -1 -5 -7 32.70 3.40 1 -5 7 30.60 3.00 -1 -5 -7 33.00 3.30 1 -5 7 32.70 2.50 -1 5 -7 31.40 3.60 1 5 7 37.60 2.90 1 5 7 36.30 3.20 -1 5 -7 32.10 2.30 -1 5 -7 37.80 3.40 -2 -5 -7 50.79 3.70 2 -5 7 46.00 3.20 -2 -5 -7 43.60 2.10 2 -5 7 49.99 4.20 2 -5 7 47.50 3.20 -2 -5 -7 47.40 4.10 -2 -5 -7 45.20 1.90 2 5 7 49.40 3.60 -2 5 -7 49.80 4.20 -2 5 -7 45.90 1.70 -2 5 -7 45.50 3.60 2 5 7 49.90 2.30 2 5 7 46.60 3.40 3 -5 7 4.90 1.90 3 -5 7 5.30 2.50 3 -5 7 4.90 1.60 -3 -5 -7 3.70 2.30 3 5 7 2.40 1.70 -3 5 -7 5.90 2.10 -3 5 -7 4.60 1.90 3 5 7 4.10 1.40 3 5 7 4.40 1.80 4 -5 7 37.70 3.80 -4 -5 -7 38.70 4.50 4 -5 7 35.50 3.40 4 -5 7 31.60 4.20 -4 5 -7 40.60 4.70 4 5 7 34.30 3.60 4 5 7 37.50 4.10 -5 -5 -7 5.60 3.00 5 -5 7 6.70 2.50 5 -5 7 8.00 2.20 5 5 7 5.70 3.10 -5 5 -7 4.80 2.80 6 -5 7 0.60 2.20 -6 -5 -7 3.40 2.90 6 -5 7 0.30 2.40 -6 5 -7 1.60 2.70 6 5 7 0.10 2.90 7 -5 7 3.50 2.80 7 -5 7 6.70 2.60 -7 -5 -7 -3.00 2.70 -7 5 -7 3.40 3.10 7 5 7 3.80 2.70 10 -6 -7 13.30 3.40 10 6 -7 15.90 4.10 10 6 -7 13.30 3.80 -9 -6 7 16.80 4.60 9 -6 -7 10.30 3.10 9 -6 -7 15.00 2.80 9 6 -7 14.10 4.10 9 6 -7 25.50 4.80 -8 -6 7 15.20 3.30 -8 -6 7 9.90 1.70 8 -6 -7 13.90 3.00 8 -6 -7 15.30 2.40 8 6 -7 9.30 3.10 8 6 -7 13.00 3.60 7 -6 -7 7.20 2.50 -7 -6 7 7.80 1.80 -7 -6 7 7.50 3.30 7 -6 -7 11.80 2.20 -7 6 7 12.10 1.30 7 6 -7 4.90 2.50 7 6 -7 6.40 2.50 6 -6 -7 0.80 1.20 6 -6 -7 0.30 1.40 -6 -6 7 3.00 1.50 -6 -6 7 0.60 2.30 6 6 -7 -1.40 1.80 6 6 -7 -0.40 1.70 -6 6 7 0.80 1.10 5 -6 -7 21.30 2.80 -5 -6 7 18.20 2.40 5 -6 -7 22.10 2.00 -5 -6 7 23.20 2.50 5 -6 -7 23.50 2.00 5 6 -7 11.50 3.10 5 6 -7 20.10 1.00 5 6 -7 21.90 2.30 -5 6 7 18.00 2.10 -5 6 7 20.50 2.10 5 6 -7 13.90 2.90 -4 -6 7 19.20 2.40 4 -6 -7 18.60 1.80 -4 -6 7 22.30 2.70 4 -6 -7 19.00 2.10 4 -6 -7 18.90 1.60 4 -6 -7 22.10 2.30 -4 6 7 19.70 2.20 4 6 -7 14.90 2.70 4 6 -7 20.70 2.40 4 6 -7 17.20 3.20 -4 6 7 19.00 2.30 -3 -6 7 0.40 1.50 3 -6 -7 3.30 0.80 3 -6 -7 4.90 1.40 3 -6 -7 2.50 1.00 3 -6 -7 5.60 1.50 -3 6 7 4.30 1.60 -3 6 7 2.90 0.80 3 6 -7 2.00 1.50 -3 6 7 5.40 1.50 -2 -6 7 -0.30 1.60 -2 -6 7 3.70 1.10 2 -6 -7 2.80 1.50 2 -6 -7 2.60 0.90 -2 -6 7 4.40 0.80 2 -6 -7 3.60 1.60 2 -6 -7 2.20 0.70 2 6 -7 2.50 1.60 -2 6 7 3.20 1.60 2 6 -7 1.40 1.70 2 6 -7 3.70 1.60 -2 6 7 3.00 1.00 -2 6 7 2.30 0.70 1 -6 -7 65.09 3.70 -1 -6 7 70.79 2.90 -1 -6 7 66.19 3.90 -1 -6 7 66.19 3.10 -1 -6 7 60.39 3.80 1 -6 -7 70.39 4.10 1 6 -7 67.59 4.60 -1 6 7 65.49 4.00 1 6 -7 67.89 4.40 -1 6 7 66.89 2.60 -1 6 7 66.99 3.20 1 6 -7 68.29 4.50 0 -6 -7 0.50 1.30 0 -6 7 0.10 1.10 0 -6 7 -0.30 1.50 0 -6 -7 -0.20 1.10 0 -6 7 0.90 1.10 0 6 7 -0.20 1.10 0 6 -7 1.80 1.90 0 6 7 -1.00 1.60 0 6 -7 -1.60 1.40 0 6 -7 0.00 1.10 1 -6 7 28.40 2.60 1 -6 7 30.40 3.50 1 -6 7 27.30 3.00 -1 -6 -7 31.20 3.00 -1 -6 -7 27.60 3.40 1 6 7 29.00 2.80 -1 6 -7 31.90 2.50 -1 6 -7 28.20 3.50 -1 6 -7 26.30 3.00 1 6 7 34.20 3.10 2 -6 7 35.30 3.90 -2 -6 -7 25.10 3.40 -2 -6 -7 26.50 1.90 2 -6 7 31.80 3.10 -2 -6 -7 32.70 3.70 2 -6 7 29.90 2.50 -2 6 -7 31.10 3.80 -2 6 -7 26.80 1.80 2 6 7 29.60 3.00 2 6 7 27.60 3.20 -2 6 -7 34.20 3.60 -3 -6 -7 194.68 8.50 3 -6 7 194.98 7.50 3 -6 7 192.28 8.20 3 -6 7 194.28 7.20 -3 6 -7 206.48 8.80 3 6 7 200.38 7.70 -3 6 -7 197.28 7.90 3 6 7 192.78 8.20 4 -6 7 -0.90 1.70 4 -6 7 0.20 1.80 -4 -6 -7 3.40 2.70 4 -6 7 -1.30 1.90 4 6 7 3.60 2.10 -4 6 -7 5.80 2.70 4 6 7 0.60 1.60 4 6 7 0.30 1.70 5 -6 7 5.00 2.40 -5 -6 -7 -0.20 2.70 5 -6 7 2.70 2.80 5 6 7 -3.80 2.40 -5 6 -7 4.70 2.80 -6 -6 -7 6.80 3.10 6 -6 7 2.60 2.70 6 -6 7 1.20 2.90 6 6 7 0.50 2.20 -6 6 -7 -0.80 2.80 7 -6 7 4.50 2.90 -7 -6 -7 1.70 2.80 7 -6 7 2.30 2.70 7 6 7 1.00 3.30 -7 6 -7 1.70 3.00 9 -7 -7 5.60 2.80 9 7 -7 8.20 3.20 9 7 -7 7.80 3.20 -8 -7 7 -0.90 1.80 8 -7 -7 1.10 1.90 -8 -7 7 -0.90 1.30 8 -7 -7 1.00 2.30 8 7 -7 0.50 3.00 8 7 -7 1.20 2.60 7 -7 -7 20.60 3.30 7 -7 -7 19.10 2.50 -7 -7 7 20.70 3.80 -7 -7 7 19.60 2.40 -7 7 7 17.80 1.70 7 7 -7 14.70 4.00 7 7 -7 12.10 3.20 6 -7 -7 9.70 2.60 -6 -7 7 11.80 3.10 -6 -7 7 12.70 2.20 6 -7 -7 10.80 2.00 -6 7 7 12.70 1.80 6 7 -7 10.90 2.90 6 7 -7 14.50 3.20 5 -7 -7 32.90 3.50 5 -7 -7 30.90 2.30 -5 -7 7 32.60 3.00 5 7 -7 31.10 3.00 5 7 -7 30.60 4.40 5 7 -7 39.70 5.00 -5 7 7 37.60 2.80 4 -7 -7 11.10 2.00 4 -7 -7 12.80 1.90 4 -7 -7 12.40 1.50 4 -7 -7 9.80 1.40 -4 -7 7 12.70 2.20 4 -7 -7 12.90 1.70 4 7 -7 10.30 2.10 4 7 -7 13.00 3.00 -4 7 7 14.50 2.00 -4 7 7 10.80 2.00 4 7 -7 12.70 2.70 3 -7 -7 5.00 1.50 3 -7 -7 6.30 1.10 3 -7 -7 4.10 0.90 3 -7 -7 7.40 1.80 -3 -7 7 7.90 1.70 -3 -7 7 4.90 1.90 3 7 -7 3.00 1.90 -3 7 7 5.00 1.70 3 7 -7 7.50 2.10 3 7 -7 6.00 2.30 -3 7 7 6.00 1.00 2 -7 -7 0.60 1.10 2 -7 -7 -0.40 0.70 -2 -7 7 0.00 1.00 -2 -7 7 -0.40 0.50 2 -7 -7 0.80 1.10 -2 -7 7 -2.20 1.40 2 -7 -7 0.70 0.70 -2 7 7 0.40 0.70 -2 7 7 0.10 1.10 2 7 -7 1.10 1.60 -2 7 7 0.80 0.80 2 7 -7 -1.70 1.50 2 7 -7 -0.20 1.20 1 -7 -7 3.30 1.90 -1 -7 7 3.60 1.70 -1 -7 7 4.10 1.30 1 -7 -7 7.10 2.00 -1 -7 7 2.30 1.40 1 -7 -7 2.90 0.90 -1 -7 7 4.30 1.10 -1 7 7 3.80 1.20 -1 7 7 4.90 1.90 1 7 -7 4.10 2.10 1 7 -7 3.20 1.40 1 7 -7 3.20 1.60 0 -7 -7 71.69 4.30 0 -7 7 65.19 3.40 0 -7 7 67.89 4.50 0 -7 7 76.19 4.00 0 -7 -7 66.99 4.10 0 7 -7 73.69 5.10 0 7 7 65.69 3.50 0 7 -7 64.99 4.30 0 7 -7 69.99 4.20 0 7 7 62.69 4.20 1 -7 7 57.99 3.40 -1 -7 -7 50.99 3.70 -1 -7 -7 46.10 4.10 1 -7 7 55.39 3.90 1 -7 7 55.19 4.30 1 7 7 53.39 3.70 -1 7 -7 56.69 4.60 -1 7 -7 50.49 4.40 1 7 7 54.59 3.70 -1 7 -7 53.39 3.40 -2 -7 -7 38.30 4.10 2 -7 7 45.90 3.50 2 -7 7 38.30 3.60 2 -7 7 43.80 3.60 -2 -7 -7 38.50 2.50 -2 -7 -7 39.40 3.70 -2 7 -7 38.20 3.70 2 7 7 35.10 3.20 -2 7 -7 37.50 2.60 -2 7 -7 43.30 4.10 2 7 7 40.70 3.80 3 -7 7 6.00 2.20 3 -7 7 1.90 1.80 -3 -7 -7 -0.90 2.40 -3 -7 -7 -2.00 2.10 3 -7 7 4.90 1.80 3 7 7 0.60 2.00 -3 7 -7 0.10 1.80 3 7 7 0.20 2.00 3 7 7 1.20 2.00 -3 7 -7 3.00 1.90 4 -7 7 113.59 6.00 4 -7 7 99.69 5.10 4 -7 7 102.79 6.70 -4 -7 -7 105.49 6.60 -4 7 -7 110.59 6.80 4 7 7 98.29 5.90 4 7 7 106.59 5.80 4 7 7 106.79 6.80 -5 -7 -7 13.80 3.50 5 -7 7 11.10 2.90 5 -7 7 13.70 3.20 5 7 7 7.50 2.60 -5 7 -7 15.30 3.60 -6 -7 -7 3.50 3.10 6 -7 7 -0.80 1.70 6 -7 7 0.40 2.20 6 7 7 0.40 2.70 -6 7 -7 1.60 2.90 7 -7 7 4.60 2.40 -7 -7 -7 3.80 3.10 7 -7 7 1.80 3.50 7 7 7 0.50 2.20 -7 7 -7 0.00 2.90 9 -8 -7 5.90 2.80 9 8 -7 3.70 2.20 9 8 -7 8.00 3.90 -8 -8 7 -2.90 2.70 8 -8 -7 0.80 1.60 8 -8 -7 -2.50 2.20 -8 -8 7 0.00 1.60 8 8 -7 1.60 3.30 8 8 -7 1.70 2.70 7 -8 -7 2.90 1.70 -7 -8 7 2.10 1.80 7 -8 -7 1.00 2.20 -7 -8 7 3.10 2.70 7 8 -7 4.60 2.50 -7 8 7 3.70 1.30 7 8 -7 2.70 3.00 6 -8 -7 75.69 3.90 6 -8 -7 72.89 4.70 -6 -8 7 75.39 4.30 -6 8 7 75.49 3.80 6 8 -7 79.39 6.20 6 8 -7 75.19 6.70 5 -8 -7 -0.10 1.20 5 -8 -7 0.60 1.40 -5 -8 7 -2.90 1.50 -5 8 7 1.10 1.50 5 8 -7 1.60 1.80 5 8 -7 1.80 2.60 5 8 -7 -0.40 1.40 4 -8 -7 3.40 1.30 4 -8 -7 6.00 1.70 4 -8 -7 7.20 1.50 -4 -8 7 3.40 1.80 4 -8 -7 3.70 1.40 4 -8 -7 5.00 0.90 -4 8 7 5.20 1.70 4 8 -7 4.10 2.10 4 8 -7 1.80 1.80 4 8 -7 5.20 1.90 -4 8 7 1.70 1.50 3 -8 -7 19.00 2.40 3 -8 -7 16.60 2.30 3 -8 -7 20.80 1.80 -3 -8 7 18.60 2.60 3 -8 -7 20.30 1.30 -3 -8 7 20.80 2.30 3 8 -7 23.60 3.10 3 8 -7 21.40 3.30 3 8 -7 17.90 2.90 -3 8 7 23.10 2.80 2 -8 -7 2.70 1.00 -2 -8 7 2.50 0.60 -2 -8 7 2.30 1.90 -2 -8 7 1.50 1.30 2 -8 -7 -1.30 1.50 2 -8 -7 0.00 1.50 2 -8 -7 1.90 0.70 2 8 -7 2.70 1.70 2 8 -7 2.50 1.60 -2 8 7 1.00 1.70 2 8 -7 -1.60 1.10 1 -8 -7 184.88 7.20 -1 -8 7 180.28 5.40 -1 -8 7 192.58 7.20 1 -8 -7 195.18 6.00 -1 -8 7 170.38 7.40 1 -8 -7 182.98 6.90 -1 -8 7 190.48 6.20 -1 8 7 180.38 5.90 1 8 -7 176.58 7.70 1 8 -7 178.18 8.00 -1 8 7 177.88 7.10 1 8 -7 200.88 8.90 0 -8 -7 -1.90 1.60 0 -8 7 -0.50 1.30 0 -8 7 -0.70 1.60 0 -8 7 1.90 1.40 0 -8 -7 -1.40 1.70 0 8 -7 -0.10 1.90 0 8 -7 1.10 2.10 0 8 -7 -0.40 1.60 0 8 7 -0.50 1.30 0 8 7 2.10 1.20 -1 -8 -7 -3.20 1.00 1 -8 7 0.00 1.30 -1 -8 -7 -0.90 1.40 1 -8 7 0.40 1.50 1 -8 7 1.30 1.40 1 8 7 -1.40 1.80 1 8 7 -0.60 1.30 -1 8 -7 2.60 2.10 -1 8 -7 1.00 1.40 -1 8 -7 0.60 1.70 2 -8 7 78.49 4.70 -2 -8 -7 75.59 5.50 2 -8 7 82.59 5.00 2 -8 7 75.69 4.50 -2 -8 -7 88.59 5.50 -2 -8 -7 78.89 3.90 2 8 7 84.89 5.20 -2 8 -7 76.09 5.60 -2 8 -7 83.59 5.70 -2 8 -7 79.99 4.10 2 8 7 93.59 5.20 3 -8 7 39.30 3.60 3 -8 7 43.00 4.00 -3 -8 -7 44.50 4.60 -3 -8 -7 35.40 4.50 3 -8 7 37.20 4.50 3 8 7 37.30 4.30 3 8 7 40.90 4.00 -3 8 -7 35.90 4.30 -3 8 -7 44.20 4.80 3 8 7 39.30 4.40 4 -8 7 2.00 2.00 4 -8 7 2.00 2.20 -4 -8 -7 -1.40 2.60 4 -8 7 4.10 2.00 4 8 7 1.50 2.00 -4 8 -7 3.30 2.80 4 8 7 -3.40 1.70 4 8 7 -1.70 1.40 5 -8 7 0.00 2.40 -5 -8 -7 -0.30 2.70 5 -8 7 -6.70 2.30 5 8 7 -3.50 2.20 -5 8 -7 -3.10 2.20 6 -8 7 10.20 2.70 6 -8 7 8.50 3.60 -6 -8 -7 1.00 3.00 -6 8 -7 8.60 3.30 6 8 7 5.10 2.70 7 -8 7 -2.00 3.30 7 -8 7 0.60 2.90 -7 -8 -7 -0.10 2.90 -7 8 -7 1.00 3.10 7 8 7 3.30 3.60 9 -9 -7 23.30 4.20 9 9 -7 22.40 4.70 9 9 -7 21.30 4.50 8 -9 -7 3.90 2.00 -8 -9 7 5.10 3.20 -8 -9 7 2.60 1.90 8 -9 -7 3.40 2.20 8 9 -7 2.80 3.00 8 9 -7 7.20 3.10 -7 -9 7 2.70 1.90 7 -9 -7 4.10 2.10 -7 -9 7 3.50 2.20 7 -9 -7 0.40 1.90 -7 9 7 1.30 1.30 7 9 -7 2.80 2.50 7 9 -7 2.80 2.30 -6 -9 7 24.00 3.00 6 -9 -7 29.60 3.70 6 -9 -7 22.10 2.60 -6 9 7 27.00 2.80 6 9 -7 17.20 3.70 6 9 -7 23.20 4.30 5 -9 -7 20.00 3.20 -5 -9 7 28.30 3.30 5 -9 -7 27.80 2.70 -5 9 7 28.40 3.10 5 9 -7 24.90 3.90 5 9 -7 26.10 3.00 5 9 -7 22.70 3.90 4 -9 -7 6.10 1.90 4 -9 -7 5.60 1.40 4 -9 -7 4.70 2.10 -4 -9 7 5.20 2.00 4 -9 -7 6.80 1.50 4 9 -7 3.30 2.60 4 9 -7 7.40 2.40 4 9 -7 5.60 2.10 -4 9 7 3.90 1.90 3 -9 -7 6.60 1.10 3 -9 -7 6.50 1.70 -3 -9 7 6.60 2.20 3 -9 -7 6.80 1.40 3 -9 -7 8.50 2.10 -3 -9 7 7.90 1.80 3 9 -7 5.70 2.60 3 9 -7 4.90 2.70 -3 9 7 7.10 2.20 3 9 -7 3.90 2.30 2 -9 -7 12.70 2.50 2 -9 -7 9.30 2.30 2 -9 -7 12.50 1.70 -2 -9 7 8.40 1.90 -2 -9 7 15.10 2.10 -2 -9 7 14.70 1.00 2 9 -7 13.40 2.60 2 9 -7 9.90 2.50 2 9 -7 15.00 2.90 -2 9 7 8.80 2.40 1 -9 -7 116.89 6.00 -1 -9 7 112.59 4.90 -1 -9 7 120.99 4.10 -1 -9 7 120.69 5.60 1 -9 -7 124.69 5.80 1 9 -7 133.49 6.70 1 9 -7 129.59 7.40 -1 9 7 123.59 4.40 1 9 -7 129.09 6.90 -1 9 7 129.19 6.10 0 -9 7 1.20 1.10 0 -9 -7 0.30 1.40 0 -9 7 0.50 1.40 0 -9 7 -0.10 1.70 0 -9 -7 0.80 1.40 0 9 -7 2.50 1.90 0 9 7 -0.20 1.90 0 9 -7 1.80 2.20 0 9 -7 0.30 1.50 0 9 7 0.40 1.30 1 -9 7 146.89 6.30 -1 -9 -7 141.49 6.70 1 -9 7 142.09 6.80 1 -9 7 147.19 6.00 -1 -9 -7 149.09 6.80 -1 9 -7 143.09 7.40 -1 9 -7 154.68 6.80 1 9 7 147.99 6.10 -1 9 -7 138.49 7.40 1 9 7 131.29 6.40 -2 -9 -7 -0.80 2.20 -2 -9 -7 -0.10 1.90 2 -9 7 6.40 1.80 2 -9 7 0.90 2.00 2 -9 7 6.50 2.40 -2 9 -7 3.10 2.70 2 9 7 -0.30 1.20 2 9 7 3.40 2.30 -2 9 -7 2.80 1.50 2 9 7 2.00 1.70 -2 9 -7 5.20 2.60 -3 -9 -7 7.80 2.50 3 -9 7 8.60 2.60 3 -9 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382.96 13.50 -2 4 9 375.76 9.10 2 4 -9 385.46 9.30 2 4 -9 389.96 13.50 2 4 -9 380.66 10.10 -2 4 9 383.96 11.30 -2 4 9 386.96 11.60 -1 -4 9 0.20 1.60 1 -4 -9 0.20 1.40 -1 -4 9 1.00 0.90 -1 -4 9 0.80 1.80 1 -4 -9 0.90 1.30 1 4 -9 0.20 1.40 1 4 -9 0.90 1.80 -1 4 9 -0.50 0.60 -1 4 9 2.30 1.60 -1 4 9 -0.20 1.20 1 4 -9 -0.50 1.30 0 -4 9 5.10 2.20 0 -4 -9 2.90 1.20 0 -4 -9 -0.80 1.90 0 -4 -9 5.20 1.70 0 -4 9 4.70 1.20 0 -4 9 3.80 2.00 0 4 9 3.80 2.10 0 4 -9 2.70 2.30 0 4 -9 1.20 1.30 0 4 -9 4.00 1.80 0 4 9 4.10 1.50 1 -4 9 4.20 2.20 -1 -4 -9 10.00 2.50 1 -4 9 7.00 2.10 1 -4 9 5.40 1.50 -1 -4 -9 5.50 1.90 -1 -4 -9 6.20 1.30 -1 4 -9 4.50 1.20 -1 4 -9 6.20 1.90 1 4 9 4.60 1.70 1 4 9 5.00 1.00 -1 4 -9 4.70 2.10 1 4 9 7.30 2.40 -2 -4 -9 205.48 6.00 2 -4 9 200.08 8.00 -2 -4 -9 223.38 9.00 2 -4 9 219.88 7.50 -2 -4 -9 208.28 9.00 2 -4 9 205.78 9.30 2 4 9 223.98 6.40 -2 4 -9 204.98 9.00 2 4 9 225.88 8.70 2 4 9 217.08 8.80 -2 4 -9 217.28 8.30 -3 -4 -9 82.79 5.80 3 -4 9 85.99 4.90 3 -4 9 82.69 5.80 3 -4 9 76.59 5.00 -3 4 -9 75.99 4.40 -3 4 -9 82.49 6.30 3 4 9 84.59 6.20 3 4 9 74.89 5.20 4 -4 9 39.80 4.60 -4 -4 -9 36.50 5.10 4 -4 9 33.80 3.40 4 -4 9 42.00 4.00 4 4 9 35.60 4.00 -4 4 -9 41.80 5.10 4 4 9 41.30 4.70 5 -4 9 2.80 2.40 5 -4 9 -0.10 2.20 -5 -4 -9 -1.90 2.60 5 4 9 6.10 3.50 -5 4 -9 -2.50 2.80 6 -4 9 3.90 2.70 6 -4 9 0.10 2.50 6 4 9 -1.60 3.30 -6 4 -9 -0.70 2.80 7 -4 9 7.00 3.60 -7 -4 -9 24.40 5.10 7 -4 9 19.20 3.70 7 4 9 18.50 5.50 -7 4 -9 21.80 4.70 9 -5 -9 -1.40 2.00 9 5 -9 -0.80 2.90 9 5 -9 2.40 2.40 -8 -5 9 0.60 2.90 -8 -5 9 3.90 1.50 8 -5 -9 2.80 2.20 8 5 -9 4.70 3.10 8 5 -9 2.20 2.40 7 -5 -9 -2.10 1.10 -7 -5 9 0.60 2.00 -7 -5 9 3.00 1.60 7 5 -9 -3.60 2.60 7 5 -9 -2.60 1.50 -7 5 9 -1.00 1.10 -6 -5 9 107.59 5.90 -6 -5 9 113.59 5.10 6 -5 -9 114.99 5.70 6 5 -9 116.49 8.60 -6 5 9 114.79 4.70 6 5 -9 110.09 7.50 -5 -5 9 5.40 1.90 5 -5 -9 3.40 0.90 5 -5 -9 3.80 1.60 5 5 -9 5.00 1.00 -5 5 9 3.50 1.70 5 5 -9 6.20 1.90 5 5 -9 3.80 2.20 5 5 -9 7.10 2.90 4 -5 -9 20.50 2.80 4 -5 -9 18.30 1.00 4 -5 -9 23.50 2.70 -4 -5 9 20.10 2.70 4 5 -9 13.30 3.10 4 5 -9 18.30 3.40 4 5 -9 19.80 1.60 4 5 -9 21.00 2.80 -4 5 9 20.60 2.60 -4 5 9 17.90 2.40 3 -5 -9 27.00 2.90 -3 -5 9 27.90 3.10 -3 -5 9 26.90 1.70 3 -5 -9 27.50 2.70 3 5 -9 25.60 3.80 3 5 -9 26.50 1.80 3 5 -9 37.60 3.50 3 5 -9 19.70 3.00 -3 5 9 28.40 3.10 2 -5 -9 20.70 2.90 -2 -5 9 23.50 1.80 2 -5 -9 26.80 2.70 -2 -5 9 19.50 2.80 -2 -5 9 24.70 3.00 -2 5 9 22.70 1.10 2 5 -9 16.50 2.80 2 5 -9 23.20 3.20 2 5 -9 21.50 3.10 -2 5 9 27.30 2.80 -2 5 9 27.90 2.60 -1 -5 9 10.10 2.10 1 -5 -9 8.40 1.90 -1 -5 9 9.30 1.40 -1 -5 9 7.70 2.30 1 -5 -9 10.30 2.30 1 5 -9 10.30 2.60 1 5 -9 10.70 2.10 -1 5 9 11.50 2.20 1 5 -9 10.30 2.90 -1 5 9 10.90 2.00 -1 5 9 10.90 1.20 0 -5 9 48.50 4.40 0 -5 -9 56.09 3.90 0 -5 -9 48.70 4.30 0 -5 9 42.80 3.40 0 -5 9 49.90 2.80 0 5 -9 50.29 4.20 0 5 -9 45.30 4.30 0 5 9 53.09 4.20 0 5 9 49.10 3.50 0 5 -9 57.39 3.90 1 -5 9 3.50 1.50 1 -5 9 3.50 1.70 1 -5 9 1.00 2.30 -1 -5 -9 7.00 2.10 -1 -5 -9 7.50 2.30 -1 -5 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9 14.00 4.00 8 7 -9 6.50 2.90 8 7 -9 5.30 2.90 7 -7 -9 1.90 2.20 -7 -7 9 -0.50 1.80 -7 -7 9 -2.00 1.60 -7 7 9 -1.20 1.20 7 7 -9 0.00 2.30 7 7 -9 0.40 3.00 -6 -7 9 2.30 1.90 6 -7 -9 2.50 2.10 6 7 -9 -1.00 2.00 6 7 -9 2.90 3.00 -6 7 9 2.40 1.70 5 -7 -9 5.60 1.90 -5 -7 9 4.90 2.00 5 -7 -9 6.30 1.30 5 7 -9 3.50 2.30 5 7 -9 6.10 3.10 -5 7 9 7.20 2.00 5 7 -9 3.60 2.00 -4 -7 9 1.60 2.00 4 -7 -9 3.40 0.90 4 -7 -9 1.20 1.50 4 -7 -9 4.30 1.80 4 7 -9 3.00 2.70 -4 7 9 2.50 1.90 4 7 -9 3.20 1.90 4 7 -9 1.30 2.00 -3 -7 9 31.70 3.40 3 -7 -9 26.50 3.00 3 -7 -9 25.20 2.80 -3 -7 9 22.60 1.30 -3 -7 9 24.20 2.40 3 7 -9 19.80 3.20 -3 7 9 23.50 1.50 3 7 -9 16.60 3.10 3 7 -9 21.60 3.30 -3 7 9 20.20 3.00 -2 -7 9 12.80 2.60 -2 -7 9 10.80 1.70 2 -7 -9 12.60 2.60 2 -7 -9 8.90 2.60 -2 -7 9 10.40 1.40 -2 7 9 14.50 1.40 -2 7 9 10.50 1.80 2 7 -9 8.90 2.60 -2 7 9 13.10 2.50 2 7 -9 11.10 2.80 2 7 -9 7.00 2.80 -1 -7 9 40.20 2.90 -1 -7 9 38.70 3.60 -1 -7 9 46.80 4.00 1 -7 -9 32.50 3.40 1 -7 -9 38.90 3.40 1 7 -9 39.50 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10 11.80 2.40 1 3 -10 13.90 3.10 -1 3 10 17.70 1.10 1 3 -10 13.20 2.70 -1 3 10 17.20 1.10 1 3 -10 13.70 2.50 0 -3 10 3.40 1.80 0 -3 -10 -0.70 1.40 0 -3 10 3.80 1.20 0 -3 10 0.60 1.50 0 -3 -10 1.30 1.40 0 -3 -10 0.40 2.30 0 3 -10 2.00 1.40 0 3 -10 4.40 2.60 0 3 -10 -0.70 1.60 0 3 10 2.70 2.20 0 3 10 -0.80 1.50 -1 -3 -10 -0.70 1.10 -1 -3 -10 2.60 2.30 1 -3 10 -0.60 1.20 1 -3 10 -1.00 1.90 -1 -3 -10 -3.70 2.20 1 -3 10 -3.10 1.50 1 3 10 -2.00 1.40 -1 3 -10 -0.20 1.00 -1 3 -10 2.00 2.10 1 3 10 1.40 1.60 -1 3 -10 2.10 1.70 2 -3 10 5.50 2.90 2 -3 10 4.20 2.30 -2 -3 -10 1.90 2.90 2 -3 10 0.10 1.50 -2 3 -10 2.30 1.60 2 3 10 -1.10 2.10 2 3 10 0.50 2.50 -2 3 -10 3.30 2.30 3 -3 10 10.90 2.80 -3 -3 -10 6.00 3.40 3 -3 10 10.60 2.90 3 -3 10 10.70 2.40 3 3 10 6.40 3.10 -3 3 -10 8.30 3.50 3 3 10 7.30 2.50 4 -3 10 47.10 4.50 4 -3 10 46.90 4.30 4 -3 10 45.30 5.70 -4 -3 -10 45.60 5.60 4 3 10 48.20 4.60 -4 3 -10 50.69 6.00 4 3 10 44.20 5.10 5 -3 10 15.20 2.90 5 -3 10 16.30 4.40 5 3 10 12.70 3.60 -5 3 -10 13.50 4.20 6 -3 10 4.90 2.70 -6 -3 -10 2.20 3.60 6 -3 10 -1.80 3.60 -6 3 -10 -1.30 3.20 6 3 10 0.90 2.70 9 -4 -10 1.00 2.20 9 -4 -10 -0.60 1.80 9 4 -10 -4.70 2.70 9 4 -10 -3.70 2.30 8 -4 -10 12.60 2.70 -8 -4 10 12.50 1.90 -8 -4 10 6.70 2.70 8 4 -10 7.40 3.60 8 4 -10 10.20 3.60 7 -4 -10 44.80 4.00 -7 -4 10 54.49 5.20 -7 -4 10 44.50 3.30 -7 4 10 40.90 2.90 7 4 -10 59.79 7.20 7 4 -10 37.40 5.40 -6 -4 10 33.70 4.20 -6 -4 10 26.00 2.90 6 -4 -10 29.40 3.30 6 4 -10 35.00 5.00 -6 4 10 25.90 2.90 6 4 -10 23.30 4.00 -5 -4 10 29.40 3.10 5 -4 -10 30.10 3.30 5 4 -10 30.20 3.20 5 4 -10 25.50 4.20 5 4 -10 31.40 2.20 5 4 -10 25.90 3.80 -5 4 10 29.60 3.00 -4 -4 10 1.70 1.80 4 -4 -10 1.60 1.70 4 4 -10 0.70 1.90 4 4 -10 0.90 1.80 4 4 -10 1.20 1.00 4 4 -10 3.60 1.90 -4 4 10 1.20 1.80 -4 4 10 -0.40 1.30 3 -4 -10 149.79 6.30 -3 -4 10 139.09 6.00 3 -4 -10 147.29 6.50 3 4 -10 142.49 8.10 3 4 -10 142.29 7.60 3 4 -10 143.89 5.10 -3 4 10 130.99 5.90 3 4 -10 144.29 6.80 -3 4 10 143.79 4.80 2 -4 -10 380.86 12.60 -2 -4 10 378.26 9.60 -2 -4 10 381.56 13.00 -2 -4 10 394.66 12.20 2 -4 -10 390.46 11.90 -2 4 10 401.56 12.10 -2 4 10 388.66 9.40 2 4 -10 404.66 14.20 2 4 -10 391.86 13.00 -2 4 10 388.06 12.20 2 4 -10 397.66 14.20 1 -4 -10 9.70 2.40 1 -4 -10 7.80 1.90 -1 -4 10 7.70 2.60 1 -4 -10 6.80 2.00 -1 -4 10 8.90 2.10 -1 -4 10 8.50 1.30 1 4 -10 7.90 2.80 -1 4 10 10.70 2.40 1 4 -10 6.30 2.00 1 4 -10 7.90 2.20 -1 4 10 9.90 1.10 -1 4 10 9.60 2.20 0 -4 10 22.60 3.40 0 -4 -10 20.30 3.60 0 -4 10 26.10 2.30 0 -4 -10 15.90 2.70 0 -4 10 19.60 2.90 0 -4 -10 26.10 2.90 0 4 -10 27.90 4.10 0 4 -10 20.90 3.10 0 4 -10 24.40 3.00 0 4 10 20.20 3.00 0 4 10 21.70 3.30 -1 -4 -10 50.39 3.30 1 -4 10 51.19 3.20 1 -4 10 44.30 4.30 -1 -4 -10 48.50 4.20 -1 -4 -10 49.70 4.50 1 -4 10 44.90 4.30 -1 4 -10 50.79 3.20 -1 4 -10 48.00 4.10 1 4 10 46.70 4.00 -1 4 -10 52.89 4.70 1 4 10 52.29 4.10 -2 -4 -10 5.10 3.10 2 -4 10 7.90 2.30 2 -4 10 7.90 2.10 2 -4 10 1.10 2.10 2 4 10 5.60 2.20 -2 4 -10 4.70 2.00 2 4 10 5.10 2.70 -2 4 -10 3.20 2.40 -3 -4 -10 -5.70 2.60 3 -4 10 2.30 2.00 3 -4 10 0.70 2.80 3 -4 10 -0.90 1.50 3 4 10 0.50 1.70 -3 4 -10 -0.60 2.90 3 4 10 -1.10 1.90 4 -4 10 7.10 2.50 4 -4 10 6.40 3.50 4 -4 10 7.90 2.60 -4 -4 -10 7.10 2.90 -4 4 -10 3.00 3.30 4 4 10 6.90 2.20 4 4 10 6.60 3.50 5 -4 10 -3.60 3.30 -5 -4 -10 4.40 3.20 5 -4 10 4.40 2.70 -5 4 -10 3.40 3.50 5 4 10 7.40 3.90 6 -4 10 16.40 3.60 6 -4 10 1.70 3.90 6 4 10 7.20 4.20 -6 4 -10 18.80 4.70 9 -5 -10 -1.80 2.00 9 -5 -10 -0.90 1.90 9 5 -10 -0.60 2.00 9 5 -10 -1.20 2.20 8 -5 -10 10.50 2.60 -8 -5 10 7.50 1.80 -8 -5 10 10.30 3.50 8 5 -10 11.50 3.80 8 5 -10 7.40 4.00 7 -5 -10 31.40 3.30 -7 -5 10 34.40 4.70 -7 -5 10 45.90 3.40 7 5 -10 28.50 4.80 -7 5 10 35.10 2.80 7 5 -10 29.40 4.70 6 -5 -10 18.70 3.00 -6 -5 10 22.40 2.80 -6 -5 10 20.60 3.70 -6 5 10 19.80 2.50 6 5 -10 19.00 3.80 6 5 -10 19.30 3.90 5 -5 -10 59.29 4.30 -5 -5 10 62.29 4.30 -5 5 10 57.19 3.80 5 5 -10 59.99 5.60 5 5 -10 58.89 6.50 4 -5 -10 -0.90 1.80 4 -5 -10 0.40 1.50 -4 -5 10 3.00 2.00 -4 5 10 -3.20 1.50 4 5 -10 0.00 2.20 4 5 -10 1.20 1.90 4 5 -10 0.60 0.90 4 5 -10 0.40 1.60 3 -5 -10 3.20 1.90 3 -5 -10 2.90 1.50 -3 -5 10 1.20 2.00 -3 5 10 1.20 2.10 3 5 -10 -2.20 1.70 3 5 -10 0.20 1.90 3 5 -10 2.90 2.40 -2 -5 10 25.70 3.50 2 -5 -10 32.70 3.80 -2 -5 10 30.30 3.60 -2 -5 10 29.70 2.10 2 -5 -10 32.60 3.60 -2 5 10 28.60 3.00 -2 5 10 30.80 3.20 -2 5 10 27.50 0.90 2 5 -10 23.70 3.40 2 5 -10 25.00 3.90 2 5 -10 30.00 3.50 1 -5 -10 7.50 2.30 -1 -5 10 3.20 2.30 -1 -5 10 8.20 1.50 -1 -5 10 5.60 2.60 1 -5 -10 5.10 1.90 1 5 -10 4.70 2.20 -1 5 10 7.40 2.00 1 5 -10 8.30 2.60 -1 5 10 7.80 1.10 1 5 -10 7.80 2.10 -1 5 10 11.80 2.50 0 -5 10 16.40 2.10 0 -5 -10 9.20 3.00 0 -5 -10 16.30 3.10 0 -5 -10 10.90 1.90 0 -5 10 10.50 2.50 0 -5 10 15.00 2.60 0 5 -10 11.50 2.60 0 5 -10 12.70 2.90 0 5 10 10.70 2.80 0 5 10 8.10 2.40 0 5 -10 14.40 2.20 1 -5 10 24.20 3.40 1 -5 10 28.40 2.80 -1 -5 -10 25.10 3.50 1 -5 10 29.20 3.70 -1 -5 -10 28.60 2.60 -1 -5 -10 26.50 3.80 -1 5 -10 32.40 4.60 1 5 10 27.40 3.60 -1 5 -10 31.60 2.70 1 5 10 30.40 3.90 -1 5 -10 31.90 3.80 2 -5 10 12.10 2.40 2 -5 10 10.50 2.80 -2 -5 -10 14.00 3.20 -2 -5 -10 8.40 3.00 2 -5 10 13.90 2.70 2 5 10 12.50 3.00 -2 5 -10 9.90 2.60 2 5 10 15.40 3.20 -2 5 -10 9.40 3.00 3 -5 10 14.40 2.80 3 -5 10 10.60 3.60 3 -5 10 10.70 2.50 -3 -5 -10 9.80 3.10 -3 5 -10 10.70 3.80 3 5 10 13.50 3.10 3 5 10 13.50 3.10 -4 -5 -10 -2.70 3.00 4 -5 10 -0.20 2.20 4 -5 10 -0.10 1.50 4 -5 10 -1.00 2.10 4 5 10 2.10 2.30 -4 5 -10 -3.10 2.90 4 5 10 -1.50 2.10 5 -5 10 0.20 2.50 -5 -5 -10 0.80 3.30 5 -5 10 2.00 3.50 -5 5 -10 -1.80 3.20 5 5 10 1.30 2.50 6 -5 10 4.20 3.20 6 -5 10 -0.30 2.50 -6 5 -10 0.20 3.30 6 5 10 0.60 3.90 9 -6 -10 2.90 2.50 9 6 -10 5.90 3.60 9 6 -10 -1.50 3.20 -8 -6 10 -1.00 3.00 -8 -6 10 -3.10 1.40 8 -6 -10 1.90 2.20 8 6 -10 4.00 3.30 8 6 -10 0.20 2.40 -7 -6 10 22.80 2.90 -7 -6 10 18.20 3.40 7 -6 -10 22.20 3.10 7 6 -10 18.60 4.00 7 6 -10 18.90 4.00 -7 6 10 20.00 2.30 -6 -6 10 10.10 2.20 6 -6 -10 6.70 2.00 6 6 -10 8.20 2.90 -6 6 10 6.50 2.00 6 6 -10 6.00 2.80 -5 -6 10 18.10 2.80 5 -6 -10 17.60 2.70 -5 6 10 19.60 2.80 5 6 -10 18.20 3.50 5 6 -10 15.80 3.40 -4 -6 10 31.20 3.50 4 -6 -10 26.70 2.90 4 -6 -10 28.60 3.50 4 6 -10 27.00 4.20 4 6 -10 30.90 3.70 4 6 -10 26.40 4.10 -4 6 10 29.80 3.40 3 -6 -10 109.29 5.80 3 -6 -10 108.59 5.50 -3 -6 10 110.79 5.50 3 6 -10 120.29 7.60 3 6 -10 122.89 7.40 3 6 -10 115.69 6.30 -3 6 10 120.09 6.10 -2 -6 10 1.10 1.10 -2 -6 10 1.80 1.60 2 -6 -10 5.40 2.20 2 -6 -10 5.20 2.40 2 6 -10 3.40 2.30 -2 6 10 2.30 1.70 2 6 -10 -1.50 2.00 -2 6 10 3.10 1.80 2 6 -10 2.00 2.70 -1 -6 10 0.60 1.20 1 -6 -10 -0.90 1.50 -1 -6 10 -1.30 2.00 -1 -6 10 -3.60 2.00 1 -6 -10 0.10 1.50 -1 6 10 -0.10 1.60 -1 6 10 1.60 1.60 1 6 -10 -2.30 1.90 1 6 -10 -0.80 1.50 1 6 -10 -0.50 2.30 0 -6 10 3.00 1.80 0 -6 10 3.30 1.60 0 -6 -10 0.50 2.40 0 -6 10 1.40 1.80 0 -6 -10 1.20 1.80 0 6 10 4.30 2.40 0 6 -10 2.80 1.50 0 6 10 3.50 2.00 0 6 -10 3.90 2.40 0 6 -10 6.10 2.00 1 -6 10 16.40 2.40 -1 -6 -10 16.90 3.80 1 -6 10 16.90 2.90 -1 -6 -10 16.50 2.00 1 -6 10 12.20 3.20 -1 -6 -10 13.90 2.90 -1 6 -10 11.30 2.70 1 6 10 16.00 3.30 -1 6 -10 24.30 4.40 1 6 10 14.80 3.00 -1 6 -10 17.90 2.40 -2 -6 -10 216.08 9.50 -2 -6 -10 227.08 10.10 2 -6 10 208.88 8.80 2 -6 10 199.18 9.20 2 -6 10 207.88 7.70 2 6 10 195.88 8.60 2 6 10 215.58 9.30 -2 6 -10 208.88 10.10 -2 6 -10 215.88 9.20 -3 -6 -10 6.80 3.60 3 -6 10 2.40 2.20 3 -6 10 3.90 2.00 3 -6 10 3.50 2.40 -3 6 -10 2.20 3.40 3 6 10 5.30 2.60 3 6 10 3.70 2.90 4 -6 10 0.20 2.20 -4 -6 -10 -4.10 2.00 4 -6 10 0.40 1.60 -4 6 -10 -3.10 3.00 4 6 10 -0.90 2.00 4 6 10 -1.90 1.90 5 -6 10 3.60 3.80 5 -6 10 11.40 2.80 -5 -6 -10 9.10 3.90 5 6 10 8.70 3.90 -5 6 -10 8.10 4.10 6 -6 10 0.90 2.00 6 -6 10 0.80 3.00 -6 -6 -10 3.90 3.60 6 6 10 1.10 3.80 -6 6 -10 2.70 3.60 9 -7 -10 -2.20 2.30 9 7 -10 -0.80 3.00 9 7 -10 5.40 3.10 -8 -7 10 -1.00 2.20 8 -7 -10 -1.90 2.00 -8 -7 10 -2.50 1.60 8 7 -10 -2.20 2.20 8 7 -10 3.00 3.60 -7 -7 10 6.20 2.20 -7 -7 10 8.80 3.20 7 -7 -10 1.10 1.70 7 7 -10 2.30 3.30 -7 7 10 0.60 1.50 7 7 -10 5.10 3.00 -6 -7 10 12.80 2.50 6 -7 -10 13.50 2.50 -6 7 10 10.80 2.30 6 7 -10 7.80 3.00 6 7 -10 13.20 3.50 -5 -7 10 5.10 2.20 5 -7 -10 5.40 2.40 5 7 -10 3.40 2.50 -5 7 10 6.50 2.10 5 7 -10 6.50 2.70 4 -7 -10 3.40 1.90 -4 -7 10 1.10 2.00 4 -7 -10 2.90 1.70 4 7 -10 2.00 2.00 -4 7 10 0.70 2.10 4 7 -10 0.90 2.00 4 7 -10 3.10 2.10 3 -7 -10 3.90 2.30 -3 -7 10 4.50 2.20 -3 -7 10 3.50 1.40 3 -7 -10 4.10 1.80 3 7 -10 3.40 2.30 3 7 -10 5.70 2.20 3 7 -10 4.30 2.60 -3 7 10 0.80 2.40 2 -7 -10 173.08 7.70 2 -7 -10 172.08 7.30 -2 -7 10 176.88 5.80 -2 -7 10 171.28 7.60 -2 7 10 178.98 6.50 -2 7 10 171.28 7.60 2 7 -10 174.08 8.20 2 7 -10 168.08 8.80 2 7 -10 182.08 9.10 1 -7 -10 7.10 2.80 -1 -7 10 4.10 1.60 -1 -7 10 2.90 2.60 1 -7 -10 8.70 2.30 -1 -7 10 4.10 2.10 -1 7 10 7.70 2.60 1 7 -10 8.60 3.10 1 7 -10 0.30 2.40 1 7 -10 4.60 2.00 -1 7 10 4.30 1.90 0 -7 -10 29.10 3.70 0 -7 -10 18.90 3.70 0 -7 10 24.80 3.60 0 -7 10 17.50 3.40 0 -7 10 20.30 2.40 0 7 -10 22.40 2.90 0 7 -10 23.30 3.70 0 7 10 16.40 2.70 0 7 10 21.30 3.20 0 7 -10 18.00 3.80 1 -7 10 -1.00 1.50 -1 -7 -10 -1.20 1.70 1 -7 10 -2.10 2.40 1 -7 10 0.20 1.60 -1 -7 -10 1.10 2.10 -1 7 -10 1.30 2.10 1 7 10 1.60 1.90 1 7 10 0.30 2.00 -1 7 -10 2.00 2.80 -1 7 -10 0.10 1.20 2 -7 10 6.80 3.20 -2 -7 -10 6.00 3.20 -2 -7 -10 8.40 3.20 2 -7 10 7.80 2.70 2 -7 10 8.00 2.30 2 7 10 8.60 3.00 -2 7 -10 10.00 3.70 -2 7 -10 3.30 2.30 2 7 10 3.40 2.00 3 -7 10 55.49 5.20 3 -7 10 54.19 4.50 3 -7 10 43.30 4.10 -3 -7 -10 45.30 5.10 -3 7 -10 60.29 6.50 3 7 10 65.89 5.40 -3 7 -10 55.59 5.10 3 7 10 54.29 5.00 -4 -7 -10 5.20 3.80 4 -7 10 2.40 2.40 4 -7 10 2.90 2.60 4 7 10 4.30 3.30 4 7 10 5.90 2.60 -4 7 -10 6.10 3.60 5 -7 10 7.70 3.00 5 -7 10 1.90 2.90 -5 -7 -10 18.20 4.50 5 7 10 8.00 3.20 -5 7 -10 6.90 4.00 6 -7 10 0.10 2.90 6 -7 10 2.30 3.10 -6 -7 -10 8.50 4.00 6 7 10 -2.50 2.60 -6 7 -10 1.00 3.40 9 -8 -10 5.70 2.90 9 8 -10 8.00 3.80 9 8 -10 6.30 4.30 8 -8 -10 1.50 2.40 -8 -8 10 -2.60 1.70 -8 -8 10 -0.10 2.20 8 8 -10 2.40 3.00 8 8 -10 2.10 2.60 -7 -8 10 -1.70 1.80 7 -8 -10 -0.40 2.30 -7 -8 10 -2.20 2.30 -7 8 10 0.70 1.60 7 8 -10 5.00 3.80 7 8 -10 1.50 3.40 6 -8 -10 7.90 2.30 -6 -8 10 11.20 2.60 6 8 -10 10.60 3.40 6 8 -10 6.50 3.10 -6 8 10 9.10 2.30 -5 -8 10 12.40 2.80 5 -8 -10 10.80 2.80 5 8 -10 9.20 3.00 -5 8 10 9.10 2.50 5 8 -10 9.60 3.20 4 -8 -10 7.60 2.20 -4 -8 10 5.80 2.40 4 -8 -10 4.80 2.00 4 8 -10 3.60 2.50 4 8 -10 4.10 2.20 4 8 -10 8.00 2.60 -4 8 10 5.00 2.40 3 -8 -10 174.78 7.70 -3 -8 10 183.78 6.20 -3 -8 10 196.98 8.00 3 -8 -10 176.48 7.60 -3 8 10 178.68 7.50 3 8 -10 168.48 9.20 3 8 -10 162.28 9.20 3 8 -10 173.88 7.90 2 -8 -10 70.09 5.10 -2 -8 10 63.49 4.90 -2 -8 10 57.79 3.60 2 -8 -10 60.79 4.80 -2 8 10 61.59 3.70 -2 8 10 68.89 5.10 2 8 -10 65.29 5.20 2 8 -10 65.89 5.40 2 8 -10 58.69 5.70 -1 -8 10 20.20 2.30 -1 -8 10 22.20 3.20 -1 -8 10 13.40 3.20 1 -8 -10 21.80 3.60 1 -8 -10 21.00 3.50 1 8 -10 22.30 3.60 -1 8 10 15.90 2.50 1 8 -10 16.70 3.00 -1 8 10 18.20 3.10 1 8 -10 18.00 3.80 0 -8 10 24.80 3.70 0 -8 10 27.60 2.80 0 -8 10 18.90 3.50 0 -8 -10 26.70 3.80 0 -8 -10 23.20 3.40 0 8 10 17.50 3.40 0 8 -10 20.90 3.00 0 8 -10 28.40 4.40 0 8 -10 21.70 3.80 0 8 10 19.70 2.80 -1 -8 -10 81.29 6.50 -1 -8 -10 88.99 6.30 1 -8 10 75.39 5.10 1 -8 10 83.49 4.60 1 -8 10 76.29 5.50 1 8 10 83.29 5.40 -1 8 -10 75.29 4.60 1 8 10 79.29 5.80 -1 8 -10 79.79 6.60 -1 8 -10 75.89 6.10 2 -8 10 -0.40 2.50 -2 -8 -10 6.30 3.40 2 -8 10 3.50 2.20 -2 -8 -10 -0.90 2.80 2 -8 10 0.10 2.00 2 8 10 2.40 1.90 -2 8 -10 2.60 2.40 2 8 10 0.80 2.40 -2 8 -10 6.60 3.50 3 -8 10 18.50 3.30 3 -8 10 8.10 3.50 -3 -8 -10 13.30 3.90 3 -8 10 19.80 3.30 3 8 10 15.70 3.20 -3 8 -10 15.00 4.20 3 8 10 14.30 3.60 -3 8 -10 13.50 3.00 4 -8 10 -8.80 2.50 4 -8 10 -1.30 2.40 -4 -8 -10 0.20 3.40 4 8 10 -1.80 1.40 -4 8 -10 3.30 3.50 4 8 10 -1.50 2.90 5 -8 10 1.70 2.90 5 -8 10 -2.10 2.40 -5 -8 -10 1.30 3.30 -5 8 -10 3.40 3.40 5 8 10 -1.60 3.30 -6 -8 -10 22.50 5.20 6 -8 10 10.00 4.70 6 -8 10 15.50 3.60 -6 8 -10 18.50 5.10 6 8 10 11.60 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9 10 9.80 3.10 -1 9 10 8.20 2.00 1 9 -10 10.70 3.40 1 9 -10 11.60 2.80 0 -9 10 4.30 2.50 0 -9 -10 6.90 3.10 0 -9 -10 2.30 2.60 0 -9 10 3.30 1.70 0 -9 10 1.40 1.90 0 9 10 0.50 2.50 0 9 -10 7.30 3.30 0 9 -10 5.50 1.90 0 9 10 1.60 2.00 0 9 -10 5.10 2.40 1 -9 10 33.20 3.50 1 -9 10 33.00 4.00 -1 -9 -10 34.30 4.70 1 -9 10 32.90 4.20 -1 -9 -10 26.80 4.40 1 9 10 36.10 4.60 1 9 10 26.30 3.40 -1 9 -10 37.00 5.10 -1 9 -10 26.90 4.20 2 -9 10 1.50 2.10 -2 -9 -10 6.00 3.20 2 -9 10 0.20 2.00 -2 -9 -10 1.70 2.30 2 -9 10 1.70 2.50 2 9 10 2.30 2.10 -2 9 -10 8.40 3.60 -2 9 -10 3.40 2.70 2 9 10 4.20 2.60 3 -9 10 -0.60 2.70 -3 -9 -10 -0.30 2.20 3 -9 10 -0.60 1.60 3 -9 10 0.20 1.70 -3 -9 -10 4.30 3.50 3 9 10 0.50 2.60 -3 9 -10 -1.90 2.10 -3 9 -10 0.80 3.30 3 9 10 2.30 2.60 4 -9 10 3.40 2.20 4 -9 10 -0.10 2.40 -4 -9 -10 -0.20 3.20 4 9 10 5.10 2.90 -4 9 -10 -0.40 2.50 4 9 10 1.30 2.40 -5 -9 -10 1.50 3.40 5 -9 10 3.90 2.30 5 -9 10 -2.90 3.50 -5 9 -10 2.50 3.40 5 9 10 -1.30 3.50 8 -10 -10 1.60 2.80 -8 -10 10 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14.50 3.00 4 4 -11 11.60 3.60 4 4 -11 20.90 3.20 4 4 -11 12.30 1.90 -4 4 11 15.90 2.90 3 -4 -11 60.89 4.40 -3 -4 11 61.29 4.60 3 -4 -11 52.29 4.40 -3 4 11 61.69 4.70 3 4 -11 65.99 5.10 -3 4 11 53.29 3.00 3 4 -11 48.70 6.00 3 4 -11 46.30 4.70 3 4 -11 49.70 3.10 2 -4 -11 2.70 1.90 -2 -4 11 7.60 2.20 2 -4 -11 5.60 2.30 2 -4 -11 2.80 2.40 -2 -4 11 4.00 2.40 -2 -4 11 3.80 1.00 -2 4 11 4.70 2.00 2 4 -11 5.20 2.70 2 4 -11 5.00 2.10 -2 4 11 2.90 1.00 2 4 -11 3.10 1.70 -2 4 11 3.10 1.90 1 -4 -11 36.30 3.70 1 -4 -11 33.40 3.50 -1 -4 11 37.90 3.60 -1 -4 11 33.10 4.10 -1 -4 11 38.60 2.30 1 -4 -11 38.20 4.50 -1 4 11 35.00 4.10 1 4 -11 40.70 3.90 -1 4 11 34.70 3.30 1 4 -11 32.30 4.10 1 4 -11 40.20 4.90 0 -4 -11 -1.20 2.50 0 -4 11 0.90 1.30 0 -4 -11 0.40 1.50 0 -4 11 -1.20 2.20 0 -4 -11 -3.90 1.90 0 -4 11 -1.50 2.30 0 4 -11 1.00 1.90 0 4 11 -4.00 1.80 0 4 -11 -2.20 2.40 0 4 -11 -0.20 1.20 0 4 11 0.80 1.70 -1 -4 -11 3.10 2.60 1 -4 11 3.00 2.10 1 -4 11 1.30 2.30 -1 -4 -11 0.20 1.20 -1 -4 -11 3.30 3.10 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2.40 -5 -5 11 6.90 2.30 -5 5 11 7.30 2.50 5 5 -11 4.50 3.20 5 5 -11 4.60 2.90 4 -5 -11 6.50 2.20 -4 -5 11 0.30 2.10 4 5 -11 -0.40 2.30 -4 5 11 -0.30 2.00 4 5 -11 0.90 1.80 4 5 -11 -1.00 2.80 4 5 -11 0.40 1.10 3 -5 -11 48.70 4.30 3 -5 -11 44.50 4.30 -3 -5 11 52.59 4.00 3 5 -11 45.80 5.50 3 5 -11 57.99 4.90 3 5 -11 51.39 5.60 -3 5 11 48.10 4.50 2 -5 -11 129.49 6.50 2 -5 -11 126.19 6.80 -2 -5 11 131.49 6.60 -2 -5 11 125.39 6.70 -2 -5 11 122.49 4.20 2 5 -11 125.69 7.40 -2 5 11 128.39 5.90 2 5 -11 122.39 7.30 2 5 -11 130.49 7.30 -2 5 11 124.09 6.20 -1 -5 11 4.90 1.40 1 -5 -11 9.10 2.30 1 -5 -11 4.90 1.90 1 -5 -11 3.00 2.70 -1 -5 11 -1.40 2.20 -1 -5 11 5.60 2.70 1 5 -11 4.70 2.40 1 5 -11 7.00 2.60 -1 5 11 5.30 2.10 1 5 -11 5.50 2.00 -1 5 11 10.30 2.40 0 -5 11 5.50 2.90 0 -5 -11 8.30 3.20 0 -5 11 6.40 2.60 0 -5 -11 7.40 2.00 0 -5 -11 5.80 2.30 0 -5 11 5.40 1.70 0 5 -11 6.50 2.40 0 5 -11 1.70 1.50 0 5 11 5.60 2.50 0 5 -11 5.70 2.60 0 5 11 2.90 2.50 -1 -5 -11 28.90 2.90 1 -5 11 26.10 2.80 -1 -5 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62.79 6.00 -1 -6 -11 60.89 5.80 1 -6 11 61.99 3.90 1 -6 11 59.89 4.70 1 6 11 62.19 5.50 -1 6 -11 64.19 5.60 -1 6 -11 62.79 6.40 1 6 11 66.19 5.30 2 -6 11 -0.20 2.10 -2 -6 -11 -0.50 1.90 -2 -6 -11 -1.10 2.20 2 -6 11 -2.30 2.20 2 -6 11 0.10 1.80 2 6 11 2.90 2.50 2 6 11 -0.30 2.60 -2 6 -11 1.80 3.20 -2 6 -11 -3.60 2.00 3 -6 11 2.70 2.50 3 -6 11 2.20 2.20 -3 -6 -11 4.10 3.40 3 -6 11 5.90 2.20 -3 6 -11 1.70 3.50 3 6 11 9.90 3.00 3 6 11 3.00 3.00 4 -6 11 -0.10 1.60 4 -6 11 -3.00 2.30 -4 -6 -11 -6.90 2.70 4 6 11 -2.60 3.10 -4 6 -11 0.10 3.50 4 6 11 0.60 2.40 5 -6 11 -1.00 2.60 5 -6 11 2.80 2.60 -5 -6 -11 5.80 3.90 -5 6 -11 2.30 3.70 5 6 11 -9.50 3.00 9 -7 -11 -2.40 2.20 9 7 -11 2.30 3.50 9 7 -11 1.10 3.80 8 -7 -11 16.90 3.40 -8 -7 11 13.90 2.60 -8 -7 11 15.20 4.10 8 7 -11 10.80 3.80 8 7 -11 19.80 4.40 -7 -7 11 -3.20 2.40 7 -7 -11 3.50 2.30 -7 -7 11 1.90 2.00 -7 7 11 -0.60 1.60 7 7 -11 -2.90 2.20 7 7 -11 1.80 3.40 6 -7 -11 3.60 1.80 -6 -7 11 3.10 2.00 6 7 -11 1.00 3.30 -6 7 11 0.30 1.70 6 7 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3 17 2.90 2.70 -2 3 17 -2.00 3.10 2 3 -17 4.80 4.10 1 -3 -17 3.40 4.20 1 -3 -17 -1.70 3.10 -1 -3 17 -0.90 2.30 -1 -3 17 1.40 2.70 -1 3 17 -0.10 3.50 -1 3 17 -2.40 2.90 1 3 -17 1.40 4.20 0 -3 17 3.00 2.60 0 -3 17 -4.60 3.30 0 -3 -17 -1.60 3.00 0 3 -17 -2.70 3.60 0 3 17 -2.00 3.10 0 3 17 8.80 3.70 5 -4 -17 5.70 3.70 5 -4 -17 1.30 2.80 -5 -4 17 -2.80 3.00 5 4 -17 0.30 2.80 -5 4 17 3.90 3.10 5 4 -17 -9.30 2.70 -4 -4 17 1.90 3.00 4 -4 -17 10.70 4.20 4 -4 -17 5.30 3.40 4 4 -17 3.40 3.90 4 4 -17 3.60 3.50 -4 4 17 5.80 3.60 3 -4 -17 2.90 3.20 -3 -4 17 4.60 3.50 3 -4 -17 0.20 2.70 3 4 -17 -3.90 2.80 -3 4 17 -0.20 3.10 2 -4 -17 -1.70 3.60 2 -4 -17 1.60 2.50 -2 -4 17 -2.10 3.00 -2 -4 17 3.10 2.80 -2 4 17 2.40 2.70 2 4 -17 -1.50 3.50 2 4 -17 1.20 3.20 -2 4 17 -0.90 3.40 1 -4 -17 5.40 3.60 -1 -4 17 5.50 3.80 1 -4 -17 0.40 3.40 -1 -4 17 11.80 4.00 1 4 -17 2.90 3.30 -1 4 17 5.60 3.20 -1 4 17 -0.50 3.50 0 -4 17 1.00 3.80 0 -4 -17 -6.40 3.40 0 4 -17 4.00 4.60 0 4 17 -0.80 3.40 -5 -5 17 -0.90 2.90 5 -5 -17 3.00 3.00 5 -5 -17 0.00 2.60 5 5 -17 1.60 2.60 5 5 -17 1.30 4.10 -5 5 17 3.50 3.30 -4 -5 17 -0.30 3.20 4 -5 -17 -2.50 2.90 4 -5 -17 2.60 2.60 -4 5 17 0.10 3.30 4 5 -17 -1.60 3.60 4 5 -17 -2.00 2.90 3 -5 -17 3.40 3.40 3 -5 -17 6.40 3.40 -3 -5 17 6.20 3.60 3 5 -17 10.60 4.50 -3 5 17 7.70 4.00 -2 -5 17 11.40 3.40 2 -5 -17 8.70 3.10 -2 -5 17 20.30 5.00 2 -5 -17 6.90 4.50 -2 5 17 13.00 3.40 2 5 -17 8.90 3.90 -2 5 17 10.80 4.20 2 5 -17 19.60 5.40 1 -5 -17 7.30 4.60 -1 -5 17 3.50 3.10 -1 -5 17 5.30 3.70 1 -5 -17 3.30 3.80 1 5 -17 4.10 4.60 -1 5 17 3.50 3.10 -1 5 17 4.00 3.00 -4 -6 17 2.80 2.90 4 -6 -17 -3.80 3.10 4 -6 -17 0.20 2.40 -4 6 17 1.10 3.20 4 6 -17 -0.20 3.00 4 6 -17 -0.90 3.90 3 -6 -17 11.30 4.20 -3 -6 17 10.20 4.20 -3 6 17 12.60 4.10 3 6 -17 3.00 4.10 -2 -6 17 3.00 2.90 2 -6 -17 2.30 3.40 -2 6 17 6.50 3.30 2 6 -17 6.60 4.00 2 6 -17 -0.50 3.30 -1 -6 17 16.60 4.80 -1 -6 17 5.70 3.20 1 -6 -17 8.70 3.50 -1 6 17 5.00 3.30 1 6 -17 4.90 3.60 -1 6 17 10.30 3.40 -4 -7 17 0.30 3.50 4 -7 -17 -0.60 3.20 -4 7 17 -0.10 3.40 4 7 -17 0.90 3.20 4 7 -17 3.10 3.50 3 -7 -17 2.10 3.50 -3 -7 17 5.10 3.90 3 7 -17 11.00 4.60 -3 7 17 8.70 3.80 2 -7 -17 11.20 4.40 -2 -7 17 5.20 4.20 -2 7 17 14.20 4.40 2 7 -17 5.60 4.00 2 7 -17 0.00 3.20 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 44059 _shelx_res_file ; TITL bk6cg CELL 0.71073 7.7302 17.2550 13.1989 90.000 106.079 90.000 ZERR 4.00 0.0006 0.0016 0.0011 0.000 0.002 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N O UNIT 84 64 8 8 MERG 2 OMIT -2 57.1 FMAP 2 PLAN 10 SIZE 0.14 0.160 0.20 ACTA BOND $H CONF HTAB L.S. 20 OMIT 0 1 1 TEMP 23.00 WGHT 0.051100 0.449000 FVAR 0.50046 N1 3 0.499647 0.382708 0.438571 11.00000 0.02815 0.04547 = 0.03018 0.00190 0.00413 -0.00117 N2 3 0.321337 0.367412 0.387280 11.00000 0.02870 0.05567 = 0.03671 -0.00295 0.00357 -0.00341 C3 1 0.260111 0.328605 0.456157 11.00000 0.03417 0.04493 = 0.04292 -0.00807 0.01200 -0.00353 C4 1 0.396367 0.316304 0.551955 11.00000 0.03864 0.04235 = 0.04018 -0.00008 0.01657 0.00184 C5 1 0.546344 0.351988 0.535677 11.00000 0.03131 0.04426 = 0.03092 0.00218 0.00820 0.00481 C11 1 0.609362 0.420223 0.382737 11.00000 0.02962 0.03583 = 0.03178 0.00270 0.00676 0.00153 C12 1 0.725148 0.479365 0.428485 11.00000 0.04129 0.04201 = 0.03834 -0.00522 0.00843 0.00006 AFIX 43 H12 2 0.734759 0.494927 0.497286 11.00000 -1.20000 AFIX 0 C13 1 0.826501 0.515084 0.370584 11.00000 0.04932 0.04547 = 0.06247 -0.00257 0.01662 -0.01271 AFIX 43 H13 2 0.906459 0.554355 0.400999 11.00000 -1.20000 AFIX 0 C14 1 0.809889 0.492991 0.268671 11.00000 0.07220 0.05930 = 0.06551 0.00299 0.03928 -0.01354 AFIX 43 H14 2 0.877475 0.517643 0.229840 11.00000 -1.20000 AFIX 0 C15 1 0.693338 0.434384 0.223745 11.00000 0.07670 0.06697 = 0.04511 -0.00545 0.03268 -0.01144 AFIX 43 H15 2 0.682022 0.419697 0.154415 11.00000 -1.20000 AFIX 0 C16 1 0.593567 0.397401 0.280527 11.00000 0.04936 0.04725 = 0.03802 -0.00557 0.01313 -0.00784 AFIX 43 H16 2 0.516007 0.357303 0.250291 11.00000 -1.20000 AFIX 0 C31 1 0.069069 0.302155 0.427396 11.00000 0.03950 0.07601 = 0.06419 -0.01463 0.01527 -0.01484 AFIX 137 H31A 2 0.007309 0.321337 0.358613 11.00000 -1.50000 H31B 2 0.011520 0.321554 0.478045 11.00000 -1.50000 H31C 2 0.065364 0.246542 0.427010 11.00000 -1.50000 AFIX 0 C41 1 0.383381 0.273275 0.643375 11.00000 0.05802 0.05395 = 0.05375 0.00797 0.02843 0.00382 AFIX 43 H41 2 0.488971 0.265359 0.696926 11.00000 -1.20000 AFIX 0 O41 4 0.245762 0.246708 0.655732 11.00000 0.07371 0.07338 = 0.09163 0.01652 0.05225 -0.00134 O51 4 0.721158 0.356201 0.590176 11.00000 0.02957 0.07823 = 0.02966 0.00679 0.00394 0.00505 C51 1 0.930232 0.331960 0.752299 11.00000 0.03146 0.04171 = 0.03330 0.00161 0.00760 0.00251 AFIX 43 H51 2 0.992533 0.301273 0.716296 11.00000 -1.20000 AFIX 0 C52 1 0.772651 0.365087 0.699961 11.00000 0.03292 0.04525 = 0.02906 0.00505 0.00613 0.00125 C53 1 0.672962 0.411391 0.750883 11.00000 0.03742 0.05830 = 0.04698 0.00152 0.00340 0.01541 AFIX 43 H53 2 0.565495 0.434209 0.713025 11.00000 -1.20000 AFIX 0 C54 1 0.736908 0.422153 0.856718 11.00000 0.04497 0.06055 = 0.05144 -0.01129 0.01393 0.01103 AFIX 43 H54 2 0.670226 0.451687 0.891353 11.00000 -1.20000 AFIX 0 C54A 1 0.901717 0.389719 0.915410 11.00000 0.03977 0.04542 = 0.03484 -0.00091 0.00983 -0.00306 C55 1 0.975659 0.402558 1.024887 11.00000 0.05651 0.06431 = 0.03919 -0.00892 0.01488 -0.00844 AFIX 43 H55 2 0.911588 0.431860 1.061369 11.00000 -1.20000 AFIX 0 C56 1 1.137965 0.372938 1.077402 11.00000 0.06110 0.07439 = 0.03293 0.00201 -0.00040 -0.01374 AFIX 43 H56 2 1.184189 0.382036 1.149294 11.00000 -1.20000 AFIX 0 C57 1 1.235986 0.328866 1.024096 11.00000 0.04662 0.06654 = 0.04757 0.00774 -0.00762 0.00007 AFIX 43 H57 2 1.348322 0.309561 1.060518 11.00000 -1.20000 AFIX 0 C58 1 1.168908 0.313768 0.919145 11.00000 0.04089 0.05543 = 0.04316 0.00326 0.00092 0.00682 AFIX 43 H58 2 1.234628 0.283321 0.884945 11.00000 -1.20000 AFIX 0 C58A 1 1.000274 0.344018 0.861890 11.00000 0.03258 0.03772 = 0.03499 0.00563 0.00609 -0.00194 HKLF 4 REM bk6cg REM R1 = 0.0474 for 2711 Fo > 4sig(Fo) and 0.0905 for all 4311 data REM 227 parameters refined using 0 restraints END WGHT 0.0511 0.4489 REM Instructions for potential hydrogen bonds EQIV $1 x+1, y, z HTAB C51 O41_$1 REM Highest difference peak 0.168, deepest hole -0.246, 1-sigma level 0.048 Q1 1 0.7588 0.3945 0.1741 11.00000 0.05 0.17 Q2 1 0.8984 0.6146 0.4453 11.00000 0.05 0.15 Q3 1 0.5612 0.4232 0.3205 11.00000 0.05 0.15 Q4 1 0.9016 0.4196 0.4816 11.00000 0.05 0.14 Q5 1 0.7159 0.4283 0.4152 11.00000 0.05 0.14 Q6 1 0.0366 0.2870 0.4956 11.00000 0.05 0.14 Q7 1 0.7239 0.4869 0.8973 11.00000 0.05 0.14 Q8 1 0.5426 0.3927 0.0575 11.00000 0.05 0.14 Q9 1 -0.0831 0.3569 0.5060 11.00000 0.05 0.14 Q10 1 1.3305 0.3489 0.8088 11.00000 0.05 0.13 ; _shelx_res_checksum 1852 _shelxl_version_number 2.014 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy N N1 0.49965(16) 0.38271(8) 0.43857(10) 0.0354(3) Uani d 1 N N2 0.32134(17) 0.36741(8) 0.38728(10) 0.0415(3) Uani d 1 C C3 0.2601(2) 0.32861(10) 0.45616(13) 0.0404(4) Uani d 1 C C4 0.3964(2) 0.31630(10) 0.55195(13) 0.0393(4) Uani d 1 C C5 0.5463(2) 0.35199(9) 0.53568(12) 0.0356(3) Uani d 1 C C11 0.60936(19) 0.42022(9) 0.38274(11) 0.0328(3) Uani d 1 C C12 0.7251(2) 0.47936(9) 0.42849(13) 0.0411(4) Uani d 1 H H12 0.7348 0.4949 0.4973 0.049 Uiso calc 1 C C13 0.8265(2) 0.51508(11) 0.37058(16) 0.0522(5) Uani d 1 H H13 0.9065 0.5544 0.4010 0.063 Uiso calc 1 C C14 0.8099(3) 0.49299(12) 0.26867(17) 0.0616(6) Uani d 1 H H14 0.8775 0.5176 0.2298 0.074 Uiso calc 1 C C15 0.6933(3) 0.43438(12) 0.22374(15) 0.0598(5) Uani d 1 H H15 0.6820 0.4197 0.1544 0.072 Uiso calc 1 C C16 0.5936(2) 0.39740(10) 0.28053(13) 0.0447(4) Uani d 1 H H16 0.5160 0.3573 0.2503 0.054 Uiso calc 1 C C31 0.0691(2) 0.30215(13) 0.42740(16) 0.0597(5) Uani d 1 H H31A 0.0073 0.3213 0.3586 0.090 Uiso calc 1 H H31B 0.0115 0.3216 0.4780 0.090 Uiso calc 1 H H31C 0.0654 0.2465 0.4270 0.090 Uiso calc 1 C C41 0.3834(3) 0.27328(11) 0.64338(15) 0.0526(5) Uani d 1 H H41 0.4890 0.2654 0.6969 0.063 Uiso calc 1 O O41 0.2458(2) 0.24671(9) 0.65573(13) 0.0737(5) Uani d 1 O O51 0.72116(14) 0.35620(8) 0.59018(8) 0.0467(3) Uani d 1 C C51 0.9302(2) 0.33196(9) 0.75230(12) 0.0358(3) Uani d 1 H H51 0.9925 0.3013 0.7163 0.043 Uiso calc 1 C C52 0.7727(2) 0.36509(9) 0.69996(12) 0.0362(4) Uani d 1 C C53 0.6730(2) 0.41139(11) 0.75088(14) 0.0492(4) Uani d 1 H H53 0.5655 0.4342 0.7130 0.059 Uiso calc 1 C C54 0.7369(2) 0.42215(11) 0.85672(14) 0.0522(5) Uani d 1 H H54 0.6702 0.4517 0.8914 0.063 Uiso calc 1 C C54A 0.9017(2) 0.38972(10) 0.91541(12) 0.0401(4) Uani d 1 C C55 0.9757(3) 0.40256(12) 1.02489(14) 0.0530(5) Uani d 1 H H55 0.9116 0.4319 1.0614 0.064 Uiso calc 1 C C56 1.1380(3) 0.37294(13) 1.07740(14) 0.0588(5) Uani d 1 H H56 1.1842 0.3820 1.1493 0.071 Uiso calc 1 C C57 1.2360(3) 0.32887(12) 1.02410(15) 0.0577(5) Uani d 1 H H57 1.3483 0.3096 1.0605 0.069 Uiso calc 1 C C58 1.1689(2) 0.31377(11) 0.91914(14) 0.0486(4) Uani d 1 H H58 1.2346 0.2833 0.8849 0.058 Uiso calc 1 C C58A 1.0003(2) 0.34402(9) 0.86189(12) 0.0357(4) Uani d 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 N1 0.0282(7) 0.0455(8) 0.0302(7) -0.0012(5) 0.0041(5) 0.0019(6) N2 0.0287(7) 0.0557(9) 0.0367(7) -0.0034(6) 0.0036(6) -0.0029(6) C3 0.0342(8) 0.0449(9) 0.0429(9) -0.0035(7) 0.0120(7) -0.0081(7) C4 0.0386(9) 0.0423(9) 0.0402(9) 0.0018(7) 0.0166(7) -0.0001(7) C5 0.0313(8) 0.0443(9) 0.0309(8) 0.0048(7) 0.0082(6) 0.0022(6) C11 0.0296(7) 0.0358(8) 0.0318(8) 0.0015(6) 0.0068(6) 0.0027(6) C12 0.0413(9) 0.0420(9) 0.0383(9) 0.0001(7) 0.0084(7) -0.0052(7) C13 0.0493(10) 0.0455(10) 0.0625(12) -0.0127(8) 0.0166(9) -0.0026(9) C14 0.0722(14) 0.0593(12) 0.0655(13) -0.0135(10) 0.0393(11) 0.0030(10) C15 0.0767(14) 0.0670(13) 0.0451(10) -0.0114(11) 0.0327(10) -0.0055(9) C16 0.0494(10) 0.0473(10) 0.0380(9) -0.0078(8) 0.0131(8) -0.0056(7) C31 0.0395(10) 0.0760(14) 0.0642(13) -0.0148(9) 0.0153(9) -0.0146(11) C41 0.0580(11) 0.0540(11) 0.0537(11) 0.0038(9) 0.0284(9) 0.0080(9) O41 0.0737(10) 0.0734(10) 0.0916(12) -0.0013(8) 0.0523(9) 0.0165(8) O51 0.0296(6) 0.0782(9) 0.0297(6) 0.0051(5) 0.0039(5) 0.0068(5) C51 0.0315(8) 0.0417(9) 0.0333(8) 0.0025(6) 0.0076(6) 0.0016(7) C52 0.0329(8) 0.0453(9) 0.0291(8) 0.0013(7) 0.0061(6) 0.0050(7) C53 0.0374(9) 0.0583(11) 0.0470(10) 0.0154(8) 0.0034(8) 0.0015(8) C54 0.0450(10) 0.0606(12) 0.0514(11) 0.0110(8) 0.0139(9) -0.0113(9) C54A 0.0398(9) 0.0454(9) 0.0348(8) -0.0031(7) 0.0098(7) -0.0009(7) C55 0.0565(12) 0.0643(12) 0.0392(10) -0.0084(9) 0.0149(9) -0.0089(9) C56 0.0611(12) 0.0744(14) 0.0329(9) -0.0137(10) -0.0004(9) 0.0020(9) C57 0.0466(11) 0.0665(13) 0.0476(11) 0.0001(9) -0.0076(9) 0.0077(9) C58 0.0409(9) 0.0554(11) 0.0432(10) 0.0068(8) 0.0009(8) 0.0033(8) C58A 0.0326(8) 0.0377(8) 0.0350(8) -0.0019(6) 0.0061(7) 0.0056(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C5 N1 N2 111.14(12) C5 N1 C11 129.29(12) N2 N1 C11 119.30(12) C3 N2 N1 105.01(13) N2 C3 C4 111.76(14) N2 C3 C31 119.97(16) C4 C3 C31 128.26(16) C5 C4 C3 104.03(14) C5 C4 C41 127.95(16) C3 C4 C41 127.96(16) N1 C5 O51 117.02(13) N1 C5 C4 108.04(13) O51 C5 C4 134.67(14) C16 C11 C12 120.67(14) C16 C11 N1 118.22(14) C12 C11 N1 121.09(13) C11 C12 C13 119.06(15) C11 C12 H12 120.5 C13 C12 H12 120.5 C14 C13 C12 120.38(17) C14 C13 H13 119.8 C12 C13 H13 119.8 C13 C14 C15 120.02(17) C13 C14 H14 120.0 C15 C14 H14 120.0 C16 C15 C14 120.44(17) C16 C15 H15 119.8 C14 C15 H15 119.8 C15 C16 C11 119.40(16) C15 C16 H16 120.3 C11 C16 H16 120.3 C3 C31 H31A 109.5 C3 C31 H31B 109.5 H31A C31 H31B 109.5 C3 C31 H31C 109.5 H31A C31 H31C 109.5 H31B C31 H31C 109.5 O41 C41 C4 125.07(19) O41 C41 H41 117.5 C4 C41 H41 117.5 C5 O51 C52 120.97(12) C52 C51 C58A 119.83(14) C52 C51 H51 120.1 C58A C51 H51 120.1 C51 C52 O51 116.15(13) C51 C52 C53 122.23(15) O51 C52 C53 121.41(14) C54 C53 C52 118.57(15) C54 C53 H53 120.7 C52 C53 H53 120.7 C53 C54 C54A 121.75(16) C53 C54 H54 119.1 C54A C54 H54 119.1 C54 C54A C58A 118.46(14) C54 C54A C55 123.10(16) C58A C54A C55 118.41(15) C56 C55 C54A 121.20(17) C56 C55 H55 119.4 C54A C55 H55 119.4 C55 C56 C57 120.24(17) C55 C56 H56 119.9 C57 C56 H56 119.9 C58 C57 C56 120.69(18) C58 C57 H57 119.7 C56 C57 H57 119.7 C57 C58 C58A 120.52(17) C57 C58 H58 119.7 C58A C58 H58 119.7 C51 C58A C58 121.90(15) C51 C58A C54A 119.14(14) C58 C58A C54A 118.93(15) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance N1 C5 1.3408(19) N1 N2 1.3824(17) N1 C11 1.4240(19) N2 C3 1.318(2) C3 C4 1.420(2) C3 C31 1.491(2) C4 C5 1.381(2) C4 C41 1.444(2) C5 O51 1.3455(18) C11 C16 1.378(2) C11 C12 1.381(2) C12 C13 1.382(2) C12 H12 0.9300 C13 C14 1.370(3) C13 H13 0.9300 C14 C15 1.375(3) C14 H14 0.9300 C15 C16 1.373(2) C15 H15 0.9300 C16 H16 0.9300 C31 H31A 0.9600 C31 H31B 0.9600 C31 H31C 0.9600 C41 O41 1.210(2) C41 H41 0.9300 O51 C52 1.4008(18) C51 C52 1.350(2) C51 C58A 1.412(2) C51 H51 0.9300 C52 C53 1.404(2) C53 C54 1.359(2) C53 H53 0.9300 C54 C54A 1.411(2) C54 H54 0.9300 C54A C58A 1.414(2) C54A C55 1.416(2) C55 C56 1.354(3) C55 H55 0.9300 C56 C57 1.394(3) C56 H56 0.9300 C57 C58 1.363(2) C57 H57 0.9300 C58 C58A 1.413(2) C58 H58 0.9300 loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C51 H51 O41 1_655 0.93 2.50 3.386(2) 160 no C12 H12 Cg1 3_666 0.93 2.96 3.4804(17) 117 no C53 H53 Cg2 3_666 0.93 2.78 3.6477(19) 155 no loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C5 N1 N2 C3 1.54(17) C11 N1 N2 C3 176.03(13) N1 N2 C3 C4 -1.31(18) N1 N2 C3 C31 179.93(15) N2 C3 C4 C5 0.64(19) C31 C3 C4 C5 179.27(17) N2 C3 C4 C41 -176.73(16) C31 C3 C4 C41 1.9(3) N2 N1 C5 O51 173.68(13) C11 N1 C5 O51 -0.1(2) N2 N1 C5 C4 -1.17(18) C11 N1 C5 C4 -174.96(14) C3 C4 C5 N1 0.34(17) C41 C4 C5 N1 177.71(16) C3 C4 C5 O51 -173.21(17) C41 C4 C5 O51 4.2(3) C5 N1 C11 C16 131.39(17) N2 N1 C11 C16 -42.0(2) C5 N1 C11 C12 -50.3(2) N2 N1 C11 C12 136.31(15) C16 C11 C12 C13 -0.5(2) N1 C11 C12 C13 -178.77(15) C11 C12 C13 C14 1.1(3) C12 C13 C14 C15 -0.7(3) C13 C14 C15 C16 -0.3(3) C14 C15 C16 C11 0.9(3) C12 C11 C16 C15 -0.4(3) N1 C11 C16 C15 177.84(16) C5 C4 C41 O41 175.77(19) C3 C4 C41 O41 -7.5(3) N1 C5 O51 C52 146.36(14) C4 C5 O51 C52 -40.5(3) C58A C51 C52 O51 174.26(13) C58A C51 C52 C53 -0.5(2) C5 O51 C52 C51 148.23(15) C5 O51 C52 C53 -37.0(2) C51 C52 C53 C54 -0.9(3) O51 C52 C53 C54 -175.35(16) C52 C53 C54 C54A 1.6(3) C53 C54 C54A C58A -0.9(3) C53 C54 C54A C55 177.24(18) C54 C54A C55 C56 -177.22(18) C58A C54A C55 C56 0.9(3) C54A C55 C56 C57 0.0(3) C55 C56 C57 C58 -1.2(3) C56 C57 C58 C58A 1.4(3) C52 C51 C58A C58 -176.80(16) C52 C51 C58A C54A 1.1(2) C57 C58 C58A C51 177.50(17) C57 C58 C58A C54A -0.5(3) C54 C54A C58A C51 -0.5(2) C55 C54A C58A C51 -178.71(15) C54 C54A C58A C58 177.54(16) C55 C54A C58A C58 -0.7(2) _cod_database_fobs_code 2021648