#------------------------------------------------------------------------------ #$Date: 2019-06-26 07:10:15 +0300 (Wed, 26 Jun 2019) $ #$Revision: 216559 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/16/2021687.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021687 loop_ _publ_author_name 'B\"ohme, Uwe' 'Schwarzer, Anke' 'G\"unther, Betty' _publ_section_title ; The heteroscorpionate ligand 2,2-bis(3,5-dimethylpyrazol-1-yl)-1,1-diphenylethanol and an easy preparation of its tungsten complex ; _journal_coeditor_code FN3307 _journal_issue 7 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229619008362 _journal_volume 75 _journal_year 2019 _chemical_formula_iupac '[W (C24 H25 N4 O1) Cl O2], C4 H8 O' _chemical_formula_moiety 'C24 H25 Cl N4 O3 W, C4 H8 O' _chemical_formula_sum 'C28 H33 Cl N4 O4 W' _chemical_formula_weight 708.88 _chemical_name_systematic 'cis-[2,2-Bis(3,5-dimethylpyrazolyl)-1,1-diphenylethanolato]chloridodioxidotungsten(VI) tetrahydrofuran monosolvate' _space_group_crystal_system monoclinic _space_group_IT_number 7 _space_group_name_Hall 'P -2yc' _space_group_name_H-M_alt 'P 1 c 1' _symmetry_space_group_name_Hall 'P -2yc' _symmetry_space_group_name_H-M 'P 1 c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_method SHELXL-2017/1 _cell_angle_alpha 90 _cell_angle_beta 93.222(5) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 9.3157(6) _cell_length_b 8.4063(3) _cell_length_c 17.4678(10) _cell_measurement_reflns_used 12354 _cell_measurement_temperature 153(2) _cell_measurement_theta_max 27.83 _cell_measurement_theta_min 2.69 _cell_volume 1365.75(13) _computing_cell_refinement ; X-AREA (Stoe & Cie, 2009) ; _computing_data_collection ; X-AREA (Stoe & Cie, 2009) ; _computing_data_reduction ; X-RED (Stoe & Cie, 2009) ; _computing_molecular_graphics ; ORTEP-3 (Farrugia, 2012) ; _computing_publication_material ; SHELXL2014 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick 2015) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 153 _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_measured_fraction_theta_full 0.991 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_device '2-circle goniometer' _diffrn_measurement_device_type 'Stoe IPDS 2T' _diffrn_measurement_method 'rotation method' _diffrn_radiation_monochromator 'plane graphite' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0194 _diffrn_reflns_av_unetI/netI 0.0183 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 12354 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.499 _diffrn_reflns_theta_min 3.111 _diffrn_source 'sealed X-ray tube, 12 x 0.4 mm long-fine focus' _diffrn_source_current 40 _diffrn_source_power 2.000 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 4.368 _exptl_absorpt_correction_T_max 0.6391 _exptl_absorpt_correction_T_min 0.3906 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details ; (X-RED; Stoe & Cie, 2009) ; _exptl_crystal_colour Colourless _exptl_crystal_density_diffrn 1.724 _exptl_crystal_description Prism _exptl_crystal_F_000 704 _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.180 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.937 _refine_diff_density_min -1.065 _refine_ls_abs_structure_details ; Refined as an inversion twin ; _refine_ls_abs_structure_Flack 0.489(10) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.083 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 348 _refine_ls_number_reflns 5165 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.083 _refine_ls_R_factor_all 0.0273 _refine_ls_R_factor_gt 0.0238 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0148P)^2^+4.1365P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0519 _refine_ls_wR_factor_ref 0.0545 _reflns_number_gt 4924 _reflns_number_total 5165 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file fn3307sup1.cif _cod_data_source_block 2 _cod_database_code 2021687 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.408 _shelx_estimated_absorpt_t_max 0.669 _shelx_hkl_file ; -8 -8 -1 88.81 7.79 0 -8 -7 -2 80.44 8.76 0 -8 -6 -6 198.41 7.76 0 -7 -5 -2 636.20 9.16 0 -7 -4 -12 155.12 7.87 0 -7 -4 -11 216.70 8.15 0 -7 -4 -10 440.67 8.75 0 -7 -4 -9 348.94 8.45 0 -7 -4 -8 403.57 8.35 0 -7 -4 -7 522.00 8.72 0 -7 -4 -6 268.95 8.74 0 -6 -8 6 19.83 9.88 0 -6 -7 5 275.98 10.32 0 -6 -6 4 779.79 11.93 0 -6 -3 -14 4.56 7.70 0 -6 -3 -5 1263.34 10.73 0 -5 -3 -19 384.15 9.71 0 -5 -2 -14 196.43 7.99 0 -5 -2 -5 2140.92 12.60 0 -4 -6 8 924.73 18.84 0 -4 -2 -19 229.54 9.55 0 -4 -1 -13 410.99 9.96 0 -4 -1 -12 1232.11 10.88 0 -4 -1 -7 300.67 8.63 0 -4 -1 -6 2281.41 14.00 0 -3 -1 -18 454.09 9.97 0 -2 -2 4 280.28 19.46 0 -2 0 -15 -17.00 8.82 0 -1 -8 12 15.89 14.58 0 -1 0 -18 1696.68 14.07 0 1 -6 12 829.04 15.43 0 1 -5 11 561.11 15.35 0 2 -7 13 109.53 11.04 0 2 -2 7 4242.44 21.85 0 2 1 -18 812.34 18.44 0 3 -3 9 1444.46 14.40 0 3 -1 5 1489.54 14.32 0 3 1 -19 280.71 19.68 0 4 -3 9 1234.21 13.66 0 5 -7 13 40.95 10.67 0 5 -3 9 847.74 11.25 0 5 -1 5 235.38 9.16 0 5 0 2 1838.23 13.25 0 6 -6 12 367.50 10.89 0 6 -2 7 925.74 11.24 0 8 1 -13 189.96 12.25 0 9 0 -2 1090.78 10.78 0 10 0 -5 2.03 8.88 0 -8 -8 0 22.58 8.73 0 -8 -7 -1 116.00 8.90 0 -8 -6 -4 593.95 9.06 0 -7 -6 1 41.08 8.75 0 -7 -5 -1 91.25 8.66 0 -7 -4 -14 269.40 8.41 0 -7 -4 -13 314.48 8.43 0 -7 -4 -5 163.80 7.62 0 -6 -4 0 951.35 10.46 0 -6 -3 -16 -5.40 9.07 0 -6 -3 -4 373.71 9.01 0 -5 -4 3 1030.49 12.38 0 -5 -2 -16 8.38 8.84 0 -5 -2 -4 334.68 8.87 0 -4 -7 9 352.54 18.01 0 -4 -3 3 4040.01 20.81 0 -4 -2 -20 70.40 8.88 0 -4 -2 0 1401.76 13.31 0 -4 -1 -15 397.59 9.83 0 -4 -1 -14 976.54 10.13 0 -4 -1 -5 396.06 10.41 0 -2 -1 -21 167.18 9.47 0 -2 0 -16 1319.40 12.45 0 -2 0 -4 2857.64 19.54 0 -1 0 -19 -11.44 10.34 0 0 -7 12 404.88 15.89 0 0 1 -14 1665.86 17.00 0 1 -8 13 272.11 13.98 0 1 0 -22 815.00 15.90 0 3 0 2 2854.77 18.01 0 4 -7 13 158.04 10.77 0 4 -2 7 2770.58 16.12 0 4 -1 5 407.34 9.72 0 4 0 2 2694.97 15.72 0 5 -6 12 479.58 11.47 0 5 -4 10 232.91 10.19 0 5 -2 7 1502.47 12.53 0 5 1 -3 927.37 13.36 0 6 -5 11 48.86 8.55 0 6 0 1 15.51 9.27 0 7 0 0 1321.98 12.68 0 8 0 -1 -3.86 8.37 0 8 1 -10 231.67 10.87 0 9 0 -3 -15.89 8.04 0 10 0 -7 12.34 9.14 0 10 0 -6 715.45 10.21 0 11 -1 -3 82.69 8.13 0 -8 -8 1 100.82 9.71 0 -8 -6 -3 50.64 7.59 0 -8 -5 -12 294.50 8.23 0 -8 -5 -10 306.17 8.42 0 -8 -5 -7 26.14 7.44 0 -8 -5 -6 386.65 9.26 0 -7 -8 4 -14.72 9.51 0 -7 -7 3 247.70 9.39 0 -6 -5 3 396.24 10.93 0 -6 -3 -3 1456.28 11.35 0 -5 -3 1 2069.71 14.30 0 -5 -2 -17 441.37 9.99 0 -5 -2 -3 2195.84 12.95 0 -4 -5 7 103.69 14.51 0 -4 -1 -16 244.20 9.08 0 -3 -3 5 2474.24 23.01 0 -3 -1 -19 227.70 9.29 0 -3 -1 -1 641.93 13.30 0 -3 0 -12 2440.91 14.37 0 -3 0 -11 -0.65 9.22 0 -3 0 -10 1360.87 12.44 0 -3 0 -9 7.44 9.00 0 -2 -1 1 4208.47 27.82 0 -2 0 -17 -6.97 8.85 0 0 0 -21 9.26 10.58 0 0 1 -15 178.78 12.89 0 2 -6 12 893.62 14.72 0 3 -4 10 257.81 12.31 0 3 -2 7 2266.04 15.10 0 3 1 -3 3136.46 23.48 0 4 -6 12 432.47 12.58 0 4 -4 10 238.94 10.68 0 4 1 -3 820.96 13.48 0 5 -5 11 60.24 9.53 0 6 -3 8 9.65 8.25 0 7 -6 11 -0.45 8.51 0 7 1 -15 116.96 13.87 0 7 1 -7 354.23 12.35 0 8 0 -2 825.98 11.80 0 9 0 -4 228.81 9.70 0 10 0 -9 12.96 9.82 0 10 0 -8 257.51 9.95 0 11 -1 -4 138.73 8.40 0 -8 -7 0 138.88 8.97 0 -8 -6 -2 202.28 7.97 0 -8 -5 -5 74.99 7.35 0 -7 -6 2 787.36 11.13 0 -7 -5 0 396.97 8.46 0 -7 -4 -3 673.46 9.25 0 -6 -4 1 378.06 10.07 0 -6 -3 -2 56.56 9.42 0 -6 -2 -11 305.07 9.14 0 -6 -2 -10 135.16 9.03 0 -6 -2 -9 1028.03 11.14 0 -5 -2 -18 84.95 9.14 0 -4 -1 -17 486.97 9.92 0 -4 -1 -4 691.76 10.08 0 -3 -4 7 818.65 23.24 0 -3 -1 -20 342.02 9.79 0 -3 0 -13 -23.43 9.50 0 -3 0 -8 1034.55 11.04 0 -2 -1 -22 253.89 10.03 0 -1 0 -20 835.44 13.04 0 0 1 -16 694.55 14.32 0 2 -8 13 139.91 11.77 0 2 1 -19 475.84 17.41 0 3 -5 11 136.28 11.42 0 4 -5 11 53.55 10.23 0 5 -3 8 9.31 9.94 0 5 -1 4 1938.45 13.05 0 5 0 1 13.86 8.79 0 5 1 -4 1712.53 15.32 0 6 1 -5 634.05 12.12 0 7 0 -1 -5.35 9.88 0 7 1 -14 582.47 15.51 0 7 1 -8 535.02 12.59 0 9 0 -5 16.28 8.92 0 10 0 -13 -4.02 9.66 0 10 0 -12 532.94 12.12 0 10 0 -11 -11.52 9.36 0 10 0 -10 352.14 10.35 0 11 -1 -6 259.48 9.97 0 11 -1 -5 28.08 8.01 0 -8 -8 2 57.59 9.39 0 -8 -7 1 169.28 9.55 0 -8 -6 -1 16.36 8.50 0 -8 -5 -4 233.12 7.56 0 -7 -4 -2 281.81 8.42 0 -7 -3 -13 311.10 8.49 0 -7 -3 -12 5.60 7.47 0 -7 -3 -11 524.73 8.84 0 -7 -3 -10 43.69 7.49 0 -7 -3 -9 1206.49 10.30 0 -7 -3 -8 2.66 7.39 0 -7 -3 -7 481.59 9.67 0 -6 -2 -14 131.83 8.82 0 -6 -2 -13 464.84 8.86 0 -6 -2 -12 128.69 8.05 0 -6 -2 -8 267.50 8.74 0 -6 -2 -7 918.60 10.05 0 -5 -2 -2 1125.84 10.87 0 -5 -1 -11 263.07 9.51 0 -4 -2 1 1670.45 14.11 0 -3 0 -15 -9.98 8.55 0 -3 0 -14 2221.47 13.10 0 -3 0 -7 6.38 8.03 0 -2 0 -18 1335.84 12.78 0 -1 -9 12 15.70 16.46 0 -1 1 -12 1847.74 16.56 0 -1 1 -11 450.01 12.72 0 0 -4 9 1344.29 19.64 0 0 0 -22 709.16 14.55 0 1 1 -18 545.68 15.01 0 4 0 1 -6.61 10.56 0 5 -7 12 159.66 10.73 0 5 -2 6 431.54 10.99 0 6 -6 11 2.92 8.17 0 6 0 0 1340.90 11.73 0 6 1 -16 506.71 18.86 0 6 1 -6 726.29 13.58 0 7 1 -13 204.87 13.18 0 7 1 -12 633.82 14.74 0 7 1 -10 416.27 13.12 0 8 0 -3 2.39 9.49 0 9 0 -6 944.01 11.85 0 10 -1 -3 54.96 7.87 0 11 -1 -7 159.50 9.87 0 -9 -6 -7 25.01 7.69 0 -9 -6 -6 140.92 9.18 0 -8 -6 0 509.01 9.67 0 -8 -5 -3 202.35 7.70 0 -8 -4 -13 109.76 8.97 0 -8 -4 -10 131.41 7.85 0 -8 -4 -9 311.81 8.08 0 -8 -4 -8 191.34 7.88 0 -8 -4 -7 382.00 9.41 0 -7 -8 5 379.14 11.66 0 -7 -7 4 217.70 10.19 0 -7 -6 3 61.27 9.70 0 -7 -5 1 122.46 8.61 0 -7 -4 -1 263.58 9.03 0 -7 -3 -15 208.66 8.26 0 -7 -3 -14 6.37 7.45 0 -7 -3 -6 30.14 7.56 0 -6 -4 2 251.29 10.82 0 -6 -3 -1 1546.73 11.69 0 -6 -2 -6 214.77 8.59 0 -5 -6 7 36.89 11.41 0 -5 -4 4 443.12 11.78 0 -5 -1 -14 473.45 9.74 0 -5 -1 -13 419.57 8.55 0 -5 -1 -12 699.44 9.51 0 -5 -1 -9 342.32 8.85 0 -5 -1 -8 1074.27 10.58 0 -4 -1 -18 348.94 8.59 0 -4 -1 -3 685.70 10.02 0 -3 -1 -21 186.79 9.39 0 -3 0 -16 1021.00 11.75 0 -3 0 -6 2163.77 13.86 0 -2 -8 11 355.47 21.97 0 -2 0 -19 -15.58 8.72 0 -2 0 -3 3.01 12.08 0 -1 0 -21 0.88 10.33 0 -1 1 -14 2119.08 17.22 0 -1 1 -13 355.85 12.43 0 -1 1 -9 788.59 13.44 0 0 -6 11 56.76 13.32 0 0 1 -17 671.24 14.21 0 1 -7 12 330.46 12.78 0 2 -1 4 1752.33 17.55 0 2 0 1 10.93 13.08 0 3 -3 8 159.56 10.76 0 3 -1 4 854.16 13.17 0 3 0 1 2.60 12.55 0 4 -7 12 221.97 11.73 0 4 -3 8 137.89 9.25 0 4 -1 4 689.86 10.74 0 4 1 -4 1294.14 15.90 0 5 -6 11 35.46 9.40 0 5 -4 9 781.21 11.92 0 5 1 -17 131.46 21.04 0 5 1 -5 2020.98 17.12 0 6 -3 7 1254.93 11.85 0 7 -6 10 193.21 8.66 0 7 0 -2 763.67 11.79 0 7 1 -11 406.08 12.83 0 8 0 -4 766.23 11.37 0 9 0 -7 -10.57 9.50 0 10 -1 -4 200.61 9.70 0 11 -1 -9 48.85 9.57 0 11 -1 -8 147.34 9.37 0 -9 -7 -2 25.40 8.68 0 -9 -6 -5 8.99 7.52 0 -9 -6 -4 124.27 8.38 0 -8 -8 3 185.01 10.29 0 -8 -7 2 102.25 9.64 0 -8 -5 -2 378.87 9.34 0 -8 -4 -6 92.10 7.23 0 -7 -3 -16 27.07 7.89 0 -7 -3 -5 704.41 9.46 0 -7 -3 -4 154.33 9.21 0 -6 -2 -17 370.38 9.47 0 -6 -2 -16 6.77 7.45 0 -5 -3 2 76.38 9.52 0 -5 -2 -1 2135.77 13.11 0 -5 -1 -15 191.95 7.94 0 -5 -1 -7 342.02 8.84 0 -5 -1 -6 1285.34 11.78 0 -4 -3 4 213.90 11.66 0 -3 -8 11 -0.01 5.06 0 -3 -2 3 2214.65 19.54 0 -3 -1 0 3436.85 20.55 0 -3 0 -17 -14.77 9.05 0 -3 0 -5 -14.54 9.93 0 -1 1 -15 987.92 14.17 0 -1 1 -8 3086.10 19.89 0 0 -5 10 1217.32 19.53 0 2 -7 12 514.26 12.69 0 2 1 -4 3744.90 36.00 0 3 1 -20 512.15 22.66 0 3 1 -4 2709.26 23.56 0 4 -2 6 154.46 8.95 0 5 -5 10 393.15 9.45 0 5 0 0 4327.44 18.12 0 6 -2 5 2042.38 13.24 0 6 0 -1 -0.00 9.68 0 6 1 -7 1119.59 14.74 0 7 -3 6 27.83 8.27 0 9 -1 -2 607.71 10.76 0 9 0 -15 13.14 11.43 0 9 0 -8 797.26 11.58 0 10 -1 -5 62.16 9.30 0 -9 -7 -1 121.53 8.77 0 -9 -6 -3 25.18 8.21 0 -9 -5 -10 185.28 8.07 0 -9 -5 -8 174.65 7.86 0 -9 -5 -7 29.96 8.46 0 -8 -6 1 18.08 8.37 0 -8 -5 -1 69.28 8.61 0 -8 -4 -5 274.65 7.96 0 -7 -5 2 566.33 9.81 0 -7 -4 0 347.76 9.58 0 -6 -3 0 20.14 9.52 0 -6 -2 -4 170.11 8.95 0 -5 -1 -16 309.96 8.10 0 -5 -1 -5 236.19 9.51 0 -4 -4 6 733.86 16.07 0 -4 -1 -2 1732.09 12.83 0 -4 0 -12 2685.56 14.88 0 -4 0 -11 -9.57 9.25 0 -4 0 -10 905.82 11.41 0 -3 0 -18 750.36 11.84 0 -2 0 -20 641.99 11.12 0 -1 0 -22 552.22 12.62 0 -1 1 -16 930.49 13.91 0 0 -8 12 66.42 13.20 0 0 1 -18 630.69 14.12 0 1 -4 9 1160.24 16.87 0 2 -2 6 310.94 11.59 0 2 1 -20 583.32 17.89 0 3 -2 6 852.63 11.53 0 4 -8 12 1.79 10.51 0 4 -6 11 -23.64 9.93 0 4 -5 10 631.18 11.65 0 4 -4 9 799.69 11.22 0 5 -3 7 961.00 12.17 0 5 -1 3 1073.67 11.37 0 5 1 -6 1506.97 16.75 0 6 -4 8 440.23 9.39 0 6 1 -15 223.38 15.75 0 6 1 -8 919.84 14.30 0 7 0 -3 5.38 9.87 0 8 0 -5 2.28 9.47 0 9 0 -14 475.00 12.68 0 9 0 -13 -10.87 11.09 0 9 0 -12 685.13 13.21 0 9 0 -11 9.70 10.25 0 9 0 -10 370.09 11.09 0 9 0 -9 -3.14 9.11 0 10 -1 -6 236.04 9.71 0 11 -2 -4 89.54 8.18 0 -9 -6 -2 224.97 8.77 0 -9 -5 -6 252.84 7.86 0 -9 -5 -5 58.13 8.02 0 -8 -3 -11 335.47 8.96 0 -8 -3 -10 -19.85 8.11 0 -7 -3 -3 919.15 10.04 0 -7 -2 -12 49.47 8.50 0 -7 -2 -11 470.56 9.61 0 -7 -2 -10 111.19 8.75 0 -7 -2 -9 689.28 9.90 0 -6 -2 -3 2101.70 13.44 0 -5 -1 -18 303.98 9.02 0 -4 0 -14 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625.64 9.74 0 4 -5 -11 202.26 7.86 0 4 -4 -18 179.88 8.66 0 4 -4 -17 338.73 8.98 0 4 -4 -12 835.18 10.32 0 -9 -5 11 2.26 18.48 0 -9 6 -4 120.67 8.35 0 -8 -2 10 165.57 12.09 0 -8 2 6 35.59 8.43 0 -7 -1 9 332.51 12.43 0 -7 1 7 367.64 11.18 0 -7 3 4 171.95 9.18 0 -7 6 -5 -9.77 8.19 0 -6 6 -6 814.19 10.01 0 -5 0 7 -12.15 11.49 0 -5 6 -8 732.82 9.83 0 -4 -8 7 829.40 13.90 0 -4 -5 8 1050.97 23.65 0 -4 -1 7 626.85 13.66 0 -4 4 -1 1188.30 10.98 0 -4 6 -11 3.53 8.72 0 -4 6 -10 471.31 11.25 0 -3 -8 6 26.66 9.84 0 -3 -1 6 2785.02 23.97 0 -3 0 5 2.50 11.15 0 -2 5 -10 1285.77 13.89 0 -1 -7 4 688.56 11.77 0 -1 4 -8 532.23 12.25 0 0 -10 -1 102.14 8.52 0 0 3 -7 2420.39 21.65 0 1 -7 0 1215.94 11.68 0 2 -9 -5 503.59 8.39 0 2 -8 -4 87.03 8.44 0 2 -6 -2 952.62 10.02 0 2 -4 -2 1520.64 12.28 0 3 -9 -11 485.95 8.13 0 3 -8 -8 22.80 7.24 0 3 -7 -7 442.00 9.02 0 3 -6 -6 338.21 9.44 0 3 -1 -10 1242.16 13.12 0 4 -5 -16 608.26 9.76 0 4 -5 -15 81.27 8.68 0 4 -5 -14 1033.56 10.37 0 4 -5 -13 254.25 8.02 0 4 -4 -16 284.59 8.79 0 4 -4 -15 592.57 9.53 0 4 -4 -14 430.88 9.16 0 -10 0 9 -16.42 9.85 0 -9 -4 11 224.31 16.09 0 -9 0 9 -7.22 11.07 0 -9 1 8 232.62 10.62 0 -7 2 6 156.89 10.51 0 -7 6 -4 647.20 9.76 0 -6 6 -5 80.95 9.30 0 -5 -1 8 1416.42 16.44 0 -5 1 6 1480.92 13.84 0 -5 3 3 1610.34 13.09 0 -5 6 -7 4.46 8.12 0 -4 1 5 1181.13 13.27 0 -4 5 -4 722.49 10.33 0 -4 6 -9 128.91 9.33 0 -3 -5 7 87.79 14.38 0 -3 -4 7 816.70 22.17 0 -3 5 -6 1153.40 12.28 0 -2 5 -9 360.82 11.46 0 -1 -10 1 177.85 8.29 0 0 -9 0 266.58 9.01 0 1 -10 -4 240.09 7.44 0 2 -5 -2 1466.39 10.77 0 3 -8 -10 51.55 8.38 0 3 -8 -9 712.17 8.42 0 3 -7 -8 397.66 9.00 0 3 -5 -6 1583.81 10.98 0 3 -4 -6 1426.72 10.77 0 3 -3 -7 2869.53 14.05 0 3 -2 -21 674.73 11.28 0 3 -2 -8 740.17 10.74 0 3 -1 -19 285.74 10.37 0 3 -1 -11 504.05 11.47 0 -10 -3 11 220.06 13.87 0 -10 -1 10 151.08 11.56 0 -9 -1 10 278.47 12.24 0 -8 0 9 27.60 10.90 0 -8 1 8 588.25 11.38 0 -8 3 5 343.58 9.18 0 -7 7 -10 133.52 9.56 0 -6 0 8 1169.51 14.65 0 -6 1 7 1127.78 13.14 0 -6 7 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19.02 9.83 0 -3 6 -12 798.89 11.95 0 -2 3 -1 3077.52 16.11 0 -2 5 -8 1041.68 12.77 0 -1 -10 0 246.42 8.75 0 -1 -3 4 37.09 12.83 0 -1 2 -1 7067.32 27.59 0 0 -6 2 1085.16 11.85 0 0 4 -16 415.05 20.61 0 0 4 -15 541.49 20.03 0 0 4 -14 517.36 17.78 0 1 -8 -2 56.51 7.45 0 1 -5 0 3162.98 15.00 0 1 -3 0 438.33 10.28 0 2 -9 -8 50.85 6.89 0 2 -8 -6 82.00 8.40 0 2 -7 -4 750.04 9.25 0 2 -5 -3 41.39 8.77 0 2 -3 -3 5514.33 18.42 0 2 -1 -5 948.61 13.13 0 2 1 -17 329.50 14.32 0 3 -7 -10 584.51 8.26 0 3 -6 -8 1297.26 9.99 0 3 -4 -7 832.96 9.59 0 3 -3 -21 650.57 10.99 0 3 -3 -8 255.42 9.49 0 3 -2 -20 195.01 9.82 0 3 -2 -9 2337.49 13.93 0 3 -1 -16 1429.67 13.20 0 3 -1 -15 132.28 10.72 0 3 -1 -14 1245.32 13.21 0 3 -1 -13 226.46 10.68 0 -10 -2 11 141.07 11.72 0 -9 3 6 9.86 8.00 0 -8 -4 11 305.09 16.13 0 -8 -1 10 205.05 11.93 0 -8 7 -6 73.68 8.35 0 -7 1 8 512.26 11.16 0 -7 6 -2 577.85 9.29 0 -7 7 -7 104.23 9.46 0 -6 2 6 267.57 9.61 0 -6 6 -3 147.33 9.89 0 -6 7 -9 180.14 9.48 0 -5 -7 8 407.59 14.82 0 -5 7 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1205.53 10.26 0 4 -7 -6 526.34 9.34 0 4 -6 -1 75.65 9.83 0 4 5 8 797.28 9.17 0 5 -8 -11 441.93 9.05 0 5 -8 -10 32.46 7.88 0 5 -6 1 78.14 10.11 0 5 0 9 11.96 8.44 0 5 5 9 102.70 7.41 0 6 -8 -6 5.87 8.35 0 6 5 10 303.39 8.30 0 7 -8 -3 294.05 10.83 0 7 -2 9 677.33 14.47 0 7 2 11 437.97 9.81 0 7 3 11 469.79 9.90 0 7 4 11 258.04 8.14 0 7 6 10 180.76 8.46 0 8 -8 -2 19.81 9.45 0 8 5 11 -4.82 8.12 0 10 -3 9 83.03 14.40 0 10 -2 10 22.08 12.88 0 -1 -1 -17 671.02 9.32 0 -1 0 -19 4.24 8.22 0 -1 4 -20 353.47 12.47 0 0 -3 -17 1142.93 9.09 0 0 6 -2 1060.83 11.38 0 0 8 -12 74.01 12.28 0 0 8 -11 350.28 13.00 0 0 8 -10 33.27 10.69 0 1 -5 -14 1194.00 9.82 0 1 -5 -13 34.51 6.60 0 1 -5 -12 881.55 8.57 0 1 -5 -10 1018.60 9.12 0 1 -5 -9 237.92 8.38 0 1 -4 -4 1452.73 11.03 0 1 -3 -1 2356.64 16.38 0 1 4 3 3396.32 15.34 0 2 -6 -14 1023.23 8.97 0 2 -6 -13 102.46 6.82 0 2 -6 -12 1222.08 9.30 0 2 -6 -11 168.33 7.21 0 2 -6 -10 1407.26 9.83 0 2 -5 -20 652.78 8.36 0 2 -1 4 1761.78 22.68 0 2 10 -6 215.95 9.44 0 3 2 7 2237.93 13.48 0 3 3 7 1776.49 11.98 0 4 -7 -5 355.04 9.08 0 4 -5 2 1292.24 16.62 0 4 4 8 341.88 9.26 0 5 -8 -9 482.23 9.47 0 5 -7 -2 406.67 10.14 0 5 4 9 841.71 10.25 0 6 -8 -5 594.62 9.94 0 6 1 10 356.43 9.80 0 6 4 10 405.29 8.64 0 7 -7 1 187.76 11.26 0 8 -7 2 48.44 12.73 0 8 1 11 77.36 9.78 0 9 0 11 23.58 10.77 0 -1 -2 -14 645.95 9.46 0 -1 -2 -13 1427.64 10.13 0 -1 -2 -12 667.35 8.79 0 -1 -2 -11 3027.20 13.00 0 -1 -2 -10 774.36 8.94 0 -1 -1 -18 567.07 9.06 0 -1 -1 -6 5272.06 19.62 0 -1 2 -21 486.89 9.93 0 -1 5 -19 39.10 12.38 0 0 -4 -13 763.82 9.13 0 0 -4 -12 220.85 8.26 0 0 -3 -19 793.00 9.07 0 0 -3 -5 5875.02 18.90 0 0 -2 -21 440.73 8.82 0 0 4 0 3723.46 17.66 0 0 5 -1 6.27 9.30 0 0 7 -5 415.49 11.14 0 1 -5 -16 846.26 8.42 0 1 -5 -15 164.73 6.78 0 1 -5 -8 1420.14 10.05 0 1 -4 -20 246.00 7.54 0 1 5 2 3324.21 14.72 0 1 8 -3 1576.51 12.00 0 1 9 -8 25.75 9.53 0 1 9 -7 549.49 10.83 0 2 -6 -17 20.26 7.54 0 2 -6 -16 656.57 8.15 0 2 -6 -15 79.79 6.88 0 2 -6 -8 865.71 8.90 0 2 -5 -3 54.73 7.18 0 2 -4 0 1165.54 13.13 0 2 4 5 865.76 9.24 0 2 10 -7 77.88 9.34 0 3 -7 -14 258.56 7.24 0 3 -7 -13 305.26 7.38 0 3 -7 -12 456.39 7.78 0 3 -7 -10 570.88 8.08 0 3 -7 -9 291.41 8.35 0 3 -6 -3 47.63 8.30 0 3 -5 0 1555.23 14.09 0 3 5 6 1135.45 9.99 0 4 1 8 1813.21 13.31 0 4 3 8 141.60 8.86 0 5 -8 -7 686.65 10.00 0 5 1 9 361.03 10.05 0 5 3 9 833.43 10.59 0 6 -8 -4 16.90 9.09 0 6 -7 0 214.06 10.34 0 6 2 10 131.12 8.67 0 6 3 10 15.32 7.20 0 7 0 10 1200.47 15.31 0 8 -8 -1 71.32 10.15 0 8 2 11 338.83 9.71 0 8 3 11 348.13 9.69 0 -1 -2 -16 211.52 7.94 0 -1 -2 -15 915.65 8.93 0 -1 -2 -9 3850.06 14.59 0 -1 -2 -8 471.02 9.31 0 -1 -1 -19 220.65 7.99 0 -1 0 -20 852.52 9.60 0 -1 0 -4 2727.71 21.32 0 -1 1 -21 210.96 8.39 0 -1 3 -21 689.82 11.40 0 0 -4 -16 403.35 8.29 0 0 -4 -15 575.33 7.99 0 0 -4 -14 531.31 7.81 0 0 -4 -10 300.19 7.56 0 0 -4 -9 1233.85 9.67 0 0 -2 -22 54.85 8.06 0 0 6 -3 142.11 10.45 0 1 -5 -18 497.73 8.39 0 1 -5 -17 106.33 6.54 0 1 -5 -7 363.57 7.98 0 1 -4 -21 493.43 7.97 0 1 -4 -3 3163.93 15.32 0 1 1 3 2503.14 19.38 0 1 3 3 3771.74 17.00 0 1 9 -9 395.39 11.43 0 2 -6 -18 487.79 7.94 0 2 -6 -7 68.18 7.26 0 2 -3 2 265.29 14.79 0 2 1 5 893.26 12.17 0 2 3 5 3888.64 15.33 0 2 5 4 2967.95 13.16 0 2 6 3 52.14 7.38 0 2 9 -3 421.12 9.18 0 2 10 -8 154.77 9.70 0 3 -7 -8 402.97 7.78 0 4 -8 -13 259.29 8.43 0 4 -8 -12 25.26 7.80 0 4 -7 -4 719.73 9.98 0 4 2 8 220.33 8.34 0 4 5 7 225.63 8.26 0 5 -8 -6 7.56 8.24 0 5 2 9 996.90 10.51 0 5 5 8 847.13 9.74 0 6 -3 7 1247.46 21.65 0 6 -2 8 249.51 13.38 0 6 5 9 9.56 7.76 0 7 -8 -2 25.83 8.99 0 7 4 10 445.11 9.13 0 8 -4 7 428.22 19.08 0 8 5 10 292.46 8.97 0 9 1 11 120.63 10.72 0 9 2 11 161.83 9.35 0 10 1 11 5.99 11.92 0 -2 1 -13 234.18 9.71 0 -2 1 -12 1898.77 14.24 0 -2 2 -14 386.36 11.17 0 -2 2 -13 576.89 12.04 0 -2 2 -12 434.16 11.71 0 -2 2 -11 2629.27 18.18 0 -2 3 -12 11.79 12.23 0 -1 -2 -17 1022.85 9.04 0 -1 -1 -5 1020.10 13.13 0 0 -4 -17 601.57 7.92 0 0 -4 -8 999.25 9.09 0 0 7 -6 786.14 12.39 0 1 -5 -19 103.33 6.66 0 1 -2 1 7298.00 41.04 0 1 2 3 4999.18 21.29 0 1 8 -4 66.68 8.12 0 1 9 -10 12.16 10.17 0 2 -6 -6 1244.50 10.00 0 2 -5 -2 1364.28 11.90 0 2 2 5 4695.25 17.63 0 3 -7 -7 401.67 8.06 0 3 4 6 397.73 8.29 0 4 -8 -10 37.07 6.97 0 4 -6 0 1015.28 12.77 0 4 -2 6 152.51 12.98 0 5 -8 -5 605.62 9.80 0 5 -7 -1 410.92 10.41 0 5 6 7 43.97 7.54 0 6 -8 -3 444.66 10.73 0 6 -6 3 168.13 14.46 0 6 4 9 552.40 10.33 0 7 1 10 576.41 10.86 0 7 2 10 94.83 8.81 0 7 3 10 36.53 8.81 0 8 -2 9 249.58 12.68 0 8 6 9 13.17 8.20 0 9 5 10 153.83 9.02 0 -2 1 -15 523.21 10.19 0 -2 1 -14 986.37 11.60 0 -2 1 -11 598.40 11.12 0 -2 1 -10 3107.32 17.84 0 -2 2 -15 1036.50 12.13 0 -2 2 -10 705.67 13.67 0 -2 3 -14 47.04 11.38 0 -2 3 -13 1010.35 15.53 0 -2 3 -11 2243.30 21.78 0 -1 -3 -13 1404.73 10.74 0 -1 -3 -12 65.10 8.01 0 -1 -2 -18 30.16 6.65 0 -1 -2 -7 3634.35 14.98 0 -1 -1 -20 324.43 7.51 0 -1 1 -22 351.10 8.84 0 -1 1 -3 2410.57 37.19 0 -1 5 -7 240.77 15.00 0 0 -4 -18 331.61 7.30 0 0 -4 -7 2404.97 11.80 0 0 -3 -21 676.44 8.34 0 0 -3 -4 89.65 8.03 0 0 -2 -2 1302.43 14.70 0 0 3 0 261.06 11.78 0 1 -5 -20 492.34 7.91 0 1 4 2 1609.72 12.41 0 1 6 0 1567.51 11.99 0 1 7 -2 960.35 11.44 0 2 -6 -5 40.23 8.37 0 2 4 4 1391.54 11.47 0 2 9 -4 159.85 8.31 0 3 -7 -6 491.19 8.14 0 3 5 5 254.32 8.28 0 3 10 -5 128.76 9.25 0 4 -8 -8 28.32 8.08 0 4 4 7 615.54 9.00 0 5 -6 2 855.61 15.77 0 5 -3 6 22.27 17.10 0 5 -2 7 1482.10 18.31 0 5 4 8 253.20 8.42 0 6 0 9 -6.83 9.32 0 6 3 9 1258.42 11.77 0 7 -8 -1 165.08 10.09 0 8 -3 8 7.05 12.97 0 8 0 10 583.47 12.70 0 -2 0 -15 4.25 8.20 0 -2 0 -14 1828.17 12.44 0 -2 0 -13 -6.51 8.03 0 -2 0 -12 2217.11 13.50 0 -2 0 -11 -6.19 9.04 0 -2 1 -16 926.95 11.23 0 -2 2 -16 96.68 9.11 0 -2 2 -9 3014.26 21.64 0 -2 3 -15 1074.15 14.40 0 -2 3 -10 167.36 15.04 0 -1 -3 -16 8.85 7.77 0 -1 -3 -15 1457.03 9.89 0 -1 -3 -14 64.60 7.10 0 -1 -3 -11 941.74 9.09 0 -1 -3 -10 148.28 7.32 0 -1 -2 -19 502.90 7.72 0 -1 0 -22 549.93 9.33 0 -1 4 -5 2211.95 23.17 0 0 -4 -20 442.81 8.39 0 0 -4 -19 514.64 7.64 0 0 -4 -6 1173.82 10.66 0 0 5 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14.36 12.69 0 10 1 10 73.29 10.86 0 -2 -1 -17 635.69 9.25 0 -2 -1 -16 951.33 10.13 0 -2 -1 -11 610.42 9.05 0 -2 -1 -10 3115.44 14.77 0 -2 0 -19 10.32 8.22 0 -2 1 -19 350.55 9.48 0 -2 1 -8 2135.29 17.06 0 -2 2 -19 512.86 11.53 0 -2 2 -8 497.39 15.57 0 -2 3 -18 7.31 10.55 0 -2 4 -15 660.30 17.17 0 -2 4 -14 633.82 17.64 0 -1 -4 -16 493.68 8.81 0 -1 -4 -15 539.36 7.99 0 -1 -4 -12 340.48 7.80 0 -1 -4 -11 409.12 8.77 0 -1 -3 -7 3844.96 15.36 0 -1 -2 -22 53.02 7.17 0 -1 -2 -5 5459.67 20.03 0 0 -5 -20 520.07 8.59 0 0 -5 -19 77.27 6.83 0 0 -5 -8 1545.28 10.32 0 0 2 0 33.34 12.56 0 1 -6 -7 48.33 7.28 0 1 3 2 92.50 8.85 0 2 -7 -7 321.73 7.59 0 2 -6 -3 79.23 8.65 0 2 -4 1 1737.56 16.28 0 2 9 -7 417.46 10.43 0 3 -8 -8 34.22 7.92 0 3 5 4 1125.27 10.37 0 4 4 6 175.52 8.24 0 5 -9 -7 299.77 9.35 0 5 4 7 691.80 9.54 0 6 -9 -5 259.43 9.30 0 6 -8 -1 184.22 10.07 0 6 3 8 -9.82 9.15 0 6 5 7 113.26 8.46 0 7 -8 0 10.04 10.24 0 7 -2 8 139.99 12.07 0 7 1 9 348.29 9.86 0 7 2 9 692.38 9.74 0 8 3 9 437.06 10.62 0 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9 -9 295.90 9.96 0 3 -6 0 999.92 12.69 0 3 2 5 4478.05 17.67 0 3 4 4 928.70 9.76 0 3 9 -5 286.36 9.04 0 4 -9 -7 328.74 8.84 0 4 -8 -3 603.91 10.91 0 5 -9 -5 271.89 9.28 0 5 -7 1 355.77 12.21 0 5 4 6 313.09 10.05 0 6 -7 2 193.57 13.20 0 6 5 6 611.57 9.69 0 6 6 5 81.48 7.86 0 7 -3 7 529.27 16.12 0 8 -2 8 238.73 13.01 0 8 5 7 12.73 8.36 0 9 4 8 148.09 8.88 0 10 1 9 83.67 10.74 0 10 4 8 78.52 8.87 0 -2 -3 -17 996.01 10.05 0 -2 -3 -16 22.42 6.82 0 -2 -3 -15 1120.32 9.22 0 -2 -3 -14 37.32 6.99 0 -2 -3 -13 1053.77 9.56 0 -2 -3 -12 26.06 8.44 0 -2 -2 -20 84.61 8.06 0 -2 -2 -9 3072.78 14.19 0 -2 0 -22 661.77 10.20 0 -2 0 -7 2.46 8.46 0 -2 1 -7 861.18 14.04 0 -2 4 -18 321.55 14.22 0 -1 -5 -18 498.03 7.86 0 -1 -5 -17 74.43 6.92 0 -1 -5 -12 834.02 8.58 0 -1 -5 -11 557.51 9.10 0 -1 -2 -4 706.33 10.99 0 0 6 -6 1599.32 15.19 0 1 7 -5 377.71 10.34 0 2 -8 -8 21.53 7.59 0 2 3 3 3150.20 14.89 0 2 8 -5 920.81 10.96 0 2 9 -10 27.02 9.04 0 3 -9 -11 446.16 8.65 0 3 -9 -10 -2.30 8.39 0 3 -8 -5 866.79 10.47 0 3 -7 -2 505.67 9.74 0 3 1 5 1381.20 13.05 0 3 9 -6 95.25 8.93 0 4 2 6 163.41 8.12 0 4 4 5 342.54 8.73 0 4 5 4 756.82 9.80 0 5 0 7 2.94 9.14 0 5 1 7 370.35 10.54 0 5 5 5 663.94 9.73 0 6 -9 -3 245.75 10.16 0 6 -8 0 26.67 10.39 0 6 -2 7 956.24 17.86 0 7 2 8 139.07 9.60 0 7 4 7 522.97 11.02 0 8 3 8 5.92 8.25 0 9 -2 8 103.40 12.02 0 10 -2 8 47.18 12.30 0 -2 -3 -18 22.46 6.86 0 -2 -3 -11 2339.81 11.91 0 -2 3 -21 468.67 11.83 0 -1 -5 -19 23.54 7.06 0 -1 -5 -10 1225.35 9.73 0 -1 -4 -7 1548.76 10.58 0 -1 -3 -5 4591.95 16.60 0 -1 -1 -3 2546.16 19.73 0 -1 4 -6 996.30 19.32 0 0 -7 -15 278.58 8.11 0 0 -6 -8 1817.61 10.88 0 0 -5 -5 251.37 7.75 0 0 -4 -3 2128.82 12.80 0 0 5 -4 2459.60 17.01 0 0 7 -11 466.72 13.96 0 1 -8 -15 364.20 8.87 0 1 -8 -14 30.72 7.87 0 1 -7 -7 601.23 9.24 0 1 -6 -4 1006.99 10.64 0 1 -5 -2 894.26 9.81 0 1 1 2 5406.77 26.31 0 1 5 -1 343.16 9.16 0 1 6 -3 202.23 10.18 0 1 8 -10 16.39 10.00 0 2 -8 -7 590.95 9.16 0 2 -7 -4 717.58 9.88 0 2 4 2 1400.88 11.87 0 2 5 1 13.11 7.42 0 2 9 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20.00 0 4 3 5 1397.05 12.12 0 5 3 6 11.41 8.51 0 6 -9 -2 11.67 9.97 0 6 2 7 901.71 12.30 0 6 4 6 377.72 9.15 0 6 6 4 759.25 9.83 0 7 3 7 461.21 11.12 0 8 0 8 189.26 11.12 0 8 1 8 228.76 10.35 0 8 5 6 439.52 9.47 0 9 2 8 117.59 9.92 0 9 4 7 204.30 8.95 0 10 2 8 41.24 9.44 0 10 4 7 112.16 8.84 0 -2 -4 -13 638.43 8.33 0 -2 -4 -12 289.60 7.85 0 -2 -3 -9 2222.71 11.69 0 -2 2 -7 3832.62 29.93 0 -1 -6 -16 437.98 7.74 0 -1 -6 -15 16.39 6.77 0 -1 -6 -14 1089.93 9.09 0 -1 -6 -13 207.93 7.28 0 -1 -6 -12 789.70 9.20 0 -1 -5 -8 1711.29 10.78 0 -1 5 -9 513.84 18.86 0 0 -7 -11 488.83 7.71 0 0 -7 -10 345.60 8.57 0 0 -5 -4 2415.88 13.27 0 0 6 -7 93.45 11.57 0 0 7 -12 364.54 13.63 0 1 -8 -10 38.87 6.86 0 1 -6 -3 203.81 8.94 0 1 -4 0 1316.89 14.09 0 1 8 -12 16.89 10.59 0 2 -9 -12 23.38 7.18 0 2 -9 -11 360.44 8.91 0 2 -8 -6 72.91 8.19 0 2 -7 -3 516.61 9.64 0 2 2 3 3763.05 18.63 0 3 -9 -7 370.99 9.26 0 3 -7 -1 267.17 10.16 0 3 4 3 1358.31 10.80 0 3 5 2 1429.12 11.00 0 3 8 -4 46.14 8.51 0 3 9 -8 65.37 9.44 0 4 4 4 495.34 10.42 0 4 5 3 218.14 9.98 0 5 -9 -3 326.65 10.59 0 5 4 5 528.55 9.71 0 5 5 4 734.22 11.37 0 6 1 7 643.21 11.59 0 8 -3 7 385.60 14.69 0 8 3 7 371.29 10.75 0 9 0 8 360.38 12.16 0 9 1 8 170.62 9.92 0 10 0 8 132.49 10.69 0 10 1 8 155.70 9.64 0 -3 -1 -16 527.29 9.54 0 -3 -1 -15 251.98 8.63 0 -3 -1 -14 762.38 9.76 0 -3 0 -17 -2.42 8.91 0 -3 0 -16 1040.71 10.91 0 -3 0 -15 -2.45 7.76 0 -3 0 -14 2198.07 13.52 0 -3 0 -13 -16.37 9.38 0 -3 1 -16 530.41 10.55 0 -3 1 -15 243.56 9.62 0 -2 -4 -20 341.08 8.09 0 -2 -4 -11 850.41 9.09 0 -2 -3 -8 405.36 9.25 0 -2 -2 -7 3957.07 15.57 0 -2 0 -6 3105.70 18.12 0 -2 4 -20 310.32 13.70 0 -1 -6 -11 52.33 6.72 0 -1 -3 -4 188.82 8.47 0 0 -7 -9 762.21 9.45 0 0 -6 -6 1597.87 10.64 0 1 -8 -9 448.70 7.85 0 1 -7 -5 386.79 9.23 0 1 -3 1 4713.71 26.97 0 1 8 -13 219.44 12.08 0 2 -9 -10 22.36 6.98 0 2 8 -7 579.86 11.02 0 3 -8 -3 950.16 11.94 0 3 -6 1 115.53 11.88 0 4 -9 -4 102.61 9.27 0 4 9 -6 86.39 8.50 0 5 -2 6 361.09 14.01 0 5 2 6 387.45 9.73 0 6 0 7 8.08 9.63 0 7 -2 7 910.05 16.86 0 7 2 7 840.29 12.50 0 7 4 6 284.73 9.19 0 7 5 5 95.05 8.19 0 8 -8 2 9.55 18.80 0 9 -3 7 327.88 14.43 0 10 -3 7 305.52 13.91 0 -3 -2 -17 573.54 9.11 0 -3 -2 -16 57.83 7.91 0 -3 -2 -15 641.52 9.51 0 -3 -1 -19 232.41 8.33 0 -3 -1 -18 459.04 9.17 0 -3 -1 -13 648.24 10.18 0 -3 0 -19 -5.51 8.62 0 -3 0 -18 827.22 10.19 0 -3 0 -12 2361.13 14.82 0 -3 1 -18 462.94 10.39 0 -3 1 -17 603.96 10.86 0 -3 1 -14 732.87 11.34 0 -3 1 -13 663.27 12.52 0 -2 -5 -18 646.89 9.23 0 -2 -5 -17 64.71 7.94 0 -2 -5 -16 835.62 8.62 0 -2 -5 -15 96.32 7.01 0 -2 -5 -14 843.31 9.45 0 -2 -1 -6 2360.69 14.31 0 -2 1 -6 2363.81 20.82 0 -1 -6 -10 1320.95 9.63 0 -1 -5 -7 256.37 8.07 0 -1 -4 -5 2252.75 12.45 0 -1 -2 -3 4897.99 20.71 0 0 -8 -15 381.35 8.63 0 0 -8 -14 2.34 7.85 0 0 -7 -8 421.21 8.69 0 0 -4 -2 1775.71 13.26 0 0 -3 -1 6308.31 24.08 0 0 4 -3 2126.10 16.57 0 0 7 -17 185.62 17.27 0 0 7 -14 162.80 14.33 0 1 -8 -8 18.97 7.89 0 1 -5 -1 355.54 9.56 0 1 5 -2 922.20 11.15 0 1 6 -4 995.71 11.61 0 1 7 -7 577.29 11.31 0 1 8 -14 23.75 11.50 0 2 -9 -9 291.17 7.91 0 2 -8 -5 948.73 10.43 0 2 -5 1 23.95 10.09 0 2 -4 2 1388.10 18.12 0 2 5 0 1796.04 11.97 0 2 7 -4 727.52 10.48 0 3 -9 -6 101.72 8.30 0 3 2 4 623.31 10.03 0 3 6 0 996.50 10.42 0 3 8 -5 815.92 10.87 0 3 9 -9 425.66 9.78 0 4 -8 -1 878.75 12.89 0 4 2 5 2901.34 14.67 0 5 -8 0 61.14 10.00 0 6 -8 1 411.54 13.46 0 6 4 5 390.70 10.80 0 8 2 7 276.96 10.43 0 8 4 6 57.14 8.55 0 8 5 5 46.10 8.44 0 9 4 6 131.22 8.84 0 10 4 6 38.69 8.74 0 -3 -2 -19 374.72 8.83 0 -3 -2 -18 116.67 8.16 0 -3 -2 -14 162.61 7.44 0 -3 -2 -13 734.40 9.88 0 -3 -1 -20 370.51 8.89 0 -3 -1 -12 1743.51 12.42 0 -3 0 -20 738.36 10.11 0 -3 0 -11 8.30 9.36 0 -3 1 -20 388.38 10.54 0 -3 1 -19 241.99 9.49 0 -3 1 -12 1746.50 15.23 0 -3 2 -17 547.38 12.16 0 -3 2 -16 50.91 10.57 0 -3 2 -15 680.67 12.59 0 -2 -5 -19 -12.91 6.92 0 -2 -5 -13 45.73 7.11 0 -2 -5 -12 1151.49 9.47 0 -2 -4 -9 810.82 9.27 0 -2 -3 -7 2961.67 14.19 0 -2 -2 -6 297.73 9.62 0 -1 -7 -17 149.62 7.26 0 -1 -7 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9.33 0 -3 -2 -11 2440.67 13.41 0 -3 -1 -21 202.67 8.66 0 -3 -1 -11 554.98 10.24 0 -3 0 -21 -12.58 8.15 0 -3 1 -21 209.44 10.34 0 -3 2 -18 106.06 9.95 0 -3 2 -14 142.75 10.69 0 -2 -5 -11 200.29 7.48 0 -2 -4 -8 457.37 9.46 0 -1 -7 -13 142.53 7.06 0 -1 -7 -12 324.97 7.61 0 -1 -6 -8 1681.88 10.68 0 0 -8 -11 399.04 7.68 0 0 -7 -7 631.49 8.59 0 0 2 -1 7170.20 35.11 0 0 6 -8 1784.68 17.20 0 1 -9 -11 477.37 9.34 0 1 -6 -2 1183.56 11.67 0 1 2 1 7231.33 27.20 0 1 4 -1 1593.97 13.43 0 1 7 -8 400.33 11.54 0 2 -9 -7 440.24 9.31 0 2 -8 -4 57.67 8.61 0 2 -6 0 1580.14 14.53 0 2 1 3 2262.17 17.02 0 2 7 -5 429.90 9.58 0 2 8 -9 668.72 11.53 0 3 -8 -2 8.60 9.47 0 3 -7 0 931.01 13.23 0 3 3 3 2970.81 14.67 0 3 4 2 1491.37 12.41 0 3 8 -6 32.79 8.38 0 4 -9 -3 373.18 10.65 0 4 -2 5 2895.18 24.95 0 4 1 5 377.34 10.82 0 4 3 4 94.83 8.30 0 4 5 2 1334.98 11.43 0 4 9 -8 34.72 8.76 0 5 0 6 941.61 12.43 0 5 5 3 103.56 8.72 0 5 9 -6 98.87 9.05 0 6 2 6 190.24 9.90 0 7 4 5 172.02 8.88 0 7 5 4 393.13 9.54 0 8 1 7 191.53 10.51 0 8 3 6 11.80 9.70 0 9 -4 6 128.61 15.29 0 9 -2 7 268.19 12.29 0 9 1 7 156.55 10.12 0 10 -4 6 41.88 14.43 0 10 -2 7 94.89 11.47 0 10 1 7 17.43 9.10 0 11 0 7 -3.12 9.20 0 11 3 6 6.87 8.63 0 -3 -3 -20 3.43 7.98 0 -3 -3 -12 13.90 8.46 0 -3 -1 -10 1811.88 12.88 0 -3 0 -10 1359.73 13.23 0 -3 1 -11 548.15 11.76 0 -3 2 -20 82.50 9.87 0 -3 2 -19 381.09 11.11 0 -3 2 -13 707.83 13.52 0 -2 -6 -18 448.29 7.93 0 -2 -6 -16 439.96 7.72 0 -2 -6 -15 58.08 6.79 0 -2 -6 -14 747.36 9.33 0 -2 -6 -13 30.33 7.76 0 -2 -5 -10 1271.76 10.03 0 -1 -7 -11 534.91 7.94 0 -1 -6 -7 60.06 8.64 0 -1 -4 -4 2714.56 13.66 0 -1 -3 -3 3703.88 16.64 0 0 -8 -10 37.85 6.84 0 0 -7 -6 766.40 10.02 0 0 -6 -4 1547.94 11.88 0 0 3 -2 1148.96 15.84 0 1 -8 -6 140.48 8.26 0 1 3 0 447.30 11.54 0 1 6 -5 38.46 10.01 0 2 5 -1 123.41 9.43 0 3 -9 -4 112.84 9.12 0 3 1 4 863.38 12.52 0 3 6 -1 71.31 8.18 0 4 4 3 1186.01 11.03 0 6 3 5 1349.29 13.52 0 7 2 6 197.67 11.15 0 8 0 7 36.45 9.50 0 8 4 5 307.02 9.19 0 8 5 4 231.52 8.97 0 9 0 7 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1116.40 11.08 0 -3 -1 -9 504.95 10.08 0 -3 0 -9 1.21 9.38 0 -3 1 -10 1799.40 15.29 0 -3 2 -21 315.42 10.34 0 -3 2 -12 657.09 13.44 0 -2 -6 -11 69.87 7.38 0 -2 -5 -8 1032.96 9.69 0 -2 -2 -5 4676.73 17.73 0 -1 -8 -15 377.84 8.10 0 -1 -8 -13 308.11 8.92 0 -1 -7 -9 746.55 8.71 0 -1 -6 -6 1805.50 12.15 0 -1 -1 -2 5320.62 26.28 0 -1 5 -10 1186.23 22.78 0 0 -9 -12 36.37 8.30 0 0 -8 -8 13.44 6.81 0 0 -7 -5 437.80 9.37 0 0 -5 -2 2375.76 13.27 0 0 -4 -1 1689.21 13.76 0 0 6 -9 41.44 12.41 0 1 -9 -8 7.67 8.36 0 1 -8 -5 687.01 9.06 0 1 -5 0 3050.25 16.64 0 2 -7 -1 386.66 10.19 0 2 7 -6 374.95 9.63 0 2 8 -11 389.35 11.78 0 3 5 0 1630.61 12.65 0 3 7 -4 793.40 10.76 0 4 -9 -2 242.83 10.35 0 4 -8 0 147.60 10.67 0 4 5 1 172.19 9.98 0 4 9 -10 32.66 8.98 0 5 -9 -1 315.77 10.33 0 5 -8 1 257.48 11.92 0 5 3 4 196.96 10.79 0 5 5 2 1354.89 11.92 0 5 9 -8 24.53 9.28 0 6 -2 6 197.49 12.89 0 6 0 6 1243.78 14.11 0 7 -3 6 27.70 14.59 0 7 1 6 497.43 12.57 0 7 3 5 759.79 11.12 0 7 5 3 302.68 9.27 0 8 -5 5 52.61 18.38 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2050.40 15.65 0 8 1 6 394.30 11.69 0 8 3 5 825.12 11.25 0 8 4 4 196.62 8.72 0 9 -5 5 52.81 16.22 0 9 1 6 262.80 10.62 0 9 3 5 343.90 9.49 0 10 -3 6 18.87 12.09 0 10 1 6 59.59 9.70 0 10 4 4 86.48 8.60 0 11 -1 6 24.03 10.15 0 11 0 6 150.05 9.46 0 -3 -5 -13 88.89 7.29 0 -3 -5 -12 1535.36 11.26 0 -3 -4 -10 213.36 7.99 0 -3 -3 -9 1356.06 10.56 0 -3 -2 -8 900.66 10.63 0 -3 -1 -8 2147.13 13.89 0 -3 2 -11 2431.29 19.58 0 -3 3 -19 674.08 14.15 0 -3 3 -18 -11.29 10.66 0 -3 3 -15 744.21 15.62 0 -2 -7 -13 94.62 7.11 0 -2 -7 -12 511.05 8.30 0 -2 -6 -9 168.67 7.81 0 -2 -5 -7 375.48 8.45 0 -2 -3 -5 3732.22 15.27 0 -1 -8 -11 362.43 7.86 0 -1 -8 -10 118.06 8.00 0 -1 -7 -7 737.97 9.72 0 -1 -6 -5 136.28 8.99 0 -1 0 -2 6517.56 38.09 0 0 4 -4 976.51 14.44 0 1 -8 -4 84.38 8.70 0 1 -7 -2 966.46 11.27 0 1 7 -10 450.67 12.02 0 2 5 -2 1379.77 12.58 0 2 6 -4 949.75 11.51 0 2 7 -7 310.30 10.28 0 2 8 -12 29.65 10.25 0 3 -6 2 1647.23 18.56 0 3 3 2 439.03 10.84 0 3 4 1 916.34 10.69 0 4 -6 3 189.31 17.26 0 4 3 3 3141.58 15.27 0 4 4 2 698.81 10.10 0 5 1 5 266.78 9.76 0 6 5 2 934.68 11.05 0 7 0 6 1393.31 15.50 0 8 -3 6 28.11 12.39 0 9 -3 6 1.03 11.87 0 10 0 6 219.28 9.85 0 11 2 5 138.09 9.20 0 -4 -2 -19 226.42 8.58 0 -4 -2 -16 43.10 7.95 0 -4 -2 -15 774.98 10.03 0 -4 -1 -19 77.44 8.27 0 -4 -1 -18 351.02 9.28 0 -4 -1 -16 277.15 8.93 0 -4 -1 -15 397.82 9.37 0 -3 -6 -17 -14.19 7.18 0 -3 -6 -16 218.57 7.76 0 -3 -6 -15 13.62 6.96 0 -3 -4 -9 747.52 10.23 0 -3 -3 -8 168.38 8.81 0 -3 0 -8 1037.26 13.07 0 -3 1 -9 499.23 11.70 0 -3 3 -20 3.95 11.54 0 -2 -7 -11 635.04 8.82 0 -2 -6 -8 1619.30 10.74 0 -1 -8 -9 499.39 8.86 0 -1 -3 -2 75.42 9.30 0 0 -9 -9 452.05 8.34 0 0 -7 -4 573.99 8.78 0 0 -3 0 261.67 11.81 0 0 6 -10 1233.03 16.94 0 1 4 -2 1447.11 13.50 0 1 5 -4 2096.14 15.39 0 2 -10 -7 70.56 7.74 0 2 -9 -4 140.69 8.76 0 2 -6 1 105.58 11.98 0 3 -10 -5 132.15 9.11 0 3 -7 1 541.17 12.83 0 3 -5 3 220.89 15.55 0 4 -9 -1 323.57 11.53 0 4 -7 2 369.16 13.83 0 4 7 -4 740.53 10.96 0 4 8 -7 810.50 11.21 0 6 -8 2 14.04 13.97 0 6 3 4 420.92 10.32 0 6 4 3 1345.14 12.43 0 7 -2 6 184.21 11.81 0 7 2 5 995.20 12.46 0 7 5 2 646.27 10.18 0 8 0 6 683.74 12.49 0 8 2 5 460.81 11.48 0 9 -1 6 289.46 12.03 0 9 0 6 462.98 11.57 0 9 2 5 309.92 10.92 0 10 -1 6 85.18 9.43 0 10 2 5 300.12 9.76 0 -4 -3 -18 -10.21 7.05 0 -4 -3 -16 0.22 6.85 0 -4 -3 -15 725.73 9.86 0 -4 -2 -20 45.32 7.32 0 -4 -2 -14 169.60 7.58 0 -4 -2 -13 632.47 9.61 0 -4 -1 -20 309.88 9.01 0 -4 -1 -14 964.76 10.69 0 -4 0 -20 420.88 10.32 0 -4 0 -19 12.33 8.06 0 -4 0 -18 623.95 9.92 0 -4 0 -17 -8.49 8.12 0 -4 0 -16 1235.26 11.87 0 -4 0 -15 -0.70 9.19 0 -3 -6 -14 530.01 8.44 0 -3 -6 -13 27.80 7.25 0 -3 -5 -10 731.27 9.27 0 -2 -8 -14 7.91 8.28 0 -2 -5 -6 1300.09 10.60 0 -2 -2 -4 773.34 11.22 0 -2 -1 -4 1777.59 15.63 0 -2 1 -5 925.85 17.83 0 -1 -9 -12 -6.90 8.33 0 -1 -7 -6 737.03 9.12 0 -1 -5 -3 138.70 9.30 0 0 -9 -8 15.79 8.30 0 0 -6 -2 1071.20 11.64 0 0 -5 -1 11.64 9.24 0 1 -8 -3 1555.27 13.12 0 1 1 1 4560.23 26.37 0 2 -10 -6 215.30 9.35 0 2 -7 0 1024.25 13.38 0 2 -5 2 1901.81 18.52 0 2 -3 3 3188.75 43.52 0 3 -9 -2 90.56 9.91 0 3 5 -1 47.45 9.00 0 3 6 -3 58.14 9.31 0 3 8 -10 55.55 9.78 0 4 -10 -3 136.95 10.55 0 4 1 4 683.16 12.20 0 4 5 0 1611.45 12.22 0 5 -9 0 54.52 10.58 0 5 0 5 -12.31 10.07 0 5 2 4 351.65 11.38 0 5 4 2 768.66 11.99 0 6 1 5 479.29 12.91 0 7 3 4 185.84 9.84 0 7 4 3 736.01 10.58 0 8 -2 6 82.34 12.30 0 8 3 4 61.39 9.93 0 -4 -4 -19 452.28 9.48 0 -4 -4 -18 232.04 7.81 0 -4 -4 -17 288.24 7.90 0 -4 -4 -16 234.21 7.78 0 -4 -4 -15 420.93 9.16 0 -4 -3 -13 1174.58 10.86 0 -4 -2 -12 147.89 9.04 0 -4 -1 -13 403.48 9.33 0 -4 -1 -12 1228.32 12.48 0 -4 0 -14 1109.86 11.64 0 -4 1 -18 358.45 11.09 0 -4 1 -17 469.99 11.36 0 -3 -7 -16 295.88 8.74 0 -3 -6 -12 798.61 9.07 0 -3 -6 -11 118.20 8.29 0 -3 -5 -9 396.35 9.50 0 -3 -4 -8 363.30 8.58 0 -3 -3 -7 1702.80 12.11 0 -3 -2 -7 2152.74 12.79 0 -3 -1 -7 613.40 10.70 0 -3 2 -10 434.70 14.32 0 -3 3 -13 1125.08 19.29 0 -2 -8 -12 95.34 8.39 0 -2 -7 -9 452.64 8.17 0 -2 -6 -7 144.49 8.32 0 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-8 228.90 8.88 0 -2 -5 -5 473.89 9.15 0 -1 -9 -10 77.25 8.70 0 -1 -8 -7 492.15 9.39 0 -1 -7 -5 470.10 9.71 0 0 -4 0 3752.78 19.10 0 0 5 -7 473.24 13.59 0 1 -10 -7 138.73 9.13 0 1 -7 -1 609.48 11.03 0 1 -5 1 332.59 11.24 0 1 2 0 1502.32 18.26 0 1 7 -12 257.18 11.31 0 2 -10 -5 205.70 9.25 0 2 -8 -1 1148.09 12.23 0 2 1 2 3719.67 23.14 0 2 4 -1 826.22 10.57 0 3 1 3 716.73 12.07 0 3 4 0 778.13 11.41 0 3 8 -11 528.65 11.17 0 4 2 3 1737.10 14.64 0 4 4 1 1201.83 11.24 0 4 8 -9 518.14 10.48 0 5 -7 3 450.53 19.14 0 6 -9 1 194.54 14.75 0 6 2 4 171.10 11.94 0 6 4 2 668.43 11.17 0 7 5 1 131.80 8.31 0 8 1 5 244.99 10.62 0 9 1 5 71.26 9.03 0 10 0 5 7.01 8.76 0 11 -1 5 117.12 9.07 0 -4 -5 -15 17.11 7.33 0 -4 -5 -14 762.64 10.18 0 -4 -4 -12 756.71 9.29 0 -4 -3 -11 930.95 10.75 0 -4 -1 -11 714.55 10.92 0 -4 0 -12 2702.24 16.32 0 -4 1 -14 962.73 13.15 0 -3 -7 -13 309.03 7.84 0 -3 -7 -12 292.87 9.10 0 -3 -5 -8 925.27 9.85 0 -3 -4 -7 1215.73 10.38 0 -3 0 -7 3.38 10.33 0 -3 1 -8 2131.70 17.63 0 -2 -8 -10 91.40 7.53 0 -2 -6 -6 1871.89 11.62 0 -2 -4 -4 1353.08 11.19 0 -2 0 -4 2752.04 20.40 0 -1 -9 -9 644.74 10.09 0 0 -9 -6 50.56 8.53 0 0 -8 -4 27.78 8.75 0 0 6 -11 49.37 12.34 0 1 -9 -4 122.85 9.08 0 1 -8 -2 58.95 9.77 0 2 5 -3 58.76 8.16 0 3 -9 -1 394.23 11.76 0 3 6 -4 705.81 11.25 0 3 7 -7 412.40 10.06 0 4 -10 -2 70.65 10.33 0 4 3 2 502.01 10.38 0 4 6 -3 123.12 10.07 0 5 -8 2 30.02 13.35 0 6 0 5 21.83 11.21 0 6 3 3 1542.12 13.22 0 6 8 -7 515.61 10.15 0 7 2 4 227.53 11.94 0 7 4 2 295.00 9.55 0 8 2 4 117.41 10.66 0 9 -4 5 228.09 14.25 0 9 0 5 0.30 9.85 0 9 2 4 74.39 9.92 0 10 -3 5 144.91 12.05 0 10 -1 5 94.59 9.98 0 10 3 3 322.70 9.16 0 -4 -6 -16 220.09 8.79 0 -4 -5 -13 54.63 7.28 0 -4 -5 -12 808.21 9.88 0 -4 -4 -11 275.33 8.18 0 -4 -3 -10 21.94 9.12 0 -4 1 -13 387.91 11.82 0 -3 -7 -11 349.22 8.23 0 -3 -3 -6 262.65 8.18 0 -3 -2 -6 823.41 10.25 0 -3 3 -12 0.16 16.07 0 -2 -8 -9 534.20 9.76 0 -2 -7 -7 464.16 8.19 0 -1 -9 -8 53.77 8.12 0 -1 -7 -4 243.66 9.14 0 -1 -6 -3 409.81 9.23 0 -1 -5 -2 3350.48 15.95 0 -1 5 -11 555.17 18.89 0 0 -7 -2 607.56 10.68 0 0 -6 -1 117.83 9.70 0 0 3 -3 4493.50 25.73 0 1 -10 -6 224.33 9.43 0 1 4 -3 3284.46 18.81 0 1 5 -5 192.60 10.95 0 1 6 -8 916.77 13.39 0 2 -10 -4 75.48 8.78 0 2 -9 -2 16.51 9.81 0 2 2 1 3716.69 20.87 0 2 3 0 776.02 11.47 0 3 2 2 612.44 11.15 0 3 3 1 3330.11 16.16 0 3 5 -2 1451.69 11.80 0 3 8 -12 59.98 8.93 0 4 -9 0 12.93 10.49 0 4 0 4 351.91 11.74 0 4 5 -1 105.25 8.78 0 4 7 -6 500.04 10.74 0 4 8 -10 45.08 9.07 0 5 1 4 2016.83 14.85 0 5 4 1 818.96 12.42 0 5 7 -5 334.19 9.94 0 6 5 0 1494.03 12.48 0 7 -4 5 174.67 16.97 0 7 0 5 0.21 11.42 0 7 3 3 929.00 12.03 0 7 8 -7 275.20 9.17 0 8 -4 5 315.78 16.32 0 8 0 5 -2.94 10.04 0 8 3 3 505.45 10.11 0 -4 -6 -15 18.18 7.33 0 -4 -6 -14 530.71 8.44 0 -4 -5 -11 66.50 8.53 0 -4 -4 -10 203.44 9.28 0 -4 -1 -10 1061.42 11.84 0 -4 0 -11 2.24 9.03 0 -3 -8 -14 9.46 7.15 0 -3 -8 -13 313.11 8.77 0 -3 -7 -10 311.21 7.92 0 -3 -6 -8 1126.30 10.06 0 -3 -5 -7 460.54 8.83 0 -3 -4 -6 402.59 8.56 0 -3 -1 -6 1930.43 13.43 0 -2 -9 -12 68.73 7.81 0 -2 -6 -5 45.46 8.04 0 -2 -5 -4 2865.35 13.66 0 -2 -3 -3 3101.38 15.37 0 -2 -2 -3 3751.40 18.17 0 -1 -3 -1 4697.01 20.24 0 -1 -2 -1 7332.45 27.93 0 0 -9 -5 808.72 10.67 0 0 -5 0 3282.77 17.26 0 0 4 -5 1912.10 17.99 0 1 -3 2 96.32 15.80 0 1 -2 2 2758.76 39.52 0 1 7 -14 171.19 11.87 0 2 -7 1 211.83 12.53 0 2 6 -6 1211.04 12.78 0 2 7 -10 408.90 11.15 0 3 7 -8 379.45 11.19 0 3 8 -13 243.47 10.69 0 4 8 -11 465.23 11.79 0 5 2 3 2385.93 15.99 0 5 3 2 335.39 11.40 0 5 8 -9 502.21 10.52 0 6 8 -8 16.99 8.23 0 7 8 -8 -0.30 9.87 0 9 -3 5 338.61 13.19 0 9 -1 5 87.44 9.86 0 -5 -3 -19 377.01 9.20 0 -5 -3 -18 25.00 8.30 0 -5 -3 -17 473.18 9.35 0 -5 -2 -19 291.83 8.90 0 -5 -2 -18 114.82 8.55 0 -5 -2 -17 421.33 9.23 0 -4 -6 -13 56.12 7.25 0 -4 -6 -12 475.34 9.32 0 -4 -3 -9 1242.30 10.51 0 -4 -2 -9 1688.55 11.88 0 -4 1 -12 1201.48 14.63 0 -4 2 -20 57.45 10.85 0 -4 2 -19 237.52 10.73 0 -4 2 -18 139.95 10.53 0 -4 2 -17 463.31 12.55 0 -4 2 -16 43.67 10.59 0 -3 -8 -12 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2 53.58 10.01 0 6 5 -1 62.18 9.14 0 6 7 -6 391.73 10.74 0 6 8 -10 9.95 9.63 0 7 -3 5 790.59 18.72 0 7 2 3 1253.87 14.70 0 7 3 2 -23.17 10.90 0 8 2 3 749.34 12.86 0 8 3 2 -8.95 8.61 0 9 2 3 290.90 9.52 0 9 3 2 30.16 8.41 0 10 0 4 397.19 10.38 0 -5 -5 -17 30.62 7.57 0 -5 -5 -16 380.43 9.36 0 -5 -5 -15 25.60 8.17 0 -5 -4 -15 403.19 8.45 0 -5 -3 -14 5.48 7.31 0 -5 -3 -13 484.30 9.79 0 -5 -2 -14 198.82 8.98 0 -5 -1 -16 317.30 9.29 0 -5 -1 -15 195.21 9.20 0 -4 -7 -13 183.10 7.91 0 -4 -7 -12 210.13 8.72 0 -4 -6 -10 458.96 9.49 0 -4 -5 -9 12.56 7.50 0 -4 -4 -8 324.12 9.92 0 -4 -3 -8 120.22 8.34 0 -4 -2 -8 210.93 9.90 0 -3 -4 -5 858.32 9.78 0 -3 0 -6 2161.12 15.89 0 -3 1 -7 592.54 14.29 0 -2 -9 -9 538.84 9.13 0 -2 -7 -5 748.65 9.51 0 -2 -5 -3 479.35 9.23 0 -1 -10 -8 280.70 9.54 0 -1 -9 -6 2.35 7.48 0 -1 -8 -4 16.78 8.69 0 -1 -5 -1 307.87 10.35 0 -1 -1 -1 4500.29 26.55 0 0 -7 -1 723.77 11.42 0 1 -10 -4 225.60 9.40 0 1 -9 -2 93.11 9.81 0 1 -4 2 1680.31 17.77 0 1 5 -6 1683.78 15.30 0 2 -9 -1 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335.63 13.29 0 4 -7 3 259.40 16.80 0 4 6 -5 50.60 9.75 0 5 5 -2 1148.55 12.06 0 6 0 4 1824.67 16.79 0 6 4 0 899.24 11.53 0 6 7 -7 126.92 9.75 0 6 8 -11 450.24 9.63 0 7 0 4 900.48 14.03 0 8 0 4 828.34 13.73 0 9 -5 4 77.06 14.67 0 9 1 3 210.37 11.15 0 10 -4 4 81.01 11.45 0 10 2 2 35.12 8.68 0 -5 -6 -15 45.32 7.54 0 -5 -6 -14 401.40 9.43 0 -5 -5 -13 49.32 7.62 0 -5 -4 -12 453.51 8.69 0 -5 -2 -12 250.08 9.37 0 -5 -1 -13 405.00 9.76 0 -5 0 -15 -8.68 9.64 0 -4 -8 -13 242.08 8.10 0 -4 -7 -10 177.89 8.63 0 -4 -4 -7 620.49 10.60 0 -4 -3 -7 1850.32 12.04 0 -3 -9 -11 263.95 8.46 0 -3 -8 -8 29.90 8.44 0 -3 3 -11 1421.01 28.24 0 -2 -7 -4 330.44 8.73 0 -2 -4 -2 1400.61 12.82 0 -2 -3 -2 277.54 9.56 0 -1 -7 -2 1416.45 12.63 0 -1 5 -12 791.61 20.04 0 0 -4 1 1747.55 15.71 0 1 -10 -3 107.31 8.88 0 1 4 -4 1537.45 15.49 0 1 6 -10 1381.07 15.96 0 2 -10 -2 145.80 9.64 0 2 3 -1 765.33 11.72 0 2 5 -5 137.28 11.39 0 2 6 -8 891.15 13.18 0 2 7 -13 423.96 12.41 0 3 -10 -1 92.48 10.57 0 3 1 2 3543.65 21.16 0 4 -2 4 198.88 15.26 0 4 4 -1 1197.98 11.93 0 4 5 -3 188.00 11.12 0 4 7 -9 360.19 10.46 0 5 1 3 1122.57 13.22 0 5 2 2 1268.87 14.06 0 5 3 1 1893.33 13.73 0 5 7 -8 433.34 10.68 0 6 5 -2 757.70 10.88 0 8 1 3 138.75 11.44 0 8 3 1 376.50 10.97 0 9 -1 4 287.07 11.58 0 9 3 1 316.01 9.41 0 10 0 3 29.04 10.12 0 11 -1 3 39.01 9.15 0 11 1 2 98.88 8.61 0 -5 -5 -12 667.37 9.37 0 -5 -4 -11 567.02 9.22 0 -5 -2 -11 210.63 9.43 0 -5 -1 -12 723.26 10.69 0 -5 0 -14 656.83 11.70 0 -4 -8 -12 12.17 7.40 0 -4 -6 -8 977.44 9.62 0 -4 -5 -7 228.17 9.83 0 -4 -2 -7 2682.70 13.76 0 -3 -7 -6 306.96 8.13 0 -3 -6 -5 57.01 8.49 0 -3 -4 -4 917.23 10.12 0 -3 -3 -4 230.70 8.89 0 -3 -2 -4 632.24 11.24 0 -2 -8 -5 671.41 9.29 0 -2 -2 -2 1241.92 13.87 0 -1 -10 -6 263.02 9.20 0 -1 -8 -3 693.51 9.71 0 -1 -6 -1 97.46 10.35 0 0 -5 1 12.39 11.02 0 0 -2 1 7285.49 37.05 0 0 6 -14 892.54 16.69 0 1 -8 0 141.80 9.90 0 1 -7 1 974.51 14.61 0 1 -5 2 3403.12 21.11 0 2 -8 1 798.75 13.59 0 3 2 1 2023.48 15.54 0 3 4 -2 1196.84 13.10 0 3 5 -4 1460.94 13.76 0 3 6 -7 61.87 10.70 0 3 7 -11 546.14 12.16 0 4 -10 0 216.53 12.66 0 4 6 -6 597.38 11.53 0 6 -9 2 -0.52 19.48 0 6 1 3 197.68 12.46 0 6 2 2 774.66 13.31 0 6 3 1 1615.13 13.44 0 6 7 -8 368.67 10.34 0 7 1 3 524.49 13.12 0 7 2 2 332.13 12.57 0 7 3 1 828.03 11.69 0 7 7 -8 197.02 10.05 0 8 -1 4 559.51 14.03 0 8 2 2 177.55 9.32 0 8 7 -8 194.69 10.12 0 -5 -7 -14 298.69 8.42 0 -5 -6 -12 458.54 8.89 0 -5 -5 -11 50.58 7.62 0 -5 -4 -10 233.80 8.31 0 -5 0 -13 -7.73 9.48 0 -5 1 -19 133.11 10.88 0 -5 1 -18 279.01 11.20 0 -4 -8 -11 414.48 8.40 0 -4 -7 -9 261.10 7.99 0 -4 1 -10 1037.16 13.81 0 -3 -9 -9 398.67 8.83 0 -3 -8 -7 432.18 8.46 0 -3 -5 -4 1182.33 10.86 0 -2 -9 -6 20.57 7.34 0 -2 -5 -2 1943.30 12.52 0 -1 -9 -4 53.24 7.59 0 -1 -4 0 1360.89 13.66 0 -1 -3 0 426.45 12.50 0 0 -10 -4 239.87 8.47 0 0 -8 -1 1120.76 12.24 0 0 -7 0 1231.46 13.02 0 0 4 -6 1210.32 16.22 0 0 5 -9 397.34 14.04 0 1 -9 -1 323.52 10.29 0 1 5 -7 376.53 12.39 0 2 -9 0 119.96 10.70 0 2 -7 2 826.29 15.46 0 2 -5 3 488.53 15.64 0 2 2 0 262.55 13.87 0 2 4 -3 2757.21 15.67 0 2 7 -14 300.26 11.12 0 3 -8 2 25.89 12.13 0 4 -3 4 86.54 18.63 0 4 0 3 0.12 11.73 0 4 3 0 267.41 11.55 0 5 4 -1 950.85 11.56 0 5 5 -3 282.36 9.82 0 5 7 -9 343.65 10.11 0 6 4 -1 378.65 11.48 0 7 -1 4 1009.95 15.90 0 8 7 -9 127.58 10.47 0 9 -4 4 83.63 11.24 0 9 -3 4 22.38 10.63 0 9 0 3 -21.12 10.60 0 10 1 2 263.37 9.49 0 10 2 1 275.58 9.20 0 11 -4 3 81.60 11.16 0 11 0 2 252.88 10.20 0 -6 -4 -16 133.69 8.93 0 -6 -3 -17 457.12 10.06 0 -6 -3 -16 -7.27 8.36 0 -5 -7 -13 91.02 7.93 0 -5 -7 -12 158.19 8.65 0 -5 -6 -11 3.37 7.32 0 -5 -5 -10 390.41 8.44 0 -5 -1 -11 262.43 9.67 0 -5 1 -17 241.89 10.52 0 -5 1 -16 299.09 11.32 0 -4 -8 -10 53.43 7.46 0 -4 -7 -8 124.39 7.47 0 -4 -6 -7 35.78 7.86 0 -4 -5 -6 1211.24 11.94 0 -4 -4 -6 169.16 8.67 0 -4 -1 -7 296.72 9.04 0 -4 0 -8 2875.39 16.48 0 -4 2 -12 139.28 13.29 0 -3 -9 -8 32.69 7.72 0 -3 -8 -6 35.23 8.23 0 -3 -7 -5 726.02 9.73 0 -3 -6 -4 934.93 11.58 0 -2 -8 -4 151.45 8.03 0 -2 -7 -3 905.65 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565.40 17.45 0 -4 3 -18 5.01 14.01 0 -4 3 -17 521.48 17.81 0 -3 -4 -3 1363.49 12.22 0 -3 -1 -4 827.07 12.70 0 -3 0 -5 -0.19 9.66 0 -3 2 -8 866.24 18.84 0 -2 -9 -5 577.90 9.15 0 -2 1 -4 1756.63 23.98 0 -1 -7 -1 907.42 11.24 0 0 -10 -3 132.02 9.43 0 0 -6 1 138.12 10.53 0 0 3 -4 97.55 13.55 0 1 -6 2 2346.00 18.40 0 2 5 -6 1421.17 14.21 0 3 -10 0 263.60 11.57 0 3 -7 3 302.61 16.76 0 3 5 -5 46.01 10.77 0 3 6 -8 1246.89 13.61 0 3 7 -13 302.49 11.71 0 4 1 2 1999.37 16.84 0 4 2 1 1891.97 14.58 0 4 4 -2 921.41 11.39 0 4 6 -7 -5.03 9.84 0 4 7 -11 383.19 10.58 0 5 -2 4 354.52 15.66 0 5 3 0 156.66 9.71 0 7 3 0 84.58 11.12 0 7 7 -10 119.73 10.13 0 8 0 3 -16.04 10.97 0 8 3 0 76.07 8.74 0 9 6 -7 -14.48 8.83 0 10 -2 3 316.27 11.39 0 10 0 2 472.72 11.46 0 11 -1 2 106.06 9.51 0 -6 -5 -14 331.49 8.22 0 -6 -4 -13 331.34 9.59 0 -6 -3 -14 6.72 7.43 0 -6 -3 -13 463.66 10.04 0 -6 -2 -15 165.73 9.20 0 -6 -2 -14 93.44 8.98 0 -6 -1 -18 235.04 9.37 0 -5 -6 -9 56.29 7.70 0 -5 -3 -8 18.00 9.39 0 -5 -2 -9 1033.02 10.99 0 -5 -1 -10 781.43 11.52 0 -5 1 -14 465.75 12.43 0 -4 -9 -10 32.07 7.88 0 -4 -8 -8 30.69 7.39 0 -4 -6 -6 811.26 9.77 0 -4 -4 -5 352.24 8.98 0 -4 -3 -5 1375.09 12.20 0 -4 1 -9 188.97 12.24 0 -3 -9 -7 400.81 8.72 0 -3 -7 -4 414.98 10.16 0 -3 -5 -3 222.02 8.97 0 -3 -3 -3 2863.83 14.73 0 -2 -10 -6 232.65 9.72 0 -2 -8 -3 776.51 10.87 0 -2 -7 -2 725.60 11.20 0 -2 -4 -1 1837.36 13.12 0 -2 -1 -2 3556.66 21.78 0 -1 -10 -4 231.15 9.60 0 -1 -6 0 1576.07 13.99 0 -1 5 -13 82.39 15.40 0 0 6 -16 672.94 15.98 0 1 -9 0 179.87 11.18 0 1 -8 1 1241.21 14.85 0 1 6 -12 1682.43 17.47 0 2 7 -17 191.97 11.86 0 3 3 -1 688.43 11.30 0 4 7 -12 322.23 10.50 0 5 0 3 -3.87 11.73 0 5 2 1 2300.65 16.32 0 5 4 -2 823.46 12.75 0 5 5 -4 869.90 11.39 0 5 6 -7 69.91 9.51 0 5 7 -11 295.80 10.82 0 6 0 3 6.19 11.85 0 6 3 0 34.85 9.65 0 6 5 -4 1009.61 12.32 0 7 -5 4 441.81 20.04 0 7 0 3 -0.73 11.83 0 7 2 1 738.39 13.14 0 8 -4 4 145.17 12.66 0 8 -3 4 30.84 10.34 0 8 1 2 369.98 10.32 0 8 2 1 654.38 10.93 0 8 6 -7 13.18 8.29 0 9 -1 3 254.52 11.49 0 10 -5 3 25.81 11.86 0 10 2 0 69.52 8.76 0 -6 -6 -14 286.17 8.37 0 -6 -5 -13 40.82 7.42 0 -6 -5 -12 676.37 10.07 0 -6 -4 -12 251.01 9.38 0 -6 -3 -12 -9.34 8.77 0 -6 -2 -13 453.87 10.17 0 -6 -1 -16 273.65 9.42 0 -6 -1 -15 300.45 10.37 0 -5 -8 -11 318.52 8.11 0 -5 -5 -8 879.40 9.79 0 -5 0 -11 6.98 10.38 0 -4 -7 -6 226.12 9.40 0 -4 -5 -5 486.31 9.36 0 -4 -1 -6 2240.58 15.08 0 -4 3 -16 3.10 15.97 0 -3 -9 -6 13.87 8.78 0 -3 -6 -3 275.32 9.22 0 -3 -2 -3 1284.65 13.32 0 -3 1 -6 1903.05 18.78 0 -2 -5 -1 18.73 8.34 0 -2 -3 -1 3004.53 16.41 0 0 -9 -1 475.90 10.94 0 0 -8 0 11.95 9.39 0 0 5 -10 1202.98 17.68 0 0 6 -17 6.66 12.87 0 1 -10 -1 183.97 10.66 0 1 1 0 6090.27 33.27 0 1 4 -5 1809.51 15.97 0 1 5 -8 1485.65 16.86 0 2 -9 1 314.40 12.32 0 2 -6 3 40.72 13.20 0 2 3 -2 49.89 11.19 0 2 4 -4 493.74 12.26 0 2 6 -10 1404.00 14.41 0 3 6 -9 114.81 11.42 0 3 7 -15 341.29 12.08 0 3 7 -14 262.04 10.64 0 4 -10 1 123.81 14.41 0 4 -9 2 21.17 13.85 0 4 6 -8 924.81 12.53 0 4 7 -13 219.93 11.18 0 5 1 2 2114.81 15.73 0 5 7 -12 466.00 11.28 0 6 1 2 1606.66 15.53 0 6 2 1 1742.03 14.08 0 6 4 -2 267.79 10.01 0 6 7 -11 332.21 9.45 0 7 -3 4 170.13 13.03 0 7 1 2 1467.55 14.28 0 7 6 -7 22.45 8.52 0 7 7 -11 223.53 9.34 0 9 -6 3 8.89 14.21 0 9 6 -8 157.22 9.45 0 10 -4 3 148.56 10.22 0 10 5 -6 240.54 9.15 0 11 -2 2 32.95 9.26 0 11 0 1 3.82 8.02 0 -6 -6 -12 381.48 9.62 0 -6 -5 -11 60.38 8.88 0 -6 -4 -11 271.47 9.56 0 -6 -1 -14 404.10 11.07 0 -5 -8 -10 22.17 8.81 0 -5 -7 -9 267.01 8.40 0 -5 -6 -8 710.04 9.41 0 -5 -5 -7 308.68 9.85 0 -5 -4 -7 604.74 10.98 0 -5 1 -13 378.95 12.00 0 -4 -9 -8 34.38 8.90 0 -4 -8 -7 304.84 8.31 0 -4 -6 -5 15.20 8.02 0 -4 -2 -5 2908.03 15.56 0 -4 0 -7 0.20 9.30 0 -4 2 -11 1212.76 18.14 0 -2 -6 -1 96.51 10.44 0 -2 4 -12 277.10 26.22 0 -1 -8 -1 1123.46 11.31 0 -1 -7 0 1103.92 12.80 0 -1 3 -6 916.53 23.24 0 0 -7 1 724.00 12.20 0 0 6 -18 285.38 14.91 0 1 -7 2 1376.04 15.91 0 1 3 -3 2912.78 19.46 0 2 -10 0 209.25 11.53 0 3 2 0 334.44 13.53 0 3 7 -16 225.87 12.10 0 4 -8 3 510.68 19.12 0 4 3 -1 1767.39 13.88 0 4 5 -5 33.52 9.45 0 5 -3 4 204.90 17.08 0 5 6 -8 612.83 11.57 0 5 7 -13 353.87 11.79 0 6 -5 4 585.96 24.30 0 7 -4 4 194.31 14.47 0 7 5 -5 146.43 10.05 0 7 6 -8 324.24 10.41 0 7 7 -12 179.68 9.50 0 8 -1 3 151.59 11.81 0 8 3 -1 812.35 10.74 0 8 6 -8 195.15 9.10 0 9 -2 3 285.21 11.54 0 9 0 2 524.42 10.74 0 9 2 0 307.36 9.45 0 9 6 -9 19.88 9.60 0 10 -1 2 250.03 10.19 0 -6 -7 -12 155.49 9.01 0 -6 -6 -11 1.20 8.70 0 -6 -3 -11 472.18 9.19 0 -6 -2 -12 161.94 8.11 0 -6 -1 -13 237.30 10.42 0 -6 0 -18 358.26 10.73 0 -6 0 -17 -14.93 9.77 0 -5 -7 -8 310.48 8.65 0 -5 -3 -7 942.66 10.61 0 -5 0 -10 500.78 12.14 0 -5 2 -19 279.48 12.80 0 -5 2 -18 92.98 11.99 0 -4 -7 -5 539.65 10.35 0 -4 -5 -4 721.85 11.31 0 -4 -4 -4 463.74 9.63 0 -4 3 -15 703.85 20.03 0 -3 -9 -5 403.34 9.74 0 -3 -8 -4 20.64 7.86 0 -3 -7 -3 256.65 8.92 0 -3 -5 -2 1424.07 12.91 0 -3 -4 -2 1489.59 11.92 0 -2 -2 -1 3709.32 19.99 0 -1 -10 -3 160.59 9.55 0 -1 2 -4 755.35 34.29 0 0 -4 2 1818.78 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4 1160.04 38.57 0 3 1 1 682.84 14.18 0 3 6 -10 1546.54 14.03 0 4 5 -6 1366.73 14.05 0 5 -4 4 238.72 21.03 0 5 4 -3 1020.64 11.91 0 5 6 -9 14.28 9.62 0 6 -4 4 101.87 17.16 0 6 -1 3 214.35 14.33 0 6 4 -3 863.50 11.53 0 7 2 0 206.96 11.58 0 7 6 -9 91.57 9.57 0 8 1 1 59.14 9.25 0 9 -5 3 89.87 11.69 0 9 -4 3 106.85 11.17 0 9 -1 2 412.91 12.96 0 9 5 -7 56.14 9.68 0 10 -2 2 53.00 9.49 0 10 5 -8 225.72 10.19 0 11 0 0 239.23 8.93 0 -7 -4 -15 308.22 9.92 0 -7 -3 -16 26.73 9.16 0 -6 -7 -10 230.07 9.13 0 -6 -5 -9 71.56 8.97 0 -6 -4 -9 579.80 10.50 0 -6 -1 -12 331.77 10.01 0 -6 0 -15 -16.54 9.79 0 -5 -7 -7 278.37 8.44 0 -5 -6 -6 737.51 10.53 0 -5 -3 -6 32.13 9.80 0 -5 2 -16 14.59 11.94 0 -4 -8 -5 389.81 9.85 0 -4 -7 -4 293.53 9.29 0 -4 -1 -5 383.33 11.00 0 -4 1 -8 1756.95 17.19 0 -3 -9 -4 57.99 8.86 0 -3 -8 -3 284.30 9.52 0 -3 -1 -3 714.18 13.32 0 -2 -5 0 1809.35 14.09 0 -2 -4 0 1153.81 13.15 0 -1 -10 -2 248.13 9.82 0 -1 -9 -1 528.06 10.99 0 -1 -8 0 121.79 9.73 0 -1 -6 1 5.30 10.64 0 0 -10 -1 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1209.56 18.82 0 1 -8 2 3.09 11.71 0 1 -4 3 3352.29 27.01 0 1 4 -6 1610.40 16.70 0 1 6 -15 71.99 11.91 0 2 -10 1 194.02 12.29 0 2 2 -1 1490.19 16.97 0 2 5 -8 1777.67 16.73 0 3 5 -7 89.50 11.08 0 3 6 -11 39.81 10.37 0 4 0 2 2857.81 20.41 0 4 1 1 421.07 13.36 0 4 4 -4 1111.58 13.38 0 5 6 -10 541.96 11.29 0 6 0 2 1657.08 16.27 0 6 1 1 463.26 12.64 0 7 3 -2 26.83 9.93 0 7 4 -4 215.72 9.46 0 8 5 -7 40.78 8.69 0 9 0 1 5.13 8.64 0 9 5 -8 176.76 9.18 0 10 -1 1 13.75 9.61 0 -7 -6 -13 42.07 7.83 0 -7 -5 -12 333.49 9.66 0 -7 -4 -12 159.92 8.98 0 -7 -3 -13 334.83 9.87 0 -7 -2 -15 152.67 9.43 0 -6 -8 -10 40.19 7.92 0 -6 -7 -9 174.65 8.18 0 -6 -6 -8 458.62 9.12 0 -6 -5 -8 847.78 10.10 0 -6 -2 -9 1030.51 11.80 0 -5 -9 -8 70.36 8.07 0 -5 -6 -5 114.96 9.17 0 -5 -5 -5 641.73 9.89 0 -5 -4 -5 508.94 9.64 0 -5 -2 -6 367.31 11.03 0 -5 -1 -7 351.26 10.93 0 -5 1 -11 251.58 11.47 0 -4 -9 -5 360.02 9.75 0 -4 -8 -4 0.76 8.90 0 -4 2 -10 266.75 14.99 0 -3 -4 -1 860.22 12.17 0 -3 -2 -2 551.64 10.95 0 -2 -3 0 751.69 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1760.89 15.82 0 3 4 -5 1766.20 14.21 0 3 5 -8 1305.69 14.32 0 4 6 -12 837.94 12.45 0 5 -9 3 490.06 29.11 0 5 6 -12 816.22 12.29 0 6 2 -1 1154.33 13.90 0 6 4 -5 723.35 12.76 0 6 5 -8 522.70 11.23 0 6 6 -12 640.39 10.55 0 7 -1 2 1499.42 17.41 0 7 1 0 752.03 13.04 0 7 3 -3 1310.47 12.80 0 7 5 -8 474.05 9.96 0 7 6 -13 19.59 10.11 0 8 4 -6 295.39 10.19 0 9 -1 1 113.42 10.86 0 9 0 0 304.75 10.79 0 9 1 -1 181.62 9.15 0 9 5 -10 290.64 9.52 0 10 4 -8 129.48 8.92 0 11 3 -7 125.46 10.28 0 -7 -7 -10 161.73 9.10 0 -7 -6 -10 191.18 8.13 0 -7 -5 -10 497.77 9.35 0 -7 -4 -10 460.43 9.33 0 -7 -2 -12 56.48 9.09 0 -7 -1 -15 175.49 9.32 0 -7 -1 -14 314.14 10.46 0 -6 -7 -7 232.91 8.17 0 -6 -5 -6 669.94 10.63 0 -6 -3 -7 1181.50 11.37 0 -6 -2 -8 260.42 9.31 0 -6 1 -15 295.52 11.62 0 -5 -9 -6 33.50 8.34 0 -5 -8 -5 460.13 9.25 0 -5 -7 -4 220.29 9.55 0 -5 -6 -4 816.79 10.07 0 -5 -4 -4 242.97 9.21 0 -5 -2 -5 2068.52 14.29 0 -5 1 -10 737.51 13.68 0 -4 -4 -2 677.90 10.24 0 -4 -2 -3 1614.45 13.87 0 -4 -1 -4 673.23 11.92 0 -4 1 -7 311.74 13.02 0 -3 -9 -2 58.64 7.89 0 -3 1 -5 1467.67 18.98 0 -3 2 -7 2166.37 26.81 0 -2 -8 0 93.13 8.82 0 -2 -5 1 120.98 10.74 0 -2 -1 -1 1559.16 18.78 0 -2 0 -2 5238.24 33.00 0 -1 -5 2 912.52 13.27 0 0 -8 2 55.55 11.14 0 1 -9 2 174.91 12.44 0 2 1 0 5113.19 28.88 0 3 -10 2 64.95 14.16 0 3 3 -3 2874.50 17.60 0 3 6 -14 970.92 14.32 0 4 -9 3 535.88 21.05 0 4 2 -1 1664.64 14.21 0 4 4 -5 1341.53 12.90 0 4 5 -8 1042.98 12.25 0 4 6 -13 49.40 10.01 0 5 2 -1 2729.96 15.75 0 5 4 -5 914.88 11.95 0 5 5 -8 915.69 11.46 0 5 6 -13 16.68 10.01 0 6 3 -3 1298.78 12.92 0 6 6 -13 61.15 10.09 0 7 -3 3 929.93 16.37 0 7 0 1 -9.66 11.64 0 7 5 -9 14.06 9.84 0 7 6 -14 512.92 11.91 0 8 -8 2 12.81 19.25 0 8 -2 2 181.47 12.02 0 8 2 -2 200.61 9.72 0 9 5 -11 32.17 8.72 0 10 -3 1 213.43 11.20 0 10 -1 0 421.62 10.74 0 10 0 -1 -0.31 8.35 0 10 3 -6 35.67 8.39 0 11 -1 -1 23.12 8.16 0 -7 -6 -9 42.95 7.69 0 -7 -5 -9 7.77 8.14 0 -7 -4 -9 361.39 10.32 0 -7 -3 -10 42.28 9.21 0 -7 -2 -11 446.53 10.33 0 -7 -1 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2 2066.37 19.68 0 5 4 -6 884.64 11.99 0 6 -3 3 1634.00 21.25 0 6 2 -2 155.84 11.53 0 6 3 -4 47.63 11.26 0 6 5 -10 725.23 11.88 0 7 -4 3 681.63 14.98 0 7 4 -7 478.84 10.08 0 8 2 -3 1156.43 12.06 0 8 4 -8 284.67 9.59 0 8 5 -12 222.57 10.33 0 9 -1 0 589.87 12.12 0 9 4 -9 348.62 9.44 0 10 -6 1 11.16 11.38 0 10 -5 1 -2.82 10.20 0 10 0 -2 284.25 9.17 0 11 2 -7 155.53 10.04 0 -8 -5 -11 -4.38 8.09 0 -8 -4 -11 287.74 9.53 0 -8 -3 -13 307.74 8.81 0 -7 -7 -7 131.66 9.39 0 -7 -6 -7 35.65 8.00 0 -7 -5 -7 73.37 8.28 0 -7 -3 -8 13.83 9.47 0 -7 -1 -11 338.84 11.23 0 -7 0 -15 7.56 8.91 0 -6 -8 -5 284.02 8.54 0 -5 -3 -3 2469.74 15.13 0 -5 -2 -4 337.00 9.68 0 -5 -1 -5 230.10 10.75 0 -5 2 -12 240.84 14.29 0 -4 -10 -3 156.03 8.53 0 -4 -4 -1 1159.64 11.61 0 -3 -8 0 174.23 8.98 0 -3 -3 0 192.52 11.14 0 -3 0 -3 -7.74 12.12 0 -2 -3 1 747.91 12.88 0 -2 4 -13 629.23 24.90 0 0 -4 3 2195.12 20.87 0 0 5 -14 1129.49 18.86 0 1 -10 2 232.19 12.37 0 1 5 -12 952.91 16.35 0 2 2 -2 966.22 15.41 0 2 4 -7 523.98 14.10 0 2 5 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334.48 12.34 0 4 3 -4 228.83 10.04 0 5 4 -7 1450.87 14.70 0 6 5 -11 177.66 9.46 0 7 -1 1 90.12 12.05 0 7 0 0 1315.37 13.46 0 7 2 -3 909.95 12.05 0 7 4 -8 467.86 10.48 0 7 5 -12 437.15 10.05 0 8 1 -2 737.92 11.51 0 8 2 -4 163.35 10.95 0 8 3 -6 22.56 8.62 0 8 4 -9 465.95 10.29 0 8 5 -14 348.94 11.04 0 9 -3 1 352.17 11.13 0 9 1 -3 118.23 9.02 0 9 2 -5 285.16 10.44 0 9 4 -11 246.18 11.02 0 10 -3 0 31.94 9.38 0 10 3 -9 376.99 10.55 0 11 2 -8 30.46 8.67 0 -8 -5 -9 48.10 9.26 0 -8 -3 -11 380.68 9.09 0 -8 -2 -13 170.58 9.65 0 -7 -7 -6 116.08 8.21 0 -7 -3 -7 509.81 10.69 0 -7 -1 -10 589.50 11.09 0 -7 0 -13 6.07 10.09 0 -6 -4 -4 126.30 9.23 0 -6 -1 -7 584.25 11.74 0 -6 2 -18 91.95 14.22 0 -5 -4 -2 776.72 11.07 0 -4 -6 0 991.97 12.80 0 -4 -5 0 1574.02 14.03 0 -4 -3 -1 2703.11 15.09 0 -4 1 -6 2275.26 19.88 0 -3 -7 1 215.03 10.90 0 -3 -5 1 18.96 9.31 0 -2 -7 2 629.69 12.67 0 -2 -5 2 1396.78 14.39 0 -1 -9 2 109.36 11.17 0 -1 -6 3 227.43 13.08 0 1 3 -5 4085.39 24.19 0 1 4 -8 490.78 14.44 0 3 -8 4 41.30 17.73 0 3 4 -7 827.42 13.76 0 3 5 -11 162.09 11.43 0 4 4 -7 1707.38 15.59 0 4 5 -11 193.10 11.22 0 6 1 -1 566.27 11.14 0 6 3 -5 1310.03 13.89 0 6 4 -8 220.44 11.26 0 6 5 -12 583.44 11.51 0 7 5 -13 52.97 9.05 0 8 -4 2 71.51 10.82 0 8 -2 1 738.24 12.88 0 8 -1 0 765.71 13.15 0 8 0 -1 1.41 10.75 0 8 4 -10 174.58 10.63 0 9 -2 0 257.19 11.35 0 10 2 -7 305.78 10.85 0 11 -4 -1 53.87 9.68 0 -8 -4 -9 317.88 8.94 0 -8 -3 -10 -7.44 9.23 0 -8 -2 -12 40.47 9.43 0 -8 -1 -15 129.86 9.43 0 -7 -8 -6 11.33 8.22 0 -7 -2 -8 135.61 8.71 0 -7 0 -12 599.83 11.95 0 -6 -3 -4 396.85 11.03 0 -6 -2 -5 1841.52 14.54 0 -6 2 -17 380.03 14.55 0 -5 -6 -1 88.30 10.16 0 -5 0 -6 947.92 13.08 0 -5 1 -8 1050.34 16.13 0 -5 3 -18 38.01 21.20 0 -4 -8 0 94.95 9.97 0 -4 -7 0 441.80 9.83 0 -4 0 -4 318.06 12.92 0 -3 -8 1 625.82 11.51 0 -3 -4 1 942.82 13.07 0 -2 -8 2 13.89 10.39 0 -2 -4 2 1524.79 15.15 0 -1 -5 3 161.15 13.13 0 1 -7 4 257.09 18.03 0 1 1 -1 3140.58 28.47 0 1 5 -13 46.58 11.86 0 2 -8 4 154.28 16.67 0 2 5 -12 1562.63 16.27 0 3 -10 3 126.47 17.27 0 4 -10 3 142.01 20.89 0 5 5 -12 1033.95 13.39 0 6 -4 3 1355.96 21.02 0 6 0 0 1343.14 14.92 0 6 2 -3 1544.52 13.56 0 6 5 -13 12.52 10.29 0 7 1 -2 774.03 13.06 0 7 3 -6 7.52 9.31 0 7 4 -9 671.23 10.80 0 7 5 -14 387.26 10.09 0 8 -7 2 43.68 13.45 0 9 -1 -1 150.88 9.67 0 9 1 -4 210.34 10.64 0 9 2 -6 25.47 9.88 0 9 4 -12 144.83 9.77 0 10 3 -10 14.76 8.63 0 11 0 -5 3.51 8.20 0 11 1 -7 147.72 9.98 0 11 2 -9 143.20 9.14 0 -8 -5 -8 310.37 8.92 0 -8 -2 -11 377.57 10.05 0 -8 -1 -14 298.75 9.86 0 -7 -8 -5 166.77 9.52 0 -7 -7 -5 188.06 8.50 0 -7 -5 -5 65.26 8.34 0 -7 -3 -6 39.72 9.67 0 -7 -1 -9 330.91 10.22 0 -7 1 -17 53.62 11.38 0 -6 -4 -3 1295.98 13.19 0 -6 0 -8 1198.61 14.55 0 -6 1 -11 188.13 11.12 0 -6 2 -16 2.89 12.67 0 -5 -5 -1 176.60 9.65 0 -5 -3 -2 343.79 9.87 0 -5 -2 -3 2153.81 13.91 0 -5 -1 -4 1866.25 14.55 0 -5 2 -11 211.81 14.86 0 -4 -4 0 845.35 11.17 0 -4 3 -12 22.83 22.57 0 -2 1 -3 2375.09 32.08 0 -1 -8 3 1497.24 15.52 0 -1 3 -7 3955.34 35.40 0 0 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666.11 11.39 0 8 3 -10 6.86 8.73 0 8 4 -15 103.74 9.34 0 9 0 -4 204.11 9.08 0 9 1 -6 349.89 10.32 0 10 -3 -2 18.86 9.21 0 10 -1 -4 195.20 9.72 0 10 1 -8 267.59 10.32 0 10 2 -11 157.47 9.89 0 11 -1 -6 248.05 9.64 0 11 1 -10 109.11 8.70 0 -9 -5 -8 173.36 8.37 0 -9 -3 -10 9.62 9.29 0 -9 -2 -12 34.94 8.89 0 -8 -5 -5 53.67 8.39 0 -8 0 -14 475.55 10.77 0 -7 -3 -4 170.25 10.60 0 -7 1 -13 149.37 10.76 0 -6 -5 -1 187.42 9.27 0 -6 1 -9 230.80 12.96 0 -5 -4 0 1288.25 12.38 0 -5 -1 -3 1012.85 12.14 0 -4 -7 2 479.07 11.16 0 -4 1 -5 378.21 14.20 0 -3 0 -2 2940.62 21.61 0 -2 -9 3 454.49 12.61 0 -1 -7 4 586.60 12.74 0 -1 -6 4 948.55 15.93 0 -1 4 -12 335.82 17.79 0 0 -9 4 28.10 13.70 0 1 -4 4 2718.61 29.94 0 1 3 -6 525.20 13.25 0 1 5 -20 499.88 14.57 0 1 5 -19 79.71 12.70 0 1 5 -18 492.01 13.45 0 2 5 -17 187.29 11.89 0 3 3 -6 182.44 11.75 0 3 5 -17 151.81 11.68 0 3 5 -16 786.73 12.66 0 4 4 -10 315.05 12.13 0 4 5 -18 482.45 11.79 0 4 5 -17 90.50 10.32 0 5 -4 3 1083.98 20.33 0 5 3 -7 1749.94 14.80 0 6 2 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11.51 0 2 4 -10 609.88 14.05 0 2 5 -19 28.28 11.41 0 3 4 -10 245.26 12.06 0 3 5 -19 49.15 11.72 0 3 5 -18 594.47 12.06 0 5 4 -11 503.55 10.26 0 6 -1 0 1869.27 16.04 0 6 1 -3 397.48 10.45 0 6 3 -8 35.80 9.90 0 6 4 -13 398.00 10.66 0 7 -5 2 636.53 15.30 0 7 1 -4 970.50 11.52 0 7 4 -15 224.29 9.92 0 8 -3 0 74.73 10.90 0 8 -1 -2 728.72 12.63 0 8 2 -8 160.55 10.14 0 9 -2 -2 133.86 9.93 0 9 0 -5 -1.82 9.50 0 9 1 -7 180.52 9.68 0 9 3 -14 -3.96 8.47 0 10 -1 -5 64.71 9.22 0 10 1 -9 149.57 8.47 0 10 2 -12 67.75 8.41 0 11 -1 -7 149.96 9.47 0 11 0 -9 8.75 8.91 0 -9 -6 -6 142.26 8.49 0 -9 -4 -7 207.03 9.37 0 -8 -2 -7 203.20 9.73 0 -8 -1 -9 131.76 9.24 0 -8 0 -12 524.83 11.71 0 -7 -1 -6 454.99 11.19 0 -7 1 -12 386.46 11.67 0 -6 -6 0 826.09 10.46 0 -6 -1 -4 1489.06 13.96 0 -6 0 -6 1157.04 13.64 0 -5 -5 1 295.60 10.08 0 -4 -5 2 1918.10 14.08 0 -4 -3 1 1709.53 14.86 0 -4 -2 0 1382.83 13.25 0 -3 -5 3 41.96 11.36 0 -2 -10 3 99.76 11.02 0 -1 -9 4 147.95 13.43 0 -1 -5 4 2092.50 18.51 0 -1 -1 1 3100.35 28.50 0 0 4 -11 471.75 15.26 0 1 -10 4 223.16 14.46 0 2 -10 4 317.25 16.70 0 3 0 0 4911.86 26.61 0 4 1 -2 3611.96 18.29 0 4 2 -4 544.13 10.83 0 4 3 -7 2027.86 15.29 0 4 4 -11 599.06 11.96 0 5 4 -12 343.60 11.11 0 7 -8 2 50.86 14.61 0 7 -2 0 210.64 11.71 0 7 -1 -1 345.08 10.47 0 7 2 -7 559.83 11.53 0 7 3 -10 8.76 8.77 0 7 4 -17 197.73 10.29 0 7 4 -16 199.27 9.07 0 8 -8 1 45.08 13.77 0 8 -5 1 104.49 10.30 0 8 -2 -1 423.16 11.34 0 8 3 -12 -5.56 8.24 0 9 -7 0 30.68 11.59 0 9 -6 0 293.39 12.12 0 10 -4 -2 101.43 9.27 0 10 -2 -4 26.44 9.31 0 10 0 -7 -14.47 8.28 0 10 1 -10 132.77 9.64 0 11 -2 -6 25.94 9.05 0 -9 -5 -6 272.66 8.26 0 -9 -3 -8 18.00 7.90 0 -9 -2 -10 28.98 8.69 0 -9 -1 -13 30.78 8.98 0 -8 -3 -5 812.49 11.05 0 -7 -4 -2 276.23 9.14 0 -7 -2 -4 240.60 10.84 0 -7 0 -8 865.21 12.19 0 -6 -5 0 1376.07 12.08 0 -6 2 -12 133.44 13.36 0 -5 -3 0 122.03 9.49 0 -5 -2 -1 2126.59 14.06 0 -5 0 -4 885.69 12.59 0 -4 -1 -1 365.95 12.00 0 -3 -9 3 292.49 9.25 0 -3 -3 2 -5.69 11.43 0 -3 -2 1 1739.35 15.74 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2 -7 -17 198.91 7.00 0 2 -6 -16 665.06 8.34 0 2 -5 -15 282.15 7.83 0 2 -3 1 2857.62 20.78 0 3 -8 -13 270.42 7.00 0 3 -8 2 19.95 8.57 0 3 -6 -12 1420.14 9.26 0 3 -6 1 116.98 9.25 0 3 -5 -10 1207.36 8.93 0 -11 4 -3 100.69 9.43 0 -10 4 -6 61.28 11.61 0 -10 4 -2 127.78 9.53 0 -10 4 -1 141.35 9.10 0 -9 4 -6 123.13 11.94 0 -9 4 -2 79.12 8.91 0 -9 4 -1 150.58 9.24 0 -8 4 -4 157.02 10.89 0 -7 3 5 687.23 9.90 0 -5 3 1 2062.40 13.73 0 -4 -1 13 300.41 7.70 0 -3 2 2 800.91 11.07 0 -2 -5 15 290.57 8.36 0 -2 -2 -20 88.64 7.79 0 -2 -1 10 1854.16 11.93 0 -1 -3 -20 -17.47 6.42 0 -1 -1 -16 939.21 9.58 0 0 -5 -20 544.17 8.80 0 0 -4 -19 529.89 8.37 0 0 -3 -18 -2.45 6.34 0 0 -2 -16 282.04 7.84 0 1 -5 -18 539.81 7.60 0 1 -3 -15 1185.49 8.81 0 1 -1 -8 1154.05 9.52 0 2 -9 6 12.02 10.97 0 2 -7 -16 207.36 6.80 0 2 -4 -13 550.16 7.44 0 3 -10 0 252.28 8.36 0 3 -9 -11 456.88 8.31 0 3 -9 1 295.07 9.02 0 3 -8 -12 45.80 6.15 0 3 -7 -12 483.36 7.49 0 3 -7 -11 530.69 8.32 0 3 -6 -11 36.11 6.49 0 3 -5 -9 242.05 7.14 0 3 -5 -8 1325.49 10.10 0 -11 4 -1 56.73 9.48 0 -11 4 0 49.60 8.96 0 -10 4 0 3.99 7.70 0 -9 4 -7 193.75 13.63 0 -8 4 -6 71.96 12.67 0 -8 4 -5 305.55 11.88 0 -8 4 -3 267.26 9.73 0 -8 4 -2 52.82 8.75 0 -8 4 -1 77.13 8.68 0 -6 3 4 70.98 8.37 0 -5 -3 17 608.38 8.65 0 -5 3 2 83.39 8.23 0 -4 -3 16 112.21 6.78 0 -3 -2 -21 350.40 8.93 0 -3 -1 12 1611.53 10.56 0 -3 1 7 1783.29 11.18 0 -2 -3 -21 540.48 9.27 0 -1 -2 10 319.34 8.48 0 -1 -1 8 1136.38 10.87 0 -1 0 5 1.66 10.02 0 0 -1 -13 200.99 7.32 0 1 -6 -18 448.75 7.23 0 1 -5 -17 117.01 7.49 0 1 -4 -16 484.53 7.23 0 1 -1 -7 388.05 7.92 0 2 -6 -15 122.77 6.52 0 2 -5 -14 876.90 8.15 0 3 -9 -10 18.47 6.82 0 3 -8 -11 537.89 7.59 0 3 -8 1 591.54 10.27 0 3 -7 -10 556.46 8.37 0 3 -7 1 522.32 10.44 0 3 -6 -9 141.31 7.56 0 3 -5 -7 82.72 6.75 0 3 -5 -6 1565.55 10.79 0 3 -5 -3 43.66 7.61 0 3 -5 -2 1426.93 11.32 0 -11 4 1 40.81 8.36 0 -10 4 1 91.88 7.97 0 -10 4 2 125.15 8.93 0 -9 4 1 176.28 8.55 0 -8 4 -7 394.56 16.76 0 -8 4 0 208.36 9.43 0 -6 3 5 1286.68 11.02 0 -4 3 -4 77.60 13.43 0 -4 3 -3 2796.43 22.48 0 -3 -1 -19 208.04 8.04 0 -2 0 8 1989.59 11.73 0 -1 -4 -20 380.99 8.46 0 -1 -3 -19 684.03 8.48 0 0 -5 -19 49.16 6.79 0 0 -4 -18 333.81 8.10 0 0 -3 -17 1164.17 8.85 0 0 -1 5 1951.04 17.35 0 1 -1 -6 1935.10 12.48 0 1 -1 -5 1974.06 14.11 0 1 -1 -2 2452.22 17.70 0 2 -10 5 112.38 10.29 0 2 -6 -14 1018.32 8.45 0 2 -3 -9 2911.16 11.84 0 3 -10 -7 90.46 6.34 0 3 -10 -6 180.75 7.41 0 3 -10 -5 132.44 7.18 0 3 -10 -4 75.51 7.11 0 3 -10 -3 149.05 7.89 0 3 -9 -9 432.91 7.35 0 3 -9 -8 68.91 7.17 0 3 -9 0 52.93 7.39 0 3 -8 -9 700.61 8.72 0 3 -6 -8 1246.57 9.62 0 3 -5 -5 37.49 6.61 0 3 -5 -4 1404.14 10.11 0 -11 4 2 28.91 8.22 0 -11 4 3 75.90 8.78 0 -10 4 3 158.30 9.09 0 -9 4 2 178.68 8.56 0 -7 4 -5 175.42 12.78 0 -7 4 -3 684.90 13.17 0 -7 4 -2 294.63 10.85 0 -7 4 -1 239.60 10.49 0 -5 3 3 1564.97 11.97 0 -4 -1 14 1644.44 10.40 0 -4 3 -2 458.99 12.69 0 -3 2 3 2262.78 13.49 0 -2 -3 14 10.56 6.94 0 -2 -2 -19 524.79 8.14 0 1 -7 -17 205.85 6.92 0 1 -6 -17 32.16 6.23 0 1 -5 -16 876.72 8.27 0 1 -4 -15 527.89 7.41 0 1 -1 -4 1344.73 12.86 0 1 -1 -3 3073.80 18.03 0 2 -8 -14 54.83 6.35 0 2 -7 -14 301.55 6.89 0 2 -3 -8 234.45 6.82 0 2 -3 -7 2755.31 12.70 0 3 -9 -7 362.57 7.91 0 3 -9 -5 295.77 8.22 0 3 -8 -8 35.88 6.84 0 3 -8 -7 644.57 8.59 0 3 -7 -8 370.10 7.09 0 3 -7 -7 430.77 8.05 0 3 -6 -7 74.02 6.26 0 3 -6 -5 77.59 7.53 0 3 -6 -2 1128.02 11.05 0 -11 4 4 23.69 8.95 0 -10 4 4 37.35 8.20 0 -9 4 3 224.89 8.58 0 -8 4 2 297.79 9.01 0 -7 4 0 362.38 9.86 0 -5 -3 18 68.48 6.75 0 -5 3 4 45.50 7.88 0 -4 3 -1 2619.89 17.85 0 -2 -1 11 523.67 8.04 0 -1 -4 -19 554.94 8.57 0 -1 -3 -18 33.68 7.28 0 0 -5 -18 654.52 7.90 0 0 -4 -17 652.06 8.71 0 0 -3 -16 16.33 6.47 0 2 -8 -13 287.47 7.40 0 2 -6 -13 95.39 6.53 0 2 -4 -10 629.35 7.79 0 2 -3 -6 45.94 7.51 0 3 -9 -4 101.24 7.10 0 3 -8 -6 14.48 7.23 0 3 -8 -5 858.05 9.40 0 3 -8 -4 38.09 8.15 0 3 -8 -3 976.62 10.46 0 3 -8 -2 4.36 7.65 0 3 -7 -6 519.82 8.26 0 3 -7 -5 452.76 8.40 0 3 -7 -2 529.31 9.41 0 3 -6 -4 707.08 9.21 0 3 -6 -3 61.41 7.48 0 -10 4 5 81.22 8.54 0 -9 4 4 151.41 8.18 0 -8 4 3 358.62 9.01 0 -7 4 -6 278.92 15.30 0 -7 4 1 380.11 9.78 0 -4 3 0 237.93 9.75 0 -2 0 9 -5.62 6.48 0 -1 -2 11 2989.58 14.23 0 -1 -1 9 1808.29 12.10 0 -1 1 0 5780.07 36.55 0 0 -6 -18 395.27 7.26 0 1 -7 -16 132.62 6.41 0 1 -5 -15 174.24 6.55 0 1 -4 -14 512.72 7.39 0 1 -3 -12 193.35 6.79 0 2 -10 4 283.06 10.05 0 2 -8 -12 35.82 6.81 0 2 -6 -12 1232.72 8.83 0 2 -5 -11 244.40 6.85 0 2 -3 -5 3481.32 14.31 0 2 -3 -4 7.88 7.61 0 2 -3 -2 41.67 8.21 0 3 -7 -4 811.05 9.22 0 3 -7 -3 742.61 9.31 0 -10 4 6 101.62 8.77 0 -9 4 5 108.16 8.38 0 -8 4 4 314.48 8.81 0 -7 4 2 276.67 9.21 0 -5 3 5 2500.18 13.19 0 -4 3 1 1649.18 13.57 0 -2 -4 -20 328.12 7.70 0 -1 -5 -19 54.98 6.68 0 0 -5 -17 56.69 6.26 0 0 -3 -15 1206.32 8.84 0 1 -10 10 -0.16 2.95 0 1 -5 -14 1184.17 9.42 0 1 -2 -9 2402.43 11.44 0 2 -9 -11 369.33 6.90 0 2 -3 -3 5144.12 17.89 0 -9 4 6 86.27 8.11 0 -8 4 5 206.46 8.41 0 -7 4 3 967.56 10.31 0 -5 -3 19 567.59 8.21 0 -4 3 2 45.02 9.00 0 -1 -4 -18 326.69 7.06 0 0 -7 -17 192.75 7.67 0 0 -6 -17 33.35 6.13 0 1 -3 -11 1623.75 9.82 0 2 -10 3 168.23 9.03 0 2 -8 -11 429.67 7.09 0 2 -7 -11 595.33 7.44 0 -10 4 7 103.28 7.21 0 -9 4 7 362.22 8.72 0 -8 4 6 299.51 8.34 0 -7 4 4 223.59 8.32 0 -6 4 -3 1267.67 15.26 0 -6 4 -1 594.05 11.90 0 -6 4 0 916.27 11.63 0 -2 0 10 2862.00 12.50 0 0 -5 -16 738.77 7.95 0 0 -3 -14 57.29 6.33 0 1 -6 -14 594.74 7.47 0 1 -5 -13 39.23 6.10 0 2 -10 -7 70.47 7.06 0 2 -9 -9 301.08 6.97 0 2 -8 -10 26.81 6.12 0 2 -7 -10 404.65 7.03 0 2 -6 5 38.03 12.04 0 2 -4 -6 1082.05 9.61 0 -10 4 8 118.76 8.17 0 -7 4 5 475.13 9.04 0 -6 4 -4 110.01 12.09 0 -6 4 1 369.09 9.90 0 -4 3 3 3898.63 16.13 0 -3 2 6 234.15 7.18 0 -1 -6 -18 410.57 7.29 0 -1 -4 -17 813.45 8.23 0 -1 1 1 2885.57 22.05 0 0 -7 -16 298.54 6.76 0 0 -6 -16 721.00 7.56 0 1 -6 -13 235.27 6.71 0 1 -3 -10 150.92 6.51 0 2 -10 -6 212.32 7.12 0 2 -10 2 174.99 8.29 0 2 -9 -8 49.03 6.13 0 2 -9 4 54.72 8.93 0 2 -8 -9 685.24 7.68 0 2 -8 5 684.95 12.77 0 2 -7 -9 730.77 7.85 0 2 -5 -8 1723.67 9.90 0 2 -4 -5 2634.98 12.58 0 -9 4 8 100.82 7.29 0 -8 4 7 489.92 8.11 0 -7 4 6 273.71 8.25 0 -6 4 2 275.49 8.68 0 -6 4 3 817.11 9.99 0 -4 3 4 200.89 8.24 0 -2 -5 -19 -7.93 6.71 0 0 -5 -15 164.35 6.56 0 2 -10 -4 57.07 6.70 0 2 -9 -7 434.46 7.20 0 2 -8 -8 14.72 5.85 0 2 -7 -8 222.00 7.34 0 2 -6 -8 866.93 8.17 0 2 -5 -7 189.94 6.86 0 2 -4 -4 462.60 8.72 0 2 -4 1 1695.73 14.66 0 -10 5 0 149.49 10.00 0 -8 4 8 258.19 7.50 0 -7 4 7 490.97 8.60 0 -6 4 4 728.13 9.79 0 -5 3 8 67.73 6.85 0 -4 3 5 2288.16 12.47 0 -3 2 7 2015.43 11.09 0 -2 2 -1 3312.28 24.90 0 -2 2 0 236.71 11.40 0 -1 1 2 2452.33 18.00 0 0 -7 -15 293.59 6.70 0 0 -6 -15 48.33 6.12 0 1 -6 -12 1746.08 9.60 0 2 -9 -6 98.02 6.36 0 2 -9 -5 498.53 8.05 0 2 -8 -7 612.86 7.47 0 2 -7 -7 318.50 7.63 0 2 -6 -7 62.19 7.14 0 2 -5 -6 1392.63 9.50 0 2 -4 -3 2628.17 13.37 0 2 -4 -2 1418.43 11.45 0 -10 5 -2 207.55 10.14 0 -10 5 -1 2.76 8.79 0 -10 5 1 48.94 8.85 0 -10 5 2 185.97 9.31 0 -10 5 3 46.62 8.62 0 -6 4 5 737.54 9.64 0 0 -5 -14 1125.50 8.56 0 1 -8 -11 595.75 7.39 0 2 -9 2 48.56 7.84 0 2 -8 -6 77.40 6.23 0 2 -8 -5 956.21 9.21 0 2 -7 -6 400.25 7.93 0 2 -6 -6 1291.03 9.90 0 2 -6 4 850.06 14.16 0 2 -5 -5 133.43 7.46 0 -10 5 -3 16.22 10.21 0 -10 5 4 139.42 8.29 0 -10 5 5 6.45 8.55 0 -9 5 -2 312.23 11.24 0 -9 5 -1 29.97 8.43 0 -9 5 0 325.95 10.04 0 -9 5 1 72.66 7.88 0 -9 5 3 53.28 8.62 0 -7 4 8 455.27 7.91 0 -6 4 6 498.24 8.96 0 -5 3 9 2272.25 11.17 0 -4 3 6 69.41 6.48 0 -3 2 8 708.72 8.03 0 1 -5 -10 981.95 8.33 0 2 -9 -2 35.85 6.82 0 2 -8 -4 48.69 7.34 0 2 -8 3 764.03 11.30 0 2 -7 -5 425.24 8.17 0 2 -7 4 330.93 10.91 0 2 -6 -5 37.00 7.14 0 2 -5 -4 1749.31 10.94 0 -10 5 6 196.04 8.65 0 -9 5 -3 87.52 10.85 0 -9 5 4 263.27 8.44 0 -9 5 5 90.77 7.90 0 -8 2 17 332.86 7.64 0 -8 5 0 336.42 10.24 0 -8 5 1 60.59 8.29 0 -8 5 2 551.81 9.99 0 -7 3 13 512.74 7.88 0 -7 4 9 641.76 8.20 0 -6 2 15 441.12 7.55 0 -5 3 10 83.68 6.79 0 -5 4 0 1345.64 13.28 0 -5 4 1 895.55 11.16 0 -5 4 2 805.06 10.74 0 -2 2 3 1150.76 11.01 0 1 -10 -7 163.58 7.16 0 1 -9 -9 395.67 6.99 0 1 -2 -4 1808.55 12.44 0 2 -8 -3 1076.71 9.71 0 2 -8 -2 10.63 7.99 0 2 -8 2 64.10 8.17 0 2 -7 -4 763.78 8.88 0 2 -6 -4 978.98 9.40 0 2 -5 -3 47.10 7.27 0 2 -5 -2 1406.82 11.24 0 -10 5 7 43.67 8.13 0 -9 5 6 315.09 8.85 0 -8 3 15 365.07 7.71 0 -8 4 11 320.04 7.54 0 -8 5 -1 86.87 9.58 0 -8 5 3 -10.58 7.64 0 -8 5 4 372.83 9.58 0 -7 3 14 12.72 6.48 0 -5 2 14 172.74 6.81 0 -5 4 -1 748.02 12.06 0 -5 4 3 984.28 10.37 0 -5 4 4 431.48 9.57 0 1 -10 -6 235.00 7.29 0 1 -9 -8 12.11 6.61 0 1 -5 -9 245.50 6.71 0 1 -4 -8 467.49 7.04 0 1 -2 -3 2693.94 15.80 0 2 -8 -1 1082.89 9.75 0 2 -7 -3 545.81 8.46 0 2 -7 -2 684.86 9.70 0 2 -6 -3 75.71 7.32 0 2 -6 3 36.15 8.92 0 -9 5 7 52.14 7.89 0 -8 5 5 73.07 7.57 0 -6 0 20 340.04 7.84 0 -5 1 17 170.07 6.81 0 -5 4 5 889.69 9.68 0 -1 -1 -10 2438.83 11.69 0 1 -9 -7 557.17 8.16 0 1 -6 -9 80.65 6.26 0 2 -7 -1 409.67 8.88 0 2 -7 2 742.95 10.70 0 2 -6 -2 958.03 9.64 0 -9 5 8 184.34 7.25 0 -8 5 6 313.75 8.40 0 -8 5 7 21.01 7.66 0 -7 5 2 540.43 9.71 0 -6 4 9 686.21 8.11 0 -5 2 15 954.88 8.22 0 -5 4 6 853.55 9.51 0 -3 3 0 168.83 9.10 0 -3 3 2 7.05 7.40 0 -3 3 3 2622.90 13.82 0 1 -9 -6 150.62 7.22 0 1 -2 -2 2165.73 15.83 0 -9 5 9 36.68 6.65 0 -9 5 10 239.91 7.95 0 -8 5 8 408.98 8.50 0 -7 5 4 791.57 9.72 0 -7 5 5 138.10 7.99 0 -6 2 17 601.13 7.74 0 -6 4 10 650.37 7.95 0 -5 -1 21 46.94 6.71 0 -5 1 18 553.22 7.62 0 -5 4 7 1373.55 10.62 0 -4 3 10 137.03 7.76 0 -3 3 4 206.76 7.12 0 -3 3 5 2321.52 12.34 0 1 -10 -3 96.48 6.61 0 1 -9 -5 739.55 8.49 0 -6 3 15 490.11 7.41 0 -5 0 20 567.92 7.86 0 -2 -2 -13 609.06 7.86 0 ; _shelx_hkl_checksum 41457 _shelx_res_file ; TITL BG880 bg880.res created by SHELXL-2017/1 at 10:09:02 on 15-Jun-2018 CELL 0.71073 9.3157 8.4063 17.4678 90.000 93.222 90.000 ZERR 2.00 0.0006 0.0003 0.0010 0.000 0.005 0.000 LATT -1 SYMM X, -Y, Z+ 0.50000 SFAC C H N O CL W UNIT 56 66 8 8 2 2 FMAP 2 PLAN 5 OMIT -3 55 L.S. 20 OMIT -4 7 10 ACTA BOND $H CONF MPLA 4 O2 O3 N2 N4 W1 MPLA 4 C11 C12 O1 W1 Cl1 MPLA 5 N1 N2 C2 C3 C4 C1 C5 C11 C12 MPLA 5 N3 N4 C7 C8 C9 C6 C10 C11 C12 MPLA 4 C11 C12 O1 W1 Cl1 MPLA 6 C13 > C18 C12 MPLA 6 C19 > C24 C12 MPLA 5 C25 > C28 O4 REM Instructions for potential hydrogen bonds HTAB C5 O3 HTAB C10 O2 TEMP -120 SIZE 0.1 0.18 0.25 TWIN WGHT 0.014800 4.136500 BASF 0.48921 FVAR 0.52827 W1 6 1.041078 0.910506 0.751704 11.00000 0.03934 0.02519 = 0.01392 -0.00254 0.00483 -0.00067 CL1 5 0.982933 0.655041 0.703728 11.00000 0.06010 0.02975 = 0.02561 -0.00628 0.00427 -0.00427 O1 4 1.051916 1.075391 0.827120 11.00000 0.03422 0.02308 = 0.01180 -0.00028 0.00215 -0.00080 O2 4 0.948782 1.012465 0.676677 11.00000 0.05824 0.04754 = 0.01924 0.00949 0.00608 -0.00552 O3 4 1.217093 0.911888 0.726322 11.00000 0.04696 0.03927 = 0.02449 -0.00806 0.01561 0.00103 N1 3 1.058329 0.797273 0.929783 11.00000 0.02864 0.02173 = 0.01308 -0.00015 0.00536 0.00352 N2 3 1.114176 0.765328 0.859928 11.00000 0.03260 0.02392 = 0.01918 -0.00192 0.00285 0.00692 C1 1 1.057962 0.695059 1.064369 11.00000 0.04485 0.02660 = 0.01861 0.00623 0.00389 0.00724 AFIX 137 H1A 2 1.097589 0.790459 1.089940 11.00000 -1.50000 H1B 2 1.093916 0.600175 1.091828 11.00000 -1.50000 H1C 2 0.952780 0.697684 1.064274 11.00000 -1.50000 AFIX 0 C2 1 1.102692 0.690314 0.984375 11.00000 0.02937 0.02089 = 0.02369 0.00050 -0.00040 -0.00058 C3 1 1.191094 0.584899 0.948696 11.00000 0.03330 0.02263 = 0.02949 -0.00206 -0.00330 0.01045 AFIX 43 H3 2 1.239197 0.495853 0.971711 11.00000 -1.20000 AFIX 0 C4 1 1.196543 0.633853 0.872249 11.00000 0.02908 0.02761 = 0.03238 -0.00313 0.00155 0.00521 C5 1 1.278955 0.562311 0.810852 11.00000 0.05277 0.04112 = 0.03923 -0.00333 0.01416 0.02191 AFIX 137 H5A 2 1.225357 0.471908 0.788262 11.00000 -1.50000 H5B 2 1.372457 0.525620 0.832552 11.00000 -1.50000 H5C 2 1.293579 0.642069 0.771120 11.00000 -1.50000 AFIX 0 N3 3 0.828856 0.904460 0.892742 11.00000 0.02757 0.01659 = 0.01695 -0.00126 0.00166 0.00400 N4 3 0.827935 0.878914 0.815027 11.00000 0.03002 0.02093 = 0.01696 -0.00194 -0.00070 0.00164 C6 1 0.662998 0.911031 1.002140 11.00000 0.03235 0.03256 = 0.03342 -0.00027 0.00984 0.00055 AFIX 137 H6A 2 0.709143 0.822947 1.030853 11.00000 -1.50000 H6B 2 0.558954 0.907368 1.007703 11.00000 -1.50000 H6C 2 0.701219 1.012312 1.022199 11.00000 -1.50000 AFIX 0 C7 1 0.692937 0.896527 0.919469 11.00000 0.02840 0.01768 = 0.02979 0.00203 0.00764 0.00323 C8 1 0.604191 0.866064 0.856057 11.00000 0.02461 0.02786 = 0.03632 0.00192 -0.00100 0.00235 AFIX 43 H8 2 0.502680 0.854436 0.855246 11.00000 -1.20000 AFIX 0 C9 1 0.689030 0.855009 0.792559 11.00000 0.03281 0.02231 = 0.03134 0.00159 -0.00863 0.00166 C10 1 0.641650 0.823960 0.710639 11.00000 0.04525 0.04359 = 0.03632 -0.00552 -0.01672 0.00403 AFIX 137 H10A 2 0.700576 0.886772 0.677059 11.00000 -1.50000 H10B 2 0.540452 0.854172 0.701891 11.00000 -1.50000 H10C 2 0.652895 0.710605 0.699322 11.00000 -1.50000 AFIX 0 C11 1 0.963901 0.933359 0.935373 11.00000 0.02361 0.01872 = 0.01657 -0.00119 0.00282 0.00307 AFIX 13 H11 2 0.943686 0.948290 0.990534 11.00000 -1.20000 AFIX 0 C12 1 1.034734 1.088715 0.906571 11.00000 0.02879 0.01769 = 0.01188 0.00072 0.00390 -0.00084 C13 1 1.182427 1.121342 0.948083 11.00000 0.02403 0.01955 = 0.01812 0.00101 0.00396 0.00358 C14 1 1.200967 1.122769 1.027793 11.00000 0.02363 0.03486 = 0.01591 0.00075 0.00268 -0.00029 AFIX 43 H14 2 1.126007 1.085861 1.057938 11.00000 -1.20000 AFIX 0 C15 1 1.328591 1.177923 1.063441 11.00000 0.02403 0.04212 = 0.02225 -0.00135 0.00403 0.00034 AFIX 43 H15 2 1.340200 1.180257 1.117811 11.00000 -1.20000 AFIX 0 C16 1 1.439344 1.229727 1.019288 11.00000 0.02213 0.03620 = 0.03392 0.00063 0.00029 0.00053 AFIX 43 H16 2 1.525014 1.271422 1.043636 11.00000 -1.20000 AFIX 0 C17 1 1.425385 1.220864 0.940778 11.00000 0.02331 0.03702 = 0.03077 0.00361 0.00827 -0.00072 AFIX 43 H17 2 1.502847 1.252174 0.911013 11.00000 -1.20000 AFIX 0 C18 1 1.297884 1.166063 0.904750 11.00000 0.03431 0.02665 = 0.01632 -0.00041 0.00692 0.00377 AFIX 43 H18 2 1.289046 1.158918 0.850413 11.00000 -1.20000 AFIX 0 C19 1 0.933451 1.229834 0.920696 11.00000 0.02375 0.01673 = 0.01935 -0.00283 0.00130 -0.00057 C20 1 0.893184 1.333115 0.861184 11.00000 0.03612 0.02308 = 0.02038 0.00397 -0.00096 0.00202 AFIX 43 H20 2 0.926695 1.315324 0.811532 11.00000 -1.20000 AFIX 0 C21 1 0.804691 1.461642 0.873648 11.00000 0.03712 0.02283 = 0.03476 0.00454 -0.00471 0.00451 AFIX 43 H21 2 0.778288 1.531871 0.832634 11.00000 -1.20000 AFIX 0 C22 1 0.754302 1.488415 0.945870 11.00000 0.02924 0.01816 = 0.04347 -0.00382 0.00358 0.00399 AFIX 43 H22 2 0.691265 1.574893 0.953942 11.00000 -1.20000 AFIX 0 C23 1 0.796041 1.389218 1.005642 11.00000 0.02721 0.02105 = 0.03083 -0.00455 0.00475 -0.00047 AFIX 43 H23 2 0.764144 1.409418 1.055429 11.00000 -1.20000 AFIX 0 C24 1 0.884288 1.260062 0.993692 11.00000 0.02984 0.01978 = 0.02186 0.00004 0.00441 0.00179 AFIX 43 H24 2 0.911690 1.191508 1.035213 11.00000 -1.20000 AFIX 0 O4 4 0.597896 0.401680 0.618848 11.00000 0.04754 0.05472 = 0.03733 0.01682 0.00086 -0.01595 C25 1 0.673680 0.327401 0.682395 11.00000 0.04673 0.05753 = 0.03467 0.00401 -0.00104 -0.00129 AFIX 23 H25A 2 0.739923 0.403989 0.709070 11.00000 -1.20000 H25B 2 0.730398 0.236015 0.664967 11.00000 -1.20000 AFIX 0 C26 1 0.561755 0.272374 0.734794 11.00000 0.05381 0.04615 = 0.03395 0.00782 0.00249 0.00881 AFIX 23 H26A 2 0.539426 0.356030 0.772203 11.00000 -1.20000 H26B 2 0.592886 0.174829 0.762814 11.00000 -1.20000 AFIX 0 C27 1 0.433320 0.239551 0.679159 11.00000 0.04810 0.04337 = 0.04764 0.00279 0.01037 -0.00630 AFIX 23 H27A 2 0.439564 0.132565 0.655889 11.00000 -1.20000 H27B 2 0.341570 0.248830 0.704791 11.00000 -1.20000 AFIX 0 C28 1 0.447702 0.368849 0.620138 11.00000 0.04225 0.04720 = 0.04009 0.00757 0.00069 0.00434 AFIX 23 H28A 2 0.409240 0.332480 0.569121 11.00000 -1.20000 H28B 2 0.394489 0.465268 0.634551 11.00000 -1.20000 AFIX 0 HKLF 4 REM BG880 REM R1 = 0.0238 for 4924 Fo > 4sig(Fo) and 0.0273 for all 5165 data REM 348 parameters refined using 2 restraints END WGHT 0.0150 4.1107 REM Highest difference peak 0.937, deepest hole -1.065, 1-sigma level 0.089 Q1 1 1.0308 0.8302 0.7745 11.00000 0.05 0.94 Q2 1 1.0398 1.2581 0.7512 11.00000 0.05 0.84 Q3 1 1.0543 0.8316 0.7309 11.00000 0.05 0.82 Q4 1 0.9530 1.1107 0.6996 11.00000 0.05 0.64 Q5 1 1.1399 1.1101 0.8075 11.00000 0.05 0.62 ; _shelx_res_checksum 54599 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy W W1 1.04108(2) 0.91051(2) 0.75170(2) 0.02602(7) Uani d 1 Cl Cl1 0.9829(2) 0.6550(2) 0.70373(11) 0.0384(4) Uani d 1 O O1 1.0519(5) 1.0754(5) 0.8271(2) 0.0230(9) Uani d 1 O O2 0.9488(7) 1.0125(7) 0.6767(3) 0.0415(13) Uani d 1 O O3 1.2171(6) 0.9119(6) 0.7263(3) 0.0364(12) Uani d 1 N N1 1.0583(6) 0.7973(6) 0.9298(3) 0.0210(11) Uani d 1 N N2 1.1142(6) 0.7653(7) 0.8599(3) 0.0252(11) Uani d 1 C C1 1.0580(8) 0.6951(8) 1.0644(4) 0.0299(15) Uani d 1 H H1A 1.097589 0.790459 1.089940 0.045 Uiso calc 1 H H1B 1.093916 0.600175 1.091828 0.045 Uiso calc 1 H H1C 0.952780 0.697684 1.064274 0.045 Uiso calc 1 C C2 1.1027(7) 0.6903(7) 0.9844(4) 0.0247(13) Uani d 1 C C3 1.1911(7) 0.5849(8) 0.9487(4) 0.0287(14) Uani d 1 H H3 1.239197 0.495853 0.971711 0.034 Uiso calc 1 C C4 1.1965(7) 0.6339(8) 0.8722(4) 0.0297(15) Uani d 1 C C5 1.2790(9) 0.5623(10) 0.8109(5) 0.044(2) Uani d 1 H H5A 1.225357 0.471908 0.788262 0.066 Uiso calc 1 H H5B 1.372457 0.525620 0.832552 0.066 Uiso calc 1 H H5C 1.293579 0.642069 0.771120 0.066 Uiso calc 1 N N3 0.8289(5) 0.9045(6) 0.8927(3) 0.0204(10) Uani d 1 N N4 0.8279(6) 0.8789(6) 0.8150(3) 0.0227(11) Uani d 1 C C6 0.6630(8) 0.9110(9) 1.0021(4) 0.0325(15) Uani d 1 H H6A 0.709143 0.822947 1.030853 0.049 Uiso calc 1 H H6B 0.558954 0.907368 1.007703 0.049 Uiso calc 1 H H6C 0.701219 1.012312 1.022199 0.049 Uiso calc 1 C C7 0.6929(7) 0.8965(7) 0.9195(4) 0.0251(13) Uani d 1 C C8 0.6042(7) 0.8661(8) 0.8561(4) 0.0297(15) Uani d 1 H H8 0.502680 0.854436 0.855246 0.036 Uiso calc 1 C C9 0.6890(7) 0.8550(8) 0.7926(4) 0.0292(14) Uani d 1 C C10 0.6416(9) 0.8240(10) 0.7106(5) 0.0424(19) Uani d 1 H H10A 0.700576 0.886772 0.677059 0.064 Uiso calc 1 H H10B 0.540452 0.854172 0.701891 0.064 Uiso calc 1 H H10C 0.652895 0.710605 0.699322 0.064 Uiso calc 1 C C11 0.9639(6) 0.9334(7) 0.9354(4) 0.0196(12) Uani d 1 H H11 0.943686 0.948290 0.990534 0.023 Uiso calc 1 C C12 1.0347(6) 1.0887(7) 0.9066(3) 0.0194(11) Uani d 1 C C13 1.1824(6) 1.1213(7) 0.9481(4) 0.0205(12) Uani d 1 C C14 1.2010(7) 1.1228(8) 1.0278(4) 0.0247(14) Uani d 1 H H14 1.126007 1.085861 1.057938 0.030 Uiso calc 1 C C15 1.3286(7) 1.1779(9) 1.0634(4) 0.0294(15) Uani d 1 H H15 1.340200 1.180257 1.117811 0.035 Uiso calc 1 C C16 1.4393(7) 1.2297(9) 1.0193(4) 0.0308(15) Uani d 1 H H16 1.525014 1.271422 1.043636 0.037 Uiso calc 1 C C17 1.4254(7) 1.2209(8) 0.9408(4) 0.0301(15) Uani d 1 H H17 1.502847 1.252174 0.911013 0.036 Uiso calc 1 C C18 1.2979(7) 1.1661(8) 0.9048(4) 0.0256(13) Uani d 1 H H18 1.289046 1.158918 0.850413 0.031 Uiso calc 1 C C19 0.9335(6) 1.2298(7) 0.9207(4) 0.0199(12) Uani d 1 C C20 0.8932(7) 1.3331(8) 0.8612(4) 0.0266(13) Uani d 1 H H20 0.926695 1.315324 0.811532 0.032 Uiso calc 1 C C21 0.8047(8) 1.4616(8) 0.8736(4) 0.0318(15) Uani d 1 H H21 0.778288 1.531871 0.832634 0.038 Uiso calc 1 C C22 0.7543(7) 1.4884(8) 0.9459(5) 0.0302(15) Uani d 1 H H22 0.691265 1.574893 0.953942 0.036 Uiso calc 1 C C23 0.7960(7) 1.3892(7) 1.0056(4) 0.0262(13) Uani d 1 H H23 0.764144 1.409418 1.055429 0.031 Uiso calc 1 C C24 0.8843(7) 1.2601(8) 0.9937(4) 0.0237(13) Uani d 1 H H24 0.911690 1.191508 1.035213 0.028 Uiso calc 1 O O4 0.5979(6) 0.4017(7) 0.6188(3) 0.0466(14) Uani d 1 C C25 0.6737(9) 0.3274(12) 0.6824(5) 0.046(2) Uani d 1 H H25A 0.739923 0.403989 0.709070 0.056 Uiso calc 1 H H25B 0.730398 0.236015 0.664967 0.056 Uiso calc 1 C C26 0.5618(10) 0.2724(10) 0.7348(5) 0.045(2) Uani d 1 H H26A 0.539426 0.356030 0.772203 0.054 Uiso calc 1 H H26B 0.592886 0.174829 0.762814 0.054 Uiso calc 1 C C27 0.4333(9) 0.2396(10) 0.6792(5) 0.046(2) Uani d 1 H H27A 0.439564 0.132565 0.655889 0.055 Uiso calc 1 H H27B 0.341570 0.248830 0.704791 0.055 Uiso calc 1 C C28 0.4477(9) 0.3688(10) 0.6201(5) 0.0432(19) Uani d 1 H H28A 0.409240 0.332480 0.569121 0.052 Uiso calc 1 H H28B 0.394489 0.465268 0.634551 0.052 Uiso calc 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 W1 0.03934(12) 0.02519(10) 0.01392(10) -0.0007(2) 0.00483(7) -0.0025(2) Cl1 0.0601(12) 0.0297(8) 0.0256(9) -0.0043(8) 0.0043(8) -0.0063(7) O1 0.034(2) 0.023(2) 0.012(2) -0.001(2) 0.0021(17) -0.0003(17) O2 0.058(4) 0.048(3) 0.019(3) -0.006(3) 0.006(2) 0.009(2) O3 0.047(3) 0.039(3) 0.024(3) 0.001(2) 0.016(2) -0.008(2) N1 0.029(3) 0.022(2) 0.013(3) 0.004(2) 0.005(2) -0.0001(19) N2 0.033(3) 0.024(3) 0.019(3) 0.007(2) 0.003(2) -0.002(2) C1 0.045(4) 0.027(3) 0.019(3) 0.007(3) 0.004(3) 0.006(3) C2 0.029(3) 0.021(3) 0.024(3) -0.001(3) 0.000(3) 0.001(2) C3 0.033(3) 0.023(3) 0.029(4) 0.010(3) -0.003(3) -0.002(3) C4 0.029(3) 0.028(3) 0.032(4) 0.005(3) 0.002(3) -0.003(3) C5 0.053(5) 0.041(4) 0.039(5) 0.022(4) 0.014(4) -0.003(3) N3 0.028(3) 0.017(2) 0.017(3) 0.004(2) 0.0017(19) -0.001(2) N4 0.030(3) 0.021(3) 0.017(3) 0.002(2) -0.001(2) -0.002(2) C6 0.032(3) 0.033(3) 0.033(4) 0.001(3) 0.010(3) 0.000(3) C7 0.028(3) 0.018(3) 0.030(4) 0.003(3) 0.008(3) 0.002(3) C8 0.025(3) 0.028(3) 0.036(4) 0.002(3) -0.001(3) 0.002(3) C9 0.033(4) 0.022(3) 0.031(4) 0.002(3) -0.009(3) 0.002(3) C10 0.045(5) 0.044(4) 0.036(5) 0.004(4) -0.017(3) -0.006(3) C11 0.024(3) 0.019(3) 0.017(3) 0.003(2) 0.003(2) -0.001(2) C12 0.029(3) 0.018(3) 0.012(3) -0.001(2) 0.004(2) 0.001(2) C13 0.024(3) 0.020(3) 0.018(3) 0.004(2) 0.004(2) 0.001(2) C14 0.024(3) 0.035(4) 0.016(3) 0.000(3) 0.003(2) 0.001(3) C15 0.024(3) 0.042(4) 0.022(4) 0.000(3) 0.004(3) -0.001(3) C16 0.022(3) 0.036(4) 0.034(4) 0.001(3) 0.000(3) 0.001(3) C17 0.023(3) 0.037(4) 0.031(4) -0.001(3) 0.008(3) 0.004(3) C18 0.034(3) 0.027(3) 0.016(3) 0.004(3) 0.007(3) 0.000(2) C19 0.024(3) 0.017(3) 0.019(3) -0.001(2) 0.001(2) -0.003(2) C20 0.036(4) 0.023(3) 0.020(3) 0.002(3) -0.001(3) 0.004(2) C21 0.037(4) 0.023(3) 0.035(4) 0.005(3) -0.005(3) 0.005(3) C22 0.029(3) 0.018(3) 0.043(4) 0.004(3) 0.004(3) -0.004(3) C23 0.027(3) 0.021(3) 0.031(4) 0.000(2) 0.005(3) -0.005(3) C24 0.030(3) 0.020(3) 0.022(3) 0.002(3) 0.004(3) 0.000(2) O4 0.048(3) 0.055(3) 0.037(3) -0.016(3) 0.001(2) 0.017(3) C25 0.047(5) 0.058(5) 0.035(5) -0.001(4) -0.001(4) 0.004(4) C26 0.054(6) 0.046(4) 0.034(6) 0.009(4) 0.002(4) 0.008(3) C27 0.048(5) 0.043(4) 0.048(5) -0.006(4) 0.010(4) 0.003(4) C28 0.042(4) 0.047(5) 0.040(5) 0.004(4) 0.001(3) 0.008(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 3 -7 1 0.0840 -2 5 0 0.0840 1 0 6 0.1460 -1 0 -7 0.1220 -1 4 8 0.1210 -7 -2 0 0.0550 10 3 1 0.0570 1 -4 -8 0.1380 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_publ_flag O3 W1 O2 103.8(3) y O3 W1 O1 99.1(2) y O2 W1 O1 99.5(3) y O3 W1 N2 88.5(2) y O2 W1 N2 167.7(2) y O1 W1 N2 79.52(19) y O3 W1 N4 165.3(2) y O2 W1 N4 90.9(2) y O1 W1 N4 76.70(19) y N2 W1 N4 76.9(2) y O3 W1 Cl1 96.76(19) ? O2 W1 Cl1 95.0(2) ? O1 W1 Cl1 155.24(14) ? N2 W1 Cl1 82.04(15) ? N4 W1 Cl1 83.14(13) ? C12 O1 W1 137.0(4) ? C2 N1 N2 112.2(5) ? C2 N1 C11 129.6(5) ? N2 N1 C11 118.3(5) ? C4 N2 N1 104.9(5) ? C4 N2 W1 134.1(4) ? N1 N2 W1 120.7(4) ? C2 C1 H1A 109.5 ? C2 C1 H1B 109.5 ? H1A C1 H1B 109.5 ? C2 C1 H1C 109.5 ? H1A C1 H1C 109.5 ? H1B C1 H1C 109.5 ? N1 C2 C3 105.9(6) ? N1 C2 C1 123.6(6) ? C3 C2 C1 130.5(6) ? C2 C3 C4 107.2(6) ? C2 C3 H3 126.4 ? C4 C3 H3 126.4 ? N2 C4 C3 109.9(6) ? N2 C4 C5 121.9(7) ? C3 C4 C5 128.2(6) ? C4 C5 H5A 109.5 ? C4 C5 H5B 109.5 ? H5A C5 H5B 109.5 ? C4 C5 H5C 109.5 ? H5A C5 H5C 109.5 ? H5B C5 H5C 109.5 ? N4 N3 C7 111.9(5) ? N4 N3 C11 119.5(5) ? C7 N3 C11 128.6(5) ? C9 N4 N3 105.3(6) ? C9 N4 W1 134.9(5) ? N3 N4 W1 119.4(4) ? C7 C6 H6A 109.5 ? C7 C6 H6B 109.5 ? H6A C6 H6B 109.5 ? C7 C6 H6C 109.5 ? H6A C6 H6C 109.5 ? H6B C6 H6C 109.5 ? C8 C7 N3 105.1(6) ? C8 C7 C6 131.4(6) ? N3 C7 C6 123.4(6) ? C7 C8 C9 108.1(6) ? C7 C8 H8 125.9 ? C9 C8 H8 125.9 ? N4 C9 C8 109.6(6) ? N4 C9 C10 122.1(7) ? C8 C9 C10 128.3(7) ? C9 C10 H10A 109.5 ? C9 C10 H10B 109.5 ? H10A C10 H10B 109.5 ? C9 C10 H10C 109.5 ? H10A C10 H10C 109.5 ? H10B C10 H10C 109.5 ? N3 C11 N1 110.3(5) ? N3 C11 C12 110.3(5) ? N1 C11 C12 111.7(5) ? N3 C11 H11 108.2 ? N1 C11 H11 108.2 ? C12 C11 H11 108.2 ? O1 C12 C13 109.2(5) ? O1 C12 C19 108.8(5) ? C13 C12 C19 109.0(5) ? O1 C12 C11 108.9(5) ? C13 C12 C11 112.3(5) ? C19 C12 C11 108.6(5) ? C14 C13 C18 118.8(6) ? C14 C13 C12 121.9(5) ? C18 C13 C12 119.0(6) ? C15 C14 C13 120.3(6) ? C15 C14 H14 119.8 ? C13 C14 H14 119.8 ? C14 C15 C16 119.9(7) ? C14 C15 H15 120.1 ? C16 C15 H15 120.1 ? C17 C16 C15 120.3(6) ? C17 C16 H16 119.8 ? C15 C16 H16 119.8 ? C16 C17 C18 120.0(6) ? C16 C17 H17 120.0 ? C18 C17 H17 120.0 ? C17 C18 C13 120.4(6) ? C17 C18 H18 119.8 ? C13 C18 H18 119.8 ? C20 C19 C24 118.6(6) ? C20 C19 C12 120.1(5) ? C24 C19 C12 121.2(5) ? C21 C20 C19 120.5(6) ? C21 C20 H20 119.7 ? C19 C20 H20 119.7 ? C20 C21 C22 120.3(7) ? C20 C21 H21 119.9 ? C22 C21 H21 119.9 ? C23 C22 C21 119.7(6) ? C23 C22 H22 120.1 ? C21 C22 H22 120.1 ? C22 C23 C24 120.4(6) ? C22 C23 H23 119.8 ? C24 C23 H23 119.8 ? C23 C24 C19 120.4(6) ? C23 C24 H24 119.8 ? C19 C24 H24 119.8 ? C25 O4 C28 110.2(6) ? O4 C25 C26 106.2(7) ? O4 C25 H25A 110.5 ? C26 C25 H25A 110.5 ? O4 C25 H25B 110.5 ? C26 C25 H25B 110.5 ? H25A C25 H25B 108.7 ? C25 C26 C27 102.4(7) ? C25 C26 H26A 111.3 ? C27 C26 H26A 111.3 ? C25 C26 H26B 111.3 ? C27 C26 H26B 111.3 ? H26A C26 H26B 109.2 ? C28 C27 C26 102.0(7) ? C28 C27 H27A 111.4 ? C26 C27 H27A 111.4 ? C28 C27 H27B 111.4 ? C26 C27 H27B 111.4 ? H27A C27 H27B 109.2 ? O4 C28 C27 105.9(7) ? O4 C28 H28A 110.5 ? C27 C28 H28A 110.5 ? O4 C28 H28B 110.5 ? C27 C28 H28B 110.5 ? H28A C28 H28B 108.7 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_publ_flag W1 O3 1.723(5) y W1 O2 1.751(6) y W1 O1 1.911(4) y W1 N2 2.320(6) y W1 N4 2.342(6) y W1 Cl1 2.3572(18) y O1 C12 1.410(7) ? N1 C2 1.358(8) ? N1 N2 1.380(7) ? N1 C11 1.450(7) ? N2 C4 1.356(8) ? C1 C2 1.481(9) ? C1 H1A 0.9800 ? C1 H1B 0.9800 ? C1 H1C 0.9800 ? C2 C3 1.382(9) ? C3 C4 1.401(10) ? C3 H3 0.9500 ? C4 C5 1.481(9) ? C5 H5A 0.9800 ? C5 H5B 0.9800 ? C5 H5C 0.9800 ? N3 N4 1.374(8) ? N3 C7 1.376(8) ? N3 C11 1.446(8) ? N4 C9 1.346(9) ? C6 C7 1.491(10) ? C6 H6A 0.9800 ? C6 H6B 0.9800 ? C6 H6C 0.9800 ? C7 C8 1.369(10) ? C8 C9 1.401(10) ? C8 H8 0.9500 ? C9 C10 1.497(10) ? C10 H10A 0.9800 ? C10 H10B 0.9800 ? C10 H10C 0.9800 ? C11 C12 1.559(8) ? C11 H11 1.0000 ? C12 C13 1.543(9) ? C12 C19 1.544(8) ? C13 C14 1.393(9) ? C13 C18 1.401(8) ? C14 C15 1.390(9) ? C14 H14 0.9500 ? C15 C16 1.392(9) ? C15 H15 0.9500 ? C16 C17 1.372(10) ? C16 H16 0.9500 ? C17 C18 1.391(10) ? C17 H17 0.9500 ? C18 H18 0.9500 ? C19 C20 1.390(9) ? C19 C24 1.402(8) ? C20 C21 1.384(9) ? C20 H20 0.9500 ? C21 C22 1.389(10) ? C21 H21 0.9500 ? C22 C23 1.375(10) ? C22 H22 0.9500 ? C23 C24 1.385(9) ? C23 H23 0.9500 ? C24 H24 0.9500 ? O4 C25 1.426(10) ? O4 C28 1.428(10) ? C25 C26 1.499(11) ? C25 H25A 0.9900 ? C25 H25B 0.9900 ? C26 C27 1.524(13) ? C26 H26A 0.9900 ? C26 H26B 0.9900 ? C27 C28 1.509(11) ? C27 H27A 0.9900 ? C27 H27B 0.9900 ? C28 H28A 0.9900 ? C28 H28B 0.9900 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag C5 H5C O3 . 0.98 2.49 3.325(10) 142.8 yes C10 H10A O2 . 0.98 2.54 3.353(11) 140.0 yes C15 H15 O3 2_575 0.95 2.40 3.174(9) 138.7 yes C6 H6A O4 2_565 0.98 2.68 3.402(10) 130.8 yes C23 H23 O4 2_575 0.95 2.52 3.289(8) 138.4 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C2 N1 N2 C4 -0.2(7) C11 N1 N2 C4 -180.0(5) C2 N1 N2 W1 173.8(4) C11 N1 N2 W1 -5.9(7) N2 N1 C2 C3 0.1(8) C11 N1 C2 C3 179.8(6) N2 N1 C2 C1 -179.3(6) C11 N1 C2 C1 0.4(11) N1 C2 C3 C4 0.0(8) C1 C2 C3 C4 179.4(7) N1 N2 C4 C3 0.2(7) W1 N2 C4 C3 -172.6(5) N1 N2 C4 C5 -178.7(7) W1 N2 C4 C5 8.5(11) C2 C3 C4 N2 -0.2(8) C2 C3 C4 C5 178.6(8) C7 N3 N4 C9 0.2(7) C11 N3 N4 C9 179.6(5) C7 N3 N4 W1 173.9(4) C11 N3 N4 W1 -6.7(7) N4 N3 C7 C8 -0.4(7) C11 N3 C7 C8 -179.7(6) N4 N3 C7 C6 176.6(6) C11 N3 C7 C6 -2.7(10) N3 C7 C8 C9 0.5(7) C6 C7 C8 C9 -176.2(7) N3 N4 C9 C8 0.1(7) W1 N4 C9 C8 -172.2(4) N3 N4 C9 C10 179.5(6) W1 N4 C9 C10 7.2(10) C7 C8 C9 N4 -0.4(8) C7 C8 C9 C10 -179.7(7) N4 N3 C11 N1 -61.5(7) C7 N3 C11 N1 117.8(6) N4 N3 C11 C12 62.4(6) C7 N3 C11 C12 -118.4(6) C2 N1 C11 N3 -110.3(7) N2 N1 C11 N3 69.3(7) C2 N1 C11 C12 126.7(7) N2 N1 C11 C12 -53.7(7) W1 O1 C12 C13 110.3(6) W1 O1 C12 C19 -130.9(5) W1 O1 C12 C11 -12.7(8) N3 C11 C12 O1 -56.6(6) N1 C11 C12 O1 66.4(6) N3 C11 C12 C13 -177.7(5) N1 C11 C12 C13 -54.7(6) N3 C11 C12 C19 61.8(6) N1 C11 C12 C19 -175.3(5) O1 C12 C13 C14 -172.9(5) C19 C12 C13 C14 68.4(7) C11 C12 C13 C14 -51.9(7) O1 C12 C13 C18 13.5(7) C19 C12 C13 C18 -105.2(6) C11 C12 C13 C18 134.5(6) C18 C13 C14 C15 4.3(10) C12 C13 C14 C15 -169.3(6) C13 C14 C15 C16 -1.0(11) C14 C15 C16 C17 -2.5(11) C15 C16 C17 C18 2.7(11) C16 C17 C18 C13 0.7(10) C14 C13 C18 C17 -4.2(9) C12 C13 C18 C17 169.6(6) O1 C12 C19 C20 -9.5(8) C13 C12 C19 C20 109.5(6) C11 C12 C19 C20 -127.9(6) O1 C12 C19 C24 172.8(5) C13 C12 C19 C24 -68.2(7) C11 C12 C19 C24 54.4(8) C24 C19 C20 C21 -0.9(10) C12 C19 C20 C21 -178.8(6) C19 C20 C21 C22 -0.4(11) C20 C21 C22 C23 1.9(11) C21 C22 C23 C24 -2.0(10) C22 C23 C24 C19 0.7(10) C20 C19 C24 C23 0.8(10) C12 C19 C24 C23 178.6(6) C28 O4 C25 C26 -11.7(10) O4 C25 C26 C27 29.8(9) C25 C26 C27 C28 -35.7(9) C25 O4 C28 C27 -11.7(9) C26 C27 C28 O4 29.6(9)