#------------------------------------------------------------------------------ #$Date: 2019-07-06 06:56:05 +0300 (Sat, 06 Jul 2019) $ #$Revision: 216788 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/16/2021698.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021698 loop_ _publ_author_name 'Marandi, Farzin' 'Moeini, Keyvan' 'Mardani, Zahra' 'Krautscheid, Harald' _publ_section_title ; Spectral, structural and theoretical study of the effects of thiocyanato and dicyanamido ligands on the geometry of PbII complexes containing a triazinic ligand ; _journal_coeditor_code YP3186 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section C Structural Chemistry' _journal_paper_doi 10.1107/S2053229619008301 _journal_volume 75 _journal_year 2019 _chemical_formula_iupac 'C16 H10 N4 O2' _chemical_formula_moiety 'C16 H10 N4 O2' _chemical_formula_sum 'C16 H10 N4 O2' _chemical_formula_weight 290.28 _chemical_name_systematic ; 5,6-Bis(furan-2-yl)-3-(pyridin-2-yl)-1,2,4-triazine ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 92.350(8) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.0313(5) _cell_length_b 10.2649(6) _cell_length_c 14.3901(10) _cell_measurement_reflns_used 4572 _cell_measurement_temperature 213(2) _cell_measurement_theta_max 27.8 _cell_measurement_theta_min 2.3 _cell_volume 1332.92(14) _computing_cell_refinement ; IPDS (Stoe & Cie, 2016) ; _computing_data_collection ; IPDS (Stoe & Cie, 2016) ; _computing_data_reduction ; IPDS (Stoe & Cie, 2016) ; _computing_molecular_graphics ; ORTEPIII (Burnett & Johnson, 1996), ORTEP-3 for Windows (Farrugia, 2012) and DIAMOND (Bergerhof et al., 1996) ; _computing_publication_material ; SHELXL2014 (Sheldrick, 2015) ; _computing_structure_refinement ; SHELXL2014 (Sheldrick, 2015) ; _computing_structure_solution ; SHELXS97 (Sheldrick, 2008) ; _diffrn_ambient_temperature 213(2) _diffrn_measured_fraction_theta_full 0.987 _diffrn_measured_fraction_theta_max 0.985 _diffrn_measurement_device_type 'Stoe IPDS-I' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0327 _diffrn_reflns_av_unetI/netI 0.0516 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 9209 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.999 _diffrn_reflns_theta_min 2.438 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 0.100 _exptl_absorpt_correction_type none _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.447 _exptl_crystal_description fragment _exptl_crystal_F_000 600 _exptl_crystal_size_max 0.450 _exptl_crystal_size_mid 0.300 _exptl_crystal_size_min 0.250 _refine_diff_density_max 0.136 _refine_diff_density_min -0.180 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.790 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 199 _refine_ls_number_reflns 2582 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.790 _refine_ls_R_factor_all 0.0517 _refine_ls_R_factor_gt 0.0294 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0340P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0598 _refine_ls_wR_factor_ref 0.0629 _reflns_number_gt 1612 _reflns_number_total 2582 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yp3186sup1.cif _cod_data_source_block DFPT _cod_database_code 2021698 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.956 _shelx_estimated_absorpt_t_max 0.975 _shelx_hkl_file ; -7 -9 -6 8.26 8.53 2-0.40651-0.15753-0.59672-0.02710 0.67416-0.99283 -7 -8 -6 13.62 8.39 2-0.40651-0.15797-0.59672 0.04174 0.67416-0.99217 -7 5 8 149.67 8.29 2-0.40651-0.12822-0.59672 0.94550 0.67416-0.30279 -5 -11 -6 -2.86 8.60 2-0.40651-0.00016-0.59672-0.16477 0.67416-0.98570 -5 3 2 166.54 8.59 2-0.40651 0.01604-0.59672 0.80421 0.67416-0.59200 -3 -9 -6 23.74 6.44 2-0.40651 0.15756-0.59672-0.02662 0.67416-0.97986 -3 -8 -6 88.52 6.92 2-0.40651 0.15761-0.59672 0.04161 0.67416-0.97926 -2 -5 -5 19.70 5.05 2-0.40651 0.23762-0.59672 0.24960 0.67416-0.92792 -2 -3 -4 525.21 12.10 2-0.40651 0.23988-0.59672 0.38782 0.67416-0.87897 -2 5 10 6.03 4.85 2-0.40651 0.26927-0.59672 0.94245 0.67416-0.18705 -2 5 17 3.61 8.50 2-0.40651 0.28510-0.59672 0.94774 0.67416 0.15774 -1 4 7 654.39 11.39 2-0.40651 0.34223-0.59672 0.87368 0.67416-0.33117 0 -12 -4 6.08 8.13 2-0.40651 0.39695-0.59672-0.23319 0.67416-0.87082 0 4 18 7.46 8.79 2-0.40651 0.44405-0.59672 0.87512 0.67416 0.21344 2 -5 -2 186.03 7.90 2-0.40651 0.55940-0.59672 0.24953 0.67416-0.76662 2 3 13 10.22 6.32 2-0.40651 0.59110-0.59672 0.80549 0.67416-0.02661 2 3 14 7.37 6.35 2-0.40651 0.59292-0.59672 0.80582 0.67416 0.02170 2 3 15 0.35 6.35 2-0.40651 0.59302-0.59672 0.80444 0.67416 0.07141 3 2 12 425.20 10.61 2-0.40651 0.66876-0.59672 0.73713 0.67416-0.07318 3 2 15 5.30 6.33 2-0.40651 0.67497-0.59672 0.73703 0.67416 0.07505 4 -9 0 47.81 6.84 2-0.40651 0.72070-0.59672-0.02626 0.67416-0.66250 4 -8 0 4.64 4.95 2-0.40651 0.72060-0.59672 0.04381 0.67416-0.66172 5 -12 3 0.33 8.70 2-0.40651 0.80591-0.59672-0.23279 0.67416-0.51067 -10 -5 -4 2.09 11.91 3-0.40617-0.39001-0.60377 0.25791 0.66754-0.89861 -10 4 8 10.19 12.20 3-0.40617-0.36640-0.60377 0.88342 0.66754-0.30512 -9 -6 -5 -0.59 11.75 3-0.40617-0.31242-0.60377 0.18777 0.66754-0.94279 -8 5 9 17.19 9.29 3-0.40617-0.20572-0.60377 0.94832 0.66754-0.24796 -7 -7 -6 85.68 9.96 3-0.40617-0.15688-0.60377 0.11888 0.66754-0.98578 -7 -4 -5 487.25 13.72 3-0.40617-0.15596-0.60377 0.32643 0.66754-0.93720 -6 -6 -6 281.14 11.32 3-0.40617-0.07824-0.60377 0.18756 0.66754-0.98113 -6 -2 -4 4.05 6.80 3-0.40617-0.07450-0.60377 0.46436 0.66754-0.88388 -5 -6 -6 43.72 9.15 3-0.40617-0.00007-0.60377 0.18786 0.66754-0.98100 -4 -11 -6 7.53 11.82 3-0.40617 0.07907-0.60377-0.15806 0.66754-0.98053 -4 -6 -6 1564.21 17.87 3-0.40617 0.07866-0.60377 0.18820 0.66754-0.97457 -4 -2 -4 147.49 9.47 3-0.40617 0.08302-0.60377 0.46453 0.66754-0.87660 -4 5 8 605.45 11.97 3-0.40617 0.10725-0.60377 0.95068 0.66754-0.28447 -3 -10 -6 -2.13 9.05 3-0.40617 0.15778-0.60377-0.08873 0.66754-0.97641 -3 -7 -6 -4.06 6.79 3-0.40617 0.15771-0.60377 0.11865 0.66754-0.97284 -3 -4 -5 7.85 6.80 3-0.40617 0.15975-0.60377 0.32647 0.66754-0.92366 -3 4 5 184.99 8.95 3-0.40617 0.17920-0.60377 0.88052 0.66754-0.42935 -3 5 9 349.53 10.18 3-0.40617 0.18832-0.60377 0.95185 0.66754-0.23203 -2 4 6 847.28 14.35 3-0.40617 0.26055-0.60377 0.88340 0.66754-0.37673 -2 5 11 21.52 8.66 3-0.40617 0.27129-0.60377 0.95157 0.66754-0.13140 -1 -11 -5 -2.01 8.93 3-0.40617 0.31780-0.60377-0.15834 0.66754-0.92143 0 4 10 3.68 6.73 3-0.40617 0.42716-0.60377 0.88321 0.66754-0.17406 0 4 17 8.85 11.77 3-0.40617 0.44153-0.60377 0.88425 0.66754 0.17157 2 2 7 393.37 11.28 3-0.40617 0.57738-0.60377 0.74207 0.66754-0.31510 3 -12 -1 -2.26 11.70 3-0.40617 0.63983-0.60377-0.22638 0.66754-0.70819 3 1 7 19.38 7.21 3-0.40617 0.65592-0.60377 0.67376 0.66754-0.31181 3 2 13 139.16 10.17 3-0.40617 0.66816-0.60377 0.74260 0.66754-0.01616 3 2 14 54.62 9.38 3-0.40617 0.67024-0.60377 0.74207 0.66754 0.03256 4 -10 0 8.71 9.03 3-0.40617 0.72148-0.60377-0.08843 0.66754-0.65696 4 -7 0 8.14 6.93 3-0.40617 0.71974-0.60377 0.11876 0.66754-0.65384 5 -10 2 -1.82 9.02 3-0.40617 0.80455-0.60377-0.08755 0.66754-0.55429 5 -8 2 93.16 9.95 3-0.40617 0.80657-0.60377 0.05075 0.66754-0.55546 5 -1 10 10.09 8.66 3-0.40617 0.82187-0.60377 0.53566 0.66754-0.15894 -6 5 8 2.35 6.25 3-0.40582-0.05151-0.61079 0.95720 0.66087-0.28416 -5 5 8 42.49 6.62 3-0.40582 0.02705-0.61079 0.95819 0.66087-0.28076 -3 -11 -6 -3.25 8.20 3-0.40582 0.15838-0.61079-0.15051 0.66087-0.96910 -2 5 12 3.25 6.05 3-0.40582 0.27122-0.61079 0.95817 0.66087-0.07446 -2 5 14 15.06 6.49 3-0.40582 0.27676-0.61079 0.96057 0.66087 0.02520 -2 5 15 4.68 6.47 3-0.40582 0.27816-0.61079 0.95834 0.66087 0.07408 -2 5 16 -0.11 8.23 3-0.40582 0.27822-0.61079 0.95399 0.66087 0.12295 -1 -6 -5 -2.00 4.77 3-0.40582 0.31702-0.61079 0.19487 0.66087-0.91403 0 -5 -4 466.69 10.36 3-0.40582 0.39864-0.61079 0.26462 0.66087-0.86044 1 -13 -3 -0.18 8.59 3-0.40582 0.47985-0.61079-0.28905 0.66087-0.80933 1 -10 -4 12.31 6.35 3-0.40582 0.47640-0.61079-0.08097 0.66087-0.85584 1 -9 -4 9.60 6.12 3-0.40582 0.47769-0.61079-0.01209 0.66087-0.85851 1 -8 -4 160.62 6.79 3-0.40582 0.47757-0.61079 0.05720 0.66087-0.85657 1 -3 -2 195.12 9.34 3-0.40582 0.48137-0.61079 0.40241 0.66087-0.75725 1 3 8 213.61 7.84 3-0.40582 0.50018-0.61079 0.81756 0.66087-0.26108 2 -13 -2 -1.71 8.56 3-0.40582 0.55941-0.61079-0.28857 0.66087-0.75488 2 -10 -3 5.79 6.27 3-0.40582 0.55810-0.61079-0.08100 0.66087-0.80292 2 -9 -3 299.72 8.94 3-0.40582 0.55874-0.61079-0.01178 0.66087-0.80609 2 -8 -3 8.70 4.91 3-0.40582 0.55799-0.61079 0.05683 0.66087-0.80452 -11 2 4 12.52 14.87 3-0.40583-0.45312-0.61049 0.74920 0.66171-0.49954 -10 -3 -3 -0.14 11.31 3-0.40583-0.38865-0.61049 0.40327 0.66171-0.84269 -8 3 3 12.66 10.69 3-0.40583-0.21850-0.61049 0.81833 0.66171-0.53828 6 -11 5 3.82 15.09 3-0.40583 0.88851-0.61049-0.14995 0.66171-0.39755 -10 3 5 4.08 10.38 4-0.40547-0.37219-0.61731 0.82467 0.65543-0.43877 -9 4 7 47.44 9.78 4-0.40547-0.29095-0.61731 0.89835 0.65543-0.33864 -8 -8 -6 1.54 12.20 4-0.40547-0.23658-0.61731 0.06408 0.65543-0.97808 -8 5 10 10.37 11.60 4-0.40547-0.20503-0.61731 0.96216 0.65543-0.18563 -7 -6 -6 6.77 8.87 4-0.40547-0.15710-0.61731 0.20095 0.65543-0.97195 -7 4 5 35.52 9.00 4-0.40547-0.13666-0.61731 0.89418 0.65543-0.42927 -7 5 9 11.48 9.06 4-0.40547-0.12854-0.61731 0.96471 0.65543-0.23255 -4 5 9 19.29 7.11 4-0.40547 0.10867-0.61731 0.96696 0.65543-0.22319 -3 5 10 6.08 6.85 4-0.40547 0.18937-0.61731 0.96512 0.65543-0.16984 -3 5 17 7.82 12.13 4-0.40547 0.20242-0.61731 0.96523 0.65543 0.17530 -2 -10 -6 19.20 9.02 4-0.40547 0.23583-0.61731-0.07441 0.65543-0.95886 -2 -9 -6 9.56 8.76 4-0.40547 0.23608-0.61731-0.00530 0.65543-0.96143 -2 -8 -6 5.35 8.59 4-0.40547 0.23553-0.61731 0.06315 0.65543-0.95935 -2 5 13 54.47 9.20 4-0.40547 0.27321-0.61731 0.96124 0.65543-0.01910 -1 -12 -5 15.22 11.84 4-0.40547 0.31813-0.61731-0.21401 0.65543-0.91062 -1 4 8 140.78 8.23 4-0.40547 0.34380-0.61731 0.89641 0.65543-0.26262 0 -13 -4 -0.52 12.13 4-0.40547 0.39913-0.61731-0.28257 0.65543-0.85630 0 -9 -5 42.00 8.99 4-0.40547 0.39554-0.61731-0.00589 0.65543-0.90176 0 3 6 1487.80 18.31 4-0.40547 0.41793-0.61731 0.82661 0.65543-0.35701 0 4 11 123.36 7.97 4-0.40547 0.42725-0.61731 0.89432 0.65543-0.11147 0 4 12 1.29 8.55 4-0.40547 0.43107-0.61731 0.89825 0.65543-0.06314 0 4 15 -0.22 8.86 4-0.40547 0.43607-0.61731 0.89723 0.65543 0.08604 0 4 16 10.74 9.26 4-0.40547 0.43528-0.61731 0.89269 0.65543 0.13470 1 -11 -4 5.49 8.95 4-0.40547 0.47556-0.61731-0.14334 0.65543-0.84848 1 -7 -4 20.58 6.87 4-0.40547 0.47530-0.61731 0.13263 0.65543-0.84951 1 2 5 1.70 7.08 4-0.40547 0.49478-0.61731 0.75603 0.65543-0.40569 1 3 18 -3.27 12.10 4-0.40547 0.52010-0.61731 0.82650 0.65543 0.23722 2 -7 -3 3.78 6.80 4-0.40547 0.55682-0.61731 0.13174 0.65543-0.79661 2 -2 0 35.28 9.57 4-0.40547 0.56361-0.61731 0.47857 0.65543-0.64851 3 -9 -2 589.28 13.07 4-0.40547 0.63675-0.61731-0.00530 0.65543-0.74477 4 -11 0 82.19 10.09 4-0.40547 0.72272-0.61731-0.14403 0.65543-0.64676 4 0 8 85.09 8.49 4-0.40547 0.73527-0.61731 0.61722 0.65543-0.24758 5 -11 2 4.05 11.83 4-0.40547 0.80501-0.61731-0.14382 0.65543-0.54315 5 -7 2 81.05 8.25 4-0.40547 0.80580-0.61731 0.13387 0.65543-0.54344 5 -5 3 95.79 9.41 4-0.40547 0.80565-0.61731 0.27184 0.65543-0.49247 5 -1 15 39.41 12.14 4-0.40547 0.83153-0.61731 0.55104 0.65543 0.10117 5 -1 16 20.63 12.30 4-0.40547 0.82830-0.61731 0.54794 0.65543 0.14948 6 -3 15 1.65 12.22 4-0.40547 0.90878-0.61731 0.41154 0.65543 0.10343 -8 5 11 29.66 8.86 4-0.40513-0.20298-0.62379 0.97116 0.64995-0.13065 -4 4 5 0.13 4.73 4-0.40513 0.09880-0.62379 0.90155 0.64995-0.41461 -3 -12 -6 9.83 8.68 4-0.40513 0.15744-0.62379-0.20710 0.64995-0.95898 -3 -6 -6 108.14 6.29 4-0.40513 0.15674-0.62379 0.20823 0.64995-0.95781 -3 5 16 2.76 8.36 4-0.40513 0.20126-0.62379 0.97205 0.64995 0.13135 -2 -11 -6 10.15 6.52 4-0.40513 0.23509-0.62379-0.13735 0.64995-0.95233 -1 -1 -2 24.95 7.42 4-0.40513 0.32205-0.62379 0.55383 0.64995-0.75282 0 -10 -5 16.80 6.39 4-0.40513 0.39476-0.62379-0.06853 0.64995-0.89977 0 -8 -5 38.58 5.28 4-0.40513 0.39628-0.62379 0.07036 0.64995-0.89856 0 -3 -3 14.62 5.56 4-0.40513 0.39877-0.62379 0.41688 0.64995-0.79904 0 4 13 8.96 6.11 4-0.40513 0.43115-0.62379 0.90187 0.64995-0.00728 0 4 14 15.54 6.46 4-0.40513 0.43242-0.62379 0.90140 0.64995 0.04154 2 -11 -3 38.31 6.82 4-0.40513 0.55792-0.62379-0.13772 0.64995-0.79563 3 -13 -1 8.69 8.71 4-0.40513 0.63940-0.62379-0.27543 0.64995-0.69224 3 -10 -2 4.77 6.22 4-0.40513 0.63810-0.62379-0.06793 0.64995-0.74083 3 -8 -2 0.89 4.82 4-0.40513 0.63746-0.62379 0.07086 0.64995-0.74076 -7 -1 -3 1.19 9.61 4-0.40556-0.15242-0.61706 0.54785 0.65596-0.82684 5 -2 7 47.17 11.09 4-0.40556 0.81366-0.61706 0.47896 0.65596-0.29508 -9 -2 -3 8.21 10.83 4-0.40523-0.31060-0.62375 0.48598 0.64981-0.82752 -9 3 4 6.81 10.88 4-0.40523-0.29631-0.62375 0.83135 0.64981-0.47969 -3 -1 -3 41.73 9.69 4-0.40523 0.16272-0.62375 0.55390 0.64981-0.80785 5 -1 11 4.26 10.61 4-0.40523 0.82103-0.62375 0.55655 0.64981-0.09133 6 -3 11 61.41 12.34 4-0.40523 0.89981-0.62375 0.41746 0.64981-0.08841 6 -3 14 30.71 14.94 4-0.40523 0.90774-0.62375 0.41862 0.64981 0.05986 -11 -4 -3 1.93 12.15 5-0.40493-0.46821-0.63017 0.35314 0.64422-0.82714 -10 4 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161.48 10.33 9-0.40231-0.08601-0.67994 0.26458 0.59591-0.96271 -6 -4 -6 9.58 6.96 9-0.40231-0.08233-0.67994 0.40314 0.59591-0.91326 -5 3 3 53.41 7.59 9-0.40231 0.01375-0.67994 0.88560 0.59591-0.46186 -4 -6 -7 72.39 7.68 9-0.40231 0.07222-0.67994 0.26469 0.59591-0.95758 -4 4 7 5.69 6.78 9-0.40231 0.10021-0.67994 0.95824 0.59591-0.26241 -3 4 8 144.96 8.23 9-0.40231 0.18155-0.67994 0.95881 0.59591-0.21028 -3 4 17 6.45 11.84 9-0.40231 0.19852-0.67994 0.95434 0.59591 0.23341 -2 -12 -7 9.04 12.07 9-0.40231 0.22993-0.67994-0.15103 0.59591-0.95176 -2 4 10 17.57 6.95 9-0.40231 0.26440-0.67994 0.95715 0.59591-0.10813 -2 4 14 34.86 9.02 9-0.40231 0.27237-0.67994 0.95936 0.59591 0.08970 -1 -4 -5 148.95 8.65 9-0.40231 0.31343-0.67994 0.40232 0.59591-0.84653 -1 3 6 3169.62 25.38 9-0.40231 0.33492-0.67994 0.88772 0.59591-0.30182 -1 3 18 -3.32 12.04 9-0.40231 0.36016-0.67994 0.89168 0.59591 0.29100 0 -12 -6 5.74 11.85 9-0.40231 0.38921-0.67994-0.15076 0.59591-0.89276 0 -8 -6 3.71 6.82 9-0.40231 0.39057-0.67994 0.12689 0.59591-0.89542 1 -7 -5 29.41 7.01 9-0.40231 0.47068-0.67994 0.19560 0.59591-0.84078 2 -7 -4 112.00 7.88 9-0.40231 0.55188-0.67994 0.19591 0.59591-0.78786 2 -5 -3 48.98 7.28 9-0.40231 0.55418-0.67994 0.33432 0.59591-0.73941 2 0 3 -0.01 7.81 9-0.40231 0.56587-0.67994 0.68091 0.59591-0.44181 2 1 18 5.30 12.01 9-0.40231 0.59743-0.67994 0.75376 0.59591 0.30017 3 -12 -3 28.53 12.16 9-0.40231 0.63160-0.67994-0.15029 0.59591-0.73506 3 -8 -3 276.64 9.74 9-0.40231 0.63390-0.67994 0.12634 0.59591-0.73717 3 0 18 -1.54 12.20 9-0.40231 0.67651-0.67994 0.68381 0.59591 0.30289 3 1 11 51.23 7.34 9-0.40231 0.65974-0.67994 0.74885 0.59591-0.04312 3 1 12 10.38 8.66 9-0.40231 0.66220-0.67994 0.74972 0.59591 0.00658 3 1 13 77.83 9.44 9-0.40231 0.66298-0.67994 0.74881 0.59591 0.05522 4 -5 0 194.57 9.84 9-0.40231 0.71638-0.67994 0.33398 0.59591-0.58352 4 -4 1 0.74 6.66 9-0.40231 0.71998-0.67994 0.40438 0.59591-0.53485 6 -11 3 7.91 12.25 9-0.40231 0.88115-0.67994-0.08031 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0.90118 0.58341-0.34146 -1 -11 -7 42.06 10.81 10-0.40157 0.30895-0.69231-0.06961 0.58341-0.93570 -1 -9 -7 161.29 9.86 10-0.40157 0.30897-0.69231 0.06906 0.58341-0.93568 -1 2 3 9518.38 54.51 10-0.40157 0.32664-0.69231 0.83069 0.58341-0.43786 -1 3 17 60.88 12.22 10-0.40157 0.35726-0.69231 0.90340 0.58341 0.25385 0 -7 -6 87.47 7.72 10-0.40157 0.38940-0.69231 0.20773 0.58341-0.88132 0 3 10 251.82 9.19 10-0.40157 0.42181-0.69231 0.90105 0.58341-0.08916 0 3 13 1.26 8.57 10-0.40157 0.42852-0.69231 0.90325 0.58341 0.05884 0 3 14 32.83 9.05 10-0.40157 0.42843-0.69231 0.89968 0.58341 0.10817 1 2 7 587.17 12.84 10-0.40157 0.49511-0.69231 0.83187 0.58341-0.23286 2 1 6 7.51 7.43 10-0.40157 0.57117-0.69231 0.76410 0.58341-0.27877 3 -7 -3 3.03 6.76 10-0.40157 0.63116-0.69231 0.20784 0.58341-0.72202 3 -4 -1 248.87 10.81 10-0.40157 0.63668-0.69231 0.41541 0.58341-0.62444 3 -3 0 74.21 8.92 10-0.40157 0.63761-0.69231 0.48469 0.58341-0.57365 4 -11 -2 -2.13 9.07 10-0.40157 0.71196-0.69231-0.06805 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11-0.40044-0.13337-0.70429 0.98052 0.57063-0.14769 -6 -8 -8 1.02 9.22 11-0.40044-0.08908-0.70429 0.14999 0.57063-0.98734 -6 -5 -7 189.67 10.58 11-0.40044-0.08637-0.70429 0.35680 0.57063-0.93271 -6 4 8 3.41 8.59 11-0.40044-0.05633-0.70429 0.97973 0.57063-0.19361 -5 -5 -7 74.27 7.76 11-0.40044-0.00746-0.70429 0.35769 0.57063-0.93330 -5 4 8 -0.66 6.82 11-0.40044 0.02155-0.70429 0.98125 0.57063-0.19050 -5 4 16 -0.79 12.01 11-0.40044 0.03748-0.70429 0.97855 0.57063 0.20437 -4 -5 -7 2.07 6.94 11-0.40044 0.07131-0.70429 0.35739 0.57063-0.92768 -4 4 15 18.27 10.42 11-0.40044 0.11477-0.70429 0.98150 0.57063 0.15894 -3 4 10 89.27 7.70 11-0.40044 0.18316-0.70429 0.97893 0.57063-0.08566 -3 4 11 95.18 9.32 11-0.40044 0.18532-0.70429 0.98198 0.57063-0.03620 -3 4 12 13.83 8.54 11-0.40044 0.18734-0.70429 0.98256 0.57063 0.01331 -3 4 13 11.40 8.85 11-0.40044 0.18902-0.70429 0.98074 0.57063 0.06215 -2 -6 -7 4.89 6.87 11-0.40044 0.22790-0.70429 0.28833 0.57063-0.92042 -2 -1 -3 103.00 10.30 11-0.40044 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0.35854 0.57063-0.66069 3 0 6 -1.25 6.78 11-0.40044 0.64808-0.70429 0.70483 0.57063-0.26507 4 -8 -2 28.16 7.24 11-0.40044 0.71180-0.70429 0.15108 0.57063-0.65776 4 -6 -1 76.98 7.87 11-0.40044 0.71474-0.70429 0.28960 0.57063-0.60858 4 -1 16 39.19 12.09 11-0.40044 0.74613-0.70429 0.63530 0.57063 0.23191 5 -8 0 10.35 8.78 11-0.40044 0.79484-0.70429 0.15141 0.57063-0.55635 5 -2 9 48.69 8.11 11-0.40044 0.81220-0.70429 0.56687 0.57063-0.11068 5 -2 13 -0.51 8.99 11-0.40044 0.82147-0.70429 0.56882 0.57063 0.08730 5 -2 14 0.84 9.13 11-0.40044 0.81967-0.70429 0.56461 0.57063 0.13580 6 -10 2 3.62 11.47 11-0.40044 0.87370-0.70429 0.01282 0.57063-0.45177 -7 4 10 2.60 6.22 11-0.39973-0.13226-0.71003 0.98728 0.56416-0.09138 -7 4 14 5.01 8.51 11-0.39973-0.12511-0.71003 0.98581 0.56416 0.10548 -6 4 15 11.21 8.76 11-0.39973-0.04435-0.71003 0.98614 0.56416 0.15767 -5 -7 -8 1.37 6.28 11-0.39973-0.01137-0.71003 0.22431 0.56416-0.97414 -5 4 15 -0.05 8.19 11-0.39973 0.03523-0.71003 0.98640 0.56416 0.16207 -4 4 9 4.62 4.84 11-0.39973 0.10185-0.71003 0.98558 0.56416-0.13196 -4 4 14 2.42 6.35 11-0.39973 0.11190-0.71003 0.98765 0.56416 0.11532 -3 -8 -8 6.93 6.22 11-0.39973 0.14775-0.71003 0.15657 0.56416-0.97001 -2 -11 -8 -0.16 8.33 11-0.39973 0.22448-0.71003-0.05114 0.56416-0.96353 -2 -10 -8 1.37 6.36 11-0.39973 0.22464-0.71003 0.01794 0.56416-0.96469 -1 -7 -7 21.18 5.09 11-0.39973 0.30648-0.71003 0.22513 0.56416-0.91219 0 2 5 1147.45 17.16 11-0.39973 0.40976-0.71003 0.84985 0.56416-0.31639 0 2 18 8.84 8.50 11-0.39973 0.43439-0.71003 0.84687 0.56416 0.32519 1 -12 -6 -0.83 8.33 11-0.39973 0.46577-0.71003-0.12001 0.56416-0.85764 1 2 8 3.82 4.82 11-0.39973 0.49455-0.71003 0.84991 0.56416-0.16521 1 2 15 14.10 6.44 11-0.39973 0.50770-0.71003 0.84717 0.56416 0.18003 2 -12 -5 25.72 8.59 11-0.39973 0.54730-0.71003-0.12058 0.56416-0.80593 2 1 16 9.80 6.49 11-0.39973 0.58941-0.71003 0.78094 0.56416 0.23262 3 -11 -4 2.72 6.41 11-0.39973 0.62767-0.71003-0.05084 0.56416-0.75147 3 -10 -4 13.22 6.42 11-0.39973 0.62809-0.71003 0.01862 0.56416-0.75262 -5 1 -1 179.44 22.78 9-0.40205 0.00472-0.68027 0.74927 0.59574-0.66066 6 -5 6 5.49 17.51 9-0.40205 0.88729-0.68027 0.33491 0.59574-0.28151 -8 -1 -3 125.69 15.49 11-0.40028-0.23676-0.70421 0.63441 0.57040-0.74404 -9 2 3 168.84 13.29 11-0.39969-0.30449-0.71015 0.84804 0.56389-0.44437 -5 2 1 24.12 8.86 11-0.39969 0.00742-0.71015 0.84765 0.56389-0.52961 5 -5 2 185.62 12.11 11-0.39969 0.79741-0.71015 0.36467 0.56389-0.44976 6 -4 13 2.75 14.18 11-0.39969 0.89885-0.71015 0.43502 0.56389 0.09738 -10 3 9 10.61 11.99 12-0.39896-0.37067-0.71590 0.91944 0.55724-0.14272 -9 -7 -7 -0.80 12.32 12-0.39896-0.32421-0.71590 0.23001 0.55724-0.92955 -9 -5 -6 0.42 11.66 12-0.39896-0.32341-0.71590 0.36931 0.55724-0.88309 -8 -6 -7 62.13 11.20 12-0.39896-0.24660-0.71590 0.30092 0.55724-0.93009 -7 -8 -8 4.88 11.89 12-0.39896-0.17017-0.71590 0.16253 0.55724-0.97782 -7 4 11 1.29 8.96 12-0.39896-0.13073-0.71590 0.99081 0.55724-0.03516 -7 4 12 -2.52 10.36 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17.66 9.05 14-0.39645 0.53978-0.73822 0.04613 0.53076-0.81862 2 -3 -2 339.91 12.15 14-0.39645 0.55102-0.73822 0.52995 0.53076-0.62322 2 1 8 21.69 7.01 14-0.39645 0.57029-0.73822 0.80818 0.53076-0.12920 2 1 13 2.83 8.65 14-0.39645 0.58020-0.73822 0.80967 0.53076 0.11831 3 0 7 126.70 8.96 14-0.39645 0.64610-0.73822 0.73747 0.53076-0.17486 3 0 14 3.03 8.78 14-0.39645 0.65989-0.73822 0.73828 0.53076 0.17025 4 -2 17 37.84 12.51 14-0.39645 0.74507-0.73822 0.60014 0.53076 0.32224 4 -1 8 174.73 10.05 14-0.39645 0.72851-0.73822 0.66918 0.53076-0.12271 4 -1 13 17.07 8.85 14-0.39645 0.73761-0.73822 0.66951 0.53076 0.12436 6 -11 1 12.55 12.27 14-0.39645 0.86792-0.73822-0.02247 0.53076-0.46145 6 -10 1 27.66 9.75 14-0.39645 0.86722-0.73822 0.04682 0.53076-0.46120 -9 3 9 -0.46 8.12 14-0.39556-0.29635-0.74371 0.94988 0.52404-0.10715 -5 3 17 2.62 8.68 14-0.39556 0.03506-0.74371 0.95302 0.52404 0.30182 -3 -9 -9 22.52 6.60 14-0.39556 0.13997-0.74371 0.11998 0.52404-0.97667 -3 -6 -8 8.68 4.88 14-0.39556 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0.61787-0.07349-0.76792 -1 -5 14 9.07 8.94 53-0.24926 0.19786-0.96730 0.62452-0.07349 0.76449 0 -1 -9 117.54 8.08 53-0.24926 0.22991-0.96730 0.89594-0.07349-0.37081 0 -1 6 100.17 8.50 53-0.24926 0.26127-0.96730 0.89725-0.07349 0.36990 0 0 -3 -0.39 9.07 53-0.24926 0.24376-0.96730 0.96684-0.07349-0.07456 1 -7 15 3.15 11.80 53-0.24926 0.35547-0.96730 0.48336-0.07349 0.81522 1 -6 14 16.27 9.10 53-0.24926 0.35474-0.96730 0.55438-0.07349 0.76838 1 -5 -16 -1.64 11.69 53-0.24926 0.29502-0.96730 0.61987-0.07349-0.71446 1 -3 -13 106.49 9.42 53-0.24926 0.30095-0.96730 0.75827-0.07349-0.56579 2 -5 12 57.32 9.25 53-0.24926 0.43006-0.96730 0.62298-0.07349 0.67266 2 -3 -12 0.36 6.71 53-0.24926 0.38258-0.96730 0.75807-0.07349-0.51291 3 -8 14 6.34 12.16 53-0.24926 0.51126-0.96730 0.41622-0.07349 0.77357 4 -7 12 2.20 9.21 53-0.24926 0.58525-0.96730 0.48383-0.07349 0.67604 4 -4 -11 289.26 10.70 53-0.24926 0.54141-0.96730 0.69109-0.07349-0.45810 4 -2 -2 145.46 9.71 53-0.24926 0.56000-0.96730 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0.73466-0.30366 0.60688 2 -1 -14 9.51 6.31 67-0.16118 0.29123-0.94171 0.87202-0.30366-0.38177 2 0 -9 4.63 4.68 67-0.16118 0.30221-0.94171 0.94220-0.30366-0.13551 3 -6 9 4.47 6.07 67-0.16118 0.41564-0.94171 0.52821-0.30366 0.75785 4 -2 -14 51.02 6.86 67-0.16118 0.44751-0.94171 0.80310-0.30366-0.37610 6 -4 -15 18.24 8.53 67-0.16118 0.60275-0.94171 0.66443-0.30366-0.41833 6 -3 -12 33.37 6.59 67-0.16118 0.61020-0.94171 0.73569-0.30366-0.27154 7 -4 -12 0.34 6.49 67-0.16118 0.68761-0.94171 0.66457-0.30366-0.26708 9 -8 0 22.60 17.64 67-0.16434 0.87390-0.94348 0.39237-0.29594 0.32412 -7 -1 0 278.71 12.92 67-0.16110-0.39092-0.94163 0.87093-0.30372 0.28105 -6 0 -8 2.68 8.29 67-0.16110-0.32717-0.94163 0.93927-0.30372-0.11103 3 -3 5 406.74 15.17 67-0.16110 0.40795-0.94163 0.73400-0.30372 0.56067 6 -3 -1 5.19 8.32 67-0.16110 0.63205-0.94163 0.73525-0.30372 0.27375 9 -7 -2 -1.97 14.30 67-0.16110 0.86667-0.94163 0.45920-0.30372 0.23331 -10 -5 4 4.87 11.65 68-0.15790-0.62472-0.93967 0.59544-0.31147 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77-0.09316-0.20254-0.88865 0.26658-0.45277 0.93328 -3 -2 4 184.69 7.92 77-0.09316-0.13567-0.88865 0.74987-0.45277 0.64143 -1 -11 11 12.29 8.90 77-0.09316 0.03612-0.88865 0.12817-0.45277 0.99177 -1 1 -15 30.52 6.61 77-0.09316-0.01504-0.88865 0.95628-0.45277-0.29224 1 -9 10 1.57 6.37 77-0.09316 0.19089-0.88865 0.26709-0.45277 0.95164 1 -7 9 10.48 6.14 77-0.09316 0.18971-0.88865 0.40490-0.45277 0.90158 1 0 -18 1.27 8.38 77-0.09316 0.13643-0.88865 0.88766-0.45277-0.43409 1 1 -14 1.61 6.07 77-0.09316 0.14401-0.88865 0.95922-0.45277-0.23766 2 -4 6 109.26 6.93 77-0.09316 0.26271-0.88865 0.61213-0.45277 0.75621 4 -1 -18 8.02 8.85 77-0.09316 0.37190-0.88865 0.81823-0.45277-0.42360 6 -1 -13 68.57 7.04 77-0.09316 0.53939-0.88865 0.82021-0.45277-0.17098 6 -1 -6 170.31 7.38 77-0.09316 0.55387-0.88865 0.81908-0.45277 0.17523 7 -2 -14 18.99 8.53 77-0.09316 0.61623-0.88865 0.75011-0.45277-0.21682 -10 -3 -5 25.85 16.91 77-0.09654-0.70232-0.89193 0.68377-0.44588 0.16631 -4 0 -1 0.40 8.29 77-0.09314-0.22440-0.88862 0.88836-0.45300 0.39081 6 -8 6 3.33 10.97 77-0.09314 0.57644-0.88862 0.33576-0.45300 0.76826 -10 -7 3 3.31 12.19 78-0.08978-0.69060-0.88534 0.39940-0.45997 0.57396 -8 -6 5 -3.08 8.82 78-0.08978-0.53156-0.88534 0.47057-0.45997 0.68183 -8 -5 4 15.30 8.88 78-0.08978-0.53171-0.88534 0.53846-0.45997 0.63123 -8 -3 1 28.79 8.86 78-0.08978-0.53672-0.88534 0.67573-0.45997 0.48246 -7 -9 8 0.87 12.01 78-0.08978-0.44783-0.88534 0.26363-0.45997 0.83538 -7 -7 7 1.77 8.91 78-0.08978-0.44695-0.88534 0.39945-0.45997 0.78146 -7 -4 4 10.83 6.92 78-0.08978-0.45245-0.88534 0.60691-0.45997 0.63420 -6 -6 7 14.90 8.74 78-0.08978-0.36860-0.88534 0.46967-0.45997 0.78647 -6 -5 6 17.70 8.56 78-0.08978-0.37199-0.88534 0.54052-0.45997 0.73876 -6 -4 5 3.20 6.72 78-0.08978-0.37209-0.88534 0.60703-0.45997 0.68630 -5 -8 9 4.96 8.96 78-0.08978-0.28608-0.88534 0.33129-0.45997 0.88673 -4 -3 5 0.83 6.57 78-0.08978-0.21548-0.88534 0.67697-0.45997 0.69441 -4 0 -17 -1.69 12.17 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0.46582-0.88534 0.88534-0.45997 0.03106 6 -2 -2 72.36 8.38 78-0.08978 0.55919-0.88534 0.74848-0.45997 0.38055 6 -1 -14 8.61 9.04 78-0.08978 0.53229-0.88534 0.81390-0.45997-0.21287 7 -2 -5 24.60 7.12 78-0.08978 0.63073-0.88534 0.74793-0.45997 0.23517 9 -4 -7 49.57 9.70 78-0.08978 0.78531-0.88534 0.61005-0.45997 0.14262 10 -6 -6 -1.57 12.26 78-0.08978 0.86724-0.88534 0.47245-0.45997 0.19541 -7 -6 6 10.93 6.27 78-0.08639-0.45318-0.88198 0.46585-0.46714 0.74083 -7 -5 5 7.07 6.12 78-0.08639-0.45590-0.88198 0.53631-0.46714 0.69100 -5 0 -16 0.36 8.49 78-0.08639-0.33946-0.88198 0.88122-0.46714-0.34091 -4 -10 10 5.79 8.51 78-0.08639-0.20916-0.88198 0.19086-0.46714 0.94981 -4 -6 8 442.39 9.80 78-0.08639-0.21268-0.88198 0.46666-0.46714 0.84922 -3 -9 10 1.14 6.43 78-0.08639-0.12952-0.88198 0.25968-0.46714 0.95100 -3 -7 9 1.18 6.15 78-0.08639-0.13204-0.88198 0.39826-0.46714 0.90174 0 -9 10 13.00 6.49 78-0.08639 0.10581-0.88198 0.26034-0.46714 0.96340 0 -2 4 3735.06 33.86 78-0.08639 0.09433-0.88198 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0.94340-0.48131-0.31606 -1 -2 4 2910.92 28.18 79-0.07924 0.00816-0.87482 0.73609-0.48131 0.67698 1 -3 5 132.51 7.56 79-0.07924 0.16812-0.87482 0.66708-0.48131 0.73247 1 1 -16 1.98 6.34 79-0.07924 0.12543-0.87482 0.94160-0.48131-0.30701 2 1 -15 -0.51 6.21 79-0.07924 0.20685-0.87482 0.94276-0.48131-0.25314 3 1 -13 83.40 6.81 79-0.07924 0.28998-0.87482 0.94317-0.48131-0.15141 3 1 -7 192.90 7.47 79-0.07924 0.30194-0.87482 0.94438-0.48131 0.14488 7 -9 5 1.59 14.36 79-0.07929 0.64042-0.87486 0.25340-0.48125 0.75077 8 -4 -2 16.24 10.81 79-0.07929 0.70571-0.87486 0.59913-0.48125 0.40771 9 -5 -3 -0.59 10.96 79-0.07929 0.78195-0.87486 0.52970-0.48125 0.36134 10 -7 -3 5.02 15.11 79-0.07929 0.85964-0.87486 0.39083-0.48125 0.36469 10 -6 -5 1.18 14.89 79-0.07929 0.85737-0.87486 0.46061-0.48125 0.26591 -10 -7 2 1.44 12.27 80-0.07574-0.71100-0.87121 0.38807-0.48826 0.55705 -10 -6 1 4.05 11.72 80-0.07574-0.71085-0.87121 0.45655-0.48826 0.50568 -9 -7 4 14.03 11.72 80-0.07574-0.62326-0.87121 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80-0.07224 0.03817-0.86754 0.93655-0.49519-0.34606 0 1 -3 48.51 7.93 80-0.07224 0.06633-0.86754 0.93702-0.49519 0.34595 2 -9 9 4.07 6.27 80-0.07224 0.24776-0.86754 0.24533-0.49519 0.94665 3 0 -2 -0.71 5.19 80-0.07224 0.30542-0.86754 0.86757-0.49519 0.40523 3 1 -14 144.22 7.53 80-0.07224 0.28103-0.86754 0.93879-0.49519-0.18749 4 0 -17 -4.73 8.29 80-0.07224 0.35326-0.86754 0.86831-0.49519-0.33337 5 0 -15 12.68 6.56 80-0.07224 0.43559-0.86754 0.86507-0.49519-0.23091 7 -1 -11 7.07 6.31 80-0.07224 0.60081-0.86754 0.79791-0.49519-0.02654 7 -1 -10 1.94 6.22 80-0.07224 0.60342-0.86754 0.79759-0.49519 0.02347 8 -2 -12 2.11 8.18 80-0.07224 0.67823-0.86754 0.72817-0.49519-0.07226 8 -2 -11 1.38 6.37 80-0.07224 0.68151-0.86754 0.73018-0.49519-0.02367 -10 -3 -6 5.56 16.70 80-0.07580-0.72406-0.87120 0.66307-0.48817 0.15913 4 -3 3 2.36 9.51 80-0.07580 0.39718-0.87120 0.66423-0.48817 0.64943 -9 -3 -2 11.86 11.01 80-0.07227-0.64022-0.86748 0.65958-0.49511 0.36729 -8 -1 -13 25.81 15.64 80-0.07227-0.58378-0.86748 0.79761-0.49511-0.17350 -7 0 -10 0.56 10.76 80-0.07227-0.49897-0.86748 0.86639-0.49511-0.02163 -6 0 -15 3.91 14.59 80-0.07227-0.43064-0.86748 0.86728-0.49511-0.26597 -5 1 -8 30.07 8.95 80-0.07227-0.33798-0.86748 0.93597-0.49511 0.08377 -4 1 -5 6.89 8.34 80-0.07227-0.25294-0.86748 0.93580-0.49511 0.23502 6 -7 5 55.35 11.70 80-0.07227 0.55430-0.86748 0.38350-0.49511 0.76083 -9 -4 0 86.66 9.90 81-0.06878-0.63900-0.86372 0.58591-0.50197 0.47218 -8 -9 6 2.68 12.07 81-0.06878-0.55139-0.86372 0.24255-0.50197 0.77534 -8 -7 5 -0.60 9.01 81-0.06878-0.55014-0.86372 0.37869-0.50197 0.72151 -8 -6 4 54.54 9.35 81-0.06878-0.55555-0.86372 0.44995-0.50197 0.67628 -8 -5 3 22.79 8.97 81-0.06878-0.55666-0.86372 0.51846-0.50197 0.62615 -8 -3 0 5.52 8.54 81-0.06878-0.56287-0.86372 0.65736-0.50197 0.47794 -7 -9 7 7.41 11.78 81-0.06878-0.47056-0.86372 0.24220-0.50197 0.82884 -7 -7 6 8.87 8.93 81-0.06878-0.47099-0.86372 0.37983-0.50197 0.77658 -6 -1 -1 100.54 9.11 81-0.06878-0.40657-0.86372 0.79494-0.50197 0.43359 -5 -8 8 6.70 8.92 81-0.06878-0.31017-0.86372 0.31158-0.50197 0.88500 -5 -5 6 9.63 6.82 81-0.06878-0.31384-0.86372 0.51854-0.50197 0.78219 -5 -4 5 129.24 8.10 81-0.06878-0.31512-0.86372 0.58676-0.50197 0.73274 -5 1 -12 9.56 8.87 81-0.06878-0.34921-0.86372 0.93230-0.50197-0.10676 -4 -9 9 0.37 9.06 81-0.06878-0.22788-0.86372 0.24133-0.50197 0.93341 -4 -7 8 24.07 8.80 81-0.06878-0.23088-0.86372 0.38085-0.50197 0.88541 -4 -2 3 42.67 7.28 81-0.06878-0.23935-0.86372 0.72435-0.50197 0.63655 -4 1 -15 15.55 9.22 81-0.06878-0.27576-0.86372 0.93033-0.50197-0.25205 -3 -4 6 116.18 7.80 81-0.06878-0.15584-0.86372 0.58617-0.50197 0.78830 -3 1 -16 10.11 9.28 81-0.06878-0.20024-0.86372 0.93509-0.50197-0.29973 -2 -11 10 5.05 12.01 81-0.06878-0.06872-0.86372 0.10341-0.50197 0.98872 -2 1 -17 12.10 11.84 81-0.06878-0.12322-0.86372 0.93195-0.50197-0.34526 -1 -11 10 -3.26 12.01 81-0.06878 0.00958-0.86372 0.10385-0.50197 0.99416 -1 -6 8 309.91 9.59 81-0.06878 0.00656-0.86372 0.44904-0.50197 0.89319 -1 2 -10 2.32 6.68 81-0.06878-0.03062-0.86372 0.99951-0.50197 0.00373 0 -11 10 5.25 12.09 81-0.06878 0.08809-0.86372 0.10355-0.50197 0.99350 0 -8 9 143.20 9.81 81-0.06878 0.08688-0.86372 0.31116-0.50197 0.94923 1 -4 6 488.34 12.19 81-0.06878 0.15932-0.86372 0.58568-0.50197 0.80076 1 1 -17 -4.65 10.49 81-0.06878 0.11394-0.86372 0.93300-0.50197-0.33624 2 -7 8 27.76 8.77 81-0.06878 0.24139-0.86372 0.37956-0.50197 0.90231 2 -2 3 16.71 7.70 81-0.06878 0.23263-0.86372 0.72535-0.50197 0.65708 2 0 -1 -0.67 9.13 81-0.06878 0.22481-0.86372 0.86466-0.50197 0.45839 2 1 -16 12.51 9.01 81-0.06878 0.19473-0.86372 0.93622-0.50197-0.28427 3 -11 9 -1.05 12.16 81-0.06878 0.32208-0.86372 0.10363-0.50197 0.95330 3 -8 8 8.16 8.84 81-0.06878 0.32013-0.86372 0.31102-0.50197 0.90720 3 -5 6 1.83 6.80 81-0.06878 0.31670-0.86372 0.51707-0.50197 0.80758 3 -4 5 8.76 6.70 81-0.06878 0.31469-0.86372 0.58718-0.50197 0.75816 3 1 -15 18.62 8.90 81-0.06878 0.27468-0.86372 0.93080-0.50197-0.22985 3 1 -6 63.45 7.61 81-0.06878 0.29406-0.86372 0.93410-0.50197 0.21489 4 1 -11 11.63 6.84 81-0.06878 0.36100-0.86372 0.93164-0.50197-0.02896 4 1 -10 0.51 6.79 81-0.06878 0.36321-0.86372 0.93180-0.50197 0.02000 5 -9 7 17.23 9.44 81-0.06878 0.47621-0.86372 0.24220-0.50197 0.86398 5 -7 6 145.85 10.96 81-0.06878 0.47401-0.86372 0.37956-0.50197 0.81320 5 -1 -2 194.37 10.48 81-0.06878 0.45846-0.86372 0.79381-0.50197 0.41835 6 -9 6 4.16 11.42 81-0.06878 0.55392-0.86372 0.24207-0.50197 0.81845 7 -1 -13 5.16 9.08 81-0.06878 0.59338-0.86372 0.79243-0.50197-0.11787 7 -1 -12 -2.65 8.95 81-0.06878 0.59828-0.86372 0.79591-0.50197-0.06970 7 -1 -9 31.21 8.94 81-0.06878 0.60344-0.86372 0.79572-0.50197 0.07917 8 -3 -4 8.43 8.85 81-0.06878 0.69089-0.86372 0.65745-0.50197 0.32905 8 -2 -13 6.95 11.93 81-0.06878 0.67310-0.86372 0.72570-0.50197-0.11598 8 -2 -9 3.86 8.97 81-0.06878 0.68370-0.86372 0.72791-0.50197 0.08257 8 -2 -8 70.61 9.54 81-0.06878 0.68185-0.86372 0.72428-0.50197 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4.77 83-0.05170 0.18499-0.84439 0.98100-0.53598-0.05131 2 2 -11 44.17 5.34 83-0.05170 0.18717-0.84439 0.98236-0.53598-0.00217 2 2 -10 1.90 4.78 83-0.05170 0.18971-0.84439 0.98115-0.53598 0.04834 6 0 -15 0.17 8.19 83-0.05170 0.49485-0.84439 0.84389-0.53598-0.18687 -9 -2 -6 9.06 14.27 82-0.05849-0.66304-0.85215 0.71422-0.52268 0.19662 -7 0 -8 -0.05 13.60 82-0.05849-0.50920-0.85215 0.85136-0.52268 0.10442 8 -5 0 5.16 13.89 82-0.05849 0.68821-0.85215 0.50680-0.52268 0.54750 -10 -3 -7 -0.40 16.79 83-0.05505-0.74662-0.84816 0.63976-0.52947 0.15088 6 -6 4 39.47 13.02 83-0.05505 0.53559-0.84816 0.43411-0.52947 0.74616 -7 0 -13 16.32 14.60 83-0.05163-0.52647-0.84414 0.84284-0.53632-0.12929 4 -5 5 175.98 11.27 83-0.05163 0.37630-0.84414 0.49905-0.53632 0.79608 5 -6 5 181.09 11.73 83-0.05163 0.45512-0.84414 0.42963-0.53632 0.79855 6 -10 6 2.96 14.66 83-0.05163 0.53570-0.84414 0.15329-0.53632 0.85183 7 -3 -1 6.55 8.51 83-0.05163 0.60073-0.84414 0.63665-0.53632 0.50896 9 -4 -4 47.10 11.55 83-0.05163 0.75209-0.84414 0.56770-0.53632 0.36678 -9 -4 -1 66.82 9.75 84-0.04821-0.66405-0.84016 0.56304-0.54295 0.46454 -9 -3 -3 4.91 8.79 84-0.04821-0.66735-0.84016 0.63261-0.54295 0.36536 -8 -9 5 6.09 12.10 84-0.04821-0.57350-0.84016 0.21803-0.54295 0.76570 -8 -7 4 -0.26 8.94 84-0.04821-0.57406-0.84016 0.35570-0.54295 0.71369 -8 -4 1 85.76 9.44 84-0.04821-0.57963-0.84016 0.56251-0.54295 0.56571 -7 -3 1 6.55 6.87 84-0.04821-0.50132-0.84016 0.63263-0.54295 0.56975 -6 -9 7 2.63 11.54 84-0.04821-0.41043-0.84016 0.21756-0.54295 0.86825 -6 -7 6 42.71 9.02 84-0.04821-0.41304-0.84016 0.35656-0.54295 0.82076 -5 -10 8 4.09 11.68 84-0.04821-0.32906-0.84016 0.14855-0.54295 0.91847 -5 1 -15 42.87 12.23 84-0.04821-0.37501-0.84016 0.90481-0.54295-0.21422 -4 -4 5 0.27 6.55 84-0.04821-0.25618-0.84016 0.56295-0.54295 0.77528 -4 1 -17 2.58 12.04 84-0.04821-0.30024-0.84016 0.90545-0.54295-0.31004 -3 -11 9 3.17 11.82 84-0.04821-0.16956-0.84016 0.08003-0.54295 0.97460 -3 -6 7 164.61 8.41 84-0.04821-0.17404-0.84016 0.42623-0.54295 0.88038 -3 -2 3 165.09 9.33 84-0.04821-0.18296-0.84016 0.70177-0.54295 0.68127 -3 1 -18 3.25 12.31 84-0.04821-0.22491-0.84016 0.90915-0.54295-0.35768 -3 2 -12 454.27 12.91 84-0.04821-0.21189-0.84016 0.97570-0.54295-0.05997 -3 2 -11 112.45 8.38 84-0.04821-0.20969-0.84016 0.97759-0.54295-0.01118 -3 2 -10 106.20 8.47 84-0.04821-0.20766-0.84016 0.97695-0.54295 0.03873 -2 -10 9 18.70 9.41 84-0.04821-0.09209-0.84016 0.14899-0.54295 0.98014 -2 2 -14 76.70 9.59 84-0.04821-0.13783-0.84016 0.97853-0.54295-0.15663 -1 -10 9 0.29 8.96 84-0.04821-0.01331-0.84016 0.14960-0.54295 0.98749 -1 -7 8 22.19 6.94 84-0.04821-0.01487-0.84016 0.35592-0.54295 0.93350 -1 2 -15 20.68 8.94 84-0.04821-0.06046-0.84016 0.97758-0.54295-0.20238 0 -10 9 7.14 9.09 84-0.04821 0.06627-0.84016 0.14969-0.54295 0.98861 0 2 -15 4.89 8.78 84-0.04821 0.01847-0.84016 0.97924-0.54295-0.19964 1 -11 9 2.97 11.73 84-0.04821 0.14475-0.84016 0.08062-0.54295 0.99140 1 2 -15 9.28 8.84 84-0.04821 0.09627-0.84016 0.97494-0.54295-0.19546 2 2 -13 220.05 10.35 84-0.04821 0.17970-0.84016 0.97851-0.54295-0.09376 2 2 -9 56.06 7.29 84-0.04821 0.18710-0.84016 0.97788-0.54295 0.10409 3 -7 7 12.29 7.94 84-0.04821 0.29840-0.84016 0.35720-0.54295 0.89714 4 -4 4 5.45 6.89 84-0.04821 0.37155-0.84016 0.56391-0.54295 0.75314 4 1 -16 58.48 11.01 84-0.04821 0.33200-0.84016 0.90943-0.54295-0.23636 5 -11 7 3.66 12.43 84-0.04821 0.45540-0.84016 0.08065-0.54295 0.90466 5 1 -12 6.94 8.64 84-0.04821 0.41735-0.84016 0.90758-0.54295-0.03393 5 1 -11 22.63 8.68 84-0.04821 0.41994-0.84016 0.90789-0.54295 0.01532 6 0 -16 52.24 12.73 84-0.04821 0.48706-0.84016 0.83731-0.54295-0.22842 6 0 -7 -0.45 6.72 84-0.04821 0.50727-0.84016 0.83986-0.54295 0.21675 7 -2 -3 3.14 6.76 84-0.04821 0.59466-0.84016 0.70246-0.54295 0.41693 7 -1 -6 67.99 7.71 84-0.04821 0.58768-0.84016 0.77200-0.54295 0.26863 8 -2 -6 83.92 9.77 84-0.04821 0.66765-0.84016 0.70376-0.54295 0.27249 10 -4 -9 -0.43 12.15 84-0.04821 0.81999-0.84016 0.56500-0.54295 0.12998 -9 -8 3 3.38 8.54 84-0.04473-0.65942-0.83587 0.28185-0.54988 0.66956 -8 -6 3 23.90 6.55 84-0.04473-0.58020-0.83587 0.42128-0.54988 0.67304 -7 -9 6 4.58 8.30 84-0.04473-0.49501-0.83587 0.21275-0.54988 0.82171 -7 -7 5 4.36 6.27 84-0.04473-0.49685-0.83587 0.35101-0.54988 0.77303 -5 -11 8 20.87 8.79 84-0.04473-0.33351-0.83587 0.07506-0.54988 0.92544 -5 -6 6 19.68 5.12 84-0.04473-0.33759-0.83587 0.42021-0.54988 0.82827 -4 -9 8 5.48 6.22 84-0.04473-0.25510-0.83587 0.21367-0.54988 0.93208 -3 -8 8 100.86 7.20 84-0.04473-0.17607-0.83587 0.28324-0.54988 0.93516 -2 -11 9 9.65 8.52 84-0.04473-0.09524-0.83587 0.07542-0.54988 0.98799 1 2 -7 1110.15 15.23 84-0.04473 0.10996-0.83587 0.97370-0.54988 0.20604 2 2 -14 5.78 6.16 84-0.04473 0.17360-0.83587 0.97428-0.54988-0.13628 3 -10 8 0.17 6.41 84-0.04473 0.29664-0.83587 0.14577-0.54988 0.95541 3 1 -18 3.01 8.51 84-0.04473 0.24542-0.83587 0.90675-0.54988-0.33190 4 1 -6 324.88 9.00 84-0.04473 0.34820-0.83587 0.90380-0.54988 0.26570 5 1 -13 72.43 6.95 84-0.04473 0.41342-0.83587 0.90602-0.54988-0.07696 5 1 -10 6.74 4.89 84-0.04473 0.41934-0.83587 0.90674-0.54988 0.07207 -10 -5 -2 12.09 14.52 84-0.04457-0.74770-0.83589 0.48962-0.54962 0.41759 -10 -4 -4 -1.20 14.23 84-0.04457-0.75214-0.83589 0.55816-0.54962 0.31907 6 -2 -1 3.03 8.17 84-0.04457 0.51551-0.83589 0.69801-0.54962 0.51920 7 -8 4 1.93 11.13 84-0.04457 0.60396-0.83589 0.28362-0.54962 0.76952 8 -3 -3 11.40 10.67 84-0.04457 0.66872-0.83589 0.62824-0.54962 0.42634 9 -5 -2 5.57 11.03 84-0.04457 0.74817-0.83589 0.49004-0.54962 0.47887 -8 -5 2 -0.07 8.66 85-0.04100-0.58405-0.83154 0.48350-0.55638 0.62783 -8 -2 -3 86.26 10.34 85-0.04100-0.59577-0.83154 0.69250-0.55638 0.38213 -7 -10 6 48.13 12.59 85-0.04100-0.50119-0.83154 0.14054-0.55638 0.83274 -7 -2 -1 48.53 7.77 85-0.04100-0.51325-0.83154 0.69355-0.55638 0.48444 -7 0 -14 -0.47 11.87 85-0.04100-0.53872-0.83154 0.83056-0.55638-0.15910 -6 -10 7 9.59 11.97 85-0.04100-0.41683-0.83154 0.13965-0.55638 0.88052 -6 -6 5 13.27 8.61 85-0.04100-0.42321-0.83154 0.41825-0.55638 0.78611 -6 -3 2 7.37 6.76 85-0.04100-0.42764-0.83154 0.62423-0.55638 0.63626 -5 -8 7 22.77 8.93 85-0.04100-0.33921-0.83154 0.27847-0.55638 0.88421 -5 -5 5 0.40 6.66 85-0.04100-0.34398-0.83154 0.48656-0.55638 0.78882 -5 -3 3 51.82 7.34 85-0.04100-0.34649-0.83154 0.62297-0.55638 0.68715 -4 -7 7 22.41 8.67 85-0.04100-0.26050-0.83154 0.34805-0.55638 0.88953 -3 2 -13 147.19 10.23 85-0.04100-0.22230-0.83154 0.97069-0.55638-0.09679 -3 2 -9 430.54 12.44 85-0.04100-0.21405-0.83154 0.97059-0.55638 0.10097 -2 2 -15 1.88 9.01 85-0.04100-0.14738-0.83154 0.97088-0.55638-0.19267 -2 2 -7 385.11 12.09 85-0.04100-0.13068-0.83154 0.96937-0.55638 0.20320 -1 -11 9 12.72 11.95 85-0.04100-0.02015-0.83154 0.07173-0.55638 0.99566 -1 0 0 3.85 9.32 85-0.04100-0.03861-0.83154 0.83111-0.55638 0.55382 -1 2 -16 61.78 9.55 85-0.04100-0.07012-0.83154 0.96899-0.55638-0.23798 0 -11 9 4.21 11.69 85-0.04100 0.05822-0.83154 0.07152-0.55638 0.99739 0 2 -16 12.83 9.13 85-0.04100 0.00945-0.83154 0.97127-0.55638-0.23587 1 -8 8 151.25 9.93 85-0.04100 0.13594-0.83154 0.27908-0.55638 0.95579 1 -6 7 1.65 6.73 85-0.04100 0.13332-0.83154 0.41698-0.55638 0.90442 1 2 -16 16.40 9.17 85-0.04100 0.08774-0.83154 0.96773-0.55638-0.23142 2 -5 6 15.20 7.00 85-0.04100 0.20972-0.83154 0.48490-0.55638 0.85771 2 -3 4 512.47 15.23 85-0.04100 0.20741-0.83154 0.62429-0.55638 0.76204 2 2 -15 30.07 9.15 85-0.04100 0.16833-0.83154 0.96799-0.55638-0.17859 2 2 -8 113.78 7.90 85-0.04100 0.18320-0.83154 0.97034-0.55638 0.16748 3 -11 8 5.50 12.05 85-0.04100 0.29439-0.83154 0.07216-0.55638 0.96433 3 2 -12 89.36 8.39 85-0.04100 0.25248-0.83154 0.96704-0.55638-0.02742 3 2 -11 18.20 6.98 85-0.04100 0.25420-0.83154 0.96733-0.55638 0.02151 4 1 -17 -2.69 12.01 85-0.04100 0.32272-0.83154 0.90214-0.55638-0.27256 5 -8 6 6.43 8.84 85-0.04100 0.44643-0.83154 0.27929-0.55638 0.86820 5 0 -4 0.32 6.60 85-0.04100 0.42658-0.83154 0.83151-0.55638 0.37507 5 1 -14 46.88 9.27 85-0.04100 0.40796-0.83154 0.90280-0.55638-0.12045 5 1 -9 48.67 7.36 85-0.04100 0.41810-0.83154 0.90219-0.55638 0.12748 6 -1 -3 421.15 12.62 85-0.04100 0.50690-0.83154 0.76111-0.55638 0.42701 8 -1 -13 2.35 11.74 85-0.04100 0.64410-0.83154 0.76035-0.55638-0.06137 8 -1 -12 9.44 11.54 85-0.04100 0.64692-0.83154 0.76214-0.55638-0.01166 8 -1 -11 5.33 8.96 85-0.04100 0.64869-0.83154 0.76157-0.55638 0.03799 9 -3 -6 5.86 9.01 85-0.04100 0.73799-0.83154 0.62442-0.55638 0.28836 9 -2 -12 0.88 12.02 85-0.04100 0.72294-0.83154 0.69045-0.55638-0.00864 10 -5 -5 -0.76 11.77 85-0.04100 0.81855-0.83154 0.48651-0.55638 0.34052 10 -4 -8 4.49 12.23 85-0.04100 0.81544-0.83154 0.55739-0.55638 0.19277 -9 -7 2 -1.54 8.20 85-0.03727-0.66857-0.82715 0.34350-0.56284 0.63179 -7 -6 4 13.85 6.16 85-0.03727-0.50594-0.82715 0.41228-0.56284 0.73661 -7 -4 2 99.01 6.44 85-0.03727-0.51067-0.82715 0.55073-0.56284 0.63914 -5 -4 4 13.13 4.96 85-0.03727-0.34816-0.82715 0.54988-0.56284 0.74481 -4 -10 8 12.64 8.17 85-0.03727-0.26142-0.82715 0.13613-0.56284 0.94421 -3 -5 6 1.97 4.77 85-0.03727-0.18692-0.82715 0.48109-0.56284 0.84865 -3 2 -14 50.87 7.05 85-0.03727-0.22753-0.82715 0.96469-0.56284-0.13954 -2 -8 8 52.42 6.57 85-0.03727-0.10417-0.82715 0.27478-0.56284 0.95109 -2 -6 7 23.84 5.00 85-0.03727-0.10637-0.82715 0.41212-0.56284 0.90025 0 2 -6 36.64 5.61 85-0.03727 0.02463-0.82715 0.96426-0.56284 0.26582 2 -9 8 1.25 6.18 85-0.03727 0.21078-0.82715 0.20542-0.56284 0.96382 3 2 -13 52.52 6.58 85-0.03727 0.24758-0.82715 0.96553-0.56284-0.07097 3 2 -10 3.00 4.80 85-0.03727 0.25372-0.82715 0.96515-0.56284 0.07823 5 1 -15 24.37 6.68 85-0.03727 0.40115-0.82715 0.89822-0.56284-0.16338 5 1 -8 53.40 5.52 85-0.03727 0.41456-0.82715 0.89525-0.56284 0.18282 6 0 -6 43.34 5.47 85-0.03727 0.49767-0.82715 0.82640-0.56284 0.28568 7 0 -12 -1.69 6.29 85-0.03727 0.56360-0.82715 0.82578-0.56284-0.00878 7 0 -11 45.15 6.75 85-0.03727 0.56508-0.82715 0.82525-0.56284 0.04101 8 -1 -14 -3.29 8.56 85-0.03727 0.63963-0.82715 0.75784-0.56284-0.10397 8 -1 -10 5.93 6.40 85-0.03727 0.64777-0.82715 0.75935-0.56284 0.09415 9 -2 -11 5.21 8.30 85-0.03727 0.72505-0.82715 0.68899-0.56284 0.04736 6 -5 3 85.92 12.92 85-0.04092 0.51936-0.83152 0.48639-0.55622 0.72421 -8 -3 -1 3.86 10.46 85-0.03732-0.59496-0.82710 0.61900-0.56290 0.48795 5 -5 4 195.35 12.71 85-0.03732 0.43896-0.82710 0.48161-0.56290 0.77672 6 -8 5 13.47 11.05 85-0.03732 0.52019-0.82710 0.27545-0.56290 0.82956 -10 -7 0 -0.32 12.13 86-0.03362-0.75219-0.82263 0.33699-0.56935 0.53488 -10 -6 -1 13.85 12.01 86-0.03362-0.75413-0.82263 0.40602-0.56935 0.48470 -9 -6 1 15.39 9.33 86-0.03362-0.67361-0.82263 0.40709-0.56935 0.58874 -9 -5 0 -0.52 8.90 86-0.03362-0.67386-0.82263 0.47463-0.56935 0.53813 -8 -8 4 10.99 11.56 86-0.03362-0.58767-0.82263 0.26906-0.56935 0.73838 -7 -8 5 8.36 9.03 86-0.03362-0.50907-0.82263 0.26984-0.56935 0.79587 -7 -5 3 5.86 8.50 86-0.03362-0.51206-0.82263 0.47618-0.56935 0.69345 -6 -8 6 -7.37 8.83 86-0.03362-0.42661-0.82263 0.26905-0.56935 0.84540 -6 -5 4 3.50 6.63 86-0.03362-0.43107-0.82263 0.47693-0.56935 0.74789 -6 -4 3 220.51 9.21 86-0.03362-0.43400-0.82263 0.54618-0.56935 0.69833 -5 -9 7 14.32 8.96 86-0.03362-0.34745-0.82263 0.20090-0.56935 0.90102 -5 1 -16 9.95 12.31 86-0.03362-0.39304-0.82263 0.89166-0.56935-0.23851 -4 -11 8 2.41 11.89 86-0.03362-0.26556-0.82263 0.06243-0.56935 0.95040 -3 -9 8 18.21 8.96 86-0.03362-0.18594-0.82263 0.20083-0.56935 0.95354 -3 -4 5 174.92 8.69 86-0.03362-0.19259-0.82263 0.54620-0.56935 0.80706 -3 -3 4 426.53 11.31 86-0.03362-0.19508-0.82263 0.61445-0.56935 0.75629 -3 2 -15 1.17 9.08 86-0.03362-0.23214-0.82263 0.95699-0.56935-0.18147 -3 2 -8 143.63 9.10 86-0.03362-0.21909-0.82263 0.96029-0.56935 0.16360 -2 2 -16 0.85 9.10 86-0.03362-0.15721-0.82263 0.96183-0.56935-0.22876 -1 -8 8 3.06 8.63 86-0.03362-0.02934-0.82263 0.26955-0.56935 0.96078 -1 -6 7 65.04 7.38 86-0.03362-0.03113-0.82263 0.40744-0.56935 0.91105 -1 2 -17 40.72 11.92 86-0.03362-0.07899-0.82263 0.95886-0.56935-0.27451 -1 2 -6 509.34 13.35 86-0.03362-0.05742-0.82263 0.96114-0.56935 0.26826 0 -8 8 2.87 8.64 86-0.03362 0.04913-0.82263 0.26949-0.56935 0.96324 0 -6 7 6.72 6.88 86-0.03362 0.04734-0.82263 0.40728-0.56935 0.91367 0 2 -17 0.85 11.59 86-0.03362-0.00113-0.82263 0.96187-0.56935-0.27235 1 2 -17 3.01 11.56 86-0.03362 0.07792-0.82263 0.95906-0.56935-0.26811 2 -4 5 381.08 12.16 86-0.03362 0.20091-0.82263 0.54542-0.56935 0.82194 2 2 -16 23.13 9.20 86-0.03362 0.15928-0.82263 0.96161-0.56935-0.21627 2 2 -7 239.26 9.38 86-0.03362 0.17745-0.82263 0.95916-0.56935 0.22895 3 1 -4 142.69 8.98 86-0.03362 0.26275-0.82263 0.89142-0.56935 0.38110 3 2 -14 30.52 8.96 86-0.03362 0.24220-0.82263 0.96230-0.56935-0.11413 3 2 -9 3.04 6.65 86-0.03362 0.25200-0.82263 0.96010-0.56935 0.13395 4 -9 7 9.36 8.81 86-0.03362 0.36109-0.82263 0.20066-0.56935 0.92501 4 1 -18 14.03 12.41 86-0.03362 0.31344-0.82263 0.89317-0.56935-0.30912 5 1 -16 4.76 11.74 86-0.03362 0.39494-0.82263 0.89140-0.56935-0.20623 7 -1 -5 109.44 8.33 86-0.03362 0.57445-0.82263 0.75370-0.56935 0.34439 7 0 -14 4.18 11.63 86-0.03362 0.55673-0.82263 0.82172-0.56935-0.10080 7 0 -13 59.42 9.77 86-0.03362 0.56065-0.82263 0.82506-0.56935-0.05128 7 0 -10 -0.28 8.70 86-0.03362 0.56507-0.82263 0.82217-0.56935 0.09771 8 -2 -5 284.04 11.91 86-0.03362 0.65386-0.82263 0.68581-0.56935 0.34792 8 -1 -9 -0.37 8.84 86-0.03362 0.64586-0.82263 0.75398-0.56935 0.15019 9 -2 -10 -3.42 11.59 86-0.03362 0.72445-0.82263 0.68594-0.56935 0.10391 10 -4 -7 3.62 11.99 86-0.03362 0.80755-0.82263 0.54712-0.56935 0.25534 -4 -6 6 435.12 9.32 86-0.02996-0.27371-0.81804 0.40424-0.57582 0.86095 -3 -7 7 221.26 7.27 86-0.02996-0.19206-0.81804 0.33523-0.57582 0.91388 -2 -2 3 294.48 10.17 86-0.02996-0.12218-0.81804 0.67919-0.57582 0.71853 1 2 -6 39.61 5.62 86-0.02996 0.09647-0.81804 0.95585-0.57582 0.28236 2 -10 8 4.21 6.37 86-0.02996 0.20305-0.81804 0.12716-0.57582 0.97853 2 -7 7 17.40 5.13 86-0.02996 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0.88192-0.58222-0.03079 -6 1 -11 0.52 8.72 87-0.02641-0.46874-0.81344 0.88215-0.58222 0.01855 -5 -10 7 -2.08 11.56 87-0.02641-0.35375-0.81344 0.12201-0.58222 0.91208 -5 -7 6 214.63 10.19 87-0.02641-0.35488-0.81344 0.32891-0.58222 0.85994 -4 -8 7 107.76 9.40 87-0.02641-0.27460-0.81344 0.26040-0.58222 0.91368 -4 -2 2 143.67 8.94 87-0.02641-0.28549-0.81344 0.67490-0.58222 0.66836 -4 2 -12 118.16 10.26 87-0.02641-0.31241-0.81344 0.94960-0.58222-0.02426 -4 2 -11 26.81 8.86 87-0.02641-0.31098-0.81344 0.94942-0.58222 0.02506 -3 -11 8 0.10 11.71 87-0.02641-0.19473-0.81344 0.05323-0.58222 0.97061 -3 -10 8 3.12 9.15 87-0.02641-0.19311-0.81344 0.12203-0.58222 0.96487 -3 2 -16 36.79 11.92 87-0.02641-0.24078-0.81344 0.94759-0.58222-0.21813 -2 -9 8 21.15 8.96 87-0.02641-0.11502-0.81344 0.19121-0.58222 0.96935 -2 -5 6 552.41 11.52 87-0.02641-0.11895-0.81344 0.46715-0.58222 0.87078 -2 2 -17 3.60 11.82 87-0.02641-0.16554-0.81344 0.95129-0.58222-0.26548 -1 2 -18 8.84 11.85 87-0.02641-0.08820-0.81344 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6.66 87-0.02286-0.11925-0.80879 0.11860-0.58859 0.98010 -1 -9 8 40.13 6.64 87-0.02286-0.04082-0.80879 0.18606-0.58859 0.97929 -1 -5 6 92.89 6.10 87-0.02286-0.04404-0.80879 0.46354-0.58859 0.88268 0 -9 8 11.82 6.39 87-0.02286 0.03809-0.80879 0.18634-0.58859 0.98259 0 -5 6 33.62 5.29 87-0.02286 0.03505-0.80879 0.46392-0.58859 0.88616 4 2 -14 49.71 6.79 87-0.02286 0.30897-0.80879 0.94556-0.58859-0.09144 4 2 -13 103.43 7.31 87-0.02286 0.31266-0.80879 0.94856-0.58859-0.04129 4 2 -11 10.28 4.93 87-0.02286 0.31636-0.80879 0.94788-0.58859 0.05779 6 1 -14 3.31 6.47 87-0.02286 0.46705-0.80879 0.87836-0.58859-0.08547 6 1 -11 6.45 6.04 87-0.02286 0.47405-0.80879 0.87978-0.58859 0.06448 7 0 -8 -0.61 6.05 87-0.02286 0.55709-0.80879 0.80827-0.58859 0.21582 10 -7 -2 2.35 19.42 86-0.03010 0.81367-0.81807 0.33501-0.57577 0.50895 8 -4 -1 84.85 14.02 87-0.02644 0.65441-0.81347 0.53819-0.58214 0.55852 -10 -4 -5 4.96 14.36 87-0.02283-0.77515-0.80879 0.53143-0.58850 0.30850 -6 1 -13 2.21 11.11 87-0.02283-0.47637-0.80879 0.87705-0.58850-0.07375 -6 1 -10 120.24 12.92 87-0.02283-0.46994-0.80879 0.87725-0.58850 0.07450 5 -9 6 5.11 11.11 87-0.02283 0.42851-0.80879 0.18757-0.58850 0.90089 9 -4 -3 1.10 10.81 87-0.02283 0.72454-0.80879 0.53265-0.58850 0.46797 -10 -7 -1 -0.33 12.31 88-0.01926-0.77342-0.80407 0.31988-0.59478 0.51466 -10 -6 -2 41.78 12.61 88-0.01926-0.77540-0.80407 0.38948-0.59478 0.46424 -9 -4 -2 90.33 10.16 88-0.01926-0.69206-0.80407 0.52533-0.59478 0.46557 -9 -3 -4 79.72 10.54 88-0.01926-0.69806-0.80407 0.59564-0.59478 0.36740 -8 -6 2 2.83 8.75 88-0.01926-0.60750-0.80407 0.38896-0.59478 0.66680 -8 -5 1 -1.15 8.63 88-0.01926-0.61026-0.80407 0.45826-0.59478 0.62028 -8 -4 0 0.98 8.54 88-0.01926-0.60992-0.80407 0.52560-0.59478 0.56710 -7 -10 5 0.58 11.95 88-0.01926-0.52444-0.80407 0.11259-0.59478 0.82171 -7 -7 4 8.58 8.86 88-0.01926-0.52309-0.80407 0.31912-0.59478 0.76802 -6 -10 6 3.03 11.75 88-0.01926-0.44179-0.80407 0.11214-0.59478 0.87119 -6 -2 0 4.57 6.66 88-0.01926-0.45379-0.80407 0.66439-0.59478 0.57436 -6 1 -14 2.02 11.59 88-0.01926-0.48123-0.80407 0.87057-0.59478-0.11706 -5 -2 1 23.25 6.99 88-0.01926-0.37311-0.80407 0.66662-0.59478 0.62921 -4 -9 7 11.75 8.94 88-0.01926-0.28236-0.80407 0.18188-0.59478 0.92953 -4 -5 5 4.77 6.58 88-0.01926-0.28639-0.80407 0.45829-0.59478 0.82890 -4 2 -14 3.61 9.01 88-0.01926-0.32367-0.80407 0.94068-0.59478-0.11109 -4 2 -13 61.69 9.59 88-0.01926-0.32311-0.80407 0.94475-0.59478-0.06119 -4 2 -10 21.98 7.20 88-0.01926-0.31649-0.80407 0.94291-0.59478 0.08752 -3 -1 1 277.18 12.61 88-0.01926-0.21600-0.80407 0.73414-0.59478 0.63426 -3 2 -7 36.73 7.39 88-0.01926-0.23107-0.80407 0.94059-0.59478 0.23837 -2 -12 8 2.89 12.22 88-0.01926-0.12320-0.80407-0.02565-0.59478 0.98616 -2 -11 8 10.71 11.64 88-0.01926-0.12302-0.80407 0.04386-0.59478 0.98556 -2 -7 7 10.25 6.88 88-0.01926-0.12451-0.80407 0.32036-0.59478 0.93323 -2 -4 5 678.12 12.98 88-0.01926-0.12871-0.80407 0.52667-0.59478 0.83435 -2 -3 4 164.55 8.97 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0.30371-0.80407 0.94169-0.59478-0.13426 4 2 -10 5.01 6.78 88-0.01926 0.31466-0.80407 0.94423-0.59478 0.11367 6 0 -5 -3.11 6.75 88-0.01926 0.48179-0.80407 0.80485-0.59478 0.36756 6 1 -15 2.04 11.65 88-0.01926 0.46279-0.80407 0.87464-0.59478-0.12824 6 1 -10 60.71 9.11 88-0.01926 0.47308-0.80407 0.87594-0.59478 0.11905 8 -1 -7 87.43 9.47 88-0.01926 0.63334-0.80407 0.73385-0.59478 0.27383 10 -4 -6 15.07 12.03 88-0.01926 0.79527-0.80407 0.52876-0.59478 0.33074 10 -3 -9 -0.93 12.15 88-0.01926 0.78859-0.80407 0.59735-0.59478 0.18205 -9 -7 1 6.67 8.33 88-0.01566-0.69133-0.79929 0.31462-0.60094 0.62106 -6 -11 6 -2.79 8.58 88-0.01566-0.44531-0.79929 0.03860-0.60094 0.87551 -5 -8 6 27.63 6.37 88-0.01566-0.36683-0.79929 0.24640-0.60094 0.88113 -5 -6 5 83.98 6.02 88-0.01566-0.36814-0.79929 0.38379-0.60094 0.83083 -3 -8 7 -0.31 6.07 88-0.01566-0.20731-0.79929 0.24621-0.60094 0.93742 -3 -6 6 1.31 4.72 88-0.01566-0.20952-0.79929 0.38565-0.60094 0.88908 -3 2 -17 10.02 8.72 88-0.01566-0.25475-0.79929 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0.28166 6 -9 5 28.03 11.62 88-0.01573 0.49805-0.79930 0.17810-0.60101 0.86856 7 -9 4 7.37 14.38 88-0.01573 0.57431-0.79930 0.17801-0.60101 0.82215 10 -5 -4 -0.91 14.41 88-0.01573 0.79473-0.79930 0.45452-0.60101 0.43578 -9 -6 0 -0.72 9.11 89-0.01216-0.69776-0.79447 0.37861-0.60717 0.57825 -9 -5 -1 13.25 9.12 89-0.01216-0.69890-0.79447 0.44749-0.60717 0.52788 -8 -8 3 15.02 11.70 89-0.01216-0.61107-0.79447 0.24013-0.60717 0.72824 -7 -6 3 -3.88 8.62 89-0.01216-0.53408-0.79447 0.37895-0.60717 0.73275 -7 -3 0 166.13 9.19 89-0.01216-0.53843-0.79447 0.58479-0.60717 0.58327 -6 -6 4 97.02 9.38 89-0.01216-0.45345-0.79447 0.37943-0.60717 0.78684 -6 -1 -2 478.05 16.16 89-0.01216-0.46522-0.79447 0.72437-0.60717 0.48820 -4 -11 7 2.55 11.76 89-0.01216-0.29080-0.79447 0.03404-0.60717 0.94342 -4 -10 7 8.35 8.96 89-0.01216-0.28991-0.79447 0.10293-0.60717 0.93875 -4 -7 6 29.83 7.91 89-0.01216-0.29161-0.79447 0.31062-0.60717 0.89180 -4 -4 4 80.99 7.58 89-0.01216-0.29501-0.79447 0.51692-0.60717 0.79049 -4 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0.81917 -4 3 -10 4.57 6.93 100 0.06580-0.40230-0.67420 0.88241-0.73159 0.22440 -3 -3 2 931.56 16.01 100 0.06580-0.29884-0.67420 0.46506-0.73159 0.81965 -3 -1 0 45.93 8.66 100 0.06580-0.30258-0.67420 0.60466-0.73159 0.72280 -3 3 -8 214.12 10.14 100 0.06580-0.31916-0.67420 0.88376-0.73159 0.32687 -2 4 -11 -1.21 6.74 100 0.06580-0.24481-0.67420 0.94998-0.73159 0.18120 -1 -12 5 -2.83 11.59 100 0.06580-0.13505-0.67420-0.15500-0.73159 0.97241 -1 -8 5 0.22 6.68 100 0.06580-0.13531-0.67420 0.12075-0.73159 0.97688 -1 -5 4 2.87 6.83 100 0.06580-0.13717-0.67420 0.32860-0.73159 0.92765 0 -12 5 11.01 11.80 100 0.06580-0.05666-0.67420-0.15637-0.73159 0.98305 0 -7 5 6.61 6.83 100 0.06580-0.05666-0.67420 0.18923-0.73159 0.97694 0 -3 3 18.72 7.56 100 0.06580-0.05927-0.67420 0.46629-0.73159 0.87899 0 4 -9 1.39 6.72 100 0.06580-0.08495-0.67420 0.95280-0.73159 0.28650 1 -7 5 0.28 6.84 100 0.06580 0.02153-0.67420 0.18992-0.73159 0.98145 1 -3 3 1896.65 25.88 100 0.06580 0.01949-0.67420 0.46546-0.73159 0.88450 2 -12 5 0.49 11.80 100 0.06580 0.10042-0.67420-0.15540-0.73159 0.98615 2 4 -9 120.46 8.01 100 0.06580 0.07344-0.67420 0.95390-0.73159 0.29326 3 -11 5 10.97 9.22 100 0.06580 0.17897-0.67420-0.08618-0.73159 0.98667 3 -10 5 13.73 8.94 100 0.06580 0.18025-0.67420-0.01712-0.73159 0.99007 3 -9 5 -1.35 8.63 100 0.06580 0.17993-0.67420 0.05209-0.73159 0.98884 3 3 -6 3.04 6.50 100 0.06580 0.15897-0.67420 0.88393-0.73159 0.44559 4 4 -11 283.12 10.75 100 0.06580 0.22773-0.67420 0.95484-0.73159 0.20071 5 -8 4 219.95 11.43 100 0.06580 0.33627-0.67420 0.12158-0.73159 0.94690 5 1 -3 18.49 6.92 100 0.06580 0.32191-0.67420 0.74386-0.73159 0.59835 5 2 -5 -0.16 6.63 100 0.06580 0.31876-0.67420 0.81273-0.73159 0.50041 5 4 -16 4.45 11.97 100 0.06580 0.29607-0.67420 0.95395-0.73159-0.04413 5 4 -15 -2.39 11.60 100 0.06580 0.29870-0.67420 0.95473-0.73159 0.00567 5 4 -14 6.86 9.13 100 0.06580 0.30020-0.67420 0.95327-0.73159 0.05535 5 4 -13 23.76 9.01 100 0.06580 0.30102-0.67420 0.94948-0.73159 0.10444 6 -1 -1 3.45 6.74 100 0.06580 0.40457-0.67420 0.60563-0.73159 0.70125 6 1 -4 152.25 8.68 100 0.06580 0.39874-0.67420 0.74373-0.73159 0.55258 7 2 -8 83.27 9.29 100 0.06580 0.47080-0.67420 0.81449-0.73159 0.35895 7 3 -13 11.71 11.64 100 0.06580 0.46025-0.67420 0.88351-0.73159 0.11117 8 0 -5 -2.26 8.56 100 0.06580 0.55383-0.67420 0.67475-0.73159 0.51066 9 -1 -5 68.37 9.68 100 0.06580 0.63115-0.67420 0.60447-0.73159 0.51217 9 0 -7 8.51 8.80 100 0.06580 0.62830-0.67420 0.67454-0.73159 0.41402 9 1 -10 5.24 11.52 100 0.06580 0.62282-0.67420 0.74512-0.73159 0.26589 10 0 -10 2.65 12.11 100 0.06580 0.69964-0.67420 0.67378-0.73159 0.26842 -7 -6 0 53.61 6.72 100 0.06926-0.62186-0.66847 0.25314-0.73677 0.71474 -6 -11 2 29.84 8.71 100 0.06926-0.53796-0.66847-0.09234-0.73677 0.81527 -6 -10 2 0.89 8.15 100 0.06926-0.54038-0.66847-0.02369-0.73677 0.81829 -6 -9 2 14.48 6.35 100 0.06926-0.53944-0.66847 0.04612-0.73677 0.81794 -5 -10 3 0.43 6.43 100 0.06926-0.45849-0.66847-0.02391-0.73677 0.86890 -5 -9 3 -3.99 6.21 100 0.06926-0.45790-0.66847 0.04589-0.73677 0.86830 -4 -6 3 84.21 5.85 100 0.06926-0.37920-0.66847 0.25317-0.73677 0.87356 -3 -12 4 13.79 8.49 100 0.06926-0.29864-0.66847-0.16232-0.73677 0.92756 -3 -7 4 329.03 8.35 100 0.06926-0.29727-0.66847 0.18333-0.73677 0.92397 -1 -11 5 2.71 6.30 100 0.06926-0.13802-0.66847-0.09220-0.73677 0.97970 -1 -10 5 3.93 6.06 100 0.06926-0.13867-0.66847-0.02322-0.73677 0.98357 -1 -9 5 142.51 7.44 100 0.06926-0.13866-0.66847 0.04672-0.73677 0.98271 1 -12 5 9.80 8.42 100 0.06926 0.01898-0.66847-0.16142-0.73677 0.98671 2 -8 5 13.34 4.99 100 0.06926 0.09900-0.66847 0.11580-0.73677 0.99152 3 4 -9 204.86 7.30 100 0.06926 0.14901-0.66847 0.94393-0.73677 0.30056 6 2 -6 76.60 5.92 100 0.06926 0.39151-0.66847 0.80637-0.73677 0.45929 6 3 -9 16.69 6.20 100 0.06926 0.38453-0.66847 0.87508-0.73677 0.31013 7 3 -12 -1.86 6.41 100 0.06926 0.45865-0.66847 0.87674-0.73677 0.16568 8 1 -7 85.81 7.18 100 0.06926 0.54725-0.66847 0.73827-0.73677 0.41705 8 -6 1 10.93 19.14 97 0.04805 0.58421-0.70364 0.28982-0.70540 0.78177 -9 -2 -9 3.06 18.38 99 0.06230-0.78997-0.68011 0.54169-0.72640 0.25198 -7 -1 -5 34.74 10.54 100 0.06584-0.62809-0.67417 0.60478-0.73156 0.46179 -7 1 -11 108.75 15.62 100 0.06584-0.64006-0.67417 0.74318-0.73156 0.16471 -9 -3 -7 0.83 10.99 100 0.06929-0.79414-0.66822 0.46072-0.73662 0.36197 -5 2 -8 -0.64 8.21 100 0.06929-0.47901-0.66822 0.80640-0.73662 0.32490 7 -1 -2 232.61 12.16 100 0.06929 0.47836-0.66822 0.59970-0.73662 0.66059 -8 -8 -1 1.91 11.44 101 0.07276-0.70721-0.66231 0.10870-0.74168 0.66904 -6 -4 0 60.17 7.48 101 0.07276-0.54502-0.66231 0.38491-0.74168 0.72157 -5 -4 1 29.47 6.98 101 0.07276-0.46550-0.66231 0.38600-0.74168 0.77640 -5 3 -15 1.30 11.74 101 0.07276-0.49603-0.66231 0.86788-0.74168-0.01664 -5 3 -14 1.39 9.09 101 0.07276-0.49388-0.66231 0.86748-0.74168 0.03271 -3 -2 1 158.04 9.58 101 0.07276-0.30795-0.66231 0.52307-0.74168 0.78104 -3 4 -16 2.21 11.82 101 0.07276-0.34084-0.66231 0.93875-0.74168-0.05952 -3 4 -15 2.93 9.17 101 0.07276-0.33991-0.66231 0.94016-0.74168-0.01001 -3 4 -14 3.38 8.94 101 0.07276-0.33720-0.66231 0.93963-0.74168 0.03925 -3 4 -13 34.65 9.11 101 0.07276-0.33414-0.66231 0.93661-0.74168 0.08866 -2 -13 4 0.79 12.09 101 0.07276-0.22342-0.66231-0.23740-0.74168 0.93565 -2 -6 4 -1.35 6.69 101 0.07276-0.22218-0.66231 0.24717-0.74168 0.93313 -2 -4 3 33.27 7.15 101 0.07276-0.22490-0.66231 0.38596-0.74168 0.88448 -2 2 -4 248.40 12.61 101 0.07276-0.23900-0.66231 0.80183-0.74168 0.53674 -1 4 -9 43.70 7.27 101 0.07276-0.16928-0.66231 0.93849-0.74168 0.29285 0 -11 5 31.82 9.17 101 0.07276-0.06367-0.66231-0.09838-0.74168 0.98975 0 -8 5 43.33 7.12 101 0.07276-0.06336-0.66231 0.10890-0.74168 0.98856 1 -11 5 -0.36 8.95 101 0.07276 0.01553-0.66231-0.09827-0.74168 0.99490 1 -8 5 232.93 9.10 101 0.07276 0.01617-0.66231 0.10882-0.74168 0.99370 1 2 -3 9080.11 53.08 101 0.07276-0.00010-0.66231 0.80273-0.74168 0.59540 2 -11 5 3.74 8.99 101 0.07276 0.09396-0.66231-0.09768-0.74168 0.99382 2 -10 5 63.80 9.49 101 0.07276 0.09465-0.66231-0.02909-0.74168 0.99813 2 -9 5 3.89 8.62 101 0.07276 0.09495-0.66231 0.04006-0.74168 0.99770 2 -5 4 11.52 6.77 101 0.07276 0.09300-0.66231 0.31619-0.74168 0.94698 4 2 -4 252.78 9.84 101 0.07276 0.23547-0.66231 0.80236-0.74168 0.55741 4 4 -10 79.52 7.57 101 0.07276 0.22314-0.66231 0.94180-0.74168 0.26052 5 -11 4 6.72 11.78 101 0.07276 0.32721-0.66231-0.09782-0.74168 0.95246 5 -10 4 -1.74 9.07 101 0.07276 0.32911-0.66231-0.02907-0.74168 0.95648 5 -9 4 36.62 9.32 101 0.07276 0.32893-0.66231 0.04064-0.74168 0.95609 5 4 -12 3.58 8.81 101 0.07276 0.29845-0.66231 0.94235-0.74168 0.16438 7 1 -5 100.82 8.05 101 0.07276 0.46770-0.66231 0.73070-0.74168 0.51615 7 3 -11 28.84 9.08 101 0.07276 0.45501-0.66231 0.86786-0.74168 0.21903 8 -2 -2 376.34 14.53 101 0.07276 0.55306-0.66231 0.52536-0.74168 0.66871 8 2 -10 10.30 9.02 101 0.07276 0.53912-0.66231 0.80391-0.74168 0.27390 10 -1 -7 1.70 11.67 101 0.07276 0.69977-0.66231 0.59338-0.74168 0.42651 -9 -8 -3 4.61 8.49 101 0.07627-0.79147-0.65611 0.10221-0.74655 0.56982 -8 -10 -1 -2.41 8.61 101 0.07627-0.71104-0.65611-0.03508-0.74655 0.67291 -6 -6 1 15.39 4.96 101 0.07627-0.54804-0.65611 0.24122-0.74655 0.77772 -5 -6 2 27.21 5.12 101 0.07627-0.46660-0.65611 0.24148-0.74655 0.83095 -3 -11 4 0.78 6.33 101 0.07627-0.30421-0.65611-0.10448-0.74655 0.93385 -3 -8 4 344.71 8.48 101 0.07627-0.30405-0.65611 0.10241-0.74655 0.93392 -3 -5 3 9.93 4.66 101 0.07627-0.30713-0.65611 0.31063-0.74655 0.88603 -3 4 -17 3.37 8.74 101 0.07627-0.34716-0.65611 0.93322-0.74655-0.10455 -2 4 -10 4.12 4.78 101 0.07627-0.25325-0.65611 0.93240-0.74655 0.24596 0 -10 5 16.33 6.30 101 0.07627-0.06651-0.65611-0.03493-0.74655 0.99368 0 -9 5 42.10 6.62 101 0.07627-0.06706-0.65611 0.03383-0.74655 0.99361 0 -5 4 458.74 10.65 101 0.07627-0.06851-0.65611 0.30979-0.74655 0.94452 0 2 -3 5007.67 42.29 101 0.07627-0.08157-0.65611 0.79478-0.74655 0.59690 1 -10 5 -0.15 6.18 101 0.07627 0.01277-0.65611-0.03503-0.74655 0.99903 1 -9 5 20.65 6.27 101 0.07627 0.01111-0.65611 0.03367-0.74655 0.99897 1 3 -5 148.38 7.42 101 0.07627-0.00718-0.65611 0.86423-0.74655 0.50169 1 4 -8 143.69 6.78 101 0.07627-0.01309-0.65611 0.93427-0.74655 0.35477 2 2 -3 282.81 10.04 101 0.07627 0.07600-0.65611 0.79477-0.74655 0.60420 2 4 -8 36.56 5.32 101 0.07627 0.06612-0.65611 0.93272-0.74655 0.35630 5 3 -7 194.70 7.24 101 0.07627 0.30391-0.65611 0.86279-0.74655 0.41588 5 4 -11 131.10 7.45 101 0.07627 0.29580-0.65611 0.93281-0.74655 0.21803 6 4 -15 18.69 8.72 101 0.07627 0.36606-0.65611 0.93084-0.74655 0.02331 9 1 -9 19.87 6.82 101 0.07627 0.61542-0.65611 0.72687-0.74655 0.33015 8 -3 -1 29.43 12.77 101 0.07279 0.55512-0.66219 0.45561-0.74168 0.71827 -6 -2 -2 57.17 9.20 101 0.07627-0.55351-0.65620 0.51787-0.74669 0.62844 -6 2 -11 23.55 11.26 101 0.07627-0.57127-0.65620 0.79378-0.74669 0.18288 -4 2 -6 80.62 10.44 101 0.07627-0.40365-0.65620 0.79394-0.74669 0.43682 6 -7 3 3.52 10.53 101 0.07627 0.40230-0.65620 0.17242-0.74669 0.91488 10 -3 -4 11.44 11.35 101 0.07627 0.70246-0.65620 0.44906-0.74669 0.58088 -9 -6 -4 -0.20 11.52 102 0.07977-0.79650-0.64999 0.23412-0.75157 0.52397 -8 -9 -1 4.44 11.73 102 0.07977-0.70992-0.64999 0.02737-0.75157 0.67402 -8 -6 -2 3.27 8.97 102 0.07977-0.71537-0.64999 0.23495-0.75157 0.62787 -7 -7 0 4.31 8.81 102 0.07977-0.63211-0.64999 0.16568-0.75157 0.73024 -6 -3 -1 22.34 7.01 102 0.07977-0.55371-0.64999 0.44201-0.75157 0.68196 -5 3 -16 1.57 12.25 102 0.07977-0.50755-0.64999 0.86041-0.75157-0.05657 -5 3 -13 20.67 9.27 102 0.07977-0.50052-0.64999 0.85783-0.75157 0.09229 -4 -12 3 0.72 12.01 102 0.07977-0.38895-0.64999-0.18031-0.75157 0.88687 -4 -7 3 6.98 6.80 102 0.07977-0.39026-0.64999 0.16577-0.75157 0.88878 -4 -3 1 61.57 7.87 102 0.07977-0.39342-0.64999 0.44227-0.75157 0.78884 -4 3 -9 19.99 7.23 102 0.07977-0.41224-0.64999 0.85632-0.75157 0.29260 -3 -10 4 17.15 8.82 102 0.07977-0.30774-0.64999-0.04133-0.75157 0.93719 -3 -9 4 38.68 8.89 102 0.07977-0.30788-0.64999 0.02733-0.75157 0.93760 -3 4 -12 8.34 8.77 102 0.07977-0.33997-0.64999 0.92614-0.75157 0.14712 -2 -12 4 3.04 11.60 102 0.07977-0.22991-0.64999-0.18037-0.75157 0.94622 -1 -13 4 -1.27 12.04 102 0.07977-0.15164-0.64999-0.24966-0.75157 0.94949 0 3 -5 -0.99 6.89 102 0.07977-0.09036-0.64999 0.85626-0.75157 0.50402 0 4 -8 335.97 10.12 102 0.07977-0.09617-0.64999 0.92790-0.75157 0.35542 0 5 -16 0.66 11.73 102 0.07977-0.11176-0.64999 0.99302-0.75157-0.03979 0 5 -15 24.66 9.27 102 0.07977-0.10934-0.64999 0.99379-0.75157 0.00987 1 -5 4 480.96 12.07 102 0.07977 0.00650-0.64999 0.30384-0.75157 0.95207 1 5 -17 -1.21 12.00 102 0.07977-0.03456-0.64999 0.99578-0.75157-0.08635 1 5 -16 -0.62 11.65 102 0.07977-0.03353-0.64999 0.99876-0.75157-0.03753 1 5 -15 0.16 9.06 102 0.07977-0.03159-0.64999 0.99938-0.75157 0.01218 1 5 -14 11.33 8.88 102 0.07977-0.02930-0.64999 0.99751-0.75157 0.06209 1 5 -13 39.10 8.99 102 0.07977-0.02746-0.64999 0.99323-0.75157 0.11107 2 3 -5 549.40 12.42 102 0.07977 0.06842-0.64999 0.85862-0.75157 0.51023 2 5 -17 1.49 12.03 102 0.07977 0.04370-0.64999 0.99548-0.75157-0.08331 2 5 -16 3.20 11.55 102 0.07977 0.04576-0.64999 0.99835-0.75157-0.03432 2 5 -15 2.14 9.15 102 0.07977 0.04807-0.64999 0.99879-0.75157 0.01575 2 5 -14 14.48 8.96 102 0.07977 0.04987-0.64999 0.99678-0.75157 0.06522 4 -12 4 28.57 12.35 102 0.07977 0.24282-0.64999-0.17955-0.75157 0.96248 4 -7 4 16.50 7.17 102 0.07977 0.24404-0.64999 0.16664-0.75157 0.96453 4 1 -2 775.89 16.36 102 0.07977 0.23141-0.64999 0.71869-0.75157 0.66464 4 3 -6 13.66 6.74 102 0.07977 0.22431-0.64999 0.85950-0.75157 0.46821 4 4 -9 3.17 6.82 102 0.07977 0.21715-0.64999 0.92560-0.75157 0.31896 6 4 -14 4.25 11.50 102 0.07977 0.36559-0.64999 0.92896-0.75157 0.07802 6 4 -13 19.21 9.14 102 0.07977 0.36555-0.64999 0.92433-0.75157 0.12692 7 2 -7 51.56 9.01 102 0.07977 0.45819-0.64999 0.78905-0.75157 0.42825 8 -1 -3 273.22 11.62 102 0.07977 0.54298-0.64999 0.58072-0.75157 0.62862 8 2 -9 2.66 8.93 102 0.07977 0.53219-0.64999 0.78787-0.75157 0.33245 10 0 -9 4.95 11.75 102 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0.13089-0.71119-0.55133 0.68984-0.81761 0.10163 -6 -2 -3 38.66 8.93 109 0.13089-0.61055-0.55133 0.41273-0.81761 0.64948 -6 -1 -4 61.94 9.88 109 0.13089-0.61220-0.55133 0.48215-0.81761 0.60009 4 -6 3 1.67 8.26 109 0.13089 0.18961-0.55133 0.13669-0.81761 0.97935 10 -3 -3 9.16 11.33 109 0.13089 0.65099-0.55133 0.34550-0.81761 0.70270 -9 -4 -8 1.06 11.68 110 0.13417-0.86061-0.54436 0.26770-0.82152 0.39653 -8 -9 -4 -5.25 12.07 110 0.13417-0.77295-0.54436-0.07813-0.82152 0.59716 -8 -8 -4 3.87 11.59 110 0.13417-0.77510-0.54436-0.00930-0.82152 0.59909 -8 -7 -4 8.77 9.10 110 0.13417-0.77365-0.54436 0.05931-0.82152 0.59810 -8 -3 -6 106.65 10.69 110 0.13417-0.77704-0.54436 0.33626-0.82152 0.49880 -6 -10 -1 23.22 10.59 110 0.13417-0.60998-0.54436-0.14753-0.82152 0.75276 -6 3 -13 3.16 9.14 110 0.13417-0.63288-0.54436 0.75117-0.82152 0.15833 -5 -5 0 26.09 6.94 110 0.13417-0.52680-0.54436 0.19719-0.82152 0.80405 -5 -3 -1 20.58 6.97 110 0.13417-0.53000-0.54436 0.33663-0.82152 0.75533 -5 4 -15 5.15 11.93 110 0.13417-0.56030-0.54436 0.82317-0.82152 0.06303 -5 4 -14 2.30 11.63 110 0.13417-0.55594-0.54436 0.81950-0.82152 0.11226 -4 -3 0 2674.02 26.34 110 0.13417-0.44998-0.54436 0.33598-0.82152 0.80776 -3 -9 2 568.47 12.42 110 0.13417-0.36668-0.54436-0.07819-0.82152 0.91111 -3 -7 2 74.21 7.39 110 0.13417-0.36709-0.54436 0.05962-0.82152 0.91221 -3 5 -12 1.22 8.67 110 0.13417-0.39405-0.54436 0.88842-0.82152 0.21708 -2 4 -7 7.69 6.83 110 0.13417-0.30632-0.54436 0.82098-0.82152 0.46791 -2 5 -10 6.23 6.79 110 0.13417-0.31152-0.54436 0.88965-0.82152 0.31953 -1 -9 3 -1.47 7.65 110 0.13417-0.20789-0.54436-0.07731-0.82152 0.96567 -1 -8 3 100.43 7.77 110 0.13417-0.20777-0.54436-0.00913-0.82152 0.96868 -1 -7 3 4.07 6.74 110 0.13417-0.20759-0.54436 0.06064-0.82152 0.96685 -1 6 -14 16.72 9.13 110 0.13417-0.24143-0.54436 0.96060-0.82152 0.12547 0 -13 2 8.70 11.95 110 0.13417-0.13079-0.54436-0.35420-0.82152 0.91992 0 5 -8 178.17 8.72 110 0.13417-0.14971-0.54436 0.88914-0.82152 0.42527 0 6 -12 47.47 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110 0.13417 0.49171-0.54436 0.47586-0.82152 0.74919 8 0 -3 0.21 6.77 110 0.13417 0.49009-0.54436 0.54509-0.82152 0.70020 -6 -6 -1 8.91 4.91 110 0.13746-0.61148-0.53704 0.12099-0.82537 0.75571 -5 -10 0 97.16 7.43 110 0.13746-0.53200-0.53704-0.15478-0.82537 0.80991 -4 -10 1 264.48 8.79 110 0.13746-0.45021-0.53704-0.15454-0.82537 0.86021 -3 -12 1 -6.70 8.20 110 0.13746-0.37199-0.53704-0.29245-0.82537 0.86512 -3 -8 2 0.64 4.76 110 0.13746-0.36847-0.53704-0.01611-0.82537 0.91343 -2 -11 2 105.27 7.33 110 0.13746-0.29089-0.53704-0.22353-0.82537 0.91765 -1 -12 2 -0.06 6.46 110 0.13746-0.21291-0.53704-0.29339-0.82537 0.92264 -1 6 -13 15.30 6.33 110 0.13746-0.24220-0.53704 0.95122-0.82537 0.17885 0 -10 3 108.51 7.19 110 0.13746-0.13106-0.53704-0.15416-0.82537 0.97317 0 1 -1 955.48 28.54 110 0.13746-0.13895-0.53704 0.60746-0.82537 0.77510 1 -13 2 1.84 8.50 110 0.13746-0.05591-0.53704-0.36128-0.82537 0.92795 1 -5 3 4.85 4.82 110 0.13746-0.05317-0.53704 0.19123-0.82537 0.97690 1 6 -11 167.24 7.76 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112 0.14738-0.22288-0.51645-0.24460-0.83628 0.93397 -1 5 -8 192.49 8.94 112 0.14738-0.24144-0.51645 0.86095-0.83628 0.43634 0 -12 2 8.33 9.34 112 0.14738-0.14328-0.51645-0.31184-0.83628 0.93290 0 -8 3 3.96 6.73 112 0.14738-0.14159-0.51645-0.03620-0.83628 0.98266 0 -7 3 6.96 6.73 112 0.14738-0.14141-0.51645 0.03222-0.83628 0.98276 1 -9 3 54.00 8.23 112 0.14738-0.06281-0.51645-0.10542-0.83628 0.98912 1 -6 3 22.06 6.84 112 0.14738-0.06286-0.51645 0.10185-0.83628 0.98931 1 5 -7 38.57 7.11 112 0.14738-0.08228-0.51645 0.86327-0.83628 0.49337 1 6 -10 151.31 9.75 112 0.14738-0.08886-0.51645 0.93286-0.83628 0.34420 2 -9 3 61.05 9.12 112 0.14738 0.01552-0.51645-0.10627-0.83628 0.99410 2 7 -16 4.89 12.39 112 0.14738-0.02159-0.51645 0.99840-0.83628 0.05011 3 -12 2 10.58 11.82 112 0.14738 0.09282-0.51645-0.31343-0.83628 0.94830 3 -9 3 33.45 8.94 112 0.14738 0.09424-0.51645-0.10496-0.83628 0.99311 3 -8 3 120.48 8.23 112 0.14738 0.09481-0.51645-0.03622-0.83628 0.99791 3 -6 3 54.94 7.66 112 0.14738 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0.37921-0.83628 0.62409 11 -1 -6 -1.62 12.08 112 0.14738 0.70705-0.51645 0.44867-0.83628 0.57530 -8 -9 -5 19.83 8.91 112 0.15077-0.79233-0.50952-0.11245-0.84007 0.56692 -7 -6 -3 6.45 6.22 112 0.15077-0.70937-0.50952 0.09415-0.84007 0.66885 -5 -11 -1 1.28 8.10 112 0.15077-0.54816-0.50952-0.25114-0.84007 0.77492 -4 -11 0 70.42 7.34 112 0.15077-0.46720-0.50952-0.25084-0.84007 0.82821 -4 5 -14 0.77 8.21 112 0.15077-0.49369-0.50952 0.85532-0.84007 0.13437 -2 -12 1 4.40 8.06 112 0.15077-0.30718-0.50952-0.31968-0.84007 0.88323 -2 -9 2 126.77 7.35 112 0.15077-0.30478-0.50952-0.11246-0.84007 0.93258 -2 -6 2 68.04 5.63 112 0.15077-0.30506-0.50952 0.09478-0.84007 0.93430 -2 5 -9 7.31 5.00 112 0.15077-0.32570-0.50952 0.85553-0.84007 0.38803 -1 -4 2 352.41 10.04 112 0.15077-0.22575-0.50952 0.23198-0.84007 0.93604 1 -12 2 5.57 6.40 112 0.15077-0.06805-0.50952-0.31962-0.84007 0.94164 1 -8 3 35.52 5.30 112 0.15077-0.06590-0.50952-0.04318-0.84007 0.99338 1 7 -16 1.16 8.66 112 0.15077-0.10378-0.50952 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0.32737-0.73392-0.00425-0.20348-0.93037 0.61693 -4 -2 -4 142.42 9.39 144 0.32737-0.65120-0.00425-0.13449-0.93037 0.71908 -4 8 -9 1.30 8.98 144 0.32737-0.66202-0.00425 0.55768-0.93037 0.47216 -4 9 -11 40.83 12.60 144 0.32737-0.66628-0.00425 0.62777-0.93037 0.37364 -3 -8 -7 2.27 8.68 144 0.32737-0.58035-0.00425-0.55061-0.93037 0.57556 -3 -5 -4 93.03 7.78 144 0.32737-0.57149-0.00425-0.34119-0.93037 0.72194 -3 -3 -3 415.72 12.30 144 0.32737-0.57052-0.00425-0.20335-0.93037 0.77125 -3 8 -7 4.91 8.64 144 0.32737-0.57708-0.00425 0.55640-0.93037 0.57284 -2 3 -2 161.71 10.85 144 0.32737-0.48975-0.00425 0.21233-0.93037 0.82431 -2 5 -3 29.72 7.18 144 0.32737-0.49115-0.00425 0.35097-0.93037 0.77587 -2 9 -7 8.97 8.84 144 0.32737-0.49890-0.00425 0.62622-0.93037 0.57741 -1 -11 -9 -0.56 11.67 144 0.32737-0.42462-0.00425-0.75545-0.93037 0.48120 -1 -5 -2 129.54 8.31 144 0.32737-0.41040-0.00425-0.34184-0.93037 0.82762 0 6 -2 186.58 8.92 144 0.32737-0.33088-0.00425 0.41908-0.93037 0.83082 0 11 -8 5.24 11.70 144 0.32737-0.34219-0.00425 0.76311-0.93037 0.53315 1 -11 -7 5.16 10.25 144 0.32737-0.26363-0.00425-0.75654-0.93037 0.58714 1 -9 -4 10.63 8.56 144 0.32737-0.25614-0.00425-0.61636-0.93037 0.73343 1 -8 -3 90.44 7.82 144 0.32737-0.25460-0.00425-0.54856-0.93037 0.78519 1 3 0 135.29 10.46 144 0.32737-0.24839-0.00425 0.21192-0.93037 0.93394 2 -6 -1 40.73 7.25 144 0.32737-0.17224-0.00425-0.41036-0.93037 0.88759 2 4 0 112.02 8.39 144 0.32737-0.16938-0.00425 0.28143-0.93037 0.93656 2 10 -5 1.73 8.71 144 0.32737-0.17975-0.00425 0.69456-0.93037 0.68834 3 -11 -6 -3.37 11.58 144 0.32737-0.10343-0.00425-0.75539-0.93037 0.64228 4 -11 -6 1.77 11.63 144 0.32737-0.02549-0.00425-0.75923-0.93037 0.64876 4 11 -6 -4.70 11.64 144 0.32737-0.02445-0.00425 0.76291-0.93037 0.64438 5 -11 -6 -0.12 11.95 144 0.32737 0.05328-0.00425-0.75840-0.93037 0.65129 5 1 1 174.18 10.77 144 0.32737 0.06876-0.00425 0.07383-0.93037 0.99690 5 11 -6 -1.66 11.72 144 0.32737 0.05411-0.00425 0.76183-0.93037 0.64719 6 6 -1 13.21 6.92 144 0.32737 0.14357-0.00425 0.42010-0.93037 0.90128 7 -10 -5 6.26 12.05 144 0.32737 0.21309-0.00425-0.68535-0.93037 0.70458 7 7 -2 1.52 8.77 144 0.32737 0.21959-0.00425 0.48826-0.93037 0.85310 7 8 -3 12.51 8.90 144 0.32737 0.21844-0.00425 0.55962-0.93037 0.80793 7 9 -4 11.70 11.58 144 0.32737 0.21656-0.00425 0.62711-0.93037 0.75668 9 -8 -4 -0.40 12.14 144 0.32737 0.37306-0.00425-0.54873-0.93037 0.76298 9 8 -4 6.08 11.99 144 0.32737 0.37145-0.00425 0.55600-0.93037 0.75856 10 4 -2 -0.52 9.20 144 0.32737 0.45537-0.00425 0.28094-0.93037 0.86318 11 4 -3 25.44 12.51 144 0.32737 0.53338-0.00425 0.28195-0.93037 0.81919 -4 -9 -11 32.89 8.97 144 0.32944-0.66848 0.00406-0.62719-0.92950 0.37224 -4 -8 -9 5.81 6.32 144 0.32944-0.66358 0.00406-0.55794-0.92950 0.47077 -2 -9 -7 13.32 6.23 144 0.32944-0.50113 0.00406-0.62608-0.92950 0.57643 -2 -5 -3 28.83 5.19 144 0.32944-0.49386 0.00406-0.34962-0.92950 0.77499 -2 -3 -2 157.03 8.08 144 0.32944-0.49206 0.00406-0.21183-0.92950 0.82315 -1 5 -2 129.65 7.08 144 0.32944-0.41178 0.00406 0.34220-0.92950 0.82630 -1 11 -9 2.74 8.39 144 0.32944-0.42581 0.00406 0.75517-0.92950 0.47935 0 -11 -8 9.78 8.22 144 0.32944-0.34545 0.00406-0.76267-0.92950 0.53244 0 -6 -2 188.49 7.38 144 0.32944-0.33395 0.00406-0.41908-0.92950 0.82980 1 -3 0 135.76 8.82 144 0.32944-0.25103 0.00406-0.21276-0.92950 0.93305 1 8 -3 93.08 6.08 144 0.32944-0.25634 0.00406 0.54895-0.92950 0.78378 1 11 -7 3.95 6.44 144 0.32944-0.26485 0.00406 0.75653-0.92950 0.58576 2 -10 -5 3.26 6.18 144 0.32944-0.18259 0.00406-0.69468-0.92950 0.68787 2 -4 0 115.88 7.50 144 0.32944-0.17228 0.00406-0.28169-0.92950 0.93599 2 6 -1 40.84 5.31 144 0.32944-0.17441 0.00406 0.41104-0.92950 0.88645 3 11 -6 0.09 8.04 144 0.32944-0.10585 0.00406 0.75562-0.92950 0.64101 7 10 -5 2.48 8.47 144 0.32944 0.21158 0.00406 0.68666-0.92950 0.70366 5 -1 1 177.44 21.63 142 0.32068 0.07577-0.02959-0.03967-0.93249 0.99864 -6 4 -9 76.74 15.88 143 0.32511-0.81611-0.01273 0.28910-0.93121 0.46575 3 1 1 109.46 11.47 144 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65.49 9.27 145 0.33150-0.02278 0.01243 0.60875-0.92865 0.79113 6 -10 -5 -0.04 11.70 145 0.33150 0.13012 0.01243-0.70456-0.92865 0.70265 6 -6 -1 17.69 7.06 145 0.33150 0.13821 0.01243-0.42692-0.92865 0.89880 7 -9 -4 11.14 11.55 145 0.33150 0.21071 0.01243-0.63316-0.92865 0.75310 7 -8 -3 9.35 9.03 145 0.33150 0.21298 0.01243-0.56639-0.92865 0.80450 8 5 -1 -1.92 8.67 145 0.33150 0.29609 0.01243 0.33428-0.92865 0.90632 9 7 -3 3.84 11.73 145 0.33150 0.37239 0.01243 0.47366-0.92865 0.81297 10 6 -3 1.17 11.98 145 0.33150 0.45094 0.01243 0.40327-0.92865 0.81445 -6 -6 -12 -1.83 8.31 145 0.33356-0.83010 0.02080-0.43578-0.92775 0.31374 -4 -7 -8 15.22 6.25 145 0.33356-0.66617 0.02080-0.50589-0.92775 0.52026 -3 10 -10 8.86 8.60 145 0.33356-0.58957 0.02080 0.67157-0.92775 0.42290 -2 -8 -6 2.21 6.00 145 0.33356-0.50481 0.02080-0.57319-0.92775 0.62432 -1 -11 -10 -2.71 8.49 145 0.33356-0.43389 0.02080-0.78186-0.92775 0.42998 0 -8 -4 3.13 4.83 145 0.33356-0.34216 0.02080-0.57429-0.92775 0.72917 0 -7 -3 9.11 4.87 145 0.33356-0.33981 0.02080-0.50515-0.92775 0.77877 0 -4 -1 278.50 9.60 145 0.33356-0.33627 0.02080-0.29871-0.92775 0.87850 1 -10 -6 11.52 6.54 145 0.33356-0.26757 0.02080-0.71400-0.92775 0.63574 1 -5 -1 223.84 8.21 145 0.33356-0.25717 0.02080-0.36770-0.92775 0.88237 1 10 -5 1.66 6.08 145 0.33356-0.26461 0.02080 0.66990-0.92775 0.68159 2 -11 -7 5.19 8.21 145 0.33356-0.19021 0.02080-0.78028-0.92775 0.58781 2 -9 -4 69.51 6.79 145 0.33356-0.18445 0.02080-0.64248-0.92775 0.73578 2 -7 -2 -0.43 4.71 145 0.33356-0.18095 0.02080-0.50518-0.92775 0.83581 2 11 -6 0.56 6.33 145 0.33356-0.18787 0.02080 0.74032-0.92775 0.63661 3 -10 -5 109.36 7.43 145 0.33356-0.10649 0.02080-0.71110-0.92775 0.69028 3 9 -3 29.03 6.46 145 0.33356-0.10256 0.02080 0.60060-0.92775 0.78767 4 8 -2 22.87 5.17 145 0.33356-0.02240 0.02080 0.53332-0.92775 0.84371 4 10 -4 -2.09 6.46 145 0.33356-0.02666 0.02080 0.66956-0.92775 0.74022 5 5 0 31.02 5.16 145 0.33356 0.06011 0.02080 0.32572-0.92775 0.94512 5 8 -2 1.64 6.04 145 0.33356 0.05648 0.02080 0.53354-0.92775 0.84531 5 9 -3 -0.06 6.14 145 0.33356 0.05390 0.02080 0.60379-0.92775 0.79666 7 6 -1 217.17 8.44 145 0.33356 0.21523 0.02080 0.39485-0.92775 0.90129 8 8 -3 17.74 8.31 145 0.33356 0.28998 0.02080 0.53329-0.92775 0.80601 8 9 -4 0.70 8.38 145 0.33356 0.28813 0.02080 0.60210-0.92775 0.75592 10 -4 -2 1.24 15.90 144 0.32720 0.45668-0.00429-0.27203-0.93040 0.86541 -6 6 -11 3.37 14.11 145 0.33353-0.82826 0.02092 0.39384-0.92764 0.36266 -5 -6 -9 0.83 8.81 146 0.33556-0.74704 0.02935-0.44377-0.92663 0.46375 -5 -5 -8 40.17 8.95 146 0.33556-0.74776 0.02935-0.37643-0.92663 0.51552 -5 -4 -7 13.88 7.06 146 0.33556-0.74325 0.02935-0.30634-0.92663 0.56335 -5 8 -11 4.92 11.82 146 0.33556-0.75247 0.02935 0.52426-0.92663 0.36575 -4 -9 -12 -2.56 12.12 146 0.33556-0.67562 0.02935-0.65063-0.92663 0.31914 -4 -5 -6 203.50 9.14 146 0.33556-0.66468 0.02935-0.37608-0.92663 0.61746 -4 6 -6 1442.91 21.83 146 0.33556-0.66169 0.02935 0.38446-0.92663 0.61485 -4 7 -7 32.64 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38.43 9.62 150 0.35033-0.76730 0.09666-0.51125-0.91598 0.35524 -5 -4 -8 286.06 10.51 150 0.35033-0.75884 0.09666-0.37195-0.91598 0.50252 -4 -7 -10 27.82 9.25 150 0.35033-0.68730 0.09666-0.58067-0.91598 0.40791 -4 -5 -7 2.12 6.80 150 0.35033-0.67999 0.09666-0.44222-0.91598 0.55615 -4 -4 -6 140.92 8.59 150 0.35033-0.67754 0.09666-0.37262-0.91598 0.60532 -3 -9 -12 8.13 11.96 150 0.35033-0.61073 0.09666-0.71684-0.91598 0.31162 -3 10 -8 -2.02 9.18 150 0.35033-0.60130 0.09666 0.59385-0.91598 0.50738 -2 -6 -5 150.81 8.28 150 0.35033-0.51878 0.09666-0.51190-0.91598 0.66281 -2 -5 -4 7.42 6.82 150 0.35033-0.51637 0.09666-0.44247-0.91598 0.71123 -2 11 -8 0.48 11.76 150 0.35033-0.52325 0.09666 0.66305-0.91598 0.51137 -1 -9 -8 4.74 8.71 150 0.35033-0.44590 0.09666-0.71780-0.91598 0.51645 -1 -7 -5 -0.61 6.84 150 0.35033-0.43976 0.09666-0.58096-0.91598 0.66644 -1 -5 -3 2.76 6.68 150 0.35033-0.43508 0.09666-0.44310-0.91598 0.76523 0 -10 -9 1.82 9.09 150 0.35033-0.37120 0.09666-0.79006-0.91598 0.47290 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150 0.35217-0.53124 0.10503-0.72679-0.91423 0.41321 -1 -6 -4 218.09 7.60 150 0.35217-0.43978 0.10503-0.52033-0.91423 0.71308 -1 8 -3 32.79 5.32 150 0.35217-0.43712 0.10503 0.44740-0.91423 0.76040 -1 9 -4 -0.85 6.09 150 0.35217-0.44016 0.10503 0.51865-0.91423 0.71299 0 -9 -7 71.90 6.76 150 0.35217-0.36576 0.10503-0.72590-0.91423 0.56706 0 -3 -1 370.14 11.94 150 0.35217-0.35487 0.10503-0.31418-0.91423 0.86487 0 3 0 -0.46 5.85 150 0.35217-0.35182 0.10503 0.10270-0.91423 0.91445 0 12 -7 7.88 8.46 150 0.35217-0.36701 0.10503 0.72454-0.91423 0.56644 1 -10 -8 2.40 6.32 150 0.35217-0.28990 0.10503-0.79482-0.91423 0.52102 1 5 0 188.09 7.77 150 0.35217-0.27332 0.10503 0.24116-0.91423 0.91847 2 -7 -3 1.93 4.82 150 0.35217-0.20155 0.10503-0.59008-0.91423 0.77296 2 -6 -2 69.88 5.86 150 0.35217-0.19932 0.10503-0.52021-0.91423 0.82162 2 6 0 44.70 5.43 150 0.35217-0.19484 0.10503 0.31053-0.91423 0.92095 2 9 -2 133.28 7.41 150 0.35217-0.19891 0.10503 0.51814-0.91423 0.82215 2 10 -3 7.28 6.16 150 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151 0.35402-0.27750 0.11349-0.38951-0.91268 0.86619 1 -2 0 1468.32 29.77 151 0.35402-0.27574 0.11349-0.25313-0.91268 0.91513 1 12 -6 2.17 11.77 151 0.35402-0.28807 0.11349 0.71860-0.91268 0.61927 2 -11 -10 0.02 12.03 151 0.35402-0.21813 0.11349-0.87435-0.91268 0.42505 2 11 -4 21.55 9.09 151 0.35402-0.20520 0.11349 0.64951-0.91268 0.72202 3 -10 -7 3.76 8.96 151 0.35402-0.13257 0.11349-0.80331-0.91268 0.57545 3 -5 -1 157.59 8.96 151 0.35402-0.12005 0.11349-0.46022-0.91268 0.87432 3 12 -5 -5.21 11.84 151 0.35402-0.12883 0.11349 0.71892-0.91268 0.67615 4 -11 -9 -3.05 12.13 151 0.35402-0.05876 0.11349-0.87364-0.91268 0.48110 4 7 0 8.79 6.81 151 0.35402-0.03879 0.11349 0.37065-0.91268 0.92508 5 -9 -5 5.05 8.93 151 0.35402 0.02882 0.11349-0.73330-0.91268 0.68069 5 7 0 148.09 8.21 151 0.35402 0.03940 0.11349 0.37070-0.91268 0.92835 6 -10 -7 14.54 12.12 151 0.35402 0.10344 0.11349-0.80596-0.91268 0.58753 6 4 1 11.96 6.91 151 0.35402 0.12090 0.11349 0.16390-0.91268 0.98311 7 -7 -3 5.87 9.01 151 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0.36785-0.53575 0.17962 0.57965-0.89629 0.58994 -1 -9 -11 6.41 9.06 155 0.36785-0.47005 0.17962-0.80214-0.89629 0.34946 -1 -6 -5 -2.73 6.71 155 0.36785-0.45647 0.17962-0.59229-0.89629 0.64498 -1 -4 -3 212.48 9.54 155 0.36785-0.45401 0.17962-0.45708-0.89629 0.74565 -1 6 -1 184.09 8.87 155 0.36785-0.44784 0.17962 0.23523-0.89629 0.84262 -1 8 -2 96.88 7.80 155 0.36785-0.44970 0.17962 0.37264-0.89629 0.79149 0 -8 -7 16.26 8.61 155 0.36785-0.38249 0.17962-0.73097-0.89629 0.54959 0 -5 -3 851.26 14.36 155 0.36785-0.37387 0.17962-0.52593-0.89629 0.74825 0 9 -2 1.76 6.75 155 0.36785-0.37277 0.17962 0.44364-0.89629 0.79792 1 -9 -8 41.79 8.97 155 0.36785-0.30599 0.17962-0.80013-0.89629 0.50371 2 -7 -4 104.45 7.80 155 0.36785-0.21904 0.17962-0.66408-0.89629 0.70589 2 -4 -1 68.73 7.97 155 0.36785-0.21311 0.17962-0.45745-0.89629 0.85418 2 5 1 64.91 7.49 155 0.36785-0.20863 0.17962 0.16661-0.89629 0.95381 3 -10 -9 -2.30 11.51 155 0.36785-0.15024 0.17962-0.87088-0.89629 0.46242 3 -8 -5 52.68 8.92 155 0.36785-0.14212 0.17962-0.73300-0.89629 0.65962 3 -3 0 70.08 8.78 155 0.36785-0.13100 0.17962-0.38752-0.89629 0.90668 3 6 1 3.72 6.55 155 0.36785-0.12899 0.17962 0.23594-0.89629 0.95656 4 11 -2 1.19 8.98 155 0.36785-0.05710 0.17962 0.58051-0.89629 0.80835 5 11 -2 7.44 11.51 155 0.36785 0.02174 0.17962 0.58122-0.89629 0.81291 5 12 -3 19.40 12.44 155 0.36785 0.01973 0.17962 0.64817-0.89629 0.76057 7 8 0 7.28 8.91 155 0.36785 0.18332 0.17962 0.37237-0.89629 0.91626 8 -6 -3 26.90 9.30 155 0.36785 0.25485 0.17962-0.59375-0.89629 0.77401 8 3 1 2.69 8.66 155 0.36785 0.26523 0.17962 0.02839-0.89629 0.97406 8 4 1 8.85 8.69 155 0.36785 0.26334 0.17962 0.09687-0.89629 0.96996 8 7 0 9.86 9.01 155 0.36785 0.26313 0.17962 0.30548-0.89629 0.92504 9 6 0 4.16 9.06 155 0.36785 0.34003 0.17962 0.23524-0.89629 0.92377 9 8 -1 3.68 11.88 155 0.36785 0.33899 0.17962 0.37413-0.89629 0.87629 11 4 -1 51.13 12.96 155 0.36785 0.49570 0.17962 0.09671-0.89629 0.88313 -4 -6 -11 38.83 6.78 155 0.36938-0.70813 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0.18769 0.64325-0.89390 0.75923 5 10 -1 17.07 6.62 155 0.36938 0.02151 0.18769 0.50549-0.89390 0.86212 6 10 -1 3.50 6.44 155 0.36938 0.10109 0.18769 0.50240-0.89390 0.86164 6 11 -2 22.27 8.89 155 0.36938 0.09858 0.18769 0.57460-0.89390 0.81527 7 -9 -7 1.75 8.28 155 0.36938 0.16727 0.18769-0.80892-0.89390 0.57109 8 9 -1 -3.40 8.36 155 0.36938 0.25902 0.18769 0.43550-0.89390 0.87182 10 7 -1 18.14 8.84 155 0.36938 0.41563 0.18769 0.29660-0.89390 0.87631 -7 5 -13 0.58 22.54 153 0.36270-0.94174 0.15502 0.19150-0.90292 0.23610 -6 2 -8 70.74 17.59 153 0.36270-0.85193 0.15502-0.01622-0.90292 0.48687 -5 5 -6 162.54 12.18 155 0.36946-0.77460 0.18791 0.15775-0.89394 0.57913 2 0 1 0.61 11.33 155 0.36946-0.21069 0.18791-0.18838-0.89394 0.94975 11 1 -1 1.05 14.38 155 0.36946 0.49477 0.18791-0.11916-0.89394 0.88099 -6 -2 -11 23.81 9.12 156 0.37103-0.86858 0.19607-0.33549-0.89150 0.32826 -6 7 -10 15.27 11.77 156 0.37103-0.86400 0.19607 0.28845-0.89150 0.37571 -5 8 -8 119.77 10.76 156 0.37103-0.78160 0.19607 0.35684-0.89150 0.47798 -4 -5 -9 25.54 8.85 156 0.37103-0.70293 0.19607-0.54062-0.89150 0.43283 -4 7 -5 72.75 8.21 156 0.37103-0.69462 0.19607 0.28789-0.89150 0.62920 -4 10 -8 28.57 11.89 156 0.37103-0.70150 0.19607 0.49584-0.89150 0.48145 -3 -5 -7 50.54 7.36 156 0.37103-0.62346 0.19607-0.54260-0.89150 0.53681 -3 6 -3 56.40 7.63 156 0.37103-0.61318 0.19607 0.21912-0.89150 0.73229 -3 9 -5 4.32 8.67 156 0.37103-0.61795 0.19607 0.42704-0.89150 0.63315 -3 10 -6 4.18 9.02 156 0.37103-0.61889 0.19607 0.49511-0.89150 0.58274 -2 -8 -11 26.48 9.31 156 0.37103-0.55244 0.19607-0.74963-0.89150 0.34178 -1 -9 -12 3.40 11.72 156 0.37103-0.47601 0.19607-0.82085-0.89150 0.29621 -1 -8 -9 14.26 8.67 156 0.37103-0.46995 0.19607-0.75083-0.89150 0.44474 0 -9 -10 6.99 9.09 156 0.37103-0.39289 0.19607-0.82086-0.89150 0.39850 0 8 -1 125.08 8.01 156 0.37103-0.37217 0.19607 0.35659-0.89150 0.84018 1 3 1 143.28 9.95 156 0.37103-0.28965 0.19607 0.01215-0.89150 0.94403 1 9 -1 8.10 6.79 156 0.37103-0.29412 0.19607 0.42553-0.89150 0.84227 1 12 -4 2.97 11.58 156 0.37103-0.30101 0.19607 0.63543-0.89150 0.69715 2 -6 -3 8.23 6.81 156 0.37103-0.21945 0.19607-0.61174-0.89150 0.75075 2 8 0 27.56 7.14 156 0.37103-0.21413 0.19607 0.35754-0.89150 0.89886 3 10 -1 28.23 9.09 156 0.37103-0.13643 0.19607 0.49535-0.89150 0.85092 3 12 -3 44.54 12.03 156 0.37103-0.14103 0.19607 0.63439-0.89150 0.75280 4 -10 -9 15.67 11.65 156 0.37103-0.07506 0.19607-0.88439-0.89150 0.45801 4 -8 -5 20.79 8.69 156 0.37103-0.06644 0.19607-0.74843-0.89150 0.65726 4 7 1 12.42 6.97 156 0.37103-0.05477 0.19607 0.28781-0.89150 0.95268 5 -10 -9 -6.93 12.08 156 0.37103 0.00391 0.19607-0.88661-0.89150 0.46316 5 -8 -5 9.50 8.82 156 0.37103 0.01217 0.19607-0.75012-0.89150 0.66187 5 7 1 -2.57 6.68 156 0.37103 0.02433 0.19607 0.28774-0.89150 0.95729 5 9 0 131.14 9.78 156 0.37103 0.02268 0.19607 0.42470-0.89150 0.90478 6 -10 -9 6.11 12.26 156 0.37103 0.08208 0.19607-0.88366-0.89150 0.46481 6 -8 -5 4.52 8.87 156 0.37103 0.09087 0.19607-0.74690-0.89150 0.66268 7 -7 -4 11.47 8.99 156 0.37103 0.17203 0.19607-0.68157-0.89150 0.71853 7 6 1 33.66 8.88 156 0.37103 0.18212 0.19607 0.21977-0.89150 0.96498 8 -8 -6 0.36 11.74 156 0.37103 0.24711 0.19607-0.75078-0.89150 0.62318 9 -7 -5 1.29 11.81 156 0.37103 0.32581 0.19607-0.67825-0.89150 0.67244 10 2 0 56.63 10.13 156 0.37103 0.41537 0.19607-0.05759-0.89150 0.92453 10 3 0 2.56 9.01 156 0.37103 0.41660 0.19607 0.01133-0.89150 0.92570 10 4 0 31.56 9.82 156 0.37103 0.41503 0.19607 0.08063-0.89150 0.92278 11 5 -1 16.06 12.76 156 0.37103 0.49249 0.19607 0.14988-0.89150 0.87709 -5 -5 -13 36.02 8.64 156 0.37268-0.79332 0.20444-0.54963-0.88904 0.22904 -3 -7 -11 19.56 6.55 156 0.37268-0.63025 0.20444-0.68733-0.88904 0.33509 -2 12 -7 8.11 8.57 156 0.37268-0.54424 0.20444 0.62597-0.88904 0.53485 -1 -7 -7 20.30 5.09 156 0.37268-0.46533 0.20444-0.68686-0.88904 0.53903 0 6 0 194.88 7.55 156 0.37268-0.37266 0.20444 0.21089-0.88904 0.88721 1 -10 -12 11.32 8.49 156 0.37268-0.31879 0.20444-0.89535-0.88904 0.29824 1 -7 -5 24.57 5.13 156 0.37268-0.30449 0.20444-0.68852-0.88904 0.64555 1 2 1 638.97 17.12 156 0.37268-0.29118 0.20444-0.06508-0.88904 0.94156 1 4 1 16.40 5.39 156 0.37268-0.29089 0.20444 0.07175-0.88904 0.94106 2 -9 -8 22.49 6.57 156 0.37268-0.23158 0.20444-0.82783-0.88904 0.50159 2 -8 -6 32.95 6.36 156 0.37268-0.22876 0.20444-0.75857-0.88904 0.60072 2 -5 -2 182.34 7.79 156 0.37268-0.21846 0.20444-0.55016-0.88904 0.79666 2 6 1 0.71 4.75 156 0.37268-0.21234 0.20444 0.21106-0.88904 0.94428 3 -10 -10 8.82 8.39 156 0.37268-0.15734 0.20444-0.89764-0.88904 0.40555 4 -9 -7 10.28 6.38 156 0.37268-0.07218 0.20444-0.82606-0.88904 0.55617 4 9 0 49.23 6.73 156 0.37268-0.05837 0.20444 0.41795-0.88904 0.90301 6 -9 -7 7.40 8.19 156 0.37268 0.08518 0.20444-0.82528-0.88904 0.56205 6 7 1 36.36 6.49 156 0.37268 0.10108 0.20444 0.27995-0.88904 0.95781 6 9 0 31.15 6.66 156 0.37268 0.09966 0.20444 0.41736-0.88904 0.90626 7 10 -1 -5.42 8.44 156 0.37268 0.17672 0.20444 0.48713-0.88904 0.86145 8 5 1 56.01 7.00 156 0.37268 0.25916 0.20444 0.14105-0.88904 0.96532 -4 1 -4 66.64 15.64 155 0.36768-0.69094 0.17983-0.11035-0.89626 0.68474 -7 2 -12 5.95 13.12 156 0.37092-0.94756 0.19619-0.05714-0.89146 0.27422 -6 0 -9 -1.15 10.52 156 0.37244-0.86412 0.20439-0.20412-0.88895 0.42336 -5 7 -7 0.82 10.67 156 0.37244-0.78039 0.20439 0.27988-0.88895 0.52550 6 -3 0 0.54 8.22 156 0.37244 0.10013 0.20439-0.41213-0.88895 0.90941 8 1 1 174.48 12.19 156 0.37244 0.25907 0.20439-0.13557-0.88895 0.96650 -7 0 -14 0.86 11.89 157 0.37397-0.95427 0.21271-0.21277-0.88638 0.16986 -6 -3 -13 -0.50 9.21 157 0.37397-0.87075 0.21271-0.41793-0.88638 0.22257 -6 -1 -10 116.60 10.52 157 0.37397-0.86838 0.21271-0.28123-0.88638 0.37181 -6 8 -11 2.55 12.09 157 0.37397-0.86885 0.21271 0.34128-0.88638 0.32155 -5 -3 -9 4.18 6.68 157 0.37397-0.78433 0.21271-0.41906-0.88638 0.42436 -5 -2 -8 1.00 6.73 157 0.37397-0.78605 0.21271-0.35142-0.88638 0.47536 -5 -1 -7 33.87 7.49 157 0.37397-0.78193 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53.96 7.33 176 0.40704-0.50181 0.50843-0.78471-0.74222 0.34405 -1 10 2 0.52 8.62 176 0.40704-0.48114 0.50843 0.18334-0.74222 0.83658 0 -3 -4 225.97 10.17 176 0.40704-0.41494 0.50843-0.71622-0.74222 0.54463 0 9 3 4.81 6.78 176 0.40704-0.40158 0.50843 0.11471-0.74222 0.89124 0 12 2 8.25 9.20 176 0.40704-0.40276 0.50843 0.32114-0.74222 0.83946 1 -6 -12 17.27 8.87 176 0.40704-0.35180 0.50843-0.92124-0.74222 0.15255 1 13 2 2.81 11.98 176 0.40704-0.32472 0.50843 0.39244-0.74222 0.84599 2 -6 -10 -1.27 8.53 176 0.40704-0.27071 0.50843-0.92542-0.74222 0.25509 2 -4 -4 84.87 7.97 176 0.40704-0.25797 0.50843-0.78597-0.74222 0.55192 2 5 4 13.59 6.80 176 0.40704-0.24155 0.50843-0.16241-0.74222 0.94623 3 11 4 0.26 9.01 176 0.40704-0.16187 0.50843 0.25151-0.74222 0.94644 4 -7 -15 1.43 12.08 176 0.40704-0.12238 0.50843-0.99232-0.74222 0.01396 4 -7 -14 -5.03 11.82 176 0.40704-0.11992 0.50843-0.99054-0.74222 0.06301 4 -6 -8 463.43 12.15 176 0.40704-0.10803 0.50843-0.92499-0.74222 0.36088 4 -5 -5 3.05 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-0.67 8.37 176 0.40721-0.36166 0.51561-0.93157-0.73727-0.05071 1 -6 -14 5.19 6.29 176 0.40721-0.35733 0.51561-0.93191-0.73727 0.04881 1 -6 -13 0.16 6.29 176 0.40721-0.35510 0.51561-0.92818-0.73727 0.09797 1 -4 -5 235.37 8.16 176 0.40721-0.33848 0.51561-0.79271-0.73727 0.49380 1 -3 -3 721.85 14.88 176 0.40721-0.33422 0.51561-0.72291-0.73727 0.59153 2 10 4 19.06 6.49 176 0.40721-0.24267 0.51561 0.17640-0.73727 0.94295 3 -6 -9 86.69 6.99 176 0.40721-0.18934 0.51561-0.93170-0.73727 0.30324 5 -7 -14 7.93 8.45 176 0.40721-0.04219 0.51561-0.99720-0.73727 0.06135 5 -5 -5 -0.11 4.83 176 0.40721-0.02323 0.51561-0.86168-0.73727 0.50672 5 3 4 8.59 4.96 176 0.40721-0.00517 0.51561-0.30826-0.73727 0.95070 5 7 5 13.71 6.29 176 0.40721-0.00285 0.51561-0.03223-0.73727 0.99856 5 8 5 5.08 6.18 176 0.40721-0.00313 0.51561 0.03812-0.73727 0.99825 9 7 4 -0.77 8.39 176 0.40721 0.30880 0.51561-0.03089-0.73727 0.96252 9 8 4 10.91 8.79 176 0.40721 0.30924 0.51561 0.03797-0.73727 0.96204 ; _shelx_hkl_checksum 82994 _shelx_res_file ; IP1-1931.res created by SHELXL-2014/7 TITL IP1-1931 in P2(1)/n: FM-2 [ligand] CELL 0.71073 9.0313 10.2649 14.3901 90.000 92.350 90.000 ZERR 4.000 0.0005 0.0006 0.0010 0.000 0.008 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N O UNIT 64 40 16 8 TEMP -60 SIZE .25 .30 .45 OMIT -2 52 L.S. 6 BOND $H FMAP 2 PLAN -10 MPLA N1 C1 C2 C3 C4 C5 MPLA C6 N2 N3 C7 C8 N4 MPLA C9 C10 C11 C12 O1 MPLA C13 C14 C15 C16 O2 MPLA C6 N2 N3 C7 C8 N4 ACTA WGHT 0.034000 FVAR 0.72648 O1 4 0.086780 0.467078 0.585378 11.00000 0.03258 0.04065 = 0.04617 0.01194 -0.00781 -0.00872 O2 4 0.408018 0.420063 0.827445 11.00000 0.03695 0.05602 = 0.03367 0.00688 0.00534 0.01176 N1 3 0.308806 0.823485 0.449361 11.00000 0.03651 0.03451 = 0.03886 0.00429 -0.00026 -0.00403 N2 3 0.586614 0.641956 0.578111 11.00000 0.03312 0.05337 = 0.04695 0.01437 -0.00006 -0.00501 N3 3 0.597821 0.555383 0.647634 11.00000 0.03219 0.05251 = 0.04439 0.01209 -0.00122 -0.00304 N4 3 0.326597 0.610548 0.563869 11.00000 0.03127 0.03128 = 0.03279 0.00052 0.00125 -0.00311 C1 1 0.301305 0.923195 0.390074 11.00000 0.04547 0.03569 = 0.04755 0.00762 -0.00261 -0.00397 AFIX 43 H1 2 0.207010 0.955108 0.371760 11.00000 -1.20000 AFIX 0 C2 1 0.423132 0.982419 0.353952 11.00000 0.05702 0.03663 = 0.04362 0.00650 0.00422 -0.00828 AFIX 43 H2 2 0.411801 1.051245 0.311162 11.00000 -1.20000 AFIX 0 C3 1 0.560876 0.938764 0.381788 11.00000 0.05225 0.04204 = 0.04333 0.00023 0.01485 -0.01391 AFIX 43 H3 2 0.646149 0.977234 0.358395 11.00000 -1.20000 AFIX 0 C4 1 0.573145 0.837361 0.444751 11.00000 0.03519 0.04038 = 0.03928 -0.00210 0.00652 -0.00514 AFIX 43 H4 2 0.666699 0.806847 0.465911 11.00000 -1.20000 AFIX 0 C5 1 0.444840 0.781633 0.476026 11.00000 0.03493 0.03107 = 0.02957 -0.00412 0.00260 -0.00478 C6 1 0.452050 0.672225 0.543918 11.00000 0.02840 0.03428 = 0.02962 -0.00333 0.00145 -0.00277 C7 1 0.476008 0.496370 0.676216 11.00000 0.02961 0.03424 = 0.02989 -0.00309 0.00100 0.00021 C8 1 0.338139 0.516819 0.628224 11.00000 0.03003 0.02965 = 0.02626 -0.00167 0.00270 0.00081 C9 1 0.208684 0.435964 0.640173 11.00000 0.02845 0.03214 = 0.02915 -0.00079 -0.00320 0.00102 C10 1 0.179973 0.325059 0.688002 11.00000 0.03842 0.03554 = 0.03923 0.00688 -0.00085 -0.00052 AFIX 43 H10 2 0.244751 0.282160 0.730664 11.00000 -1.20000 AFIX 0 C11 1 0.034411 0.286817 0.661297 11.00000 0.04297 0.03524 = 0.04341 0.00445 0.00231 -0.01094 AFIX 43 H11 2 -0.016535 0.213604 0.682766 11.00000 -1.20000 AFIX 0 C12 1 -0.017129 0.374710 0.599594 11.00000 0.03217 0.04467 = 0.04444 0.00342 -0.00269 -0.01420 AFIX 43 H12 2 -0.111999 0.372766 0.570209 11.00000 -1.20000 AFIX 0 C13 1 0.502284 0.409566 0.755317 11.00000 0.02769 0.03666 = 0.03013 -0.00189 0.00169 -0.00215 C14 1 0.604148 0.317784 0.774738 11.00000 0.03340 0.04051 = 0.04237 -0.00228 0.00201 0.00286 AFIX 43 H14 2 0.681866 0.292876 0.737037 11.00000 -1.20000 AFIX 0 C15 1 0.572802 0.265242 0.862802 11.00000 0.04215 0.04305 = 0.04749 0.01036 -0.00558 0.00392 AFIX 43 H15 2 0.624957 0.198440 0.894587 11.00000 -1.20000 AFIX 0 C16 1 0.454810 0.329173 0.891709 11.00000 0.04102 0.05964 = 0.03496 0.01580 0.00093 -0.00114 AFIX 43 H16 2 0.409877 0.313921 0.948473 11.00000 -1.20000 AFIX 0 HKLF 4 REM IP1-1931 in P2(1)/n: FM-2 [ligand] REM R1 = 0.0294 for 1612 Fo > 4sig(Fo) and 0.0517 for all 2582 data REM 199 parameters refined using 0 restraints END WGHT 0.0339 0.0000 REM Highest difference peak 0.136, deepest hole -0.180, 1-sigma level 0.029 Q1 1 0.3672 0.3444 0.9433 11.00000 0.05 0.14 Q2 1 -0.1243 0.4288 0.5558 11.00000 0.05 0.14 Q3 1 -0.0959 0.4007 0.5383 11.00000 0.05 0.14 Q4 1 0.5984 0.4011 0.7718 11.00000 0.05 0.13 Q5 1 0.4883 0.4654 0.7178 11.00000 0.05 0.13 Q6 1 0.4178 0.4781 0.6349 11.00000 0.05 0.12 Q7 1 0.2226 0.3582 0.6426 11.00000 0.05 0.11 Q8 1 0.5013 0.8351 0.4781 11.00000 0.05 0.11 Q9 1 0.2730 0.4932 0.6415 11.00000 0.05 0.11 Q10 1 0.6998 0.5073 0.6774 11.00000 0.05 0.10 ; _shelx_res_checksum 57487 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy O O1 0.08678(11) 0.46708(9) 0.58538(6) 0.0401(3) Uani d 1 O O2 0.40802(11) 0.42006(10) 0.82745(6) 0.0421(3) Uani d 1 N N1 0.30881(13) 0.82349(10) 0.44936(8) 0.0367(3) Uani d 1 N N2 0.58661(14) 0.64196(12) 0.57811(8) 0.0445(3) Uani d 1 N N3 0.59782(13) 0.55538(12) 0.64763(8) 0.0431(3) Uani d 1 N N4 0.32660(13) 0.61055(10) 0.56387(7) 0.0318(3) Uani d 1 C C1 0.30131(18) 0.92320(13) 0.39007(10) 0.0430(4) Uani d 1 H H1 0.2070 0.9551 0.3718 0.052 Uiso calc 1 C C2 0.42313(19) 0.98242(14) 0.35395(10) 0.0457(4) Uani d 1 H H2 0.4118 1.0512 0.3112 0.055 Uiso calc 1 C C3 0.56088(19) 0.93876(14) 0.38179(10) 0.0455(4) Uani d 1 H H3 0.6461 0.9772 0.3584 0.055 Uiso calc 1 C C4 0.57315(16) 0.83736(13) 0.44475(9) 0.0381(3) Uani d 1 H H4 0.6667 0.8068 0.4659 0.046 Uiso calc 1 C C5 0.44484(16) 0.78163(12) 0.47603(9) 0.0318(3) Uani d 1 C C6 0.45205(15) 0.67223(12) 0.54392(9) 0.0308(3) Uani d 1 C C7 0.47601(15) 0.49637(12) 0.67622(9) 0.0313(3) Uani d 1 C C8 0.33814(15) 0.51682(12) 0.62822(8) 0.0286(3) Uani d 1 C C9 0.20868(15) 0.43596(12) 0.64017(9) 0.0300(3) Uani d 1 C C10 0.17997(16) 0.32506(13) 0.68800(10) 0.0378(3) Uani d 1 H H10 0.2448 0.2822 0.7307 0.045 Uiso calc 1 C C11 0.03441(17) 0.28682(14) 0.66130(10) 0.0405(4) Uani d 1 H H11 -0.0165 0.2136 0.6828 0.049 Uiso calc 1 C C12 -0.01713(17) 0.37471(13) 0.59959(10) 0.0405(4) Uani d 1 H H12 -0.1120 0.3728 0.5702 0.049 Uiso calc 1 C C13 0.50228(15) 0.40957(13) 0.75532(9) 0.0315(3) Uani d 1 C C14 0.60415(16) 0.31778(13) 0.77474(10) 0.0387(3) Uani d 1 H H14 0.6819 0.2929 0.7370 0.046 Uiso calc 1 C C15 0.57280(17) 0.26524(14) 0.86280(10) 0.0444(4) Uani d 1 H H15 0.6250 0.1984 0.8946 0.053 Uiso calc 1 C C16 0.45481(17) 0.32917(15) 0.89171(10) 0.0452(4) Uani d 1 H H16 0.4099 0.3139 0.9485 0.054 Uiso calc 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1 0.0326(6) 0.0407(5) 0.0462(6) -0.0087(5) -0.0078(5) 0.0119(5) O2 0.0370(6) 0.0560(6) 0.0337(5) 0.0118(5) 0.0053(5) 0.0069(5) N1 0.0365(8) 0.0345(6) 0.0389(6) -0.0040(5) -0.0003(5) 0.0043(5) N2 0.0331(8) 0.0534(8) 0.0470(7) -0.0050(6) -0.0001(6) 0.0144(6) N3 0.0322(8) 0.0525(8) 0.0444(7) -0.0030(6) -0.0012(6) 0.0121(6) N4 0.0313(7) 0.0313(6) 0.0328(6) -0.0031(5) 0.0013(5) 0.0005(5) C1 0.0455(10) 0.0357(8) 0.0476(8) -0.0040(7) -0.0026(7) 0.0076(7) C2 0.0570(12) 0.0366(8) 0.0436(8) -0.0083(8) 0.0042(8) 0.0065(7) C3 0.0523(11) 0.0420(8) 0.0433(8) -0.0139(8) 0.0149(8) 0.0002(7) C4 0.0352(9) 0.0404(8) 0.0393(8) -0.0051(7) 0.0065(7) -0.0021(6) C5 0.0349(9) 0.0311(7) 0.0296(7) -0.0048(6) 0.0026(6) -0.0041(6) C6 0.0284(9) 0.0343(7) 0.0296(7) -0.0028(6) 0.0015(6) -0.0033(6) C7 0.0296(9) 0.0342(7) 0.0299(7) 0.0002(6) 0.0010(6) -0.0031(5) C8 0.0300(8) 0.0297(7) 0.0263(6) 0.0008(6) 0.0027(6) -0.0017(5) C9 0.0284(8) 0.0321(7) 0.0292(7) 0.0010(6) -0.0032(6) -0.0008(6) C10 0.0384(9) 0.0355(7) 0.0392(8) -0.0005(6) -0.0009(6) 0.0069(6) C11 0.0430(10) 0.0352(8) 0.0434(8) -0.0109(7) 0.0023(7) 0.0044(7) C12 0.0322(9) 0.0447(8) 0.0444(8) -0.0142(7) -0.0027(7) 0.0034(7) C13 0.0277(8) 0.0367(7) 0.0301(7) -0.0022(6) 0.0017(6) -0.0019(6) C14 0.0334(9) 0.0405(8) 0.0424(8) 0.0029(7) 0.0020(6) -0.0023(6) C15 0.0422(10) 0.0430(8) 0.0475(9) 0.0039(7) -0.0056(7) 0.0104(7) C16 0.0410(10) 0.0596(10) 0.0350(8) -0.0011(8) 0.0009(7) 0.0158(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C12 O1 C9 107.22(10) C16 O2 C13 105.87(11) C1 N1 C5 116.79(12) C6 N2 N3 118.15(11) C7 N3 N2 119.55(12) C8 N4 C6 116.50(12) N1 C1 C2 124.07(16) N1 C1 H1 118.0 C2 C1 H1 118.0 C3 C2 C1 118.44(14) C3 C2 H2 120.8 C1 C2 H2 120.8 C2 C3 C4 119.13(14) C2 C3 H3 120.4 C4 C3 H3 120.4 C3 C4 C5 118.62(15) C3 C4 H4 120.7 C5 C4 H4 120.7 N1 C5 C4 122.91(13) N1 C5 C6 116.36(11) C4 C5 C6 120.71(13) N2 C6 N4 125.37(12) N2 C6 C5 115.73(11) N4 C6 C5 118.87(12) N3 C7 C8 120.14(12) N3 C7 C13 114.08(13) C8 C7 C13 125.73(12) N4 C8 C7 119.16(12) N4 C8 C9 117.00(12) C7 C8 C9 123.72(11) C10 C9 O1 108.78(12) C10 C9 C8 135.26(13) O1 C9 C8 115.63(11) C9 C10 C11 106.85(13) C9 C10 H10 126.6 C11 C10 H10 126.6 C12 C11 C10 106.77(12) C12 C11 H11 126.6 C10 C11 H11 126.6 C11 C12 O1 110.37(13) C11 C12 H12 124.8 O1 C12 H12 124.8 C14 C13 O2 109.85(11) C14 C13 C7 133.01(12) O2 C13 C7 117.14(12) C13 C14 C15 107.10(12) C13 C14 H14 126.5 C15 C14 H14 126.5 C16 C15 C14 106.47(13) C16 C15 H15 126.8 C14 C15 H15 126.8 C15 C16 O2 110.71(12) C15 C16 H16 124.6 O2 C16 H16 124.6 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C12 1.3554(16) O1 C9 1.3655(16) O2 C16 1.3683(17) O2 C13 1.3734(15) N1 C1 1.3324(17) N1 C5 1.3426(18) N2 C6 1.3291(18) N2 N3 1.3389(16) N3 C7 1.3355(17) N4 C8 1.3365(15) N4 C6 1.3393(17) C1 C2 1.377(2) C1 H1 0.9400 C2 C3 1.367(2) C2 H2 0.9400 C3 C4 1.3815(19) C3 H3 0.9400 C4 C5 1.3839(18) C4 H4 0.9400 C5 C6 1.4882(18) C7 C8 1.4145(19) C7 C13 1.4573(18) C8 C9 1.4498(18) C9 C10 1.3607(18) C10 C11 1.410(2) C10 H10 0.9400 C11 C12 1.336(2) C11 H11 0.9400 C12 H12 0.9400 C13 C14 1.3383(19) C14 C15 1.4165(19) C14 H14 0.9400 C15 C16 1.333(2) C15 H15 0.9400 C16 H16 0.9400 _cod_database_fobs_code 2021698