#------------------------------------------------------------------------------ #$Date: 2019-07-10 07:34:45 +0300 (Wed, 10 Jul 2019) $ #$Revision: 216919 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/17/2021724.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021724 _cell_angle_alpha 90.000 _cell_angle_beta 103.193 _cell_angle_gamma 90.000 _cell_length_a 10.9993 _cell_length_b 15.2290 _cell_length_c 24.0797 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file cu3152LESUREFormIIsup5.hkl _cod_data_source_block LESUREFormII _shelx_title ' RED1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 356.18 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2757.86 3307.04 246.68 o 3 0 0 6515.43 7255.66 335.98 o 4 0 0 3136.00 3575.28 333.97 o 5 0 0 16352.55 17884.80 610.29 o 6 0 0 1029.37 1087.22 221.39 o 7 0 0 20231.77 18925.22 1051.24 o 8 0 0 1110.35 1048.47 179.02 o 9 0 0 2266.76 2055.21 264.22 o 10 0 0 3667.07 4383.58 399.74 o 11 0 0 1228.70 1373.55 378.79 o 12 0 0 1803.93 2847.43 829.12 o 13 0 0 141.26 599.29 357.19 o 2 1 0 3475.51 3784.43 110.66 o 3 1 0 1720.83 1857.40 113.95 o 4 1 0 11810.53 12458.95 408.39 o 5 1 0 1872.37 1751.76 138.14 o 6 1 0 7851.75 6847.20 334.12 o 7 1 0 1794.53 1678.58 174.43 o 8 1 0 6482.64 6264.98 304.51 o 9 1 0 864.81 1125.17 138.79 o 10 1 0 2.24 73.98 38.61 o 11 1 0 38.12 -0.99 79.57 o 12 1 0 7.55 306.35 186.17 o 13 1 0 899.00 514.93 297.21 o 2 2 0 903.67 1216.45 54.08 o 3 2 0 3362.25 3850.20 139.43 o 4 2 0 634.96 750.76 85.35 o 5 2 0 4.23 23.27 33.59 o 6 2 0 2428.81 2496.86 204.79 o 7 2 0 84.22 182.21 72.92 o 8 2 0 6450.11 6468.38 419.54 o 9 2 0 28.26 50.87 28.95 o 10 2 0 1930.85 2473.00 295.00 o 11 2 0 1616.58 2032.91 272.95 o 12 2 0 595.01 1032.65 269.26 o 13 2 0 217.40 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