#------------------------------------------------------------------------------ #$Date: 2019-07-30 07:29:31 +0300 (Tue, 30 Jul 2019) $ #$Revision: 217305 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/17/2021734.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021734 _cell_angle_alpha 90.000 _cell_angle_beta 113.077 _cell_angle_gamma 90.000 _cell_length_a 12.6321 _cell_length_b 13.9512 _cell_length_c 14.7923 _exptl_crystal_F_000 1052.00 _reflns_d_resolution_high 0.8200 _cod_data_source_file cu3139Isup2.hkl _cod_data_source_block I _shelx_title ' [b-D-Val]2-ASC.2Cu2+.CO3(2-).H2O in P2(1) @20070731' _shelx_refln_list_code 4 _shelx_f_calc_maximum 243.04 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -14 0 648.49 1200.59 123.59 o 1 -13 0 693.32 1255.04 143.79 o 0 -12 0 830.17 1232.71 95.51 o 1 -12 0 877.26 1241.43 90.26 o 2 -12 0 834.08 915.11 62.79 o 1 -11 0 37.26 41.04 23.46 o 2 -11 0 478.17 470.56 35.00 o 4 -11 0 608.46 724.95 93.63 o 5 -11 0 53.88 134.99 51.32 o 1 -10 0 125.00 181.26 28.72 o 2 -10 0 379.39 449.94 31.35 o 3 -10 0 1211.20 1154.67 96.83 o 5 -10 0 240.42 290.59 61.03 o 7 -10 0 6.05 15.88 37.92 o 8 -10 0 4.79 9.96 46.34 o 9 -10 0 155.36 212.02 79.29 o 2 -9 0 1017.30 951.27 54.37 o 3 -9 0 2490.98 2356.52 180.73 o 4 -9 0 28.86 39.69 13.16 o 5 -9 0 46.24 51.32 35.08 o 6 -9 0 88.52 79.76 38.99 o 7 -9 0 686.48 776.26 105.95 o 9 -9 0 523.55 633.33 114.25 o 10 -9 0 571.86 647.08 123.37 o 11 -9 0 60.03 65.66 75.49 o 2 -8 0 1580.16 1277.22 121.24 o 3 -8 0 468.51 414.76 81.30 o 4 -8 0 4149.31 3901.69 271.16 o 5 -8 0 573.12 523.95 74.54 o 7 -8 0 296.33 270.57 64.35 o 8 -8 0 273.37 441.34 86.16 o 9 -8 0 520.58 645.30 113.30 o 10 -8 0 408.74 516.24 109.62 o 11 -8 0 244.85 281.59 98.25 o 12 -8 0 314.62 339.90 108.68 o 2 -7 0 169.12 170.75 16.11 o 4 -7 0 3587.67 3382.25 236.79 o 6 -7 0 24.09 45.98 31.88 o 7 -7 0 507.08 756.71 103.34 o 8 -7 0 417.44 369.29 77.86 o 10 -7 0 121.20 137.71 74.66 o 11 -7 0 94.36 111.17 76.68 o 12 -7 0 151.77 180.50 97.54 o 2 -6 0 1670.32 1705.04 88.06 o 4 -6 0 2430.56 2272.49 163.55 o 7 -6 0 248.57 373.67 72.65 o 8 -6 0 35.30 54.63 44.44 o 9 -6 0 172.13 223.75 74.19 o 10 -6 0 680.95 801.62 132.97 o 11 -6 0 70.11 65.66 70.04 o 12 -6 0 194.57 296.76 100.50 o 13 -6 0 50.35 84.97 89.83 o 1 -5 0 2462.55 2735.04 124.97 o 2 -5 0 3006.74 2437.58 185.83 o 6 -5 0 119.56 229.92 54.99 o 8 -5 0 746.16 902.95 121.71 o 10 -5 0 25.54 35.55 51.67 o 11 -5 0 115.81 135.82 74.31 o 12 -5 0 58.27 53.69 68.15 o 13 -5 0 115.10 173.74 104.29 o 1 -4 0 2688.56 2310.75 104.71 o 2 -4 0 417.09 677.66 69.09 o 3 -4 0 384.41 366.56 32.59 o 7 -4 0 151.48 241.41 63.52 o 8 -4 0 397.86 473.34 93.86 o 9 -4 0 87.13 143.40 67.32 o 10 -4 0 1020.95 1279.47 172.67 o 11 -4 0 177.77 216.52 84.86 o 12 -4 0 298.40 335.16 113.18 o 13 -4 0 8.69 17.78 82.60 o 1 -3 0 4166.36 5178.32 228.75 o 5 -3 0 160.59 284.67 54.28 o 6 -3 0 38.01 91.61 41.36 o 8 -3 0 279.66 237.74 69.80 o 9 -3 0 2437.33 2992.46 295.10 o 10 -3 0 171.45 217.59 78.46 o 11 -3 0 185.15 366.30 169.83 o 12 -3 0 29.02 69.73 58.08 o 13 -3 0 302.27 404.84 136.53 o 2 -2 0 10161.34 10990.21 743.20 o 6 -2 0 2425.24 3741.35 343.81 o 7 -2 0 511.18 811.10 116.38 o 8 -2 0 145.21 254.11 89.48 o 9 -2 0 511.17 570.29 108.80 o 10 -2 0 1177.78 1286.94 183.93 o 11 -2 0 294.53 513.09 131.73 o 12 -2 0 293.04 386.23 124.56 o 13 -2 0 384.93 464.10 145.89 o 14 -2 0 29.09 26.19 88.17 o 2 -1 0 4030.37 4094.04 334.09 o 3 -1 0 5892.77 11309.96 780.41 o 4 -1 0 1592.59 1952.12 143.88 o 5 -1 0 1189.84 2065.76 136.26 o 6 -1 0 120.63 164.68 30.57 o 7 -1 0 882.08 1082.14 137.24 o 8 -1 0 148.11 235.78 44.62 o 9 -1 0 1821.42 2041.98 226.36 o 10 -1 0 40.04 55.49 34.90 o 11 -1 0 76.52 98.92 43.26 o 12 -1 0 7.84 29.15 70.63 o 13 -1 0 761.20 930.80 187.84 o 14 -1 0 37.84 38.64 91.02 o -15 0 0 0.00 41.96 61.36 o -13 0 0 0.01 57.69 39.04 o 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2824.46 2740.81 141.74 o 3 5 0 4665.66 4138.84 225.33 o 4 5 0 1719.97 2020.18 192.23 o 5 5 0 1829.02 1584.64 166.04 o 6 5 0 111.94 168.91 31.57 o 7 5 0 1808.55 1733.35 210.95 o 8 5 0 674.94 502.60 71.59 o 9 5 0 2062.41 2574.46 292.14 o 10 5 0 17.87 47.88 47.29 o 11 5 0 113.99 100.26 71.46 o 12 5 0 47.65 28.44 73.95 o 13 5 0 98.32 161.53 107.14 o 0 6 0 12039.83 10599.71 720.44 o 1 6 0 3320.22 2745.38 147.14 o 2 6 0 1704.42 1956.91 92.94 o 3 6 0 3004.49 2742.63 162.05 o 4 6 0 2745.73 2336.61 216.52 o 5 6 0 777.31 866.33 98.48 o 6 6 0 751.85 843.53 112.29 o 7 6 0 217.40 192.64 32.21 o 8 6 0 39.50 27.73 25.61 o 9 6 0 165.60 174.80 49.20 o 10 6 0 603.06 389.91 102.04 o 11 6 0 60.18 46.22 58.78 o 12 6 0 180.29 219.72 99.91 o 13 6 0 50.59 87.82 98.37 o 1 7 0 5521.69 5206.19 251.83 o 2 7 0 178.97 217.39 25.56 o 3 7 0 12887.31 11532.68 578.09 o 4 7 0 3540.73 3414.44 175.30 o 5 7 0 444.74 489.44 72.29 o 6 7 0 19.66 36.86 17.18 o 7 7 0 496.53 520.75 105.24 o 8 7 0 397.90 204.51 46.15 o 9 7 0 1214.26 1096.25 175.04 o 10 7 0 100.15 101.74 45.43 o 11 7 0 89.95 46.10 63.88 o 12 7 0 148.91 164.14 90.19 o 0 8 0 11573.11 9898.91 491.75 o 1 8 0 3180.79 2770.67 130.12 o 2 8 0 1627.12 1287.94 73.47 o 3 8 0 499.69 408.04 38.54 o 4 8 0 4011.98 3880.26 177.80 o 5 8 0 618.43 427.44 58.72 o 6 8 0 648.16 696.11 86.04 o 7 8 0 256.40 146.72 53.39 o 8 8 0 279.56 190.93 45.05 o 9 8 0 521.18 459.83 120.65 o 10 8 0 413.03 327.06 69.13 o 11 8 0 248.79 188.74 68.92 o 12 8 0 288.02 207.40 103.34 o 1 9 0 2208.32 1726.07 91.10 o 2 9 0 991.04 759.31 55.21 o 3 9 0 2718.17 2436.42 121.56 o 4 9 0 15.72 19.50 11.08 o 5 9 0 29.21 22.46 14.87 o 6 9 0 78.16 42.14 21.53 o 7 9 0 844.17 588.30 114.84 o 8 9 0 603.88 412.31 102.40 o 9 9 0 601.51 410.34 90.13 o 10 9 0 575.40 371.27 73.87 o 11 9 0 55.46 30.15 51.81 o 12 9 0 65.30 43.26 71.34 o 1 10 0 119.78 101.09 18.70 o 2 10 0 349.75 300.41 35.93 o 3 10 0 1203.80 1034.87 69.09 o 4 10 0 2232.10 1946.44 109.14 o 5 10 0 292.96 292.56 50.68 o 6 10 0 1108.37 840.61 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398.82 59.25 o 2 14 0 686.36 575.13 70.32 o 3 14 0 19.45 12.94 30.01 o 4 14 0 75.01 55.46 57.83 o 5 14 0 184.04 139.61 74.78 o 6 14 0 657.74 412.43 109.03 o 7 14 0 140.36 116.74 83.20 o 8 14 0 96.95 60.09 85.92 o 1 15 0 227.80 191.79 49.55 o 2 15 0 287.59 297.09 58.68 o 3 15 0 355.65 320.34 84.97 o 4 15 0 351.45 198.39 77.51 o 5 15 0 38.92 16.95 59.61 o 6 15 0 52.94 69.09 70.63 o 0 16 0 601.52 695.32 121.59 o 1 16 0 456.14 399.50 69.13 o 2 16 0 17.96 36.74 56.77 o 3 16 0 9.90 26.67 57.36 o -1 -15 1 96.10 163.73 67.54 o 0 -15 1 317.14 614.74 85.62 o -2 -14 1 375.15 663.38 96.23 o -1 -14 1 553.75 1103.45 115.74 o 0 -14 1 192.57 327.50 60.24 o 1 -14 1 42.87 57.83 56.77 o -3 -13 1 300.33 551.44 86.01 o -2 -13 1 345.08 657.72 86.72 o -1 -13 1 201.31 347.74 42.98 o 0 -13 1 788.71 1445.39 162.01 o 1 -13 1 413.32 620.42 92.56 o -2 -12 1 138.57 191.70 30.10 o -1 -12 1 233.13 347.29 37.78 o 0 -12 1 183.26 307.18 46.93 o 1 -12 1 657.17 812.57 63.22 o 2 -12 1 64.95 34.98 21.07 o 3 -12 1 398.44 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51.20 o 7 -9 1 94.86 134.04 49.89 o 8 -9 1 86.66 142.33 56.89 o 9 -9 1 244.11 301.97 86.51 o 10 -9 1 45.19 52.74 67.43 o 11 -9 1 95.39 130.60 90.31 o -12 -8 1 175.16 186.07 96.59 o -11 -8 1 112.40 110.69 76.20 o -10 -8 1 79.62 71.11 63.29 o -9 -8 1 172.41 228.14 72.53 o -6 -8 1 394.65 469.91 71.23 o -5 -8 1 615.49 837.18 98.01 o -4 -8 1 174.07 162.84 48.59 o -3 -8 1 1474.49 1189.69 71.25 o -2 -8 1 607.50 538.93 44.37 o 2 -8 1 108.82 127.73 18.93 o 3 -8 1 874.88 863.25 73.72 o 4 -8 1 430.92 488.99 42.19 o 6 -8 1 357.03 397.61 71.58 o 7 -8 1 107.15 149.68 52.26 o 8 -8 1 86.23 112.82 53.81 o 9 -8 1 626.89 741.54 122.78 o 10 -8 1 696.29 722.93 127.16 o 11 -8 1 550.85 570.40 133.68 o 12 -8 1 136.79 199.69 107.02 o -13 -7 1 144.05 89.95 92.91 o -12 -7 1 23.46 14.10 69.09 o -11 -7 1 98.05 125.98 73.83 o -10 -7 1 903.00 1083.45 157.50 o -9 -7 1 130.95 231.34 71.46 o -7 -7 1 528.20 606.20 93.15 o -6 -7 1 392.91 468.36 71.11 o -5 -7 1 210.62 203.96 23.74 o -3 -7 1 962.10 1066.26 105.24 o -2 -7 1 1597.51 1458.34 73.99 o 2 -7 1 6270.34 5257.49 365.26 o 3 -7 1 817.38 728.62 60.44 o 4 -7 1 1235.56 1376.41 96.00 o 5 -7 1 241.85 283.24 31.81 o 7 -7 1 114.19 138.31 51.08 o 8 -7 1 212.50 233.47 69.80 o 9 -7 1 109.08 173.50 70.16 o 10 -7 1 100.02 114.01 72.17 o 11 -7 1 127.85 148.02 88.29 o 12 -7 1 157.53 230.98 99.67 o -13 -6 1 224.21 286.92 112.59 o -12 -6 1 50.99 76.44 68.03 o -11 -6 1 166.92 208.58 83.20 o -10 -6 1 155.59 203.96 71.70 o -8 -6 1 157.74 212.61 61.63 o -6 -6 1 333.23 444.90 71.11 o -5 -6 1 973.57 1337.78 134.28 o -4 -6 1 242.04 251.30 74.96 o -2 -6 1 576.44 592.69 34.45 o 2 -6 1 423.51 468.48 54.16 o 3 -6 1 5299.94 4463.33 302.21 o 6 -6 1 175.47 213.92 52.38 o 7 -6 1 127.00 211.66 60.56 o 8 -6 1 49.54 117.33 57.00 o 10 -6 1 140.66 207.28 83.20 o 11 -6 1 439.31 552.27 124.32 o 12 -6 1 89.46 123.96 93.74 o -13 -5 1 153.88 220.67 107.25 o -12 -5 1 95.42 93.98 76.80 o -10 -5 1 850.82 944.55 141.74 o -9 -5 1 210.91 325.67 81.42 o -7 -5 1 131.70 147.90 49.78 o -6 -5 1 80.05 122.31 41.36 o -4 -5 1 3117.56 3358.55 231.34 o -2 -5 1 3796.89 4007.44 175.41 o 0 -5 1 2715.64 2950.39 212.38 o 1 -5 1 4336.57 3403.94 242.36 o 2 -5 1 4500.00 3386.04 240.23 o 3 -5 1 1059.74 990.30 73.12 o 4 -5 1 835.38 883.04 68.50 o 5 -5 1 834.83 1204.33 129.77 o 7 -5 1 30.30 106.42 48.71 o 8 -5 1 803.65 984.85 135.11 o 9 -5 1 237.95 380.90 90.90 o 10 -5 1 320.74 337.53 97.42 o 11 -5 1 150.60 106.07 81.42 o 12 -5 1 172.44 168.29 90.19 o 13 -5 1 0.42 -2.73 71.11 o -14 -4 1 1.93 -6.76 85.09 o -13 -4 1 512.13 652.65 152.41 o -12 -4 1 80.30 86.04 69.57 o -11 -4 1 720.16 656.45 125.27 o -10 -4 1 73.90 130.60 62.93 o -9 -4 1 519.83 717.12 110.45 o -8 -4 1 251.46 393.23 79.29 o -5 -4 1 31.11 5.93 21.21 o -4 -4 1 460.52 660.12 74.54 o -2 -4 1 233.79 175.18 13.50 o 0 -4 1 1880.57 1655.32 78.80 o 1 -4 1 3287.52 2947.07 220.55 o 2 -4 1 51.35 65.23 11.44 o 3 -4 1 6858.91 7665.91 523.35 o 7 -4 1 246.50 421.43 81.18 o 8 -4 1 46.58 49.78 45.04 o 9 -4 1 1634.32 2372.28 268.43 o 10 -4 1 14.02 21.45 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