#------------------------------------------------------------------------------ #$Date: 2019-07-30 07:30:28 +0300 (Tue, 30 Jul 2019) $ #$Revision: 217307 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/17/2021738.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021738 _cell_angle_alpha 90.000 _cell_angle_beta 91.836 _cell_angle_gamma 90.000 _cell_length_a 9.1043 _cell_length_b 21.4770 _cell_length_c 13.8106 _exptl_crystal_F_000 1020.00 _reflns_d_resolution_high 0.8121 _cod_data_source_file fp3073IIIsup3.hkl _cod_data_source_block III _shelx_title ' cmpd3 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 163.38 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 -23 0 57.42 59.33 3.16 o 5 -22 0 9.82 11.99 1.46 o 5 -21 0 120.36 128.39 4.38 o 6 -21 0 14.82 16.43 1.34 o 6 -20 0 37.49 36.67 2.19 o 7 -20 0 22.18 26.53 1.06 o 6 -19 0 4.46 8.43 1.28 o 7 -19 0 35.91 41.37 2.01 o 0 -18 0 562.55 510.97 16.05 o 1 -18 0 2.38 2.75 1.17 o 2 -18 0 9.74 11.78 2.02 o 6 -18 0 4.04 4.38 1.17 o 7 -18 0 44.59 50.88 2.16 o 8 -18 0 2.60 3.13 0.47 o 1 -17 0 86.52 79.80 3.47 o 2 -17 0 166.01 173.56 5.29 o 3 -17 0 92.07 95.32 4.02 o 6 -17 0 192.39 190.15 6.57 o 7 -17 0 6.89 5.25 2.19 o 8 -17 0 37.69 37.68 0.99 o 0 -16 0 330.13 328.53 12.52 o 1 -16 0 134.55 136.32 4.31 o 2 -16 0 294.60 280.43 9.70 o 3 -16 0 358.53 374.59 9.59 o 4 -16 0 159.31 158.75 5.69 o 6 -16 0 68.31 65.65 3.89 o 7 -16 0 35.39 41.27 2.67 o 8 -16 0 4.29 6.17 0.56 o 1 -15 0 246.47 236.66 6.01 o 2 -15 0 15.51 13.54 1.98 o 3 -15 0 549.45 499.01 13.03 o 4 -15 0 157.57 136.89 5.52 o 5 -15 0 93.45 82.19 15.81 o 6 -15 0 154.21 139.82 5.84 o 7 -15 0 73.57 80.97 5.71 o 8 -15 0 197.84 195.40 2.98 o 9 -15 0 49.88 46.39 1.11 o 0 -14 0 825.19 837.03 23.34 o 1 -14 0 9.18 15.45 1.70 o 2 -14 0 196.45 203.95 5.75 o 3 -14 0 633.91 618.64 10.83 o 4 -14 0 1490.20 1531.06 19.15 o 5 -14 0 246.13 257.09 8.30 o 6 -14 0 284.04 239.03 8.02 o 7 -14 0 64.94 62.03 2.86 o 8 -14 0 9.64 11.90 0.87 o 9 -14 0 15.84 17.79 0.72 o 1 -13 0 357.23 372.19 6.64 o 2 -13 0 428.55 447.00 11.02 o 3 -13 0 363.41 384.83 7.66 o 4 -13 0 731.61 742.86 11.65 o 5 -13 0 23.21 29.77 2.80 o 6 -13 0 121.67 111.86 5.35 o 7 -13 0 6.75 6.30 1.39 o 8 -13 0 24.47 23.22 2.78 o 9 -13 0 249.00 254.76 3.75 o 0 -12 0 1744.37 1939.96 42.07 o 1 -12 0 208.74 216.37 5.41 o 2 -12 0 537.04 598.78 9.88 o 3 -12 0 352.30 339.08 6.91 o 4 -12 0 418.37 415.52 8.01 o 5 -12 0 1181.02 1224.92 16.80 o 6 -12 0 135.15 142.92 6.09 o 7 -12 0 91.51 85.20 5.71 o 8 -12 0 30.40 28.38 1.54 o 9 -12 0 13.44 14.88 0.84 o 1 -11 0 4367.08 4140.60 40.08 o 2 -11 0 211.11 229.77 5.38 o 3 -11 0 654.28 598.35 9.36 o 4 -11 0 659.29 660.17 8.73 o 5 -11 0 363.40 386.37 6.71 o 6 -11 0 167.46 155.91 4.52 o 7 -11 0 16.53 11.92 1.75 o 8 -11 0 344.71 329.14 5.37 o 9 -11 0 70.66 71.58 1.61 o 10 -11 0 2.87 4.34 0.48 o 0 -10 0 1324.32 1670.44 155.14 o 1 -10 0 6385.09 6142.85 60.22 o 2 -10 0 1328.73 1417.15 16.94 o 3 -10 0 389.64 368.85 5.62 o 4 -10 0 22.88 22.58 1.53 o 5 -10 0 686.49 684.43 9.41 o 6 -10 0 112.99 107.04 3.73 o 7 -10 0 279.44 306.27 7.06 o 8 -10 0 718.20 652.51 9.55 o 9 -10 0 75.45 65.50 1.53 o 10 -10 0 51.37 48.30 1.14 o 1 -9 0 99.70 99.48 3.23 o 2 -9 0 562.72 546.34 8.47 o 3 -9 0 3073.98 3268.26 68.66 o 4 -9 0 477.98 549.46 6.80 o 5 -9 0 118.38 110.87 3.30 o 6 -9 0 8.61 10.21 1.46 o 7 -9 0 41.03 41.46 1.86 o 8 -9 0 281.03 280.53 4.84 o 9 -9 0 2.02 2.73 0.56 o 10 -9 0 82.58 80.81 2.33 o 0 -8 0 1234.69 1432.89 22.18 o 1 -8 0 3030.53 2909.75 23.21 o 2 -8 0 622.45 632.28 7.17 o 3 -8 0 644.98 691.13 8.07 o 4 -8 0 297.36 296.75 4.52 o 5 -8 0 134.34 129.81 6.08 o 6 -8 0 87.95 90.83 3.27 o 7 -8 0 50.13 52.90 2.96 o 8 -8 0 509.09 471.64 6.81 o 9 -8 0 134.00 140.56 2.14 o 10 -8 0 65.36 64.55 2.13 o 1 -7 0 3192.38 3021.86 34.17 o 2 -7 0 679.66 671.55 6.86 o 3 -7 0 1941.63 1761.46 24.83 o 4 -7 0 578.02 617.31 11.73 o 5 -7 0 89.62 91.67 2.89 o 6 -7 0 474.10 484.97 8.01 o 7 -7 0 462.01 506.85 9.19 o 8 -7 0 119.21 119.05 3.23 o 9 -7 0 144.13 136.81 2.16 o 10 -7 0 10.16 10.89 0.73 o 0 -6 0 1714.42 1980.21 27.55 o 1 -6 0 4856.66 4513.66 50.77 o 2 -6 0 2231.91 2123.08 15.84 o 3 -6 0 872.57 950.86 22.40 o 4 -6 0 3326.59 3402.09 29.98 o 5 -6 0 1491.96 1411.25 15.49 o 6 -6 0 181.08 183.11 4.42 o 7 -6 0 50.22 44.27 2.95 o 8 -6 0 744.09 712.71 8.15 o 9 -6 0 93.15 86.79 1.93 o 10 -6 0 26.40 25.07 1.00 o 1 -5 0 11842.02 12318.68 110.86 o 2 -5 0 785.01 631.51 7.90 o 3 -5 0 1485.31 1385.44 25.14 o 4 -5 0 128.15 187.45 4.84 o 5 -5 0 475.90 402.63 6.13 o 6 -5 0 555.56 571.43 9.03 o 7 -5 0 306.75 282.90 6.88 o 8 -5 0 2051.29 1910.85 21.99 o 9 -5 0 251.56 237.27 3.42 o 10 -5 0 0.20 1.01 0.54 o 11 -5 0 5.60 5.35 1.46 o 0 -4 0 1229.89 1502.18 26.36 o 1 -4 0 11499.06 11250.36 110.24 o 2 -4 0 820.02 983.24 10.51 o 3 -4 0 1994.29 1701.73 15.55 o 4 -4 0 2619.25 2599.17 36.34 o 5 -4 0 1668.53 1743.73 18.05 o 6 -4 0 510.86 528.62 8.42 o 7 -4 0 566.83 593.25 11.36 o 8 -4 0 69.08 80.03 2.13 o 9 -4 0 208.22 201.82 2.74 o 10 -4 0 17.25 14.53 0.78 o 11 -4 0 5.43 5.57 0.62 o 1 -3 0 6041.68 5807.77 106.53 o 2 -3 0 1047.98 1093.80 15.66 o 3 -3 0 906.71 874.52 7.02 o 4 -3 0 1877.94 1905.27 38.25 o 5 -3 0 420.35 471.25 10.57 o 6 -3 0 221.01 241.65 5.59 o 7 -3 0 228.25 224.09 7.48 o 8 -3 0 935.44 863.57 18.81 o 9 -3 0 173.36 173.70 2.76 o 10 -3 0 112.82 108.21 3.12 o 11 -3 0 7.46 9.39 1.00 o 0 -2 0 21325.50 19088.43 287.51 o 1 -2 0 595.90 639.76 7.20 o 2 -2 0 9196.39 8918.77 154.54 o 3 -2 0 769.16 734.26 9.74 o 4 -2 0 291.80 305.32 4.15 o 5 -2 0 193.83 224.80 4.03 o 6 -2 0 790.81 809.01 12.24 o 7 -2 0 945.91 947.73 18.55 o 8 -2 0 345.30 366.97 4.05 o 9 -2 0 112.62 130.42 3.44 o 10 -2 0 8.38 9.59 0.80 o 11 -2 0 3.59 2.72 0.50 o 1 -1 0 1383.47 1479.22 21.41 o 2 -1 0 1787.28 1842.26 21.09 o 3 -1 0 6415.01 6397.50 69.30 o 4 -1 0 3148.69 3330.61 26.60 o 5 -1 0 592.51 562.22 7.65 o 6 -1 0 1480.25 1463.35 16.73 o 7 -1 0 959.82 977.26 18.90 o 8 -1 0 160.44 154.65 2.43 o 9 -1 0 357.10 311.12 4.47 o 10 -1 0 1.26 1.53 0.52 o 11 -1 0 0.83 0.14 0.33 o 1 0 0 26693.29 24064.59 353.91 o 2 0 0 156.59 199.43 4.29 o 3 0 0 1152.50 1076.39 11.34 o 4 0 0 15.90 13.12 1.45 o 5 0 0 75.48 79.39 2.39 o 6 0 0 15.11 17.46 2.42 o 7 0 0 1019.78 899.45 17.68 o 8 0 0 117.40 111.08 4.48 o 9 0 0 661.93 693.03 7.96 o 10 0 0 16.54 29.04 1.19 o 11 0 0 0.31 2.10 0.45 o 1 1 0 1394.29 1500.94 21.36 o 2 1 0 1786.35 1820.92 20.95 o 3 1 0 6426.01 6427.71 74.61 o 4 1 0 3144.83 3354.46 25.58 o 5 1 0 585.42 543.33 8.52 o 6 1 0 1476.04 1444.35 19.74 o 7 1 0 965.70 1006.43 18.90 o 8 1 0 160.12 156.47 2.28 o 9 1 0 359.51 314.06 4.40 o 10 1 0 1.24 0.86 0.46 o 11 1 0 0.79 0.06 0.65 o 0 2 0 21385.62 19380.46 927.06 o 1 2 0 601.83 632.56 7.91 o 2 2 0 9211.62 8732.93 99.61 o 3 2 0 771.81 765.13 6.22 o 4 2 0 292.05 304.16 3.36 o 5 2 0 194.10 230.45 3.79 o 6 2 0 790.22 798.40 12.72 o 7 2 0 951.27 963.82 26.99 o 8 2 0 344.98 364.59 3.34 o 9 2 0 114.95 134.36 2.07 o 10 2 0 8.38 10.26 0.77 o 11 2 0 3.24 3.27 0.39 o 1 3 0 6045.37 5885.18 69.30 o 2 3 0 1042.31 1064.21 14.95 o 3 3 0 909.84 895.36 6.66 o 4 3 0 1864.06 1910.20 20.30 o 5 3 0 412.42 460.43 11.10 o 6 3 0 221.06 236.12 5.00 o 7 3 0 231.45 220.56 7.18 o 8 3 0 939.71 875.34 6.64 o 9 3 0 176.35 178.94 2.43 o 10 3 0 111.28 107.66 1.82 o 11 3 0 7.01 8.03 0.54 o 0 4 0 1221.12 1500.08 31.61 o 1 4 0 11487.16 11054.14 139.37 o 2 4 0 821.97 970.33 17.13 o 3 4 0 1987.68 1711.07 14.21 o 4 4 0 2645.16 2587.27 17.61 o 5 4 0 1665.45 1701.36 14.85 o 6 4 0 514.36 530.16 8.22 o 7 4 0 566.96 576.84 11.18 o 8 4 0 70.44 82.79 1.46 o 9 4 0 210.14 201.64 2.31 o 10 4 0 16.32 14.27 0.69 o 11 4 0 5.94 5.04 0.58 o 1 5 0 11834.95 12185.48 132.35 o 2 5 0 781.67 617.87 4.69 o 3 5 0 1486.85 1395.38 8.94 o 4 5 0 126.72 192.62 2.95 o 5 5 0 471.35 395.72 6.22 o 6 5 0 557.62 563.53 8.67 o 7 5 0 304.27 277.88 10.03 o 8 5 0 2049.96 1929.57 11.31 o 9 5 0 248.96 235.69 2.54 o 10 5 0 0.26 0.67 0.34 o 0 6 0 1712.11 1955.52 46.20 o 1 6 0 4841.22 4549.39 31.95 o 2 6 0 2216.99 2133.32 16.69 o 3 6 0 871.46 934.70 8.89 o 4 6 0 3326.48 3449.34 23.24 o 5 6 0 1496.45 1403.55 14.36 o 6 6 0 180.28 170.29 4.50 o 7 6 0 50.52 41.75 3.94 o 8 6 0 742.94 712.18 4.66 o 9 6 0 93.28 87.06 1.31 o 10 6 0 25.90 23.34 0.75 o 1 7 0 3189.28 2984.52 33.23 o 2 7 0 673.25 678.02 7.43 o 3 7 0 1932.57 1763.93 12.68 o 4 7 0 577.16 611.75 7.44 o 5 7 0 87.58 93.07 2.64 o 6 7 0 471.33 466.46 7.07 o 7 7 0 463.34 526.33 15.44 o 8 7 0 118.09 117.33 1.47 o 9 7 0 142.91 135.11 1.47 o 10 7 0 9.97 11.92 0.54 o 0 8 0 1238.35 1430.50 14.02 o 1 8 0 3027.32 2982.93 16.28 o 2 8 0 623.34 649.86 4.65 o 3 8 0 651.93 703.80 6.80 o 4 8 0 301.70 294.71 3.97 o 5 8 0 131.35 133.57 3.63 o 6 8 0 87.36 88.13 2.97 o 7 8 0 51.15 54.12 4.15 o 8 8 0 513.58 478.69 3.11 o 9 8 0 135.10 141.16 1.47 o 10 8 0 64.27 64.99 1.13 o 1 9 0 101.56 111.14 1.48 o 2 9 0 571.72 563.93 4.66 o 3 9 0 3068.43 3298.80 24.24 o 4 9 0 475.43 554.29 6.13 o 5 9 0 115.56 102.91 2.50 o 6 9 0 8.07 9.43 1.35 o 7 9 0 41.38 41.52 0.74 o 8 9 0 275.87 272.26 2.13 o 9 9 0 2.06 3.73 0.40 o 10 9 0 80.63 80.08 1.17 o 0 10 0 1337.29 1691.68 38.86 o 1 10 0 6409.03 6301.02 34.44 o 2 10 0 1325.54 1424.93 9.81 o 3 10 0 392.82 370.37 4.30 o 4 10 0 24.53 23.18 1.35 o 5 10 0 694.64 702.93 7.79 o 6 10 0 112.40 102.78 4.02 o 7 10 0 277.34 303.03 2.04 o 8 10 0 720.26 670.94 3.81 o 9 10 0 74.86 62.90 0.90 o 10 10 0 51.70 48.90 0.87 o 1 11 0 4376.52 4207.39 25.05 o 2 11 0 213.52 233.24 3.05 o 3 11 0 662.12 613.28 6.18 o 4 11 0 663.65 662.13 7.29 o 5 11 0 366.08 389.11 5.82 o 6 11 0 166.95 157.04 4.44 o 7 11 0 16.30 11.27 0.44 o 8 11 0 346.72 333.35 2.11 o 9 11 0 70.43 69.59 0.89 o 10 11 0 2.79 3.38 0.40 o 0 12 0 1758.37 1987.61 20.53 o 1 12 0 207.05 223.77 2.71 o 2 12 0 544.32 598.29 5.76 o 3 12 0 348.58 342.78 4.38 o 4 12 0 420.95 415.57 5.60 o 5 12 0 1178.97 1213.61 12.67 o 6 12 0 134.87 137.07 2.79 o 7 12 0 89.54 86.51 0.95 o 8 12 0 30.78 32.17 0.60 o 9 12 0 13.26 14.40 0.52 o 1 13 0 361.53 385.23 3.94 o 2 13 0 430.18 446.08 6.24 o 3 13 0 362.03 377.45 4.81 o 4 13 0 731.46 734.31 8.74 o 5 13 0 23.39 28.02 1.86 o 6 13 0 120.99 124.98 1.42 o 7 13 0 7.56 8.47 0.39 o 8 13 0 23.50 23.80 0.53 o 9 13 0 249.25 246.71 1.74 o 0 14 0 827.52 862.90 11.04 o 1 14 0 9.65 15.84 1.04 o 2 14 0 194.98 208.70 3.64 o 3 14 0 625.73 607.71 7.18 o 4 14 0 1494.30 1499.79 14.86 o 5 14 0 245.64 249.36 4.76 o 6 14 0 284.15 264.14 1.88 o 7 14 0 67.18 63.79 0.78 o 8 14 0 9.74 11.92 0.39 o 9 14 0 16.19 19.53 0.43 o 1 15 0 247.25 239.99 3.97 o 2 15 0 15.14 17.27 1.32 o 3 15 0 544.82 519.87 11.92 o 4 15 0 156.87 138.66 3.44 o 5 15 0 93.30 80.91 1.30 o 6 15 0 155.78 147.40 1.14 o 7 15 0 71.83 77.59 0.82 o 8 15 0 195.18 194.49 1.35 o 9 15 0 48.91 43.73 0.64 o 0 16 0 322.96 325.06 7.61 o 1 16 0 133.89 139.88 3.42 o 2 16 0 296.66 289.09 4.93 o 3 16 0 361.55 385.31 7.33 o 4 16 0 160.66 159.16 3.55 o 5 16 0 437.00 393.60 2.24 o 6 16 0 68.59 67.78 0.77 o 7 16 0 35.64 38.67 0.60 o 8 16 0 4.37 5.28 0.27 o 1 17 0 85.99 80.98 2.98 o 2 17 0 166.75 177.08 4.58 o 3 17 0 91.54 96.24 3.17 o 4 17 0 144.49 136.09 1.23 o 5 17 0 350.50 359.57 2.16 o 6 17 0 191.52 193.43 1.35 o 7 17 0 6.56 5.14 0.29 o 8 17 0 37.08 38.46 0.50 o 0 18 0 563.68 524.36 24.07 o 1 18 0 2.12 2.59 1.12 o 2 18 0 9.63 12.83 1.22 o 3 18 0 194.50 204.93 1.72 o 4 18 0 45.01 54.96 0.78 o 5 18 0 156.05 151.40 1.22 o 6 18 0 3.88 3.61 0.28 o 7 18 0 44.09 50.84 0.64 o 8 18 0 2.63 2.57 0.22 o 1 19 0 145.92 148.76 1.75 o 2 19 0 379.00 376.47 2.88 o 3 19 0 43.85 41.88 0.80 o 4 19 0 3.00 3.43 0.34 o 5 19 0 2.05 1.04 0.26 o 6 19 0 4.37 7.22 0.32 o 7 19 0 36.40 43.00 0.56 o 0 20 0 245.88 263.33 4.01 o 1 20 0 201.39 190.27 2.02 o 2 20 0 149.58 138.62 1.63 o 3 20 0 81.36 83.85 1.08 o 4 20 0 20.73 23.19 0.58 o 5 20 0 57.02 55.03 0.68 o 6 20 0 38.94 41.26 0.57 o 7 20 0 22.78 26.03 0.44 o 1 21 0 132.01 130.44 1.62 o 2 21 0 21.73 22.74 0.78 o 3 21 0 5.11 6.86 0.43 o 4 21 0 211.41 198.09 1.47 o 5 21 0 119.26 123.11 1.02 o 6 21 0 13.94 14.35 0.33 o 0 22 0 22.74 30.83 1.08 o 1 22 0 13.46 12.58 0.61 o 2 22 0 39.11 35.24 1.28 o 3 22 0 8.12 7.38 0.41 o 4 22 0 106.07 116.40 1.10 o 5 22 0 9.27 11.38 0.35 o 6 22 0 1.27 0.74 0.23 o 1 23 0 186.20 188.55 1.86 o 2 23 0 59.57 58.65 1.09 o 3 23 0 10.94 8.55 0.45 o 4 23 0 10.81 11.79 0.42 o 5 23 0 57.50 64.78 1.17 o 0 24 0 20.70 21.77 1.28 o 1 24 0 33.63 33.47 0.91 o 2 24 0 31.61 30.56 0.89 o 3 24 0 93.08 81.38 1.21 o 4 24 0 4.07 3.77 0.29 o 1 25 0 23.06 29.14 0.93 o 2 25 0 115.50 126.19 1.56 o 3 25 0 16.33 15.90 0.64 o -4 -24 1 1.93 1.70 0.73 o -5 -23 1 42.69 46.74 2.07 o -6 -22 1 21.35 32.10 2.43 o -5 -22 1 29.11 35.50 2.19 o 5 -22 1 11.35 8.27 1.70 o 6 -22 1 7.62 9.24 1.22 o -6 -21 1 63.71 64.34 2.33 o 5 -21 1 57.39 63.47 4.13 o 6 -21 1 12.85 16.29 1.95 o -7 -20 1 74.33 74.97 3.02 o -6 -20 1 9.37 11.17 1.34 o 6 -20 1 12.25 13.86 2.19 o 7 -20 1 2.16 3.40 0.73 o -7 -19 1 48.65 59.26 2.16 o -6 -19 1 19.09 16.96 1.52 o 6 -19 1 128.47 129.38 3.62 o 7 -19 1 1.89 0.58 1.30 o -8 -18 1 9.89 8.56 0.77 o -7 -18 1 39.53 36.47 2.02 o -6 -18 1 57.90 68.33 3.65 o -2 -18 1 19.11 17.14 2.91 o -1 -18 1 8.20 11.51 2.43 o 0 -18 1 41.27 48.42 2.67 o 1 -18 1 99.82 97.44 4.68 o 2 -18 1 221.40 216.80 6.05 o 6 -18 1 4.87 5.41 1.21 o 7 -18 1 10.48 12.93 0.99 o 8 -18 1 32.43 40.32 2.92 o -8 -17 1 12.20 15.09 0.92 o -7 -17 1 14.87 16.87 1.62 o -6 -17 1 341.28 350.40 9.73 o -3 -17 1 49.61 43.68 2.55 o -2 -17 1 10.16 10.86 1.74 o -1 -17 1 739.71 712.80 12.70 o 0 -17 1 4.11 5.48 1.20 o 1 -17 1 770.79 680.60 10.97 o 2 -17 1 367.00 333.21 9.60 o 3 -17 1 82.28 66.29 3.92 o 6 -17 1 4.59 6.32 1.25 o 7 -17 1 43.33 48.06 2.44 o 8 -17 1 89.31 86.23 1.56 o -8 -16 1 95.64 102.52 2.04 o -7 -16 1 63.30 56.98 2.69 o -6 -16 1 100.80 108.94 5.11 o -4 -16 1 334.17 334.65 7.63 o -3 -16 1 11.68 11.32 1.68 o -2 -16 1 610.95 587.23 10.29 o -1 -16 1 64.89 55.58 2.76 o 0 -16 1 24.44 22.59 1.84 o 1 -16 1 173.50 178.14 5.56 o 2 -16 1 284.72 244.97 6.96 o 3 -16 1 747.14 708.85 12.10 o 4 -16 1 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