#------------------------------------------------------------------------------
#$Date: 2019-08-06 07:13:51 +0300 (Tue, 06 Aug 2019) $
#$Revision: 217427 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/17/2021739.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2021739
loop_
_publ_author_name
'Breton, Gary W.'
'Hahn, Lauren A.'
'Martin, Kenneth L.'
_publ_section_title
;
Structural verification of a tetrahydrotetrazole compound
;
_journal_coeditor_code UK3181
_journal_issue 9
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first
;
;
_journal_paper_doi 10.1107/S2053229619010210
_journal_volume 75
_journal_year 2019
_chemical_formula_iupac 'C25 H30 N4 O4'
_chemical_formula_moiety 'C25 H30 N4 O4'
_chemical_formula_sum 'C25 H30 N4 O4'
_chemical_formula_weight 450.53
_chemical_melting_point 369
_chemical_name_common 'Tetrahydrotetrazole 5'
_chemical_name_systematic
;1,2-Di-tert-butyl
3-phenyl-1H,2H,3H,10bH-[1,2,3,4]tetrazolo[5,1-a]isoquinoline-1,2-dicarboxylate
;
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_Hall '-P 2ybc'
_space_group_name_H-M_alt 'P 1 21/c 1'
_symmetry_space_group_name_Hall '-P 2ybc'
_symmetry_space_group_name_H-M 'P 1 21/c 1'
_atom_sites_solution_hydrogens difmap
_atom_sites_solution_primary dual
_audit_creation_method
;
Olex2 1.2-beta
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_cell_angle_alpha 90
_cell_angle_beta 95.54(3)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 9.2613(19)
_cell_length_b 10.882(2)
_cell_length_c 23.583(5)
_cell_measurement_reflns_used 79687
_cell_measurement_temperature 90.0(3)
_cell_measurement_theta_max 49.2360
_cell_measurement_theta_min 1.7310
_cell_volume 2365.6(8)
_computing_cell_refinement
;
CrysAlis PRO (Rigaku OD, 2018)
;
_computing_data_collection
;
CrysAlis PRO (Rigaku OD, 2018)
;
_computing_data_reduction
;
CrysAlis PRO (Rigaku OD, 2018)
;
_computing_molecular_graphics
;
OLEX2 (Dolomanov et al., 2009)
;
_computing_publication_material
;
OLEX2 (Dolomanov et al., 2009)
;
_computing_structure_refinement
;
SHELXL2017 (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 90.0(3)
_diffrn_detector 'CCD plate'
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device 'four-circle diffractometer'
_diffrn_measurement_device_type 'XtaLAB Synergy Dualflex HyPix'
_diffrn_measurement_method '\w scans'
_diffrn_radiation_monochromator mirror
_diffrn_radiation_probe x-ray
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0355
_diffrn_reflns_av_unetI/netI 0.0227
_diffrn_reflns_limit_h_max 19
_diffrn_reflns_limit_h_min -19
_diffrn_reflns_limit_k_max 23
_diffrn_reflns_limit_k_min -21
_diffrn_reflns_limit_l_max 50
_diffrn_reflns_limit_l_min -45
_diffrn_reflns_number 183544
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 49.836
_diffrn_reflns_theta_min 1.735
_diffrn_source 'micro-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu 0.087
_exptl_absorpt_correction_T_max 1.000
_exptl_absorpt_correction_T_min 0.372
_exptl_absorpt_correction_type gaussian
_exptl_absorpt_process_details
;
(CrysAlis PRO; Rigaku OD, 2018)
;
_exptl_crystal_colour colourless
_exptl_crystal_density_diffrn 1.265
_exptl_crystal_density_method 'not measured'
_exptl_crystal_description block
_exptl_crystal_F_000 960
_exptl_crystal_size_max 0.544
_exptl_crystal_size_mid 0.329
_exptl_crystal_size_min 0.277
_refine_diff_density_max 0.705
_refine_diff_density_min -0.254
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.035
_refine_ls_hydrogen_treatment refall
_refine_ls_matrix_type full
_refine_ls_number_parameters 418
_refine_ls_number_reflns 24326
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.035
_refine_ls_R_factor_all 0.0570
_refine_ls_R_factor_gt 0.0419
_refine_ls_shift/su_max 0.003
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0602P)^2^+0.2083P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1098
_refine_ls_wR_factor_ref 0.1159
_reflns_number_gt 19422
_reflns_number_total 24326
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file uk3181sup1.cif
_cod_data_source_block I
_cod_original_cell_volume 2365.7(8)
_cod_database_code 2021739
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
0 0 -2 3156.60 89.1639 26
0 0 -2 3227.34 88.9746 13
0 0 -2 3188.47 89.1837 21
0 0 -3 1.44321 1.51045 7
0 0 -3 2.47030 1.36496 13
0 0 -3 1.40965 1.85272 26
0 0 3 0.89424 1.23282 35
0 0 -3 0.94157 1.17584 29
0 0 -3 0.43939 1.73669 9
0 0 -3 4.80390 1.42733 5
0 0 -3 1.57533 1.76837 21
0 0 -4 5055.62 136.891 5
0 0 -4 5369.71 137.502 26
0 0 -4 4895.54 137.965 1
0 0 -4 4763.20 137.242 9
0 0 -4 4823.91 136.876 13
0 0 4 4797.56 136.459 35
0 0 -4 4608.46 136.919 7
0 0 -4 5019.77 136.596 2
0 0 -4 4889.23 136.730 29
0 0 -4 4964.33 137.308 21
0 0 5 2.76693 2.43590 1
0 0 5 1.37101 1.79686 39
0 0 -5 2.13356 2.38094 13
0 0 -5 1.15692 3.16545 26
0 0 -5 2.69039 2.01185 29
0 0 -5 14.0204 2.51707 5
0 0 5 4.94126 2.27383 29
0 0 5 2.84455 2.13009 35
0 0 -5 2.48650 2.56013 9
0 0 -5 0.36308 2.92771 21
0 0 -5 2.68405 1.91109 2
0 0 5 3.94789 2.27091 17
0 0 6 1958.54 55.6103 17
0 0 -6 1899.75 55.3589 28
0 0 -6 2052.04 55.0525 2
0 0 6 1891.27 55.7827 16
0 0 -6 1828.44 55.6267 7
0 0 6 1914.46 55.4929 29
0 0 6 1980.16 54.6847 39
0 0 6 1944.14 55.0245 35
0 0 -6 1898.67 55.2449 12
0 0 -6 1937.98 55.2685 29
0 0 -6 1926.30 55.9862 9
0 0 6 1905.89 56.8030 1
0 0 -6 1965.71 55.5362 5
0 0 -6 1925.69 56.0586 21
0 0 7-0.78847 2.02734 39
0 0 7 1.62554 2.64173 17
0 0 -7 0.72706 2.34251 28
0 0 7 2.20369 2.60918 29
0 0 -7 2.89479 2.15121 2
0 0 -7 2.09873 2.45492 29
0 0 7 2.60290 2.73210 16
0 0 7 9.52048 2.76545 22
0 0 -7 4.11432 3.25497 9
0 0 -7 2.71058 2.60740 12
0 0 -7 8.80823 2.73060 5
0 0 7 3.07859 3.09971 1
0 0 7-0.28791 3.22598 9
0 0 -8 251.036 9.67404 5
0 0 8 249.678 10.1534 10
0 0 8 260.006 10.0641 16
0 0 -8 264.433 8.94549 2
0 0 8 258.563 10.9509 1
0 0 8 229.941 9.44494 29
0 0 8 255.404 9.68233 17
0 0 8 240.061 8.53890 39
0 0 8 274.060 9.89796 22
0 0 9 10.0711 3.33430 17
0 0 9 1.96966 2.26435 38
0 0 9 4.53006 3.86400 9
0 0 9-3.38898 3.18984 16
0 0 -9 3.76786 2.30599 2
0 0 9 3.80868 3.29511 10
0 0 9 1.44938 2.27191 39
0 0 9 0.26285 2.86193 29
0 0 10 2380.35 68.8032 29
0 0 10 2324.90 66.8458 38
0 0 10 2403.13 69.6384 31
0 0 10 2378.63 67.3345 39
0 0 10 2369.17 69.3411 16
0 0 10 2426.41 69.0630 17
0 0 10 2368.61 68.9884 22
0 0 10 2428.05 69.5106 10
0 0 10 2288.38 70.2080 9
0 0 11-0.34131 3.66663 17
0 0 11 9.10257 4.00504 22
0 0 11-0.94024 3.76819 9
0 0 11 3.81910 2.80350 38
0 0 11 1.30328 3.49124 29
0 0 11 2.32131 3.98105 10
0 0 11-0.37761 3.60258 16
0 0 11 3.69857 2.78093 39
0 0 12 5.65513 4.15478 17
0 0 12 5.73689 2.97457 39
0 0 12-0.71434 3.94603 29
0 0 12 6.71784 4.64932 9
0 0 12-1.26218 4.25730 10
0 0 12 5.55872 2.99078 38
0 0 12-0.41082 3.92112 16
0 0 13 2.28840 4.54987 10
0 0 13 10.5057 4.30926 29
0 0 13 4.54946 4.52428 17
0 0 13 4.88586 4.55948 16
0 0 13 7.74558 4.44223 22
0 0 13 14.0955 5.07278 9
0 0 13 2.46274 3.30503 38
0 0 13 3.09172 3.16259 39
0 0 14 350.762 12.2676 39
0 0 14 337.492 14.6908 22
0 0 14 366.322 14.4388 29
0 0 14 349.326 14.5515 17
0 0 14 369.265 16.2745 9
0 0 14 357.693 14.7110 16
0 0 14 340.274 15.2293 36
0 0 14 329.054 11.8008 38
0 0 14 339.412 13.8323 20
0 0 15 6.33251 5.15123 17
0 0 15-1.59408 6.89988 6
0 0 15 0.19232 3.77331 38
0 0 -15 5.61625 2.13756 25
0 0 15 4.53156 4.39129 20
0 0 15-2.25512 4.78233 29
0 0 15 5.98192 5.66917 31
0 0 15-6.17036 7.04232 36
0 0 15 1.52260 5.10375 16
0 0 16 2552.03 75.9734 20
0 0 16 2523.51 78.1196 31
0 0 16 2638.05 77.8223 19
0 0 16 2530.56 73.4212 38
0 0 -16 2550.94 72.3373 25
0 0 16 2485.02 80.2241 6
0 0 16 2574.14 79.0012 26
0 0 16 2696.66 76.6910 30
0 0 16 2590.75 78.0027 36
0 0 16 2601.74 77.0268 17
0 0 16 2589.66 77.1486 32
0 0 16 2594.79 76.5336 29
0 0 17-3.04365 6.54605 30
0 0 17-3.70205 7.65393 6
0 0 17 6.36219 7.07609 19
0 0 17 1.76041 7.36665 32
0 0 17-1.83093 5.15187 20
0 0 17-0.59485 6.05120 10
0 0 17 6.66750 6.57748 22
0 0 17 1.69319 5.70834 17
0 0 17-1.53635 5.47243 29
0 0 17 3.10114 7.09948 26
0 0 17 2.10408 7.39633 31
0 0 17 1.96294 7.58566 36
0 0 -17 3.28356 2.24043 25
0 0 17 1.10478 4.57554 38
0 0 18 2355.18 72.7180 31
0 0 18 2484.50 70.5433 29
0 0 18 2351.30 66.9793 38
0 0 18 2311.98 71.1623 10
0 0 18 2396.74 75.2727 6
0 0 18 2451.53 71.8717 22
0 0 18 2354.16 73.2380 9
0 0 -18 2238.82 65.1840 25
0 0 18 2363.83 70.4978 23
0 0 18 2353.60 71.8309 19
0 0 18 2293.72 70.3348 30
0 0 18 2346.95 72.1245 36
0 0 19 1.25965 7.20523 16
0 0 19 13.0313 5.45738 38
0 0 19 11.7210 8.52288 3
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0 0 19 9.50607 9.14395 6
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0 0 19 9.71333 8.49122 31
0 0 19 0.72213 8.82364 19
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0 0 19-3.31028 6.96423 10
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0 0 20 4558.39 137.949 31
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0 0 21 28.1412 6.60347 38
0 0 21-3.64299 9.13058 10
0 0 21-1.86141 7.93625 29
0 0 21 9.68936 9.37368 30
0 0 21 3.51708 8.89403 3
0 0 21-2.38593 10.8863 6
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0 0 22 797.819 32.8633 31
0 0 22 784.468 25.8135 38
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0 0 22 763.560 31.3833 19
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0 0 22 780.546 30.6263 10
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0 0 22 798.053 29.3912 29
0 0 22 796.705 35.2684 6
0 0 22 838.280 32.8328 36
0 0 22 737.945 32.0813 9
0 0 23 12.5440 11.5146 31
0 0 23 4.89076 8.96845 23
0 0 23 7.38112 8.78237 16
0 0 23-3.17321 9.21824 10
0 0 23 5.32696 12.4099 6
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0 0 23-0.65931 8.26233 29
0 0 23-3.13125 10.5878 9
0 0 23 0.96177 11.7512 36
0 0 23 8.25007 6.94765 38
0 0 23 7.20080 11.6984 19
0 0 23 6.81433 11.1357 3
0 0 23 10.3314 7.59064 20
0 0 24 2299.56 75.8727 36
0 0 24 2398.12 73.0395 16
0 0 24 2232.42 73.4502 10
0 0 24 2330.08 72.6765 23
0 0 24 2402.89 75.9163 3
0 0 24 2286.29 76.2610 9
0 0 24 2312.45 76.6921 31
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0 0 -24 2257.45 72.9583 41
0 0 24 2259.10 74.9228 19
0 0 24 2313.04 68.2061 38
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0 0 24 2401.52 72.1546 29
0 0 25 12.4709 11.0261 9
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0 0 25-2.33469 8.67845 16
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0 0 25 10.5275 11.7283 31
0 0 25 23.5111 13.7405 6
0 0 25 6.05095 9.95208 23
0 0 25 3.96404 7.60236 38
0 0 -25 8.94941 9.32919 41
0 0 25 0.60198 7.79828 20
0 0 26 2132.36 69.7913 10
0 0 26 2145.43 68.8503 16
0 0 26 2136.40 76.3709 6
0 0 26 2141.26 78.0116 8
0 0 26 2178.35 73.7008 31
0 0 26 2385.46 73.3110 3
0 0 26 2125.15 72.0517 19
0 0 -26 2077.44 68.9331 41
0 0 26 2084.35 69.1521 30
0 0 26 2173.57 73.1176 9
0 0 26 2191.63 64.0620 38
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0 0 26 2137.04 66.7620 20
0 0 26 2237.18 69.1985 23
0 0 27 8.03302 13.2311 6
0 0 27 24.3940 12.8650 9
0 0 27 14.6656 10.1929 23
0 0 27 5.51198 11.1821 10
0 0 -27 17.3941 10.4367 41
0 0 27 8.31950 13.1892 36
0 0 27 1.77011 15.2640 8
0 0 27 14.0448 12.6387 3
0 0 27 0.81912 9.78943 16
0 0 27 2.48450 8.38309 20
0 0 27 12.9590 12.3641 31
0 0 27 12.9140 11.8609 30
0 0 28 337.385 20.1518 23
0 0 28 369.864 24.2911 36
0 0 28 400.388 24.2363 3
0 0 28 378.880 21.2945 10
0 0 28 360.830 20.8972 30
0 0 28 398.889 26.6426 6
0 0 28 392.857 29.1219 8
0 0 28 388.885 18.0233 20
0 0 28 356.696 24.0532 31
0 0 29 6.92186 12.2324 23
0 0 29 10.0938 8.70525 20
0 0 29-0.97107 11.1847 10
0 0 29 15.0055 11.5510 30
0 0 29 27.0410 16.5877 8
0 0 -29 16.2406 13.4485 11
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0 0 29-6.51489 14.3531 36
0 0 29 10.4520 14.2185 6
0 0 29-2.85004 13.6831 31
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0 0 -30 2059.83 73.3297 11
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0 0 30 2123.39 68.9757 10
0 0 30 2107.84 64.7820 20
0 0 30 2078.44 67.6287 23
0 0 30 2095.74 68.6109 30
0 0 30 2047.82 72.8265 36
0 0 31 12.5261 19.5901 8
0 0 31 36.6092 14.4660 30
0 0 31-7.75920 16.8018 31
0 0 31 18.4923 13.9326 10
0 0 31 15.1697 10.0097 20
0 0 31 21.2863 16.3839 36
0 0 -31 23.2011 15.5002 11
0 0 31 13.6708 13.5982 23
0 0 31 2.69862 16.5559 3
0 0 31 5.61121 17.6114 6
0 0 -32 97.2502 18.9660 11
0 0 32 101.936 16.5022 30
0 0 32 121.084 24.7280 8
0 0 32 116.245 17.0840 10
0 0 32 134.855 16.4521 23
0 0 32 121.611 22.7681 6
0 0 32 126.017 20.8365 3
0 0 32 124.222 20.1014 31
0 0 32 122.538 20.0597 36
0 0 32 126.375 12.7223 20
0 0 33-3.25805 14.8877 30
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0 0 33-9.69740 13.7793 10
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0 0 -34 12.6400 15.9338 11
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0 0 37 9.47432 18.7701 31
0 0 -37 11.7533 17.6114 11
0 0 38 39.0264 19.6006 3
0 0 38 21.3341 20.3000 31
0 0 38 19.5423 15.3554 23
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0 0 -38 32.3610 18.7271 11
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0 0 -41-1.70658 18.4717 11
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0 0 41 17.3329 18.0447 30
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0 0 -42 15.1974 19.4962 11
0 0 43-13.5595 19.7580 30
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0 0 44 202.842 25.0376 30
0 0 44 325.642 30.5791 31
0 0 45 2.01775 21.9521 31
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0 0 47-22.5820 21.5624 30
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0 0 48 50.7235 23.3483 31
0 0 49 18.1158 21.2860 31
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0 0 50-32.1570 22.0219 30
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0 -1 0 128.237 2.39138 42
0 1 0 0.43726 1.63569 18
0 1 -1 70947.4 1972.39 18
0 1 1 72118.0 1972.42 41
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-10 -14 -4 18.9473 18.9041 40
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-10 -16 27 9.71608 23.1285 33
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10 -16 -13 256.937 29.4409 18
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-10 -16 -2 3.22194 21.4141 40
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-10 -16 -3 62.7445 21.5338 40
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-10 -16 -4 559.204 35.5854 40
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10 -16 5 106.243 19.6051 35
10 16 5 97.6549 24.1658 34
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10 16 6 89.8531 25.2359 17
-10 -16 -6 137.783 24.5485 40
10 -16 6 147.890 19.6496 35
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10 16 7 23.0431 23.8570 17
-10 -16 -7 19.2522 21.1112 40
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-10 -16 -8-6.42225 21.0127 40
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10 16 9 65.7787 26.1956 17
-10 -16 -9 76.9501 23.3510 40
10 -16 9 115.510 19.8191 35
10 16 9 97.1678 23.7369 34
10 -16 10 651.075 35.7495 18
10 16 10 552.316 40.8130 17
-10 -16 -10 553.778 35.8960 40
10 -16 10 595.549 30.7168 35
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10 16 11 72.8796 27.2570 17
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-10 -16 -13 115.141 23.8616 40
10 -16 13 133.420 19.7724 35
10 16 13 168.116 26.0873 34
-10 -16 -14 6.36911 21.3819 40
10 -16 14 27.9758 16.6251 35
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10 -16 15-14.8561 16.1849 35
10 16 15 9.50727 21.4513 34
10 -16 16 85.8400 18.4164 35
10 16 16 66.7130 24.0272 34
10 16 17 26.6527 22.5655 34
10 16 18-3.79770 23.6117 34
10 16 19 260.020 31.5314 34
10 16 20-24.4442 23.8361 34
10 16 21 35.4733 24.6224 34
10 16 22 18.3920 23.9074 34
10 16 23 16.2611 22.4279 34
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-10 -17 18 8.48861 22.3350 40
-10 17 18 4.63250 25.6381 39
-10 -17 18 14.4298 25.0772 33
-10 -17 17 122.095 24.8541 40
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-10 -17 13-1.67749 21.6477 40
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-10 -17 8 24.4524 22.2936 40
-10 -17 8 39.5763 22.7307 33
-10 -17 7 198.243 25.8492 40
-10 -17 7 170.209 25.9901 33
-10 -17 6 27.4965 20.9530 40
-10 -17 6 11.7797 21.2120 33
10 -17 -5 306.633 30.3311 18
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10 -17 -4 236.020 28.4248 18
-10 -17 4 194.753 25.3873 40
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10 -17 -3 15.7774 21.0772 18
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-10 -17 3-6.48747 20.8197 33
10 -17 -2 135.254 24.8191 18
-10 -17 2 121.751 23.4676 40
-10 -17 2 95.9184 23.4520 33
10 -17 -1 17.5003 20.7804 18
-10 -17 1 28.7718 20.8122 40
10 17 -1 16.0630 21.1464 34
-10 -17 1-12.5982 19.9943 33
10 -17 0 86.4732 22.9477 18
-10 -17 0 41.4864 20.7589 40
10 17 0 84.1236 23.5083 34
-10 -17 0 81.9760 21.7915 33
10 -17 1-7.59325 21.4652 18
-10 -17 -1-23.8114 22.3055 40
10 17 1 1.79555 20.9995 34
-10 -17 -1 22.8002 20.9687 33
10 -17 2-16.8342 23.0339 18
-10 -17 -2 6.33810 20.9517 40
10 17 2 1.79698 21.3336 34
-10 -17 -2 1.49208 19.7294 33
-10 -17 -3 379.657 30.4802 40
10 17 3 392.772 32.1520 34
-10 -17 -3 364.132 29.2071 33
-10 -17 -4 82.1757 22.6531 40
10 17 4 48.9383 23.1859 34
-10 -17 -4 35.8076 20.7483 33
-10 -17 -5 137.097 23.8477 40
10 17 5 153.155 25.0751 34
-10 -17 -5 168.039 23.3447 33
-10 -17 -6 17.2708 20.8024 40
10 17 6 62.3378 22.2723 34
-10 -17 -6-8.18961 18.2995 33
-10 -17 -7 104.867 22.9762 40
10 17 7 119.850 24.8855 34
-10 -17 -7 130.266 22.5095 33
-10 -17 -8 156.080 25.2152 40
10 17 8 196.740 26.2840 34
-10 -17 -8 170.433 22.2909 33
-10 -17 -9 234.539 26.8389 40
10 17 9 218.539 28.2526 34
-10 -17 -9 223.208 23.7763 33
-10 -17 -10 96.0842 23.4251 40
10 17 10 122.080 26.4927 34
-10 -17 -10 145.385 20.3282 33
-10 -17 -11 208.633 26.1043 40
10 17 11 258.608 28.7576 34
-10 -17 -11 203.775 21.8372 33
-10 -17 -12 12.2805 20.7753 40
10 17 12-9.45274 23.4177 34
-10 -17 -13 24.4898 20.5642 40
10 17 13 39.7547 23.6006 34
-10 -17 -14 40.9327 21.2643 40
10 17 14 79.5195 24.9568 34
-10 -17 -15 144.526 23.5580 40
10 17 15 170.721 27.1178 34
-10 -17 -16 14.9001 20.0346 40
10 17 16-7.54673 21.9212 34
-10 -17 -17 33.8169 20.5012 40
10 17 17 47.0293 23.2820 34
-10 -17 -18 200.252 25.2117 40
10 17 18 201.489 28.8059 34
-10 -17 -19 11.3839 20.0803 40
10 17 19 72.0463 23.8170 34
10 17 20 89.2191 25.5106 34
-10 -18 22 15.2544 23.6757 33
-10 18 21 8.48245 26.0117 39
-10 -18 21-10.3109 23.3332 33
-10 18 20 133.551 28.5011 39
-10 -18 20 191.572 27.7620 33
-10 18 19 2.18866 24.1674 39
-10 -18 19 17.6248 23.2270 33
-10 18 18-8.85890 25.1592 39
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-10 -18 8-1.56959 20.6527 40
-10 -18 8 38.2212 23.4403 33
-10 -18 7-12.5145 20.9644 40
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-10 -18 5 49.7103 22.3478 40
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-10 -18 4 46.4752 22.9837 33
-10 -18 3 530.490 33.4206 40
-10 -18 3 526.894 34.9737 33
-10 -18 2 52.4375 22.5241 40
10 18 -2 30.5924 23.1584 34
-10 -18 2 20.9746 22.8272 33
-10 -18 1 15.3870 21.1988 40
10 18 -1 34.2387 22.2400 34
-10 -18 1 4.76028 21.3055 33
-10 -18 0 16.8959 20.9894 40
10 18 0 1.80808 21.6906 34
-10 -18 0-17.1364 21.8568 33
-10 -18 -1 13.7273 20.3074 40
10 18 1-47.0334 24.1646 34
-10 -18 -1-1.52874 21.2882 33
-10 -18 -2 10.6551 20.9288 40
10 18 2 72.4243 22.0165 34
-10 -18 -2 40.4461 21.4856 33
-10 -18 -3 106.287 23.7808 40
10 18 3 109.289 24.7790 34
-10 -18 -3 130.364 23.1225 33
-10 -18 -4 213.314 25.5419 40
10 18 4 250.602 29.5449 34
-10 -18 -4 207.462 24.0858 33
-10 -18 -5 42.2347 21.3880 40
10 18 5 62.4620 23.1810 34
-10 -18 -5 30.6723 20.6046 33
-10 -18 -6 46.4797 21.7096 40
10 18 6 1.84330 22.3112 34
-10 -18 -6 43.3721 21.7912 33
-10 -18 -7 132.821 23.9268 40
10 18 7 146.290 26.6507 34
-10 -18 -7 140.702 21.6656 33
-10 -18 -8 185.593 25.7136 40
10 18 8 159.888 28.3228 34
-10 -18 -8 232.713 24.8759 33
-10 -18 -9 88.3520 22.7540 40
10 18 9 37.3028 24.2632 34
-10 -18 -9 66.0023 20.8994 33
-10 -18 -10 179.928 25.5890 40
10 18 10 220.645 28.4553 34
-10 -18 -11 40.5434 21.6078 40
10 18 11 59.8321 24.8856 34
-10 -18 -12 63.2233 23.4909 40
10 18 12 108.250 24.9550 34
-10 -18 -13 32.6544 20.3460 40
10 18 13 65.0106 24.6346 34
-10 -18 -14 35.1168 20.9079 40
10 18 14 20.3540 24.6456 34
-10 -18 -15-5.55403 19.7308 40
10 18 15-57.1619 25.5683 34
-10 -18 -16-1.36757 20.1210 40
10 18 16 7.33735 22.2318 34
-10 19 17 29.2536 26.0949 39
-10 -19 15 13.2441 21.6563 40
-10 -19 15 22.6310 24.0197 33
-10 -19 14 181.720 24.8135 40
-10 -19 14 210.948 27.3894 33
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-10 -19 13 24.4404 23.5556 33
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-10 -19 8 76.8643 24.9388 33
-10 -19 7 5.88342 20.9470 40
-10 -19 7 11.8562 22.4731 33
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-10 -19 6-20.1219 24.5049 33
-10 -19 5 29.2002 21.3047 40
-10 -19 5 56.3515 22.8572 33
-10 -19 4 183.212 25.3204 40
10 19 -4 134.751 26.3250 34
-10 -19 4 165.226 25.6239 33
-10 -19 3 40.6411 20.6799 40
10 19 -3 23.0839 22.3008 34
-10 -19 3 3.22925 23.0023 33
-10 -19 2 10.1061 21.4449 40
10 19 -2-14.2616 22.6733 34
-10 -19 2-9.53222 21.5016 33
-10 -19 1 53.3538 20.5982 40
10 19 -1 33.8924 22.0839 34
-10 -19 1 38.9564 21.1219 33
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10 19 0 3.56727 21.9698 34
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-10 -19 -1 27.1402 20.7946 40
10 19 1 14.3361 22.7170 34
-10 -19 -1 29.9283 23.1754 33
-10 -19 -2 24.2006 19.8593 40
10 19 2 43.0761 23.2908 34
-10 -19 -2-5.85101 22.7076 33
-10 -19 -3 120.377 22.6062 40
10 19 3 64.7876 23.9482 34
-10 -19 -3 64.2024 22.1254 33
-10 -19 -4 15.5272 21.3162 40
10 19 4 30.7157 23.1598 34
-10 -19 -4 34.6920 20.8738 33
-10 -19 -5 142.603 24.3990 40
10 19 5 128.444 26.2655 34
-10 -19 -5 88.8330 22.7610 33
-10 -19 -6 66.7296 22.3944 40
10 19 6 59.8960 23.3778 34
-10 -19 -6 85.0043 22.1589 33
-10 -19 -7 6.90958 21.4995 40
10 19 7-18.1748 22.3814 34
-10 -19 -7 1.26002 21.2664 33
-10 -19 -8 132.564 23.5059 40
10 19 8 112.779 25.0504 34
-10 -19 -9 6.78021 20.5040 40
10 19 9 49.1602 23.1675 34
-10 -19 -10 144.953 22.9766 40
10 19 10 154.089 26.4384 34
-10 -19 -11 176.020 24.6653 40
10 19 11 213.195 28.0920 34
10 20 -7 74.1177 25.1103 34
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10 20 -6 224.518 27.5736 34
-10 -20 6 193.523 27.0465 33
10 20 -5 79.6539 24.7573 34
-10 -20 5 105.967 25.0969 33
10 20 -4-8.52656 21.9291 34
-10 -20 4 32.7961 21.9466 33
10 20 -3 29.0528 22.3636 34
-10 -20 3 66.0996 23.8613 33
10 20 -2 169.106 27.1240 34
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10 20 -1 49.6849 23.8953 34
-10 -20 1 50.5071 22.0491 33
10 20 0 36.1051 24.3238 34
10 20 1 285.061 29.0665 34
10 20 2 67.7028 25.1148 34
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0 0 0 0.00 0.00 0
TITL laurenh1-FI-1 in P2(1)/c
REM P2(1)/c (#14 in standard setting)
CELL 0.71073 9.261350 10.882175 23.582874 90.0000 95.5376 90.0000
ZERR 1.00 0.000088 0.000097 0.000181 0.0000 0.0008 0.0000
LATT 1
SYMM -x, y+1/2,-z+1/2
SFAC C H N O
UNIT 100.00 120.00 16.00 16.00
TREF
HKLF 4
END
;
_shelx_hkl_checksum 50145
_shelx_res_file
;
TITL LH1_90K in P2(1)/c
lh1_90k.res
created by SHELXL-2017/1 at 12:05:02 on 15-Mar-2019
CELL 0.71073 9.2613 10.8822 23.5829 90 95.538 90
ZERR 4 0.0019 0.0022 0.0047 0 0.03 0
LATT 1
SYMM -X,0.5+Y,0.5-Z
SFAC C H N O
UNIT 100 120 16 16
L.S. 4
PLAN 20
LIST 6
BOND
CONF
fmap 2
acta
REM
REM
REM
WGHT 0.060200 0.208300
FVAR 2.33590
O1 4 0.275814 0.739211 0.785413 11.00000 0.01323 0.01518 =
0.01316 0.00513 0.00428 0.00325
O2 4 0.427183 0.600488 0.833111 11.00000 0.01207 0.01753 =
0.01774 0.00487 0.00256 0.00354
O3 4 0.316195 0.674351 0.967327 11.00000 0.01592 0.01261 =
0.00963 -0.00066 0.00040 -0.00433
O4 4 0.202841 0.499593 0.993172 11.00000 0.02262 0.01558 =
0.01255 0.00363 0.00139 -0.00587
N1 3 0.024130 0.526441 0.829667 11.00000 0.01166 0.01191 =
0.01202 -0.00217 -0.00027 0.00010
N2 3 0.059461 0.653381 0.837767 11.00000 0.01000 0.01155 =
0.01165 -0.00086 0.00063 0.00056
N3 3 0.205323 0.651332 0.863635 11.00000 0.01013 0.01134 =
0.00999 0.00175 0.00076 -0.00032
N4 3 0.215839 0.547382 0.899816 11.00000 0.01248 0.01003 =
0.00980 0.00090 -0.00029 -0.00225
C1 1 0.063899 0.487327 0.776112 11.00000 0.01354 0.01697 =
0.01221 -0.00345 -0.00055 0.00117
H1 2 0.038993 0.546723 0.746167 11.00000 0.01919
C2 1 0.120327 0.376537 0.767640 11.00000 0.01536 0.01701 =
0.01575 -0.00531 0.00109 0.00058
H2 2 0.134893 0.351592 0.728526 11.00000 0.02351
C3 1 0.152729 0.292757 0.815200 11.00000 0.01249 0.01263 =
0.01995 -0.00415 0.00180 -0.00107
C4 1 0.200677 0.172638 0.807035 11.00000 0.01706 0.01319 =
0.02859 -0.00574 0.00533 -0.00098
H4 2 0.212748 0.143900 0.766801 11.00000 0.03024
C5 1 0.227374 0.093296 0.852902 11.00000 0.01895 0.01170 =
0.03582 -0.00189 0.00599 -0.00012
H5 2 0.261028 0.009575 0.847011 11.00000 0.03167
C6 1 0.205951 0.133033 0.907717 11.00000 0.01834 0.01174 =
0.03121 0.00242 0.00164 -0.00076
H6 2 0.223837 0.077177 0.940626 11.00000 0.03337
C7 1 0.159945 0.252919 0.916656 11.00000 0.01558 0.01189 =
0.02187 0.00124 0.00032 -0.00184
H7 2 0.149334 0.281389 0.955275 11.00000 0.02031
C8 1 0.134122 0.332976 0.870692 11.00000 0.01170 0.01050 =
0.01775 -0.00148 0.00054 -0.00152
C9 1 0.090168 0.463944 0.881031 11.00000 0.01114 0.01069 =
0.01283 -0.00070 0.00041 -0.00145
H9 2 0.023293 0.467756 0.910859 11.00000 0.01288
C10 1 -0.035698 0.717251 0.872375 11.00000 0.01197 0.01124 =
0.01148 0.00019 0.00191 0.00070
C11 1 -0.175513 0.674799 0.877617 11.00000 0.01255 0.01596 =
0.01807 -0.00334 0.00365 -0.00103
H11 2 -0.205240 0.594109 0.861080 11.00000 0.02506
C12 1 -0.270248 0.746300 0.906300 11.00000 0.01477 0.02046 =
0.02190 -0.00420 0.00680 -0.00054
H12 2 -0.366484 0.716183 0.908058 11.00000 0.02887
C13 1 -0.226304 0.859582 0.928852 11.00000 0.01936 0.01922 =
0.02430 -0.00541 0.00862 0.00141
H13 2 -0.293949 0.909371 0.948815 11.00000 0.02998
C14 1 -0.085832 0.900872 0.923722 11.00000 0.02111 0.01592 =
0.03153 -0.00849 0.00915 -0.00126
H14 2 -0.050400 0.982296 0.938578 11.00000 0.04152
C15 1 0.009908 0.829975 0.895832 11.00000 0.01639 0.01323 =
0.02544 -0.00486 0.00671 -0.00203
H15 2 0.107555 0.859258 0.891555 11.00000 0.02791
C16 1 0.314770 0.656362 0.825252 11.00000 0.01117 0.01158 =
0.01117 0.00151 0.00149 0.00015
C17 1 0.375569 0.771514 0.742422 11.00000 0.01572 0.01339 =
0.01403 0.00371 0.00582 0.00324
C18 1 0.290491 0.869992 0.707874 11.00000 0.02573 0.02020 =
0.01822 0.00857 0.00849 0.01002
H18A 2 0.274634 0.941655 0.733210 11.00000 0.03379
H18B 2 0.347413 0.900153 0.676579 11.00000 0.03523
H18C 2 0.200448 0.834322 0.690509 11.00000 0.02729
C19 1 0.515942 0.823668 0.771468 11.00000 0.01873 0.02050 =
0.02546 0.00382 0.00518 -0.00404
H19A 2 0.577408 0.759873 0.790196 11.00000 0.02778
H19B 2 0.492797 0.886623 0.800681 11.00000 0.03254
H19C 2 0.566692 0.861485 0.743328 11.00000 0.03379
C20 1 0.400792 0.659142 0.706424 11.00000 0.02767 0.01729 =
0.01667 0.00060 0.00709 0.00551
H20A 2 0.461715 0.600407 0.728885 11.00000 0.03150
H20B 2 0.455440 0.684011 0.674935 11.00000 0.02640
H20C 2 0.312521 0.624641 0.688601 11.00000 0.02574
C21 1 0.240796 0.571020 0.958072 11.00000 0.01299 0.01130 =
0.01033 0.00086 0.00034 -0.00198
C22 1 0.353144 0.718570 1.026050 11.00000 0.01253 0.01427 =
0.01080 -0.00206 0.00060 -0.00043
C23 1 0.214850 0.739703 1.054620 11.00000 0.01573 0.02806 =
0.01812 -0.00534 0.00463 0.00095
H23A 2 0.240207 0.785842 1.091037 11.00000 0.03084
H23B 2 0.172632 0.663311 1.064590 11.00000 0.03683
H23C 2 0.145151 0.785652 1.028744 11.00000 0.02800
C24 1 0.427131 0.840329 1.015942 11.00000 0.02259 0.01579 =
0.01981 -0.00359 0.00075 -0.00553
H24A 2 0.455828 0.880344 1.052847 11.00000 0.02966
H24B 2 0.515999 0.825123 0.996073 11.00000 0.03501
H24C 2 0.359965 0.894388 0.992734 11.00000 0.03592
C25 1 0.458444 0.629851 1.058086 11.00000 0.01928 0.02031 =
0.01514 -0.00109 -0.00306 0.00355
H25A 2 0.496493 0.666531 1.094438 11.00000 0.02770
H25B 2 0.411257 0.550994 1.064509 11.00000 0.02792
H25C 2 0.539724 0.616735 1.035837 11.00000 0.03081
HKLF 4
REM LH1_90K in P2(1)/c
REM R1 = 0.0419 for 19422 Fo > 4sig(Fo) and 0.0570 for all 24326 data
REM 418 parameters refined using 0 restraints
END
WGHT 0.0601 0.2081
REM Highest difference peak 0.705, deepest hole -0.254, 1-sigma level 0.062
Q1 1 0.2123 0.1375 0.8301 11.00000 0.05 0.70
Q2 1 0.2231 0.1016 0.8789 11.00000 0.05 0.70
Q3 1 0.0905 0.4344 0.7727 11.00000 0.05 0.68
Q4 1 0.1487 0.2991 0.8926 11.00000 0.05 0.68
Q5 1 -0.1008 0.6963 0.8744 11.00000 0.05 0.67
Q6 1 0.3680 0.6282 0.8275 11.00000 0.05 0.66
Q7 1 0.1490 0.3117 0.8410 11.00000 0.05 0.63
Q8 1 -0.2263 0.7122 0.8912 11.00000 0.05 0.60
Q9 1 -0.2504 0.8051 0.9165 11.00000 0.05 0.60
Q10 1 0.2195 0.5400 0.9746 11.00000 0.05 0.60
Q11 1 0.1323 0.3412 0.7892 11.00000 0.05 0.60
Q12 1 0.1753 0.2319 0.8115 11.00000 0.05 0.60
Q13 1 -0.0355 0.8635 0.9084 11.00000 0.05 0.58
Q14 1 -0.0103 0.7712 0.8855 11.00000 0.05 0.58
Q15 1 0.2266 0.5586 0.9280 11.00000 0.05 0.57
Q16 1 -0.1603 0.8856 0.9255 11.00000 0.05 0.56
Q17 1 0.1812 0.1899 0.9123 11.00000 0.05 0.55
Q18 1 0.3870 0.7195 0.7251 11.00000 0.05 0.50
Q19 1 0.4018 0.6750 1.0403 11.00000 0.05 0.49
Q20 1 0.1091 0.4021 0.8754 11.00000 0.05 0.48
;
_shelx_res_checksum 13049
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
O O1 0.27581(3) 0.73921(3) 0.78541(2) 0.01366(4) Uani d 1
O O2 0.42718(3) 0.60049(3) 0.83311(2) 0.01571(5) Uani d 1
O O3 0.31619(3) 0.67435(3) 0.96733(2) 0.01277(4) Uani d 1
O O4 0.20284(4) 0.49959(3) 0.99317(2) 0.01693(5) Uani d 1
N N1 0.02413(3) 0.52644(3) 0.82967(2) 0.01196(4) Uani d 1
N N2 0.05946(3) 0.65338(3) 0.83777(2) 0.01109(4) Uani d 1
N N3 0.20532(3) 0.65133(3) 0.86364(2) 0.01050(4) Uani d 1
N N4 0.21584(3) 0.54738(3) 0.89982(2) 0.01086(4) Uani d 1
C C1 0.06390(4) 0.48733(4) 0.77611(2) 0.01436(5) Uani d 1
H H1 0.0390(9) 0.5467(8) 0.7462(4) 0.0192(18) Uiso d 1
C C2 0.12033(4) 0.37654(4) 0.76764(2) 0.01607(6) Uani d 1
H H2 0.1349(10) 0.3516(8) 0.7285(4) 0.024(2) Uiso d 1
C C3 0.15273(4) 0.29276(3) 0.81520(2) 0.01501(5) Uani d 1
C C4 0.20068(5) 0.17264(4) 0.80703(2) 0.01941(7) Uani d 1
H H4 0.2127(11) 0.1439(9) 0.7668(4) 0.030(2) Uiso d 1
C C5 0.22737(5) 0.09330(4) 0.85290(2) 0.02194(7) Uani d 1
H H5 0.2610(11) 0.0096(9) 0.8470(4) 0.032(2) Uiso d 1
C C6 0.20595(5) 0.13303(4) 0.90772(2) 0.02048(7) Uani d 1
H H6 0.2238(11) 0.0772(10) 0.9406(4) 0.033(2) Uiso d 1
C C7 0.15994(4) 0.25292(3) 0.91666(2) 0.01655(6) Uani d 1
H H7 0.1493(10) 0.2814(8) 0.9553(4) 0.0203(18) Uiso d 1
C C8 0.13412(4) 0.33298(3) 0.87069(2) 0.01338(5) Uani d 1
C C9 0.09017(4) 0.46394(3) 0.88103(2) 0.01160(4) Uani d 1
H H9 0.0233(8) 0.4678(7) 0.9109(3) 0.0129(15) Uiso d 1
C C10 -0.03570(4) 0.71725(3) 0.87237(2) 0.01151(4) Uani d 1
C C11 -0.17551(4) 0.67480(4) 0.87762(2) 0.01539(5) Uani d 1
H H11 -0.2052(10) 0.5941(9) 0.8611(4) 0.025(2) Uiso d 1
C C12 -0.27025(5) 0.74630(4) 0.90630(2) 0.01872(6) Uani d 1
H H12 -0.3665(11) 0.7162(9) 0.9081(4) 0.029(2) Uiso d 1
C C13 -0.22630(5) 0.85958(4) 0.92885(2) 0.02054(7) Uani d 1
H H13 -0.2939(11) 0.9094(9) 0.9488(4) 0.030(2) Uiso d 1
C C14 -0.08583(5) 0.90087(4) 0.92372(2) 0.02242(8) Uani d 1
H H14 -0.0504(12) 0.9823(10) 0.9386(5) 0.042(3) Uiso d 1
C C15 0.00991(5) 0.82997(4) 0.89583(2) 0.01805(6) Uani d 1
H H15 0.1076(11) 0.8593(9) 0.8916(4) 0.028(2) Uiso d 1
C C16 0.31477(4) 0.65636(3) 0.82525(2) 0.01128(4) Uani d 1
C C17 0.37557(4) 0.77151(3) 0.74242(2) 0.01410(5) Uani d 1
C C18 0.29049(5) 0.86999(4) 0.70787(2) 0.02097(7) Uani d 1
H H18A 0.2746(11) 0.9417(10) 0.7332(4) 0.034(2) Uiso d 1
H H18B 0.3474(11) 0.9002(10) 0.6766(4) 0.035(2) Uiso d 1
H H18C 0.2004(10) 0.8343(9) 0.6905(4) 0.027(2) Uiso d 1
C C19 0.51594(5) 0.82367(5) 0.77147(2) 0.02137(7) Uani d 1
H H19A 0.5774(10) 0.7599(9) 0.7902(4) 0.028(2) Uiso d 1
H H19B 0.4928(11) 0.8866(9) 0.8007(4) 0.033(2) Uiso d 1
H H19C 0.5667(12) 0.8615(9) 0.7433(4) 0.034(2) Uiso d 1
C C20 0.40079(6) 0.65914(4) 0.70642(2) 0.02022(7) Uani d 1
H H20A 0.4617(11) 0.6004(9) 0.7289(4) 0.032(2) Uiso d 1
H H20B 0.4554(10) 0.6840(9) 0.6749(4) 0.026(2) Uiso d 1
H H20C 0.3125(10) 0.6246(9) 0.6886(4) 0.026(2) Uiso d 1
C C21 0.24080(4) 0.57102(3) 0.95807(2) 0.01159(4) Uani d 1
C C22 0.35314(4) 0.71857(3) 1.02605(2) 0.01257(5) Uani d 1
C C23 0.21485(5) 0.73970(5) 1.05462(2) 0.02044(7) Uani d 1
H H23A 0.2402(11) 0.7858(9) 1.0910(4) 0.031(2) Uiso d 1
H H23B 0.1726(12) 0.6633(10) 1.0646(5) 0.037(3) Uiso d 1
H H23C 0.1452(10) 0.7857(9) 1.0287(4) 0.028(2) Uiso d 1
C C24 0.42713(5) 0.84033(4) 1.01594(2) 0.01948(6) Uani d 1
H H24A 0.4558(11) 0.8803(9) 1.0528(4) 0.030(2) Uiso d 1
H H24B 0.5160(12) 0.8251(10) 0.9961(4) 0.035(2) Uiso d 1
H H24C 0.3600(12) 0.8944(10) 0.9927(5) 0.036(2) Uiso d 1
C C25 0.45844(5) 0.62985(4) 1.05809(2) 0.01855(6) Uani d 1
H H25A 0.4965(10) 0.6665(9) 1.0944(4) 0.028(2) Uiso d 1
H H25B 0.4113(11) 0.5510(9) 1.0645(4) 0.028(2) Uiso d 1
H H25C 0.5397(11) 0.6167(9) 1.0358(4) 0.031(2) Uiso d 1
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
O1 0.01323(9) 0.01518(10) 0.01316(9) 0.00325(7) 0.00428(7) 0.00513(7)
O2 0.01207(9) 0.01753(11) 0.01774(10) 0.00354(8) 0.00256(8) 0.00487(8)
O3 0.01592(10) 0.01261(9) 0.00963(8) -0.00433(7) 0.00040(7) -0.00066(7)
O4 0.02262(12) 0.01558(11) 0.01255(9) -0.00587(9) 0.00139(8) 0.00363(8)
N1 0.01166(9) 0.01191(10) 0.01202(9) 0.00010(7) -0.00027(7) -0.00217(7)
N2 0.01000(9) 0.01155(9) 0.01165(9) 0.00056(7) 0.00063(7) -0.00086(7)
N3 0.01013(9) 0.01134(9) 0.00999(8) -0.00032(7) 0.00076(7) 0.00175(7)
N4 0.01248(9) 0.01003(9) 0.00980(8) -0.00225(7) -0.00029(7) 0.00090(7)
C1 0.01354(12) 0.01697(13) 0.01221(11) 0.00117(10) -0.00055(9) -0.00345(9)
C2 0.01536(13) 0.01701(13) 0.01575(12) 0.00058(10) 0.00109(10) -0.00531(10)
C3 0.01249(11) 0.01263(12) 0.01995(13) -0.00107(9) 0.00180(10) -0.00415(10)
C4 0.01706(14) 0.01319(13) 0.02859(18) -0.00098(10) 0.00533(13) -0.00574(12)
C5 0.01895(15) 0.01170(13) 0.0358(2) -0.00012(11) 0.00599(15) -0.00189(13)
C6 0.01834(15) 0.01174(13) 0.0312(2) -0.00076(11) 0.00164(13) 0.00242(12)
C7 0.01558(13) 0.01189(12) 0.02187(15) -0.00184(10) 0.00032(11) 0.00124(10)
C8 0.01170(11) 0.01050(11) 0.01775(12) -0.00152(8) 0.00054(9) -0.00148(9)
C9 0.01114(10) 0.01069(10) 0.01283(10) -0.00145(8) 0.00041(8) -0.00070(8)
C10 0.01197(10) 0.01124(10) 0.01148(10) 0.00070(8) 0.00191(8) 0.00019(8)
C11 0.01255(11) 0.01596(13) 0.01807(13) -0.00103(9) 0.00365(9) -0.00334(10)
C12 0.01477(13) 0.02046(16) 0.02190(15) -0.00054(11) 0.00680(11) -0.00420(12)
C13 0.01936(15) 0.01922(16) 0.02430(17) 0.00141(12) 0.00862(13) -0.00541(13)
C14 0.02111(17) 0.01592(15) 0.0315(2) -0.00126(12) 0.00915(15) -0.00849(14)
C15 0.01639(13) 0.01323(13) 0.02544(16) -0.00203(10) 0.00671(12) -0.00486(11)
C16 0.01117(10) 0.01158(10) 0.01117(10) 0.00015(8) 0.00149(8) 0.00151(8)
C17 0.01572(12) 0.01339(12) 0.01403(11) 0.00324(9) 0.00582(9) 0.00371(9)
C18 0.02573(18) 0.02020(16) 0.01822(14) 0.01002(14) 0.00849(13) 0.00857(12)
C19 0.01873(15) 0.02050(16) 0.02546(18) -0.00404(12) 0.00518(13) 0.00382(13)
C20 0.02767(19) 0.01729(15) 0.01667(14) 0.00551(13) 0.00709(13) 0.00060(11)
C21 0.01299(11) 0.01130(10) 0.01033(9) -0.00198(8) 0.00034(8) 0.00086(8)
C22 0.01253(11) 0.01427(12) 0.01080(10) -0.00043(9) 0.00060(8) -0.00206(8)
C23 0.01573(14) 0.02806(19) 0.01812(14) 0.00095(13) 0.00463(11) -0.00534(13)
C24 0.02259(16) 0.01579(14) 0.01981(15) -0.00553(12) 0.00075(12) -0.00359(11)
C25 0.01928(15) 0.02031(16) 0.01514(13) 0.00355(12) -0.00306(11) -0.00109(11)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_exptl_crystal_face_index_h
_exptl_crystal_face_index_k
_exptl_crystal_face_index_l
_exptl_crystal_face_perp_dist
-10 5 -15 0.2956
12 0 10 0.2005
12 5 4 0.1828
-12 -5 1 0.2230
-10 -8 17 0.1455
-8 -12 10 0.1338
3 14 11 0.1496
-1 14 15 0.1698
-8 2 27 0.1450
-13 0 1 0.2426
3 14 9 0.1487
-5 14 10 0.2263
0 -1 0 0.1258
3 -1 -33 0.1697
10 10 -5 0.1308
1 2 33 0.2066
-11 -1 22 0.1320
9 -9 9 0.1894
4 2 -32 0.1651
-8 7 24 0.1589
5 -4 28 0.2190
9 -7 -21 0.2144
13 0 -12 0.1951
-11 1 -16 0.2581
8 -1 25 0.2119
9 11 -6 0.1319
-4 -15 -2 0.0990
-3 -4 -30 0.1875
-3 -1 33 0.1942
7 3 -29 0.1598
1 -15 7 0.1266
-2 -5 -30 0.1643
11 6 11 0.1838
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C16 O1 C17 120.13(3)
C21 O3 C22 120.02(3)
N2 N1 C9 105.40(3)
C1 N1 N2 109.53(3)
C1 N1 C9 118.23(3)
N1 N2 C10 113.49(3)
N3 N2 N1 103.72(3)
N3 N2 C10 111.82(3)
N4 N3 N2 106.11(3)
N4 N3 C16 113.73(3)
C16 N3 N2 115.47(3)
N3 N4 C9 107.33(3)
C21 N4 N3 116.22(3)
C21 N4 C9 116.75(3)
C2 C1 N1 122.96(4)
C1 C2 C3 120.32(4)
C4 C3 C2 121.60(4)
C4 C3 C8 119.19(4)
C8 C3 C2 119.21(4)
C5 C4 C3 120.59(4)
C4 C5 C6 119.92(4)
C7 C6 C5 120.18(4)
C8 C7 C6 119.95(4)
C3 C8 C9 120.25(3)
C7 C8 C3 120.14(4)
C7 C8 C9 119.59(4)
N1 C9 N4 102.20(3)
N1 C9 C8 113.65(3)
C8 C9 N4 113.80(3)
C11 C10 N2 121.12(4)
C11 C10 C15 120.38(3)
C15 C10 N2 118.16(3)
C10 C11 C12 119.47(4)
C13 C12 C11 120.41(4)
C12 C13 C14 119.68(4)
C15 C14 C13 120.44(4)
C14 C15 C10 119.61(4)
O1 C16 N3 108.34(3)
O2 C16 O1 128.61(4)
O2 C16 N3 122.73(3)
O1 C17 C18 102.08(3)
O1 C17 C19 110.10(4)
O1 C17 C20 109.37(4)
C18 C17 C19 110.80(4)
C20 C17 C18 111.58(4)
C20 C17 C19 112.42(4)
O3 C21 N4 110.60(3)
O4 C21 O3 127.75(3)
O4 C21 N4 121.53(3)
O3 C22 C23 109.65(4)
O3 C22 C24 101.79(3)
O3 C22 C25 109.81(4)
C24 C22 C23 110.43(4)
C25 C22 C23 113.77(4)
C25 C22 C24 110.73(4)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
O1 C16 1.3268(5)
O1 C17 1.4784(6)
O2 C16 1.2044(5)
O3 C21 1.3305(5)
O3 C22 1.4748(5)
O4 C21 1.2120(5)
N1 N2 1.4282(5)
N1 C1 1.4148(6)
N1 C9 1.4700(6)
N2 N3 1.4277(6)
N2 C10 1.4369(5)
N3 N4 1.4146(4)
N3 C16 1.4237(6)
N4 C9 1.5086(5)
N4 C21 1.3949(5)
C1 C2 1.3367(6)
C2 C3 1.4541(6)
C3 C4 1.3998(6)
C3 C8 1.4062(6)
C4 C5 1.3875(8)
C5 C6 1.3953(8)
C6 C7 1.3948(6)
C7 C8 1.3933(6)
C8 C9 1.5085(6)
C10 C11 1.3915(6)
C10 C15 1.3943(6)
C11 C12 1.3955(6)
C12 C13 1.3879(7)
C13 C14 1.3926(7)
C14 C15 1.3880(6)
C17 C18 1.5196(6)
C17 C19 1.5197(7)
C17 C20 1.5195(6)
C22 C23 1.5211(7)
C22 C24 1.5210(6)
C22 C25 1.5204(6)
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
N1 N2 N3 N4 -35.80(3)
N1 N2 N3 C16 91.19(3)
N1 N2 C10 C11 -23.78(5)
N1 N2 C10 C15 162.85(3)
N1 C1 C2 C3 -4.16(6)
N2 N1 C1 C2 141.94(4)
N2 N1 C9 N4 -27.23(3)
N2 N1 C9 C8 -150.29(3)
N2 N3 N4 C9 18.43(3)
N2 N3 N4 C21 -114.35(4)
N2 N3 C16 O1 42.68(4)
N2 N3 C16 O2 -143.34(4)
N2 C10 C11 C12 -172.86(4)
N2 C10 C15 C14 172.36(4)
N3 N2 C10 C11 -140.69(3)
N3 N2 C10 C15 45.94(4)
N3 N4 C9 N1 5.38(3)
N3 N4 C9 C8 128.33(3)
N3 N4 C21 O3 -29.91(4)
N3 N4 C21 O4 153.80(4)
N4 N3 C16 O1 165.71(3)
N4 N3 C16 O2 -20.31(5)
C1 N1 N2 N3 -88.77(4)
C1 N1 N2 C10 149.67(3)
C1 N1 C9 N4 95.55(4)
C1 N1 C9 C8 -27.50(4)
C1 C2 C3 C4 174.71(4)
C1 C2 C3 C8 -4.67(6)
C2 C3 C4 C5 -178.34(4)
C2 C3 C8 C7 177.88(3)
C2 C3 C8 C9 -3.83(5)
C3 C4 C5 C6 0.21(7)
C3 C8 C9 N1 19.40(5)
C3 C8 C9 N4 -97.05(5)
C4 C3 C8 C7 -1.51(5)
C4 C3 C8 C9 176.78(3)
C4 C5 C6 C7 -1.01(7)
C5 C6 C7 C8 0.53(6)
C6 C7 C8 C3 0.73(6)
C6 C7 C8 C9 -177.57(3)
C7 C8 C9 N1 -162.30(3)
C7 C8 C9 N4 81.25(5)
C8 C3 C4 C5 1.04(6)
C9 N1 N2 N3 39.42(4)
C9 N1 N2 C10 -82.14(4)
C9 N1 C1 C2 21.26(5)
C9 N4 C21 O3 -158.24(3)
C9 N4 C21 O4 25.47(5)
C10 N2 N3 N4 86.87(4)
C10 N2 N3 C16 -146.14(3)
C10 C11 C12 C13 0.80(7)
C11 C10 C15 C14 -1.06(7)
C11 C12 C13 C14 -1.24(8)
C12 C13 C14 C15 0.53(8)
C13 C14 C15 C10 0.62(8)
C15 C10 C11 C12 0.36(6)
C16 O1 C17 C18 -178.18(4)
C16 O1 C17 C19 -60.47(5)
C16 O1 C17 C20 63.53(5)
C16 N3 N4 C9 -109.59(3)
C16 N3 N4 C21 117.63(4)
C17 O1 C16 O2 1.27(6)
C17 O1 C16 N3 174.78(3)
C21 O3 C22 C23 -59.09(5)
C21 O3 C22 C24 -176.04(3)
C21 O3 C22 C25 66.61(4)
C21 N4 C9 N1 137.87(3)
C21 N4 C9 C8 -99.17(4)
C22 O3 C21 O4 -5.01(6)
C22 O3 C21 N4 178.99(3)
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_phase_calc
1 0 0 6056.02 167.54 0.0
2 0 0 15401.70 246.04 180.0
3 0 0 4383.84 56.14 180.0
4 0 0 4278.70 52.99 0.0
5 0 0 3243.59 54.70 0.0
6 0 0 195.05 3.67 180.0
7 0 0 381.43 8.32 180.0
8 0 0 722.60 12.25 180.0
9 0 0 237.09 4.30 0.0
10 0 0 144.77 3.37 0.0
11 0 0 173.99 4.72 180.0
12 0 0 205.60 4.18 180.0
13 0 0 6.40 1.36 0.0
14 0 0 352.93 7.58 0.0
15 0 0 3.22 1.52 0.0
16 0 0 30.99 2.60 180.0
17 0 0 80.30 4.01 180.0
18 0 0 3.13 3.14 180.0
19 0 0 62.37 4.68 0.0
1 1 0 1808.00 28.24 0.0
2 1 0 45706.40 364.40 180.0
3 1 0 59.42 0.82 0.0
4 1 0 2477.02 22.97 0.0
5 1 0 1299.38 13.80 0.0
6 1 0 39.41 0.71 0.0
7 1 0 12.53 0.42 0.0
8 1 0 31.01 1.13 180.0
9 1 0 489.72 12.14 180.0
10 1 0 72.01 1.66 0.0
11 1 0 11.18 0.97 0.0
12 1 0 7.96 0.95 0.0
13 1 0 117.88 2.33 180.0
14 1 0 3.14 1.09 0.0
15 1 0 6.23 1.22 180.0
16 1 0 2.17 1.31 0.0
17 1 0 27.59 2.43 0.0
18 1 0 1.56 2.33 0.0
19 1 0 8.05 2.34 0.0
0 2 0 21930.54 278.51 180.0
1 2 0 4087.79 39.78 0.0
2 2 0 3683.13 30.81 0.0
3 2 0 8.77 0.41 180.0
4 2 0 588.50 6.41 0.0
5 2 0 139.26 2.02 0.0
6 2 0 1941.62 24.35 180.0
7 2 0 1205.68 15.26 180.0
8 2 0 126.43 1.74 180.0
9 2 0 676.58 7.73 0.0
10 2 0 107.80 2.00 0.0
11 2 0 17.56 0.97 180.0
12 2 0 38.47 1.48 0.0
13 2 0 27.82 1.69 0.0
14 2 0 9.27 1.36 180.0
15 2 0 7.45 1.41 180.0
16 2 0 3.97 1.35 0.0
17 2 0 5.43 1.69 0.0
18 2 0 20.51 2.51 180.0
19 2 0 39.28 2.91 180.0
1 3 0 19.16 0.41 180.0
2 3 0 349.03 5.02 180.0
3 3 0 468.11 4.84 0.0
4 3 0 1709.52 22.05 180.0
5 3 0 313.45 4.33 0.0
6 3 0 152.76 2.34 180.0
7 3 0 1085.25 13.95 0.0
8 3 0 1358.23 17.18 0.0
9 3 0 71.75 1.28 0.0
10 3 0 76.65 1.63 0.0
11 3 0 142.44 2.74 180.0
12 3 0 5.09 1.10 180.0
13 3 0 62.60 2.00 0.0
14 3 0 0.97 1.44 0.0
15 3 0 3.64 1.65 180.0
16 3 0 5.62 1.44 180.0
17 3 0 2.11 1.44 0.0
18 3 0 23.18 2.45 180.0
19 3 0 3.65 3.37 180.0
0 4 0 2689.21 60.28 180.0
1 4 0 3894.80 33.46 0.0
2 4 0 510.55 5.72 180.0
3 4 0 1891.06 22.91 0.0
4 4 0 73.79 1.65 0.0
5 4 0 66.92 0.95 0.0
6 4 0 195.00 2.39 0.0
7 4 0 17.89 0.57 180.0
8 4 0 350.27 5.53 0.0
9 4 0 1157.10 13.71 180.0
10 4 0 247.87 3.62 180.0
11 4 0 388.71 7.35 0.0
12 4 0 1.50 1.17 0.0
13 4 0 26.27 1.71 180.0
14 4 0 3.78 1.53 0.0
15 4 0 11.90 1.60 180.0
16 4 0 202.70 4.64 180.0
17 4 0 64.27 2.12 180.0
18 4 0 0.23 3.54 0.0
19 4 0 6.19 3.56 180.0
1 5 0 152.11 1.38 0.0
2 5 0 857.69 9.28 0.0
3 5 0 3459.05 32.16 180.0
4 5 0 2094.30 21.33 180.0
5 5 0 112.53 1.45 180.0
6 5 0 676.41 7.12 0.0
7 5 0 595.47 6.19 180.0
8 5 0 444.62 5.61 180.0
9 5 0 588.57 7.35 0.0
10 5 0 82.71 4.75 0.0
11 5 0 285.83 5.12 0.0
12 5 0 48.95 1.56 0.0
13 5 0 91.37 3.24 180.0
14 5 0 16.82 1.62 180.0
15 5 0 43.23 2.42 0.0
16 5 0 14.81 1.91 180.0
17 5 0 3.35 1.74 0.0
18 5 0 29.62 4.17 0.0
19 5 0 21.13 3.91 0.0
0 6 0 4268.87 83.92 0.0
1 6 0 938.14 8.83 0.0
2 6 0 983.39 10.58 0.0
3 6 0 101.29 1.17 180.0
4 6 0 1.64 0.28 0.0
5 6 0 118.31 1.97 0.0
6 6 0 1457.98 13.98 0.0
7 6 0 122.38 2.07 180.0
8 6 0 948.88 11.43 180.0
9 6 0 36.67 1.29 0.0
10 6 0 492.30 7.81 0.0
11 6 0 220.71 3.70 180.0
12 6 0 23.98 1.26 180.0
13 6 0 3.34 1.12 0.0
14 6 0 6.73 1.52 180.0
15 6 0 228.30 6.60 0.0
16 6 0 186.32 4.15 0.0
17 6 0 1.08 2.50 0.0
18 6 0 20.88 2.78 180.0
19 6 0 5.35 3.64 0.0
1 7 0 156.78 1.89 0.0
2 7 0 38.28 0.84 0.0
3 7 0 173.74 1.46 180.0
4 7 0 373.12 3.85 0.0
5 7 0 30.09 0.59 0.0
6 7 0 250.13 2.67 0.0
7 7 0 23.81 0.60 0.0
8 7 0 23.70 0.59 0.0
9 7 0 1.00 0.89 180.0
10 7 0 545.82 8.16 0.0
11 7 0 11.89 1.07 0.0
12 7 0 32.63 1.71 180.0
13 7 0 78.93 2.30 0.0
14 7 0 40.34 2.58 0.0
15 7 0 3.98 2.70 180.0
16 7 0 30.52 2.50 0.0
17 7 0 5.54 2.07 180.0
18 7 0 3.21 2.53 180.0
0 8 0 1387.61 19.39 0.0
1 8 0 10.35 0.41 0.0
2 8 0 257.85 3.43 180.0
3 8 0 6.01 0.41 180.0
4 8 0 54.40 0.80 0.0
5 8 0 1.55 0.42 180.0
6 8 0 390.66 3.66 180.0
7 8 0 0.76 0.51 180.0
8 8 0 45.57 1.00 180.0
9 8 0 41.39 1.88 180.0
10 8 0 2.09 1.19 180.0
11 8 0 108.67 2.62 0.0
12 8 0 270.31 4.59 180.0
13 8 0 42.97 1.71 180.0
14 8 0 81.72 4.77 0.0
15 8 0 29.82 2.20 0.0
16 8 0 24.23 2.15 180.0
17 8 0 1.41 2.55 180.0
18 8 0 22.22 4.02 0.0
1 9 0 164.07 1.81 0.0
2 9 0 9.54 0.52 180.0
3 9 0 4.60 0.38 180.0
4 9 0 0.57 0.37 180.0
5 9 0 80.40 1.31 0.0
6 9 0 54.52 0.80 0.0
7 9 0 290.12 2.83 0.0
8 9 0 23.89 0.81 0.0
9 9 0 4.88 1.22 0.0
10 9 0 12.83 1.32 180.0
11 9 0 218.80 4.12 0.0
12 9 0 1.64 1.45 180.0
13 9 0 25.18 1.46 180.0
14 9 0 2.67 1.43 180.0
15 9 0 16.64 1.78 0.0
16 9 0 19.62 2.63 0.0
17 9 0 8.40 2.69 180.0
18 9 0 3.73 3.85 180.0
0 10 0 1298.66 16.24 180.0
1 10 0 0.69 0.34 180.0
2 10 0 674.91 8.05 0.0
3 10 0 3.19 0.62 180.0
4 10 0 210.00 3.11 180.0
5 10 0 9.15 0.44 180.0
6 10 0 17.97 0.50 0.0
7 10 0 0.22 0.52 180.0
8 10 0 1.34 0.73 180.0
9 10 0 2.33 0.74 0.0
10 10 0 92.62 2.02 180.0
11 10 0 4.71 1.49 0.0
12 10 0 55.46 1.84 0.0
13 10 0 0.42 1.18 180.0
14 10 0 9.54 1.36 180.0
15 10 0 62.64 2.09 180.0
16 10 0 9.72 2.76 0.0
17 10 0 5.63 4.37 0.0
1 11 0 561.74 5.25 180.0
2 11 0 43.30 0.83 180.0
3 11 0 32.33 1.20 180.0
4 11 0 217.60 2.51 180.0
5 11 0 261.64 2.86 180.0
6 11 0 128.08 1.47 180.0
7 11 0 38.09 0.98 0.0
8 11 0 76.59 2.07 0.0
9 11 0 202.64 2.83 0.0
10 11 0 32.79 1.54 180.0
11 11 0 0.35 1.19 0.0
12 11 0 186.43 3.61 0.0
13 11 0 7.01 1.33 0.0
14 11 0 2.53 1.46 0.0
15 11 0 9.92 4.52 0.0
16 11 0 8.02 2.76 180.0
17 11 0 4.38 2.61 0.0
0 12 0 1058.26 12.43 0.0
1 12 0 10.07 0.52 180.0
2 12 0 231.04 2.48 180.0
3 12 0 13.75 0.65 180.0
4 12 0 83.55 1.31 0.0
5 12 0 67.24 1.45 0.0
6 12 0 1.92 0.77 0.0
7 12 0 26.59 1.11 0.0
8 12 0 82.50 1.65 180.0
9 12 0 41.43 1.24 180.0
10 12 0 36.60 1.55 0.0
11 12 0 27.98 1.89 180.0
12 12 0 98.40 2.87 0.0
13 12 0 0.00 1.50 180.0
14 12 0 11.19 1.97 0.0
15 12 0 62.30 3.71 0.0
16 12 0 89.94 6.60 0.0
1 13 0 118.60 1.46 180.0
2 13 0 165.88 2.09 180.0
3 13 0 39.98 1.14 0.0
4 13 0 44.75 1.14 0.0
5 13 0 8.82 0.90 0.0
6 13 0 2.48 1.00 0.0
7 13 0 46.68 2.17 0.0
8 13 0 232.21 3.49 0.0
9 13 0 6.35 1.02 180.0
10 13 0 494.99 7.59 0.0
11 13 0 29.61 2.57 0.0
12 13 0 30.20 1.95 0.0
13 13 0 18.73 1.54 0.0
14 13 0 13.72 2.51 0.0
15 13 0 1.53 3.92 180.0
16 13 0 1.54 2.48 0.0
0 14 0 82.51 2.03 180.0
1 14 0 5.63 0.82 180.0
2 14 0 38.94 1.20 180.0
3 14 0 17.39 0.92 0.0
4 14 0 2.00 0.83 0.0
5 14 0 136.02 2.11 0.0
6 14 0 23.14 1.41 180.0
7 14 0 274.04 4.50 180.0
8 14 0 3.72 1.43 0.0
9 14 0 3.67 1.42 180.0
10 14 0 91.47 5.11 180.0
11 14 0 47.45 4.40 180.0
12 14 0 94.98 2.99 180.0
13 14 0 0.18 1.60 180.0
14 14 0 1.67 1.98 180.0
15 14 0 12.42 3.26 0.0
1 15 0 68.90 1.84 0.0
2 15 0 2.81 1.02 180.0
3 15 0 92.39 3.26 0.0
4 15 0 32.18 1.47 180.0
5 15 0 111.84 3.27 180.0
6 15 0 2.55 1.21 0.0
7 15 0 0.05 1.34 180.0
8 15 0 5.12 2.27 0.0
9 15 0 2.03 1.59 180.0
10 15 0 66.66 2.84 180.0
11 15 0 2.36 1.74 180.0
12 15 0 25.43 1.72 0.0
13 15 0 27.51 3.44 0.0
14 15 0 43.17 2.27 180.0
15 15 0 5.74 4.19 180.0
0 16 0 230.47 8.98 180.0
1 16 0 25.14 1.69 180.0
2 16 0 344.80 6.44 180.0
3 16 0 275.25 3.50 180.0
4 16 0 97.16 3.01 0.0
5 16 0 51.63 2.11 180.0
6 16 0 31.27 1.94 0.0
7 16 0 36.81 3.26 0.0
8 16 0 5.65 1.77 0.0
9 16 0 14.63 1.48 180.0
10 16 0 4.11 1.63 0.0
11 16 0 47.54 1.86 0.0
12 16 0 21.91 1.72 180.0
13 16 0 3.74 1.75 0.0
14 16 0 2.32 3.97 180.0
1 17 0 113.67 2.59 180.0
2 17 0 108.12 2.68 0.0
3 17 0 15.20 1.27 180.0
4 17 0 62.03 2.04 0.0
5 17 0 12.30 1.75 0.0
6 17 0 82.13 3.05 180.0
7 17 0 8.87 2.55 180.0
8 17 0 0.00 2.54 0.0
9 17 0 67.55 5.00 0.0
10 17 0 13.64 2.03 180.0
11 17 0 15.79 2.46 0.0
12 17 0 7.26 2.32 0.0
13 17 0 23.89 3.06 0.0
0 18 0 102.98 3.12 0.0
1 18 0 18.91 1.45 180.0
2 18 0 27.49 1.83 0.0
3 18 0 13.36 2.16 0.0
4 18 0 73.21 2.06 180.0
5 18 0 21.55 1.87 0.0
6 18 0 45.08 2.25 0.0
7 18 0 5.68 2.64 180.0
8 18 0 5.11 1.89 180.0
9 18 0 17.37 2.43 0.0
10 18 0 0.14 2.28 0.0
11 18 0 12.91 2.53 180.0
12 18 0 2.05 2.26 180.0
1 19 0 15.15 1.31 0.0
2 19 0 69.15 2.74 180.0
3 19 0 5.43 1.50 180.0
4 19 0 25.87 2.11 0.0
5 19 0 10.99 1.79 180.0
6 19 0 7.28 1.86 180.0
7 19 0 25.08 8.90 180.0
8 19 0 9.66 2.37 180.0
9 19 0 12.46 3.93 0.0
10 19 0 3.21 2.24 180.0
11 19 0 36.71 3.91 180.0
0 20 0 3.19 1.66 180.0
1 20 0 1.31 1.35 0.0
2 20 0 47.83 1.97 180.0
3 20 0 65.97 3.76 180.0
4 20 0 2.63 2.00 180.0
5 20 0 4.94 3.74 0.0
6 20 0 83.65 4.51 180.0
7 20 0 12.04 2.52 180.0
8 20 0 48.41 2.93 180.0
9 20 0 1.57 2.24 180.0
10 20 0 6.62 4.46 0.0
1 21 0 19.83 4.87 0.0
2 21 0 15.29 2.98 0.0
3 21 0 0.35 4.09 0.0
4 21 0 25.07 4.85 180.0
5 21 0 23.09 4.85 0.0
6 21 0 25.70 2.71 0.0
7 21 0 2.85 2.69 0.0
8 21 0 34.65 4.91 180.0
0 22 0 2.44 3.87 0.0
1 22 0 9.23 2.96 180.0
2 22 0 29.45 4.98 180.0
3 22 0 12.53 4.47 180.0
4 22 0 20.21 4.61 0.0
5 22 0 15.18 7.06 0.0
6 22 0 2.21 3.13 180.0
1 23 0 2.41 4.05 0.0
2 23 0 11.54 4.42 0.0
3 23 0 9.87 4.38 0.0
-19 1 1 3.80 4.37 0.0
-18 1 1 1.65 2.23 0.0
-17 1 1 63.74 2.28 0.0
-16 1 1 1.61 1.31 0.0
-15 1 1 9.66 1.29 0.0
-14 1 1 0.00 1.08 0.0
-13 1 1 1.67 1.03 0.0
-12 1 1 2.07 0.86 180.0
-11 1 1 1.18 0.82 180.0
-10 1 1 141.28 1.99 0.0
-9 1 1 100.26 1.91 180.0
-8 1 1 226.49 3.98 0.0
-7 1 1 39.80 1.91 0.0
-6 1 1 38.34 0.62 180.0
-5 1 1 318.86 3.32 0.0
-4 1 1 170.68 1.76 0.0
-3 1 1 12046.35 104.91 0.0
-2 1 1 4645.16 43.10 0.0
-1 1 1 1557.79 24.91 0.0
0 1 1 13036.56 180.74 180.0
1 1 1 4832.57 76.42 180.0
2 1 1 129.68 1.21 180.0
3 1 1 5676.22 52.23 180.0
4 1 1 1000.27 11.52 180.0
5 1 1 1540.94 20.37 180.0
6 1 1 72.16 1.05 180.0
7 1 1 51.02 0.87 0.0
8 1 1 162.82 2.89 0.0
9 1 1 4.33 0.78 180.0
10 1 1 85.08 2.09 180.0
11 1 1 49.67 1.48 0.0
12 1 1 151.73 2.98 0.0
13 1 1 0.88 0.96 0.0
14 1 1 24.96 1.45 0.0
15 1 1 17.47 1.52 180.0
16 1 1 8.37 1.36 180.0
17 1 1 5.17 1.63 180.0
18 1 1 32.79 2.78 0.0
19 1 1 14.46 2.10 180.0
-19 2 1 20.39 2.56 0.0
-18 2 1 6.06 2.26 180.0
-17 2 1 19.50 1.84 180.0
-16 2 1 13.94 1.42 0.0
-15 2 1 1.00 1.22 0.0
-14 2 1 3.15 1.27 0.0
-13 2 1 205.15 4.36 180.0
-12 2 1 140.67 2.80 180.0
-11 2 1 33.59 1.17 180.0
-10 2 1 219.60 3.02 0.0
-9 2 1 81.55 1.53 180.0
-8 2 1 5837.86 66.21 180.0
-7 2 1 93.60 1.67 180.0
-6 2 1 38.01 0.78 0.0
-5 2 1 11823.38 124.01 0.0
-4 2 1 833.53 8.99 0.0
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0 2 1 2432.45 34.88 0.0
1 2 1 17239.09 213.46 180.0
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3 2 1 5424.36 56.78 0.0
4 2 1 882.89 10.29 0.0
5 2 1 917.23 9.20 0.0
6 2 1 1634.98 17.57 180.0
7 2 1 932.13 11.13 180.0
8 2 1 6.17 0.52 180.0
9 2 1 268.54 3.52 0.0
10 2 1 19.20 0.98 180.0
11 2 1 236.20 4.36 180.0
12 2 1 131.07 2.70 0.0
13 2 1 1.23 1.04 0.0
14 2 1 12.89 1.40 180.0
15 2 1 1.14 1.39 0.0
16 2 1 2.92 1.70 0.0
17 2 1 6.90 3.37 180.0
18 2 1 10.87 2.40 0.0
19 2 1 45.35 4.48 0.0
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0 3 1 122.64 1.09 180.0
1 3 1 195.75 1.66 180.0
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3 3 1 2522.03 50.17 0.0
4 3 1 2400.80 25.08 180.0
5 3 1 4860.26 119.56 180.0
6 3 1 118.08 1.89 180.0
7 3 1 18.66 0.62 0.0
8 3 1 56.96 1.40 180.0
9 3 1 129.29 2.36 180.0
10 3 1 79.31 1.67 180.0
11 3 1 122.51 2.36 180.0
12 3 1 534.80 8.72 180.0
13 3 1 4.42 1.32 180.0
14 3 1 323.87 5.12 180.0
15 3 1 3.82 1.54 180.0
16 3 1 17.46 1.53 0.0
17 3 1 26.99 1.75 0.0
18 3 1 24.93 2.75 180.0
19 3 1 0.00 3.51 0.0
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0 4 1 12.09 0.38 0.0
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5 4 1 52.24 0.85 180.0
6 4 1 58.27 1.17 0.0
7 4 1 765.90 13.09 0.0
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11 4 1 2.62 1.31 180.0
12 4 1 6.55 1.21 180.0
13 4 1 3.99 1.41 0.0
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19 4 1 17.96 3.76 180.0
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7 5 1 252.38 3.81 0.0
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10 5 1 0.73 0.98 0.0
11 5 1 22.65 1.26 0.0
12 5 1 410.64 5.19 0.0
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16 5 1 8.58 2.10 0.0
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13 6 1 86.20 2.05 180.0
14 6 1 16.78 1.45 180.0
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19 6 1 56.14 4.81 180.0
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8 7 1 373.74 5.64 0.0
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11 7 1 106.76 3.04 180.0
12 7 1 212.70 3.84 0.0
13 7 1 1.47 1.98 0.0
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0 8 1 233.78 2.38 0.0
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4 8 1 494.75 5.14 180.0
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6 8 1 44.69 0.82 0.0
7 8 1 1286.47 12.51 180.0
8 8 1 252.89 3.20 180.0
9 8 1 38.81 1.85 180.0
10 8 1 11.80 1.24 0.0
11 8 1 234.53 4.42 180.0
12 8 1 7.44 1.29 0.0
13 8 1 79.54 2.17 0.0
14 8 1 0.00 1.57 180.0
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16 8 1 9.88 2.04 180.0
17 8 1 0.99 2.53 180.0
18 8 1 21.37 4.21 0.0
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5 9 1 359.50 3.10 180.0
6 9 1 62.22 0.87 0.0
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8 9 1 134.94 1.91 180.0
9 9 1 17.34 1.21 0.0
10 9 1 114.20 2.54 0.0
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13 9 1 76.49 2.17 0.0
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16 9 1 20.07 2.30 0.0
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0 10 1 356.61 2.78 180.0
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3 10 1 2.27 0.33 0.0
4 10 1 1924.81 15.75 0.0
5 10 1 7.29 0.48 0.0
6 10 1 29.34 0.68 0.0
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10 10 1 6.45 1.01 180.0
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13 10 1 1.89 1.06 180.0
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0 11 1 140.76 1.49 0.0
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4 11 1 1.01 0.58 180.0
5 11 1 36.87 0.76 180.0
6 11 1 2.09 0.59 0.0
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8 11 1 4.56 0.78 0.0
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10 11 1 1.08 1.10 0.0
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12 11 1 0.00 1.26 0.0
13 11 1 11.35 1.30 0.0
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15 11 1 0.99 2.54 180.0
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0 12 1 67.27 1.14 180.0
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4 12 1 131.11 1.81 180.0
5 12 1 253.90 3.31 0.0
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9 12 1 83.92 1.79 0.0
10 12 1 15.63 1.22 180.0
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13 12 1 44.91 1.89 180.0
14 12 1 9.39 1.82 180.0
15 12 1 66.53 3.83 180.0
16 12 1 0.29 2.59 0.0
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0 13 1 73.12 1.05 180.0
1 13 1 163.21 1.93 180.0
2 13 1 294.07 3.52 0.0
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4 13 1 77.19 1.58 180.0
5 13 1 29.40 1.11 180.0
6 13 1 15.17 1.16 180.0
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9 13 1 172.92 3.21 0.0
10 13 1 36.52 1.69 0.0
11 13 1 46.80 2.13 0.0
12 13 1 139.04 2.98 0.0
13 13 1 38.48 2.11 0.0
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15 13 1 3.27 3.42 180.0
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7 15 1 0.98 1.70 0.0
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10 15 1 8.47 2.71 0.0
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4 17 1 1.18 1.17 180.0
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13 17 1 2.18 2.68 180.0
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0 18 1 157.66 2.97 180.0
1 18 1 11.86 1.81 0.0
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1 2 8 649.00 4.65 0.0
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10 2 8 266.22 3.38 0.0
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12 2 8 377.82 5.29 0.0
13 2 8 173.25 5.45 0.0
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-5 18 8 192.77 3.56 0.0
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-3 18 8 17.05 1.64 180.0
-2 18 8 0.10 1.41 0.0
-1 18 8 14.51 1.47 0.0
0 18 8 243.56 3.80 0.0
1 18 8 37.19 2.73 0.0
2 18 8 1.12 1.55 0.0
3 18 8 0.00 1.54 0.0
4 18 8 1.16 1.72 180.0
5 18 8 0.52 1.71 180.0
6 18 8 1.51 2.39 0.0
7 18 8 39.55 2.79 0.0
8 18 8 28.06 2.20 0.0
9 18 8 46.33 2.42 180.0
10 18 8 36.71 3.78 180.0
11 18 8 9.75 3.11 180.0
-11 19 8 7.32 2.96 0.0
-10 19 8 10.79 3.12 0.0
-9 19 8 2.61 2.82 0.0
-8 19 8 10.42 2.36 0.0
-7 19 8 27.49 2.59 0.0
-6 19 8 29.29 2.17 0.0
-5 19 8 6.23 1.68 0.0
-4 19 8 57.74 2.06 180.0
-3 19 8 17.89 1.88 180.0
-2 19 8 303.17 7.20 0.0
-1 19 8 16.24 1.56 0.0
0 19 8 18.29 1.72 180.0
1 19 8 13.31 1.49 180.0
2 19 8 3.45 1.75 0.0
3 19 8 2.65 2.04 180.0
4 19 8 0.70 2.11 180.0
5 19 8 32.92 5.84 0.0
6 19 8 78.15 3.76 0.0
7 19 8 0.00 1.86 180.0
8 19 8 6.50 1.93 180.0
9 19 8 40.82 3.57 180.0
10 19 8 22.74 3.14 180.0
-9 20 8 66.26 3.94 0.0
-8 20 8 2.76 2.34 180.0
-7 20 8 15.00 3.19 180.0
-6 20 8 27.13 3.52 180.0
-5 20 8 13.40 3.32 0.0
-4 20 8 88.69 4.11 0.0
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-2 20 8 56.56 2.24 180.0
-1 20 8 7.60 1.85 180.0
0 20 8 18.46 1.68 180.0
1 20 8 1.29 1.54 180.0
2 20 8 8.81 1.66 180.0
3 20 8 7.62 2.86 0.0
4 20 8 85.40 6.86 0.0
5 20 8 75.87 6.56 0.0
6 20 8 0.00 4.13 0.0
7 20 8 49.24 3.89 180.0
8 20 8 27.91 3.63 180.0
9 20 8 11.97 4.74 0.0
-8 21 8 0.00 4.15 0.0
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-6 21 8 3.63 3.08 0.0
-5 21 8 4.58 4.36 180.0
-4 21 8 20.26 4.78 0.0
-3 21 8 6.01 3.12 180.0
-2 21 8 164.28 6.21 180.0
-1 21 8 12.74 3.29 180.0
0 21 8 0.79 2.42 180.0
1 21 8 0.00 2.70 0.0
2 21 8 17.54 4.77 0.0
3 21 8 10.48 6.86 0.0
4 21 8 16.20 3.38 180.0
5 21 8 3.41 3.15 180.0
6 21 8 6.51 3.12 180.0
7 21 8 26.86 4.57 0.0
-6 22 8 49.88 5.61 0.0
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-4 22 8 3.33 2.97 0.0
-3 22 8 5.85 4.94 180.0
-2 22 8 0.25 2.40 180.0
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0 22 8 49.28 3.11 0.0
1 22 8 4.57 4.35 180.0
2 22 8 16.43 3.34 180.0
3 22 8 8.39 3.25 0.0
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0 23 8 11.44 4.71 0.0
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-16 1 9 72.12 2.06 0.0
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-14 1 9 223.04 4.17 180.0
-13 1 9 51.58 1.55 180.0
-12 1 9 170.80 2.60 0.0
-11 1 9 4.00 0.79 0.0
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-9 1 9 49.63 0.94 180.0
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-6 1 9 0.93 0.34 0.0
-5 1 9 124.33 1.22 0.0
-4 1 9 7.15 0.26 0.0
-3 1 9 1219.25 10.97 0.0
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0 1 9 12.36 0.20 180.0
1 1 9 5938.78 40.24 180.0
2 1 9 3351.05 36.17 0.0
3 1 9 1273.67 16.08 0.0
4 1 9 327.02 3.18 0.0
5 1 9 143.54 1.27 0.0
6 1 9 397.92 3.19 0.0
7 1 9 550.51 4.32 0.0
8 1 9 34.36 0.69 0.0
9 1 9 68.04 0.92 0.0
10 1 9 161.37 1.84 180.0
11 1 9 93.92 1.63 180.0
12 1 9 23.13 1.24 0.0
13 1 9 11.48 1.97 0.0
14 1 9 2.33 1.54 0.0
15 1 9 2.55 1.41 180.0
16 1 9 4.91 2.10 0.0
17 1 9 21.72 2.11 180.0
18 1 9 6.54 1.83 180.0
-19 2 9 10.66 3.84 180.0
-18 2 9 6.40 2.37 180.0
-17 2 9 18.71 1.75 180.0
-16 2 9 0.00 1.41 0.0
-15 2 9 2.60 1.26 180.0
-14 2 9 31.00 2.20 180.0
-13 2 9 37.30 1.76 0.0
-12 2 9 130.79 2.66 0.0
-11 2 9 77.36 1.54 0.0
-10 2 9 618.09 6.27 180.0
-9 2 9 64.09 1.12 0.0
-8 2 9 298.46 3.17 180.0
-7 2 9 6.40 0.38 180.0
-6 2 9 48.87 0.73 180.0
-5 2 9 757.19 7.06 180.0
-4 2 9 1055.51 11.72 0.0
-3 2 9 3521.21 28.13 180.0
-2 2 9 527.18 3.59 180.0
-1 2 9 2215.62 12.16 180.0
0 2 9 1902.13 12.15 0.0
1 2 9 5932.25 41.27 0.0
2 2 9 191.72 1.48 180.0
3 2 9 4427.20 41.66 0.0
4 2 9 989.79 13.77 0.0
5 2 9 671.77 5.48 0.0
6 2 9 57.17 0.96 180.0
7 2 9 5.23 0.36 0.0
8 2 9 109.19 1.54 180.0
9 2 9 0.97 0.51 180.0
10 2 9 151.57 1.95 0.0
11 2 9 136.74 2.16 180.0
12 2 9 51.97 1.94 0.0
13 2 9 133.97 3.01 0.0
14 2 9 11.05 2.01 0.0
15 2 9 208.35 3.92 180.0
16 2 9 13.07 1.47 180.0
17 2 9 35.58 2.50 0.0
18 2 9 29.81 2.49 0.0
-19 3 9 118.45 6.29 180.0
-18 3 9 2.78 2.31 0.0
-17 3 9 30.07 1.73 180.0
-16 3 9 186.03 3.81 180.0
-15 3 9 106.69 2.65 180.0
-14 3 9 6.44 1.18 0.0
-13 3 9 6.51 1.30 0.0
-12 3 9 70.73 1.79 180.0
-11 3 9 105.34 1.89 180.0
-10 3 9 507.70 5.38 180.0
-9 3 9 74.66 1.20 0.0
-8 3 9 1141.66 10.94 0.0
-7 3 9 30.45 0.55 0.0
-6 3 9 396.39 4.02 0.0
-5 3 9 63.36 0.89 180.0
-4 3 9 1.23 0.16 0.0
-3 3 9 657.30 4.88 0.0
-2 3 9 1239.18 8.21 180.0
-1 3 9 174.36 1.23 180.0
0 3 9 6669.20 47.66 180.0
1 3 9 1783.58 14.47 0.0
2 3 9 221.98 1.72 180.0
3 3 9 75.65 0.91 180.0
4 3 9 256.41 2.40 180.0
5 3 9 22.49 0.48 0.0
6 3 9 2.15 0.33 180.0
7 3 9 1064.94 8.52 0.0
8 3 9 373.42 4.12 0.0
9 3 9 197.03 2.42 180.0
10 3 9 58.26 1.32 0.0
11 3 9 344.80 6.62 0.0
12 3 9 19.36 1.43 180.0
13 3 9 458.68 7.40 180.0
14 3 9 335.22 5.47 180.0
15 3 9 56.59 2.43 180.0
16 3 9 8.43 1.28 0.0
17 3 9 34.76 2.41 0.0
18 3 9 29.78 4.85 180.0
-19 4 9 7.12 2.58 180.0
-18 4 9 0.00 3.51 180.0
-17 4 9 7.35 1.49 0.0
-16 4 9 32.73 2.01 0.0
-15 4 9 12.95 2.40 180.0
-14 4 9 1.24 1.18 180.0
-13 4 9 43.73 1.70 180.0
-12 4 9 45.08 2.44 180.0
-11 4 9 58.41 2.01 0.0
-10 4 9 56.70 2.18 0.0
-9 4 9 95.33 2.14 180.0
-8 4 9 624.02 8.06 0.0
-7 4 9 0.83 0.34 0.0
-6 4 9 7.36 0.29 180.0
-5 4 9 179.39 1.65 180.0
-4 4 9 122.01 1.16 180.0
-3 4 9 125.66 1.43 180.0
-2 4 9 12.35 0.28 0.0
-1 4 9 159.66 1.14 180.0
0 4 9 47.53 0.96 180.0
1 4 9 743.27 6.74 180.0
2 4 9 21.64 0.40 180.0
3 4 9 61.50 0.87 0.0
4 4 9 73.22 1.70 180.0
5 4 9 120.10 1.39 0.0
6 4 9 469.41 6.53 180.0
7 4 9 651.84 6.18 180.0
8 4 9 193.91 3.35 0.0
9 4 9 59.98 1.22 0.0
10 4 9 118.67 2.19 180.0
11 4 9 3.16 1.49 180.0
12 4 9 15.89 1.43 0.0
13 4 9 19.99 1.56 0.0
14 4 9 19.18 1.58 0.0
15 4 9 95.23 2.28 0.0
16 4 9 5.10 2.15 0.0
17 4 9 32.82 4.26 0.0
18 4 9 25.45 4.77 180.0
-19 5 9 2.98 2.27 0.0
-18 5 9 0.32 2.49 180.0
-17 5 9 13.44 1.83 0.0
-16 5 9 9.25 2.20 0.0
-15 5 9 2.74 1.84 0.0
-14 5 9 2.99 2.27 180.0
-13 5 9 76.97 2.89 0.0
-12 5 9 19.53 1.20 180.0
-11 5 9 12.76 0.92 180.0
-10 5 9 185.19 2.43 0.0
-9 5 9 207.45 2.20 180.0
-8 5 9 1.35 0.31 0.0
-7 5 9 69.41 0.98 0.0
-6 5 9 349.58 3.39 0.0
-5 5 9 43.06 0.88 180.0
-4 5 9 8.72 0.37 0.0
-3 5 9 10.17 0.28 0.0
-2 5 9 465.22 3.14 0.0
-1 5 9 233.39 1.67 0.0
0 5 9 533.44 4.54 180.0
1 5 9 62.93 1.33 0.0
2 5 9 23.46 0.58 180.0
3 5 9 639.07 5.95 0.0
4 5 9 14.54 0.51 0.0
5 5 9 580.97 5.51 180.0
6 5 9 418.97 5.06 0.0
7 5 9 100.42 1.40 0.0
8 5 9 1025.80 9.53 0.0
9 5 9 418.83 4.14 0.0
10 5 9 9.71 0.80 0.0
11 5 9 73.36 1.93 180.0
12 5 9 36.74 1.91 0.0
13 5 9 25.15 1.66 0.0
14 5 9 2.87 1.51 180.0
15 5 9 3.96 1.52 180.0
16 5 9 55.76 2.83 180.0
17 5 9 12.50 2.86 180.0
18 5 9 2.33 4.25 0.0
-19 6 9 19.55 3.77 0.0
-18 6 9 5.80 1.96 180.0
-17 6 9 3.08 2.69 180.0
-16 6 9 5.83 2.03 0.0
-15 6 9 4.46 3.47 180.0
-14 6 9 232.24 6.89 180.0
-13 6 9 94.32 4.08 180.0
-12 6 9 22.71 1.77 180.0
-11 6 9 245.84 3.27 180.0
-10 6 9 22.08 0.95 180.0
-9 6 9 6.70 0.70 180.0
-8 6 9 94.03 1.84 180.0
-7 6 9 251.85 2.70 0.0
-6 6 9 11.91 0.40 180.0
-5 6 9 38.40 0.72 180.0
-4 6 9 1042.89 7.57 180.0
-3 6 9 6.88 0.29 0.0
-2 6 9 0.41 0.18 180.0
-1 6 9 857.85 6.29 0.0
0 6 9 450.54 3.66 180.0
1 6 9 2.29 0.21 180.0
2 6 9 686.33 5.54 0.0
3 6 9 152.62 1.76 180.0
4 6 9 339.03 2.68 0.0
5 6 9 0.83 0.43 180.0
6 6 9 739.32 7.01 0.0
7 6 9 599.47 5.89 0.0
8 6 9 36.13 0.79 0.0
9 6 9 71.12 1.25 180.0
10 6 9 36.15 1.76 180.0
11 6 9 18.68 1.34 180.0
12 6 9 91.69 2.77 0.0
13 6 9 78.04 4.32 0.0
14 6 9 23.53 2.10 180.0
15 6 9 1.87 1.50 0.0
16 6 9 21.45 1.98 0.0
17 6 9 0.17 3.00 0.0
18 6 9 3.10 2.20 0.0
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-13 7 9 230.80 5.93 180.0
-12 7 9 27.02 1.92 0.0
-11 7 9 104.41 2.94 0.0
-10 7 9 0.82 0.86 0.0
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-8 7 9 53.73 0.91 180.0
-7 7 9 221.09 1.80 0.0
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-5 7 9 100.50 0.97 180.0
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-1 7 9 988.05 7.49 0.0
0 7 9 64.13 0.68 0.0
1 7 9 2200.08 17.83 180.0
2 7 9 121.46 1.31 0.0
3 7 9 349.11 2.85 0.0
4 7 9 211.59 1.95 0.0
5 7 9 2.89 0.42 0.0
6 7 9 71.88 1.15 180.0
7 7 9 63.42 1.30 180.0
8 7 9 1.20 0.63 180.0
9 7 9 6.87 0.69 180.0
10 7 9 4.36 1.04 180.0
11 7 9 25.27 1.69 180.0
12 7 9 78.32 2.91 180.0
13 7 9 167.34 4.71 0.0
14 7 9 1.63 1.62 0.0
15 7 9 51.48 2.30 180.0
16 7 9 25.64 2.58 180.0
17 7 9 5.23 2.25 180.0
18 7 9 36.71 3.46 0.0
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-14 8 9 2.66 1.34 180.0
-13 8 9 135.86 2.91 180.0
-12 8 9 6.82 1.30 0.0
-11 8 9 202.68 3.04 0.0
-10 8 9 22.44 0.94 0.0
-9 8 9 5.14 0.69 180.0
-8 8 9 221.48 2.12 180.0
-7 8 9 86.25 0.93 180.0
-6 8 9 81.35 0.94 0.0
-5 8 9 46.13 0.67 0.0
-4 8 9 715.99 5.30 180.0
-3 8 9 2.23 0.31 180.0
-2 8 9 190.93 1.72 180.0
-1 8 9 1474.85 12.56 180.0
0 8 9 31.66 0.44 180.0
1 8 9 80.81 0.82 180.0
2 8 9 6.83 0.31 0.0
3 8 9 1392.69 9.91 0.0
4 8 9 586.77 4.67 0.0
5 8 9 1.55 0.46 180.0
6 8 9 16.88 0.76 0.0
7 8 9 43.63 1.06 0.0
8 8 9 71.04 1.34 0.0
9 8 9 0.36 0.76 180.0
10 8 9 63.29 1.69 180.0
11 8 9 86.71 2.14 0.0
12 8 9 15.38 1.40 180.0
13 8 9 4.72 1.49 180.0
14 8 9 40.70 2.21 0.0
15 8 9 3.22 1.50 180.0
16 8 9 117.13 4.68 0.0
17 8 9 34.86 3.97 0.0
-18 9 9 18.16 3.77 0.0
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-16 9 9 90.02 4.10 180.0
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-13 9 9 4.89 1.37 0.0
-12 9 9 0.69 1.27 180.0
-11 9 9 44.67 1.71 0.0
-10 9 9 58.14 1.99 180.0
-9 9 9 1.24 0.62 180.0
-8 9 9 2.66 0.45 0.0
-7 9 9 0.45 0.38 0.0
-6 9 9 37.49 0.66 180.0
-5 9 9 188.16 2.52 0.0
-4 9 9 364.40 3.86 180.0
-3 9 9 1256.64 9.73 180.0
-2 9 9 54.16 0.87 180.0
-1 9 9 1016.59 9.78 180.0
0 9 9 802.35 5.99 180.0
1 9 9 297.90 2.39 0.0
2 9 9 23.02 0.42 180.0
3 9 9 250.33 2.16 180.0
4 9 9 17.98 0.50 180.0
5 9 9 64.63 0.93 0.0
6 9 9 54.46 1.02 0.0
7 9 9 66.96 1.40 0.0
8 9 9 17.39 0.79 180.0
9 9 9 322.43 3.63 0.0
10 9 9 0.48 1.08 0.0
11 9 9 2.22 1.11 0.0
12 9 9 1.27 1.21 0.0
13 9 9 11.26 1.47 180.0
14 9 9 20.56 1.41 0.0
15 9 9 2.53 1.39 180.0
16 9 9 22.45 3.51 180.0
17 9 9 3.40 2.59 0.0
-17 10 9 0.00 2.54 0.0
-16 10 9 26.89 3.98 180.0
-15 10 9 0.69 1.54 0.0
-14 10 9 8.35 1.48 0.0
-13 10 9 11.26 1.39 180.0
-12 10 9 43.39 1.80 180.0
-11 10 9 218.44 3.97 180.0
-10 10 9 6.83 1.08 180.0
-9 10 9 211.00 2.94 180.0
-8 10 9 77.12 1.37 0.0
-7 10 9 26.94 0.65 0.0
-6 10 9 0.86 0.47 0.0
-5 10 9 222.88 2.37 180.0
-4 10 9 5.39 0.60 180.0
-3 10 9 1188.23 9.60 180.0
-2 10 9 1.97 0.49 180.0
-1 10 9 449.92 4.84 0.0
0 10 9 297.86 2.76 180.0
1 10 9 88.26 1.12 180.0
2 10 9 406.52 3.83 0.0
3 10 9 43.62 0.64 0.0
4 10 9 67.74 0.87 0.0
5 10 9 136.25 1.47 0.0
6 10 9 12.35 0.66 0.0
7 10 9 172.27 2.32 0.0
8 10 9 188.03 2.61 180.0
9 10 9 4.62 0.94 180.0
10 10 9 3.79 1.11 0.0
11 10 9 1.60 1.16 180.0
12 10 9 8.75 1.28 180.0
13 10 9 2.13 1.33 180.0
14 10 9 2.39 1.37 0.0
15 10 9 31.72 3.45 0.0
16 10 9 6.65 2.56 180.0
17 10 9 8.72 2.85 180.0
-17 11 9 1.79 2.49 0.0
-16 11 9 11.01 4.21 180.0
-15 11 9 38.50 2.65 180.0
-14 11 9 24.06 1.91 0.0
-13 11 9 41.00 2.71 180.0
-12 11 9 1.50 1.41 180.0
-11 11 9 10.90 1.15 0.0
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-8 11 9 204.55 2.55 0.0
-7 11 9 309.76 2.95 0.0
-6 11 9 3.64 0.50 0.0
-5 11 9 270.73 3.04 180.0
-4 11 9 58.60 1.00 0.0
-3 11 9 168.01 1.86 0.0
-2 11 9 85.37 1.35 180.0
-1 11 9 0.35 0.78 0.0
0 11 9 60.84 1.08 0.0
1 11 9 299.81 3.21 180.0
2 11 9 231.21 2.96 0.0
3 11 9 121.46 1.39 0.0
4 11 9 0.73 0.57 180.0
5 11 9 0.00 0.61 0.0
6 11 9 187.64 2.64 180.0
7 11 9 0.84 0.88 0.0
8 11 9 92.55 1.74 0.0
9 11 9 46.86 1.58 180.0
10 11 9 1.43 1.13 180.0
11 11 9 7.73 1.30 180.0
12 11 9 29.61 1.63 0.0
13 11 9 1.83 1.41 180.0
14 11 9 2.02 1.51 0.0
15 11 9 25.27 2.60 180.0
16 11 9 10.20 2.39 180.0
-16 12 9 3.05 2.21 180.0
-15 12 9 60.25 2.97 180.0
-14 12 9 14.81 1.74 180.0
-13 12 9 38.17 1.89 0.0
-12 12 9 109.14 2.51 180.0
-11 12 9 33.04 1.72 0.0
-10 12 9 13.74 1.24 0.0
-9 12 9 1.92 1.10 0.0
-8 12 9 17.27 1.05 180.0
-7 12 9 0.00 0.74 0.0
-6 12 9 8.79 0.79 0.0
-5 12 9 32.40 0.92 180.0
-4 12 9 193.08 2.10 180.0
-3 12 9 43.26 0.98 0.0
-2 12 9 46.83 1.22 180.0
-1 12 9 163.20 2.58 180.0
0 12 9 27.22 0.82 0.0
1 12 9 10.91 0.76 180.0
2 12 9 2.23 0.66 180.0
3 12 9 249.05 3.14 0.0
4 12 9 108.95 1.74 180.0
5 12 9 19.03 0.91 180.0
6 12 9 28.80 1.02 0.0
7 12 9 4.68 0.99 180.0
8 12 9 58.17 1.57 0.0
9 12 9 20.94 1.14 180.0
10 12 9 1.58 1.13 0.0
11 12 9 32.19 1.69 0.0
12 12 9 148.56 4.51 0.0
13 12 9 2.89 1.48 0.0
14 12 9 4.69 2.25 0.0
15 12 9 21.98 2.55 0.0
16 12 9 23.15 3.00 0.0
-16 13 9 31.10 2.65 0.0
-15 13 9 1.22 1.72 0.0
-14 13 9 35.93 2.36 180.0
-13 13 9 10.95 1.49 0.0
-12 13 9 41.10 3.19 0.0
-11 13 9 100.91 3.11 180.0
-10 13 9 86.41 2.47 0.0
-9 13 9 2.12 1.03 0.0
-8 13 9 39.59 1.73 180.0
-7 13 9 3.99 0.84 180.0
-6 13 9 9.81 0.94 180.0
-5 13 9 0.00 0.76 180.0
-4 13 9 331.64 4.84 180.0
-3 13 9 36.52 1.09 180.0
-2 13 9 179.26 3.13 0.0
-1 13 9 30.46 1.36 0.0
0 13 9 39.73 1.04 0.0
1 13 9 7.44 0.90 0.0
2 13 9 144.42 2.21 180.0
3 13 9 134.09 1.98 0.0
4 13 9 28.75 1.45 0.0
5 13 9 215.77 3.07 180.0
6 13 9 117.38 2.32 180.0
7 13 9 40.01 1.34 180.0
8 13 9 0.05 1.00 180.0
9 13 9 57.43 1.66 0.0
10 13 9 1.21 1.30 180.0
11 13 9 21.98 1.59 180.0
12 13 9 36.11 2.08 0.0
13 13 9 90.08 2.76 0.0
14 13 9 12.37 2.87 0.0
15 13 9 13.70 2.33 180.0
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0 14 9 1.89 0.95 0.0
1 14 9 490.68 6.57 0.0
2 14 9 16.67 1.21 0.0
3 14 9 14.33 1.18 180.0
4 14 9 102.28 2.43 0.0
5 14 9 197.64 4.18 0.0
6 14 9 72.28 1.75 0.0
7 14 9 0.89 1.24 0.0
8 14 9 18.65 1.37 180.0
9 14 9 2.05 1.18 0.0
10 14 9 188.13 6.43 0.0
11 14 9 12.22 1.37 180.0
12 14 9 36.59 1.81 180.0
13 14 9 12.56 2.00 180.0
14 14 9 2.71 3.11 0.0
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0 15 9 21.72 1.39 180.0
1 15 9 17.15 1.27 180.0
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3 15 9 27.52 1.54 180.0
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5 15 9 148.83 3.70 180.0
6 15 9 166.46 3.27 180.0
7 15 9 1.28 1.56 0.0
8 15 9 59.72 2.34 0.0
9 15 9 19.66 1.45 180.0
10 15 9 3.36 1.35 180.0
11 15 9 20.99 1.72 0.0
12 15 9 2.46 2.25 180.0
13 15 9 17.12 2.44 0.0
14 15 9 26.10 3.02 180.0
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0 16 9 129.40 4.70 0.0
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5 16 9 208.42 6.02 0.0
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10 16 9 16.67 1.87 180.0
11 16 9 3.86 2.17 0.0
12 16 9 100.78 5.01 180.0
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0 17 9 111.10 2.53 180.0
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0 18 9 46.18 2.14 180.0
1 18 9 50.80 2.52 180.0
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5 18 9 74.33 2.51 180.0
6 18 9 32.20 2.69 0.0
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10 18 9 12.21 2.38 0.0
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1 19 9 0.51 1.36 0.0
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0 21 9 73.09 4.57 180.0
1 21 9 27.57 3.15 0.0
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0 0 10 435.22 4.21 0.0
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13 0 10 254.56 6.38 180.0
14 0 10 16.67 2.09 0.0
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0 1 10 125.93 0.94 180.0
1 1 10 2851.59 19.25 180.0
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4 1 10 458.06 3.53 180.0
5 1 10 64.34 0.71 180.0
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8 1 10 454.09 3.81 0.0
9 1 10 345.77 3.19 0.0
10 1 10 9.45 0.62 0.0
11 1 10 0.97 0.78 180.0
12 1 10 8.66 1.11 0.0
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14 1 10 60.90 2.52 0.0
15 1 10 9.44 1.45 0.0
16 1 10 22.63 3.30 0.0
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1 2 10 863.40 7.09 0.0
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10 2 10 20.31 0.79 180.0
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12 3 10 2.47 1.40 180.0
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-4 9 10 0.47 0.36 180.0
-3 9 10 224.57 2.07 0.0
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-1 9 10 274.76 3.33 0.0
0 9 10 542.50 4.58 0.0
1 9 10 201.67 1.82 0.0
2 9 10 3.59 0.28 180.0
3 9 10 113.30 1.25 0.0
4 9 10 53.72 0.73 0.0
5 9 10 246.86 2.09 180.0
6 9 10 157.24 1.96 180.0
7 9 10 127.54 1.84 180.0
8 9 10 127.59 1.76 0.0
9 9 10 18.16 1.00 180.0
10 9 10 4.06 1.08 0.0
11 9 10 133.45 2.55 180.0
12 9 10 0.85 1.16 0.0
13 9 10 42.31 1.70 0.0
14 9 10 32.89 1.48 180.0
15 9 10 26.98 2.41 180.0
16 9 10 0.00 2.40 180.0
17 9 10 7.69 2.75 0.0
-17 10 10 8.78 2.65 180.0
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-13 10 10 0.56 1.33 0.0
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-11 10 10 0.76 1.25 0.0
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-8 10 10 34.88 0.89 180.0
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-5 10 10 4.93 0.51 0.0
-4 10 10 272.98 2.55 180.0
-3 10 10 256.74 2.23 180.0
-2 10 10 1.05 0.48 0.0
-1 10 10 201.12 2.63 0.0
0 10 10 146.52 1.85 180.0
1 10 10 43.07 0.85 0.0
2 10 10 46.18 0.74 0.0
3 10 10 7.67 0.44 0.0
4 10 10 26.28 0.58 0.0
5 10 10 6.87 0.61 180.0
6 10 10 228.94 2.78 0.0
7 10 10 46.13 1.25 180.0
8 10 10 19.74 1.01 180.0
9 10 10 82.77 1.59 180.0
10 10 10 82.72 1.81 180.0
11 10 10 35.28 1.37 180.0
12 10 10 153.67 2.58 180.0
13 10 10 15.81 1.44 0.0
14 10 10 1.15 1.32 180.0
15 10 10 5.48 2.47 180.0
16 10 10 15.70 2.45 0.0
17 10 10 8.77 4.15 0.0
-17 11 10 0.00 1.97 180.0
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-13 11 10 0.00 1.48 180.0
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-11 11 10 142.01 2.43 0.0
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-9 11 10 18.50 0.96 0.0
-8 11 10 84.14 1.49 0.0
-7 11 10 120.04 1.49 180.0
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-1 11 10 1.44 0.73 180.0
0 11 10 304.60 4.33 0.0
1 11 10 354.24 3.72 0.0
2 11 10 52.72 0.93 0.0
3 11 10 327.38 2.86 180.0
4 11 10 125.08 1.48 0.0
5 11 10 9.11 0.72 0.0
6 11 10 65.56 1.38 0.0
7 11 10 57.53 1.41 180.0
8 11 10 50.77 1.30 180.0
9 11 10 6.80 1.00 0.0
10 11 10 18.49 1.30 0.0
11 11 10 88.91 2.04 0.0
12 11 10 0.34 1.36 180.0
13 11 10 18.51 2.22 180.0
14 11 10 1.00 1.51 180.0
15 11 10 55.52 3.01 180.0
16 11 10 30.12 2.96 180.0
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-13 12 10 1.89 1.53 180.0
-12 12 10 2.36 1.43 0.0
-11 12 10 105.03 2.40 0.0
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-9 12 10 283.27 3.87 180.0
-8 12 10 12.23 0.89 180.0
-7 12 10 144.22 2.01 0.0
-6 12 10 12.03 0.78 180.0
-5 12 10 23.62 0.79 0.0
-4 12 10 254.47 3.97 180.0
-3 12 10 206.49 2.62 0.0
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-1 12 10 133.06 3.02 180.0
0 12 10 5.31 0.66 0.0
1 12 10 11.37 0.79 0.0
2 12 10 224.41 3.02 0.0
3 12 10 77.45 1.41 180.0
4 12 10 132.94 1.95 0.0
5 12 10 16.16 0.89 0.0
6 12 10 100.78 1.71 0.0
7 12 10 276.13 3.47 0.0
8 12 10 43.50 1.29 0.0
9 12 10 16.43 1.14 0.0
10 12 10 33.65 1.48 0.0
11 12 10 257.46 4.39 0.0
12 12 10 3.64 1.48 0.0
13 12 10 168.02 3.18 180.0
14 12 10 30.68 2.70 180.0
15 12 10 55.74 3.03 0.0
16 12 10 41.01 3.45 0.0
-16 13 10 2.06 2.12 180.0
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-14 13 10 0.00 1.90 0.0
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-12 13 10 3.77 1.25 0.0
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-8 13 10 6.00 1.05 180.0
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-6 13 10 263.61 3.03 180.0
-5 13 10 4.47 0.77 0.0
-4 13 10 26.95 1.37 0.0
-3 13 10 7.99 0.81 180.0
-2 13 10 432.28 5.25 0.0
-1 13 10 265.50 3.55 0.0
0 13 10 30.76 1.23 0.0
1 13 10 65.94 1.68 0.0
2 13 10 301.68 3.88 0.0
3 13 10 28.42 1.23 0.0
4 13 10 28.17 1.64 180.0
5 13 10 42.65 1.38 0.0
6 13 10 213.82 3.29 180.0
7 13 10 3.69 1.02 0.0
8 13 10 17.37 1.05 180.0
9 13 10 97.21 1.91 0.0
10 13 10 50.29 1.82 180.0
11 13 10 36.51 1.77 180.0
12 13 10 18.59 1.69 180.0
13 13 10 0.00 1.89 0.0
14 13 10 14.09 4.37 0.0
15 13 10 0.71 2.28 180.0
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-10 14 10 1.83 1.53 0.0
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-7 14 10 1.39 1.16 180.0
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-5 14 10 59.98 1.92 180.0
-4 14 10 309.05 4.41 0.0
-3 14 10 42.46 1.53 0.0
-2 14 10 4.11 1.08 180.0
-1 14 10 7.15 0.94 180.0
0 14 10 78.91 2.01 180.0
1 14 10 89.19 2.04 180.0
2 14 10 18.15 1.23 0.0
3 14 10 113.09 3.47 180.0
4 14 10 992.97 13.50 180.0
5 14 10 22.97 1.57 0.0
6 14 10 110.21 2.15 0.0
7 14 10 47.69 2.06 0.0
8 14 10 29.86 1.40 180.0
9 14 10 8.07 1.24 0.0
10 14 10 10.15 1.46 0.0
11 14 10 13.06 1.52 180.0
12 14 10 0.23 1.35 0.0
13 14 10 3.33 2.45 180.0
14 14 10 2.39 2.71 0.0
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-10 15 10 0.00 1.55 180.0
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-4 15 10 7.00 1.24 0.0
-3 15 10 56.96 1.75 0.0
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-1 15 10 23.11 1.05 180.0
0 15 10 254.50 4.23 0.0
1 15 10 48.10 1.62 180.0
2 15 10 31.87 1.43 180.0
3 15 10 40.61 1.50 0.0
4 15 10 27.97 1.82 180.0
5 15 10 17.33 1.38 180.0
6 15 10 0.23 1.32 180.0
7 15 10 10.21 1.98 180.0
8 15 10 10.92 1.44 180.0
9 15 10 28.39 1.56 180.0
10 15 10 7.82 1.41 180.0
11 15 10 19.42 1.57 180.0
12 15 10 50.12 4.20 0.0
13 15 10 61.24 3.43 0.0
14 15 10 5.96 4.00 0.0
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-8 16 10 191.70 3.40 180.0
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-1 16 10 1.11 1.26 180.0
0 16 10 112.81 2.84 0.0
1 16 10 155.18 5.67 0.0
2 16 10 555.92 7.65 180.0
3 16 10 37.63 2.00 0.0
4 16 10 176.53 3.77 0.0
5 16 10 148.63 3.78 0.0
6 16 10 27.99 1.92 0.0
7 16 10 0.59 1.61 0.0
8 16 10 10.13 1.66 0.0
9 16 10 1.61 1.59 0.0
10 16 10 109.52 3.00 0.0
11 16 10 4.84 2.43 180.0
12 16 10 22.93 2.47 180.0
13 16 10 18.18 6.75 180.0
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-11 17 10 6.82 2.96 180.0
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-9 17 10 3.50 1.69 0.0
-8 17 10 1.27 1.77 180.0
-7 17 10 22.51 1.95 180.0
-6 17 10 73.10 3.83 0.0
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-3 17 10 11.50 1.32 180.0
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-1 17 10 236.15 3.86 0.0
0 17 10 107.28 2.50 180.0
1 17 10 0.00 1.81 0.0
2 17 10 2.68 1.51 180.0
3 17 10 72.19 2.17 0.0
4 17 10 393.84 6.39 0.0
5 17 10 8.16 1.61 180.0
6 17 10 3.08 2.53 180.0
7 17 10 0.16 1.66 180.0
8 17 10 27.04 1.94 0.0
9 17 10 51.45 2.45 180.0
10 17 10 23.33 2.43 180.0
11 17 10 3.31 2.17 180.0
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-8 18 10 36.39 2.51 180.0
-7 18 10 49.63 2.33 180.0
-6 18 10 20.77 1.90 0.0
-5 18 10 283.07 4.85 0.0
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-2 18 10 39.40 2.09 180.0
-1 18 10 23.84 2.28 0.0
0 18 10 3.84 1.68 0.0
1 18 10 0.27 1.74 180.0
2 18 10 56.49 2.87 0.0
3 18 10 17.77 2.83 180.0
4 18 10 53.86 2.90 0.0
5 18 10 28.23 2.14 0.0
6 18 10 4.25 1.75 180.0
7 18 10 12.31 1.80 180.0
8 18 10 9.65 2.29 0.0
9 18 10 94.42 8.31 0.0
10 18 10 36.69 3.73 0.0
11 18 10 0.00 2.84 180.0
-11 19 10 3.48 4.02 0.0
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-8 19 10 3.26 2.34 180.0
-7 19 10 2.64 2.34 180.0
-6 19 10 73.06 3.33 0.0
-5 19 10 10.42 1.88 0.0
-4 19 10 113.42 2.64 180.0
-3 19 10 126.51 2.95 180.0
-2 19 10 54.18 2.11 180.0
-1 19 10 14.24 1.65 0.0
0 19 10 11.98 1.66 180.0
1 19 10 18.99 1.54 180.0
2 19 10 12.56 1.84 0.0
3 19 10 21.80 3.19 0.0
4 19 10 21.42 2.64 180.0
5 19 10 1.57 2.21 180.0
6 19 10 5.73 3.80 180.0
7 19 10 28.08 4.06 0.0
8 19 10 66.88 3.20 0.0
9 19 10 4.19 2.93 180.0
10 19 10 27.31 3.18 180.0
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-5 20 10 27.19 3.58 180.0
-4 20 10 1.52 4.40 180.0
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-1 20 10 13.60 1.78 180.0
0 20 10 20.20 1.70 0.0
1 20 10 16.69 2.39 180.0
2 20 10 0.62 1.53 180.0
3 20 10 17.88 3.32 180.0
4 20 10 17.91 3.38 180.0
5 20 10 8.97 3.09 0.0
6 20 10 100.53 6.55 0.0
7 20 10 15.31 3.12 0.0
8 20 10 4.98 2.21 0.0
9 20 10 0.00 4.24 0.0
-8 21 10 17.02 4.82 180.0
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-5 21 10 0.00 4.40 0.0
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-1 21 10 13.18 3.31 180.0
0 21 10 12.96 4.77 0.0
1 21 10 8.30 3.93 180.0
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4 21 10 0.82 3.23 0.0
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6 21 10 0.00 4.18 0.0
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0 22 10 4.05 2.95 0.0
1 22 10 78.80 6.56 0.0
2 22 10 5.82 3.26 180.0
3 22 10 0.00 3.17 180.0
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-5 1 11 910.97 8.58 180.0
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0 1 11 350.61 2.79 0.0
1 1 11 55.01 0.66 0.0
2 1 11 8.27 0.22 0.0
3 1 11 133.18 1.18 0.0
4 1 11 9.20 0.30 0.0
5 1 11 209.77 1.83 180.0
6 1 11 104.10 1.21 180.0
7 1 11 65.80 0.85 0.0
8 1 11 265.96 2.36 0.0
9 1 11 13.07 0.58 0.0
10 1 11 4.87 0.62 180.0
11 1 11 19.07 1.09 0.0
12 1 11 42.41 1.49 0.0
13 1 11 3.76 1.30 0.0
14 1 11 7.30 1.52 180.0
15 1 11 32.88 2.20 0.0
16 1 11 4.70 1.91 0.0
17 1 11 55.84 3.66 0.0
18 1 11 0.00 1.98 0.0
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-15 2 11 19.82 1.48 180.0
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-13 2 11 6.56 1.36 180.0
-12 2 11 21.40 1.12 0.0
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-10 2 11 223.79 2.75 0.0
-9 2 11 66.58 1.27 180.0
-8 2 11 1.49 0.45 0.0
-7 2 11 151.25 2.26 180.0
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-5 2 11 18.49 0.43 0.0
-4 2 11 30.20 0.72 180.0
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-2 2 11 71.32 0.83 0.0
-1 2 11 298.15 1.72 180.0
0 2 11 135.54 1.09 0.0
1 2 11 625.50 4.54 180.0
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3 2 11 2839.97 23.88 180.0
4 2 11 84.12 0.96 180.0
5 2 11 491.92 3.86 0.0
6 2 11 15.64 0.68 180.0
7 2 11 47.72 0.73 180.0
8 2 11 43.89 0.84 180.0
9 2 11 234.46 2.81 0.0
10 2 11 4.53 0.67 180.0
11 2 11 9.19 0.99 180.0
12 2 11 41.68 1.67 180.0
13 2 11 41.82 2.14 0.0
14 2 11 20.43 1.74 180.0
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-8 3 11 148.01 1.60 180.0
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-1 3 11 6.14 0.18 0.0
0 3 11 6102.88 45.06 180.0
1 3 11 3503.22 27.75 180.0
2 3 11 57.78 0.68 180.0
3 3 11 964.17 7.43 0.0
4 3 11 465.99 4.31 180.0
5 3 11 2852.39 22.33 180.0
6 3 11 1123.18 9.59 180.0
7 3 11 11.61 0.48 180.0
8 3 11 275.57 3.21 0.0
9 3 11 171.40 2.17 180.0
10 3 11 48.19 1.11 180.0
11 3 11 1.46 1.11 180.0
12 3 11 331.59 6.09 0.0
13 3 11 259.31 6.58 0.0
14 3 11 1.56 1.33 180.0
15 3 11 59.15 1.97 180.0
16 3 11 60.67 2.08 0.0
17 3 11 43.96 5.30 0.0
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-13 4 11 12.22 1.46 0.0
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-1 4 11 960.93 6.41 0.0
0 4 11 1377.72 11.22 180.0
1 4 11 50.57 0.63 0.0
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3 4 11 97.68 0.90 180.0
4 4 11 12.45 0.43 0.0
5 4 11 255.09 2.59 180.0
6 4 11 97.63 1.28 0.0
7 4 11 153.62 1.70 180.0
8 4 11 262.10 3.29 0.0
9 4 11 29.90 0.98 0.0
10 4 11 29.67 1.24 180.0
11 4 11 16.89 1.40 180.0
12 4 11 24.06 1.55 180.0
13 4 11 20.34 1.45 0.0
14 4 11 42.15 2.45 0.0
15 4 11 23.89 1.77 180.0
16 4 11 7.11 1.84 180.0
17 4 11 29.07 3.16 0.0
18 4 11 72.01 5.90 0.0
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-5 5 11 39.36 0.51 0.0
-4 5 11 22.73 0.55 180.0
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-2 5 11 2.75 0.18 0.0
-1 5 11 355.09 2.31 0.0
0 5 11 0.59 0.25 180.0
1 5 11 718.27 8.85 180.0
2 5 11 211.55 2.30 0.0
3 5 11 153.69 1.45 0.0
4 5 11 4.43 0.41 180.0
5 5 11 2.83 0.43 0.0
6 5 11 86.81 2.36 0.0
7 5 11 232.45 2.42 0.0
8 5 11 112.38 1.36 180.0
9 5 11 236.14 3.67 0.0
10 5 11 14.98 0.97 180.0
11 5 11 2.21 1.89 0.0
12 5 11 34.98 1.67 0.0
13 5 11 4.98 1.53 0.0
14 5 11 6.94 1.50 0.0
15 5 11 0.00 1.98 180.0
16 5 11 5.30 1.90 0.0
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-15 6 11 0.56 2.36 0.0
-14 6 11 8.78 2.07 0.0
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0 6 11 36.10 0.47 0.0
1 6 11 17.89 0.54 0.0
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5 6 11 129.25 1.55 180.0
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11 6 11 211.02 3.83 180.0
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15 6 11 6.17 1.89 180.0
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1 7 11 295.54 2.80 0.0
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10 7 11 1.21 0.98 180.0
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12 7 11 144.81 3.69 180.0
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10 8 11 0.03 1.03 180.0
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10 9 11 189.27 3.20 0.0
11 9 11 32.18 1.34 180.0
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16 9 11 33.49 3.52 180.0
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0 12 11 166.53 2.71 180.0
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1 13 11 3.72 1.01 180.0
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6 15 13 68.09 2.14 0.0
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10 15 13 36.52 1.90 0.0
11 15 13 16.95 5.69 180.0
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0 16 13 0.66 1.17 180.0
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10 16 13 25.58 2.55 180.0
11 16 13 29.15 2.50 0.0
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10 3 14 2.65 0.69 180.0
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10 8 15 18.88 1.11 0.0
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12 8 15 65.19 1.85 180.0
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14 8 15 7.94 1.74 0.0
15 8 15 1.92 4.20 180.0
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0 13 20 30.05 1.16 180.0
1 13 20 79.53 2.54 180.0
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3 13 20 98.90 2.71 0.0
4 13 20 34.96 1.72 180.0
5 13 20 254.00 4.02 180.0
6 13 20 2.40 1.28 180.0
7 13 20 48.50 1.68 180.0
8 13 20 9.88 1.31 180.0
9 13 20 0.20 1.42 0.0
10 13 20 78.85 2.15 180.0
11 13 20 86.26 3.45 180.0
12 13 20 2.29 2.79 0.0
13 13 20 9.13 2.84 0.0
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0 14 20 17.80 1.16 0.0
1 14 20 32.60 1.37 180.0
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0 15 20 2.21 1.28 0.0
1 15 20 19.76 1.39 180.0
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10 15 20 6.24 2.67 180.0
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0 18 20 6.14 2.03 180.0
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1 19 20 13.32 3.45 180.0
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1 1 21 262.56 1.86 0.0
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10 1 21 4.38 0.99 0.0
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0 2 21 71.56 0.89 180.0
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0 3 21 188.25 1.25 180.0
1 3 21 563.15 3.55 180.0
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3 3 21 380.06 2.45 0.0
4 3 21 2.48 0.34 180.0
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10 3 21 56.64 1.35 180.0
11 3 21 171.10 2.57 180.0
12 3 21 65.01 2.34 0.0
13 3 21 23.36 1.58 0.0
14 3 21 6.70 1.59 180.0
15 3 21 10.02 2.65 180.0
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0 4 21 105.20 0.90 0.0
1 4 21 0.56 0.38 180.0
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10 4 21 108.47 2.03 0.0
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12 4 21 23.70 1.56 0.0
13 4 21 16.81 1.51 0.0
14 4 21 47.15 2.01 180.0
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1 5 21 216.98 1.75 0.0
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5 5 21 418.08 3.76 180.0
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10 5 21 16.48 1.01 180.0
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12 5 21 37.54 2.16 180.0
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1 6 21 386.56 2.88 180.0
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10 6 21 1.86 1.02 180.0
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14 6 21 9.44 3.29 0.0
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1 7 21 63.16 0.86 0.0
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14 7 21 23.14 4.60 180.0
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1 8 21 281.51 2.40 180.0
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10 8 21 0.34 1.15 180.0
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15 8 21 64.47 5.30 180.0
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10 9 21 199.80 2.67 180.0
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1 10 21 381.07 3.34 0.0
2 10 21 69.40 1.22 180.0
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11 10 21 12.62 1.28 180.0
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14 10 21 9.56 2.46 180.0
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1 11 21 26.91 1.13 180.0
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1 12 21 3.95 1.07 0.0
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1 14 28 37.76 1.56 0.0
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_cod_database_fobs_code 2021739