#------------------------------------------------------------------------------ #$Date: 2019-09-08 06:42:15 +0300 (Sun, 08 Sep 2019) $ #$Revision: 218078 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/17/2021768.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021768 _cell_angle_alpha 90.000 _cell_angle_beta 91.521 _cell_angle_gamma 90.000 _cell_length_a 17.5693 _cell_length_b 11.6121 _cell_length_c 20.6085 _exptl_crystal_F_000 1776.00 _reflns_d_resolution_high 0.7682 _cod_data_source_file jx3045x821bsup5.hkl _cod_data_source_block x821b _shelx_title ' x821b_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 316.59 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 54203.37 53893.65 1330.17 o 3 0 0 9259.92 8171.45 287.90 o 4 0 0 74355.87 75418.70 1171.23 o 5 0 0 84138.62 87890.84 1410.62 o 6 0 0 64947.00 64094.42 1025.15 o 7 0 0 46691.67 45058.82 735.11 o 8 0 0 30478.21 30875.01 746.01 o 9 0 0 49794.50 50852.64 2021.68 o 10 0 0 110.15 56.29 36.57 o 11 0 0 1080.63 1001.43 157.98 o 12 0 0 13016.43 13247.83 493.89 o 13 0 0 389.87 301.06 104.14 o 14 0 0 5754.92 6290.91 399.93 o 15 0 0 11055.79 11919.04 616.84 o 16 0 0 40.27 47.68 48.72 o 17 0 0 1649.66 1686.05 289.46 o 18 0 0 22.06 -0.21 56.99 o 19 0 0 210.26 144.98 72.18 o 20 0 0 996.47 903.58 328.89 o 21 0 0 536.71 644.83 295.94 o 22 0 0 64.89 -86.94 86.94 o 1 1 0 15917.29 11791.24 1218.79 o 2 1 0 16230.44 16276.86 269.86 o 3 1 0 7579.65 7806.52 169.87 o 4 1 0 32075.11 35089.61 399.34 o 5 1 0 3786.87 4235.40 118.15 o 6 1 0 4257.92 4524.48 135.21 o 7 1 0 14918.69 16870.93 333.55 o 8 1 0 8.04 -6.87 33.71 o 9 1 0 24585.57 25515.87 429.95 o 10 1 0 2437.35 2648.70 157.71 o 11 1 0 42.91 6.29 27.86 o 12 1 0 157.89 110.59 33.49 o 13 1 0 1283.79 1349.61 131.49 o 14 1 0 48.77 76.87 50.05 o 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148.45 226.10 71.17 o 15 4 0 1353.95 1595.89 188.45 o 16 4 0 289.85 261.27 104.43 o 17 4 0 103.14 196.61 86.34 o 18 4 0 70.03 81.20 67.09 o 19 4 0 477.25 478.62 141.13 o 20 4 0 162.09 184.28 92.59 o 21 4 0 833.82 785.77 192.26 o 1 5 0 3298.19 3202.79 171.29 o 2 5 0 2671.97 3138.04 91.35 o 3 5 0 47.66 65.76 32.46 o 4 5 0 3702.96 3686.10 222.83 o 5 5 0 1107.92 1078.13 112.03 o 6 5 0 387.20 287.73 56.32 o 7 5 0 714.24 596.13 124.62 o 8 5 0 1702.11 1691.63 155.35 o 9 5 0 857.37 778.25 156.20 o 10 5 0 1985.53 2117.21 185.78 o 11 5 0 4731.18 4566.85 296.38 o 12 5 0 35.84 41.40 57.43 o 13 5 0 800.77 923.67 191.03 o 14 5 0 605.70 761.54 165.65 o 15 5 0 567.81 737.91 195.95 o 16 5 0 401.30 491.87 136.11 o 17 5 0 1871.86 2129.30 455.63 o 18 5 0 160.25 200.89 92.90 o 19 5 0 553.87 691.83 185.31 o 20 5 0 158.94 609.68 167.63 o 21 5 0 8.94 -75.30 86.48 o 0 6 0 2884.10 3412.23 199.42 o 1 6 0 8843.83 9505.36 269.46 o 2 6 0 8498.92 9452.53 299.54 o 3 6 0 42.35 23.74 23.54 o 4 6 0 2174.11 2361.44 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