#------------------------------------------------------------------------------ #$Date: 2019-09-08 06:42:53 +0300 (Sun, 08 Sep 2019) $ #$Revision: 218079 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/17/2021769.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2021769 _cell_angle_alpha 90.000 _cell_angle_beta 110.904 _cell_angle_gamma 90.000 _cell_length_a 18.8929 _cell_length_b 12.8744 _cell_length_c 8.4047 _exptl_crystal_F_000 956.00 _reflns_d_resolution_high 0.8194 _cod_data_source_file lf3098sv0120sup2.hkl _cod_data_source_block sv0120 _shelx_title ' SV0120 in P2(1)/n: [Cu(C14H10N4)(NO3)2(HOEt)]' _shelx_refln_list_code 4 _shelx_f_calc_maximum 255.65 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10396.54 10884.76 92.77 o 4 0 0 324.10 369.26 2.89 o 6 0 0 9.42 8.33 0.96 o 8 0 0 4080.49 3838.82 23.33 o 10 0 0 8230.91 8034.66 45.15 o 12 0 0 9743.01 9725.04 18.02 o 14 0 0 1425.50 1415.87 7.92 o 16 0 0 1836.04 1843.18 13.38 o 18 0 0 1810.60 1862.31 16.39 o 20 0 0 1205.54 1252.85 7.72 o 1 1 0 3302.58 3524.63 13.69 o 2 1 0 10.70 21.71 1.49 o 3 1 0 139.13 139.30 1.51 o 4 1 0 16692.98 17256.70 31.65 o 5 1 0 1378.62 1534.32 5.61 o 6 1 0 1857.54 2001.48 8.80 o 7 1 0 2.97 8.67 0.88 o 8 1 0 4.89 10.28 1.09 o 9 1 0 311.94 298.46 3.08 o 10 1 0 255.10 311.26 2.33 o 11 1 0 71.38 85.90 1.75 o 12 1 0 109.31 136.99 1.77 o 13 1 0 1364.03 1332.72 5.61 o 14 1 0 134.20 126.63 1.51 o 15 1 0 1382.44 1317.62 6.42 o 16 1 0 157.37 149.75 2.25 o 17 1 0 66.95 67.01 1.82 o 18 1 0 276.23 269.96 2.70 o 19 1 0 2.79 4.40 0.85 o 20 1 0 265.40 260.67 3.09 o 0 2 0 3914.20 4312.45 25.35 o 1 2 0 22470.43 21753.59 59.46 o 2 2 0 28.90 35.33 0.85 o 3 2 0 628.60 658.10 10.53 o 4 2 0 6323.27 6554.94 23.43 o 5 2 0 1026.10 985.40 5.88 o 6 2 0 1943.57 2217.21 9.11 o 7 2 0 7044.53 6866.15 25.13 o 8 2 0 3671.08 3943.07 11.69 o 9 2 0 1898.02 1630.88 8.44 o 10 2 0 586.76 558.09 15.00 o 11 2 0 3230.74 3135.57 7.80 o 12 2 0 1236.18 1220.36 9.88 o 13 2 0 2754.10 2677.07 13.57 o 14 2 0 1172.26 1156.68 4.20 o 15 2 0 653.45 660.67 4.12 o 16 2 0 352.80 354.18 3.34 o 17 2 0 2.89 3.79 0.96 o 18 2 0 311.09 317.51 3.30 o 19 2 0 210.40 243.12 3.48 o 20 2 0 5.02 3.23 1.20 o 21 2 0 116.10 116.83 3.39 o 1 3 0 62.84 71.22 1.82 o 2 3 0 18889.51 19270.15 95.12 o 3 3 0 1399.00 1382.31 7.09 o 4 3 0 1397.94 1447.40 16.07 o 5 3 0 886.21 947.17 4.15 o 6 3 0 1512.36 1475.63 9.06 o 7 3 0 453.52 514.59 4.99 o 8 3 0 1222.24 1414.27 7.02 o 9 3 0 1562.56 1881.13 6.62 o 10 3 0 1676.46 1832.87 8.10 o 11 3 0 1718.16 1763.68 9.78 o 12 3 0 2855.20 2950.34 9.56 o 13 3 0 179.93 181.72 1.62 o 14 3 0 888.74 896.53 3.65 o 15 3 0 2.34 4.15 0.84 o 16 3 0 435.53 427.20 2.89 o 17 3 0 32.84 29.76 1.13 o 18 3 0 371.33 356.45 3.88 o 19 3 0 0.15 2.11 0.93 o 20 3 0 0.99 0.75 0.80 o 0 4 0 12476.79 12234.06 80.89 o 1 4 0 642.68 619.38 3.29 o 2 4 0 12403.69 12267.57 39.60 o 3 4 0 7216.22 7167.73 17.72 o 4 4 0 1365.25 1415.74 10.98 o 5 4 0 608.67 563.62 6.57 o 6 4 0 3651.61 3843.35 14.52 o 7 4 0 4746.58 5038.89 32.86 o 8 4 0 4260.83 4251.43 9.94 o 9 4 0 5099.24 5139.46 17.29 o 10 4 0 2733.83 2538.52 11.30 o 11 4 0 1531.58 1548.83 8.37 o 12 4 0 3462.47 3417.44 23.51 o 13 4 0 67.42 77.72 1.25 o 14 4 0 1.12 2.28 0.70 o 15 4 0 686.96 743.48 6.00 o 16 4 0 709.56 680.86 3.40 o 17 4 0 1409.56 1409.69 5.15 o 18 4 0 763.08 785.36 5.34 o 19 4 0 858.98 865.70 6.97 o 20 4 0 102.65 109.50 3.82 o 1 5 0 45.80 31.57 0.44 o 2 5 0 703.85 922.73 6.00 o 3 5 0 668.67 669.01 5.61 o 4 5 0 1572.80 1667.14 7.92 o 5 5 0 729.19 854.64 11.03 o 6 5 0 863.38 929.35 5.55 o 7 5 0 16.00 30.21 1.18 o 8 5 0 420.19 503.31 3.98 o 9 5 0 114.70 121.50 2.08 o 10 5 0 296.78 345.89 6.42 o 11 5 0 57.70 48.30 1.51 o 12 5 0 134.96 156.33 1.30 o 13 5 0 43.23 48.49 1.05 o 14 5 0 24.43 19.13 0.83 o 15 5 0 143.28 120.28 1.41 o 16 5 0 1261.33 1173.03 5.19 o 17 5 0 238.99 218.12 2.38 o 18 5 0 138.31 147.06 1.86 o 19 5 0 7.61 6.28 0.72 o 20 5 0 7.68 9.91 1.04 o 0 6 0 217.27 307.76 8.75 o 1 6 0 192.01 185.38 1.29 o 2 6 0 3467.13 3248.75 20.60 o 3 6 0 0.52 27.62 1.81 o 4 6 0 11514.32 11526.34 53.85 o 5 6 0 378.68 367.33 2.60 o 6 6 0 5167.68 5180.41 17.17 o 7 6 0 165.44 156.05 1.80 o 8 6 0 1630.45 1542.65 9.86 o 9 6 0 653.59 640.50 4.41 o 10 6 0 408.52 369.63 3.33 o 11 6 0 59.62 56.86 1.24 o 12 6 0 925.17 927.38 3.65 o 13 6 0 530.19 525.03 2.93 o 14 6 0 2400.18 2493.90 6.38 o 15 6 0 220.43 219.22 2.13 o 16 6 0 1603.72 1652.92 6.70 o 17 6 0 109.95 85.23 1.70 o 18 6 0 1464.16 1442.06 9.95 o 19 6 0 2.69 2.23 0.68 o 1 7 0 169.54 184.26 1.49 o 2 7 0 356.20 384.15 6.32 o 3 7 0 781.28 868.07 15.27 o 4 7 0 136.42 133.56 1.30 o 5 7 0 232.79 274.96 1.98 o 6 7 0 61.39 67.79 1.29 o 7 7 0 290.59 307.63 3.30 o 8 7 0 796.51 764.28 4.93 o 9 7 0 111.46 98.41 1.58 o 10 7 0 87.14 101.78 1.11 o 11 7 0 0.30 3.57 0.61 o 12 7 0 297.10 302.90 2.46 o 13 7 0 34.29 36.26 0.97 o 14 7 0 168.11 150.07 1.59 o 15 7 0 6.03 11.26 0.69 o 16 7 0 130.32 127.37 1.36 o 17 7 0 16.28 21.14 1.06 o 18 7 0 27.90 38.98 1.08 o 19 7 0 206.57 222.46 2.26 o 0 8 0 1929.91 2189.92 26.12 o 1 8 0 955.42 858.66 6.72 o 2 8 0 31.16 36.19 1.63 o 3 8 0 1115.50 998.72 13.48 o 4 8 0 297.52 367.47 3.55 o 5 8 0 3283.85 3264.40 13.23 o 6 8 0 4.69 6.54 1.17 o 7 8 0 1518.12 1431.79 10.92 o 8 8 0 25.69 27.24 1.33 o 9 8 0 2573.64 2615.99 7.96 o 10 8 0 119.36 147.95 1.54 o 11 8 0 243.44 266.34 2.02 o 12 8 0 451.75 449.38 2.68 o 13 8 0 1385.09 1391.62 6.15 o 14 8 0 60.05 66.64 1.19 o 15 8 0 2111.72 2063.90 7.38 o 16 8 0 17.68 12.30 0.81 o 17 8 0 635.63 602.76 3.74 o 18 8 0 173.99 166.72 1.82 o 1 9 0 4.57 8.81 2.71 o 2 9 0 279.81 296.89 3.41 o 3 9 0 167.86 166.69 3.53 o 4 9 0 6.91 19.27 2.83 o 5 9 0 477.10 518.38 6.24 o 6 9 0 56.89 72.74 1.64 o 7 9 0 266.33 276.13 2.49 o 8 9 0 283.26 310.78 2.50 o 9 9 0 3.17 5.76 1.12 o 10 9 0 42.40 46.81 1.27 o 11 9 0 267.81 244.43 2.70 o 12 9 0 832.41 799.38 4.07 o 13 9 0 15.43 16.97 0.94 o 14 9 0 1.81 1.36 0.72 o 15 9 0 14.94 20.58 0.77 o 16 9 0 30.95 23.46 0.73 o 17 9 0 68.78 66.65 1.36 o 1 10 0 3506.67 3426.80 59.98 o 2 10 0 1003.96 981.37 6.37 o 3 10 0 2958.17 2960.87 8.81 o 4 10 0 222.36 215.53 2.35 o 5 10 0 2138.04 2083.42 12.31 o 6 10 0 2467.69 2446.87 8.18 o 7 10 0 386.15 367.20 3.11 o 8 10 0 300.90 288.69 2.81 o 9 10 0 12.88 14.34 1.02 o 10 10 0 148.43 154.09 2.14 o 11 10 0 1.05 5.04 0.96 o 12 10 0 252.15 283.46 2.47 o 13 10 0 2681.69 2605.69 10.06 o 14 10 0 624.33 599.74 3.19 o 15 10 0 1025.28 1016.28 5.88 o 16 10 0 826.33 805.13 4.19 o 1 11 0 104.82 109.31 2.88 o 2 11 0 192.95 194.74 2.76 o 3 11 0 1087.28 1114.72 8.20 o 4 11 0 466.83 461.41 4.07 o 5 11 0 1533.44 1586.20 13.99 o 6 11 0 122.84 138.58 2.22 o 7 11 0 109.62 108.27 1.99 o 8 11 0 228.30 224.30 3.01 o 9 11 0 171.24 171.92 2.46 o 10 11 0 23.38 27.59 1.34 o 11 11 0 38.38 42.02 1.13 o 12 11 0 667.90 656.53 4.48 o 13 11 0 203.00 198.70 1.92 o 14 11 0 55.67 47.41 1.18 o 15 11 0 5.18 9.82 0.80 o 0 12 0 837.81 850.07 11.03 o 1 12 0 89.97 92.44 4.13 o 2 12 0 1392.82 1397.60 9.20 o 3 12 0 810.26 813.61 6.86 o 4 12 0 8.31 13.62 1.45 o 5 12 0 121.43 124.66 2.21 o 6 12 0 2834.54 2830.10 17.91 o 7 12 0 242.47 240.87 2.42 o 8 12 0 765.76 776.19 4.14 o 9 12 0 24.12 31.71 1.27 o 10 12 0 761.96 772.61 5.68 o 11 12 0 10.93 8.22 0.64 o 12 12 0 133.13 136.67 1.52 o 13 12 0 74.78 71.76 1.16 o 1 13 0 51.80 49.35 2.18 o 2 13 0 113.10 107.77 2.63 o 3 13 0 953.96 951.95 7.24 o 4 13 0 430.09 420.13 5.42 o 5 13 0 50.38 58.30 1.82 o 6 13 0 42.73 42.24 1.65 o 7 13 0 716.12 719.88 14.17 o 8 13 0 1.91 4.06 0.98 o 9 13 0 15.33 19.78 0.95 o 10 13 0 57.33 59.60 1.19 o 11 13 0 28.14 26.31 1.01 o 12 13 0 0.40 4.50 1.42 o 0 14 0 105.72 108.45 3.76 o 1 14 0 1488.15 1475.51 8.63 o 2 14 0 88.07 84.37 2.37 o 3 14 0 337.95 349.93 4.25 o 4 14 0 2.29 3.88 0.96 o 5 14 0 620.97 653.25 5.19 o 6 14 0 356.04 335.44 3.31 o 7 14 0 972.90 990.10 8.66 o 8 14 0 43.72 44.44 1.40 o 9 14 0 789.54 738.00 8.13 o 4 15 0 243.82 217.05 4.25 o 5 15 0 176.71 158.34 3.76 o -21 0 1 1715.96 1687.64 8.68 o -19 0 1 2455.33 2480.63 13.04 o -17 0 1 24.96 35.42 1.69 o -15 0 1 3082.80 3019.91 28.07 o -13 0 1 9039.80 8898.02 20.75 o -11 0 1 2001.49 1898.51 8.84 o -9 0 1 1551.90 1473.85 7.68 o -7 0 1 177.72 276.35 4.44 o -5 0 1 9229.55 8788.44 32.02 o -3 0 1 24182.78 23348.53 48.85 o -1 0 1 30405.90 30162.54 315.30 o 1 0 1 35083.24 34264.62 128.38 o 3 0 1 2184.60 2020.07 13.32 o 5 0 1 4855.51 4857.30 20.87 o 7 0 1 5166.25 4895.35 57.70 o 9 0 1 7969.62 7861.25 54.44 o 11 0 1 3138.22 2922.10 28.79 o 13 0 1 1105.18 1107.38 5.90 o 15 0 1 1086.51 1144.27 7.60 o 17 0 1 361.47 337.61 3.62 o 19 0 1 111.90 124.34 4.06 o -21 1 1 8.16 10.43 1.37 o -20 1 1 126.23 132.98 1.94 o -19 1 1 60.02 71.81 1.94 o -18 1 1 10.03 12.92 0.97 o -17 1 1 269.28 253.72 2.39 o -16 1 1 258.40 251.93 2.90 o -15 1 1 6376.87 6341.19 24.68 o -14 1 1 562.05 545.82 7.38 o -13 1 1 251.55 277.29 6.86 o -12 1 1 24.89 30.83 1.37 o -11 1 1 350.59 335.93 2.62 o -10 1 1 384.46 434.51 2.58 o -9 1 1 3.62 13.48 1.18 o -8 1 1 1462.01 1536.27 5.83 o -7 1 1 243.59 303.49 2.06 o -6 1 1 179.56 178.63 1.45 o -5 1 1 228.46 223.00 4.76 o -4 1 1 272.14 306.86 3.28 o -3 1 1 7631.81 7881.57 19.40 o -2 1 1 2730.95 2858.93 22.20 o -1 1 1 6078.25 6567.50 16.96 o 0 1 1 4827.92 4920.44 27.18 o 1 1 1 5510.48 5812.10 8.04 o 2 1 1 6131.75 6829.15 29.83 o 3 1 1 4441.94 4627.21 7.30 o 4 1 1 23.98 42.63 1.02 o 5 1 1 969.07 904.56 7.16 o 6 1 1 1094.37 1215.14 3.32 o 7 1 1 2238.99 2301.63 7.10 o 8 1 1 4.69 13.64 0.76 o 9 1 1 1446.01 1456.37 4.71 o 10 1 1 1232.82 1272.51 7.20 o 11 1 1 1859.54 1868.05 10.56 o 12 1 1 1274.86 1305.95 5.46 o 13 1 1 203.54 194.78 1.59 o 14 1 1 11.22 15.80 1.00 o 15 1 1 2621.74 2613.77 12.33 o 16 1 1 315.87 318.38 2.58 o 17 1 1 1028.42 1047.25 6.13 o 18 1 1 134.55 138.08 2.09 o 19 1 1 1097.79 1100.95 10.15 o 20 1 1 29.28 34.30 2.28 o -21 2 1 166.07 184.03 2.42 o -20 2 1 350.69 354.10 4.83 o -19 2 1 647.36 629.79 9.21 o -18 2 1 8.03 9.85 1.04 o -17 2 1 430.98 445.45 3.09 o -16 2 1 9.16 11.44 0.86 o -15 2 1 51.08 70.03 1.38 o -14 2 1 4098.69 4140.08 18.76 o -13 2 1 1520.05 1386.45 15.14 o -12 2 1 1441.64 1397.71 18.37 o -11 2 1 114.13 132.48 1.41 o -10 2 1 2684.27 2566.97 11.88 o -9 2 1 396.00 387.17 2.04 o -8 2 1 1467.70 1286.75 3.56 o -7 2 1 3439.03 3468.87 12.17 o -6 2 1 5467.66 5334.34 30.08 o -5 2 1 4622.29 4515.41 13.37 o -4 2 1 4373.00 4155.52 8.14 o -3 2 1 10609.62 10539.03 25.58 o -2 2 1 3037.93 3011.90 13.92 o -1 2 1 3315.15 3438.50 10.37 o 0 2 1 205.37 201.75 1.10 o 1 2 1 766.43 812.84 7.90 o 2 2 1 8556.81 8839.48 21.14 o 3 2 1 173.61 166.73 1.20 o 4 2 1 12716.88 12939.24 66.33 o 5 2 1 653.53 744.23 6.89 o 6 2 1 8159.53 8031.45 34.56 o 7 2 1 36.32 63.30 1.11 o 8 2 1 8474.75 8601.03 44.19 o 9 2 1 364.84 382.67 5.32 o 10 2 1 1064.32 987.74 6.18 o 11 2 1 3376.57 3366.59 14.38 o 12 2 1 988.09 994.68 12.01 o 13 2 1 696.18 732.93 4.18 o 14 2 1 1793.45 1738.79 11.42 o 15 2 1 27.14 28.45 1.30 o 16 2 1 36.38 34.69 1.65 o 17 2 1 253.09 248.34 2.65 o 18 2 1 168.38 177.55 2.99 o 19 2 1 119.73 127.02 2.83 o 20 2 1 681.16 672.68 7.64 o -21 3 1 186.44 182.91 2.95 o -20 3 1 18.95 20.43 1.13 o -19 3 1 111.30 106.17 1.58 o -18 3 1 13.04 16.15 1.03 o -17 3 1 479.57 462.66 4.87 o -16 3 1 49.95 55.55 1.30 o -15 3 1 47.11 50.53 1.51 o -14 3 1 27.67 31.93 1.13 o -13 3 1 255.69 259.96 4.21 o -12 3 1 30.93 41.87 1.79 o -11 3 1 122.89 159.29 2.85 o -10 3 1 5.35 22.62 1.95 o -9 3 1 2611.47 2912.73 11.65 o -8 3 1 5548.05 5949.95 9.63 o -7 3 1 201.43 252.23 3.86 o -6 3 1 338.06 304.85 2.32 o -5 3 1 4084.32 4209.44 12.14 o -4 3 1 916.24 878.57 2.66 o -3 3 1 280.77 294.22 2.51 o -2 3 1 26.84 48.19 1.37 o -1 3 1 113.55 144.03 1.21 o 0 3 1 1059.72 1062.65 5.86 o 1 3 1 401.42 424.27 5.40 o 2 3 1 647.08 739.43 3.87 o 3 3 1 7.16 182.30 9.51 o 4 3 1 361.30 444.39 3.52 o 5 3 1 59.92 87.36 1.71 o 6 3 1 987.45 950.01 5.70 o 7 3 1 173.44 232.75 3.13 o 8 3 1 3730.88 3725.88 14.21 o 9 3 1 670.49 647.52 4.14 o 10 3 1 2776.51 2735.78 9.27 o 11 3 1 852.15 849.36 5.15 o 12 3 1 4299.24 4258.62 15.22 o 13 3 1 2412.79 2363.89 11.26 o 14 3 1 122.25 119.96 1.66 o 15 3 1 278.51 283.12 3.12 o 16 3 1 437.05 453.03 3.65 o 17 3 1 75.28 79.85 1.63 o 18 3 1 241.04 243.02 2.55 o 19 3 1 1.24 2.66 1.05 o 20 3 1 132.14 113.69 3.45 o -21 4 1 427.86 404.64 4.78 o -20 4 1 705.25 718.73 8.07 o -19 4 1 311.14 342.44 3.49 o -18 4 1 1529.83 1533.66 8.66 o -17 4 1 101.97 114.60 1.65 o -16 4 1 914.77 914.35 4.19 o -15 4 1 296.51 310.86 2.79 o -14 4 1 182.50 188.66 2.07 o -13 4 1 160.19 163.01 1.91 o -12 4 1 1350.42 1328.69 11.56 o -11 4 1 203.69 167.62 1.94 o -10 4 1 5115.83 5102.82 38.30 o -9 4 1 1131.58 1123.17 6.51 o -8 4 1 3989.46 3570.57 16.28 o -7 4 1 10295.40 11326.82 54.66 o -6 4 1 14610.74 14976.75 87.20 o -5 4 1 1089.97 898.04 4.42 o -4 4 1 1736.44 1660.02 7.74 o -3 4 1 13227.32 12900.80 46.66 o -2 4 1 20.34 46.19 0.63 o -1 4 1 3141.06 2988.31 12.74 o 0 4 1 1079.64 1010.16 2.31 o 1 4 1 158.76 235.92 3.61 o 2 4 1 5.37 23.07 0.87 o 3 4 1 3634.52 3572.42 26.31 o 4 4 1 4055.43 4111.14 18.59 o 5 4 1 3494.25 3608.86 20.16 o 6 4 1 5026.63 5029.38 27.27 o 7 4 1 861.71 804.83 5.26 o 8 4 1 2181.58 2108.76 15.19 o 9 4 1 1022.68 961.20 5.43 o 10 4 1 473.38 506.44 5.17 o 11 4 1 45.35 35.75 1.71 o 12 4 1 3246.10 3268.07 11.07 o 13 4 1 2515.48 2511.19 9.92 o 14 4 1 105.80 98.44 1.87 o 15 4 1 443.23 467.64 3.56 o 16 4 1 52.12 39.98 1.34 o 17 4 1 166.42 158.29 1.99 o 18 4 1 625.76 595.78 3.90 o 19 4 1 2.51 1.76 0.73 o -21 5 1 93.96 94.91 2.27 o -20 5 1 10.33 9.96 0.89 o -19 5 1 138.54 148.53 1.77 o -18 5 1 105.41 127.70 1.58 o -17 5 1 310.08 321.78 2.78 o -16 5 1 505.01 543.01 3.69 o -15 5 1 154.60 162.61 1.95 o -14 5 1 124.09 117.85 1.51 o -13 5 1 209.81 197.77 1.87 o -12 5 1 16.54 23.68 1.61 o -11 5 1 68.34 47.50 1.64 o -10 5 1 424.40 473.76 3.01 o -9 5 1 520.55 563.35 3.82 o -8 5 1 19.95 43.29 3.14 o -7 5 1 1415.98 1593.37 3.68 o -6 5 1 5418.02 5678.96 31.61 o -5 5 1 3277.54 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o 5 6 2 287.94 300.68 3.06 o 6 6 2 214.22 252.27 3.06 o 7 6 2 622.84 649.20 3.93 o 8 6 2 467.65 443.76 4.64 o 9 6 2 3.20 7.03 0.70 o 10 6 2 1349.64 1370.07 5.76 o 11 6 2 670.04 681.00 3.32 o 12 6 2 11.50 10.91 1.27 o 13 6 2 98.99 100.05 1.81 o 14 6 2 2.97 6.92 0.98 o 15 6 2 104.61 86.33 1.54 o 16 6 2 37.39 30.69 1.01 o 17 6 2 5.21 8.03 0.58 o -20 7 2 198.86 187.63 2.25 o -19 7 2 289.59 282.55 1.69 o -18 7 2 3.85 2.91 0.59 o -17 7 2 2.65 5.43 0.65 o -16 7 2 429.11 406.69 2.78 o -15 7 2 70.59 51.69 1.18 o -14 7 2 309.48 244.63 2.02 o -13 7 2 891.77 875.14 5.75 o -12 7 2 122.29 109.29 1.69 o -11 7 2 664.51 663.13 4.07 o -10 7 2 3003.29 2935.43 7.28 o -9 7 2 1695.95 1736.66 10.33 o -8 7 2 3354.43 3294.78 14.01 o -7 7 2 171.27 134.92 1.85 o -6 7 2 1309.95 1269.17 5.38 o -5 7 2 0.58 10.13 0.62 o -4 7 2 801.19 836.75 4.23 o -3 7 2 442.71 371.84 2.29 o -2 7 2 573.60 516.34 3.15 o -1 7 2 1401.93 1333.25 11.94 o 0 7 2 1955.00 1898.50 10.20 o 1 7 2 323.26 277.78 4.39 o 2 7 2 2785.67 2713.65 16.59 o 3 7 2 3274.00 3348.38 14.33 o 4 7 2 3064.74 3060.27 16.06 o 5 7 2 3332.67 3543.06 23.20 o 6 7 2 428.46 459.55 9.93 o 7 7 2 339.51 316.46 2.50 o 8 7 2 1194.73 1213.80 4.55 o 9 7 2 1212.23 1206.44 5.55 o 10 7 2 1024.44 1038.02 4.35 o 11 7 2 78.80 69.31 1.45 o 12 7 2 619.68 641.27 6.79 o 13 7 2 118.62 109.77 1.67 o 14 7 2 730.97 732.09 3.90 o 15 7 2 224.14 229.41 2.09 o 16 7 2 262.59 269.03 2.04 o 17 7 2 351.47 351.62 2.61 o -19 8 2 765.62 721.47 5.00 o -18 8 2 141.15 121.26 1.20 o -17 8 2 439.23 448.93 2.30 o -16 8 2 2.78 2.61 0.62 o -15 8 2 1010.11 985.55 4.40 o -14 8 2 1668.80 1510.06 6.29 o -13 8 2 614.04 702.20 4.73 o -12 8 2 974.66 947.81 4.21 o -11 8 2 1120.67 1135.30 3.90 o -10 8 2 76.03 77.89 1.38 o -9 8 2 444.16 431.14 2.49 o -8 8 2 196.55 188.28 2.95 o -7 8 2 752.77 706.07 4.07 o -6 8 2 221.62 201.71 2.37 o -5 8 2 577.05 567.82 3.04 o -4 8 2 45.69 44.54 1.13 o -3 8 2 3328.12 3346.52 15.91 o -2 8 2 586.46 486.32 2.72 o -1 8 2 2231.25 2161.91 8.36 o 0 8 2 355.59 322.48 2.74 o 1 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o 2 9 2 662.27 650.40 6.18 o 3 9 2 3057.23 2950.15 9.89 o 4 9 2 296.53 285.19 2.13 o 5 9 2 1327.13 1292.47 8.72 o 6 9 2 200.87 234.86 1.93 o 7 9 2 273.25 268.72 2.18 o 8 9 2 39.74 43.43 1.05 o 9 9 2 203.49 209.98 1.81 o 10 9 2 450.01 441.44 2.46 o 11 9 2 1889.99 1921.20 8.86 o 12 9 2 291.78 278.68 2.04 o 13 9 2 934.10 950.03 4.60 o 14 9 2 66.64 70.30 0.97 o 15 9 2 637.77 605.85 5.55 o -17 10 2 155.19 156.88 1.70 o -16 10 2 25.48 26.62 0.77 o -15 10 2 136.23 138.32 1.55 o -14 10 2 104.45 101.18 1.38 o -13 10 2 40.12 38.66 0.93 o -12 10 2 370.63 362.16 2.70 o -11 10 2 177.42 182.74 1.80 o -10 10 2 1057.16 1114.44 4.28 o -9 10 2 0.55 1.95 0.75 o -8 10 2 1668.24 1699.36 8.01 o -7 10 2 2950.43 3005.85 17.77 o -6 10 2 250.46 242.65 2.83 o -5 10 2 654.85 656.37 3.99 o -4 10 2 1142.64 1180.78 5.16 o -3 10 2 1.65 3.93 0.94 o -2 10 2 330.92 346.67 7.28 o -1 10 2 351.40 333.78 3.11 o 0 10 2 350.56 356.07 3.54 o 1 10 2 72.79 71.50 1.57 o 2 10 2 57.46 67.01 1.70 o 3 10 2 23.49 25.92 1.25 o 4 10 2 46.13 47.19 1.19 o 5 10 2 30.03 30.04 1.14 o 6 10 2 4.55 4.94 0.90 o 7 10 2 251.97 252.78 2.15 o 8 10 2 365.54 371.73 2.47 o 9 10 2 52.01 56.39 1.37 o 10 10 2 70.68 64.86 1.26 o 11 10 2 45.64 48.76 0.99 o 12 10 2 0.07 1.42 0.54 o 13 10 2 94.08 86.61 0.96 o 14 10 2 19.19 14.83 1.10 o -16 11 2 16.93 21.83 0.88 o -15 11 2 69.72 72.64 1.14 o -14 11 2 233.04 234.71 2.45 o -13 11 2 93.26 84.03 1.44 o -12 11 2 521.89 519.39 3.24 o -11 11 2 61.47 56.97 1.49 o -10 11 2 1376.50 1364.83 8.65 o -9 11 2 636.69 631.41 3.78 o -8 11 2 361.25 368.23 2.67 o -7 11 2 2.16 6.78 0.83 o -6 11 2 162.94 165.86 1.99 o -5 11 2 176.85 164.75 2.30 o -4 11 2 1202.46 1190.27 11.86 o -3 11 2 126.45 129.32 1.87 o -2 11 2 1550.73 1510.27 11.71 o -1 11 2 313.61 308.92 3.61 o 0 11 2 2101.71 2107.84 8.48 o 1 11 2 110.45 113.72 2.22 o 2 11 2 907.43 887.25 6.59 o 3 11 2 27.78 31.80 1.24 o 4 11 2 191.31 187.58 2.22 o 5 11 2 39.12 38.17 1.26 o 6 11 2 1026.50 1039.71 7.78 o 7 11 2 6.96 8.52 1.33 o 8 11 2 1967.13 1951.70 12.83 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334.99 4.49 o -7 13 2 401.66 398.45 3.40 o -6 13 2 582.46 577.83 6.01 o -5 13 2 432.51 432.50 7.00 o -4 13 2 384.49 382.61 5.29 o -3 13 2 289.18 296.50 4.70 o -2 13 2 12.06 12.60 1.24 o -1 13 2 595.52 626.00 4.98 o 0 13 2 77.92 86.42 1.65 o 1 13 2 187.50 210.17 3.00 o 2 13 2 284.90 253.74 2.82 o 3 13 2 206.07 185.00 2.89 o 4 13 2 970.45 917.99 16.18 o 5 13 2 339.63 310.51 3.23 o 6 13 2 102.85 102.82 1.97 o 7 13 2 213.74 219.92 2.36 o 8 13 2 258.38 270.33 3.06 o 9 13 2 201.72 200.66 2.33 o -9 14 2 15.87 16.87 2.16 o -8 14 2 120.44 117.70 3.23 o -7 14 2 3.67 5.93 1.22 o -6 14 2 30.13 28.11 1.65 o -5 14 2 347.53 342.95 4.35 o -4 14 2 82.91 76.40 2.39 o -3 14 2 389.01 395.31 4.72 o -2 14 2 195.16 200.33 3.48 o -1 14 2 285.11 268.17 3.96 o 0 14 2 244.31 216.56 2.73 o 1 14 2 206.71 195.75 2.52 o 2 14 2 10.97 11.60 0.95 o 3 14 2 628.70 611.11 5.06 o 4 14 2 487.67 496.86 3.70 o 6 14 2 6.66 8.25 1.54 o 7 14 2 204.57 195.24 3.51 o -4 15 2 44.65 40.77 2.46 o -3 15 2 701.81 685.19 7.33 o -2 15 2 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9 2.10 1.69 1.20 o 1 2 9 14.34 14.15 0.84 o 2 2 9 20.21 17.40 1.35 o -16 3 9 379.82 403.35 5.85 o -15 3 9 12.54 14.07 0.99 o -14 3 9 395.21 415.16 4.68 o -13 3 9 193.15 186.69 1.95 o -12 3 9 5.89 4.24 0.76 o -11 3 9 94.05 93.26 2.33 o -10 3 9 543.08 551.26 7.27 o -9 3 9 237.81 210.37 2.75 o -8 3 9 181.05 204.68 3.23 o -7 3 9 92.32 93.58 2.55 o -6 3 9 985.45 1024.71 6.04 o -5 3 9 3.25 3.06 0.82 o -4 3 9 769.96 754.58 7.08 o -3 3 9 6.54 5.98 0.94 o -2 3 9 409.21 397.57 3.33 o -1 3 9 25.12 25.79 1.07 o 0 3 9 163.37 182.27 2.38 o 1 3 9 88.01 87.32 1.41 o 2 3 9 619.50 615.34 3.72 o -15 4 9 0.10 0.67 0.78 o -14 4 9 318.86 294.59 2.49 o -13 4 9 96.01 94.83 2.26 o -12 4 9 284.46 270.54 3.91 o -11 4 9 84.04 76.08 1.78 o -10 4 9 27.91 23.28 1.03 o -9 4 9 41.47 44.95 1.20 o -8 4 9 41.04 42.31 1.20 o -7 4 9 30.30 34.80 1.28 o -6 4 9 115.18 109.23 1.87 o -5 4 9 8.71 9.46 0.75 o -4 4 9 24.30 23.29 0.87 o -3 4 9 6.15 5.09 0.71 o -2 4 9 121.43 120.10 1.71 o -1 4 9 2.86 14.39 1.26 o 0 4 9 46.97 38.80 2.09 o 1 4 9 86.20 87.88 2.71 o -14 5 9 74.74 80.86 1.65 o -13 5 9 476.00 487.93 5.73 o -12 5 9 361.83 370.32 2.94 o -11 5 9 80.58 92.56 1.29 o -10 5 9 104.72 113.75 1.46 o -9 5 9 397.29 403.74 2.57 o -8 5 9 45.24 48.70 1.11 o -7 5 9 511.03 521.24 4.13 o -6 5 9 20.44 23.27 0.96 o -5 5 9 166.43 178.15 1.88 o -4 5 9 32.57 24.10 1.02 o -3 5 9 136.11 144.42 2.46 o -2 5 9 97.62 96.78 1.70 o -1 5 9 224.74 230.10 2.96 o 0 5 9 69.64 64.64 2.71 o -13 6 9 2.70 5.72 1.26 o -12 6 9 54.33 54.07 1.34 o -11 6 9 14.58 18.45 1.08 o -10 6 9 53.51 58.96 0.96 o -9 6 9 3.06 4.19 0.58 o -8 6 9 249.50 230.06 3.27 o -7 6 9 33.64 28.29 0.92 o -6 6 9 6.19 5.35 0.74 o -5 6 9 5.25 6.15 0.75 o -4 6 9 36.92 37.29 0.94 o -3 6 9 30.70 28.66 0.99 o -2 6 9 16.47 17.31 1.28 o -10 7 9 46.95 46.32 1.28 o -9 7 9 136.54 143.22 1.72 o -8 7 9 97.23 106.88 2.13 o -7 7 9 142.48 134.79 1.66 o -6 7 9 49.96 59.99 1.43 o -5 7 9 17.63 22.26 1.41 o -4 7 9 1.72 2.89 1.09 o -12 0 10 338.72 324.43 4.93 o -10 0 10 4.02 3.82 1.42 o -12 1 10 37.73 46.06 2.34 o -11 1 10 11.39 14.43 1.24 o -10 1 10 50.70 55.36 2.46 o -11 2 10 0.27 1.05 1.66 o -10 2 10 9.61 12.07 1.91 o -9 2 10 106.66 96.57 3.14 o -9 3 10 506.74 486.50 5.85 o