#------------------------------------------------------------------------------
#$Date: 2019-10-05 06:59:42 +0300 (Sat, 05 Oct 2019) $
#$Revision: 219111 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/17/2021788.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2021788
loop_
_publ_author_name
'Bloomfield, Hannah R.'
'Ritch, Jamie S.'
_publ_section_title
;
A new polymorph of phenylselenium trichloride
;
_journal_coeditor_code KY3190
_journal_issue 11
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first
;
;
_journal_paper_doi 10.1107/S2053229619013019
_journal_volume 75
_journal_year 2019
_chemical_formula_iupac 'C6 H5 Cl3 Se'
_chemical_formula_moiety 'C6 H5 Cl3 Se'
_chemical_formula_sum 'C6 H5 Cl3 Se'
_chemical_formula_weight 262.41
_chemical_name_systematic
;
Phenylselenium trichloride
;
_space_group_crystal_system triclinic
_space_group_IT_number 2
_space_group_name_Hall '-P 1'
_space_group_name_H-M_alt 'P -1'
_symmetry_space_group_name_Hall '-P 1'
_symmetry_space_group_name_H-M 'P -1'
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary dual
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_cell_angle_alpha 78.332(2)
_cell_angle_beta 77.789(2)
_cell_angle_gamma 66.341(2)
_cell_formula_units_Z 4
_cell_length_a 8.6245(3)
_cell_length_b 9.5342(4)
_cell_length_c 11.7229(5)
_cell_measurement_reflns_used 8248
_cell_measurement_temperature 150(2)
_cell_measurement_theta_max 32.60
_cell_measurement_theta_min 2.61
_cell_volume 855.50(6)
_computing_cell_refinement
;
SAINT (Bruker, 2016)
;
_computing_data_collection
;
APEX3 (Bruker, 2016
;
_computing_data_reduction
;
SAINT (Bruker, 2016
;
_computing_molecular_graphics
;
OLEX2 (Dolomanov et al., 2009)
;
_computing_publication_material
;
OLEX2 (Dolomanov et al., 2009)
;
_computing_structure_refinement
;
SHELXL (Sheldrick, 2015b)
;
_computing_structure_solution
;
SHELXT (Sheldrick, 2015a)
;
_diffrn_ambient_temperature 150.0
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type 'Bruker APEXII CCD'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0374
_diffrn_reflns_av_unetI/netI 0.0410
_diffrn_reflns_limit_h_max 11
_diffrn_reflns_limit_h_min -11
_diffrn_reflns_limit_k_max 12
_diffrn_reflns_limit_k_min -12
_diffrn_reflns_limit_l_max 15
_diffrn_reflns_limit_l_min -15
_diffrn_reflns_number 15455
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 28.699
_diffrn_reflns_theta_min 2.606
_exptl_absorpt_coefficient_mu 5.244
_exptl_absorpt_correction_T_max 0.7465
_exptl_absorpt_correction_T_min 0.4564
_exptl_absorpt_correction_type numerical
_exptl_absorpt_process_details
;
(SADABS; Bruker, 2016)
;
_exptl_crystal_colour 'clear colourless'
_exptl_crystal_density_diffrn 2.037
_exptl_crystal_description prism
_exptl_crystal_F_000 504
_exptl_crystal_size_max 0.533
_exptl_crystal_size_mid 0.518
_exptl_crystal_size_min 0.345
_refine_diff_density_max 0.462
_refine_diff_density_min -0.569
_refine_ls_extinction_coef 0.0114(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method
;
SHELXL2018 (Sheldrick, 2015b)
;
_refine_ls_goodness_of_fit_ref 1.053
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 182
_refine_ls_number_reflns 4426
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.053
_refine_ls_R_factor_all 0.0484
_refine_ls_R_factor_gt 0.0292
_refine_ls_shift/su_max 0.001
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0095P)^2^+0.5686P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0466
_refine_ls_wR_factor_ref 0.0507
_reflns_number_gt 3470
_reflns_number_total 4426
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file ky3190sup1.cif
_cod_data_source_block global
_cod_database_code 2021788
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.166
_shelx_estimated_absorpt_t_max 0.265
_shelx_hkl_file
;
-1 0 0 2198.28 56.99
-1 0 0 2165.08 56.69
-2 0 0 33.30 4.20
-2 0 0 23.60 3.30
-2 0 0 31.90 3.00
-2 0 0 30.60 3.20
2 0 0 27.60 3.70
2 0 0 26.60 3.00
-3 0 0 27.80 3.70
-3 0 0 30.10 4.00
-3 0 0 27.80 3.80
-3 0 0 39.10 6.20
3 0 0 29.60 4.20
3 0 0 30.10 4.30
-4 0 0 10.10 3.70
-4 0 0 14.70 3.20
-4 0 0 21.70 5.90
-4 0 0 17.70 3.90
4 0 0 14.50 3.90
4 0 0 14.10 4.50
-5 0 0 181.08 13.70
-5 0 0 174.28 10.60
-5 0 0 194.48 10.20
-5 0 0 186.58 12.50
5 0 0 196.28 12.10
5 0 0 182.78 11.20
-6 0 0 448.46 18.80
-6 0 0 432.76 21.90
-6 0 0 439.46 18.10
6 0 0 406.96 19.70
6 0 0 412.36 19.90
-7 0 0 11.50 9.10
-7 0 0 0.90 5.40
-7 0 0 6.30 6.40
7 0 0 3.60 7.50
-8 0 0 83.79 13.90
-8 0 0 97.89 14.60
-8 0 0 64.89 13.50
8 0 0 85.49 14.40
-9 0 0 552.54 33.30
-9 0 0 541.35 27.40
-10 0 0 184.68 30.20
-10 0 0 166.88 22.90
10 0 0 178.68 21.20
-11 0 0 14.50 24.00
10 -1 0 272.67 27.80
-10 1 0 282.37 37.20
-10 1 0 270.07 27.30
9 -1 0 116.19 16.30
-9 1 0 111.39 15.90
-9 1 0 92.79 18.50
8 -1 0 2.80 8.40
-8 1 0 0.50 8.90
-8 1 0 -2.40 11.50
7 -1 0 4.90 8.60
-7 1 0 7.40 7.80
-7 1 0 19.90 7.60
-7 1 0 23.70 9.60
6 -1 0 108.99 11.60
-6 1 0 125.49 11.40
-6 1 0 123.49 11.00
5 -1 0 400.46 19.00
5 -1 0 367.66 16.90
-5 1 0 364.86 22.30
-5 1 0 389.96 17.50
-5 1 0 374.36 16.90
4 -1 0 2842.12 79.69
4 -1 0 2820.52 77.89
-4 1 0 2635.04 79.69
-4 1 0 2943.81 80.29
-4 1 0 2862.61 77.69
-4 1 0 2910.61 77.79
3 -1 0 2408.36 64.29
3 -1 0 2422.46 65.79
-3 1 0 2276.37 65.79
-3 1 0 2104.89 69.29
-3 1 0 2468.15 65.99
-3 1 0 2401.96 64.29
2 -1 0 210.28 9.70
2 -1 0 210.28 8.60
-2 1 0 219.48 9.30
-2 1 0 206.18 9.70
-2 1 0 207.58 8.80
-2 1 0 211.78 9.90
1 -1 0 71.69 4.40
1 -1 0 74.69 4.80
-1 1 0 70.79 4.90
-1 1 0 77.59 4.20
-1 1 0 70.29 4.80
-1 1 0 70.19 4.00
1 1 0 1529.25 40.20
-2 -1 0 933.51 26.60
-2 -1 0 945.71 26.40
-2 -1 0 927.41 26.20
2 1 0 967.80 26.20
2 1 0 918.71 26.60
-3 -1 0 627.34 18.40
-3 -1 0 601.84 19.60
-3 -1 0 621.14 20.20
-3 -1 0 619.64 19.60
3 1 0 645.44 20.60
3 1 0 606.94 19.30
-4 -1 0 3.20 3.40
-4 -1 0 1.00 2.60
-4 -1 0 4.50 3.20
-4 -1 0 5.00 3.40
4 1 0 4.30 3.10
-5 -1 0 640.94 23.70
-5 -1 0 666.13 24.80
-5 -1 0 630.44 21.30
-5 -1 0 641.04 22.80
5 1 0 628.44 22.90
5 1 0 637.64 24.40
-6 -1 0 564.64 22.60
-6 -1 0 571.14 20.90
-6 -1 0 567.64 24.60
-6 -1 0 575.64 25.00
6 1 0 554.34 22.60
6 1 0 560.44 23.90
-7 -1 0 59.49 10.00
-7 -1 0 45.70 11.00
-7 -1 0 49.30 8.20
7 1 0 54.69 9.80
-8 -1 0 173.98 21.10
-8 -1 0 132.19 14.20
-8 -1 0 157.48 14.10
8 1 0 166.38 15.90
-9 -1 0 73.09 15.90
9 1 0 63.39 11.70
-10 -1 0 376.86 31.20
10 1 0 347.17 24.80
-11 -1 0 239.98 32.40
11 1 0 220.48 17.80
-10 2 0 -9.60 16.70
9 -2 0 39.60 13.30
-9 2 0 68.49 14.10
-9 2 0 71.69 19.20
8 -2 0 194.98 17.70
-8 2 0 245.38 24.70
-8 2 0 226.28 18.90
7 -2 0 279.47 18.30
-7 2 0 306.77 21.50
-7 2 0 320.77 19.20
-7 2 0 293.77 21.90
6 -2 0 104.89 11.70
-6 2 0 116.19 14.20
-6 2 0 104.49 13.40
-6 2 0 92.29 12.60
5 -2 0 74.69 10.70
5 -2 0 78.29 14.20
-5 2 0 84.39 10.20
-5 2 0 88.39 10.20
-5 2 0 82.39 10.10
4 -2 0 13.10 4.80
4 -2 0 9.80 5.80
-4 2 0 8.00 6.50
-4 2 0 10.40 6.20
-4 2 0 10.70 4.80
-4 2 0 9.30 4.80
3 -2 0 3157.68 86.39
3 -2 0 3046.30 83.19
-3 2 0 3066.49 85.69
-3 2 0 3052.69 83.49
-3 2 0 3087.19 84.29
2 -2 0 4674.23 124.29
2 -2 0 4691.83 121.59
-2 2 0 4611.54 121.79
-2 2 0 4683.63 123.49
-2 2 0 4650.83 122.39
1 -2 0 1441.66 42.60
1 -2 0 1484.15 40.00
-1 2 0 1459.15 41.20
-1 2 0 1446.56 40.70
-1 2 0 1427.16 40.50
-1 2 0 1424.96 43.00
0 -2 0 290.47 11.10
0 -2 0 310.37 12.70
0 2 0 319.87 12.80
0 2 0 305.17 11.10
0 2 0 319.87 10.90
0 2 0 323.07 11.00
-1 -2 0 2289.77 62.19
-1 -2 0 2348.57 61.59
1 2 0 2343.67 60.99
1 2 0 2344.77 61.49
1 2 0 2310.27 62.29
1 2 0 2458.95 62.09
-2 -2 0 531.05 16.50
2 2 0 499.45 16.50
2 2 0 537.55 16.00
2 2 0 532.25 15.90
2 2 0 509.25 16.80
-3 -2 0 171.38 8.10
-3 -2 0 165.78 7.40
-3 -2 0 159.78 8.00
3 2 0 168.58 7.70
3 2 0 168.28 7.00
3 2 0 161.68 7.90
-4 -2 0 158.68 8.80
-4 -2 0 155.88 8.60
-4 -2 0 160.88 9.00
4 2 0 167.48 9.10
4 2 0 160.08 9.20
4 2 0 152.38 7.00
-5 -2 0 148.39 10.00
-5 -2 0 132.09 10.10
-5 -2 0 142.19 9.60
5 2 0 132.89 7.20
5 2 0 144.69 9.20
5 2 0 149.69 11.50
-6 -2 0 1802.32 55.49
-6 -2 0 1812.12 53.99
-6 -2 0 1754.72 54.29
6 2 0 1852.51 55.89
6 2 0 1806.22 53.79
-7 -2 0 4158.78 116.39
-7 -2 0 4154.98 117.19
7 2 0 4409.46 119.09
7 2 0 4178.28 116.49
-8 -2 0 979.20 36.10
-8 -2 0 848.22 36.40
8 2 0 958.50 31.10
8 2 0 889.91 34.70
-9 -2 0 3.90 11.30
9 2 0 -5.70 9.00
-10 -2 0 1.00 13.20
10 2 0 7.90 12.60
10 2 0 -13.70 7.60
-11 -2 0 21.40 16.40
11 2 0 -9.30 16.70
11 2 0 24.30 10.20
-12 -2 0 47.30 23.40
-10 3 0 8.80 21.20
9 -3 0 25.20 13.70
-9 3 0 66.79 20.20
-9 3 0 53.59 16.00
8 -3 0 38.00 11.60
-8 3 0 46.50 12.20
-8 3 0 40.40 14.70
7 -3 0 267.17 19.90
-7 3 0 251.67 20.90
-7 3 0 242.48 20.50
-7 3 0 241.88 22.50
6 -3 0 788.72 31.50
-6 3 0 815.42 34.20
-6 3 0 836.12 33.40
-6 3 0 760.92 34.30
5 -3 0 128.09 12.60
-5 3 0 129.29 12.90
-5 3 0 105.29 14.00
-5 3 0 99.99 12.40
4 -3 0 389.96 18.00
4 -3 0 425.06 22.50
-4 3 0 388.36 20.30
-4 3 0 403.26 19.90
-4 3 0 389.46 18.70
3 -3 0 1654.03 48.00
3 -3 0 1658.63 51.79
-3 3 0 1608.34 48.40
-3 3 0 1579.94 51.69
-3 3 0 1620.64 49.40
-3 3 0 1602.94 50.69
2 -3 0 581.54 20.20
2 -3 0 589.34 23.40
-2 3 0 582.34 21.10
-2 3 0 556.34 22.00
-2 3 0 555.94 21.20
1 -3 0 38.10 6.40
-1 3 0 36.90 5.70
-1 3 0 44.00 5.80
-1 3 0 39.30 7.40
-1 3 0 44.90 7.00
0 -3 0 214.58 10.00
0 -3 0 223.48 11.90
0 3 0 219.18 10.40
0 3 0 223.58 9.90
0 3 0 210.08 11.50
0 3 0 217.18 9.70
-1 -3 0 1153.68 35.00
-1 -3 0 1159.88 33.70
1 3 0 1140.59 35.10
1 3 0 1194.58 33.20
1 3 0 1225.08 34.40
1 3 0 1202.08 33.50
-2 -3 0 101.39 6.70
-2 -3 0 97.89 7.00
2 3 0 95.69 6.50
2 3 0 100.79 5.70
2 3 0 94.69 6.30
2 3 0 94.29 5.60
-3 -3 0 5232.48 135.49
3 3 0 5181.88 138.39
3 3 0 5436.56 138.89
3 3 0 5402.56 137.09
3 3 0 5248.38 136.99
-4 -3 0 2055.29 58.59
-4 -3 0 2085.59 56.39
4 3 0 2097.49 59.29
4 3 0 2140.79 57.29
4 3 0 2077.99 57.89
4 3 0 2107.59 59.79
-5 -3 0 12.70 3.90
-5 -3 0 10.10 3.60
-5 -3 0 8.90 4.00
5 3 0 14.90 4.50
5 3 0 11.90 3.20
5 3 0 9.70 3.90
-6 -3 0 10.90 4.30
-6 -3 0 9.00 4.90
-6 -3 0 -4.80 5.10
6 3 0 -0.40 5.70
6 3 0 -2.40 5.00
6 3 0 1.30 3.50
-7 -3 0 118.89 11.80
-7 -3 0 150.68 13.80
-7 -3 0 144.29 13.20
7 3 0 137.49 13.40
7 3 0 114.29 8.90
7 3 0 149.79 15.80
-8 -3 0 315.67 19.40
-8 -3 0 314.67 20.10
8 3 0 305.37 18.70
8 3 0 306.17 14.80
-9 -3 0 168.48 19.80
9 3 0 192.48 13.30
9 3 0 196.88 18.10
-10 -3 0 135.29 18.40
10 3 0 105.69 13.10
10 3 0 97.99 16.30
-11 -3 0 61.89 15.20
11 3 0 47.10 11.10
11 3 0 64.59 16.90
-12 -3 0 103.19 19.80
-9 4 0 66.29 18.70
8 -4 0 82.09 15.50
-8 4 0 61.79 18.90
7 -4 0 598.34 28.30
-7 4 0 566.54 33.00
-7 4 0 609.44 33.20
6 -4 0 113.59 13.30
-6 4 0 121.49 17.50
-6 4 0 117.49 15.30
-6 4 0 156.98 21.10
5 -4 0 119.79 14.20
-5 4 0 84.59 13.20
-5 4 0 120.29 14.20
-5 4 0 134.09 17.00
4 -4 0 16.60 6.60
-4 4 0 -2.60 5.70
-4 4 0 9.80 8.50
3 -4 0 230.78 14.10
3 -4 0 219.78 16.40
-3 4 0 234.98 13.90
-3 4 0 234.68 14.70
-3 4 0 222.98 17.30
2 -4 0 122.19 11.50
2 -4 0 121.59 9.10
-2 4 0 112.99 10.30
-2 4 0 130.39 11.80
-2 4 0 132.19 14.90
-2 4 0 119.19 10.20
1 -4 0 1136.29 39.10
-1 4 0 1125.79 41.10
-1 4 0 1125.19 36.30
-1 4 0 1140.19 36.60
0 -4 0 1381.16 43.30
0 -4 0 1528.45 47.10
0 4 0 1455.05 42.60
0 4 0 1521.75 47.80
0 4 0 1407.76 43.60
0 4 0 1476.05 43.40
-1 -4 0 25.70 4.50
-1 -4 0 32.60 4.80
1 4 0 26.90 4.60
1 4 0 36.30 5.80
1 4 0 40.80 6.80
1 4 0 21.20 4.20
-2 -4 0 35.40 5.70
2 4 0 31.90 5.20
2 4 0 29.40 4.30
2 4 0 44.20 5.90
2 4 0 32.30 4.50
-3 -4 0 452.95 18.30
-3 -4 0 510.55 18.60
3 4 0 491.25 18.00
3 4 0 499.05 19.00
3 4 0 495.85 16.00
3 4 0 477.35 17.00
-4 -4 0 3784.52 98.69
-4 -4 0 3783.62 101.79
4 4 0 3756.52 100.69
4 4 0 3795.92 102.89
4 4 0 3729.93 102.29
4 4 0 3833.72 100.59
-5 -4 0 4105.59 110.49
-5 -4 0 3932.81 106.79
5 4 0 4193.48 111.49
5 4 0 4150.78 108.59
5 4 0 4178.28 111.99
5 4 0 3906.31 108.69
-6 -4 0 99.29 9.70
-6 -4 0 118.89 8.40
6 4 0 89.09 10.10
6 4 0 99.09 12.30
6 4 0 99.59 9.90
6 4 0 108.39 9.30
-7 -4 0 148.59 10.30
-7 -4 0 115.89 14.50
7 4 0 118.39 15.30
7 4 0 121.39 12.90
-8 -4 0 176.18 13.00
-8 -4 0 202.28 17.90
8 4 0 165.88 12.20
8 4 0 131.99 15.30
-9 -4 0 168.88 15.10
9 4 0 124.89 16.10
9 4 0 117.89 11.60
10 4 0 3.20 9.90
10 4 0 -3.60 8.60
11 4 0 4.90 10.60
11 4 0 19.90 14.30
8 -5 0 -12.80 13.70
-8 5 0 -31.30 16.40
7 -5 0 12.20 11.70
-7 5 0 0.10 12.60
-7 5 0 8.50 16.00
6 -5 0 539.55 27.70
-6 5 0 508.25 29.60
-6 5 0 571.54 31.90
-6 5 0 578.44 34.50
5 -5 0 881.91 34.10
-5 5 0 964.20 36.50
-5 5 0 812.42 37.70
-5 5 0 867.41 38.50
4 -5 0 146.99 14.60
-4 5 0 156.08 19.30
-4 5 0 113.49 17.00
-4 5 0 134.19 14.00
3 -5 0 29.80 7.70
-3 5 0 39.00 7.90
-3 5 0 33.20 10.10
2 -5 0 102.89 9.30
2 -5 0 111.49 13.80
-2 5 0 78.29 9.70
-2 5 0 105.79 14.50
1 -5 0 206.78 13.00
1 -5 0 233.78 16.10
-1 5 0 218.68 19.60
-1 5 0 236.28 15.50
-1 5 0 193.68 13.10
0 -5 0 4562.54 125.59
0 -5 0 4590.34 129.89
0 5 0 4832.42 126.99
0 5 0 4777.12 124.89
0 5 0 4535.95 131.19
0 5 0 4788.42 126.19
-1 -5 0 2532.05 71.99
-1 -5 0 2489.95 68.59
1 5 0 2483.65 68.09
1 5 0 2381.16 69.29
1 5 0 2384.56 67.79
1 5 0 2325.47 71.79
-2 -5 0 167.58 11.00
-2 -5 0 171.48 9.90
2 5 0 180.48 12.80
2 5 0 158.48 9.70
2 5 0 171.38 9.70
2 5 0 150.28 10.80
-3 -5 0 285.67 13.90
-3 -5 0 276.27 14.70
3 5 0 285.07 12.60
3 5 0 280.07 13.10
3 5 0 295.37 12.90
3 5 0 285.17 14.40
-4 -5 0 742.23 26.40
4 5 0 784.62 23.60
4 5 0 723.53 24.80
4 5 0 747.03 27.40
4 5 0 750.42 26.20
-5 -5 0 349.67 16.20
5 5 0 342.37 15.90
5 5 0 345.87 16.40
5 5 0 356.36 16.60
5 5 0 353.36 18.70
-6 -5 0 1.20 4.70
-6 -5 0 -3.30 4.50
6 5 0 -0.20 7.30
6 5 0 3.40 6.30
6 5 0 0.90 4.90
6 5 0 1.60 6.10
-7 -5 0 -11.10 5.80
-7 -5 0 -2.10 5.60
7 5 0 -4.20 6.70
7 5 0 -14.30 9.60
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0 3 14 343.57 33.90
1 3 14 -2.60 17.00
1 3 14 -24.40 13.20
2 3 14 30.50 12.90
2 3 14 49.40 16.30
3 3 14 -10.60 10.10
3 3 14 -6.00 12.00
4 3 14 -3.70 9.50
4 3 14 14.10 11.00
4 3 14 3.80 13.20
5 3 14 26.40 11.40
5 3 14 7.20 11.70
5 3 14 -3.50 12.20
6 3 14 -11.50 11.50
6 3 14 4.20 12.00
-7 -3 -14 52.79 22.40
7 3 14 5.30 13.10
7 3 14 34.00 13.90
8 3 14 3.30 14.00
9 3 14 190.88 29.80
-4 4 14 110.19 53.19
-3 4 14 261.87 37.00
-2 4 14 47.90 18.30
-1 4 14 45.90 17.80
0 4 14 -13.00 18.10
1 4 14 39.90 14.10
1 4 14 29.40 19.80
2 4 14 8.20 16.70
3 4 14 28.00 13.60
3 4 14 -2.10 12.50
4 4 14 0.60 9.50
4 4 14 1.90 11.60
5 4 14 718.43 33.90
5 4 14 647.94 37.60
6 4 14 389.66 27.50
6 4 14 359.26 28.10
7 4 14 116.59 18.10
-2 5 14 9.50 17.40
-1 5 14 7.70 18.30
0 5 14 72.79 22.70
1 5 14 114.39 25.20
1 5 14 182.88 20.10
2 5 14 171.38 33.00
2 5 14 180.68 23.90
3 5 14 63.79 17.40
3 5 14 82.79 19.20
4 5 14 28.90 16.90
4 5 14 61.49 16.00
5 5 14 35.60 15.10
5 5 14 30.50 12.80
6 5 14 147.19 22.60
6 5 14 180.28 23.40
7 5 14 249.58 23.70
7 5 14 166.78 28.70
-1 6 14 43.90 20.60
0 6 14 77.79 22.70
1 6 14 24.10 19.80
2 6 14 323.17 38.70
2 6 14 352.66 24.70
3 6 14 482.65 32.80
3 6 14 520.35 41.70
4 6 14 319.97 33.60
4 6 14 294.27 28.80
5 6 14 -0.60 14.50
5 6 14 6.00 16.50
6 6 14 21.80 15.30
6 6 14 -5.80 15.50
7 6 14 17.70 17.00
7 6 14 0.90 16.30
0 7 14 98.49 45.60
1 7 14 25.40 25.50
2 7 14 8.80 25.40
3 7 14 25.40 15.40
3 7 14 17.40 24.60
4 7 14 92.19 19.10
4 7 14 80.89 22.90
5 7 14 2.50 17.00
5 7 14 -3.00 15.40
6 7 14 89.29 21.20
6 7 14 106.39 20.60
7 7 14 17.70 19.90
1 8 14 15.20 17.00
2 8 14 41.60 14.90
3 8 14 56.09 15.30
3 8 14 52.49 33.20
4 8 14 88.59 33.40
4 8 14 60.79 18.70
5 8 14 33.20 37.30
5 8 14 21.90 18.20
6 8 14 21.90 21.40
1 9 14 -18.70 21.90
2 9 14 -8.50 17.70
3 9 14 173.88 25.40
4 9 14 -3.60 15.60
5 9 14 92.29 24.60
-2 4 -15 25.90 18.40
2 3 -15 302.67 32.80
1 3 -15 43.80 18.20
0 3 -15 21.30 17.10
-1 3 -15 67.09 19.20
-2 3 -15 227.38 31.00
-2 3 -15 157.88 24.10
-3 3 -15 123.49 20.80
-4 3 -15 0.60 20.80
3 2 -15 45.80 20.10
2 2 -15 565.04 34.80
1 2 -15 572.74 33.90
0 2 -15 32.90 14.90
-1 2 -15 62.59 16.00
-2 2 -15 1.70 14.90
2 -2 15 22.10 14.80
-4 2 -15 195.08 30.70
-4 2 -15 198.48 27.50
4 -2 15 208.78 31.60
-5 2 -15 32.20 26.60
4 1 -15 113.59 20.80
3 1 -15 9.00 16.90
2 1 -15 21.50 16.00
1 1 -15 57.79 15.70
0 1 -15 172.18 20.80
-1 1 -15 9.50 13.10
1 -1 15 17.20 15.40
-2 1 -15 43.90 14.40
2 -1 15 43.60 15.30
3 -1 15 122.79 19.20
4 -1 15 394.76 29.80
-5 1 -15 132.49 25.40
5 -1 15 134.99 23.00
4 0 -15 239.88 31.60
3 0 -15 55.49 16.40
2 0 -15 22.30 14.70
1 0 -15 148.59 21.50
0 0 -15 -5.70 11.20
0 0 15 -10.90 19.10
-1 0 -15 0.70 11.70
1 0 15 1.30 15.90
-2 0 -15 19.40 11.60
2 0 15 24.90 13.60
2 0 15 -6.70 10.70
3 0 15 108.39 15.50
4 0 15 360.66 22.30
4 0 15 291.27 25.80
-5 0 -15 495.95 36.60
5 0 15 529.35 33.40
6 0 15 233.68 34.70
-1 1 15 11.10 20.30
0 -1 -15 102.39 17.10
0 1 15 28.60 21.40
-1 -1 -15 509.55 26.40
1 1 15 447.96 33.90
-2 -1 -15 729.23 31.60
2 1 15 679.73 31.20
2 1 15 689.73 37.30
3 1 15 239.18 20.90
3 1 15 247.88 25.10
3 1 15 227.68 30.30
3 1 15 265.77 24.00
4 1 15 3.10 12.50
4 1 15 13.60 14.20
4 1 15 8.30 11.00
5 1 15 1.50 11.40
5 1 15 6.30 16.00
-6 -1 -15 105.39 23.90
6 1 15 108.19 17.70
7 1 15 133.29 23.30
-2 2 15 360.16 33.80
-1 2 15 71.39 20.70
0 2 15 -22.80 19.00
1 2 15 -23.50 17.60
2 2 15 20.90 13.10
2 2 15 37.20 16.00
3 2 15 335.37 23.10
3 2 15 362.86 27.80
4 2 15 55.59 14.10
4 2 15 63.49 20.20
4 2 15 50.59 12.50
5 2 15 171.38 21.70
5 2 15 208.98 23.60
5 2 15 223.08 22.10
6 2 15 16.60 14.70
6 2 15 47.50 14.80
7 2 15 32.40 17.30
8 2 15 0.40 21.10
-3 3 15 45.10 23.90
-1 3 15 527.85 40.10
0 3 15 10.20 20.70
1 3 15 22.30 20.30
2 3 15 108.79 20.70
2 3 15 79.59 18.20
3 3 15 12.10 12.60
3 3 15 29.00 15.60
4 3 15 12.50 14.60
4 3 15 1.50 11.30
5 3 15 6.50 12.90
5 3 15 2.20 14.40
6 3 15 19.40 14.60
-3 4 15 -22.00 41.90
-2 4 15 306.47 36.80
-1 4 15 261.97 33.30
0 4 15 20.10 20.70
1 4 15 71.19 23.70
2 4 15 11.90 16.00
2 4 15 20.80 20.20
3 4 15 -9.30 14.80
3 4 15 9.90 16.70
4 4 15 211.68 27.50
4 4 15 217.48 23.10
5 4 15 257.87 24.10
5 4 15 187.38 27.60
6 4 15 29.10 15.40
6 4 15 68.39 16.90
-1 5 15 277.97 36.00
0 5 15 57.69 23.60
1 5 15 27.70 23.30
2 5 15 2.80 22.30
2 5 15 -3.30 14.70
3 5 15 8.70 18.00
3 5 15 -21.20 15.40
4 5 15 25.30 17.40
4 5 15 26.90 17.80
5 5 15 101.19 19.30
5 5 15 103.09 21.50
6 5 15 409.86 39.50
6 5 15 460.25 31.00
1 6 15 17.10 25.40
2 6 15 283.87 25.80
2 6 15 217.28 36.40
3 6 15 229.28 36.80
3 6 15 195.98 26.30
4 6 15 -12.80 17.40
4 6 15 13.30 22.40
5 6 15 152.08 27.40
5 6 15 151.78 23.70
6 6 15 66.99 21.60
2 7 15 226.98 25.10
3 7 15 47.70 16.10
4 7 15 127.69 22.30
5 7 15 55.49 21.90
6 7 15 117.59 27.20
2 8 15 280.57 28.10
3 8 15 330.27 28.70
4 8 15 131.89 22.30
5 8 15 16.80 19.40
2 9 15 -9.40 23.90
2 2 -16 182.58 39.00
1 2 -16 26.40 17.80
0 2 -16 7.90 17.90
-1 2 -16 12.30 17.90
-2 2 -16 47.20 19.20
3 -2 16 63.69 31.30
3 1 -16 86.69 22.30
2 1 -16 29.20 17.10
1 1 -16 21.00 15.60
0 1 -16 0.90 14.60
-1 1 -16 76.19 16.30
-2 1 -16 31.70 15.10
2 -1 16 16.70 17.30
3 -1 16 52.39 18.00
4 -1 16 -5.80 19.90
1 0 -16 33.80 15.30
0 0 -16 22.10 13.70
-1 0 -16 -15.30 13.30
1 0 16 -1.60 19.70
-2 0 -16 18.60 13.80
2 0 16 6.50 16.80
3 0 16 163.08 26.20
3 0 16 173.88 26.90
3 0 16 187.68 22.20
4 0 16 252.67 30.50
4 0 16 275.17 23.50
4 0 16 264.87 27.90
5 0 16 241.18 31.80
0 1 16 -34.00 23.40
1 1 16 76.69 23.60
2 1 16 56.59 18.60
3 1 16 -10.60 12.70
3 1 16 35.20 15.30
4 1 16 45.90 24.80
4 1 16 37.70 17.40
4 1 16 37.40 14.40
5 1 16 -5.00 19.10
5 1 16 -10.90 24.90
5 1 16 4.50 15.00
6 1 16 -4.30 19.40
7 1 16 28.10 38.20
-1 2 16 38.60 22.40
0 2 16 -20.00 23.20
1 2 16 2.70 21.80
2 2 16 12.90 19.10
3 2 16 21.10 13.70
3 2 16 27.30 17.00
4 2 16 158.88 27.40
4 2 16 138.39 19.50
5 2 16 209.68 32.70
5 2 16 219.38 25.40
-1 3 16 72.59 24.20
0 3 16 9.50 22.50
1 3 16 253.47 38.40
2 3 16 200.38 34.30
3 3 16 54.79 19.80
3 3 16 26.50 16.10
4 3 16 14.90 17.80
5 3 16 -18.30 14.30
5 3 16 43.50 32.10
-1 4 16 114.79 27.30
0 4 16 -7.40 23.60
1 4 16 -1.80 25.50
2 4 16 111.59 27.60
3 4 16 63.29 23.10
3 4 16 -2.40 18.10
4 4 16 20.70 19.00
4 4 16 -24.50 16.10
5 4 16 -22.10 15.20
1 5 16 0.60 31.40
2 5 16 3.30 27.80
3 5 16 -18.60 26.50
3 5 16 -21.10 16.80
5 5 16 -25.70 18.50
3 6 16 46.20 19.10
4 6 16 142.79 23.80
5 6 16 97.99 25.90
3 7 16 33.60 17.50
4 7 16 57.09 22.40
3 8 16 312.57 34.20
0 1 -17 82.39 19.20
-1 1 -17 293.47 31.70
2 0 17 163.98 31.20
3 0 17 50.69 22.60
1 1 17 5.30 26.40
2 1 17 -10.70 22.80
3 1 17 17.30 22.10
4 1 17 -27.80 18.20
0 2 17 16.40 29.10
1 2 17 -17.40 27.90
2 2 17 1.20 25.30
3 2 17 304.47 42.30
4 2 17 502.15 35.70
0 3 17 64.09 35.40
1 3 17 140.79 34.90
2 3 17 8.80 32.40
4 3 17 -5.90 18.20
4 4 17 -13.40 23.30
4 6 17 -18.50 24.70
0 0 0 0.00 0.00
_computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)'
;
_shelx_hkl_checksum 66716
_shelx_res_file
;
TITL jsr027_0m_a.res in P-1
jsr027_0m.res
created by SHELXL-2018/1 at 13:09:05 on 09-Sep-2019
REM Old TITL jsr027_0m in P-1
REM SHELXT solution in P-1
REM R1 0.087, Rweak 0.004, Alpha 0.054, Orientation as input
REM Formula found by SHELXT: C12 Cl6 Se2
CELL 0.71073 8.6245 9.5342 11.7229 78.332 77.789 66.341
ZERR 4 0.0003 0.0004 0.0005 0.002 0.002 0.002
LATT 1
SFAC C H Cl Se
UNIT 24 20 12 4
EQIV $1 1-X,1-Y,1-Z
L.S. 16 0 0
PLAN 20
SIZE 0.533 0.518 0.345
TEMP -123.15
BIND Se2 Cl1
BIND Se2 Cl3_$1
BIND Se1 Cl4_$1
BIND Se1 Cl4
BOND $H
list 4
fmap 2 53
acta
SHEL 8 0.74
REM
REM
REM
WGHT 0.009500 0.568600
EXTI 0.011401
FVAR 0.51765
SE1 4 0.468731 0.371744 0.377013 11.00000 0.01433 0.01787 =
0.01336 -0.00121 -0.00342 -0.00551
SE2 4 0.331346 0.827302 0.291232 11.00000 0.01727 0.01849 =
0.01750 0.00074 -0.00562 -0.00836
CL4 3 0.239556 0.645577 0.463264 11.00000 0.02017 0.02675 =
0.01385 -0.00281 -0.00125 -0.00996
CL1 3 0.572578 0.550871 0.213255 11.00000 0.01600 0.03201 =
0.02006 -0.00117 0.00043 -0.01049
CL3 3 0.375547 0.227398 0.532851 11.00000 0.03405 0.03539 =
0.01969 0.00925 -0.01044 -0.02086
CL2 3 0.675269 0.170967 0.307192 11.00000 0.02344 0.02348 =
0.03373 -0.00829 -0.00492 0.00284
CL5 3 0.155145 1.028793 0.374429 11.00000 0.04052 0.02155 =
0.03870 -0.01184 -0.01048 -0.00621
CL6 3 0.445197 0.963733 0.143717 11.00000 0.03135 0.03750 =
0.03654 0.01460 -0.01162 -0.02350
C1 1 0.300836 0.384034 0.283174 11.00000 0.01838 0.01602 =
0.01482 -0.00159 -0.00566 -0.00782
C7 1 0.169614 0.822201 0.199302 11.00000 0.01798 0.01393 =
0.01890 0.00022 -0.00826 -0.00429
C8 1 0.004941 0.841229 0.253902 11.00000 0.01658 0.01991 =
0.01994 -0.00283 -0.00345 -0.00302
AFIX 43
H8 2 -0.029076 0.855370 0.334641 11.00000 -1.20000
AFIX 0
C2 1 0.132856 0.414016 0.336602 11.00000 0.01986 0.02207 =
0.01324 -0.00414 -0.00092 -0.00750
AFIX 43
H2 2 0.100984 0.424952 0.417965 11.00000 -1.20000
AFIX 0
C6 1 0.351062 0.366931 0.164879 11.00000 0.01923 0.02853 =
0.01598 -0.00564 0.00120 -0.00945
AFIX 43
H6 2 0.466331 0.347356 0.129613 11.00000 -1.20000
AFIX 0
C9 1 -0.109450 0.839031 0.186951 11.00000 0.01559 0.02270 =
0.03131 -0.00115 -0.00839 -0.00486
AFIX 43
H9 2 -0.223387 0.852156 0.222208 11.00000 -1.20000
AFIX 0
C4 1 0.061327 0.409624 0.150566 11.00000 0.02789 0.02359 =
0.01983 0.00119 -0.01107 -0.01378
AFIX 43
H4 2 -0.021439 0.418381 0.104667 11.00000 -1.20000
AFIX 0
C3 1 0.012976 0.427626 0.269015 11.00000 0.01819 0.02578 =
0.02233 -0.00184 -0.00363 -0.01046
AFIX 43
H3 2 -0.102844 0.449365 0.303758 11.00000 -1.20000
AFIX 0
C12 1 0.223640 0.798383 0.082821 11.00000 0.01924 0.02769 =
0.02029 -0.00463 -0.00219 -0.00700
AFIX 43
H12 2 0.337873 0.784085 0.047616 11.00000 -1.20000
AFIX 0
C10 1 -0.058666 0.817974 0.070013 11.00000 0.02798 0.02089 =
0.03103 -0.00258 -0.01541 -0.00825
AFIX 43
H10 2 -0.138341 0.818728 0.024752 11.00000 -1.20000
AFIX 0
C5 1 0.229045 0.379063 0.099088 11.00000 0.03009 0.03335 =
0.01503 -0.00622 -0.00193 -0.01536
AFIX 43
H5 2 0.261162 0.366247 0.018056 11.00000 -1.20000
AFIX 0
C11 1 0.107547 0.795770 0.018253 11.00000 0.03387 0.03117 =
0.01955 -0.00522 -0.00738 -0.00999
AFIX 43
H11 2 0.142480 0.778644 -0.061869 11.00000 -1.20000
AFIX 0
HKLF 4
REM jsr027_0m_a.res in P-1
REM R1 = 0.0292 for 3470 Fo > 4sig(Fo) and 0.0484 for all 4426 data
REM 182 parameters refined using 0 restraints
END
WGHT 0.0095 0.5686
REM Highest difference peak 0.462, deepest hole -0.569, 1-sigma level 0.105
Q1 1 0.2247 0.9787 0.1591 11.00000 0.05 0.46
Q2 1 0.3909 0.7874 0.3786 11.00000 0.05 0.45
Q3 1 0.3632 0.8396 0.4417 11.00000 0.05 0.45
Q4 1 0.2303 0.5370 0.3960 11.00000 0.05 0.45
Q5 1 0.3775 0.3932 0.3114 11.00000 0.05 0.44
Q6 1 0.5846 0.2610 0.3420 11.00000 0.05 0.44
Q7 1 0.5464 0.2416 0.3590 11.00000 0.05 0.43
Q8 1 0.5147 0.0340 0.3712 11.00000 0.05 0.42
Q9 1 0.0874 0.8655 0.2279 11.00000 0.05 0.42
Q10 1 0.2412 0.8340 0.2408 11.00000 0.05 0.41
Q11 1 0.6187 0.1729 0.2921 11.00000 0.05 0.40
Q12 1 0.1195 1.0011 0.1338 11.00000 0.05 0.40
Q13 1 0.0936 0.7147 0.4330 11.00000 0.05 0.39
Q14 1 0.7617 0.1273 0.3788 11.00000 0.05 0.39
Q15 1 0.3063 0.5813 0.4491 11.00000 0.05 0.39
Q16 1 0.1591 0.6780 0.2147 11.00000 0.05 0.39
Q17 1 0.3804 0.2367 0.3201 11.00000 0.05 0.38
Q18 1 0.3781 0.5023 0.3160 11.00000 0.05 0.37
Q19 1 0.5484 0.3205 0.4773 11.00000 0.05 0.37
Q20 1 0.7019 0.1398 0.4820 11.00000 0.05 0.37
;
_shelx_res_checksum 76465
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
Se Se1 0.46873(3) 0.37174(3) 0.37701(2) 0.01526(7) Uani d 1
Se Se2 0.33135(3) 0.82730(3) 0.29123(2) 0.01719(7) Uani d 1
Cl Cl4 0.23956(8) 0.64558(7) 0.46326(5) 0.02005(13) Uani d 1
Cl Cl1 0.57258(8) 0.55087(8) 0.21325(5) 0.02304(14) Uani d 1
Cl Cl3 0.37555(9) 0.22740(8) 0.53285(6) 0.02807(16) Uani d 1
Cl Cl2 0.67527(8) 0.17097(8) 0.30719(6) 0.02984(16) Uani d 1
Cl Cl5 0.15514(9) 1.02879(8) 0.37443(6) 0.03339(17) Uani d 1
Cl Cl6 0.44520(9) 0.96373(8) 0.14372(6) 0.03359(17) Uani d 1
C C1 0.3008(3) 0.3840(3) 0.2832(2) 0.0155(5) Uani d 1
C C7 0.1696(3) 0.8222(3) 0.1993(2) 0.0170(5) Uani d 1
C C8 0.0049(3) 0.8412(3) 0.2539(2) 0.0199(5) Uani d 1
H H8 -0.029076 0.855370 0.334641 0.024 Uiso calc 1
C C2 0.1329(3) 0.4140(3) 0.3366(2) 0.0185(5) Uani d 1
H H2 0.100984 0.424952 0.417965 0.022 Uiso calc 1
C C6 0.3511(3) 0.3669(3) 0.1649(2) 0.0213(5) Uani d 1
H H6 0.466331 0.347356 0.129613 0.026 Uiso calc 1
C C9 -0.1095(3) 0.8390(3) 0.1870(2) 0.0235(6) Uani d 1
H H9 -0.223387 0.852156 0.222208 0.028 Uiso calc 1
C C4 0.0613(3) 0.4096(3) 0.1506(2) 0.0218(6) Uani d 1
H H4 -0.021439 0.418381 0.104667 0.026 Uiso calc 1
C C3 0.0130(3) 0.4276(3) 0.2690(2) 0.0215(6) Uani d 1
H H3 -0.102844 0.449365 0.303758 0.026 Uiso calc 1
C C12 0.2236(3) 0.7984(3) 0.0828(2) 0.0229(6) Uani d 1
H H12 0.337873 0.784085 0.047616 0.027 Uiso calc 1
C C10 -0.0587(3) 0.8180(3) 0.0700(2) 0.0253(6) Uani d 1
H H10 -0.138341 0.818728 0.024752 0.030 Uiso calc 1
C C5 0.2290(3) 0.3791(3) 0.0991(2) 0.0248(6) Uani d 1
H H5 0.261162 0.366247 0.018056 0.030 Uiso calc 1
C C11 0.1075(4) 0.7958(3) 0.0183(2) 0.0281(6) Uani d 1
H H11 0.142480 0.778644 -0.061869 0.034 Uiso calc 1
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Se1 0.01433(13) 0.01787(13) 0.01336(13) -0.00551(10) -0.00342(10) -0.00121(10)
Se2 0.01727(13) 0.01849(14) 0.01750(14) -0.00836(11) -0.00562(10) 0.00074(10)
Cl4 0.0202(3) 0.0267(3) 0.0139(3) -0.0100(3) -0.0013(2) -0.0028(2)
Cl1 0.0160(3) 0.0320(4) 0.0201(3) -0.0105(3) 0.0004(2) -0.0012(3)
Cl3 0.0340(4) 0.0354(4) 0.0197(3) -0.0209(3) -0.0104(3) 0.0092(3)
Cl2 0.0234(3) 0.0235(3) 0.0337(4) 0.0028(3) -0.0049(3) -0.0083(3)
Cl5 0.0405(4) 0.0216(3) 0.0387(4) -0.0062(3) -0.0105(3) -0.0118(3)
Cl6 0.0313(4) 0.0375(4) 0.0365(4) -0.0235(3) -0.0116(3) 0.0146(3)
C1 0.0184(12) 0.0160(12) 0.0148(12) -0.0078(10) -0.0057(10) -0.0016(10)
C7 0.0180(12) 0.0139(12) 0.0189(13) -0.0043(10) -0.0083(10) 0.0002(10)
C8 0.0166(12) 0.0199(13) 0.0199(13) -0.0030(10) -0.0034(10) -0.0028(11)
C2 0.0199(13) 0.0221(13) 0.0132(12) -0.0075(11) -0.0009(10) -0.0041(10)
C6 0.0192(13) 0.0285(14) 0.0160(13) -0.0094(11) 0.0012(10) -0.0056(11)
C9 0.0156(13) 0.0227(14) 0.0313(15) -0.0049(11) -0.0084(11) -0.0011(12)
C4 0.0279(15) 0.0236(14) 0.0198(13) -0.0138(12) -0.0111(11) 0.0012(11)
C3 0.0182(13) 0.0258(14) 0.0223(14) -0.0105(11) -0.0036(11) -0.0018(11)
C12 0.0192(13) 0.0277(14) 0.0203(13) -0.0070(11) -0.0022(11) -0.0046(11)
C10 0.0280(14) 0.0209(14) 0.0310(15) -0.0082(12) -0.0154(12) -0.0026(12)
C5 0.0301(15) 0.0333(16) 0.0150(13) -0.0154(13) -0.0019(11) -0.0062(11)
C11 0.0339(16) 0.0312(16) 0.0195(14) -0.0100(13) -0.0074(12) -0.0052(12)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_3
_geom_angle
Cl4 Se1 Cl4 2_666 90.204(17)
Cl1 Se1 Cl4 . 84.71(2)
Cl1 Se1 Cl4 2_666 89.433(18)
Cl3 Se1 Cl4 2_666 87.29(2)
Cl3 Se1 Cl4 . 91.45(2)
Cl3 Se1 Cl1 . 174.95(2)
Cl2 Se1 Cl4 2_666 83.89(2)
Cl2 Se1 Cl4 . 172.03(2)
Cl2 Se1 Cl1 . 89.87(3)
Cl2 Se1 Cl3 . 93.60(3)
C1 Se1 Cl4 . 89.59(7)
C1 Se1 Cl4 2_666 179.21(7)
C1 Se1 Cl1 . 89.78(7)
C1 Se1 Cl3 . 93.48(7)
C1 Se1 Cl2 . 96.25(7)
Cl4 Se2 Cl1 . 84.06(2)
Cl4 Se2 Cl3 2_666 81.751(18)
Cl1 Se2 Cl3 2_666 83.668(19)
Cl5 Se2 Cl4 . 90.83(3)
Cl5 Se2 Cl1 . 172.41(3)
Cl5 Se2 Cl3 2_666 90.06(2)
Cl5 Se2 Cl6 . 94.38(3)
Cl6 Se2 Cl4 . 172.72(3)
Cl6 Se2 Cl1 . 90.24(3)
Cl6 Se2 Cl3 2_666 93.14(2)
C7 Se2 Cl4 . 90.64(7)
C7 Se2 Cl1 . 89.74(7)
C7 Se2 Cl3 2_666 170.39(7)
C7 Se2 Cl5 . 95.94(7)
C7 Se2 Cl6 . 93.87(7)
Se2 Cl4 Se1 . 95.36(2)
Se1 Cl1 Se2 . 95.70(2)
C2 C1 Se1 . 118.78(17)
C6 C1 Se1 . 119.29(18)
C6 C1 C2 . 121.9(2)
C8 C7 Se2 . 118.66(18)
C12 C7 Se2 . 119.06(18)
C12 C7 C8 . 122.3(2)
C7 C8 H8 . 121.0
C7 C8 C9 . 118.0(2)
C9 C8 H8 . 121.0
C1 C2 H2 . 120.7
C3 C2 C1 . 118.7(2)
C3 C2 H2 . 120.7
C1 C6 H6 . 120.8
C1 C6 C5 . 118.4(2)
C5 C6 H6 . 120.8
C8 C9 H9 . 119.7
C10 C9 C8 . 120.5(2)
C10 C9 H9 . 119.7
C3 C4 H4 . 119.8
C5 C4 H4 . 119.8
C5 C4 C3 . 120.3(2)
C2 C3 C4 . 120.2(2)
C2 C3 H3 . 119.9
C4 C3 H3 . 119.9
C7 C12 H12 . 120.7
C7 C12 C11 . 118.6(2)
C11 C12 H12 . 120.7
C9 C10 H10 . 119.8
C9 C10 C11 . 120.3(2)
C11 C10 H10 . 119.8
C6 C5 H5 . 119.8
C4 C5 C6 . 120.5(2)
C4 C5 H5 . 119.8
C12 C11 H11 . 119.9
C10 C11 C12 . 120.3(2)
C10 C11 H11 . 119.9
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Se1 Cl4 2_666 3.3760(6)
Se1 Cl4 . 2.7975(7)
Se1 Cl1 . 2.5648(7)
Se1 Cl3 . 2.2643(7)
Se1 Cl2 . 2.1881(7)
Se1 C1 . 1.951(2)
Se2 Cl4 . 2.5900(6)
Se2 Cl1 . 2.8070(7)
Se2 Cl3 2_666 3.4099(7)
Se2 Cl5 . 2.1769(7)
Se2 Cl6 . 2.2458(7)
Se2 C7 . 1.955(2)
C1 C2 . 1.389(3)
C1 C6 . 1.385(3)
C7 C8 . 1.384(3)
C7 C12 . 1.380(3)
C8 H8 . 0.9500
C8 C9 . 1.393(3)
C2 H2 . 0.9500
C2 C3 . 1.382(3)
C6 H6 . 0.9500
C6 C5 . 1.388(3)
C9 H9 . 0.9500
C9 C10 . 1.378(4)
C4 H4 . 0.9500
C4 C3 . 1.388(3)
C4 C5 . 1.380(4)
C3 H3 . 0.9500
C12 H12 . 0.9500
C12 C11 . 1.387(3)
C10 H10 . 0.9500
C10 C11 . 1.381(4)
C5 H5 . 0.9500
C11 H11 . 0.9500