#------------------------------------------------------------------------------ #$Date: 2020-11-06 07:08:33 +0200 (Fri, 06 Nov 2020) $ #$Revision: 258773 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/22/2022270.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022270 _cell_angle_alpha 90.000 _cell_angle_beta 91.185 _cell_angle_gamma 90.000 _cell_length_a 3.9652 _cell_length_b 16.7005 _cell_length_c 12.4252 _exptl_crystal_F_000 376.00 _reflns_d_resolution_high 0.8087 _cod_data_source_file ky3199Isup2.hkl _cod_data_source_block I _shelx_title ' shelxt_a.res in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.86 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 -16 0 358.42 327.67 4.54 o 3 -16 0 573.45 416.41 4.22 o 1 -15 0 681.91 613.94 13.15 o 2 -15 0 92.34 91.07 1.61 o 3 -15 0 171.30 159.04 3.29 o 1 -14 0 859.46 815.87 25.83 o 2 -14 0 152.05 152.62 2.28 o 3 -14 0 38.80 36.07 1.46 o 1 -13 0 25.32 22.11 1.84 o 2 -13 0 80.31 81.33 1.95 o 3 -13 0 224.17 209.44 13.03 o 1 -12 0 74.16 76.96 4.20 o 2 -12 0 188.07 181.38 3.33 o 3 -12 0 324.75 305.28 3.48 o 1 -11 0 744.93 677.12 17.20 o 2 -11 0 77.16 77.73 1.94 o 3 -11 0 86.28 83.80 1.77 o 4 -11 0 22.99 25.40 0.68 o 0 -10 0 873.84 815.43 11.03 o 1 -10 0 92.79 94.33 3.29 o 2 -10 0 559.60 570.55 6.42 o 3 -10 0 100.46 92.96 1.93 o 4 -10 0 155.17 156.22 1.59 o 1 -9 0 155.80 142.38 2.63 o 2 -9 0 399.68 385.90 5.20 o 3 -9 0 31.01 32.56 1.23 o 4 -9 0 197.27 199.92 1.94 o 0 -8 0 3236.63 3236.81 20.34 o 1 -8 0 165.50 170.49 1.66 o 2 -8 0 326.44 304.19 6.10 o 3 -8 0 149.54 141.10 2.87 o 4 -8 0 17.48 17.32 0.70 o 1 -7 0 1114.79 1099.36 15.00 o 2 -7 0 52.65 51.48 1.36 o 3 -7 0 9.66 9.58 0.49 o 4 -7 0 31.12 29.43 0.69 o 0 -6 0 194.82 222.50 43.40 o 1 -6 0 22.92 16.94 0.72 o 2 -6 0 571.87 578.58 22.32 o 3 -6 0 50.20 50.23 1.11 o 4 -6 0 96.95 98.15 1.97 o 1 -5 0 1682.50 1562.64 9.26 o 2 -5 0 608.87 590.21 3.47 o 3 -5 0 229.26 216.05 2.79 o 4 -5 0 124.29 121.64 3.02 o 1 -4 0 471.79 431.05 4.35 o 2 -4 0 956.75 917.48 6.98 o 3 -4 0 256.61 254.06 2.09 o 4 -4 0 6.62 7.24 0.69 o 1 -3 0 1586.81 1524.07 8.51 o 2 -3 0 778.90 812.04 17.51 o 3 -3 0 213.86 223.74 1.82 o 4 -3 0 15.59 14.86 0.51 o 1 -2 0 87.98 79.18 1.23 o 2 -2 0 855.63 879.32 11.13 o 3 -2 0 207.42 220.69 1.60 o 4 -2 0 81.04 85.35 1.47 o 1 -1 0 22.24 24.18 0.73 o 2 -1 0 1000.81 941.65 6.67 o 3 -1 0 451.06 437.94 4.23 o 4 -1 0 120.08 121.28 3.81 o 1 0 0 569.75 579.65 7.82 o 2 0 0 632.70 554.06 2.98 o 3 0 0 380.02 367.33 3.03 o 4 0 0 85.17 80.46 2.67 o 1 1 0 37.93 43.28 0.79 o 2 1 0 1015.79 961.01 10.32 o 3 1 0 437.23 426.44 4.39 o 4 1 0 125.99 132.84 2.39 o 0 2 0 1264.51 1324.13 11.95 o 1 2 0 75.75 69.46 1.08 o 2 2 0 783.42 808.01 7.69 o 3 2 0 184.91 194.68 1.34 o 4 2 0 101.34 103.25 1.93 o 1 3 0 1598.79 1630.01 25.98 o 2 3 0 723.78 738.65 17.35 o 3 3 0 200.63 208.66 1.50 o 4 3 0 12.61 11.01 0.52 o 0 4 0 1921.75 2260.91 21.09 o 1 4 0 502.62 522.24 6.99 o 2 4 0 875.37 839.95 11.94 o 3 4 0 224.28 223.32 1.86 o 4 4 0 10.61 9.98 0.59 o 1 5 0 1738.70 1778.38 13.97 o 2 5 0 671.46 677.32 3.78 o 3 5 0 210.16 204.34 1.56 o 4 5 0 153.92 146.93 2.04 o 0 6 0 304.79 341.27 14.75 o 1 6 0 27.58 21.45 0.93 o 2 6 0 581.51 599.56 5.64 o 3 6 0 55.41 56.27 1.32 o 4 6 0 106.84 113.40 1.79 o 1 7 0 1167.95 1140.77 7.48 o 2 7 0 38.08 36.03 0.65 o 3 7 0 9.27 9.12 0.54 o 4 7 0 41.09 41.39 1.09 o 0 8 0 3291.09 3761.81 52.36 o 1 8 0 164.08 203.56 6.65 o 2 8 0 328.26 329.27 5.04 o 3 8 0 169.35 164.60 3.99 o 4 8 0 23.50 20.21 3.32 o 1 9 0 204.07 225.25 5.14 o 2 9 0 417.07 413.87 4.71 o 3 9 0 19.53 20.97 0.65 o 4 9 0 182.36 192.15 2.57 o 0 10 0 992.09 951.56 62.22 o 1 10 0 86.55 96.41 1.19 o 2 10 0 593.78 607.45 4.19 o 3 10 0 128.82 123.41 1.89 o 4 10 0 144.63 130.88 77.00 o 1 11 0 746.76 754.33 5.73 o 2 11 0 98.30 94.20 5.10 o 3 11 0 102.05 100.67 1.38 o 4 11 0 17.46 19.01 3.49 o 0 12 0 207.77 215.63 2.00 o 1 12 0 80.95 85.44 0.70 o 2 12 0 170.12 173.33 2.08 o 3 12 0 312.04 298.74 5.65 o 1 13 0 31.51 30.38 0.46 o 2 13 0 73.20 81.60 0.93 o 3 13 0 237.06 246.94 3.40 o 0 14 0 1903.94 1924.85 7.66 o 1 14 0 885.93 918.33 7.33 o 2 14 0 199.05 211.15 1.72 o 3 14 0 25.43 26.12 0.65 o 1 15 0 584.56 599.03 4.91 o 2 15 0 63.61 69.26 0.97 o 3 15 0 172.46 174.56 3.13 o 0 16 0 112.32 107.18 1.63 o 1 16 0 67.08 68.14 0.86 o 2 16 0 293.17 297.68 5.49 o 3 16 0 560.09 587.27 23.99 o 1 17 0 26.65 28.85 0.71 o 2 17 0 3.03 2.69 0.26 o 0 18 0 6.42 6.99 0.75 o 1 18 0 57.55 61.42 1.72 o 2 18 0 227.22 243.30 2.95 o 1 19 0 29.30 30.58 1.03 o 1 20 0 24.05 24.63 1.26 o -3 -16 1 239.02 200.99 2.45 o -2 -16 1 166.98 156.74 3.01 o 2 -16 1 466.02 438.31 5.54 o 3 -16 1 104.98 81.19 1.50 o -3 -15 1 74.46 68.56 1.33 o -2 -15 1 179.99 175.79 3.33 o 1 -15 1 696.26 675.52 14.23 o 2 -15 1 827.82 775.95 8.54 o 3 -15 1 208.94 204.83 2.26 o -3 -14 1 177.44 171.25 2.31 o -2 -14 1 422.98 400.10 5.85 o -1 -14 1 663.20 693.98 14.12 o 1 -14 1 90.76 78.06 3.22 o 2 -14 1 462.99 394.84 3.88 o 3 -14 1 34.12 29.74 0.68 o -3 -13 1 4.39 3.73 0.31 o -2 -13 1 360.63 336.12 17.63 o -1 -13 1 107.47 101.68 3.54 o 1 -13 1 0.15 1.73 1.03 o 2 -13 1 19.79 20.26 0.91 o 3 -13 1 31.16 27.91 0.92 o -3 -12 1 18.39 17.93 0.63 o -2 -12 1 6.78 7.72 0.87 o -1 -12 1 296.19 299.55 6.02 o 0 -12 1 199.77 183.50 5.44 o 1 -12 1 155.30 145.08 6.44 o 2 -12 1 19.87 18.74 0.74 o 3 -12 1 47.58 44.30 1.62 o -4 -11 1 104.54 97.35 1.64 o -3 -11 1 10.44 10.51 0.53 o -2 -11 1 517.45 506.45 6.19 o -1 -11 1 1142.68 1093.64 17.96 o 0 -11 1 11.92 12.45 0.98 o 1 -11 1 1318.40 1253.07 15.86 o 2 -11 1 139.69 130.92 2.71 o 3 -11 1 75.47 68.40 2.80 o 4 -11 1 215.71 212.13 2.18 o -4 -10 1 52.96 48.25 1.27 o -3 -10 1 243.04 248.57 3.31 o -2 -10 1 639.19 622.17 7.99 o -1 -10 1 35.63 36.52 1.01 o 0 -10 1 1366.66 1257.15 13.87 o 1 -10 1 561.91 501.02 18.34 o 2 -10 1 615.09 607.08 10.25 o 3 -10 1 804.83 775.16 8.36 o 4 -10 1 27.07 27.43 0.87 o -4 -9 1 6.39 6.39 0.28 o -3 -9 1 253.96 240.45 6.24 o -2 -9 1 30.92 32.99 1.51 o -1 -9 1 478.51 421.53 4.84 o 0 -9 1 487.29 498.45 5.23 o 1 -9 1 1212.21 1106.85 11.72 o 2 -9 1 33.89 35.31 1.24 o 3 -9 1 164.12 163.45 4.26 o 4 -9 1 161.24 163.74 2.06 o -4 -8 1 88.01 90.12 1.18 o -3 -8 1 149.48 156.19 2.98 o -2 -8 1 245.43 259.67 4.67 o -1 -8 1 256.05 259.20 4.11 o 0 -8 1 417.06 447.25 3.95 o 1 -8 1 161.87 141.85 4.74 o 2 -8 1 5.89 7.42 0.57 o 3 -8 1 149.22 142.70 3.53 o 4 -8 1 138.07 132.47 3.55 o -4 -7 1 112.34 113.53 1.46 o -3 -7 1 131.09 130.04 1.68 o -2 -7 1 42.45 45.08 0.95 o -1 -7 1 8.40 13.90 0.68 o 0 -7 1 384.53 406.10 9.26 o 1 -7 1 1090.19 1095.74 16.99 o 2 -7 1 204.06 190.26 5.18 o 3 -7 1 57.90 56.24 1.09 o 4 -7 1 128.98 127.86 1.25 o -4 -6 1 10.74 10.89 0.53 o -3 -6 1 235.46 234.44 2.03 o -2 -6 1 486.31 479.50 6.41 o -1 -6 1 1583.67 1598.76 11.12 o 0 -6 1 1957.78 1901.86 10.11 o 1 -6 1 235.17 224.33 2.27 o 2 -6 1 18.08 19.87 2.19 o 3 -6 1 206.40 188.69 1.62 o 4 -6 1 117.49 114.16 1.24 o -4 -5 1 144.10 149.76 2.28 o -3 -5 1 531.17 520.49 2.98 o -2 -5 1 248.72 278.39 2.41 o -1 -5 1 772.48 729.99 6.62 o 0 -5 1 708.06 687.59 5.73 o 1 -5 1 1826.22 1726.54 12.75 o 2 -5 1 1408.27 1412.19 7.09 o 3 -5 1 128.19 122.69 1.18 o 4 -5 1 387.98 388.78 3.00 o -4 -4 1 34.06 38.48 0.85 o -3 -4 1 293.62 295.98 2.73 o -2 -4 1 1482.74 1457.85 7.83 o -1 -4 1 279.65 277.44 4.06 o 0 -4 1 1029.46 964.15 9.70 o 1 -4 1 228.95 223.21 2.38 o 2 -4 1 498.60 502.24 3.13 o 3 -4 1 16.90 16.10 0.44 o 4 -4 1 41.84 39.55 0.71 o -4 -3 1 88.95 93.55 1.80 o -3 -3 1 149.39 146.91 1.58 o -2 -3 1 367.03 352.73 2.78 o -1 -3 1 531.15 519.27 5.54 o 0 -3 1 846.50 830.51 14.45 o 1 -3 1 364.59 325.78 5.13 o 2 -3 1 436.09 428.78 3.06 o 3 -3 1 180.55 184.64 1.32 o 4 -3 1 96.82 103.90 1.27 o -4 -2 1 273.13 296.19 3.22 o -3 -2 1 109.02 104.95 0.91 o -2 -2 1 114.75 109.15 1.17 o -1 -2 1 5949.22 5421.49 31.86 o 0 -2 1 244.46 241.73 4.69 o 1 -2 1 4241.98 3958.99 30.48 o 2 -2 1 1454.60 1405.41 5.01 o 3 -2 1 259.13 257.50 2.01 o 4 -2 1 37.22 36.21 0.63 o -4 -1 1 226.31 238.79 2.41 o -3 -1 1 223.82 218.08 1.37 o -2 -1 1 1093.43 1077.41 5.54 o -1 -1 1 12659.77 11582.66 64.94 o 0 -1 1 54.09 48.45 2.07 o 1 -1 1 9745.22 9316.32 53.86 o 2 -1 1 135.56 123.46 1.11 o 3 -1 1 7.12 5.89 0.26 o 4 -1 1 130.58 134.67 2.26 o -4 0 1 21.74 21.08 0.60 o -3 0 1 3.22 3.74 0.46 o -2 0 1 5.15 10.05 0.29 o -1 0 1 1702.88 1716.18 15.63 o 0 0 1 563.69 504.89 4.20 o 1 0 1 377.28 337.32 3.76 o 2 0 1 1556.62 1460.91 12.08 o 3 0 1 136.41 130.08 1.21 o 4 0 1 144.99 145.19 4.20 o -4 1 1 213.50 224.02 3.69 o -3 1 1 197.11 185.88 1.91 o -2 1 1 1084.79 1123.23 10.72 o -1 1 1 12965.03 12027.56 94.14 o 0 1 1 41.27 40.78 2.48 o 1 1 1 9026.41 8024.55 57.04 o 2 1 1 124.12 110.87 2.05 o 3 1 1 6.64 5.44 0.26 o 4 1 1 127.46 134.66 2.03 o -4 2 1 262.12 288.01 5.60 o -3 2 1 106.60 99.54 1.26 o -2 2 1 106.31 103.31 1.43 o -1 2 1 5767.46 5451.90 32.02 o 0 2 1 195.19 210.49 2.51 o 1 2 1 4323.89 4001.99 68.67 o 2 2 1 1471.82 1402.99 8.72 o 3 2 1 245.98 242.13 1.54 o 4 2 1 46.10 46.79 1.08 o -4 3 1 98.09 100.05 1.65 o -3 3 1 127.62 122.07 1.83 o -2 3 1 347.38 338.63 3.27 o -1 3 1 532.05 542.51 5.25 o 0 3 1 914.81 899.18 6.05 o 1 3 1 357.02 349.82 3.75 o 2 3 1 469.61 472.69 4.68 o 3 3 1 195.23 200.30 1.47 o 4 3 1 89.88 89.88 1.39 o -4 4 1 39.57 43.88 1.31 o -3 4 1 254.20 254.97 2.83 o -2 4 1 1540.30 1566.96 8.70 o -1 4 1 312.34 347.66 3.03 o 0 4 1 1021.79 1090.16 8.48 o 1 4 1 279.72 282.76 4.33 o 2 4 1 426.63 441.59 13.25 o 3 4 1 17.67 15.89 0.47 o 4 4 1 42.36 40.56 1.28 o -4 5 1 120.43 121.16 5.82 o -3 5 1 513.64 484.91 5.16 o -2 5 1 226.70 254.22 2.76 o -1 5 1 739.80 784.36 20.01 o 0 5 1 717.40 751.84 4.87 o 1 5 1 1724.96 1742.89 26.76 o 2 5 1 1292.21 1349.68 10.29 o 3 5 1 144.86 141.24 1.29 o 4 5 1 376.99 374.98 3.23 o -4 6 1 13.03 13.35 0.66 o -3 6 1 266.36 268.58 4.60 o -2 6 1 501.61 494.36 11.14 o -1 6 1 1591.82 1771.41 21.19 o 0 6 1 1838.90 1926.94 10.48 o 1 6 1 284.43 285.55 6.45 o 2 6 1 29.58 30.81 1.34 o 3 6 1 225.12 211.69 2.74 o 4 6 1 115.93 115.17 1.53 o -4 7 1 90.89 79.91 45.75 o -3 7 1 126.00 129.98 2.40 o -2 7 1 67.78 71.73 1.52 o -1 7 1 8.98 13.72 0.82 o 0 7 1 344.48 415.73 7.05 o 1 7 1 1124.26 1126.11 8.57 o 2 7 1 184.89 175.92 1.69 o 3 7 1 48.51 48.26 0.83 o 4 7 1 133.22 138.31 3.21 o -4 8 1 82.61 73.38 24.91 o -3 8 1 169.39 175.71 1.93 o -2 8 1 236.02 243.13 1.90 o -1 8 1 289.62 300.89 11.91 o 0 8 1 430.97 496.24 7.26 o 1 8 1 172.57 178.59 6.16 o 2 8 1 6.03 8.96 0.38 o 3 8 1 133.48 128.40 2.11 o 4 8 1 140.94 147.09 2.08 o -4 9 1 13.24 12.58 0.55 o -3 9 1 298.96 301.24 4.66 o -2 9 1 17.95 18.83 0.40 o -1 9 1 483.90 486.41 13.97 o 0 9 1 474.49 538.22 8.12 o 1 9 1 1094.34 1225.52 88.89 o 2 9 1 60.24 63.16 0.79 o 3 9 1 138.41 137.54 3.26 o 4 9 1 183.21 172.86 22.21 o -4 10 1 42.38 41.23 1.06 o -3 10 1 257.61 243.45 13.85 o -2 10 1 647.91 637.29 3.60 o -1 10 1 30.17 35.77 0.55 o 0 10 1 1333.03 1349.14 14.88 o 1 10 1 591.96 594.71 3.83 o 2 10 1 690.37 724.51 6.68 o 3 10 1 770.64 766.11 5.90 o 4 10 1 33.78 30.08 7.06 o -4 11 1 106.31 106.64 2.67 o -3 11 1 9.77 10.29 0.38 o -2 11 1 542.07 556.75 3.55 o -1 11 1 1203.32 1181.54 6.98 o 0 11 1 10.17 11.72 0.28 o 1 11 1 1320.49 1341.64 6.02 o 2 11 1 105.30 106.57 1.19 o 3 11 1 74.41 71.03 1.24 o 4 11 1 242.44 242.13 11.54 o -3 12 1 25.73 24.46 0.93 o -2 12 1 1.83 2.32 0.19 o -1 12 1 339.14 351.03 2.06 o 0 12 1 194.53 200.38 1.44 o 1 12 1 161.27 171.47 1.17 o 2 12 1 14.30 15.08 0.42 o 3 12 1 35.55 36.44 0.82 o -3 13 1 10.79 10.88 0.46 o -2 13 1 334.08 321.57 4.53 o -1 13 1 113.87 113.25 0.87 o 0 13 1 506.53 531.09 3.68 o 1 13 1 1.70 2.43 0.20 o 2 13 1 18.84 21.37 0.50 o 3 13 1 23.60 21.61 0.54 o -3 14 1 167.03 173.84 2.56 o -2 14 1 329.03 334.00 3.63 o -1 14 1 618.46 680.10 4.04 o 0 14 1 749.51 791.16 4.25 o 1 14 1 71.06 69.53 0.84 o 2 14 1 483.48 481.96 4.48 o 3 14 1 24.61 24.54 0.78 o -3 15 1 92.15 93.64 1.85 o -2 15 1 215.35 233.05 3.06 o -1 15 1 1854.23 1877.36 10.97 o 0 15 1 278.63 302.81 2.24 o 1 15 1 615.35 650.46 5.91 o 2 15 1 792.22 833.81 4.70 o 3 15 1 189.13 202.60 3.85 o -3 16 1 223.38 227.09 9.73 o -2 16 1 179.17 185.69 2.23 o -1 16 1 84.11 91.25 1.03 o 0 16 1 127.26 146.96 1.23 o 1 16 1 35.35 33.57 0.52 o 2 16 1 474.44 513.02 4.36 o 3 16 1 145.15 147.44 2.45 o -2 17 1 63.72 71.30 1.14 o -1 17 1 6.94 9.51 0.51 o 0 17 1 123.09 118.72 1.33 o 1 17 1 55.57 59.50 0.92 o 2 17 1 149.15 168.69 2.65 o -2 18 1 19.67 21.06 0.62 o -1 18 1 15.20 15.11 0.56 o 0 18 1 1.33 2.38 0.30 o 1 18 1 11.25 16.19 0.73 o 2 18 1 83.30 89.59 2.15 o -1 19 1 150.98 167.11 2.50 o 0 19 1 5.27 6.35 0.47 o 1 19 1 357.44 407.94 17.81 o -1 20 1 65.91 57.15 9.49 o 0 20 1 309.04 313.50 19.96 o 1 20 1 112.53 98.01 2.60 o -2 -17 2 465.14 419.70 5.05 o 2 -17 2 153.82 147.80 2.58 o -2 -16 2 889.28 826.48 6.28 o 2 -16 2 78.45 75.53 1.86 o 3 -16 2 117.51 72.89 1.47 o -3 -15 2 80.23 74.59 1.19 o -2 -15 2 220.77 217.34 3.94 o -1 -15 2 104.48 91.61 4.94 o 1 -15 2 209.17 173.41 6.93 o 2 -15 2 209.03 201.61 3.56 o 3 -15 2 31.66 29.15 2.02 o -3 -14 2 174.72 166.99 1.72 o -2 -14 2 247.35 244.38 4.46 o -1 -14 2 191.51 175.17 6.62 o 1 -14 2 161.25 153.32 6.48 o 2 -14 2 44.50 40.79 1.54 o 3 -14 2 58.84 57.27 1.19 o -3 -13 2 144.89 135.48 1.76 o -2 -13 2 113.56 105.76 4.55 o -1 -13 2 301.63 297.24 8.71 o 0 -13 2 1764.86 1642.47 21.41 o 1 -13 2 161.61 140.84 4.25 o 2 -13 2 68.92 57.60 1.24 o 3 -13 2 8.09 6.72 0.48 o -3 -12 2 220.69 221.87 2.37 o -2 -12 2 218.68 217.44 3.58 o -1 -12 2 672.67 656.80 13.28 o 0 -12 2 365.16 346.21 5.81 o 1 -12 2 118.51 110.29 5.05 o 2 -12 2 124.14 109.31 1.78 o 3 -12 2 66.70 66.21 1.40 o -4 -11 2 38.67 40.11 0.84 o -3 -11 2 29.16 30.47 0.83 o -2 -11 2 202.29 205.09 2.58 o -1 -11 2 830.16 827.28 14.76 o 0 -11 2 475.32 450.14 8.46 o 1 -11 2 466.24 413.27 13.40 o 2 -11 2 450.80 412.47 5.21 o 3 -11 2 268.70 259.34 3.19 o 4 -11 2 170.94 168.33 2.47 o -4 -10 2 13.38 12.42 0.62 o -3 -10 2 63.94 64.31 2.65 o -2 -10 2 952.02 942.05 7.39 o -1 -10 2 135.37 134.36 3.39 o 0 -10 2 711.74 665.90 7.32 o 1 -10 2 203.22 197.13 3.85 o 2 -10 2 98.73 92.65 2.20 o 3 -10 2 679.12 671.49 8.70 o 4 -10 2 50.32 47.41 1.88 o -4 -9 2 151.30 152.69 1.95 o -3 -9 2 546.59 535.41 10.62 o -2 -9 2 512.26 511.65 4.77 o -1 -9 2 402.38 407.94 5.07 o 0 -9 2 608.67 872.26 486.97 o 1 -9 2 1985.55 1911.84 21.13 o 2 -9 2 389.56 375.98 3.67 o 3 -9 2 162.14 156.36 2.30 o 4 -9 2 43.54 42.66 0.63 o -4 -8 2 114.98 118.88 1.36 o -3 -8 2 7.72 9.13 0.47 o -2 -8 2 49.29 53.19 1.18 o -1 -8 2 367.41 347.00 4.69 o 0 -8 2 247.07 290.87 4.13 o 1 -8 2 158.01 182.26 5.06 o 2 -8 2 202.97 190.42 2.11 o 3 -8 2 125.76 121.95 1.60 o 4 -8 2 42.00 38.88 0.60 o -4 -7 2 135.15 141.30 1.34 o -3 -7 2 89.98 94.46 1.21 o -2 -7 2 624.68 634.61 4.62 o -1 -7 2 951.72 1017.28 8.10 o 0 -7 2 348.67 359.67 4.24 o 1 -7 2 381.59 401.27 2.60 o 2 -7 2 420.50 399.51 3.39 o 3 -7 2 133.16 129.82 1.30 o 4 -7 2 28.96 28.75 0.66 o -4 -6 2 556.87 532.47 3.66 o -3 -6 2 222.91 222.37 2.92 o -2 -6 2 288.64 258.64 4.09 o -1 -6 2 377.44 398.13 4.03 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