#------------------------------------------------------------------------------ #$Date: 2020-12-05 07:25:49 +0200 (Sat, 05 Dec 2020) $ #$Revision: 259552 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/22/2022290.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022290 loop_ _publ_author_name 'Rosiak, Damian' 'Okuniewski, Andrzej' 'Chojnacki, Jaros\/law' _publ_section_title ; The influence of the type of halogen substituent and its position on the molecular conformation, intermolecular interactions and crystal packing for a series of 1-benzoyl-3-(halogenophenyl)thioureas ; _journal_coeditor_code WP3011 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229620015594 _journal_volume 77 _journal_year 2021 _chemical_absolute_configuration ad _chemical_formula_iupac 'C14 H11 Br N2 O S' _chemical_formula_moiety 'C14 H11 Br N2 O S' _chemical_formula_sum 'C14 H11 Br N2 O S' _chemical_formula_weight 335.22 _chemical_name_common 1-Benzoyl-3-m-bromophenylthiourea _chemical_name_systematic ; 1-Benzoyl-3-(3-bromophenyl)thiourea ; _space_group_crystal_system monoclinic _space_group_IT_number 7 _space_group_name_Hall 'P -2yc' _space_group_name_H-M_alt 'P 1 c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90 _cell_angle_beta 91.052(12) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 4.6404(7) _cell_length_b 15.017(2) _cell_length_c 19.074(3) _cell_measurement_reflns_used 6776 _cell_measurement_temperature 125 _cell_measurement_theta_max 29.42 _cell_measurement_theta_min 2.53 _cell_volume 1328.9(3) _computing_cell_refinement ; X-AREA (Stoe & Cie, 2009) ; _computing_data_collection ; X-AREA (Stoe & Cie, 2009) ; _computing_data_reduction ; X-RED32 (Stoe & Cie, 2009) ; _computing_molecular_graphics ; OLEX2 (Dolomanov et al., 2009) ; _computing_publication_material ; OLEX2 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 125 _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device '2-circle goniometer' _diffrn_measurement_device_type 'Stoe IPDS 2T' _diffrn_measurement_method 'rotation method, \w scans' _diffrn_radiation_monochromator 'parabolic x-ray mirror' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0872 _diffrn_reflns_av_unetI/netI 0.0669 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 15213 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.997 _diffrn_reflns_theta_min 2.530 _diffrn_source 'GeniX Mo, 0.05 x 0.05 mm2 microfocus' _diffrn_source_current 1.000 _diffrn_source_power 0.050 _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 3.241 _exptl_absorpt_correction_T_max 0.8747 _exptl_absorpt_correction_T_min 0.3544 _exptl_absorpt_correction_type integration _exptl_absorpt_process_details ; [X-RED32 (Stoe & Cie, 2009), by Gaussian integration, analogous to Coppens (1970)] ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.675 _exptl_crystal_description needle _exptl_crystal_F_000 672 _exptl_crystal_size_max 0.678 _exptl_crystal_size_mid 0.052 _exptl_crystal_size_min 0.04 _refine_diff_density_max 1.967 _refine_diff_density_min -0.654 _refine_ls_abs_structure_details ; Flack (1983), 2288 Friedel pairs ; _refine_ls_abs_structure_Flack 0.01(2) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.021 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 343 _refine_ls_number_reflns 4909 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.021 _refine_ls_R_factor_all 0.0761 _refine_ls_R_factor_gt 0.0656 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1436P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1674 _refine_ls_wR_factor_ref 0.1832 _reflns_number_gt 4294 _reflns_number_total 4537 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file wp3011sup1.cif _cod_data_source_block 5 _cod_original_cell_volume 1329.0(3) _cod_database_code 2022290 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.217 _shelx_estimated_absorpt_t_max 0.881 _shelx_hkl_file ; -3 -12 17 4.41 9.65 -3 -11 -5 0.26 9.13 -3 -11 16 29.74 9.70 -3 -10 15 11.08 7.71 -3 -9 13 18.44 7.90 -3 -8 9 59.34 8.99 -2 -14 -13 -1.53 8.58 -2 -12 -12 2.24 6.76 -2 -8 19 78.48 8.53 -2 -7 18 14.03 5.85 -2 -6 16 0.27 7.36 -2 -4 2 368.42 14.58 -2 -4 10 19.29 4.66 -1 -13 -16 1.15 8.74 -1 -10 -14 54.90 5.41 -1 -7 22 49.39 9.14 -1 -6 -10 352.23 8.69 -1 -6 21 4.56 8.17 -1 -4 18 23.33 5.26 0 -9 -16 7.55 7.58 0 -8 -15 239.75 6.65 0 -7 -14 40.25 5.10 0 -6 24 -7.28 6.55 0 -5 -12 18.20 6.01 0 -4 21 9.48 7.70 0 -1 -4 762.90 13.94 0 0 11 -0.08 4.55 1 -7 -16 130.37 7.75 1 -6 -15 133.54 7.21 1 -4 23 -2.49 8.16 1 -3 -11 230.50 7.35 1 -2 20 5.66 5.33 1 -1 18 58.99 5.43 1 0 15 -3.77 6.97 1 1 11 62.26 6.63 2 -10 -19 5.04 7.22 2 -4 24 -3.88 7.16 2 -1 19 6.65 6.02 2 0 -6 1206.49 13.74 2 1 -3 757.98 14.23 2 1 13 7.55 5.67 3 -10 -19 0.39 7.44 3 -6 -16 44.04 5.49 3 -3 -12 59.01 5.60 3 -2 21 9.18 6.42 3 1 -3 107.06 6.88 3 1 13 0.11 6.53 4 -6 -15 4.13 6.28 5 -5 -12 -3.59 6.75 5 -2 -7 54.90 6.64 5 -1 14 0.64 7.43 6 -4 -7 -3.14 7.54 6 -3 -5 3.04 7.68 -3 -16 -9 7.15 12.11 -3 -10 -4 77.33 11.71 -3 -10 14 88.45 8.23 -3 -9 12 34.39 7.87 -3 -8 8 100.89 8.99 -2 -13 -13 53.17 7.79 -2 -10 21 38.50 7.63 -2 -9 20 54.81 6.55 -2 -7 -7 105.74 8.99 -2 -7 17 43.97 7.74 -2 -6 -5 71.62 7.75 -2 -6 15 23.19 6.67 -2 -5 13 12.52 5.39 -1 -15 -17 5.55 9.81 -1 -12 -16 -0.94 7.51 -1 -8 23 14.64 7.12 -1 -5 -9 50.28 6.32 -1 -5 19 9.05 6.67 -1 -4 17 1.15 7.09 -1 -3 15 131.36 5.75 0 -14 -19 -3.64 9.53 0 -12 -18 0.22 6.09 0 -10 -17 2.06 7.42 0 -5 22 8.42 7.51 0 -2 -7 83.48 7.04 0 0 10 969.56 11.46 1 -11 -19 5.50 6.66 1 -9 -18 66.11 8.17 1 -8 -17 74.37 6.18 1 -5 -14 141.94 5.51 1 -5 24 -5.20 6.78 1 -4 -13 494.01 8.46 1 -3 21 9.48 7.84 1 -2 19 57.36 7.48 1 1 10 22.02 6.28 2 -6 -16 5.89 4.72 2 -3 22 3.50 6.34 2 -1 -9 190.99 7.00 2 0 16 54.56 5.90 3 -8 -18 93.88 7.30 3 -7 -17 10.13 4.63 3 -5 -15 46.01 4.03 3 -4 -14 73.98 6.02 3 -3 22 6.46 6.15 3 -2 -11 13.58 5.34 3 -2 20 -0.74 8.08 3 -1 -9 68.50 5.17 3 -1 18 1.60 7.39 3 0 16 25.75 5.39 4 -2 -10 19.91 4.51 4 -2 19 5.16 7.33 4 -1 17 3.63 6.91 4 0 -5 -2.46 5.60 4 0 14 89.25 8.39 4 1 -1 45.66 9.01 5 -6 -14 6.96 6.86 5 -4 -11 -0.54 5.95 5 0 9 -1.84 7.67 6 -2 -2 -2.14 7.87 -3 -15 -9 1.20 10.23 -3 -12 16 -2.86 8.92 -3 -11 15 -2.08 7.26 -3 -10 13 41.18 7.62 -3 -8 3 89.06 10.31 -3 -8 6 11.78 8.72 -3 -8 7 122.63 8.03 -2 -15 -14 3.49 9.62 -2 -11 -12 1.29 8.40 -2 -10 -11 56.89 7.41 -2 -10 20 29.14 8.57 -2 -9 -10 54.33 7.21 -2 -9 19 37.81 7.87 -2 -8 18 30.91 7.22 -2 -5 12 86.76 7.44 -2 -4 3 10.36 7.94 -1 -14 -17 4.00 6.50 -1 -10 -15 12.41 7.00 -1 -9 -14 26.53 6.86 -1 -9 23 12.49 9.42 -1 -8 -13 9.11 6.73 -1 -8 22 -6.32 8.67 -1 -7 -12 42.07 6.60 -1 -7 21 33.88 7.93 -1 -6 20 8.56 5.30 -1 -5 18 0.72 6.82 -1 -3 -5 383.80 11.01 -1 -3 14 28.23 6.50 0 -13 -19 7.92 8.79 0 -11 -18 16.98 7.99 0 -8 -16 9.71 6.30 0 -7 24 4.63 6.07 0 -6 23 13.76 5.99 0 -4 -11 304.83 6.57 0 -4 20 136.25 7.53 0 0 9 3.87 5.79 1 -12 -20 27.79 7.12 1 -10 -19 23.60 8.38 1 -4 22 2.79 6.85 1 0 -5 5.82 6.59 1 0 14 137.69 5.96 1 1 9 436.22 9.81 2 -10 -20 25.08 6.80 2 -9 -19 38.76 5.37 2 -4 23 -4.78 5.41 2 -3 -13 8.63 6.20 2 -2 -11 143.26 5.97 2 -2 20 6.88 4.27 2 -1 18 12.60 4.60 2 0 15 -0.72 5.64 2 1 12 84.13 5.81 3 -9 -19 2.32 5.23 3 -3 -13 132.22 6.19 3 0 -7 3.13 3.95 3 0 15 2.85 6.03 3 1 12 59.85 6.25 4 -7 -17 -0.88 6.52 4 -6 -16 18.56 6.36 4 -5 -15 57.17 5.85 4 -3 -12 4.73 5.26 4 -1 -8 5.51 4.64 4 -1 16 -1.98 7.36 4 1 9 33.20 6.67 5 -5 -13 7.92 6.95 5 -3 -10 17.89 5.85 5 -2 -8 4.94 6.52 5 -1 -5 41.18 6.05 5 -1 13 8.64 7.87 5 0 -1 1.24 8.22 5 0 8 61.80 9.94 6 -3 -6 11.60 7.55 -3 -13 -8 48.98 9.12 -3 -13 16 1.02 8.93 -3 -12 -7 87.78 9.87 -3 -12 15 145.43 9.67 -3 -11 14 1.12 7.72 -3 -8 4 350.22 11.80 -3 -8 5 23.20 7.96 -2 -14 -14 41.74 8.90 -2 -12 -13 47.67 7.43 -2 -8 -9 185.06 7.84 -2 -8 17 0.63 6.99 -2 -7 16 72.90 6.10 -2 -6 14 32.65 6.37 -2 -5 -3 152.44 12.08 -2 -5 11 216.50 7.68 -2 -4 4 163.86 8.15 -1 -13 -17 11.25 8.61 -1 -11 -16 49.25 8.11 -1 -6 -11 28.81 6.37 -1 -6 19 78.51 7.37 -1 -4 16 23.49 4.81 -1 -2 10 33.05 4.39 0 -12 -19 0.51 7.69 0 -10 -18 20.47 6.99 0 -9 -17 106.10 7.64 0 -8 24 17.27 8.38 0 -6 -14 6.94 4.65 0 -6 22 11.63 7.28 0 -5 -13 68.88 6.36 0 -5 21 3.80 6.42 0 -3 18 143.58 6.07 0 0 8 32.52 6.46 1 -11 -20 15.45 8.63 1 -8 -18 -0.91 7.05 1 -7 -17 22.45 6.92 1 -6 -16 46.52 7.13 1 -6 24 14.98 6.04 1 -5 -15 80.97 6.31 1 -5 23 6.02 6.10 1 -3 -12 197.24 5.33 1 -3 20 3.74 6.62 1 -2 18 1.08 6.63 1 -1 -8 87.13 5.10 1 -1 16 16.17 5.93 1 0 13 -5.29 6.37 1 1 8 606.71 11.17 2 -8 -19 82.21 6.68 2 -7 -18 16.19 6.77 2 -6 -17 55.03 6.92 2 -3 21 28.33 4.89 2 -2 19 13.85 5.87 2 0 -7 -1.32 5.46 2 1 11 110.44 6.02 3 -8 -19 23.65 6.60 3 -7 -18 16.38 6.29 3 -6 -17 55.17 6.50 3 -5 -16 11.58 5.75 3 -4 22 1.64 8.19 3 -3 21 1.54 5.89 3 1 -4 79.63 6.82 3 1 11 19.51 5.60 4 -4 -14 20.32 5.68 4 -2 18 5.19 7.04 4 0 13 2.04 7.03 4 1 8 26.68 7.78 5 -4 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4.77 1 0 -6 1770.98 16.06 1 0 12 753.43 9.88 1 1 7 424.78 10.04 2 -10 -21 13.51 5.70 2 -7 -19 33.56 6.36 2 -6 -18 44.81 6.27 2 -3 -14 -3.54 6.15 2 -3 20 1.32 4.44 2 -2 18 4.28 6.04 2 0 -8 171.03 6.34 2 1 10 41.81 5.36 3 -8 -20 6.08 5.87 3 -7 -19 4.35 6.46 3 -6 -18 -3.77 6.05 3 -5 -17 22.11 6.15 3 -3 -14 38.91 4.23 3 -3 20 -5.56 5.90 3 -2 18 -3.15 6.84 3 0 -8 222.50 6.31 3 1 10 171.58 7.29 4 -4 -15 0.17 4.91 4 0 12 51.32 6.69 4 1 7 7.58 6.91 5 -4 -13 13.68 6.38 5 -2 -9 10.22 5.60 6 -2 -4 1.32 7.15 -3 -15 -10 -4.02 8.24 -3 -13 14 -3.42 7.78 -3 -12 13 -8.72 7.61 -3 -11 12 90.96 7.37 -3 -10 -5 24.39 9.58 -2 -12 -14 8.83 7.09 -2 -11 19 12.29 6.10 -2 -10 18 20.60 6.84 -2 -9 17 40.17 5.31 -2 -8 -10 78.18 6.14 -2 -7 14 130.54 6.78 -2 -6 12 9.53 5.82 -2 -5 9 140.02 6.76 -1 -11 -17 8.23 5.52 -1 -10 22 6.97 6.44 -1 -9 21 15.52 7.57 -1 -8 20 19.31 7.40 -1 -7 19 34.32 5.37 -1 -5 16 202.58 7.16 -1 -4 14 26.91 6.38 -1 -3 -6 154.91 7.21 -1 -2 -2 1592.90 29.30 -1 -2 7 140.62 6.89 0 -10 -19 0.98 7.19 0 -5 -14 276.65 7.43 0 -4 18 262.70 6.22 0 -1 11 3.59 3.67 0 0 5 -0.11 6.32 1 -8 -19 18.55 5.25 1 -5 -16 207.40 5.70 1 -5 21 9.02 7.01 1 -4 -15 85.67 5.64 1 -4 20 5.84 5.05 1 -1 -9 30.50 4.35 1 -1 14 87.20 6.34 1 0 11 -2.05 5.49 1 1 6 61.69 6.50 2 -9 -21 14.28 7.07 2 -8 -20 55.76 5.57 2 -6 23 8.03 7.32 2 -5 22 10.17 6.93 2 -4 -16 248.66 7.36 2 -4 21 4.15 4.60 2 0 13 2.31 4.90 3 -4 -16 17.20 5.54 3 -4 21 -0.01 5.45 3 -2 -13 282.12 6.76 3 -1 -11 20.40 5.10 3 0 13 -3.41 5.41 3 1 -5 68.08 6.13 4 -6 -18 13.97 5.64 4 -3 -14 13.55 4.69 4 -2 -12 41.45 4.86 4 -1 -10 16.93 4.22 4 -1 14 0.18 7.53 4 0 -7 -0.51 5.01 5 -5 -15 -0.58 6.60 5 -3 -12 15.05 5.07 5 -2 14 5.20 6.14 5 -1 -7 49.22 5.70 5 -1 11 3.39 7.29 6 -3 -8 1.61 7.19 -3 -14 -10 9.65 9.03 -3 -13 -9 11.69 8.69 -3 -12 -8 53.51 8.65 -3 -9 7 220.64 8.83 -2 -13 -15 21.28 7.69 -2 -12 19 6.79 8.02 -2 -11 18 49.58 7.75 -2 -9 16 87.57 6.88 -2 -8 15 173.88 7.03 -2 -7 13 82.50 6.67 -2 -6 11 122.29 6.52 -1 -12 -18 8.19 5.81 -1 -10 -17 0.20 6.05 -1 -9 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26.55 4.25 1 -5 14 109.52 4.65 1 -4 13 62.25 3.53 1 -3 -21 43.05 3.55 1 0 -15 0.77 3.90 1 0 5 1.76 4.05 1 1 -11 215.18 5.23 2 -11 20 5.51 4.12 2 -8 18 0.32 4.16 2 -7 17 3.07 4.06 2 -5 15 2.44 3.88 2 -4 -24 -0.53 5.79 2 -4 14 35.59 3.98 2 -2 -21 163.43 5.85 2 -2 11 406.87 6.00 2 -1 -19 6.34 3.47 2 0 -17 -4.47 4.55 2 0 7 -1.36 3.60 2 1 -14 88.02 4.59 2 2 -9 6.26 3.76 3 -8 18 -5.87 4.55 3 -4 14 94.98 4.46 3 2 -10 51.16 4.41 4 -3 12 3.17 4.19 4 -1 -19 12.62 3.73 4 0 6 48.86 5.74 4 1 -13 -0.03 3.97 4 2 -7 -0.72 4.87 4 2 -6 5.17 4.06 4 2 -5 157.71 5.75 4 2 -4 8.32 4.81 4 2 -3 17.87 5.45 5 -5 13 4.15 4.97 5 -3 10 3.32 5.27 5 0 -14 2.60 3.67 5 1 -9 -3.07 4.69 5 1 -8 9.80 4.09 5 1 -2 43.72 7.72 6 -2 4 0.14 7.10 -3 -16 7 87.78 6.54 -3 -14 6 164.13 6.67 -3 -13 5 99.74 7.07 -3 -12 4 15.31 5.43 -3 -11 -13 2.60 5.40 -3 -10 -11 6.11 5.04 -3 -9 -8 22.33 5.78 -2 -16 13 14.28 5.46 -2 -12 11 183.94 5.79 -2 -7 -16 17.94 4.68 -2 -6 -14 18.13 4.10 -2 -5 -11 135.72 4.73 -1 -14 16 24.10 4.89 -1 -12 15 0.33 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291.03 7.14 0 15 3 11.30 4.22 0 16 6 15.20 6.09 0 16 16 0.80 6.98 0 17 9 4.32 4.98 0 17 11 71.70 5.78 1 -8 5 312.69 7.78 1 -7 2 143.51 6.36 1 -6 0 441.31 8.87 1 -3 -4 120.03 6.99 1 14 -5 3.09 5.83 2 -11 16 9.30 7.16 2 -2 -9 1.83 4.66 2 0 -10 15.72 5.22 2 14 -9 23.39 7.00 3 -13 14 3.87 7.36 3 -13 15 0.34 8.26 3 -12 2 23.43 5.81 3 -8 -6 6.86 5.02 3 -4 -10 19.43 4.30 3 -3 -11 1.49 5.28 3 -1 -12 62.98 6.02 4 -14 7 0.37 5.12 4 -13 2 5.92 4.77 4 -10 -5 8.72 4.03 4 -8 -8 -0.08 5.45 4 -4 -12 -0.31 5.54 4 3 -15 2.92 6.57 4 10 -15 5.18 10.80 5 -11 -5 7.30 5.61 5 -9 -8 -2.30 5.62 5 -8 -9 17.23 4.69 5 -5 -12 -0.44 5.18 5 -2 -14 -0.72 5.71 5 0 -15 0.51 5.37 0 2 23 32.41 6.82 0 4 24 26.51 6.44 0 5 24 6.54 7.02 0 6 24 7.88 7.17 0 7 24 2.83 7.47 0 8 24 9.20 6.20 0 13 20 -0.55 7.27 0 14 3 19.05 5.44 0 14 19 16.09 7.61 0 15 17 11.06 6.93 0 16 8 65.16 6.60 0 16 9 54.60 6.61 0 16 10 27.24 6.13 0 16 11 32.80 6.20 0 16 12 9.27 6.58 0 16 13 19.81 6.37 0 16 14 2.85 6.54 0 16 15 3.66 5.03 1 -4 -3 72.82 4.77 1 -2 -5 1048.79 13.17 1 18 0 11.57 5.68 1 19 2 37.72 6.35 2 -10 20 3.41 9.11 2 -9 -1 159.76 6.17 2 2 -11 81.83 5.99 2 12 -10 12.85 7.97 2 19 -4 0.92 6.96 3 -10 -3 4.33 3.56 3 5 -14 34.66 6.69 3 6 -14 -0.55 7.25 4 -14 4 0.23 5.58 4 -14 5 4.55 6.91 4 -13 1 10.70 4.91 4 -12 -2 7.26 6.33 4 -10 -6 0.69 5.11 4 -3 -13 -0.35 5.77 4 -1 -14 4.52 5.69 5 -12 -4 8.00 5.46 5 -3 -14 8.12 5.24 5 -1 -15 4.34 4.97 5 2 -16 4.05 5.52 0 -3 17 28.90 7.27 0 -2 19 36.08 5.94 0 -1 20 78.81 7.30 0 0 21 8.54 6.81 0 1 22 0.78 6.55 0 4 -2 5.44 5.95 0 4 23 -6.21 7.12 0 7 23 5.63 6.90 0 8 23 1.64 7.10 0 9 23 3.98 5.58 0 10 -1 38.33 3.77 0 10 22 12.77 6.98 0 11 0 9.55 5.18 0 12 21 17.19 5.55 0 13 2 80.79 6.01 0 13 19 14.18 6.82 0 14 18 26.58 6.66 0 15 15 8.80 6.51 0 15 16 59.17 5.18 1 -9 9 44.98 6.31 1 -9 10 19.62 6.77 1 -9 11 10.47 6.46 1 -5 23 0.66 10.08 1 10 -7 19.94 6.21 1 18 1 8.69 6.31 1 19 4 20.32 6.84 2 -11 17 3.30 7.16 2 -8 -3 -0.40 3.43 2 -6 -6 37.17 5.06 2 -5 -7 59.06 5.39 2 -4 -8 261.30 6.57 2 -1 -10 4.84 4.87 2 16 -7 -0.50 7.06 2 18 -5 7.80 6.30 3 -12 1 9.10 4.19 3 -11 -2 206.70 7.17 3 -10 -4 57.16 5.65 3 -5 -10 31.79 5.53 3 -2 -12 18.33 5.31 3 0 -13 -1.04 5.24 3 4 -14 51.75 7.35 3 13 -12 3.24 10.60 3 16 -10 1.38 8.36 4 -14 3 -5.31 5.98 4 -13 0 -0.03 4.63 4 -11 -5 9.50 4.85 4 -8 -9 3.71 5.54 4 -7 -10 13.31 5.54 4 -5 -12 0.02 4.86 4 1 -15 10.50 5.72 5 -11 -6 8.80 4.25 5 -9 -9 4.33 5.56 5 -7 -11 2.57 4.23 5 -6 -12 -1.88 5.16 5 -5 -13 -0.77 5.10 5 1 -16 1.91 5.53 0 2 22 12.68 6.19 0 5 23 22.80 6.05 0 6 23 10.89 6.35 0 9 22 12.90 6.33 0 10 21 0.51 6.33 0 11 21 10.70 5.00 0 12 19 1.07 6.78 0 12 20 3.81 5.12 0 13 3 132.87 5.91 0 13 18 13.79 6.56 0 14 5 55.78 5.51 0 14 16 78.73 6.72 0 14 17 25.84 5.05 0 15 7 6.10 4.06 0 15 10 24.88 5.75 0 15 11 19.82 5.66 0 15 12 50.67 5.90 0 15 13 9.30 5.38 0 15 14 -1.16 4.62 1 -9 13 2.87 7.04 1 -7 1 44.32 5.58 1 -6 -1 1197.93 11.73 1 -4 24 1.76 8.53 1 -3 25 6.26 8.75 1 -1 -6 361.56 7.55 1 14 -4 80.01 6.56 1 15 -3 11.61 5.56 1 17 0 27.18 5.96 1 19 5 6.96 6.42 2 -10 0 590.78 8.18 2 -9 -2 149.06 5.77 2 -3 -9 121.69 5.79 2 9 -11 7.63 11.18 2 19 -3 20.18 7.04 3 -9 -6 70.10 5.53 3 -4 -11 3.21 5.18 3 3 -14 29.89 5.75 3 8 -14 15.59 9.15 4 -13 -1 -4.63 5.84 4 -10 -7 -0.83 5.17 4 -2 -14 3.98 5.74 4 0 -15 4.72 4.95 5 -11 -7 1.00 5.08 5 -4 -14 5.31 5.34 5 -2 -15 9.34 5.84 5 0 -16 10.21 5.35 0 -2 18 8.80 6.39 0 1 21 15.27 6.30 0 4 22 31.48 6.19 0 5 22 12.49 5.96 0 6 22 3.17 6.24 0 7 22 32.17 7.11 0 8 22 11.36 5.01 0 9 21 20.35 6.46 0 10 0 0.44 4.73 0 11 1 83.77 5.68 0 11 20 17.77 4.97 0 12 2 29.70 5.75 0 12 18 16.64 6.79 0 13 4 12.90 5.03 0 13 16 7.92 5.74 0 14 13 19.47 5.98 0 14 14 34.73 5.89 0 14 15 0.79 4.57 1 -8 3 9.46 4.84 1 18 3 13.58 6.00 1 19 6 46.55 5.10 1 19 7 16.05 6.44 1 19 8 11.25 6.38 2 -12 7 3.53 5.04 2 -12 8 0.47 5.33 2 -12 12 -4.78 5.57 2 -8 -4 20.39 4.78 2 18 -4 19.15 6.54 3 -14 7 6.97 5.06 3 -14 9 0.19 6.03 3 -14 10 3.04 6.27 3 -14 11 -2.11 6.17 3 -14 12 14.74 6.73 3 -14 13 2.70 7.84 3 -12 -1 43.14 5.97 3 -7 -9 65.93 5.14 3 -3 -12 45.84 5.47 3 2 -14 7.99 5.74 4 -15 5 -5.88 5.64 4 -14 1 1.94 6.36 4 -13 -2 9.92 5.86 4 -12 -4 -1.43 4.16 4 -7 -11 10.69 5.40 4 -3 -14 11.59 5.45 4 4 -16 2.30 6.91 4 5 -16 24.80 7.84 4 6 -16 5.47 7.36 5 -10 -9 2.38 5.10 5 -9 -10 6.81 5.65 5 -8 -11 -2.99 4.31 5 -7 -12 -4.65 5.23 5 -6 -13 4.18 5.49 0 -4 13 73.72 8.84 0 -3 16 26.37 6.58 0 -1 19 18.61 5.29 0 0 20 120.71 6.53 0 7 21 12.48 6.50 0 8 21 47.40 6.12 0 9 20 17.13 5.84 0 10 20 77.96 4.97 0 11 19 2.56 4.80 0 12 3 176.53 6.24 0 12 17 90.15 6.62 0 13 5 7.28 4.75 0 13 15 9.16 5.89 0 14 9 -1.33 3.81 0 14 10 4.83 4.73 1 -9 6 77.77 5.15 1 -9 14 3.13 6.92 1 -7 0 130.81 5.76 1 -5 -3 72.48 5.70 1 -4 -4 201.27 5.65 1 -3 -5 237.65 7.21 1 15 -2 32.06 4.97 1 17 1 95.43 5.86 1 18 4 9.38 5.74 2 -12 14 -0.80 5.54 2 -9 -3 43.53 4.96 2 -7 -6 100.00 5.12 2 -6 -7 765.91 9.09 2 -5 -8 83.78 5.21 2 -2 -10 7.69 4.49 2 0 -11 6.11 4.69 2 13 -9 37.94 6.44 2 19 -2 6.62 5.90 3 -14 5 -2.53 5.32 3 -14 6 2.95 6.01 3 -14 14 3.07 6.93 3 -13 1 12.37 5.38 3 -11 -4 13.98 4.83 3 -5 -11 34.07 5.14 4 -14 0 1.94 5.95 4 -12 -5 0.32 5.07 4 -5 -13 13.32 5.12 4 -1 -15 4.17 5.68 4 2 -16 3.75 6.95 4 3 -16 0.05 6.33 4 7 -16 4.97 7.36 5 -11 -8 1.70 5.50 5 -5 -14 4.22 5.39 5 -1 -16 6.28 5.53 0 1 20 70.34 6.03 0 3 21 29.17 5.60 0 4 21 32.48 5.81 0 5 21 8.35 6.10 0 6 21 19.26 5.72 0 8 20 25.44 5.65 0 10 19 -0.92 4.44 0 11 2 350.79 6.09 0 11 17 61.12 6.41 0 12 15 105.66 6.16 0 13 7 182.17 6.01 0 13 12 97.27 5.45 0 13 13 60.24 5.30 0 13 14 32.22 4.47 1 -2 -6 95.15 5.56 1 0 -7 -1.64 4.66 1 16 0 15.96 5.22 1 17 2 18.16 5.45 1 18 5 14.48 4.00 1 18 6 9.98 5.64 2 -12 15 5.44 6.79 2 -11 1 17.42 5.15 2 -10 21 0.72 11.41 2 -4 -9 5.20 4.61 2 14 -8 12.40 5.92 2 15 -7 0.27 6.17 2 16 -6 10.87 6.03 2 18 -3 4.78 5.79 2 19 -1 14.40 6.11 3 -13 0 2.72 5.08 3 -12 -2 8.51 3.94 3 -10 -6 60.55 5.18 3 -4 -12 32.05 5.42 4 -15 2 -0.41 6.00 4 -15 3 4.47 4.49 4 -14 -1 6.00 6.10 4 -8 -11 5.20 5.10 4 -4 -14 12.39 5.76 4 1 -16 4.29 5.26 4 8 -16 2.01 8.58 5 -10 -10 2.30 5.81 5 -9 -11 1.48 5.54 5 -8 -12 6.38 5.64 5 -7 -13 -3.22 5.25 5 -4 -15 -2.43 5.71 5 -2 -16 -2.26 5.48 0 -2 17 15.75 6.19 0 -1 18 49.13 6.66 0 0 19 6.21 5.36 0 6 -1 13.06 4.96 0 6 20 -1.35 6.14 0 7 20 -4.81 5.14 0 8 19 -0.04 5.13 0 9 19 6.63 4.18 0 10 17 12.91 5.59 0 10 18 3.05 4.30 0 11 3 314.07 6.77 0 11 16 113.46 6.18 0 12 5 14.70 4.63 0 12 6 25.35 4.93 0 12 13 35.23 5.27 0 12 14 19.65 5.27 0 13 10 1.52 3.57 1 -9 4 4.80 4.07 1 -9 15 13.40 7.78 1 -2 25 1.53 6.70 1 15 -1 3.57 4.86 1 16 1 83.19 5.75 1 17 3 15.03 4.02 1 17 4 -1.50 5.14 1 18 10 8.72 4.76 1 18 11 12.81 4.89 2 -11 0 128.07 5.87 2 -11 19 1.87 8.96 2 -10 -2 16.18 3.62 2 -3 -10 74.92 5.24 2 -1 -11 157.21 5.72 2 3 -12 63.42 6.28 3 -11 -5 -1.67 4.64 3 -9 -8 58.80 5.28 3 -7 -10 35.04 5.53 3 -6 -11 4.96 4.88 3 -3 -13 99.97 5.67 3 14 -11 14.89 8.36 3 17 -8 1.83 7.27 4 -15 1 6.14 5.68 4 -13 -4 4.30 3.89 4 -12 -6 -3.10 3.83 4 -10 -9 2.34 5.20 4 -9 -10 15.50 4.02 4 -6 -13 11.91 4.93 5 -6 -14 1.94 3.99 5 -5 -15 2.97 4.94 5 -3 -16 -2.18 5.17 0 1 19 20.55 5.48 0 3 20 8.99 5.24 0 5 20 15.58 4.39 0 7 19 17.11 5.42 0 8 18 65.69 5.83 0 9 18 3.58 4.01 0 10 16 91.52 5.73 0 11 14 4.39 5.09 0 11 15 32.78 3.97 0 12 8 30.72 4.93 0 12 10 7.63 4.70 0 12 11 329.00 6.24 0 12 12 43.54 3.87 1 -3 24 6.07 7.13 1 14 -2 -0.25 4.40 1 17 12 14.83 6.00 1 17 13 3.64 5.97 2 -12 2 1.20 4.42 2 -12 16 3.19 6.53 2 -7 -7 48.84 4.74 2 -6 -8 7.21 4.42 2 2 -12 8.00 5.54 2 6 -12 1.21 8.09 2 18 -2 9.27 5.57 3 -15 7 11.05 4.99 3 -15 9 0.64 5.62 3 -15 10 0.80 5.40 3 -15 11 -1.07 6.81 3 -14 2 29.12 4.38 3 -12 -4 12.36 4.50 3 -10 -7 10.87 4.65 3 -5 -12 52.95 5.40 3 15 -10 12.81 7.49 3 16 -9 -2.54 6.94 4 -15 0 -3.14 5.79 4 -13 -5 -0.54 5.22 4 -12 -7 13.41 4.71 4 -3 -15 2.86 5.46 4 -1 -16 1.68 4.88 0 -4 12 33.83 7.64 0 0 18 214.81 6.55 0 3 19 112.21 5.87 0 4 19 0.14 5.14 0 5 19 71.85 5.59 0 6 19 37.15 4.44 0 7 18 39.55 5.43 0 9 2 139.12 5.34 0 9 16 4.48 5.11 0 9 17 76.03 4.44 0 10 15 56.62 5.56 0 11 5 14.28 3.65 0 11 12 106.75 5.51 0 11 13 64.45 4.99 1 -10 9 1.34 5.41 1 -6 -3 290.12 6.52 1 -5 22 2.73 7.44 1 -4 -5 318.93 6.26 1 -4 23 0.09 6.56 1 -1 -7 448.23 8.52 1 -1 25 0.84 6.08 1 2 -8 626.70 12.66 1 17 8 10.25 5.13 1 17 9 27.40 5.05 1 17 10 11.48 5.37 2 -13 6 15.67 4.40 2 -13 7 -0.95 4.75 2 -13 8 5.09 4.90 2 -13 10 -0.47 4.91 2 -13 11 2.73 5.20 2 -13 12 7.02 6.09 2 -11 -1 10.36 3.39 2 -10 -3 108.67 4.08 2 -9 -5 104.61 4.91 2 -5 -9 84.85 4.25 2 -4 -10 14.38 4.35 2 -2 -11 93.91 4.95 2 18 -1 -1.78 5.64 2 19 1 7.30 5.55 3 -15 5 3.92 5.70 3 -15 6 -9.50 5.48 3 -15 12 -7.04 6.28 3 -11 -6 66.67 5.16 3 -9 -9 15.01 4.34 3 -8 -10 18.22 5.06 3 -2 -14 7.57 4.38 3 3 -15 22.44 6.14 3 4 -15 0.25 5.87 3 5 -15 36.99 7.24 4 -15 -1 3.19 6.09 4 -14 -4 11.67 4.95 4 -11 -9 -1.01 5.22 4 -9 -11 17.21 4.17 4 -8 -12 4.62 4.05 4 -7 -13 4.89 5.24 4 -4 -15 3.04 5.38 0 -2 16 13.93 5.05 0 -1 17 26.82 5.18 0 5 18 33.06 5.21 0 6 18 2.18 4.86 0 7 17 12.28 5.44 0 8 17 129.96 4.74 0 9 15 14.60 5.36 0 10 4 45.90 4.41 0 10 13 74.25 5.41 0 10 14 10.54 3.95 0 11 11 57.17 3.85 1 -10 7 9.09 4.39 1 -10 11 9.19 5.72 1 -3 -6 378.58 6.84 1 0 25 2.31 5.99 1 14 -1 38.43 4.63 1 15 16 32.48 5.83 1 15 17 0.70 4.43 1 16 4 9.01 4.55 1 16 5 52.74 5.13 1 16 13 -2.14 5.30 1 16 14 -0.72 4.20 2 -12 17 1.07 5.91 2 -10 -4 215.41 5.53 2 0 -12 770.21 9.53 2 14 -7 20.70 6.38 2 17 -3 4.10 4.94 2 19 2 0.87 4.55 2 19 3 7.54 5.69 3 -15 3 6.25 4.90 3 -15 4 18.33 5.90 3 -13 -3 21.48 5.06 3 -10 -8 -0.45 4.42 3 1 -15 19.10 5.36 3 2 -15 11.83 5.24 4 -6 -14 3.30 3.72 4 -2 -16 10.82 5.10 4 2 -17 10.71 5.84 4 3 -17 3.22 6.03 4 4 -17 10.36 6.07 4 5 -17 5.96 6.64 4 9 -16 3.26 9.10 0 0 17 4.99 5.50 0 3 18 128.72 5.86 0 4 18 256.86 6.59 0 6 0 14.13 4.59 0 6 17 30.43 5.20 0 7 1 314.10 7.20 0 8 15 216.81 5.78 0 8 16 6.54 3.49 0 9 3 190.54 4.70 0 10 5 190.66 4.39 0 10 12 116.61 4.01 1 -10 5 5.56 3.91 1 -10 6 707.73 8.54 1 -2 -7 130.82 5.49 1 -2 24 4.90 5.95 1 1 -8 45.36 5.39 1 1 25 0.71 6.30 1 3 25 -3.06 6.20 1 4 25 -4.15 6.13 1 13 -2 26.73 4.44 1 13 19 52.94 6.34 1 14 17 5.81 5.49 1 14 18 11.87 4.21 1 15 2 105.78 5.28 1 15 15 8.21 5.41 1 16 7 14.98 5.44 1 16 8 19.20 5.53 1 16 9 34.02 5.55 1 16 10 24.10 5.34 1 16 12 2.61 4.14 2 -13 3 39.91 4.56 2 -13 4 19.61 3.58 2 -8 -7 2.27 4.43 2 -7 -8 6.15 3.33 2 -6 -9 287.45 6.42 2 -3 -11 113.77 5.48 2 13 -8 4.47 4.67 2 16 -4 49.40 5.45 2 17 -2 -0.78 5.25 2 18 0 27.69 5.25 2 19 4 7.00 5.25 2 19 5 -2.81 5.76 3 -15 2 5.07 5.17 3 -14 -1 1.44 3.80 3 -13 -4 12.08 4.42 3 -11 -7 23.71 3.56 3 -5 -13 31.41 4.84 3 0 -15 0.98 4.97 3 6 -15 2.89 7.22 3 17 -7 -2.03 5.83 4 -14 -5 1.36 3.97 4 -11 -10 4.06 5.13 4 -10 -11 -0.99 3.95 4 -9 -12 21.51 4.19 4 -8 -13 8.03 5.03 4 -5 -15 42.01 6.05 4 -3 -16 0.41 5.02 4 0 -17 1.26 5.03 4 1 -17 3.74 5.37 4 6 -17 0.77 7.66 0 -4 11 121.15 10.67 0 -2 15 81.79 6.37 0 -1 16 30.29 5.23 0 4 17 30.05 5.11 0 5 17 77.97 5.40 0 6 16 60.39 5.14 0 7 16 63.78 4.03 0 8 14 94.68 5.12 0 9 12 46.62 4.94 0 9 13 83.99 3.95 1 -10 4 118.13 4.93 1 -6 -4 820.72 8.88 1 -4 -6 1457.13 11.65 1 -3 23 6.69 6.79 1 -1 24 4.55 6.28 1 6 24 -1.30 6.03 1 7 24 5.14 5.61 1 10 22 2.09 5.50 1 11 21 -2.11 5.03 1 12 -3 247.66 5.66 1 12 20 1.34 4.50 1 13 18 8.23 5.68 1 14 16 12.01 5.51 1 15 3 16.38 4.67 1 15 13 17.57 5.05 1 15 14 64.54 4.24 2 -13 2 10.21 4.55 2 -11 -3 4.57 3.26 2 -10 -5 7.44 4.24 2 -1 -12 404.94 7.14 3 -16 9 3.57 5.13 3 -15 1 -1.98 5.09 3 -14 -2 88.74 4.91 3 -12 -6 4.62 3.19 3 -11 -8 17.57 4.38 3 -10 -9 34.68 4.78 3 -4 -14 59.09 4.56 3 -1 -15 23.02 4.93 3 16 -8 5.36 6.57 4 -15 -4 1.62 5.63 4 -12 -9 -0.21 4.00 4 -7 -14 9.54 3.70 4 -6 -15 -1.05 4.87 4 -4 -16 3.19 5.56 4 -1 -17 0.83 5.60 0 0 16 86.23 6.02 0 2 17 13.49 4.47 0 3 17 24.91 3.75 0 5 16 70.76 5.28 0 6 15 89.40 5.52 0 7 2 473.11 7.93 0 7 14 26.74 4.78 0 7 15 26.45 3.53 0 8 13 41.07 4.75 1 -10 3 144.15 5.04 1 -10 13 1.28 5.35 1 0 -8 333.21 7.85 1 0 24 10.64 5.67 1 4 24 -0.65 5.66 1 5 24 6.04 5.84 1 7 23 2.81 5.79 1 8 23 0.66 4.36 1 9 22 7.85 5.84 1 10 21 2.19 5.25 1 11 20 29.53 5.85 1 12 19 27.79 5.19 1 13 -1 23.33 4.34 1 14 15 7.83 4.92 1 15 8 10.40 4.84 1 15 9 2.75 4.94 1 15 10 159.99 5.84 1 15 11 42.53 4.69 1 15 12 33.54 3.96 2 -14 7 -1.77 4.11 2 -14 9 -3.83 5.15 2 -13 1 59.94 5.05 2 -13 15 -2.51 6.60 2 -12 -2 29.81 4.17 2 -11 -4 33.90 4.40 2 -11 20 -2.26 11.17 2 -8 -8 23.85 4.49 2 -4 -11 46.63 4.79 2 -2 -12 10.78 4.11 2 15 -5 41.89 5.18 2 16 -3 5.45 4.63 2 17 -1 32.18 4.88 2 18 2 6.61 4.00 2 18 3 18.45 5.50 3 -16 4 -3.39 4.99 3 -16 6 3.38 5.72 3 -16 10 7.46 6.09 3 -15 0 8.55 5.10 3 -13 -5 50.91 4.17 3 -12 -7 8.76 4.73 3 -2 -15 15.87 4.47 3 12 -12 2.67 8.06 3 15 -9 5.94 6.65 4 -15 -5 0.30 4.89 4 -11 -11 6.94 5.34 4 -10 -12 5.78 4.12 4 -9 -13 44.84 5.61 4 -8 -14 4.80 4.87 4 -2 -17 11.50 5.66 0 -3 13 66.17 6.28 0 -1 15 37.18 5.75 0 2 16 21.90 4.56 0 3 16 43.29 5.00 0 4 16 35.98 4.70 0 5 15 53.42 5.24 0 6 14 11.62 5.03 0 7 13 6.13 4.77 0 8 12 10.26 3.50 1 -7 19 3.95 9.15 1 -4 22 4.10 5.75 1 -3 -7 267.88 6.62 1 -2 23 72.24 6.86 1 -1 -8 55.25 4.96 1 1 24 5.92 5.58 1 3 24 6.34 5.39 1 6 23 5.13 5.38 1 8 22 17.04 5.68 1 9 21 2.51 5.35 1 11 19 0.14 5.33 1 12 -2 18.89 4.10 1 12 18 8.27 4.87 1 13 0 88.60 4.99 1 13 16 1.65 5.21 1 14 13 20.17 4.65 1 14 14 47.70 3.96 2 -14 5 6.96 4.57 2 -14 6 9.92 4.73 2 -14 10 25.50 5.64 2 -13 0 45.72 4.81 2 10 -10 254.57 9.71 2 14 -6 22.40 4.93 2 17 0 24.00 4.87 2 18 4 46.26 4.43 2 18 5 19.14 5.50 2 18 6 7.67 5.24 2 18 7 -5.16 5.28 2 18 8 34.62 5.66 2 18 9 -1.43 5.75 3 -15 -1 4.24 5.11 3 -14 -4 7.68 4.88 3 -11 -9 3.63 4.29 3 -10 -10 107.04 5.50 3 -5 -14 32.68 4.82 3 -3 -15 28.11 4.45 3 7 -15 4.80 7.87 3 13 -11 18.17 7.40 3 17 -6 5.29 5.70 4 -13 -9 -1.12 4.98 4 -7 -15 6.27 5.00 4 -5 -16 12.06 4.61 4 -3 -17 -6.04 5.13 4 7 -17 -0.21 7.03 0 0 15 1.78 5.15 0 4 15 39.64 4.99 0 5 14 207.98 6.03 0 6 2 1108.91 10.81 0 6 13 289.37 6.30 0 7 12 256.75 6.16 1 -11 7 77.48 5.39 1 -11 8 15.61 5.18 1 -7 -4 319.93 6.13 1 -6 -5 61.09 3.45 1 -6 20 14.71 7.75 1 -5 -6 427.53 7.13 1 -5 21 8.51 6.60 1 -1 23 25.34 6.43 1 5 23 0.61 5.54 1 7 22 16.72 5.45 1 11 18 2.01 5.44 1 12 17 36.39 5.00 1 13 15 75.45 5.28 1 14 4 10.08 4.59 1 14 5 19.93 4.61 1 14 12 24.75 3.56 2 -14 3 1.12 4.45 2 -14 12 1.41 5.29 2 -13 16 1.14 5.73 2 -11 -5 3.55 4.07 2 -5 -11 197.66 5.83 2 -3 -12 77.28 5.01 2 1 -13 237.94 6.49 2 3 -13 6.92 5.14 2 13 -7 8.29 4.34 2 15 -4 55.94 4.91 2 16 -2 38.73 5.05 2 17 1 48.98 4.97 3 -16 1 2.16 5.08 3 -15 -2 49.34 5.57 3 -12 -8 2.00 4.62 3 -7 -13 9.56 3.65 3 1 -16 11.18 5.06 3 2 -16 -3.00 4.64 3 3 -16 10.18 5.47 3 16 -7 30.25 7.32 4 -15 -6 0.15 4.21 4 -12 -11 -3.01 5.41 4 -10 -13 13.11 5.74 4 -9 -14 6.56 5.73 4 -6 -16 12.45 5.59 4 -4 -17 14.49 5.07 4 0 -18 19.97 6.55 4 1 -18 8.46 5.81 4 3 -18 -0.59 6.52 0 2 15 108.81 5.32 0 3 15 114.14 4.44 0 4 14 232.05 6.11 0 5 13 53.39 5.08 0 6 12 96.71 5.24 0 7 11 124.21 4.11 1 -11 5 2.27 3.87 1 -11 6 15.06 4.07 1 -11 9 4.82 4.45 1 -10 1 8.58 4.31 1 -10 14 22.85 6.66 1 -4 -7 26.38 4.58 1 -3 22 -1.51 6.28 1 -2 -8 877.71 9.87 1 0 23 1.58 5.40 1 1 23 25.79 5.46 1 3 23 14.23 5.77 1 4 23 2.63 4.85 1 6 22 10.16 5.63 1 8 21 9.09 4.02 1 9 20 10.77 4.60 1 10 19 -5.84 4.94 1 12 -1 -0.30 4.13 1 13 1 169.70 4.43 1 13 13 9.24 4.41 1 13 14 4.47 3.65 1 14 6 101.93 4.16 1 14 8 14.35 4.47 2 -14 13 5.39 6.58 2 -13 -2 33.27 4.56 2 -12 -4 9.51 4.61 2 -8 -9 363.86 5.83 2 -4 -12 659.14 7.88 2 -1 -13 257.71 5.99 2 0 -13 -1.50 4.03 2 12 -8 2.95 4.50 2 16 -1 51.61 4.99 2 17 2 41.27 4.24 2 17 3 9.60 5.00 2 17 11 1.28 5.86 3 -17 6 2.07 5.15 3 -17 7 7.60 5.28 3 -16 0 0.03 4.76 3 -15 -3 2.00 5.06 3 -14 -5 1.77 3.48 3 -11 -10 52.33 4.80 3 -8 -13 12.76 4.19 3 -6 -14 3.27 3.41 3 -4 -15 -0.32 4.37 3 -1 -16 10.58 5.23 3 0 -16 0.75 4.96 3 4 -16 7.56 5.53 3 17 -5 -0.53 5.99 4 -15 -7 0.88 5.44 4 -14 -9 4.47 4.74 4 -13 -10 2.46 3.79 4 -8 -15 1.70 3.71 4 -1 -18 -0.12 5.84 0 -4 10 36.53 8.97 0 -3 2 63.63 8.27 0 -3 12 39.94 6.10 0 -2 1 34.87 6.89 0 0 14 276.13 7.58 0 2 0 1.99 5.46 0 2 14 0.64 4.38 0 3 14 82.67 5.10 0 4 1 428.00 8.90 0 4 13 121.59 5.49 0 5 2 51.55 5.59 0 5 12 16.30 4.61 1 -10 0 526.66 7.06 1 -9 -2 95.26 4.78 1 -7 -5 346.36 6.10 1 -6 -6 24.10 3.99 1 5 22 0.99 5.42 1 7 21 10.82 4.97 1 8 20 14.29 4.92 1 9 19 35.45 5.31 1 10 18 16.45 5.37 1 12 15 64.15 4.02 1 13 2 59.41 3.63 1 13 3 38.09 4.46 1 13 12 3.33 3.17 2 -14 0 175.40 5.72 2 -14 1 4.77 3.28 2 -11 -6 25.33 3.11 2 -6 -11 101.20 4.12 2 -2 -13 30.07 4.42 2 4 -13 166.98 7.42 2 14 -5 16.99 4.78 2 15 -3 11.39 4.49 2 16 0 23.73 4.89 2 17 4 -0.63 3.80 2 17 5 41.31 4.84 2 17 6 16.18 4.87 2 17 7 2.11 5.13 2 17 8 10.63 5.38 2 17 9 27.64 5.22 2 17 10 -3.30 4.24 3 -17 4 -1.18 5.67 3 -17 5 1.29 5.68 3 -16 -1 45.41 5.20 3 -15 -4 16.49 5.17 3 -13 -8 8.27 4.74 3 -12 -9 8.87 3.40 3 -7 -14 9.12 4.78 3 -5 -15 41.01 5.04 3 -2 -16 -1.11 4.65 3 15 -8 8.97 6.14 3 18 -2 8.12 5.87 4 -13 -11 10.37 5.73 4 -12 -12 8.18 5.29 4 -11 -13 7.10 5.73 4 -10 -14 2.78 5.81 4 -9 -15 12.78 5.17 4 -7 -16 7.57 3.86 4 -5 -17 10.01 4.26 4 -2 -18 32.02 5.65 4 5 -18 3.81 6.73 0 3 13 127.64 5.28 0 6 5 61.94 4.99 0 6 8 39.80 4.64 0 6 9 705.55 8.10 1 -11 2 136.73 5.12 1 -10 -1 34.56 4.18 1 -8 -4 19.83 4.16 1 -4 21 4.52 5.74 1 -3 -8 55.07 5.01 1 -2 22 -0.19 5.31 1 3 22 12.27 4.91 1 4 22 6.69 4.64 1 6 21 37.27 5.44 1 7 20 11.97 4.89 1 10 17 -3.89 4.94 1 11 -2 106.00 4.79 1 11 16 30.08 3.59 1 12 0 77.74 3.67 1 12 13 1.22 4.29 1 12 14 8.24 3.28 1 13 4 13.22 4.00 1 13 5 112.63 4.74 1 13 6 69.70 4.90 1 13 7 139.32 5.28 1 13 9 56.08 4.88 1 13 10 17.85 3.15 2 -15 4 93.66 5.78 2 -15 6 28.94 4.75 2 -15 7 1.16 4.38 2 -15 9 2.85 4.99 2 -14 -1 8.03 4.33 2 -12 -5 312.24 5.02 2 -11 -7 26.70 4.14 2 -10 -8 2.09 3.91 2 -8 -10 6.60 4.39 2 -7 -11 116.35 4.77 2 -5 -12 30.77 4.76 2 -3 -13 3.80 4.04 2 13 -6 16.64 5.72 2 15 -2 9.89 4.60 2 16 1 11.90 4.97 2 16 12 0.01 5.13 2 16 13 21.99 4.31 3 -17 1 0.16 4.89 3 -17 2 -4.60 5.62 3 -16 -2 9.18 5.41 3 -15 -5 15.83 5.02 3 -12 -10 5.78 4.31 3 -11 -11 36.17 4.94 3 -10 -12 15.49 4.80 3 -9 -13 26.35 4.81 3 -6 -15 -2.22 4.28 3 -3 -16 13.37 4.76 3 5 -16 9.97 5.80 3 16 -6 7.53 5.25 3 17 -4 8.23 5.48 3 18 -1 13.31 5.36 4 -8 -16 2.37 5.21 4 -6 -17 10.68 5.28 4 -4 -18 26.42 5.08 4 -3 -18 0.23 3.94 4 8 -17 8.58 8.86 0 5 3 75.00 5.34 0 6 7 48.89 3.36 1 -11 1 15.98 4.22 1 -11 12 13.73 5.59 1 -9 -3 221.67 4.42 1 -4 -8 198.07 5.47 1 -1 22 5.54 5.36 1 0 -9 1.02 4.29 1 0 22 23.88 5.52 1 2 22 6.65 4.90 1 5 21 17.39 5.49 1 8 19 13.18 3.51 1 10 -3 37.18 4.82 1 10 16 52.44 4.91 1 11 14 109.67 4.95 1 11 15 27.03 3.74 1 12 1 260.65 5.65 1 12 11 175.70 5.29 1 12 12 5.53 3.99 2 -15 2 5.07 4.64 2 -15 3 17.80 5.14 2 -15 11 0.11 5.74 2 -14 -2 -4.41 4.25 2 -13 -4 79.27 4.91 2 -12 -6 39.13 4.55 2 -12 19 3.63 10.09 2 -6 -12 4.03 4.15 2 14 -4 52.46 4.81 2 14 17 3.19 4.99 2 15 14 2.47 5.06 2 15 15 5.25 3.87 2 16 2 12.56 4.62 2 16 3 68.33 4.95 2 16 11 6.67 3.74 3 -17 0 6.98 5.33 3 -16 -3 20.80 4.19 3 -15 -6 54.73 4.94 3 -13 -9 -3.54 4.37 3 -8 -14 14.26 4.84 3 -4 -16 8.08 4.87 3 14 -9 -0.07 5.62 3 17 -3 5.36 5.30 3 18 0 4.08 5.45 4 -13 -12 5.77 5.54 4 -12 -13 10.23 4.30 4 -11 -14 6.42 4.20 4 -10 -15 7.05 5.49 4 -7 -17 8.59 5.57 4 -5 -18 12.95 5.10 4 6 -18 5.67 7.40 0 -3 11 59.14 6.87 0 -2 12 18.55 4.77 0 3 1 448.60 10.21 0 4 2 4.32 3.43 0 4 10 100.55 5.04 0 5 4 478.91 7.27 0 5 5 459.00 7.93 0 5 6 280.24 6.60 0 5 7 148.55 5.67 0 5 8 49.01 4.72 0 5 9 40.15 3.63 1 -12 5 214.06 5.24 1 -12 6 26.57 3.99 1 -12 7 72.27 4.90 1 -12 8 24.95 5.04 1 -11 0 18.76 4.08 1 -10 -2 0.14 4.25 1 -9 -4 82.64 4.37 1 -8 -5 141.97 4.74 1 -7 -6 122.48 3.84 1 -6 -7 140.51 5.07 1 -3 21 4.68 5.66 1 -2 -9 756.25 8.51 1 -1 -9 21.96 4.56 1 4 21 6.30 4.64 1 6 20 25.86 3.81 1 7 19 9.19 4.57 1 8 18 15.23 4.69 1 9 17 2.53 4.39 1 10 15 4.76 4.57 1 11 -1 33.13 3.93 1 11 13 21.83 4.26 1 12 2 97.84 3.89 1 12 3 22.29 4.43 1 12 9 213.27 5.22 1 12 10 12.43 4.27 2 -15 1 36.94 4.71 2 -15 12 -0.97 5.70 2 -14 15 2.40 6.26 2 -13 -5 196.78 5.46 2 -11 -8 78.26 4.63 2 -10 -9 -6.97 4.26 2 -9 -10 -5.59 4.45 2 -8 -11 135.63 5.00 2 -4 -13 226.26 4.91 2 5 -13 10.54 6.04 2 12 -7 0.49 5.04 2 13 18 0.65 5.07 2 14 16 -1.91 4.67 2 15 -1 1.45 4.00 2 15 13 14.58 5.03 2 16 5 43.66 4.58 2 16 6 2.85 4.37 2 16 7 -0.18 4.56 2 16 8 11.93 3.82 2 16 9 49.67 4.15 3 -17 -1 9.61 5.13 3 -16 -4 4.89 3.91 3 -14 -8 4.98 3.40 3 -12 -11 70.90 4.97 3 -11 -12 62.31 5.30 3 -10 -13 44.14 5.20 3 -7 -15 12.60 4.67 3 -5 -16 15.57 4.94 3 -1 -17 67.04 5.35 3 0 -17 -3.08 4.72 3 1 -17 70.40 5.41 3 2 -17 22.74 5.83 3 15 -7 5.84 6.36 3 16 -5 13.61 5.82 3 18 2 7.14 5.79 4 -9 -16 4.12 4.04 4 -2 -19 29.53 5.71 4 -1 -19 10.81 5.79 4 0 -19 -6.65 5.81 4 1 -19 8.32 5.67 4 2 -19 29.77 6.00 0 -1 12 49.00 5.42 0 4 3 506.16 8.79 0 4 9 647.03 8.22 1 -12 4 3.13 3.70 1 -11 13 18.25 6.21 1 -10 -3 34.47 4.03 1 -5 -8 6.56 3.80 1 -3 -9 125.08 4.93 1 -2 21 73.99 6.31 1 2 21 78.47 5.11 1 5 20 33.52 4.72 1 6 19 63.48 4.98 1 8 17 20.34 4.46 1 9 -4 84.31 4.84 1 9 16 28.09 4.90 1 11 0 17.41 4.22 1 11 12 20.90 4.37 1 12 4 3.03 2.98 1 12 5 226.10 5.18 1 12 6 28.47 4.31 1 12 7 107.27 4.40 2 -15 -1 -1.32 4.32 2 -15 0 126.84 4.49 2 -14 -3 -0.56 3.32 2 -12 -7 6.70 4.17 2 -7 -12 13.34 4.31 2 -5 -13 8.45 4.52 2 -2 -14 26.61 4.19 2 -1 -14 79.70 4.66 2 0 -14 0.88 4.05 2 1 -14 73.52 5.12 2 2 -14 23.00 5.36 2 10 21 -4.54 5.43 2 11 20 -0.63 5.58 2 12 19 6.19 4.22 2 13 -5 189.19 5.72 2 13 17 5.72 4.83 2 14 -3 3.54 4.28 2 14 15 -2.03 3.59 2 15 0 143.27 5.18 2 15 1 43.83 4.85 2 15 11 -0.31 4.80 2 15 12 0.59 3.69 3 -18 2 21.99 5.55 3 -16 -5 5.13 5.39 3 -15 -7 2.98 3.42 3 -14 -9 3.23 4.65 3 -13 -10 19.58 3.59 3 -9 -14 -6.10 3.59 3 -8 -15 76.36 5.22 3 -6 -16 31.72 4.69 3 -3 -17 30.86 4.83 3 -2 -17 19.65 4.77 3 3 -17 30.93 5.63 3 6 -16 35.36 7.52 3 13 -10 6.85 5.48 3 17 -2 2.01 4.62 4 -11 -15 -0.36 4.15 4 -10 -16 0.22 5.27 4 -8 -17 20.52 4.21 4 -6 -18 16.47 4.17 4 -3 -19 6.53 5.40 4 3 -19 6.08 6.12 0 -4 2 5.72 6.60 0 -3 1 532.56 12.63 0 2 11 491.28 7.64 0 3 2 70.75 6.08 0 3 10 186.35 5.98 0 4 4 542.09 8.57 0 4 5 49.81 4.86 0 4 6 340.45 7.12 0 4 7 1138.52 10.78 0 4 8 50.33 4.81 1 -12 2 116.25 4.88 1 -12 10 6.85 5.45 1 -11 -1 32.84 3.30 1 -9 -5 79.18 4.29 1 -8 -6 134.01 4.68 1 -7 -7 74.90 4.46 1 -6 19 56.44 7.60 1 -1 21 8.36 5.10 1 0 21 -1.78 4.77 1 3 -9 104.60 8.10 1 4 20 7.23 4.36 1 7 18 13.47 3.46 1 9 15 21.01 4.62 1 10 -2 0.31 3.86 1 10 13 4.79 4.31 1 11 1 23.58 4.14 1 11 10 117.46 4.76 1 11 11 39.01 3.24 2 -16 3 54.13 5.28 2 -16 4 11.84 4.69 2 -16 5 32.90 4.84 2 -16 6 2.97 4.44 2 -16 7 0.13 4.78 2 -16 8 9.26 4.99 2 -15 -2 12.74 4.20 2 -15 13 3.23 5.40 2 -14 -4 44.60 3.65 2 -13 -6 19.72 3.23 2 -12 -8 2.64 3.85 2 -11 -9 41.90 4.55 2 -10 -10 284.10 5.94 2 -9 -11 3.43 4.48 2 -6 -13 56.53 4.73 2 -3 -14 0.82 4.04 2 11 -8 76.11 4.95 2 11 19 4.55 5.27 2 12 18 -6.87 4.90 2 13 16 2.97 4.93 2 14 -2 -0.46 3.97 2 14 13 6.97 4.80 2 14 14 22.10 3.94 2 15 2 1.82 4.41 2 15 3 23.41 4.51 2 15 8 37.77 5.13 2 15 9 9.73 4.88 2 15 10 59.41 3.96 3 -18 0 -1.48 5.43 3 -18 1 19.74 4.01 3 -17 -4 0.95 5.03 3 -17 -3 2.99 3.91 3 -16 -6 -1.28 5.27 3 -15 -8 4.84 5.05 3 -13 -11 38.68 5.26 3 -12 -12 3.03 4.78 3 -11 -13 38.08 5.15 3 -10 -14 56.64 5.33 3 -7 -16 41.72 4.40 3 -4 -17 9.60 4.92 3 12 -11 68.39 7.25 3 16 -4 -0.28 5.03 3 17 -1 4.34 4.59 3 17 0 8.15 5.34 4 -9 -17 42.60 5.79 4 -7 -18 10.11 5.53 4 -5 -19 9.18 4.95 4 -4 -19 -2.15 4.04 4 4 -19 3.20 6.65 0 -5 4 462.59 11.08 0 -3 10 133.00 9.13 0 -1 11 0.37 5.67 0 2 1 33.48 4.71 0 2 10 66.99 5.22 0 3 9 888.28 9.99 1 -12 0 121.51 4.76 1 -12 1 277.80 4.80 1 -12 11 173.30 6.59 1 -11 -2 125.29 4.92 1 -10 -4 491.88 6.29 1 -6 -8 492.65 5.90 1 -4 -9 64.88 3.43 1 -4 20 2.14 5.18 1 2 20 7.60 5.13 1 3 20 11.34 4.28 1 5 19 13.38 3.37 1 6 18 8.00 4.59 1 7 -6 104.25 6.44 1 7 17 45.65 4.65 1 8 16 20.13 4.41 1 9 14 10.54 4.51 1 10 -1 32.77 3.89 1 10 12 134.25 4.68 1 11 2 145.06 4.77 1 11 3 83.27 4.62 2 -16 1 6.78 4.46 2 -16 2 12.93 3.69 2 -16 10 9.13 5.14 2 -15 -3 13.51 4.49 2 -14 -5 18.48 4.56 2 -13 -7 11.16 4.33 2 -4 -14 108.01 5.40 2 3 -14 2.99 4.92 2 8 -11 128.07 9.47 2 8 22 14.26 4.89 2 9 21 -0.28 5.53 2 10 -9 5.57 5.30 2 10 20 12.35 4.88 2 12 -6 34.92 5.08 2 12 17 9.45 5.17 2 13 -4 77.80 4.73 2 14 -1 2.39 4.16 2 14 12 15.93 4.73 2 15 4 103.02 3.98 2 15 5 30.64 4.21 2 15 6 35.61 4.41 2 15 7 4.26 3.61 3 -18 -1 9.15 5.57 3 -17 -5 1.27 4.81 3 -16 -7 76.42 5.58 3 -15 -9 4.95 4.56 3 -14 -10 41.14 3.82 3 -9 -15 30.37 5.01 3 -5 -17 4.44 5.18 3 4 -17 3.60 5.86 3 14 -8 5.70 4.80 3 15 -6 70.09 5.41 3 16 -3 29.41 5.04 3 17 1 6.88 5.03 4 -6 -19 12.82 5.35 0 -5 3 79.82 6.23 0 -2 0 3.11 6.15 0 2 9 998.11 10.75 0 3 3 71.55 4.89 0 3 4 146.02 6.36 0 3 7 96.83 6.07 0 3 8 236.12 5.84 1 -13 4 17.37 3.82 1 -13 5 109.36 4.65 1 -13 6 52.52 4.42 1 -12 -1 8.05 3.98 1 -11 -3 130.99 4.85 1 -9 -6 84.37 4.24 1 -8 -7 77.81 4.23 1 -5 -9 52.69 4.30 1 -3 20 10.19 5.39 1 4 19 62.74 4.80 1 5 18 8.62 4.31 1 8 15 48.84 4.53 1 9 -3 219.78 5.56 1 9 13 11.46 4.03 1 11 4 75.48 3.48 1 11 5 4.85 2.98 1 11 6 16.28 3.23 1 11 7 85.98 3.32 2 -16 -1 50.46 4.27 2 -16 0 21.45 3.26 2 -16 11 10.96 4.84 2 -15 -4 55.29 4.49 2 -15 14 1.75 5.41 2 -14 -6 25.10 4.47 2 -13 18 7.21 7.94 2 -12 -9 204.95 5.43 2 -11 -10 82.07 4.64 2 -10 -11 29.65 4.35 2 -9 -12 63.95 4.77 2 -5 -14 44.95 4.43 2 4 24 1.33 4.81 2 6 23 0.87 5.05 2 7 22 13.51 5.28 2 9 -10 3.02 5.74 2 10 19 2.61 5.22 2 11 18 11.65 3.80 2 12 16 -1.07 4.70 2 13 14 13.47 4.28 2 14 0 222.14 5.18 2 14 10 35.28 4.66 2 14 11 11.66 4.13 3 -18 -2 11.88 4.45 3 -17 -6 1.40 4.78 3 -16 -8 6.77 4.39 3 -14 -11 39.15 4.97 3 -13 -12 16.06 5.03 3 -12 -13 3.14 3.65 3 -11 -14 5.34 4.77 3 -10 -15 9.54 4.81 3 -8 -16 55.77 4.99 3 -6 -17 39.07 5.26 3 -2 -18 2.33 4.20 3 -1 -18 59.29 4.41 3 0 -18 46.21 5.79 3 10 -13 35.75 7.79 3 11 -12 59.43 6.91 3 17 2 2.82 3.83 3 17 3 31.88 4.81 3 17 4 -7.28 5.13 3 17 5 4.77 5.15 3 17 6 11.06 5.22 3 17 7 14.03 4.67 4 -3 -20 11.73 5.62 4 -2 -20 2.53 5.78 4 -1 -20 2.17 5.69 4 0 -20 44.64 6.30 4 1 -20 6.15 4.92 4 5 -19 2.82 6.92 4 7 -18 2.61 7.87 0 -4 1 454.87 10.01 0 -1 10 392.45 9.73 0 2 2 148.87 7.20 0 2 8 2.77 4.47 0 3 5 561.28 8.78 0 3 6 127.15 5.16 1 -13 2 70.66 4.35 1 -13 3 32.67 4.07 1 -13 7 117.56 4.86 1 -13 8 29.02 4.51 1 -12 -2 24.16 4.01 1 -11 -4 372.48 5.77 1 -11 14 95.59 7.99 1 -10 -5 42.07 2.87 1 -7 18 9.88 6.73 1 -6 -9 76.78 4.16 1 -3 -10 196.99 5.33 1 -2 -10 15.05 2.88 1 -2 20 2.85 4.40 1 -1 20 24.98 4.64 1 0 -10 541.95 8.31 1 0 20 7.89 4.50 1 3 19 21.07 4.30 1 6 17 64.34 4.38 1 7 16 22.48 3.08 1 8 14 104.73 4.69 1 9 12 72.10 4.14 1 10 0 494.96 5.80 1 10 1 12.52 3.93 2 -17 3 1.07 4.06 2 -17 4 1.05 4.27 2 -17 5 45.73 4.69 2 -17 6 11.22 4.21 2 -16 -2 47.94 4.69 2 -16 12 4.18 5.36 2 -15 -5 52.09 4.51 2 -14 -7 20.85 4.02 2 -13 -8 3.74 2.84 2 -8 -13 24.63 4.31 2 -6 -14 43.17 4.36 2 -3 -15 16.34 3.78 2 -1 -15 10.62 3.89 2 0 -15 3.53 4.56 2 2 24 -4.03 5.05 2 3 24 -1.53 4.52 2 5 23 28.60 5.53 2 8 21 2.48 3.67 2 9 20 1.08 3.73 2 11 17 2.38 4.65 2 12 15 16.76 4.53 2 13 -3 54.87 4.25 2 13 13 47.46 4.33 2 14 1 5.08 4.07 2 14 2 75.49 4.43 2 14 8 52.19 4.50 2 14 9 6.96 4.03 3 -15 -10 33.69 5.03 3 -9 -16 6.89 4.46 3 -7 -17 8.77 4.62 3 -3 -18 43.43 4.81 3 1 -18 63.56 5.46 3 13 -9 5.47 5.09 3 14 -7 23.47 5.88 3 15 -5 31.55 4.66 3 16 -2 13.94 4.43 3 16 -1 56.35 5.10 4 2 -20 5.27 5.50 0 -5 2 56.88 5.44 0 -3 0 652.14 11.56 0 2 7 70.72 5.20 1 -13 0 106.35 4.39 1 -13 1 234.28 5.36 1 -13 9 63.44 4.66 1 -12 12 0.83 5.16 1 -10 -6 94.44 4.33 1 -9 -7 226.16 4.84 1 -8 -8 66.09 4.11 1 -5 19 17.82 5.42 1 -4 -10 437.64 6.39 1 1 -10 126.80 5.62 1 2 19 56.27 4.33 1 4 18 66.05 4.47 1 5 17 96.70 4.69 1 6 16 54.92 4.43 1 7 15 41.81 4.34 1 8 -4 16.99 3.76 1 9 -2 106.19 4.35 1 10 2 499.30 6.26 2 -17 1 52.68 5.40 2 -17 2 37.11 5.02 2 -17 7 2.19 4.70 2 -17 8 8.71 5.00 2 -16 -3 6.66 4.45 2 -15 15 0.33 5.62 2 -13 -9 49.31 4.07 2 -12 -10 15.66 2.95 2 -10 -12 7.24 4.33 2 -9 -13 37.75 4.21 2 -7 -14 96.79 4.71 2 -4 -15 31.13 4.41 2 -4 24 0.22 5.89 2 1 -15 7.11 4.03 2 1 24 12.66 5.29 2 4 -14 94.57 6.51 2 4 23 5.55 5.10 2 6 22 3.82 4.46 2 7 21 16.28 5.01 2 8 20 7.43 4.48 2 9 19 14.78 5.07 2 10 18 23.83 3.93 2 11 -7 34.30 4.33 2 11 16 9.26 4.44 2 12 -5 357.46 6.16 2 12 14 2.38 4.31 2 13 -2 54.14 4.03 2 13 11 5.91 4.16 2 13 12 12.37 3.32 2 14 3 5.72 3.81 2 14 4 96.60 4.37 2 14 5 6.45 3.85 2 14 6 8.32 3.78 2 14 7 0.62 3.00 3 -17 -7 5.22 4.00 3 -16 -9 0.75 3.66 3 -15 -11 15.37 4.68 3 -14 -12 49.60 4.86 3 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38.06 4.35 2 13 -1 243.05 5.16 2 13 10 2.12 4.15 3 -16 -10 7.87 5.06 3 -14 -13 15.57 4.31 3 -13 -14 7.02 4.44 3 -10 -16 77.44 4.04 3 -9 -17 19.19 4.29 3 -6 -18 3.17 4.87 3 5 -17 13.36 6.31 3 15 12 8.20 5.19 3 16 1 7.66 4.54 3 16 2 22.93 5.00 3 16 3 89.88 5.41 3 16 4 -1.31 4.69 3 16 5 59.65 4.92 3 16 6 10.90 4.68 3 16 7 14.20 4.46 3 16 8 31.57 3.85 4 13 -12 6.46 6.20 0 -6 2 1375.97 12.91 0 -3 9 855.87 17.75 0 -2 9 976.66 15.36 0 -1 9 257.53 7.95 1 -14 2 137.92 4.65 1 -14 3 29.74 3.83 1 -14 4 14.54 3.87 1 -14 5 27.36 4.21 1 -14 6 135.45 5.13 1 -14 7 69.30 5.21 1 -13 -2 40.38 4.05 1 -12 -4 114.14 3.52 1 -11 -6 80.02 4.19 1 -10 -7 30.38 2.85 1 -9 -8 226.70 4.02 1 -8 -9 189.10 4.73 1 -6 -10 43.42 4.11 1 -3 19 15.39 4.71 1 -2 -11 683.47 7.35 1 -2 19 51.99 5.36 1 -1 19 35.77 4.48 1 2 -10 20.04 4.95 1 2 18 -0.17 3.97 1 4 17 25.66 3.94 1 5 16 60.07 4.50 1 6 15 43.66 4.10 1 8 12 159.21 3.81 2 -17 -2 4.85 4.24 2 -16 -5 41.85 4.82 2 -15 -7 11.06 2.99 2 -14 -9 27.08 4.40 2 -13 -10 3.75 2.98 2 -11 -12 9.15 2.94 2 -10 -13 -0.32 4.19 2 -10 21 1.45 8.95 2 -6 -15 25.81 3.04 2 2 23 0.13 4.65 2 4 22 25.21 4.88 2 6 21 14.35 3.64 2 7 20 10.37 4.48 2 8 19 26.79 4.83 2 9 18 14.98 3.62 2 10 -8 1.75 4.69 2 10 16 3.01 4.48 2 12 -4 15.07 3.82 2 12 12 6.79 4.02 2 13 0 59.24 4.15 2 13 8 7.62 4.09 2 13 9 117.85 3.83 3 -15 -12 7.68 3.76 3 -12 -15 140.40 4.53 3 -11 -16 18.78 5.14 3 -7 -18 17.35 3.83 3 -4 -19 4.39 4.06 3 -3 -19 92.24 5.17 3 -2 -19 18.07 4.50 3 -1 -19 22.77 4.42 3 3 -18 54.37 5.73 3 12 -10 12.20 4.92 3 13 -8 9.28 5.08 3 14 -6 148.47 5.82 3 14 14 1.76 4.49 3 15 -3 1.61 4.16 3 15 10 -1.06 4.78 3 15 11 12.53 4.34 4 14 -10 5.53 5.98 0 -6 1 33.51 4.43 0 -6 7 57.56 7.61 0 -5 0 1088.47 12.42 0 -3 -1 664.29 11.56 0 -2 -1 52.69 5.16 0 1 6 179.61 6.23 1 -14 0 112.41 4.55 1 -14 1 50.56 3.25 1 -14 8 17.89 5.04 1 -13 -3 259.88 5.07 1 -13 11 97.40 5.70 1 -12 -5 90.53 4.29 1 -12 13 4.21 5.87 1 -10 -8 417.19 5.28 1 -8 17 17.45 7.69 1 -7 -10 150.75 4.65 1 -4 -11 92.38 4.45 1 -3 -11 165.48 3.94 1 -1 -11 217.79 5.56 1 1 18 47.52 4.27 1 3 17 51.00 4.40 1 6 14 239.03 5.11 1 7 13 130.70 3.72 1 8 -3 308.51 6.07 1 9 0 89.91 3.32 1 9 1 391.86 5.76 2 -18 1 9.72 4.94 2 -18 2 1.47 4.60 2 -18 3 5.62 4.79 2 -18 4 56.77 5.27 2 -18 5 18.11 4.93 2 -18 6 1.43 4.57 2 -18 7 1.46 4.29 2 -17 -4 50.75 4.42 2 -17 -3 9.47 3.30 2 -17 11 2.69 5.07 2 -16 -6 7.60 4.51 2 -15 -8 37.25 4.64 2 -13 -11 34.28 4.27 2 -12 -12 -4.16 4.10 2 -11 -13 9.35 3.91 2 -9 -14 27.43 3.26 2 -7 -15 129.75 3.92 2 -6 23 -0.96 5.82 2 -4 -16 228.93 5.09 2 -3 -16 131.82 4.58 2 -2 -16 37.25 4.11 2 -1 -16 84.54 4.56 2 1 23 7.45 4.89 2 5 21 3.89 4.80 2 9 17 36.42 4.86 2 11 -6 30.26 3.94 2 11 14 51.00 3.34 2 12 -3 112.39 4.25 2 12 11 29.81 3.99 2 13 1 81.28 3.60 2 13 3 54.51 4.22 2 13 4 38.88 4.11 2 13 5 328.26 5.57 2 13 6 27.53 4.00 2 13 7 3.41 2.98 3 -15 -13 -1.12 4.24 3 -14 -14 1.15 4.92 3 -13 -15 12.42 5.19 3 -12 -16 -0.28 4.49 3 -10 -17 4.33 3.31 3 -8 -18 94.54 4.13 3 -5 -19 5.97 4.47 3 0 -19 2.37 4.95 3 13 15 5.48 4.64 3 14 13 11.16 4.37 3 15 -2 58.24 4.39 3 15 -1 13.29 4.27 3 15 9 4.36 4.74 4 6 -19 5.96 7.12 4 12 -13 -0.73 6.48 0 -7 3 350.14 7.60 0 -7 4 523.03 9.76 0 -7 5 673.84 10.90 0 -4 -1 501.31 8.34 0 -1 8 260.35 8.34 0 1 5 465.03 9.14 1 -14 -1 42.18 4.19 1 -14 9 21.19 4.65 1 -13 -4 36.66 3.96 1 -12 -6 160.61 4.42 1 -11 -7 264.85 4.13 1 -9 -9 317.01 4.45 1 -8 -10 78.44 4.07 1 -6 -11 59.42 4.20 1 -6 18 11.90 5.33 1 -5 -11 202.02 4.14 1 0 -11 0.67 3.68 1 4 16 35.49 3.94 1 5 15 40.74 4.02 1 9 2 83.00 4.01 1 9 3 107.39 4.24 1 9 4 8.74 3.63 1 9 5 206.26 4.64 2 -18 -1 7.65 4.50 2 -18 0 39.67 3.96 2 -18 8 33.29 5.17 2 -17 -5 169.92 5.62 2 -16 -7 5.05 4.32 2 -15 -9 49.56 4.35 2 -14 -10 70.77 3.44 2 -8 -15 147.64 4.09 2 -8 22 5.81 6.29 2 -6 -16 14.51 4.06 2 -5 -16 28.13 3.04 2 -1 23 1.79 5.21 2 0 -16 443.94 6.71 2 3 -15 20.69 4.74 2 3 22 8.21 3.28 2 6 20 3.14 3.40 2 7 19 5.04 3.96 2 8 18 -1.48 3.19 2 10 15 0.76 3.18 2 11 13 34.59 3.16 2 12 9 151.23 4.76 2 12 10 2.89 2.91 3 -11 -17 38.93 5.04 3 -9 -18 2.26 4.64 3 -7 -19 3.02 4.42 3 -6 -19 18.99 3.74 3 1 -19 12.36 4.82 3 11 18 7.09 5.02 3 13 14 9.88 4.37 3 14 -5 5.35 3.80 3 14 12 34.21 3.63 3 15 0 14.31 4.65 3 15 1 3.51 4.36 3 15 5 1.36 4.15 3 15 6 -5.32 4.35 3 15 7 14.13 4.04 3 15 8 40.45 3.91 4 15 -7 -0.06 4.95 0 -7 1 496.71 7.66 0 -7 2 671.02 9.10 0 -6 0 23.82 3.18 0 -5 -1 568.92 8.24 0 1 4 830.91 12.43 1 -15 1 51.38 3.78 1 -15 2 159.50 4.50 1 -15 3 23.62 3.91 1 -15 4 58.07 4.17 1 -15 5 71.17 4.38 1 -14 -3 125.76 4.38 1 -14 -2 9.64 2.67 1 -13 -5 72.23 4.28 1 -13 12 6.40 5.23 1 -11 -8 515.49 5.55 1 -10 -9 33.92 3.58 1 -7 -11 280.72 5.07 1 -5 18 8.35 4.94 1 -1 18 52.51 4.56 1 2 17 168.42 4.72 1 3 16 56.58 4.24 1 5 14 108.34 4.67 1 6 13 192.51 4.83 1 8 -2 468.67 6.51 2 -18 -3 1.69 4.27 2 -18 -2 11.02 3.34 2 -18 9 5.04 5.07 2 -17 -6 44.45 4.84 2 -14 -11 2.09 4.06 2 -13 -12 0.23 4.12 2 -12 -13 43.95 4.33 2 -11 -14 65.54 4.47 2 -9 -15 27.38 3.03 2 -7 -16 90.74 4.75 2 -4 23 2.15 4.74 2 -3 23 2.23 4.57 2 -2 23 6.20 4.65 2 1 -16 109.83 5.37 2 2 22 8.01 4.06 2 4 21 2.71 3.36 2 5 20 17.30 4.76 2 8 17 18.21 4.38 2 9 16 18.52 3.21 2 10 14 68.48 4.17 2 11 -5 5.29 3.47 2 11 12 1.76 2.53 2 12 -2 35.38 3.64 2 12 -1 218.31 4.77 2 12 8 10.45 3.83 3 -13 -16 10.47 5.01 3 -12 -17 0.78 4.47 3 -10 -18 11.62 4.48 3 -8 -19 22.11 5.05 3 2 -19 21.91 4.89 3 4 -18 132.79 6.47 3 12 16 1.26 3.45 3 13 -7 131.13 5.12 3 13 13 5.15 4.54 3 14 -4 4.63 3.81 3 14 10 15.67 4.77 3 14 11 0.61 3.26 3 15 2 13.42 3.47 3 15 3 12.46 3.35 3 15 4 48.11 3.38 4 13 -11 14.09 6.37 4 14 -9 1.73 5.20 0 -7 0 252.53 6.15 0 -7 6 449.55 9.73 0 -6 -1 23.96 4.71 0 -4 -2 6.95 3.42 0 -3 -2 124.78 5.24 0 -2 -2 179.80 7.15 0 -2 8 5.57 5.92 1 -15 -1 14.41 3.72 1 -15 0 91.17 4.19 1 -15 6 180.43 5.19 1 -15 7 37.78 4.17 1 -14 10 87.87 4.75 1 -13 -6 34.50 4.07 1 -12 -7 6.17 2.52 1 -8 -11 55.82 3.98 1 -5 -12 45.52 4.05 1 -4 -12 162.86 4.73 1 -4 18 69.97 5.15 1 -3 -12 210.35 4.86 1 -3 18 63.83 5.19 1 -2 -12 44.20 3.95 1 -2 18 -0.25 4.21 1 1 17 75.75 4.04 1 4 15 24.99 2.90 1 6 -6 27.01 5.37 1 6 12 84.00 4.15 1 7 -4 369.10 7.40 1 8 -1 204.99 4.86 2 -19 0 39.55 4.23 2 -19 1 11.36 4.83 2 -19 2 -3.82 4.68 2 -19 3 5.81 4.55 2 -19 4 4.78 4.49 2 -19 5 5.02 4.37 2 -18 -4 15.31 4.55 2 -17 -7 -0.08 4.55 2 -16 -9 21.03 4.40 2 -15 -10 143.46 3.95 2 -10 -15 1.89 4.16 2 -8 -16 92.49 4.48 2 -4 -17 33.31 3.93 2 -3 -17 52.11 3.99 2 1 22 6.42 4.63 2 6 19 6.85 3.04 2 7 18 24.90 3.23 2 9 -9 58.80 5.18 2 9 15 61.14 4.23 2 10 -7 269.99 6.35 2 10 13 67.94 4.10 2 11 11 19.51 2.71 2 12 0 50.78 3.97 2 12 1 94.49 4.08 2 12 5 275.59 4.79 2 12 6 105.77 4.42 2 12 7 4.00 2.93 3 -11 -18 4.25 4.67 3 -9 -19 1.09 4.66 3 -6 -20 25.97 4.30 3 -5 -20 -4.77 4.20 3 -4 -20 6.56 4.54 3 -3 -20 44.04 5.09 3 -2 -20 9.21 4.46 3 -1 -20 12.71 5.05 3 10 18 10.25 4.91 3 11 17 5.44 3.40 3 12 -9 10.39 4.16 3 12 15 -5.38 3.16 3 13 12 29.94 4.51 3 14 -3 16.75 3.99 3 14 8 106.28 4.83 3 14 9 2.35 3.99 4 11 -14 4.37 6.86 4 15 -6 6.33 4.92 0 -8 1 334.77 6.10 0 -8 2 116.51 5.08 0 -8 3 726.56 8.78 0 -8 4 371.70 7.03 0 -8 5 66.34 5.32 0 -6 -2 1709.32 11.88 0 -1 7 13.47 5.63 1 -15 -2 31.52 4.26 1 -15 8 7.74 4.09 1 -14 -5 20.54 4.01 1 -13 -7 40.62 3.82 1 -12 -8 17.48 3.75 1 -11 -9 118.29 3.31 1 -10 -10 21.25 3.50 1 -9 -11 148.74 4.15 1 -7 -12 190.73 4.53 1 -6 -12 168.81 4.79 1 -1 -12 46.90 4.06 1 2 16 27.17 3.65 1 5 13 203.27 4.87 1 8 0 36.69 3.60 1 8 5 500.34 5.69 2 -19 -2 22.86 4.62 2 -18 -5 9.59 3.40 2 -17 -8 28.44 4.73 2 -15 -11 15.28 4.08 2 -14 -12 2.04 3.01 2 -12 -14 16.07 3.11 2 -11 -15 6.03 4.31 2 -9 -16 107.80 4.46 2 -7 22 14.92 5.81 2 -6 -17 64.78 4.41 2 -5 -17 19.14 2.96 2 -2 -17 177.62 4.92 2 -1 -17 225.53 5.21 2 2 21 26.77 4.14 2 4 20 28.39 4.60 2 5 19 11.26 3.84 2 6 18 6.64 3.96 2 7 17 5.61 3.97 2 8 16 27.42 3.07 2 10 12 69.12 3.90 2 11 9 152.50 4.35 2 11 10 295.51 4.13 2 12 2 -1.32 2.56 2 12 3 54.21 2.93 2 12 4 28.03 2.90 3 -10 -19 1.55 4.60 3 -7 -20 21.12 4.81 3 0 -20 27.93 5.34 3 8 20 5.30 4.62 3 9 19 0.87 4.26 3 11 16 23.54 4.17 3 12 14 7.56 3.73 3 13 -6 55.17 4.40 3 13 11 18.70 4.31 3 14 -2 218.05 5.23 3 14 -1 3.40 4.15 3 14 6 32.73 4.35 3 14 7 3.33 4.29 4 14 -8 39.54 5.43 4 15 -5 0.53 4.62 4 16 1 13.40 4.39 0 -7 -2 795.48 8.46 0 -5 -3 109.32 5.27 0 -4 -3 616.47 7.98 0 -3 8 288.79 11.84 1 -16 0 33.49 3.87 1 -16 2 67.44 4.44 1 -16 3 32.12 3.96 1 -16 4 18.36 3.89 1 -16 5 59.18 4.49 1 -15 -3 24.19 2.93 1 -15 9 8.45 4.88 1 -14 -6 2.32 3.77 1 -14 11 10.65 4.58 1 -12 14 11.06 6.11 1 -8 -12 79.85 3.93 1 -1 17 75.87 4.90 1 0 -12 217.85 5.61 1 3 15 25.21 2.81 1 4 14 283.00 4.35 1 6 11 26.55 2.67 1 8 1 494.54 5.53 1 8 2 630.66 6.30 1 8 3 18.92 3.37 1 8 4 207.84 3.84 2 -19 -4 9.66 4.18 2 -19 -3 39.03 4.81 2 -18 -7 3.74 4.12 2 -16 -10 22.48 3.14 2 -15 -12 5.34 3.70 2 -14 -13 11.19 4.04 2 -13 -14 30.94 4.21 2 -8 -17 -0.15 3.95 2 -7 -17 43.19 3.31 2 -6 22 3.43 5.64 2 -2 22 5.32 4.97 2 0 -17 -1.78 4.77 2 2 -16 37.55 4.08 2 3 20 6.62 4.44 2 5 -14 53.49 7.27 2 10 11 66.71 3.71 2 11 -3 7.69 3.38 2 11 8 142.84 4.27 3 -8 -20 4.95 3.54 3 6 -17 51.34 9.21 3 9 18 7.88 4.56 3 10 -12 23.94 5.66 3 10 17 3.16 3.39 3 11 15 3.43 4.23 3 12 13 15.52 3.84 3 13 -5 123.42 5.04 3 13 10 7.91 3.90 3 14 0 67.96 4.59 3 14 1 7.74 3.93 3 14 2 123.77 4.47 3 14 3 20.63 3.87 3 14 4 33.75 4.04 3 14 5 6.30 3.64 4 15 -4 5.68 4.57 0 -9 1 429.52 6.31 0 -9 2 241.29 5.50 0 -9 3 373.26 6.53 0 -9 4 80.97 4.51 0 -8 -1 300.87 4.91 0 -8 6 2.01 3.99 0 -6 -3 113.23 4.05 0 -4 8 51.61 10.93 1 -16 -2 63.59 4.17 1 -16 -1 42.04 4.18 1 -16 6 29.23 3.94 1 -15 -5 78.92 4.22 1 -14 -7 78.12 3.97 1 -13 -8 13.28 2.73 1 -13 13 10.50 5.50 1 -10 -11 2.28 2.48 1 -7 17 47.93 6.33 1 -5 -13 72.40 4.03 1 -4 -13 512.57 6.11 1 -3 -13 13.44 3.51 1 1 16 5.18 3.45 1 2 15 13.57 3.69 1 3 -10 216.17 8.27 1 5 12 114.43 4.18 2 -19 -5 1.90 4.43 2 -18 -8 7.62 4.16 2 -17 -10 53.39 4.11 2 -16 -11 4.52 3.08 2 -12 -15 147.73 3.91 2 -11 -16 7.59 4.38 2 -11 20 3.66 8.38 2 -9 -17 24.11 4.04 2 -9 21 3.32 7.19 2 -5 -18 16.96 3.67 2 -5 22 3.96 4.82 2 -4 -18 42.79 3.78 2 -3 22 5.96 4.69 2 1 21 25.36 3.85 2 4 19 48.32 4.18 2 5 18 -4.44 3.87 2 7 16 28.71 3.88 2 10 10 56.34 3.69 2 11 -2 38.10 3.53 2 11 6 31.59 3.65 2 11 7 59.27 3.09 3 -9 -20 6.02 3.52 3 -6 -21 10.02 4.61 3 -5 -21 11.86 4.41 3 -4 -21 7.64 4.30 3 -3 -21 21.40 4.57 3 1 -20 18.87 4.51 3 6 21 1.26 4.03 3 7 20 -3.21 4.49 3 8 19 3.63 4.02 3 10 16 -3.42 4.40 3 11 -10 83.32 5.25 3 11 14 -1.09 3.89 3 12 -8 10.58 4.06 3 12 12 15.82 4.01 3 13 9 9.32 4.09 4 12 -12 5.56 5.07 4 13 -10 0.11 4.48 4 14 -7 41.73 5.51 4 15 -3 25.65 4.48 4 15 -2 11.92 4.44 4 15 6 40.66 4.73 0 -9 0 569.98 6.22 0 -9 5 66.77 4.55 0 -7 -3 416.14 5.64 0 -4 -4 648.17 7.56 0 -3 -4 149.35 5.47 1 -16 -3 405.09 5.50 1 -16 7 22.54 4.35 1 -15 -6 10.55 3.94 1 -15 10 231.45 6.34 1 -12 -10 252.49 3.84 1 -11 -11 26.82 3.81 1 -10 -12 248.67 4.64 1 -8 -13 108.62 3.94 1 -7 -13 64.01 3.14 1 -2 -13 34.75 3.61 1 -2 17 194.23 5.17 1 2 -11 882.63 11.03 1 3 14 74.40 3.83 2 -18 -9 6.63 4.15 2 -16 -12 7.90 4.02 2 -15 -13 4.93 3.03 2 -12 -16 0.79 3.89 2 -10 -17 13.51 4.14 2 -6 -18 40.03 4.48 2 -2 -18 31.62 4.25 2 0 21 0.84 4.03 2 2 20 5.87 4.18 2 4 -15 41.95 5.70 2 8 -10 14.36 5.20 2 8 14 8.70 2.85 2 9 -8 68.36 5.07 2 11 -1 11.90 3.49 2 11 1 25.53 3.78 2 11 3 99.48 4.14 2 11 4 348.87 5.09 2 11 5 54.32 3.52 3 -7 -21 6.40 4.86 3 -2 -21 47.48 4.83 3 -1 -21 38.96 5.20 3 4 22 -4.38 4.63 3 9 17 20.23 4.54 3 13 -4 -2.09 3.36 3 13 7 49.71 4.35 3 13 8 63.83 3.38 4 10 -15 10.88 6.87 4 15 -1 0.66 4.48 4 15 0 7.41 4.47 4 15 1 3.69 4.49 4 15 2 13.47 4.60 4 15 3 6.36 4.56 4 15 4 0.86 4.46 4 15 5 1.16 4.02 0 -10 0 3.29 3.89 0 -10 1 86.34 4.16 0 -10 2 24.88 3.88 0 -10 3 68.83 4.17 0 -9 6 256.72 6.78 0 -8 7 569.40 9.68 1 -17 -1 67.05 4.10 1 -17 1 183.01 5.11 1 -17 3 22.36 3.92 1 -17 4 5.43 3.82 1 -16 -5 15.45 4.03 1 -16 -4 30.63 3.07 1 -16 8 16.61 4.36 1 -15 -7 24.02 3.87 1 -13 -10 6.45 3.47 1 -12 -11 29.76 3.76 1 -4 17 37.58 4.75 1 -1 -13 9.34 3.40 1 1 -12 52.25 4.92 1 1 15 51.67 3.77 1 7 -1 127.54 4.35 1 7 5 87.60 3.85 2 -17 -11 83.60 3.74 2 -16 -13 33.56 4.02 2 -14 -15 46.73 4.45 2 -11 -17 30.36 4.43 2 -9 -18 51.55 4.01 2 -8 -18 34.30 3.16 2 1 20 35.10 4.15 2 3 19 27.66 3.93 2 4 18 17.32 3.86 2 5 17 47.34 4.34 2 6 16 6.10 3.76 2 7 15 75.31 3.34 2 8 13 58.30 3.94 2 9 11 2.34 3.46 2 10 -5 16.75 3.34 2 11 2 31.32 2.86 3 2 -20 16.09 5.14 3 5 -18 25.83 7.05 3 5 21 -1.91 3.40 3 6 20 0.94 4.01 3 8 18 0.38 3.18 3 10 15 -1.16 3.05 3 11 13 5.95 2.84 3 12 -7 33.75 4.03 3 12 10 3.50 3.85 3 13 -3 47.74 3.90 3 13 -2 49.97 3.88 3 13 5 25.30 3.94 3 13 6 17.27 3.07 4 13 -9 -0.88 4.82 4 14 -6 15.41 4.57 4 14 8 26.77 4.64 4 14 9 1.84 3.43 0 -10 -2 33.52 3.88 0 -10 -1 87.36 4.29 0 -10 5 421.88 6.95 0 -9 -3 411.06 5.95 0 -4 -5 57.44 4.48 0 -2 -4 1057.58 10.73 1 -17 -3 108.65 4.33 1 -17 -2 63.25 3.15 1 -17 5 126.60 4.80 1 -17 6 74.10 4.27 1 -16 -6 -3.76 4.03 1 -16 9 40.25 5.19 1 -15 11 65.47 5.04 1 -14 -9 14.66 2.82 1 -10 -13 31.01 3.89 1 -9 16 39.58 8.32 1 -8 -14 61.04 3.64 1 -7 -14 84.61 4.05 1 -6 -14 137.59 3.57 1 -4 -14 52.91 3.00 1 2 14 38.57 3.67 1 7 1 87.01 3.98 2 -17 -12 55.52 4.67 2 -13 -16 8.25 3.21 2 -12 -17 19.88 4.40 2 -10 -18 36.01 4.09 2 -8 21 0.55 5.17 2 -6 -19 26.05 4.04 2 -5 -19 8.93 3.58 2 -4 -19 61.86 4.76 2 -2 21 34.00 4.49 2 10 7 7.48 3.42 3 -6 -22 6.41 4.55 3 -5 -22 -2.81 4.42 3 -4 -22 38.05 4.70 3 0 -21 -0.01 4.38 3 3 22 -0.36 3.50 3 4 21 3.09 4.42 3 8 17 39.99 4.56 3 9 16 13.65 3.07 3 10 14 61.49 3.99 3 12 -6 4.26 4.38 3 12 9 40.28 3.78 3 13 -1 175.69 4.44 3 13 0 13.41 3.89 3 13 2 40.17 3.97 3 13 3 142.33 4.31 3 13 4 27.69 2.86 4 12 -11 -0.01 5.11 4 13 11 37.44 4.29 4 14 -5 2.36 4.20 4 14 7 5.08 4.61 0 -11 0 19.45 3.98 0 -11 2 883.00 7.71 0 -11 3 639.28 6.84 0 -9 -4 68.69 3.12 0 -9 7 823.21 10.06 0 -6 -6 238.14 5.18 0 -3 -5 813.96 8.33 1 -18 0 10.71 3.83 1 -18 2 28.69 3.78 1 -17 -4 20.60 3.01 1 -17 7 62.51 4.29 1 -14 -10 9.90 2.60 1 -12 -12 12.35 2.63 1 -2 -14 29.92 3.46 1 -2 16 32.06 4.29 1 0 -13 -1.21 3.68 1 5 -7 127.00 7.68 2 -16 -14 12.37 4.35 2 -14 -16 11.12 4.44 2 -13 -17 10.93 3.87 2 -7 21 14.34 5.50 2 -4 21 2.21 4.80 2 -3 -19 4.05 3.81 2 -3 21 32.72 4.66 2 0 -18 34.47 4.04 2 0 20 36.55 3.94 2 2 -17 188.18 5.58 2 2 19 9.27 2.97 2 3 18 45.52 4.18 2 8 12 21.63 2.56 2 10 -3 189.65 4.33 2 10 6 108.43 3.19 3 -2 -22 14.86 5.17 3 2 22 -0.64 4.51 3 4 -19 2.09 5.68 3 5 20 2.28 3.86 3 6 19 3.35 3.70 3 7 18 42.43 3.39 3 9 -13 33.79 5.55 3 9 15 27.30 4.13 3 10 13 2.15 3.65 3 11 -9 4.74 3.64 3 11 11 6.28 3.42 3 12 8 70.81 3.32 4 11 -13 17.90 4.96 4 12 13 6.22 3.17 4 13 -8 20.72 4.20 4 13 10 2.08 3.83 4 14 -3 53.45 4.65 4 14 5 1.67 4.20 4 14 6 32.80 3.48 0 -10 6 540.53 7.34 0 -9 -5 54.50 2.94 0 -8 -6 5.70 3.51 0 -8 8 71.78 5.76 0 -4 -6 455.09 6.43 1 -18 -3 12.83 3.49 1 -18 -1 20.00 4.36 1 -18 4 8.76 4.13 1 -17 8 25.50 4.58 1 -16 -8 30.33 4.08 1 -16 10 23.45 4.94 1 -14 -11 18.82 3.85 1 -12 -13 117.22 4.17 1 -4 -15 82.55 3.86 1 1 14 105.07 4.03 1 5 9 43.95 2.70 2 -15 -16 68.68 4.15 2 -12 -18 -1.01 4.26 2 -10 -19 3.79 3.62 2 -6 21 13.72 4.49 2 -5 21 1.79 4.37 2 -2 -19 7.41 3.85 2 1 19 -0.07 3.70 2 4 17 25.53 3.02 2 10 3 35.24 3.80 2 10 4 363.97 4.90 3 1 -21 37.39 5.37 3 3 21 3.32 4.39 3 8 16 41.88 3.98 3 10 -11 14.67 4.39 3 11 10 21.39 3.60 3 12 -5 41.77 3.82 3 12 6 26.11 3.78 4 11 14 2.39 4.12 4 12 12 -4.83 3.08 4 13 -7 43.90 5.25 4 13 9 7.28 3.28 4 14 -2 24.81 3.93 4 14 -1 7.58 4.02 4 14 0 6.18 4.35 4 14 1 5.99 4.20 4 14 2 51.11 4.54 4 14 3 11.72 3.71 4 14 4 1.70 2.93 0 -12 3 304.21 5.00 0 -11 5 35.54 3.69 0 -7 -7 181.60 4.65 0 -6 -7 56.70 3.95 0 -5 -7 251.12 5.26 1 -18 -5 79.38 3.96 1 -18 -4 123.03 4.31 1 -18 5 19.63 4.26 1 -18 6 16.65 4.52 1 -17 -7 20.43 4.03 1 -15 -11 64.18 3.68 1 -14 -12 94.64 3.99 1 -3 16 65.15 4.26 1 -1 -14 131.37 4.15 1 5 8 171.11 4.24 2 -14 -17 0.93 3.30 2 -13 -18 5.85 4.23 2 -11 -19 14.61 4.11 2 -10 20 13.60 6.80 2 -7 -20 5.90 4.23 2 -6 -20 20.49 4.09 2 -5 -20 37.51 3.77 2 -1 -19 13.99 4.27 2 1 -18 40.22 4.36 2 2 18 6.16 3.70 2 5 15 5.18 3.54 2 6 14 23.09 3.25 2 7 12 126.07 4.01 2 10 -1 39.17 2.61 2 10 1 29.93 3.63 2 10 2 69.47 2.89 3 -1 -22 22.36 4.35 3 1 22 2.78 3.13 3 5 19 58.35 4.08 3 6 18 24.49 3.67 3 7 17 5.76 3.15 3 9 14 4.55 2.73 3 10 12 72.09 3.07 3 11 -8 40.75 3.93 3 11 9 50.39 3.68 3 12 -4 15.03 3.40 3 12 -3 37.44 3.45 3 12 4 27.18 3.66 3 12 5 42.34 2.79 4 9 -16 5.75 6.48 4 10 15 1.27 4.25 4 11 13 17.01 4.10 4 12 -10 42.89 5.13 4 13 7 30.21 4.44 4 13 8 9.41 3.10 0 -12 -4 28.01 3.62 0 -12 4 19.36 3.36 0 -11 -5 27.48 3.80 0 -11 6 208.78 5.05 0 -10 7 47.69 3.85 1 -19 -1 55.72 4.43 1 -19 3 43.31 3.86 1 -18 -6 8.63 4.26 1 -18 7 6.43 4.64 1 -17 -8 41.64 2.99 1 -17 9 43.25 4.40 1 -16 -10 18.00 3.87 1 -12 -14 29.14 4.03 1 -6 -16 51.74 3.64 1 -4 16 42.54 4.63 1 -2 -15 1220.48 7.90 1 1 -13 12.68 3.88 2 -3 -20 32.57 4.33 2 0 19 -2.62 3.60 2 4 16 126.93 3.38 2 8 -9 708.06 9.14 3 0 -22 16.57 4.83 3 0 22 2.41 4.21 3 2 21 13.38 3.74 3 3 20 0.17 4.29 3 7 16 7.31 4.11 3 8 15 62.91 3.17 3 9 13 144.73 4.19 3 11 8 108.94 3.84 3 12 -2 13.22 3.13 3 12 -1 111.52 3.86 3 12 0 27.60 3.57 3 12 1 0.36 3.52 3 12 2 68.40 3.79 3 12 3 255.65 4.00 4 11 12 8.29 3.83 4 12 10 1.75 3.03 4 13 -6 11.38 3.78 4 13 5 36.12 4.05 4 13 6 15.78 3.80 0 -13 0 39.99 2.88 0 -13 3 218.81 4.59 0 -12 -5 27.42 3.64 0 -12 5 23.65 3.47 0 -10 -7 48.89 3.79 0 -8 -8 82.70 3.86 0 -7 -8 392.37 4.76 0 -6 -8 76.12 3.07 0 -5 -8 86.83 4.00 0 -3 -7 167.47 4.97 0 -2 -6 4.03 3.49 0 -2 6 1.71 5.35 1 -19 -4 74.25 4.22 1 -19 -3 36.32 3.10 1 -18 -7 27.70 4.14 1 -17 -9 53.57 3.19 1 -16 -11 6.05 3.85 1 -16 11 26.05 3.96 1 -15 -12 15.34 2.86 1 -14 -13 14.52 2.69 1 -13 -14 22.05 3.82 1 -12 -15 14.33 3.50 1 -11 -15 2.06 2.72 1 -9 -16 16.01 3.82 1 -8 -16 27.88 2.93 1 -8 16 32.79 6.10 1 -5 16 83.85 5.18 1 -4 -16 72.58 3.78 1 -2 15 19.94 3.52 1 0 -14 205.94 5.37 1 2 -12 48.02 4.54 1 4 9 15.15 3.17 1 5 7 269.29 3.95 2 -11 -20 22.01 4.37 2 -10 -20 29.86 3.29 2 -3 20 6.24 3.84 2 -1 19 2.21 3.47 2 0 -19 0.45 4.06 2 1 18 15.19 3.65 2 5 14 16.79 3.25 2 9 -5 191.49 4.84 3 -1 22 -2.94 4.09 3 1 21 11.21 4.33 3 2 -21 44.87 4.99 3 4 19 3.92 3.70 3 5 18 6.61 3.85 3 6 17 3.22 2.83 3 8 14 78.90 4.09 3 9 12 22.04 3.66 3 10 -10 229.77 5.84 3 10 10 32.44 3.31 3 11 -7 60.21 3.97 3 11 7 33.04 2.86 4 8 17 17.65 4.04 4 10 -14 1.28 4.99 4 10 14 9.36 3.01 4 11 -12 63.76 5.22 4 12 -9 1.88 4.20 4 12 9 6.84 3.01 4 13 -4 9.97 4.12 4 13 4 8.97 3.66 0 -14 -1 26.79 3.47 0 -14 0 1.05 3.59 0 -13 -5 14.12 3.24 0 -13 -4 33.95 3.62 0 -13 4 21.13 3.31 0 -12 6 34.48 4.40 0 -11 7 135.39 5.52 0 -10 -8 100.72 3.77 0 -8 -9 48.83 3.71 0 -6 -9 928.08 7.04 0 -4 -8 75.15 3.11 1 -19 -6 2.82 3.98 1 -19 -5 18.72 2.99 1 -18 -9 21.26 3.61 1 -18 -8 160.53 3.73 1 -18 8 15.48 3.96 1 -17 -10 30.20 3.01 1 -17 10 13.61 4.96 1 -16 -12 10.47 3.89 1 -15 -13 21.30 3.55 1 -14 -14 69.90 3.95 1 -13 -15 24.26 3.53 1 -10 -16 3.33 2.60 1 -7 16 27.26 4.89 1 -6 16 81.46 5.08 1 5 6 224.27 4.46 1 6 1 90.89 3.31 2 -9 -21 11.89 3.84 2 -9 20 1.80 5.30 2 -8 -21 39.09 4.41 2 -2 -20 3.73 3.78 2 2 17 132.42 3.88 2 3 16 116.79 4.14 2 6 12 53.04 3.47 2 9 -4 20.99 3.74 2 9 4 161.87 4.08 3 -2 22 2.31 4.17 3 2 20 1.64 4.15 3 7 15 3.26 3.80 3 10 9 11.76 3.41 3 11 -6 162.69 4.50 3 11 5 9.95 3.59 3 11 6 4.39 2.65 4 8 16 5.69 4.02 4 10 13 -2.54 3.41 4 11 11 9.39 2.91 4 12 8 11.84 2.98 4 13 -3 30.80 3.70 4 13 -2 14.81 3.77 4 13 -1 -6.06 3.85 4 13 0 1.19 4.13 4 13 1 39.07 4.29 4 13 2 35.94 3.69 0 -14 -3 26.93 3.70 0 -14 -2 484.04 4.73 0 -14 2 492.03 5.60 0 -14 3 24.47 3.42 0 -13 -6 75.54 3.85 0 -13 5 14.66 3.50 0 -9 -9 171.09 3.44 0 -2 -7 81.22 3.85 0 -1 -5 507.84 7.30 1 -20 -4 14.84 4.06 1 -20 -3 47.03 4.15 1 -20 -2 13.01 3.09 1 -20 -1 3.24 3.11 1 -20 0 20.41 3.23 1 -20 1 80.11 4.39 1 -20 2 5.17 4.00 1 -19 -8 80.91 3.97 1 -19 -7 19.96 3.18 1 -18 -10 -0.21 4.04 1 -18 9 14.06 4.59 1 -17 -11 3.60 3.02 1 -12 -16 43.08 4.15 1 -7 -17 16.81 3.64 1 -6 -17 26.22 3.61 1 -3 15 31.16 4.19 1 3 -11 226.88 7.48 2 -12 19 6.68 7.84 2 -8 20 8.75 4.70 2 -7 20 8.58 4.93 2 -6 20 4.51 4.63 2 -1 -20 19.25 4.46 2 0 18 23.05 3.48 2 3 -17 54.74 4.68 2 5 13 167.15 4.05 2 9 1 70.22 3.58 2 9 2 97.91 3.88 2 9 3 63.61 2.83 3 0 21 -0.33 4.08 3 1 -22 20.43 4.87 3 3 19 26.86 3.72 3 5 17 0.95 3.91 3 6 16 9.31 2.85 3 8 13 39.43 2.57 3 9 -12 37.37 5.22 3 9 11 15.65 2.44 3 11 -5 8.83 3.55 3 11 3 142.13 4.01 3 11 4 148.93 3.99 4 6 18 6.84 4.06 4 7 17 1.43 4.03 4 9 14 8.67 3.68 4 10 12 9.18 3.60 4 11 -11 18.20 5.22 4 11 10 16.90 3.00 4 12 -8 19.91 4.06 4 12 6 7.16 3.90 0 -15 -3 16.38 3.42 0 -15 -2 125.89 4.20 0 -15 -1 -0.39 3.56 0 -15 0 -0.76 3.44 0 -15 1 6.33 3.07 0 -14 4 65.95 3.76 0 -13 6 51.05 4.31 0 -12 7 245.98 5.80 0 -11 -9 17.60 3.11 0 -8 -10 123.63 3.19 0 -7 -10 155.39 3.33 0 -6 -10 4.54 3.31 0 -1 4 889.97 16.03 1 -20 4 13.80 4.09 1 -19 -9 13.94 4.26 1 -18 -11 36.63 4.28 1 -16 12 2.02 4.46 1 -15 13 17.60 4.45 1 -14 -15 30.75 3.05 1 -13 -16 16.14 3.92 1 -11 -17 55.31 4.10 1 -10 -17 12.84 2.89 1 -4 -17 7.29 3.43 1 -2 -16 75.48 3.49 1 0 13 1.20 3.08 1 5 -6 632.23 10.96 2 -8 -22 3.38 3.88 2 -7 -22 21.36 3.98 2 -3 -21 28.75 3.95 2 -3 19 27.41 4.39 2 1 -19 10.14 3.93 2 1 17 24.87 3.43 2 2 16 4.95 3.40 2 9 -2 227.06 4.22 2 9 0 64.59 3.47 3 -1 21 11.49 3.97 3 1 20 24.17 4.08 3 7 14 66.83 3.02 3 9 10 -3.41 3.14 3 10 7 19.07 3.44 3 11 -4 8.93 3.28 3 11 -3 97.34 3.87 3 11 -2 388.70 5.04 3 11 0 72.07 3.72 3 11 1 26.11 3.45 3 11 2 161.64 4.18 4 8 15 10.35 3.92 4 11 9 0.76 2.86 4 12 -7 32.17 4.17 4 12 5 25.40 3.65 0 -15 -5 109.18 4.12 0 -13 -8 160.92 3.54 0 -12 -9 48.11 2.77 0 -11 -10 7.12 3.28 0 -9 -11 335.94 4.69 0 -8 -11 511.89 5.33 0 -8 9 28.60 5.53 0 -7 9 96.79 8.75 0 -5 -10 274.42 4.01 1 -19 8 20.80 4.26 1 -18 10 12.15 4.54 1 -17 -13 31.18 3.11 1 -17 11 40.58 4.44 1 -16 -14 19.39 2.88 1 -15 -15 16.18 2.84 1 -14 -16 25.64 3.94 1 -12 -17 64.76 4.16 1 -9 -18 69.44 3.89 1 -8 -18 4.66 3.62 1 -7 -18 67.33 3.69 1 -3 -17 45.50 3.41 1 -2 14 44.91 3.84 1 0 -15 -0.65 3.89 1 1 -14 135.46 4.96 1 3 9 365.67 4.49 1 4 7 158.29 3.37 1 5 4 508.07 5.33 2 -6 -22 12.78 4.11 2 -5 -22 13.97 4.03 2 -1 18 19.88 3.58 2 5 12 149.38 3.80 3 -4 22 2.12 3.78 3 0 -23 0.35 4.62 3 2 19 39.33 3.94 3 3 18 13.64 3.56 3 4 17 17.66 3.52 3 5 16 8.20 3.49 3 7 13 5.53 3.31 3 11 -1 145.31 3.34 4 6 17 5.25 4.24 4 7 16 33.27 3.74 4 8 -17 33.05 7.23 4 11 8 6.89 2.78 4 12 -6 8.43 3.68 4 12 -5 -1.25 4.14 4 12 3 23.78 3.89 4 12 4 14.95 2.72 0 -16 -4 14.17 3.36 0 -16 -3 303.65 4.87 0 -16 0 16.57 3.51 0 -16 1 114.61 4.01 0 -15 -7 11.17 3.28 0 -14 -8 253.22 4.43 0 -14 6 391.97 6.22 0 -13 -9 105.49 3.12 0 -13 7 247.32 5.73 0 -12 -10 -3.66 2.39 0 -11 -11 119.80 3.91 0 -6 -11 78.75 2.93 0 -5 -11 271.27 4.61 0 -4 -10 163.87 3.44 0 -2 -8 5.46 2.50 1 -16 -15 63.67 4.49 1 -15 -16 9.25 4.10 1 -13 -17 17.92 3.09 1 -5 -18 1.74 3.22 1 -1 -16 9.34 3.08 1 2 -13 34.27 3.87 1 2 10 35.33 3.22 2 -4 -22 39.76 4.17 2 -4 19 44.96 4.16 2 0 17 2.45 3.13 2 8 -7 9.92 3.21 3 -2 21 10.69 3.94 3 0 20 56.66 3.93 3 4 -20 11.19 6.30 3 6 14 51.92 3.67 3 8 11 22.00 2.49 3 10 -8 2.59 3.37 4 4 19 0.05 3.02 4 5 18 4.36 2.85 4 8 14 4.64 2.91 4 9 12 5.97 3.46 4 10 10 12.81 2.85 4 11 -10 -0.37 3.89 4 12 -3 177.35 4.41 4 12 -2 13.86 3.78 4 12 -1 13.66 3.81 4 12 0 8.84 3.79 4 12 1 144.29 4.39 0 -16 -6 35.35 3.80 0 -16 -5 31.90 2.74 0 -16 2 16.65 3.63 0 -16 3 300.49 4.85 0 -15 -8 77.14 3.71 0 -15 5 97.90 4.12 0 -14 -9 4.75 2.45 0 -13 -10 3.06 2.44 0 -12 -11 453.10 4.79 0 -12 8 39.83 3.77 0 -10 -12 203.76 4.12 0 -9 -12 58.67 2.74 0 -8 -12 9.42 2.66 0 -6 -12 123.63 4.04 0 -1 -7 9.56 3.19 0 0 -3 1.25 3.84 1 -14 -17 13.66 3.08 1 -13 -18 19.57 3.97 1 -12 -18 15.14 2.91 1 -10 -19 38.60 3.51 1 -8 -19 27.61 3.68 1 -4 -18 0.68 3.16 1 3 8 596.13 5.92 2 -7 -23 7.03 4.13 2 -6 -23 14.23 3.68 2 -5 19 14.11 3.94 2 -1 -21 21.72 4.56 2 1 16 70.07 3.59 2 3 14 50.25 3.39 2 5 11 227.37 4.18 2 8 -6 152.21 4.91 3 -1 20 20.52 3.72 3 1 19 14.58 3.50 3 2 -22 11.51 5.25 3 2 18 1.36 3.81 3 5 15 11.31 3.44 3 7 12 38.41 3.46 3 8 10 80.02 3.49 3 9 -11 131.27 5.09 3 10 -7 22.00 3.58 3 10 3 9.51 3.25 4 6 16 13.34 3.94 4 9 11 68.08 3.64 4 10 9 -0.58 3.24 4 11 -9 10.33 4.22 4 11 5 6.00 3.63 4 11 6 30.34 2.88 5 12 4 8.96 3.78 5 12 5 0.74 2.86 0 -17 -5 25.62 3.84 0 -17 -4 3.82 3.40 0 -17 -3 63.98 3.68 0 -17 -2 11.10 2.59 0 -17 -1 39.01 2.96 0 -17 0 80.76 4.15 0 -17 1 52.36 4.12 0 -16 -8 92.60 3.85 0 -16 -7 179.14 3.63 0 -16 4 12.11 3.52 0 -15 -9 4.50 3.70 0 -14 -10 4.83 2.47 0 -13 -11 109.11 2.95 0 -12 -12 50.77 3.60 0 -11 -12 127.47 3.08 0 -10 -13 94.24 3.66 0 -9 -13 126.29 3.95 0 -8 -13 53.16 3.58 0 -5 -12 13.91 3.24 0 -4 -11 316.26 4.13 1 -18 11 15.03 4.80 1 -17 12 22.27 4.74 1 -12 -19 25.17 4.12 1 -6 -19 88.99 4.10 1 -3 -18 41.79 3.46 1 -3 14 70.46 3.73 1 4 5 34.62 3.32 1 5 1 539.74 6.47 2 -11 19 2.03 5.33 2 -6 19 7.01 4.18 2 -5 -23 20.89 3.83 2 -3 18 39.51 4.25 2 -1 17 22.52 3.44 2 4 12 273.77 4.47 2 7 -10 315.33 7.34 3 4 16 17.62 2.61 3 6 13 -3.85 3.47 3 9 7 97.80 2.88 3 10 -6 121.29 4.34 3 10 2 79.98 3.54 4 3 19 -2.18 2.88 4 4 18 0.06 3.41 4 5 17 7.61 3.00 4 7 14 17.07 3.68 4 10 -12 28.35 4.81 4 10 8 28.98 3.55 4 11 -8 64.86 4.78 4 11 4 3.58 3.53 5 11 7 3.28 3.73 5 12 2 1.17 3.62 5 12 3 2.62 3.31 0 -18 -3 26.35 3.57 0 -18 -2 274.47 4.71 0 -18 -1 55.91 3.68 0 -17 -6 29.89 2.94 0 -17 2 11.22 3.49 0 -16 -9 51.21 3.91 0 -16 5 22.00 3.54 0 -15 -10 22.05 2.59 0 -15 6 116.16 4.29 0 -13 8 156.43 4.56 0 -12 -13 62.65 3.51 0 -11 -13 74.10 3.84 0 -11 9 23.85 4.22 0 -7 -13 25.50 2.67 0 -6 -13 335.25 4.79 0 -4 -12 84.20 3.49 1 -10 -20 23.99 3.45 1 -9 -20 9.15 3.80 1 -8 -20 17.64 4.05 1 0 -16 27.67 3.35 1 2 9 313.06 4.88 1 3 7 410.87 5.28 2 -10 19 2.35 5.02 2 -7 19 3.17 4.13 2 -4 -23 25.75 4.13 2 -2 -22 19.57 3.83 2 0 16 65.13 3.48 2 1 -20 17.74 3.90 2 2 -19 7.30 3.88 2 3 13 13.40 3.42 2 8 -5 1094.19 7.95 2 8 0 45.52 3.37 2 8 1 212.45 3.42 3 -5 21 3.12 4.59 3 -2 20 2.92 3.72 3 0 19 -1.55 3.20 3 1 -23 29.79 5.13 3 1 18 -0.02 3.74 3 7 11 33.42 2.48 3 8 9 27.85 2.23 3 9 6 48.63 2.65 3 10 -5 10.63 3.11 3 10 -4 108.03 3.57 3 10 -3 8.85 3.01 3 10 -2 78.62 3.75 3 10 -1 15.90 3.30 3 10 0 23.27 3.26 3 10 1 2.32 2.31 4 6 15 9.46 3.72 4 9 10 6.92 2.59 4 10 7 30.56 3.72 4 11 -7 51.09 4.42 4 11 2 33.84 3.39 4 11 3 17.06 3.25 5 10 9 -3.00 3.63 5 11 6 6.57 3.66 5 12 -5 39.77 4.03 5 12 -4 0.16 3.70 5 12 -1 13.16 3.84 5 12 0 2.48 3.76 5 12 1 12.67 3.36 0 -18 -5 100.93 3.93 0 -18 -4 35.07 2.74 0 -18 0 13.28 3.82 0 -18 1 53.48 3.73 0 -17 -9 11.07 3.43 0 -17 -8 1.86 2.85 0 -17 4 14.81 3.36 0 -16 -10 37.76 3.77 0 -15 -11 24.84 2.63 0 -13 -13 62.79 3.59 0 -12 9 42.66 4.95 0 -11 -14 19.67 3.45 0 -10 -14 12.49 3.74 0 -9 -14 -3.87 2.47 0 -8 -14 113.92 3.71 0 -7 -14 39.23 3.39 0 -2 -10 81.73 3.73 0 -1 -8 257.14 4.57 0 0 -5 1.44 3.57 1 -12 -20 46.26 4.19 1 -11 -20 31.42 2.86 1 -7 -20 14.06 2.85 1 -6 -20 3.80 3.72 1 -2 -18 120.98 3.92 1 1 -15 243.89 5.14 1 1 10 27.95 3.06 1 4 4 946.21 7.20 1 5 -1 518.02 6.26 2 -9 19 24.26 4.66 2 -4 18 11.15 3.46 2 -3 -23 6.83 4.63 2 0 -21 1.66 4.28 2 1 15 64.19 2.83 2 2 14 26.57 2.52 2 3 -18 93.62 5.43 2 8 -3 4.27 2.68 3 -6 21 -1.67 4.64 3 -1 19 11.83 3.39 3 2 17 65.60 3.56 3 3 16 8.59 3.37 3 4 15 14.40 2.44 3 6 12 59.24 3.43 3 7 10 30.24 3.21 3 8 -13 6.95 4.63 3 8 8 11.61 3.24 3 9 -10 66.49 3.77 3 9 5 61.43 3.20 4 2 19 8.89 2.93 4 3 18 8.08 3.33 4 4 17 8.33 3.41 4 5 16 7.38 2.88 4 7 13 13.72 3.20 4 8 11 44.55 3.55 4 10 6 100.54 4.22 4 11 -6 49.17 3.61 4 11 0 18.33 3.31 4 11 1 5.21 3.15 5 9 11 1.65 2.59 5 10 8 2.88 3.64 5 11 5 1.64 3.65 5 12 -3 18.78 2.93 5 12 -2 4.18 2.89 0 -19 -4 1.35 3.29 0 -19 -3 8.12 3.74 0 -19 -2 56.73 4.26 0 -19 -1 35.65 3.72 0 -18 -8 43.72 4.10 0 -18 -7 24.25 2.98 0 -18 2 275.69 4.69 0 -18 3 21.32 3.47 0 -17 -10 32.18 3.81 0 -17 5 23.81 4.18 0 -16 6 23.90 3.69 0 -15 -12 58.44 2.80 0 -14 -13 34.03 2.65 0 -14 8 201.48 4.69 0 -12 -14 44.96 2.65 0 -10 -15 74.90 3.82 0 -9 -15 34.81 3.60 0 -8 -15 244.04 4.06 0 -6 -14 10.39 3.39 0 -4 -13 147.27 3.74 1 -15 14 103.73 7.91 1 -10 -21 1.87 3.50 1 -9 -21 28.65 3.98 1 -8 -21 26.33 3.72 1 -5 -20 123.40 3.92 1 -4 14 283.49 5.41 1 3 -12 185.06 6.63 2 -5 -24 13.86 4.13 2 -1 -22 54.03 4.82 2 4 11 22.14 2.33 2 7 4 107.55 2.72 3 -3 20 4.78 3.50 3 5 13 55.35 3.79 4 1 19 1.04 3.84 4 6 14 36.57 3.44 4 9 8 23.66 3.45 4 10 -11 2.39 3.67 4 10 5 78.71 3.89 4 11 -5 2.06 3.18 4 11 -4 46.91 3.63 4 11 -3 41.89 3.85 4 11 -2 60.44 3.67 4 11 -1 3.90 2.57 5 8 12 0.76 3.04 5 9 10 5.54 3.07 5 10 7 -0.26 3.59 5 11 3 11.83 3.37 5 11 4 16.73 2.71 0 -19 -7 1.56 3.78 0 -19 -5 5.54 2.80 0 -19 0 3.16 3.72 0 -19 1 23.83 3.82 0 -18 -10 25.27 3.60 0 -18 -9 7.05 2.89 0 -18 4 30.48 3.57 0 -16 -12 19.75 2.79 0 -15 -13 11.50 2.47 0 -14 -14 36.09 3.63 0 -13 -15 33.26 3.28 0 -13 9 101.53 4.53 0 -12 -15 132.34 4.08 0 -7 -15 45.87 3.31 0 -2 -11 557.58 5.85 0 -2 5 3612.10 33.68 0 -1 -9 286.89 5.21 0 0 -6 1655.36 12.94 1 -11 -21 8.73 3.04 1 -7 -21 29.78 3.98 1 -4 -20 76.07 3.73 1 2 -14 27.05 3.87 1 2 8 19.89 2.30 1 3 6 175.66 3.60 1 4 3 16.59 2.85 2 -5 18 4.08 3.40 2 -4 -24 6.63 3.47 2 -1 16 63.13 3.34 2 0 15 -1.76 3.01 2 1 14 12.11 3.16 2 2 13 24.22 3.19 2 7 -9 136.80 4.98 2 7 3 307.61 4.39 3 -2 19 34.74 3.60 3 0 18 46.68 3.04 3 1 17 9.71 3.53 3 2 16 17.29 3.41 3 6 11 57.07 3.20 3 7 9 78.50 3.30 3 9 2 31.31 3.23 3 9 3 179.79 3.22 4 2 18 0.45 3.55 4 3 17 7.95 3.41 4 4 16 19.01 3.63 4 5 15 5.79 2.70 4 7 12 20.05 2.54 4 10 -10 14.37 4.22 4 10 4 11.38 3.18 5 7 13 2.13 3.26 5 8 11 8.11 3.16 5 9 9 10.63 3.33 5 10 6 27.19 3.53 5 11 -8 3.72 4.32 5 11 2 -0.27 3.40 0 -20 -5 10.20 3.85 0 -20 -4 49.40 4.06 0 -20 -3 31.20 4.04 0 -20 -2 23.31 4.14 0 -20 -1 3.47 3.62 0 -19 -9 7.68 4.03 0 -19 -8 29.95 3.14 0 -19 2 50.73 3.96 0 -18 -11 18.25 3.90 0 -17 -12 20.36 2.96 0 -17 6 29.13 3.90 0 -16 -13 6.74 2.60 0 -16 7 192.80 4.75 0 -15 -14 5.46 2.55 0 -15 8 39.54 4.33 0 -14 -15 5.48 3.56 0 -12 -16 18.88 3.76 0 -11 -16 116.17 4.16 0 -10 -16 110.81 3.94 0 -9 -16 8.96 3.42 0 -8 -16 11.39 3.36 0 -6 -15 110.18 2.94 0 -4 -14 276.94 4.32 0 -3 -13 149.37 3.67 1 -17 13 3.83 4.96 1 -11 15 29.21 7.83 1 -10 -22 18.95 3.62 1 -9 -22 4.54 3.50 1 -8 15 53.27 4.94 1 0 -17 3.51 3.12 1 1 9 502.37 5.69 2 -6 18 10.76 4.25 3 -5 20 0.76 4.39 3 5 12 26.71 3.38 3 7 -15 20.95 5.72 3 8 6 29.54 2.30 3 9 -8 114.35 4.10 3 9 1 18.90 3.29 4 0 19 4.86 3.66 4 5 14 19.72 3.57 4 6 13 11.53 2.57 4 7 -18 8.19 6.32 4 7 11 29.18 3.25 4 8 -16 -0.78 4.78 4 8 9 12.44 3.21 4 9 6 18.93 3.35 4 10 2 96.97 3.65 4 10 3 1.06 2.33 5 9 8 -2.11 3.22 5 10 5 2.22 3.55 5 11 -7 -0.07 3.59 5 11 -6 14.30 3.49 5 11 -1 -0.23 3.46 5 11 0 20.93 3.55 5 11 1 1.87 2.50 0 -20 1 5.23 3.70 0 -19 3 7.73 3.46 0 -18 -12 34.46 4.04 0 -17 -13 22.25 2.90 0 -16 -14 13.29 2.66 0 -15 -15 1.48 3.62 0 -14 -16 78.50 3.93 0 -14 9 2.82 3.68 0 -13 -16 13.09 2.77 0 -11 -17 96.59 3.79 0 -10 -17 14.14 3.31 0 -5 -15 64.54 3.56 0 -2 -12 40.29 3.25 0 -1 3 262.03 11.31 0 0 -7 1.12 2.95 1 -9 15 33.72 5.43 1 -8 -22 3.79 3.88 1 -7 -22 50.98 3.99 1 -5 14 114.02 4.20 1 -3 -20 43.06 3.49 1 0 10 165.04 3.97 1 1 -16 7.04 3.16 1 3 5 377.58 5.22 1 4 2 100.73 3.88 2 -4 17 23.67 4.02 2 -3 -24 1.90 3.87 2 -2 16 0.82 2.96 2 0 -22 62.75 4.63 2 1 -21 16.43 3.83 2 4 -17 37.70 6.19 2 7 -8 14.09 3.57 3 -3 19 27.87 3.93 3 -1 18 2.67 2.58 3 0 17 10.35 3.53 3 2 -23 25.10 5.34 3 4 13 23.00 3.45 3 6 10 108.56 2.70 3 8 -12 54.66 4.48 3 8 5 16.09 2.31 3 9 -7 257.68 4.73 3 9 -1 144.52 3.88 3 9 0 86.51 3.63 4 1 18 13.94 3.74 4 2 17 21.15 3.60 4 3 16 0.98 3.41 4 4 15 6.52 3.49 4 6 12 18.97 3.28 4 8 8 68.36 3.56 4 9 -13 72.59 4.83 4 10 -9 9.41 3.31 4 10 -8 42.60 4.43 4 10 1 45.41 3.51 5 7 12 -0.88 2.44 5 8 10 7.84 2.38 5 9 7 -1.29 3.37 5 10 4 11.63 3.50 5 11 -5 4.57 3.09 5 11 -4 31.33 3.79 5 11 -3 0.40 3.13 5 11 -2 -0.38 3.13 0 -20 2 31.73 3.86 0 -19 4 0.65 3.62 0 -18 6 63.07 4.10 0 -17 -14 3.04 2.83 0 -17 7 113.72 4.47 0 -16 -15 23.97 2.84 0 -16 8 72.82 4.59 0 -15 -16 66.92 4.00 0 -13 -17 25.57 3.83 0 -12 -17 81.85 3.19 0 -11 10 5.68 4.71 0 -10 10 209.64 7.52 0 -9 -17 111.43 3.12 0 -8 -17 159.64 4.04 0 -7 -17 21.75 3.15 0 -6 -16 68.38 2.65 0 -4 -15 68.67 3.27 0 -3 -14 96.21 3.33 1 -10 15 8.69 5.79 1 -4 -21 3.34 3.23 1 2 7 276.23 4.19 2 -13 18 10.80 6.43 2 -1 15 65.63 3.40 2 0 14 110.08 3.88 2 2 -20 5.82 3.73 2 2 12 6.38 3.16 2 6 -12 4.09 4.72 2 7 -7 54.39 3.89 3 -6 20 3.92 3.50 3 1 16 36.52 3.25 3 3 -22 44.72 5.85 3 5 11 53.58 3.30 3 6 -17 45.88 8.01 3 8 4 18.82 2.98 3 9 -6 143.89 4.10 3 9 -5 82.58 3.37 3 9 -4 34.85 3.00 3 9 -3 50.68 3.26 3 9 -2 65.76 3.39 4 -1 19 2.69 3.88 4 5 13 12.44 3.37 4 7 10 17.90 2.38 4 9 5 46.85 2.65 4 10 -7 2.40 3.19 4 10 -6 3.73 3.45 4 10 -2 42.49 3.55 4 10 -1 22.82 3.49 4 10 0 45.88 2.80 5 5 14 4.40 3.41 5 6 13 6.71 2.58 5 7 11 4.66 3.10 5 10 3 4.12 2.89 0 -20 3 26.46 4.08 0 -19 5 9.42 3.95 0 -16 -16 6.38 3.73 0 -15 -17 12.70 3.82 0 -15 9 16.86 3.87 0 -14 -17 48.56 2.95 0 -13 -18 26.01 3.59 0 -12 -18 12.01 3.96 0 -12 10 1.37 4.53 0 -11 -18 12.75 3.69 0 -10 -18 14.15 3.70 0 -9 -18 9.49 3.52 0 -6 -17 18.91 3.15 0 -2 -13 146.10 3.84 0 -1 -11 5.10 3.10 0 0 -8 83.68 3.85 1 -9 -23 13.44 3.09 1 -8 -23 17.94 4.19 1 -5 -22 10.08 3.38 1 -2 -20 29.56 3.56 1 0 -18 20.77 3.89 1 4 1 17.61 3.14 2 -8 18 3.75 3.81 2 -5 17 47.29 4.17 2 -2 -24 11.76 3.50 2 6 4 47.69 2.29 2 7 -2 17.10 2.84 2 7 -1 114.44 2.85 3 -7 20 2.52 4.03 3 -4 19 3.79 3.43 3 -2 18 2.90 2.50 3 4 12 14.77 3.17 3 8 3 90.32 3.43 4 0 18 25.27 3.74 4 1 17 6.30 3.50 4 3 15 15.64 3.50 4 6 11 2.05 3.00 4 8 7 56.45 2.63 4 9 4 17.85 2.45 4 10 -4 68.75 3.50 4 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3 1 180.11 4.69 1 4 -5 310.11 7.52 2 -10 17 22.62 4.29 2 -2 13 18.87 3.01 2 0 11 1.55 2.97 2 3 -20 23.92 5.37 2 6 -9 321.05 6.27 2 6 -4 57.40 3.30 3 -5 17 -0.25 3.07 3 -2 15 69.54 3.45 3 2 11 292.15 4.13 3 3 -23 16.39 8.44 3 6 3 9.37 3.02 3 7 -12 69.69 4.52 3 7 -1 95.87 3.42 4 -5 18 -3.02 3.36 4 -3 17 8.14 2.56 4 -2 16 2.28 3.49 4 3 11 19.34 2.90 4 8 -11 11.54 3.47 4 8 -3 56.72 3.13 4 8 -2 6.44 2.75 5 0 15 0.78 2.48 5 1 14 -1.66 2.58 5 4 10 0.14 2.78 5 5 8 0.87 2.74 5 6 6 9.10 2.73 5 7 3 38.52 3.04 5 8 -13 1.34 3.18 5 8 -1 4.51 2.72 5 8 0 5.50 2.07 -1 -20 0 16.75 4.01 -1 -19 1 34.65 3.94 -1 -16 4 28.49 3.57 -1 -15 -17 10.52 3.10 -1 -13 -18 15.17 3.78 -1 -10 -17 1.49 3.77 -1 -10 4 544.59 6.30 -1 -9 -17 -3.00 3.16 -1 -8 -16 29.49 3.54 -1 -8 3 328.57 5.39 -1 -7 2 236.22 4.86 -1 -5 -12 73.27 3.51 -1 -4 -8 844.14 6.55 -1 -4 -7 128.90 3.81 -1 -4 -6 101.54 3.70 -1 -4 -5 51.19 3.39 0 -14 11 119.79 6.48 0 -8 -23 5.02 3.96 0 -6 -22 19.02 3.62 0 -5 -21 7.96 3.53 0 -4 -20 128.32 4.01 0 -3 -19 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8.37 -2 15 -13 13.83 7.89 -1 3 -4 211.75 8.25 -1 8 -14 123.27 6.38 -1 14 -18 7.57 7.76 0 4 15 52.07 5.75 0 9 -19 5.28 6.08 0 10 21 5.74 7.42 1 1 -12 49.27 5.31 1 7 -20 9.28 6.70 1 8 22 17.19 7.54 2 -1 11 115.60 6.26 2 5 -20 30.77 6.23 4 2 18 1.81 7.55 -4 -9 -14 3.06 7.38 -4 -7 -17 3.40 5.83 -3 -14 -5 1.20 4.47 -3 -3 -9 185.36 5.73 -3 0 -16 39.24 3.98 -2 -13 0 62.70 3.62 -2 -12 0 44.01 3.74 -2 -11 0 222.36 4.78 -2 -7 -1 251.61 6.54 -2 1 -8 18.84 3.23 -2 2 -10 98.66 3.76 -2 3 -13 20.31 2.48 -2 4 -23 2.71 3.92 -2 4 -22 38.79 4.05 -2 4 -21 5.55 3.76 -2 4 -20 26.28 3.96 -2 4 -19 32.51 3.70 -2 4 -18 12.54 3.53 -2 4 -17 26.53 3.66 -1 -19 1 44.26 3.89 -1 -17 2 42.40 3.82 -1 -12 3 423.79 5.14 -1 -11 3 196.35 3.61 -1 2 -5 664.15 7.20 -1 6 -15 45.03 3.53 0 -17 4 17.96 3.40 0 4 -5 52.23 3.57 0 7 -12 378.94 4.80 0 8 -23 -0.46 3.75 0 8 -22 8.67 3.71 0 8 -21 44.09 3.85 0 8 -20 30.29 3.69 0 8 -19 6.94 3.36 0 8 -18 60.38 3.57 0 8 -17 160.49 3.77 1 -17 5 115.59 3.99 1 -6 5 115.38 3.42 1 7 -9 320.68 4.74 1 8 -12 61.73 3.58 1 9 -23 11.29 3.79 1 9 -22 5.66 4.02 1 9 -21 25.08 4.20 1 9 -20 2.60 3.87 1 9 -19 90.34 4.26 1 9 -18 58.39 3.88 2 -16 6 3.71 2.40 2 -15 6 59.21 3.63 2 -8 6 42.74 3.29 2 -5 5 52.83 3.27 2 3 -1 186.64 8.18 2 9 -15 22.42 3.08 3 -15 6 -0.19 3.33 3 -14 6 30.43 3.88 3 -9 6 35.58 3.24 3 8 -11 94.52 3.93 3 9 -15 39.00 3.72 4 -15 5 3.55 3.87 4 -5 4 123.76 3.75 4 -3 3 25.41 3.24 4 8 -13 12.82 3.54 5 -12 4 4.82 3.59 6 -5 0 2.69 3.68 -4 -7 -16 30.97 5.84 -4 -6 -18 6.00 5.59 -3 -16 -6 1.08 4.81 -3 -13 -5 20.70 4.57 -3 -10 -5 27.33 5.47 -3 -1 -12 89.98 4.12 -3 0 -15 -2.17 3.46 -3 1 -21 0.63 3.65 -3 1 -20 8.85 3.76 -2 -5 -2 128.98 7.99 -2 3 -12 166.83 4.29 -2 4 -16 114.66 4.07 -2 4 -15 95.73 3.60 -1 -20 0 20.86 3.93 -1 -18 1 13.70 4.07 -1 -16 2 68.74 3.70 -1 -7 2 267.28 4.80 -1 4 -8 903.13 6.72 -1 6 -14 275.65 3.69 0 -20 2 24.01 4.39 0 -18 3 11.72 3.75 0 -16 4 5.36 2.70 0 -7 4 521.67 5.29 0 8 -24 7.18 3.02 0 8 -16 4.16 3.34 0 8 -15 233.05 4.02 1 -19 4 33.62 2.86 1 -16 5 54.26 3.52 1 -4 4 811.79 7.04 1 4 -3 83.53 3.78 1 9 -17 65.40 3.04 1 9 -16 16.76 3.58 2 -18 5 33.79 2.92 2 -12 6 99.20 3.65 2 -10 6 106.97 3.46 2 -3 4 82.30 2.91 2 1 1 177.62 7.40 2 8 -10 11.96 2.74 2 9 -14 27.09 2.38 3 -17 5 7.73 3.95 3 -13 6 19.55 2.59 3 -12 6 22.17 3.09 3 -11 6 1.69 2.87 3 -10 6 33.37 2.38 3 -6 5 219.55 4.00 3 9 -14 5.68 3.41 4 -14 5 0.03 3.34 4 -13 5 34.36 3.76 4 -12 5 16.45 3.65 4 -11 5 0.27 3.21 4 -10 5 75.91 3.73 4 -9 5 41.96 3.40 4 6 -7 18.24 3.54 5 -7 3 48.17 3.73 5 6 -10 0.69 3.64 5 7 -13 7.62 4.07 6 -6 0 1.37 4.11 6 -4 -1 2.38 4.73 -4 -7 -15 17.23 6.01 -4 -6 -17 7.59 5.52 -3 -17 -7 18.28 5.09 -3 -12 -5 36.73 4.78 -3 -11 -5 6.09 4.65 -3 -2 -10 49.36 3.84 -3 0 -14 117.91 4.12 -3 1 -22 -1.41 3.24 -3 1 -19 1.83 2.74 -3 1 -18 7.50 3.85 -3 1 -17 8.97 3.69 -2 -2 -4 518.59 9.35 -2 -1 -5 187.60 5.30 -2 2 -9 11.32 2.78 -2 3 -11 104.15 3.59 -2 4 -14 51.74 3.36 -1 -19 0 51.25 4.01 -1 -15 2 31.67 3.19 -1 -3 0 488.68 10.60 -1 3 -6 166.68 4.51 -1 5 -10 235.53 3.54 -1 6 -13 198.78 3.29 -1 7 -24 9.28 4.20 -1 7 -23 9.85 3.95 -1 7 -22 7.51 3.04 -1 7 -21 6.34 2.89 -1 7 -20 5.71 2.96 -1 7 -18 32.03 3.31 0 -15 4 91.89 3.09 0 -14 4 65.20 3.77 0 -8 4 345.53 4.72 0 2 -2 175.72 4.98 0 7 -11 156.45 3.08 1 -20 3 -0.46 3.03 1 -18 4 3.72 3.15 1 -15 5 71.95 3.19 1 -7 5 76.16 2.45 1 6 -6 27.03 3.11 1 7 -8 242.45 4.22 1 8 -11 54.74 2.74 1 9 -15 63.17 2.91 1 9 -14 178.78 3.85 2 -19 4 2.97 3.59 2 -16 5 71.20 3.40 2 -11 6 23.98 2.35 2 -6 5 56.41 3.18 2 7 -7 45.55 2.58 2 9 -13 47.96 2.34 2 10 -21 28.76 3.71 2 10 -20 21.52 3.32 2 10 -19 4.45 3.20 2 10 -18 29.32 3.03 3 -16 5 80.19 3.89 3 -4 4 141.54 3.53 3 -2 3 26.90 3.05 3 8 -10 28.45 3.43 3 9 -13 21.23 3.45 3 10 -19 2.15 3.71 4 -6 4 1.91 3.02 4 -2 2 64.45 4.03 4 5 -5 109.86 5.66 4 7 -9 77.33 3.61 4 8 -12 7.12 3.68 4 9 -17 50.27 4.10 4 9 -16 3.11 3.62 5 -9 3 0.62 3.21 5 -8 3 4.47 3.08 5 -5 2 3.93 3.36 5 -3 1 2.22 3.13 -4 -6 -16 10.74 5.24 -4 -5 -18 -0.81 4.97 -3 -15 -6 -0.16 4.26 -3 -1 -11 29.65 3.24 -3 0 -13 2.25 3.24 -3 1 -16 30.05 3.61 -2 0 -6 1924.08 11.68 -2 4 -13 118.00 3.63 -2 5 -23 23.11 4.01 -2 5 -22 15.98 3.10 -2 5 -21 0.95 2.78 -2 5 -20 32.30 2.81 -2 5 -19 16.51 3.64 -2 5 -18 2.64 3.40 -2 5 -17 41.65 3.31 -1 -14 2 5.84 2.40 -1 -13 2 48.87 3.41 -1 -8 2 525.41 5.79 -1 6 -12 86.15 3.51 -1 7 -16 17.37 3.33 0 -19 2 56.92 3.00 0 -17 3 52.14 2.88 0 -13 4 24.52 3.09 0 -12 4 15.97 3.31 0 -11 4 378.42 4.79 0 -3 2 82.80 4.22 0 3 -3 126.21 4.37 0 5 -6 319.06 4.27 0 7 -10 127.11 3.62 0 9 -23 2.56 3.92 0 9 -22 15.09 3.72 0 9 -21 47.10 4.00 0 9 -20 15.07 3.53 0 9 -19 1.63 3.35 1 -19 3 39.92 3.73 1 -17 4 3.54 3.13 1 -14 5 25.99 2.22 1 -1 2 751.92 9.29 1 8 -10 74.67 3.46 1 9 -13 371.27 4.42 1 10 -22 3.63 3.67 1 10 -21 -1.43 3.77 1 10 -20 14.06 3.47 2 -18 4 107.24 3.96 2 -15 5 37.26 3.23 2 6 -5 75.94 3.13 2 8 -9 511.93 4.76 2 9 -12 67.87 3.03 2 10 -17 9.71 2.90 2 10 -16 104.39 2.97 3 -17 4 -1.98 3.69 3 -15 5 7.91 2.56 3 -14 5 5.08 3.53 3 -8 5 15.13 3.00 3 -7 5 73.42 2.55 3 7 -7 27.71 3.65 3 10 -18 2.05 3.95 3 10 -17 5.58 3.69 4 -15 4 3.24 3.27 4 -14 4 -3.55 3.43 4 -7 4 65.18 3.18 4 9 -15 22.67 3.66 5 -12 3 1.89 2.78 5 -11 3 11.55 3.27 5 -10 3 7.86 3.23 5 -6 2 31.12 3.72 5 7 -12 4.09 3.93 6 -3 -2 16.59 4.34 -4 -5 -17 14.35 5.05 -3 1 -15 33.39 3.39 -3 2 -22 2.08 4.26 -3 2 -21 15.51 4.20 -3 2 -20 1.32 3.85 -3 2 -19 44.96 4.02 -3 2 -18 2.97 3.45 -2 -13 -1 108.48 3.92 -2 -12 -1 87.22 4.31 -2 1 -7 368.12 5.32 -2 3 -10 92.39 3.44 -2 5 -16 130.91 3.81 -1 -18 0 14.37 3.67 -1 -16 1 51.13 3.67 -1 -12 2 35.55 3.15 -1 -11 2 186.24 4.00 -1 -10 2 12.98 2.92 -1 4 -7 140.82 3.72 -1 5 -9 45.34 2.30 -1 6 -11 31.69 3.03 -1 7 -15 73.62 2.63 -1 7 -14 54.57 3.01 0 -20 1 6.16 2.95 0 -18 2 247.17 4.54 0 -16 3 247.41 3.70 0 8 -12 5.84 2.79 0 9 -18 8.64 2.48 0 9 -17 116.22 3.84 1 -20 2 -0.03 3.50 1 -18 3 16.77 3.34 1 -16 4 19.01 3.17 1 -5 4 432.57 4.65 1 5 -4 260.84 4.62 1 10 -19 22.55 2.81 1 10 -18 90.38 3.99 1 10 -17 8.92 3.46 2 -17 4 -0.01 3.15 2 -14 5 2.67 2.71 2 -13 5 372.75 4.33 2 -8 5 292.32 4.21 2 -7 5 177.26 3.27 2 -4 4 496.42 5.46 2 -2 3 135.83 3.99 2 9 -11 11.05 2.53 2 10 -15 13.01 2.70 3 -16 4 4.12 3.61 3 -13 5 22.24 2.49 3 -12 5 34.58 3.35 3 -11 5 11.32 3.08 3 -10 5 29.52 3.11 3 -9 5 53.24 3.05 3 8 -9 50.75 3.37 3 9 -12 31.70 3.46 4 -13 4 10.94 3.30 4 -9 4 19.22 3.28 4 -8 4 26.60 3.01 4 8 -11 12.02 3.33 5 -4 1 10.18 3.71 5 -2 0 19.71 3.17 6 -5 -1 17.59 3.58 -4 -4 -19 1.37 4.56 -3 -16 -7 31.74 4.35 -3 -2 -9 257.08 5.32 -3 1 -14 23.20 3.26 -3 2 -17 55.83 3.82 -2 -11 -1 37.57 3.35 -2 -10 -1 25.59 3.24 -2 2 -8 620.89 5.96 -2 4 -12 246.90 4.36 -2 5 -15 2.91 3.16 -2 6 -23 6.29 3.57 -2 6 -22 10.45 3.61 -2 6 -21 21.34 3.50 -2 6 -20 0.38 3.42 -1 -19 -1 18.04 3.71 -1 -15 1 4.61 3.10 -1 8 -23 4.64 2.91 -1 8 -21 25.32 2.85 -1 8 -20 21.32 2.64 -1 8 -18 25.73 3.40 0 -17 2 5.20 3.42 0 -15 3 24.03 2.58 0 -6 3 74.46 3.69 0 6 -7 52.48 3.13 0 7 -9 83.51 3.35 0 9 -16 8.88 2.28 0 9 -15 29.92 3.56 1 -15 4 64.09 2.94 1 -3 3 633.70 6.61 1 7 -7 78.15 3.24 1 8 -9 199.70 3.90 1 9 -12 233.54 3.97 1 10 -16 -2.66 3.19 2 -18 3 8.30 3.41 2 -16 4 15.32 3.04 2 -12 5 272.85 3.88 2 -11 5 54.28 2.92 2 -10 5 37.27 2.99 2 -9 5 130.20 3.57 2 10 -14 118.47 3.36 3 -15 4 49.72 3.64 3 -5 4 136.91 2.86 3 -1 2 56.28 3.35 3 6 -5 112.93 4.03 3 9 -11 124.16 3.83 3 10 -15 22.16 3.38 4 -15 3 4.57 3.64 4 -11 4 4.68 2.31 4 -10 4 13.60 2.43 4 -5 3 34.42 3.05 5 -12 2 4.15 3.54 5 -8 2 17.43 3.26 5 -7 2 3.68 2.86 6 -6 -1 0.80 3.65 -2 5 -14 15.15 2.31 -2 6 -19 8.54 2.73 -1 -17 0 55.90 3.14 -1 8 -17 19.84 2.38 0 -14 3 25.18 2.43 1 -19 2 65.79 2.93 1 -17 3 14.47 2.42 1 -14 4 14.30 2.11 1 -6 4 153.05 2.99 1 10 -15 41.65 2.52 2 11 -20 7.88 2.62 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 34412 _shelx_res_file ; TITL g73_a.res in Pc g73.res created by SHELXL-2018/1 at 13:24:59 on 10-Jul-2020 REM Old TITL G73 LIGAND REM SHELXT solution in Pc REM R1 0.116, Rweak 0.020, Alpha 0.006, Orientation as input REM Flack x = 0.104 ( 0.028 ) from Parsons' quotients REM Formula found by SHELXT: C28 Br2 N4 O2 S2 CELL 0.71073 4.6404 15.0174 19.074 90 91.052 90 ZERR 4 0.0007 0.0024 0.0025 0 0.012 0 LATT -1 SYMM +X,-Y,0.5+Z SFAC C H Br N O S UNIT 56 44 4 8 4 4 EQIV $1 -1+X,-1+Y,+Z EQIV $2 1+X,1+Y,+Z L.S. 10 PLAN 2 SIZE 0.04 0.052 0.678 TEMP -148.15 HTAB N2 O1 HTAB N2A O1A HTAB N1 S1A_$1 HTAB N1A S1_$2 list 4 BOND $H MERG MORE -1 HTAB fmap 2 53 acta OMIT -2 52 OMIT 1 5 11 OMIT 0 5 11 REM REM REM WGHT 0.143600 FVAR 0.34070 BR1A 3 0.121563 0.360146 0.600488 11.00000 0.04155 0.02330 = 0.03703 0.00175 0.00632 -0.00426 BR1 3 0.847177 0.397776 0.388041 11.00000 0.04737 0.02154 = 0.04043 0.00022 0.00915 -0.00661 S1 6 0.219299 -0.051819 0.423204 11.00000 0.04761 0.01932 = 0.03285 -0.00335 0.01469 -0.00212 S1A 6 0.835627 0.799206 0.587133 11.00000 0.05496 0.02259 = 0.03475 -0.00720 0.02018 -0.00133 O1A 5 1.111416 0.570501 0.449073 11.00000 0.03723 0.02158 = 0.02894 -0.00095 0.00494 -0.00663 O1 5 -0.122882 0.182588 0.546079 11.00000 0.03689 0.02016 = 0.02950 0.00089 0.00588 -0.00122 N2 4 0.201099 0.126684 0.446058 11.00000 0.02979 0.02110 = 0.02062 -0.00459 0.00546 -0.00092 AFIX 43 H2 2 0.116675 0.168717 0.470412 11.00000 -1.20000 AFIX 0 N2A 4 0.814232 0.624670 0.554828 11.00000 0.02924 0.02396 = 0.02769 -0.00392 0.00592 -0.00068 AFIX 43 H2A 2 0.886318 0.584080 0.526870 11.00000 -1.20000 AFIX 0 N1A 4 1.130364 0.711459 0.493640 11.00000 0.02875 0.01995 = 0.02864 -0.00223 0.00756 -0.00490 AFIX 43 H1A 2 1.221915 0.762601 0.490681 11.00000 -1.20000 AFIX 0 N1 4 -0.098513 0.038217 0.510796 11.00000 0.02669 0.01930 = 0.03025 0.00163 0.00606 -0.00298 AFIX 43 H1 2 -0.172561 -0.015048 0.517202 11.00000 -1.20000 AFIX 0 C12 1 -0.483748 0.144453 0.655878 11.00000 0.03319 0.02624 = 0.03016 -0.00384 0.00546 0.00695 AFIX 43 H12 2 -0.404248 0.202517 0.652126 11.00000 -1.20000 AFIX 0 C10 1 -0.204048 0.104555 0.552791 11.00000 0.01986 0.02177 = 0.02415 -0.00036 -0.00027 -0.00291 C1 1 0.110936 0.044145 0.459236 11.00000 0.03002 0.02480 = 0.02305 0.00078 0.00253 0.00135 C22A 1 0.527379 0.634555 0.663336 11.00000 0.03273 0.02872 = 0.01953 -0.00298 0.00668 -0.00387 AFIX 43 H22A 2 0.609316 0.690436 0.675859 11.00000 -1.20000 AFIX 0 C24 1 0.806103 0.236286 0.309912 11.00000 0.03374 0.02809 = 0.02684 0.00594 0.00643 -0.00597 AFIX 43 H24 2 0.940707 0.263197 0.279534 11.00000 -1.20000 AFIX 0 C11A 1 1.418072 0.672291 0.392588 11.00000 0.02422 0.01968 = 0.02296 -0.00147 0.00201 0.00322 C23A 1 0.330572 0.594100 0.705780 11.00000 0.03647 0.03604 = 0.02592 -0.00353 -0.00288 0.00640 AFIX 43 H23A 2 0.278747 0.622390 0.748276 11.00000 -1.20000 AFIX 0 C26 1 0.510334 0.244592 0.411880 11.00000 0.02864 0.01809 = 0.02798 0.00142 0.00218 0.00901 AFIX 43 H26 2 0.441157 0.277844 0.450456 11.00000 -1.20000 AFIX 0 C21 1 0.410202 0.156886 0.399261 11.00000 0.03118 0.02561 = 0.02587 0.00218 -0.00083 0.00253 C25 1 0.707068 0.280703 0.368028 11.00000 0.03557 0.02428 = 0.02843 -0.00421 -0.00071 0.00835 C26A 1 0.484523 0.509283 0.582899 11.00000 0.02999 0.02840 = 0.01988 -0.00250 0.00388 0.00698 AFIX 43 H26A 2 0.539187 0.479402 0.541306 11.00000 -1.20000 AFIX 0 C13A 1 1.635058 0.632493 0.284126 11.00000 0.03080 0.02398 = 0.02877 -0.00525 0.00726 0.00131 AFIX 43 H13A 2 1.656135 0.591839 0.246407 11.00000 -1.20000 AFIX 0 C11 1 -0.412565 0.078956 0.607268 11.00000 0.01906 0.02174 = 0.02922 -0.00064 -0.00267 0.00242 C23 1 0.702491 0.150992 0.297329 11.00000 0.03971 0.02838 = 0.02467 0.00018 0.00465 -0.00341 AFIX 43 H23 2 0.768490 0.119194 0.257672 11.00000 -1.20000 AFIX 0 C13 1 -0.667480 0.125118 0.708785 11.00000 0.03038 0.03337 = 0.02962 -0.00938 0.00430 0.00078 AFIX 43 H13 2 -0.711529 0.169799 0.742179 11.00000 -1.20000 AFIX 0 C21A 1 0.605551 0.591420 0.600686 11.00000 0.02722 0.02319 = 0.02322 0.00010 0.00147 0.00532 C10A 1 1.206051 0.646170 0.446622 11.00000 0.02789 0.02340 = 0.01952 -0.00365 0.00364 0.00128 C16 1 -0.534842 -0.005357 0.613207 11.00000 0.03315 0.02360 = 0.02574 -0.00120 0.00426 -0.00040 AFIX 43 H16 2 -0.488645 -0.050385 0.580284 11.00000 -1.20000 AFIX 0 C1A 1 0.921720 0.704524 0.545805 11.00000 0.02631 0.02298 = 0.02697 -0.00181 -0.00207 -0.00156 C24A 1 0.204613 0.512500 0.688143 11.00000 0.02676 0.02737 = 0.03021 0.00964 0.00355 -0.00002 AFIX 43 H24A 2 0.067460 0.485458 0.717769 11.00000 -1.20000 AFIX 0 C14A 1 1.791965 0.710235 0.284871 11.00000 0.02759 0.04143 = 0.03289 -0.00190 0.00118 0.00014 AFIX 43 H14A 2 1.921841 0.722651 0.248208 11.00000 -1.20000 AFIX 0 C22 1 0.503982 0.110596 0.341311 11.00000 0.03578 0.02162 = 0.03261 -0.00295 -0.00119 -0.00042 AFIX 43 H22 2 0.434508 0.052300 0.331595 11.00000 -1.20000 AFIX 0 C25A 1 0.284788 0.472287 0.626568 11.00000 0.03319 0.01660 = 0.02980 0.00023 -0.00273 0.00298 C12A 1 1.447046 0.612489 0.337374 11.00000 0.02814 0.02263 = 0.03087 -0.00343 0.00849 -0.00847 AFIX 43 H12A 2 1.339264 0.558708 0.336270 11.00000 -1.20000 AFIX 0 C14 1 -0.789935 0.042266 0.714667 11.00000 0.02349 0.03277 = 0.02422 0.00220 0.00310 0.00024 AFIX 43 H14 2 -0.919974 0.030087 0.751344 11.00000 -1.20000 AFIX 0 C15 1 -0.721807 -0.023916 0.666322 11.00000 0.03578 0.02560 = 0.03024 0.00331 0.00305 -0.00406 AFIX 43 H15 2 -0.804361 -0.081564 0.670121 11.00000 -1.20000 AFIX 0 C15A 1 1.759605 0.770935 0.339801 11.00000 0.03408 0.02565 = 0.03365 0.00168 0.00266 -0.00754 AFIX 43 H15A 2 1.865168 0.825140 0.340197 11.00000 -1.20000 AFIX 0 C16A 1 1.574425 0.751850 0.393222 11.00000 0.03054 0.02171 = 0.03562 -0.00558 0.00133 0.00526 AFIX 43 H16A 2 1.552695 0.792864 0.430674 11.00000 -1.20000 AFIX 0 HKLF 4 REM g73_a.res in Pc REM R1 = 0.0656 for 4294 Fo > 4sig(Fo) and 0.0761 for all 4909 data REM 343 parameters refined using 2 restraints END WGHT 0.1436 0.0000 REM Instructions for potential hydrogen bonds HTAB N2 O1 HTAB N2A O1A HTAB C22A S1A HTAB C22 S1 REM Highest difference peak 1.967, deepest hole -0.654, 1-sigma level 0.151 Q1 1 1.1210 0.8561 0.6025 11.00000 0.05 1.97 Q2 1 1.8543 0.8926 0.3878 11.00000 0.05 1.68 ; _shelx_res_checksum 25907 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br Br1A 0.1216(2) 0.36015(7) 0.60049(6) 0.0339(3) Uani d 1 . . Br Br1 0.8472(2) 0.39778(7) 0.38804(7) 0.0363(3) Uani d 1 . . S S1 0.2193(7) -0.05182(18) 0.42320(16) 0.0331(6) Uani d 1 . . S S1A 0.8356(7) 0.7992(2) 0.58713(17) 0.0372(7) Uani d 1 . . O O1A 1.1114(18) 0.5705(5) 0.4491(4) 0.0292(17) Uani d 1 . . O O1 -0.1229(18) 0.1826(5) 0.5461(4) 0.0288(17) Uani d 1 . . N N2 0.201(2) 0.1267(7) 0.4461(5) 0.0238(19) Uani d 1 . . H H2 0.116675 0.168717 0.470412 0.029 Uiso calc 1 . . N N2A 0.814(2) 0.6247(7) 0.5548(5) 0.027(2) Uani d 1 . . H H2A 0.886318 0.584080 0.526870 0.032 Uiso calc 1 . . N N1A 1.130(2) 0.7115(6) 0.4936(5) 0.0257(18) Uani d 1 . . H H1A 1.221915 0.762601 0.490681 0.031 Uiso calc 1 . . N N1 -0.099(2) 0.0382(6) 0.5108(5) 0.0253(18) Uani d 1 . . H H1 -0.172561 -0.015048 0.517202 0.030 Uiso calc 1 . . C C12 -0.484(3) 0.1445(8) 0.6559(7) 0.030(3) Uani d 1 . . H H12 -0.404248 0.202517 0.652126 0.036 Uiso calc 1 . . C C10 -0.204(2) 0.1046(7) 0.5528(6) 0.022(2) Uani d 1 . . C C1 0.111(2) 0.0441(7) 0.4592(6) 0.026(2) Uani d 1 . . C C22A 0.527(3) 0.6346(8) 0.6633(6) 0.027(2) Uani d 1 . . H H22A 0.609316 0.690436 0.675859 0.032 Uiso calc 1 . . C C24 0.806(3) 0.2363(8) 0.3099(6) 0.029(2) Uani d 1 . . H H24 0.940707 0.263197 0.279534 0.035 Uiso calc 1 . . C C11A 1.418(2) 0.6723(7) 0.3926(5) 0.022(2) Uani d 1 . . C C23A 0.331(3) 0.5941(9) 0.7058(6) 0.033(3) Uani d 1 . . H H23A 0.278747 0.622390 0.748276 0.039 Uiso calc 1 . . C C26 0.510(2) 0.2446(7) 0.4119(6) 0.025(2) Uani d 1 . . H H26 0.441157 0.277844 0.450456 0.030 Uiso calc 1 . . C C21 0.410(3) 0.1569(8) 0.3993(6) 0.028(2) Uani d 1 . . C C25 0.707(3) 0.2807(8) 0.3680(6) 0.029(2) Uani d 1 . . C C26A 0.485(2) 0.5093(8) 0.5829(6) 0.026(2) Uani d 1 . . H H26A 0.539187 0.479402 0.541306 0.031 Uiso calc 1 . . C C13A 1.635(3) 0.6325(7) 0.2841(6) 0.028(2) Uani d 1 . . H H13A 1.656135 0.591839 0.246407 0.033 Uiso calc 1 . . C C11 -0.413(2) 0.0790(7) 0.6073(6) 0.023(2) Uani d 1 . . C C23 0.702(3) 0.1510(8) 0.2973(6) 0.031(2) Uani d 1 . . H H23 0.768490 0.119194 0.257672 0.037 Uiso calc 1 . . C C13 -0.667(3) 0.1251(9) 0.7088(6) 0.031(2) Uani d 1 . . H H13 -0.711529 0.169799 0.742179 0.037 Uiso calc 1 . . C C21A 0.606(3) 0.5914(7) 0.6007(6) 0.025(2) Uani d 1 . . C C10A 1.206(3) 0.6462(7) 0.4466(6) 0.024(2) Uani d 1 . . C C16 -0.535(3) -0.0054(8) 0.6132(6) 0.027(2) Uani d 1 . . H H16 -0.488645 -0.050385 0.580284 0.033 Uiso calc 1 . . C C1A 0.922(2) 0.7045(7) 0.5458(6) 0.025(2) Uani d 1 . . C C24A 0.205(2) 0.5125(8) 0.6881(6) 0.028(2) Uani d 1 . . H H24A 0.067460 0.485458 0.717769 0.034 Uiso calc 1 . . C C14A 1.792(3) 0.7102(9) 0.2849(7) 0.034(3) Uani d 1 . . H H14A 1.921841 0.722651 0.248208 0.041 Uiso calc 1 . . C C22 0.504(3) 0.1106(8) 0.3413(7) 0.030(3) Uani d 1 . . H H22 0.434508 0.052300 0.331595 0.036 Uiso calc 1 . . C C25A 0.285(2) 0.4723(7) 0.6266(6) 0.027(2) Uani d 1 . . C C12A 1.447(3) 0.6125(8) 0.3374(7) 0.027(2) Uani d 1 . . H H12A 1.339264 0.558708 0.336270 0.033 Uiso calc 1 . . C C14 -0.790(2) 0.0423(8) 0.7147(6) 0.027(2) Uani d 1 . . H H14 -0.919974 0.030087 0.751344 0.032 Uiso calc 1 . . C C15 -0.722(3) -0.0239(8) 0.6663(6) 0.031(2) Uani d 1 . . H H15 -0.804361 -0.081564 0.670121 0.037 Uiso calc 1 . . C C15A 1.760(3) 0.7709(8) 0.3398(6) 0.031(2) Uani d 1 . . H H15A 1.865168 0.825140 0.340197 0.037 Uiso calc 1 . . C C16A 1.574(3) 0.7518(8) 0.3932(6) 0.029(2) Uani d 1 . . H H16A 1.552695 0.792864 0.430674 0.035 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Br1A 0.0415(6) 0.0233(6) 0.0370(6) -0.0043(5) 0.0063(4) 0.0017(5) Br1 0.0474(7) 0.0215(6) 0.0404(6) -0.0066(5) 0.0091(5) 0.0002(5) S1 0.0476(17) 0.0193(12) 0.0329(14) -0.0021(11) 0.0147(12) -0.0033(10) S1A 0.0550(19) 0.0226(13) 0.0347(14) -0.0013(13) 0.0202(13) -0.0072(11) O1A 0.037(4) 0.022(4) 0.029(4) -0.007(3) 0.005(3) -0.001(3) O1 0.037(4) 0.020(4) 0.029(4) -0.001(3) 0.006(3) 0.001(3) N2 0.030(5) 0.021(4) 0.021(4) -0.001(4) 0.005(4) -0.005(4) N2A 0.029(5) 0.024(4) 0.028(5) -0.001(4) 0.006(4) -0.004(4) N1A 0.029(5) 0.020(4) 0.029(4) -0.005(4) 0.008(4) -0.002(4) N1 0.027(4) 0.019(4) 0.030(5) -0.003(4) 0.006(4) 0.002(4) C12 0.033(6) 0.026(6) 0.030(6) 0.007(5) 0.005(5) -0.004(5) C10 0.020(5) 0.022(6) 0.024(5) -0.003(4) 0.000(4) 0.000(4) C1 0.030(5) 0.025(5) 0.023(5) 0.001(4) 0.003(4) 0.001(4) C22A 0.033(6) 0.029(6) 0.020(5) -0.004(4) 0.007(4) -0.003(4) C24 0.034(6) 0.028(6) 0.027(5) -0.006(5) 0.006(4) 0.006(4) C11A 0.024(5) 0.020(5) 0.023(5) 0.003(4) 0.002(4) -0.001(4) C23A 0.036(6) 0.036(7) 0.026(6) 0.006(5) -0.003(5) -0.004(4) C26 0.029(5) 0.018(5) 0.028(5) 0.009(4) 0.002(4) 0.001(4) C21 0.031(6) 0.026(5) 0.026(5) 0.003(4) -0.001(4) 0.002(4) C25 0.036(6) 0.024(5) 0.028(5) 0.008(5) -0.001(5) -0.004(4) C26A 0.030(6) 0.028(5) 0.020(5) 0.007(4) 0.004(4) -0.003(4) C13A 0.031(6) 0.024(5) 0.029(6) 0.001(4) 0.007(5) -0.005(4) C11 0.019(5) 0.022(4) 0.029(5) 0.002(4) -0.003(4) -0.001(4) C23 0.040(7) 0.028(6) 0.025(5) -0.003(5) 0.005(5) 0.000(4) C13 0.030(6) 0.033(6) 0.030(6) 0.001(5) 0.004(5) -0.009(5) C21A 0.027(5) 0.023(5) 0.023(5) 0.005(5) 0.001(4) 0.000(4) C10A 0.028(5) 0.023(6) 0.020(5) 0.001(4) 0.004(4) -0.004(4) C16 0.033(6) 0.024(5) 0.026(5) 0.000(4) 0.004(4) -0.001(4) C1A 0.026(5) 0.023(5) 0.027(5) -0.002(4) -0.002(4) -0.002(4) C24A 0.027(5) 0.027(5) 0.030(6) 0.000(4) 0.004(4) 0.010(4) C14A 0.028(6) 0.041(7) 0.033(6) 0.000(5) 0.001(4) -0.002(5) C22 0.036(7) 0.022(6) 0.033(6) 0.000(4) -0.001(5) -0.003(4) C25A 0.033(6) 0.017(5) 0.030(6) 0.003(4) -0.003(5) 0.000(4) C12A 0.028(6) 0.023(6) 0.031(6) -0.008(4) 0.008(4) -0.003(5) C14 0.023(5) 0.033(6) 0.024(5) 0.000(4) 0.003(4) 0.002(4) C15 0.036(6) 0.026(5) 0.030(6) -0.004(4) 0.003(5) 0.003(4) C15A 0.034(6) 0.026(5) 0.034(6) -0.008(4) 0.003(5) 0.002(5) C16A 0.031(6) 0.022(5) 0.036(6) 0.005(4) 0.001(5) -0.006(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C1 N2 H2 . . 115.0 ? C1 N2 C21 . . 130.0(11) ? C21 N2 H2 . . 115.0 ? C21A N2A H2A . . 113.8 ? C1A N2A H2A . . 113.8 ? C1A N2A C21A . . 132.3(10) ? C10A N1A H1A . . 116.7 ? C10A N1A C1A . . 126.5(9) ? C1A N1A H1A . . 116.7 ? C10 N1 H1 . . 115.7 ? C10 N1 C1 . . 128.6(9) ? C1 N1 H1 . . 115.7 ? C11 C12 H12 . . 120.0 ? C13 C12 H12 . . 120.0 ? C13 C12 C11 . . 120.0(12) ? O1 C10 N1 . . 120.9(11) ? O1 C10 C11 . . 121.4(10) ? N1 C10 C11 . . 117.7(9) ? N2 C1 S1 . . 128.6(10) ? N2 C1 N1 . . 114.6(10) ? N1 C1 S1 . . 116.8(8) ? C23A C22A H22A . . 120.7 ? C23A C22A C21A . . 118.7(11) ? C21A C22A H22A . . 120.7 ? C25 C24 H24 . . 121.1 ? C25 C24 C23 . . 117.8(11) ? C23 C24 H24 . . 121.1 ? C12A C11A C10A . . 115.3(10) ? C12A C11A C16A . . 120.0(11) ? C16A C11A C10A . . 124.6(10) ? C22A C23A H23A . . 119.1 ? C22A C23A C24A . . 121.8(12) ? C24A C23A H23A . . 119.1 ? C21 C26 H26 . . 120.4 ? C25 C26 H26 . . 120.4 ? C25 C26 C21 . . 119.2(11) ? N2 C21 C26 . . 114.9(10) ? C22 C21 N2 . . 125.2(11) ? C22 C21 C26 . . 119.8(12) ? C24 C25 Br1 . . 119.2(9) ? C26 C25 Br1 . . 118.2(9) ? C26 C25 C24 . . 122.5(11) ? C21A C26A H26A . . 120.6 ? C25A C26A H26A . . 120.6 ? C25A C26A C21A . . 118.9(10) ? C14A C13A H13A . . 119.4 ? C14A C13A C12A . . 121.1(11) ? C12A C13A H13A . . 119.4 ? C12 C11 C10 . . 116.6(11) ? C16 C11 C12 . . 119.0(12) ? C16 C11 C10 . . 124.4(10) ? C24 C23 H23 . . 119.1 ? C24 C23 C22 . . 121.8(12) ? C22 C23 H23 . . 119.1 ? C12 C13 H13 . . 119.4 ? C12 C13 C14 . . 121.2(11) ? C14 C13 H13 . . 119.4 ? N2A C21A C22A . . 123.6(10) ? C26A C21A N2A . . 116.2(10) ? C26A C21A C22A . . 120.2(12) ? O1A C10A N1A . . 122.8(11) ? O1A C10A C11A . . 121.0(10) ? N1A C10A C11A . . 116.2(9) ? C11 C16 H16 . . 119.7 ? C15 C16 C11 . . 120.5(11) ? C15 C16 H16 . . 119.7 ? N2A C1A S1A . . 128.2(10) ? N2A C1A N1A . . 115.4(10) ? N1A C1A S1A . . 116.3(8) ? C23A C24A H24A . . 120.9 ? C25A C24A C23A . . 118.1(11) ? C25A C24A H24A . . 120.9 ? C13A C14A H14A . . 120.1 ? C13A C14A C15A . . 119.8(12) ? C15A C14A H14A . . 120.1 ? C21 C22 C23 . . 118.9(11) ? C21 C22 H22 . . 120.6 ? C23 C22 H22 . . 120.6 ? C26A C25A Br1A . . 117.9(8) ? C26A C25A C24A . . 122.3(11) ? C24A C25A Br1A . . 119.8(9) ? C11A C12A H12A . . 120.5 ? C13A C12A C11A . . 119.1(11) ? C13A C12A H12A . . 120.5 ? C13 C14 H14 . . 120.3 ? C13 C14 C15 . . 119.5(11) ? C15 C14 H14 . . 120.3 ? C16 C15 C14 . . 119.7(11) ? C16 C15 H15 . . 120.1 ? C14 C15 H15 . . 120.1 ? C14A C15A H15A . . 120.1 ? C16A C15A C14A . . 119.8(11) ? C16A C15A H15A . . 120.1 ? C11A C16A H16A . . 119.9 ? C15A C16A C11A . . 120.2(10) ? C15A C16A H16A . . 119.9 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Br1A C25A . 1.909(11) ? Br1 C25 . 1.911(12) ? S1 C1 . 1.678(12) ? S1A C1A . 1.678(11) ? O1A C10A . 1.219(14) ? O1 C10 . 1.238(14) ? N2 H2 . 0.8800 ? N2 C1 . 1.334(15) ? N2 C21 . 1.406(17) ? N2A H2A . 0.8800 ? N2A C21A . 1.408(17) ? N2A C1A . 1.311(15) ? N1A H1A . 0.8800 ? N1A C10A . 1.379(14) ? N1A C1A . 1.405(15) ? N1 H1 . 0.8800 ? N1 C10 . 1.374(15) ? N1 C1 . 1.398(15) ? C12 H12 . 0.9500 ? C12 C11 . 1.396(16) ? C12 C13 . 1.36(2) ? C10 C11 . 1.483(17) ? C22A H22A . 0.9500 ? C22A C23A . 1.37(2) ? C22A C21A . 1.412(17) ? C24 H24 . 0.9500 ? C24 C25 . 1.380(17) ? C24 C23 . 1.388(17) ? C11A C10A . 1.490(16) ? C11A C12A . 1.392(17) ? C11A C16A . 1.398(16) ? C23A H23A . 0.9500 ? C23A C24A . 1.396(18) ? C26 H26 . 0.9500 ? C26 C21 . 1.416(16) ? C26 C25 . 1.362(18) ? C21 C22 . 1.383(19) ? C26A H26A . 0.9500 ? C26A C21A . 1.395(16) ? C26A C25A . 1.375(17) ? C13A H13A . 0.9500 ? C13A C14A . 1.376(17) ? C13A C12A . 1.384(18) ? C11 C16 . 1.393(16) ? C23 H23 . 0.9500 ? C23 C22 . 1.40(2) ? C13 H13 . 0.9500 ? C13 C14 . 1.373(18) ? C16 H16 . 0.9500 ? C16 C15 . 1.374(17) ? C24A H24A . 0.9500 ? C24A C25A . 1.378(17) ? C14A H14A . 0.9500 ? C14A C15A . 1.399(18) ? C22 H22 . 0.9500 ? C12A H12A . 0.9500 ? C14 H14 . 0.9500 ? C14 C15 . 1.396(17) ? C15 H15 . 0.9500 ? C15A H15A . 0.9500 ? C15A C16A . 1.375(18) ? C16A H16A . 0.9500 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N2 H2 O1 . 0.88 1.85 2.590(13) 140.6 yes N2A H2A O1A . 0.88 1.84 2.595(14) 142.4 yes N1A H1A S1 1_665 0.88 3.07 3.825(9) 145.2 yes N1 H1 S1A 1_445 0.88 3.09 3.888(10) 151.4 yes _cod_database_fobs_code 2022290