#------------------------------------------------------------------------------ #$Date: 2021-01-19 07:17:06 +0200 (Tue, 19 Jan 2021) $ #$Revision: 261053 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/23/2022316.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022316 _cell_angle_alpha 75.820 _cell_angle_beta 78.056 _cell_angle_gamma 73.644 _cell_length_a 12.9256 _cell_length_b 14.2779 _cell_length_c 17.0222 _exptl_crystal_F_000 1416.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file jx30602sup3.hkl _cod_data_source_block 2 _shelx_title ' (2) in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 553.07 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 274.22 333.87 8.68 o 2 0 0 578.57 439.52 14.05 o 3 0 0 27881.07 29850.42 352.02 o 4 0 0 184711.83 199118.06 1829.06 o 5 0 0 1.69 7.99 6.57 o 6 0 0 9616.70 9807.02 120.94 o 7 0 0 2581.96 2395.47 49.28 o 8 0 0 2366.89 2837.08 58.07 o 9 0 0 1277.15 1242.85 39.40 o 10 0 0 27.88 28.16 19.43 o 11 0 0 842.45 833.25 48.52 o 12 0 0 341.04 373.71 38.20 o 13 0 0 471.43 383.50 39.48 o 14 0 0 288.86 273.53 86.24 o 15 0 0 34.68 3.19 35.13 o -15 1 0 719.24 741.02 89.43 o -14 1 0 322.73 373.71 42.73 o -13 1 0 279.52 247.13 35.93 o -12 1 0 187.22 165.81 54.30 o -11 1 0 726.79 796.70 48.52 o -10 1 0 4634.12 4654.25 111.78 o -9 1 0 191.08 209.95 20.12 o -8 1 0 109.90 117.44 15.04 o -7 1 0 110.07 135.89 14.52 o -6 1 0 1087.75 971.70 29.13 o -5 1 0 565.10 570.14 20.12 o -4 1 0 4104.96 3919.22 56.21 o -3 1 0 99.50 105.97 8.46 o -2 1 0 531.39 436.88 15.98 o -1 1 0 92.18 61.02 3.69 o 1 1 0 6.28 -2.51 2.51 o 2 1 0 0.75 2.13 2.51 o 3 1 0 76.89 52.47 9.36 o 4 1 0 70.44 47.09 8.84 o 5 1 0 2966.78 2555.76 51.07 o 6 1 0 2520.14 2475.14 48.24 o 7 1 0 408.29 379.17 20.67 o 8 1 0 84.50 113.12 15.04 o 9 1 0 1270.95 1169.67 38.06 o 10 1 0 815.29 822.09 62.02 o 11 1 0 41.57 19.16 25.55 o 12 1 0 27.98 54.30 22.36 o 13 1 0 151.33 181.16 31.62 o 14 1 0 54.55 48.47 25.90 o 15 1 0 34.79 63.24 28.16 o -15 2 0 247.69 236.36 54.30 o -14 2 0 90.83 90.63 26.82 o -13 2 0 325.46 322.90 46.31 o -12 2 0 2.81 6.81 17.57 o -11 2 0 662.60 609.38 68.67 o -10 2 0 369.87 359.44 34.95 o -9 2 0 1225.39 1262.52 40.81 o -8 2 0 2772.54 2853.96 59.62 o -7 2 0 1193.27 1218.92 57.50 o -6 2 0 489.67 571.52 49.64 o -5 2 0 7024.41 6526.69 86.95 o -4 2 0 7901.92 8435.45 101.18 o -3 2 0 10477.81 12669.13 159.20 o -2 2 0 1053.69 1130.14 21.98 o -1 2 0 151.14 186.12 13.00 o 0 2 0 28958.55 33505.46 344.12 o 1 2 0 12352.28 14676.42 146.24 o 2 2 0 22684.64 24628.60 236.98 o 3 2 0 683.17 809.78 22.23 o 4 2 0 6.11 6.71 6.57 o 5 2 0 33821.86 33216.09 328.77 o 6 2 0 25245.20 27351.04 552.65 o 7 2 0 8.13 85.09 16.83 o 8 2 0 5145.80 5603.83 88.24 o 9 2 0 3030.44 3315.97 70.14 o 10 2 0 4670.83 5017.32 105.27 o 11 2 0 1536.28 1790.95 67.64 o 12 2 0 1129.79 1151.70 56.33 o 13 2 0 33.28 -6.95 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73.17 o -5 6 0 464.12 375.54 22.41 o -4 6 0 6236.67 6661.53 94.31 o -3 6 0 2054.31 1929.47 42.09 o -2 6 0 11849.24 12508.60 143.15 o -1 6 0 2662.55 3211.01 50.24 o 0 6 0 26167.57 28635.86 324.23 o 1 6 0 27766.65 28678.52 363.54 o 2 6 0 10846.02 11725.93 217.20 o 3 6 0 297.71 404.64 14.89 o 4 6 0 37483.68 37582.80 415.99 o 5 6 0 6210.00 6155.36 88.18 o 6 6 0 13380.51 13194.72 155.58 o 7 6 0 881.13 893.88 30.47 o 8 6 0 977.99 923.75 31.93 o 9 6 0 17.10 14.90 10.76 o 10 6 0 358.32 362.04 49.20 o 11 6 0 914.33 990.50 39.93 o 12 6 0 217.25 179.81 21.98 o 13 6 0 1223.94 1249.06 65.48 o 14 6 0 125.51 130.38 28.16 o 15 6 0 37.40 34.84 24.54 o 16 6 0 28.19 67.08 47.91 o -12 7 0 654.94 603.28 97.42 o -11 7 0 0.87 4.79 18.07 o -10 7 0 770.34 797.01 52.75 o -9 7 0 827.31 747.03 48.21 o -8 7 0 275.01 213.66 28.16 o -7 7 0 2.73 -8.62 11.59 o -6 7 0 641.02 617.76 29.58 o -5 7 0 806.97 775.19 31.05 o -4 7 0 43.98 33.06 11.59 o -3 7 0 362.87 361.21 20.26 o -2 7 0 430.31 412.59 19.72 o -1 7 0 6.50 -6.71 6.71 o 0 7 0 43.21 28.87 7.50 o 1 7 0 726.13 601.26 30.43 o 2 7 0 497.94 499.13 28.16 o 3 7 0 1154.79 1017.00 23.01 o 4 7 0 88.27 94.85 9.81 o 5 7 0 23.15 7.19 8.17 o 6 7 0 1000.28 988.85 36.81 o 7 7 0 716.25 718.51 39.18 o 8 7 0 0.02 8.45 9.73 o 9 7 0 10.06 -0.60 10.33 o 10 7 0 23.06 -11.59 11.59 o 11 7 0 477.23 458.06 29.51 o 12 7 0 0.14 -8.52 12.91 o 13 7 0 3.34 7.59 17.65 o 14 7 0 259.18 273.51 60.69 o 15 7 0 216.40 185.56 34.52 o -12 8 0 70.89 94.22 29.36 o -11 8 0 270.81 418.89 55.90 o -10 8 0 2.84 6.60 20.76 o -9 8 0 587.38 506.81 70.27 o -8 8 0 144.75 201.63 29.10 o -7 8 0 81.44 88.59 17.76 o -6 8 0 604.90 597.29 45.17 o -5 8 0 1954.13 1945.45 50.74 o -4 8 0 5664.76 5467.12 87.90 o -3 8 0 193.09 197.28 25.77 o -2 8 0 12211.40 12488.63 150.24 o -1 8 0 14975.80 15445.99 172.90 o 0 8 0 10191.83 9645.76 141.46 o 1 8 0 365.48 533.71 29.36 o 2 8 0 35.11 25.55 12.78 o 3 8 0 3412.32 3747.25 84.67 o 4 8 0 15210.12 15210.30 169.67 o 5 8 0 17692.32 17977.62 198.14 o 6 8 0 2115.57 2007.59 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