#------------------------------------------------------------------------------ #$Date: 2021-02-26 07:57:57 +0200 (Fri, 26 Feb 2021) $ #$Revision: 262254 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/23/2022332.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022332 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.4923 _cell_length_b 12.0133 _cell_length_c 31.7580 _exptl_crystal_F_000 1288.00 _reflns_d_resolution_high 0.7102 _cod_data_source_file zo30088asup4.hkl _cod_data_source_block 8a _shelx_title ' mo_miwiPH105F1_P212121 in P212121 No19' _shelx_refln_list_code 4 _shelx_f_calc_maximum 203.70 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1545.96 1612.41 32.72 o 4 0 0 4422.85 4204.48 70.64 o 6 0 0 12.42 5.90 18.34 o 8 0 0 2.31 14.82 36.44 o 10 0 0 9.43 51.76 73.60 o 1 1 0 4893.64 4985.36 63.31 o 2 1 0 21388.48 20694.90 261.07 o 3 1 0 5537.74 5709.75 57.83 o 4 1 0 1251.22 1274.56 23.07 o 5 1 0 2324.29 2172.96 34.59 o 6 1 0 833.37 780.22 25.67 o 7 1 0 512.55 568.51 33.14 o 8 1 0 785.01 764.36 50.63 o 9 1 0 430.44 446.25 53.30 o 10 1 0 79.44 0.66 107.38 o 0 2 0 15952.61 16110.24 168.18 o 1 2 0 8551.51 8643.57 88.18 o 2 2 0 6802.93 6707.63 183.50 o 3 2 0 3871.04 3774.32 49.34 o 4 2 0 12897.17 13206.84 126.14 o 5 2 0 3905.79 3603.81 51.07 o 6 2 0 2.03 2.30 13.99 o 7 2 0 2.33 37.02 26.51 o 8 2 0 1634.83 1603.22 60.00 o 9 2 0 369.52 385.88 46.03 o 10 2 0 16.63 92.35 67.65 o 1 3 0 13263.92 13586.30 162.51 o 2 3 0 937.37 917.18 15.67 o 3 3 0 1693.44 1845.98 29.69 o 4 3 0 1646.93 1587.11 27.09 o 5 3 0 248.21 194.66 14.27 o 6 3 0 166.60 189.41 19.27 o 7 3 0 3705.11 3655.79 80.11 o 8 3 0 349.70 353.04 46.24 o 9 3 0 1076.11 1219.36 69.35 o 10 3 0 10.45 -24.13 84.28 o 0 4 0 13289.20 14016.43 173.35 o 1 4 0 6629.20 6941.46 65.52 o 2 4 0 427.94 386.22 11.34 o 3 4 0 3.15 -2.41 6.91 o 4 4 0 112.95 100.07 10.55 o 5 4 0 134.76 122.33 12.81 o 6 4 0 43.07 64.56 16.77 o 7 4 0 3733.48 3654.55 124.32 o 8 4 0 143.36 177.66 34.51 o 9 4 0 684.94 827.53 56.49 o 10 4 0 87.28 -73.99 92.70 o 1 5 0 1148.76 1164.77 16.03 o 2 5 0 7613.03 7419.19 216.86 o 3 5 0 7163.34 7323.76 104.75 o 4 5 0 3039.38 2998.43 64.90 o 5 5 0 1125.17 1073.60 28.61 o 6 5 0 22.19 -6.52 16.24 o 7 5 0 1308.93 1250.14 93.48 o 8 5 0 1851.01 1774.90 72.69 o 9 5 0 584.76 594.63 55.49 o 10 5 0 2.86 47.07 73.32 o 0 6 0 2835.49 2636.37 78.59 o 1 6 0 698.62 667.48 15.05 o 2 6 0 77.26 100.08 7.62 o 3 6 0 394.61 481.54 15.56 o 4 6 0 3567.28 3562.83 80.08 o 5 6 0 5022.34 4913.86 78.95 o 6 6 0 757.05 806.00 36.47 o 7 6 0 20.54 42.84 27.84 o 8 6 0 145.95 113.22 37.11 o 9 6 0 129.15 177.75 52.28 o 1 7 0 462.99 438.30 11.50 o 2 7 0 14441.29 14862.08 195.95 o 3 7 0 727.31 726.28 19.40 o 4 7 0 1902.57 1849.83 44.56 o 5 7 0 1240.24 1347.11 32.05 o 6 7 0 367.41 398.52 26.97 o 7 7 0 936.48 893.61 73.64 o 8 7 0 103.27 105.45 54.87 o 9 7 0 185.39 221.45 66.46 o 0 8 0 17150.66 16677.48 212.54 o 1 8 0 1644.09 1613.79 23.07 o 2 8 0 2898.20 2909.95 42.64 o 3 8 0 140.36 160.56 12.45 o 4 8 0 3483.13 3471.83 96.89 o 5 8 0 1.77 20.23 16.58 o 6 8 0 65.87 12.23 21.07 o 7 8 0 127.65 141.57 31.81 o 8 8 0 87.03 112.34 41.44 o 9 8 0 183.29 113.71 60.56 o 1 9 0 4107.46 4267.54 48.50 o 2 9 0 11685.60 11763.97 109.50 o 3 9 0 0.97 26.69 11.13 o 4 9 0 72.25 76.71 14.79 o 5 9 0 353.63 359.77 26.40 o 6 9 0 41.72 52.11 25.23 o 7 9 0 176.48 168.54 38.11 o 8 9 0 43.52 164.03 51.67 o 0 10 0 667.42 622.02 26.48 o 1 10 0 128.68 116.74 11.37 o 2 10 0 62.04 45.71 10.99 o 3 10 0 1144.39 1091.71 28.16 o 4 10 0 3133.50 3071.39 79.94 o 5 10 0 738.69 752.91 37.53 o 6 10 0 107.26 119.20 29.16 o 7 10 0 171.68 187.93 40.72 o 8 10 0 38.91 -13.33 54.91 o 1 11 0 79.54 71.28 13.39 o 2 11 0 1329.32 1303.97 29.55 o 3 11 0 2.95 -6.28 15.79 o 4 11 0 16.96 18.09 22.48 o 5 11 0 1654.54 1574.71 53.26 o 6 11 0 1826.08 1711.03 64.64 o 7 11 0 255.20 387.73 49.14 o 8 11 0 23.23 32.20 141.59 o 0 12 0 142.01 185.03 28.63 o 1 12 0 178.43 183.00 18.25 o 2 12 0 1048.48 1068.31 35.06 o 3 12 0 217.33 220.27 21.76 o 4 12 0 8.66 17.71 22.54 o 5 12 0 337.19 301.78 48.98 o 6 12 0 291.56 189.27 55.11 o 7 12 0 517.40 514.09 74.83 o 1 13 0 156.22 185.25 29.34 o 2 13 0 312.00 360.48 26.56 o 3 13 0 359.13 360.72 28.18 o 4 13 0 323.30 393.78 42.52 o 5 13 0 114.85 172.66 38.24 o 6 13 0 771.29 813.48 71.62 o 0 14 0 2790.06 2711.54 86.99 o 1 14 0 1076.47 1022.65 43.70 o 2 14 0 195.83 212.37 32.15 o 3 14 0 35.69 33.55 30.71 o 4 14 0 90.29 142.32 36.14 o 5 14 0 7.65 28.44 43.12 o 1 15 0 34.72 9.17 33.33 o 2 15 0 1294.93 1448.32 77.05 o 3 15 0 734.37 746.77 101.88 o 4 15 0 10.24 24.78 58.21 o 0 16 0 970.41 1107.55 93.66 o 1 16 0 38.50 84.85 50.68 o 2 16 0 407.71 313.94 55.28 o 3 16 0 56.57 137.85 117.43 o 1 0 1 2489.32 2483.34 26.90 o 2 0 1 3388.14 3516.71 36.03 o 3 0 1 832.38 823.54 27.52 o 4 0 1 2165.78 2264.81 32.16 o 5 0 1 106.22 151.53 12.03 o 6 0 1 236.64 283.21 17.19 o 7 0 1 3173.76 3073.27 72.86 o 8 0 1 3535.82 3472.46 83.61 o 9 0 1 92.36 56.95 51.47 o 10 0 1 152.19 234.91 68.58 o -10 1 1 706.65 781.80 76.89 o -9 1 1 143.45 162.87 40.75 o -8 1 1 1319.22 1338.23 57.70 o -7 1 1 1478.77 1452.90 74.33 o -6 1 1 1054.65 1066.28 28.34 o -5 1 1 425.38 415.56 16.98 o -4 1 1 226.61 186.67 10.74 o -3 1 1 3318.58 3566.29 39.38 o -2 1 1 3708.77 3640.59 46.84 o -1 1 1 3911.20 3747.15 42.87 o 1 1 1 3715.27 3550.22 44.02 o 2 1 1 3703.90 3633.37 41.17 o 3 1 1 2944.68 3162.94 37.56 o 4 1 1 224.23 216.90 11.30 o 5 1 1 375.39 345.91 15.82 o 6 1 1 1028.78 1022.99 28.04 o 7 1 1 1325.18 1232.61 40.66 o 8 1 1 1444.21 1449.11 63.94 o 9 1 1 151.63 105.28 46.04 o 10 1 1 633.52 667.86 72.86 o -10 2 1 119.70 -1.50 63.95 o -9 2 1 333.35 325.81 43.31 o -8 2 1 428.68 421.65 38.53 o -7 2 1 261.64 280.23 26.66 o -6 2 1 66.71 70.27 14.78 o -5 2 1 2159.55 2054.49 36.25 o -4 2 1 3814.17 3549.45 44.92 o -3 2 1 5815.60 6156.82 79.78 o -2 2 1 109.07 116.82 7.55 o -1 2 1 9233.38 9247.57 94.07 o 0 2 1 6457.91 6638.98 55.74 o 1 2 1 10057.56 9875.63 95.29 o 2 2 1 106.46 93.27 6.11 o 3 2 1 5355.64 5576.74 60.06 o 4 2 1 3818.93 3669.03 57.74 o 5 2 1 2163.69 2066.47 35.92 o 6 2 1 98.78 163.07 15.55 o 7 2 1 267.64 256.44 27.12 o 8 2 1 364.53 386.35 35.48 o 9 2 1 285.70 392.84 53.97 o 10 2 1 147.34 148.61 63.82 o -10 3 1 159.37 36.40 56.57 o -9 3 1 127.11 158.36 43.04 o -8 3 1 529.74 591.22 44.14 o -7 3 1 382.63 386.31 31.59 o -6 3 1 927.91 937.39 30.34 o -5 3 1 293.92 246.54 14.69 o -4 3 1 1427.70 1307.56 24.50 o -3 3 1 4830.67 4601.12 58.87 o -2 3 1 5436.91 5417.10 76.27 o -1 3 1 20606.78 19802.28 299.46 o 0 3 1 1267.28 1357.79 15.28 o 1 3 1 20268.96 20310.03 238.61 o 2 3 1 5053.37 4877.30 119.41 o 3 3 1 5189.64 5018.63 64.84 o 4 3 1 1468.65 1336.41 25.85 o 5 3 1 367.34 336.86 16.95 o 6 3 1 967.70 972.30 30.79 o 7 3 1 435.91 429.09 31.46 o 8 3 1 495.76 561.33 43.14 o 9 3 1 129.15 150.63 41.12 o 10 3 1 126.68 222.84 145.51 o -10 4 1 12.19 -52.10 67.80 o -9 4 1 409.01 423.55 53.15 o -8 4 1 1110.31 1147.59 109.39 o -7 4 1 7.08 8.57 23.24 o -6 4 1 1049.32 1034.41 40.35 o -5 4 1 4327.66 4055.87 74.83 o -4 4 1 3465.62 3587.09 50.77 o -3 4 1 3991.32 4204.15 54.74 o -2 4 1 1210.05 1203.62 18.34 o -1 4 1 11559.65 11691.32 103.62 o 0 4 1 12180.57 12792.01 126.80 o 1 4 1 12830.77 12942.65 137.21 o 2 4 1 1266.91 1279.82 19.79 o 3 4 1 4217.05 4371.91 57.47 o 4 4 1 3456.77 3523.87 47.85 o 5 4 1 4370.41 4095.86 64.28 o 6 4 1 1053.71 1034.56 38.95 o 7 4 1 15.53 18.32 23.17 o 8 4 1 1082.31 1002.38 55.77 o 9 4 1 392.87 388.35 48.27 o 10 4 1 12.90 82.11 98.86 o -10 5 1 57.05 76.10 76.07 o -9 5 1 20.12 -42.89 44.31 o -8 5 1 242.07 300.93 39.34 o -7 5 1 294.51 312.82 33.26 o -6 5 1 237.66 270.54 20.24 o -5 5 1 2202.47 2113.15 35.37 o -4 5 1 632.26 626.09 21.00 o -3 5 1 17155.69 17471.29 225.53 o -2 5 1 15594.79 16216.80 254.78 o -1 5 1 1638.94 1552.87 19.92 o 0 5 1 360.81 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39.36 o -4 7 1 298.52 316.44 16.08 o -3 7 1 53.54 56.59 9.49 o -2 7 1 1170.03 1139.67 21.03 o -1 7 1 2343.75 2353.34 27.67 o 0 7 1 644.60 741.13 15.02 o 1 7 1 2317.89 2320.55 26.73 o 2 7 1 1094.73 1052.71 28.69 o 3 7 1 52.65 47.98 9.53 o 4 7 1 273.69 282.48 15.34 o 5 7 1 2005.36 1983.31 37.64 o 6 7 1 3937.64 3880.24 113.60 o 7 7 1 955.26 924.64 90.80 o 8 7 1 92.01 59.62 45.28 o 9 7 1 245.29 320.48 67.72 o -9 8 1 427.02 479.60 69.33 o -8 8 1 1396.50 1457.46 71.61 o -7 8 1 1465.05 1334.55 71.37 o -6 8 1 535.07 542.54 29.81 o -5 8 1 144.34 137.35 18.84 o -4 8 1 505.67 515.01 26.34 o -3 8 1 217.74 255.98 13.90 o -2 8 1 1785.15 1815.24 37.24 o -1 8 1 687.19 697.67 15.47 o 0 8 1 21.79 56.01 7.64 o 1 8 1 691.71 728.73 18.84 o 2 8 1 1764.20 1725.02 26.74 o 3 8 1 231.37 260.34 13.81 o 4 8 1 586.68 572.66 21.24 o 5 8 1 186.84 195.92 19.70 o 6 8 1 605.72 522.48 52.86 o 7 8 1 1494.25 1445.98 60.13 o 8 8 1 1504.49 1553.94 71.12 o 9 8 1 389.08 545.55 78.72 o -8 9 1 133.36 153.22 46.32 o -7 9 1 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11 1 251.35 253.67 46.39 o -6 11 1 555.01 567.85 39.74 o -5 11 1 359.49 366.68 36.26 o -4 11 1 141.60 116.38 21.61 o -3 11 1 2243.20 2178.93 46.74 o -2 11 1 691.18 663.63 22.65 o -1 11 1 2554.42 2519.80 39.56 o 0 11 1 256.18 256.29 15.45 o 1 11 1 2741.64 2676.85 45.38 o 2 11 1 688.93 677.79 23.21 o 3 11 1 2076.50 1994.11 48.80 o 4 11 1 208.71 204.91 23.32 o 5 11 1 381.71 348.18 29.69 o 6 11 1 481.81 546.59 43.59 o 7 11 1 322.43 386.60 55.22 o 8 11 1 135.59 148.19 149.43 o -7 12 1 50.59 -25.48 55.84 o -6 12 1 396.75 356.58 45.82 o -5 12 1 309.97 327.89 42.73 o -4 12 1 585.90 574.81 37.11 o -3 12 1 623.49 626.97 30.12 o -2 12 1 3324.83 3210.81 72.43 o -1 12 1 4330.06 4365.40 73.26 o 0 12 1 2342.93 2350.16 49.32 o 1 12 1 4091.15 4098.38 87.82 o 2 12 1 3581.22 3480.23 84.03 o 3 12 1 590.00 561.15 27.75 o 4 12 1 565.39 579.90 29.36 o 5 12 1 345.75 340.58 37.54 o 6 12 1 433.27 443.56 46.05 o 7 12 1 39.32 23.75 57.26 o -6 13 1 295.28 336.15 55.86 o -5 13 1 147.58 190.37 59.33 o -4 13 1 177.36 179.70 32.04 o -3 13 1 1062.83 1071.62 41.26 o -2 13 1 1716.70 1801.65 48.80 o -1 13 1 2256.17 2114.78 63.77 o 0 13 1 1007.65 1093.00 38.60 o 1 13 1 2098.56 2028.94 49.23 o 2 13 1 1787.33 1739.52 48.77 o 3 13 1 1050.83 1040.05 46.12 o 4 13 1 198.96 192.71 32.36 o 5 13 1 134.03 125.04 36.39 o 6 13 1 388.20 434.84 58.00 o -5 14 1 140.96 106.89 44.54 o -4 14 1 694.02 756.93 45.74 o -3 14 1 929.62 910.67 46.96 o -2 14 1 449.06 513.64 32.84 o -1 14 1 465.20 485.69 30.82 o 0 14 1 193.25 227.89 27.29 o 1 14 1 481.97 495.63 34.89 o 2 14 1 417.10 421.26 32.14 o 3 14 1 885.84 873.38 55.88 o 4 14 1 765.19 764.73 60.08 o 5 14 1 118.91 84.16 49.20 o -4 15 1 73.89 4.77 58.49 o -3 15 1 190.69 198.28 75.63 o -2 15 1 65.67 37.69 49.45 o -1 15 1 106.58 118.01 36.75 o 0 15 1 223.14 243.51 36.46 o 1 15 1 137.50 190.86 38.75 o 2 15 1 93.55 152.61 36.51 o 3 15 1 175.74 209.00 45.99 o 4 15 1 55.11 147.71 64.14 o -3 16 1 100.26 36.14 65.52 o -2 16 1 149.01 169.85 75.91 o -1 16 1 26.41 -39.23 49.50 o 0 16 1 224.81 333.05 59.58 o 1 16 1 29.66 98.73 53.96 o 2 16 1 129.48 187.19 53.77 o 3 16 1 134.61 187.13 83.16 o 2 0 2 560.79 562.33 11.25 o 3 0 2 117.66 160.03 7.96 o 4 0 2 1815.98 1776.54 27.66 o 5 0 2 6845.88 6732.59 76.23 o 6 0 2 7.21 2.39 12.36 o 7 0 2 1000.98 999.72 45.38 o 8 0 2 1211.54 1145.04 54.08 o 9 0 2 399.52 458.36 54.13 o 10 0 2 9.18 -54.50 54.50 o -10 1 2 64.34 73.31 60.21 o -9 1 2 12.23 28.23 39.32 o -8 1 2 746.05 724.08 47.88 o -7 1 2 9.32 32.28 26.26 o -6 1 2 1962.22 1876.80 38.01 o -5 1 2 426.73 467.00 17.46 o -4 1 2 2057.40 2216.38 30.32 o -3 1 2 8066.73 8034.53 84.36 o -2 1 2 157.17 127.63 6.61 o -1 1 2 30831.05 29256.27 297.87 o 1 1 2 31064.69 29837.84 305.81 o 2 1 2 71.77 62.25 5.54 o 3 1 2 7659.63 7614.52 82.22 o 4 1 2 2024.86 2193.77 31.65 o 5 1 2 356.13 355.21 15.55 o 6 1 2 1814.12 1781.10 35.14 o 7 1 2 34.41 32.92 18.77 o 8 1 2 785.99 813.82 53.15 o 9 1 2 17.90 39.86 44.50 o 10 1 2 73.01 76.01 54.41 o -10 2 2 21.95 97.75 69.16 o -9 2 2 658.08 765.06 65.60 o -8 2 2 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