#------------------------------------------------------------------------------ #$Date: 2021-02-26 07:57:57 +0200 (Fri, 26 Feb 2021) $ #$Revision: 262254 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/23/2022336.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022336 _cell_angle_alpha 90.000 _cell_angle_beta 91.880 _cell_angle_gamma 90.000 _cell_length_a 8.4709 _cell_length_b 14.1401 _cell_length_c 21.0310 _exptl_crystal_F_000 1160.00 _reflns_d_resolution_high 0.7063 _cod_data_source_file zo30086sup2.hkl _cod_data_source_block 6 _shelx_title ' MiWiPH_55_P21 in P21 No4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 376.18 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -18 0 808.11 871.68 72.90 o 1 -18 0 276.89 285.98 49.63 o 2 -18 0 827.17 845.27 50.41 o 3 -18 0 54.38 51.18 20.84 o 1 -17 0 210.48 220.72 28.45 o 2 -17 0 599.34 632.25 47.31 o 3 -17 0 132.34 124.03 23.56 o 4 -17 0 120.01 116.13 24.05 o 5 -17 0 378.58 418.73 40.54 o 0 -16 0 2180.65 2176.11 116.33 o 1 -16 0 1.04 17.18 14.13 o 2 -16 0 20.56 42.83 18.61 o 3 -16 0 163.63 142.68 23.56 o 4 -16 0 524.33 542.22 42.77 o 5 -16 0 13.04 7.15 20.94 o 6 -16 0 282.46 317.23 58.16 o 7 -16 0 48.95 52.97 21.61 o 1 -15 0 878.24 779.46 42.77 o 2 -15 0 1709.64 1619.46 65.80 o 3 -15 0 530.18 579.04 66.69 o 4 -15 0 893.15 992.72 50.45 o 5 -15 0 655.21 624.13 76.78 o 6 -15 0 84.47 120.52 22.30 o 7 -15 0 424.37 475.98 43.31 o 0 -14 0 384.06 286.94 38.78 o 1 -14 0 990.05 1003.67 47.16 o 2 -14 0 653.22 698.79 38.92 o 3 -14 0 1797.11 1758.07 68.54 o 4 -14 0 687.70 643.54 38.34 o 5 -14 0 1134.02 1203.54 55.31 o 6 -14 0 435.69 410.88 42.65 o 7 -14 0 61.62 60.49 31.02 o 1 -13 0 924.14 935.47 26.70 o 2 -13 0 3192.92 3231.79 90.67 o 3 -13 0 1285.78 1272.14 40.62 o 4 -13 0 353.64 319.71 20.64 o 5 -13 0 2130.43 2177.42 73.73 o 6 -13 0 49.35 54.56 14.53 o 0 -12 0 4656.03 4731.36 126.71 o 1 -12 0 500.02 505.34 19.25 o 2 -12 0 1120.30 1200.81 53.95 o 3 -12 0 1234.22 1238.71 32.41 o 4 -12 0 134.28 153.87 13.62 o 5 -12 0 1625.17 1597.14 57.63 o 6 -12 0 79.00 97.33 17.48 o 7 -12 0 191.97 207.84 31.02 o 8 -12 0 447.25 477.72 49.63 o 1 -11 0 1700.06 1672.67 37.80 o 2 -11 0 510.65 503.09 17.39 o 3 -11 0 559.81 572.20 21.44 o 4 -11 0 2613.55 2683.63 73.93 o 5 -11 0 561.21 585.54 17.45 o 6 -11 0 860.53 920.52 31.72 o 7 -11 0 830.25 834.33 29.90 o 8 -11 0 138.86 153.55 29.47 o 9 -11 0 1621.13 2016.35 105.47 o 0 -10 0 1976.76 2095.95 62.49 o 1 -10 0 2226.42 2139.09 87.76 o 2 -10 0 3153.45 3159.67 71.11 o 3 -10 0 1755.23 1681.70 43.55 o 4 -10 0 604.91 617.64 19.24 o 5 -10 0 391.38 408.56 16.26 o 6 -10 0 337.22 351.24 20.60 o 7 -10 0 246.95 244.03 15.83 o 8 -10 0 138.45 156.72 23.75 o 9 -10 0 207.63 207.84 34.12 o 10 -10 0 568.74 513.39 55.84 o 1 -9 0 1482.71 1459.70 40.74 o 2 -9 0 487.94 518.56 18.53 o 3 -9 0 543.27 569.31 14.05 o 4 -9 0 1230.14 1268.23 26.92 o 5 -9 0 495.07 489.76 18.12 o 6 -9 0 553.68 595.51 19.36 o 7 -9 0 1577.67 1626.57 41.60 o 8 -9 0 806.79 844.70 28.91 o 9 -9 0 1608.57 1624.44 70.43 o 10 -9 0 70.12 105.47 29.47 o 0 -8 0 13468.47 14070.53 276.04 o 1 -8 0 1919.28 2002.13 64.16 o 2 -8 0 179.70 208.13 6.45 o 3 -8 0 6691.44 6570.19 103.97 o 4 -8 0 2046.09 2044.32 38.76 o 5 -8 0 162.67 165.05 11.69 o 6 -8 0 605.46 576.35 20.97 o 7 -8 0 1382.57 1408.80 38.15 o 8 -8 0 1206.28 1202.63 41.42 o 9 -8 0 157.49 194.35 22.70 o 10 -8 0 326.87 412.58 51.18 o 1 -7 0 6804.31 7267.67 112.60 o 2 -7 0 5073.44 4785.80 64.26 o 3 -7 0 7900.00 7714.54 120.94 o 4 -7 0 622.87 620.18 16.69 o 5 -7 0 2330.81 2257.00 60.67 o 6 -7 0 902.84 939.92 27.67 o 7 -7 0 1147.76 1196.55 34.19 o 8 -7 0 370.33 391.94 21.79 o 9 -7 0 646.44 693.08 34.90 o 10 -7 0 226.13 214.04 37.22 o 11 -7 0 94.66 93.06 29.47 o 0 -6 0 1304.60 1713.76 74.61 o 1 -6 0 4716.60 4981.74 65.32 o 2 -6 0 8008.27 8050.54 104.83 o 3 -6 0 896.02 1030.55 19.74 o 4 -6 0 1139.27 1152.07 44.95 o 5 -6 0 295.52 296.35 16.57 o 6 -6 0 3171.93 3125.19 65.86 o 7 -6 0 2350.96 2380.75 65.15 o 8 -6 0 664.96 627.72 25.31 o 9 -6 0 673.42 673.04 37.63 o 10 -6 0 72.30 85.87 19.65 o 11 -6 0 316.39 285.39 44.98 o 1 -5 0 95.23 107.79 4.39 o 2 -5 0 5522.08 5560.75 75.70 o 3 -5 0 5497.19 5678.63 71.27 o 4 -5 0 612.59 578.79 15.95 o 5 -5 0 4222.93 4074.78 79.57 o 6 -5 0 661.90 640.33 22.35 o 7 -5 0 1284.74 1209.99 52.60 o 8 -5 0 57.54 68.00 11.32 o 9 -5 0 158.76 212.56 33.35 o 10 -5 0 628.74 708.97 47.31 o 11 -5 0 310.45 361.55 39.55 o 0 -4 0 6487.75 6827.16 115.70 o 1 -4 0 3595.10 3750.31 49.51 o 2 -4 0 1800.60 1798.42 25.65 o 3 -4 0 6260.23 6437.79 80.06 o 4 -4 0 2132.17 2228.65 45.26 o 5 -4 0 487.52 455.85 18.40 o 6 -4 0 5775.95 5652.55 121.35 o 7 -4 0 1974.21 1970.27 77.24 o 8 -4 0 955.16 937.52 33.60 o 9 -4 0 396.58 464.62 35.63 o 10 -4 0 327.31 314.78 30.71 o 11 -4 0 1212.63 1340.42 61.90 o 1 -3 0 6677.85 7201.50 85.87 o 2 -3 0 198.34 177.62 4.91 o 3 -3 0 838.48 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1983.69 33.52 o 3 0 0 85.71 130.18 8.12 o 4 0 0 232.52 226.53 16.76 o 5 0 0 2163.13 2055.02 66.69 o 6 0 0 672.92 649.04 45.90 o 7 0 0 280.79 261.32 18.22 o 8 0 0 867.68 899.10 33.58 o 9 0 0 380.16 386.15 32.85 o 10 0 0 9.01 8.44 13.68 o 11 0 0 25.58 10.75 15.65 o 1 1 0 4721.30 4892.98 67.90 o 2 1 0 347.43 361.78 7.84 o 3 1 0 8074.27 8376.02 118.11 o 4 1 0 4750.89 4451.98 86.96 o 5 1 0 3646.75 3397.61 66.35 o 6 1 0 1150.40 1162.89 82.17 o 7 1 0 99.29 90.41 11.98 o 8 1 0 334.98 300.46 20.99 o 9 1 0 1125.16 1217.80 55.18 o 10 1 0 84.15 89.52 19.74 o 11 1 0 31.36 17.60 15.87 o 0 2 0 55677.30 56299.38 1078.47 o 1 2 0 17588.48 18578.32 218.72 o 2 2 0 8013.52 8490.29 109.09 o 3 2 0 1197.06 1226.62 24.16 o 4 2 0 4350.19 4350.82 71.71 o 5 2 0 1876.92 1785.52 36.58 o 6 2 0 452.39 467.77 33.36 o 7 2 0 1700.03 1631.26 84.18 o 8 2 0 12.90 5.32 17.06 o 9 2 0 348.33 373.80 34.22 o 10 2 0 725.28 788.51 45.43 o 11 2 0 127.20 149.19 30.25 o 1 3 0 6564.93 7024.34 84.36 o 2 3 0 268.48 253.96 6.63 o 3 3 0 772.18 811.53 14.86 o 4 3 0 1308.56 1369.59 25.27 o 5 3 0 4789.89 4746.71 102.95 o 6 3 0 2393.55 2216.26 48.96 o 7 3 0 1870.32 1930.02 96.71 o 8 3 0 370.84 361.61 32.01 o 9 3 0 1002.13 996.51 50.13 o 10 3 0 610.45 669.06 45.27 o 11 3 0 191.77 189.83 28.45 o 0 4 0 5716.96 5997.62 123.99 o 1 4 0 3596.97 3767.56 50.30 o 2 4 0 1946.76 1964.81 29.01 o 3 4 0 6223.34 6465.68 89.68 o 4 4 0 2234.73 2258.85 41.32 o 5 4 0 612.42 604.53 30.11 o 6 4 0 5625.32 5604.09 120.22 o 7 4 0 1836.41 1882.11 85.75 o 8 4 0 995.53 1048.34 50.31 o 9 4 0 406.50 385.17 35.33 o 10 4 0 336.09 370.58 36.44 o 11 4 0 1227.22 1448.08 68.38 o 1 5 0 70.37 71.44 4.01 o 2 5 0 6257.96 6276.37 83.49 o 3 5 0 5632.36 5813.94 84.51 o 4 5 0 715.50 678.72 32.69 o 5 5 0 4243.08 4179.70 81.21 o 6 5 0 751.36 745.90 26.86 o 7 5 0 1344.45 1298.34 48.59 o 8 5 0 35.07 22.91 14.13 o 9 5 0 146.71 125.61 22.95 o 10 5 0 600.69 730.28 86.08 o 11 5 0 316.25 394.51 62.04 o 0 6 0 1156.25 1612.68 52.74 o 1 6 0 4522.85 4682.56 68.23 o 2 6 0 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551.76 20.49 o 4 9 0 1406.84 1397.51 40.95 o 5 9 0 464.50 427.50 22.53 o 6 9 0 510.63 483.76 26.75 o 7 9 0 1562.89 1501.57 64.26 o 8 9 0 869.72 896.50 50.57 o 9 9 0 1689.02 1654.38 74.40 o 10 9 0 56.26 33.43 20.49 o 0 10 0 1775.27 1790.63 58.48 o 1 10 0 2156.17 2162.18 68.56 o 2 10 0 2886.33 2835.69 60.26 o 3 10 0 1888.66 1760.57 43.49 o 4 10 0 737.06 764.04 28.81 o 5 10 0 439.19 466.89 37.28 o 6 10 0 307.29 289.27 28.68 o 7 10 0 297.76 292.96 30.65 o 8 10 0 122.12 112.83 23.41 o 9 10 0 192.17 115.58 24.94 o 10 10 0 609.48 634.99 53.44 o 1 11 0 1803.84 1718.99 42.11 o 2 11 0 426.85 408.15 18.65 o 3 11 0 540.41 516.77 39.63 o 4 11 0 2395.95 2351.36 62.60 o 5 11 0 525.66 495.56 55.39 o 6 11 0 838.24 794.39 65.92 o 7 11 0 792.15 751.89 47.59 o 8 11 0 197.45 232.81 30.90 o 9 11 0 1658.84 1847.65 82.21 o 0 12 0 4566.23 4513.75 129.19 o 1 12 0 387.26 394.85 21.27 o 2 12 0 1021.53 1058.81 36.94 o 3 12 0 1299.35 1276.98 56.64 o 4 12 0 144.66 156.89 16.31 o 5 12 0 1736.72 1682.79 112.45 o 6 12 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19.17 o 6 16 0 328.74 277.54 34.43 o 7 16 0 57.56 -10.49 18.55 o 1 17 0 206.42 216.56 32.57 o 2 17 0 553.45 512.13 62.82 o 3 17 0 137.11 136.39 23.56 o 4 17 0 98.62 146.00 34.90 o 5 17 0 436.02 475.60 42.77 o 6 17 0 109.64 83.96 50.41 o 0 18 0 908.68 822.05 66.69 o 1 18 0 205.64 191.69 53.51 o 2 18 0 809.56 826.19 48.26 o 3 18 0 46.51 63.17 20.27 o 4 18 0 85.49 107.10 24.66 o 5 18 0 89.53 49.99 21.20 o 1 19 0 479.54 461.62 51.96 o 2 19 0 0.48 0.75 16.97 o 3 19 0 536.28 504.78 43.87 o -3 -18 1 57.40 80.43 22.72 o -2 -18 1 246.13 314.31 37.22 o -1 -18 1 526.76 550.54 44.81 o 0 -18 1 526.29 499.51 42.77 o 1 -18 1 397.19 338.92 36.19 o 2 -18 1 35.47 20.16 17.55 o 3 -18 1 613.13 573.12 46.06 o -5 -17 1 194.26 274.25 34.00 o -4 -17 1 54.39 58.16 19.74 o -3 -17 1 446.18 514.66 42.73 o -2 -17 1 108.90 144.41 39.55 o -1 -17 1 180.73 190.31 35.67 o 0 -17 1 548.58 528.44 72.12 o 1 -17 1 340.16 251.03 51.18 o 2 -17 1 63.88 39.32 18.55 o 3 -17 1 130.97 96.95 21.93 o 4 -17 1 42.94 42.54 44.20 o 5 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1528.40 48.77 o -3 -14 1 167.47 165.06 26.11 o -2 -14 1 1079.07 1021.89 95.39 o -1 -14 1 1136.50 1166.27 42.38 o 0 -14 1 778.56 791.76 58.67 o 1 -14 1 191.03 199.75 44.20 o 2 -14 1 4036.83 4123.04 125.49 o 3 -14 1 1634.04 1599.62 64.60 o 4 -14 1 16.98 3.88 13.02 o 5 -14 1 365.78 355.88 33.44 o 6 -14 1 50.32 43.43 17.55 o 7 -14 1 619.38 713.83 44.93 o 8 -14 1 530.46 556.82 62.04 o -7 -13 1 789.23 763.11 54.29 o -6 -13 1 143.72 135.10 24.82 o -5 -13 1 1475.52 1491.59 56.64 o -4 -13 1 2313.36 2468.32 98.49 o -3 -13 1 348.04 371.99 21.62 o -2 -13 1 1560.38 1619.56 47.46 o -1 -13 1 490.68 492.67 27.37 o 0 -13 1 864.80 929.23 48.80 o 1 -13 1 350.42 401.58 19.25 o 2 -13 1 12.18 18.20 6.55 o 3 -13 1 129.21 145.17 23.10 o 4 -13 1 689.73 644.26 29.11 o 5 -13 1 406.35 404.15 23.66 o 6 -13 1 510.41 592.50 58.94 o 7 -13 1 71.47 111.67 32.57 o -8 -12 1 696.85 825.15 58.94 o -7 -12 1 703.84 696.42 51.18 o -6 -12 1 1745.32 1728.82 40.41 o -5 -12 1 1374.75 1380.93 31.75 o -4 -12 1 805.05 728.35 34.22 o 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