#------------------------------------------------------------------------------ #$Date: 2021-03-10 07:54:03 +0200 (Wed, 10 Mar 2021) $ #$Revision: 262961 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/23/2022341.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022341 loop_ _publ_author_name 'Shtender, Vitalii' 'Larsen, Simon R.' 'Sahlberg, Martin' _publ_section_title ; Variants of the X-phase in the Mn--Co--Ge system ; _journal_coeditor_code EF3015 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229621002370 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac 'Mn29.79 Co30.97 Ge13.25' _chemical_formula_sum 'Co30.97 Ge13.25 Mn29.79' _chemical_formula_weight 4422.90 _chemical_name_systematic ; Manganese cobalt germanide ; _space_group_crystal_system orthorhombic _space_group_IT_number 58 _space_group_name_Hall '-P 2 2n' _space_group_name_H-M_alt 'P n n m' _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 1 _cell_length_a 12.6427(10) _cell_length_b 15.6725(12) _cell_length_c 4.8374(4) _cell_measurement_reflns_used 22326 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 42.410 _cell_measurement_theta_min 2.070 _cell_volume 958.50(13) _computing_cell_refinement ; SAINT (Bruker, 2015) ; _computing_data_collection ; APEX3 (Bruker, 2015) ; _computing_data_reduction ; SAINT (Bruker, 2015) ; _computing_molecular_graphics ; DIAMOND (Brandenburg and Putz, 2006) ; _computing_publication_material ; FULLPROF (Rodriguez-Carvajal, 2001) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT2014 (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEXII CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0299 _diffrn_reflns_av_unetI/netI 0.0217 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 22326 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 42.410 _diffrn_reflns_theta_min 2.070 _exptl_absorpt_coefficient_mu 32.539 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details ; (SADABS; Bruker, 2015) ; _exptl_crystal_colour metallic _exptl_crystal_density_diffrn 7.662 _exptl_crystal_description 'irregular fragment' _exptl_crystal_F_000 2005 _exptl_crystal_size_max 0.03 _exptl_crystal_size_mid 0.02 _exptl_crystal_size_min 0.01 _refine_diff_density_max 1.241 _refine_diff_density_min -0.919 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.103 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 106 _refine_ls_number_reflns 3686 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.103 _refine_ls_R_factor_all 0.0265 _refine_ls_R_factor_gt 0.0219 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0166P)^2^+1.7225P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0502 _refine_ls_wR_factor_ref 0.0515 _reflns_number_gt 3277 _reflns_number_total 3686 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ef3015sup1.cif _cod_data_source_block Mn14.9Co15.5Ge6.6 _cod_database_code 2022341 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; 0 0 1 0.30 0.10 0 0 2 2803.62 101.39 0 0 -3 0.20 0.10 0 0 -3 0.30 0.10 0 0 3 0.10 0.20 0 0 4 9999.00 354.96 0 0 -4 9775.72 354.56 0 0 -4 9825.72 354.56 0 0 -5 0.40 0.20 0 0 -5 0.40 0.30 0 0 5 0.50 0.30 0 0 -6 434.96 16.20 0 0 6 439.96 16.30 0 0 -6 450.85 16.20 0 0 -7 3.10 0.60 0 0 -7 3.90 0.60 0 0 7 3.10 0.70 0 0 -8 1599.44 57.89 0 0 -8 1640.94 57.99 0 0 8 1567.94 58.09 0 0 -9 -0.10 0.60 0 0 -9 0.10 0.70 0 0 9 0.40 0.80 -1 0 0 0.00 0.10 -1 0 -1 20.50 1.00 1 0 1 22.30 0.90 1 0 2 0.00 0.20 -1 0 2 0.10 0.10 -1 0 3 26.40 1.10 -1 0 -3 24.50 1.00 -1 0 -3 23.60 1.00 1 0 -3 26.90 1.00 1 0 3 24.80 1.20 1 0 -3 25.10 1.00 1 0 -4 -0.40 0.20 -1 0 4 0.40 0.20 -1 0 4 0.30 0.20 1 0 -4 0.20 0.20 -1 0 -5 1.70 0.30 1 0 -5 1.30 0.30 1 0 -5 1.50 0.30 -1 0 -5 2.20 0.40 1 0 5 2.70 0.40 -1 0 -6 0.40 0.40 1 0 6 0.10 0.40 -1 0 -6 0.50 0.40 1 0 7 7.80 0.90 -1 0 7 8.60 0.90 -1 0 -7 7.10 0.80 -1 0 -7 7.80 0.80 1 0 -7 7.00 0.70 1 0 -7 8.10 0.80 -1 0 8 0.80 0.70 -1 0 -8 0.50 0.50 1 0 -8 0.70 0.60 1 0 8 1.10 0.70 1 0 -8 -0.30 0.50 -1 0 -8 0.50 0.60 1 0 -9 -0.20 0.60 -1 0 -9 -0.40 0.70 -1 0 9 0.60 0.90 1 0 -9 0.10 0.70 -1 0 -9 0.30 0.60 1 0 9 0.00 0.80 2 0 0 1.10 0.20 -2 0 0 1.10 0.20 2 0 1 6.00 0.50 -2 0 -1 8.70 0.50 2 0 2 36.80 1.60 2 0 -3 0.20 0.10 -2 0 -3 0.10 0.10 -2 0 -3 0.40 0.20 2 0 3 0.40 0.20 2 0 -3 0.70 0.20 2 0 -4 1.50 0.30 -2 0 -4 1.20 0.20 2 0 -4 1.20 0.30 -2 0 -4 1.10 0.20 2 0 5 0.30 0.30 2 0 -5 0.10 0.30 2 0 -5 0.20 0.30 -2 0 -5 0.20 0.30 -2 0 -5 0.40 0.30 2 0 -6 10.80 0.80 2 0 6 9.30 0.90 -2 0 -6 11.50 0.90 -2 0 -6 10.90 0.90 -2 0 6 11.50 1.00 2 0 -6 11.50 0.80 2 0 7 -0.30 0.50 -2 0 -7 0.30 0.50 -2 0 -7 0.30 0.50 2 0 -7 0.10 0.50 2 0 -7 0.10 0.40 -2 0 7 -0.20 0.50 2 0 -8 0.10 0.60 2 0 -8 0.40 0.50 -2 0 -8 1.60 0.60 -2 0 -8 1.40 0.60 -2 0 8 0.60 0.70 2 0 8 1.70 0.80 2 0 -9 0.60 0.60 2 0 9 0.70 0.80 -2 0 9 1.40 0.90 2 0 -9 0.50 0.70 -2 0 -9 1.60 0.70 -2 0 -9 0.00 0.70 3 0 0 0.10 0.20 -3 0 0 -0.10 0.10 -3 0 -1 11.50 0.70 3 0 1 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0.30 0.90 12 -2 -6 0.80 0.60 12 -2 -6 0.60 0.50 -12 2 7 43.90 2.70 -12 -2 -7 47.70 2.80 12 -2 -7 42.70 2.20 -12 2 -7 41.40 2.70 -13 -2 0 428.06 16.80 13 -2 0 459.45 16.50 -13 -2 0 458.05 16.70 -13 2 0 463.55 16.80 13 2 0 446.26 16.50 -13 -2 -1 0.00 0.50 -13 -2 -1 0.40 0.50 -13 2 1 0.90 0.50 13 -2 1 0.70 0.40 13 2 -1 0.20 0.40 -13 -2 1 0.80 0.50 -13 2 -1 1.30 0.50 13 2 1 0.70 0.40 -13 2 -1 0.40 0.50 13 -2 -1 0.40 0.40 13 2 -2 468.15 17.60 -13 2 2 482.15 17.70 -13 -2 -2 447.96 17.70 -13 -2 -2 501.85 17.70 -13 2 -2 481.45 17.80 13 -2 -2 491.45 17.50 13 -2 -2 484.95 17.50 -13 -2 2 473.05 17.60 13 2 2 480.45 17.50 -13 2 3 1.00 0.60 -13 -2 -3 1.20 0.60 13 -2 -3 1.00 0.50 13 -2 -3 1.30 0.50 -13 2 -3 1.50 0.70 -13 -2 -4 265.97 9.70 13 2 -4 234.08 9.50 -13 2 4 251.07 9.60 13 2 -4 249.38 9.40 -13 2 -4 264.27 9.70 -13 -2 4 251.87 9.60 13 -2 -4 246.18 9.40 13 -2 -4 247.28 9.40 13 2 -5 -0.10 0.60 -13 -2 -5 -0.30 0.80 -13 2 5 -0.60 0.70 -13 2 -5 0.50 0.80 13 -2 -5 0.90 0.60 13 -2 -5 -0.50 0.50 -13 2 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38.40 2.80 22 2 -1 37.00 2.20 -22 -2 -1 36.50 2.30 -22 2 -1 36.50 2.40 -22 -2 1 33.90 2.60 22 -2 -1 37.70 2.30 22 2 -2 10.60 1.30 -22 2 2 8.70 1.60 -22 2 2 11.20 1.60 -22 -2 -2 8.20 1.20 22 -2 -2 10.90 1.40 -22 2 -2 10.90 1.40 -22 -2 2 10.70 1.70 -22 2 3 12.70 1.70 -22 -2 -3 16.00 1.50 22 2 -3 15.50 1.50 -22 2 3 15.50 2.00 -22 2 -3 15.50 1.60 -22 -2 3 14.80 1.90 22 -2 -3 13.90 1.60 -23 -2 0 5.50 1.30 23 -2 0 7.20 1.50 -23 2 0 6.60 1.30 23 2 0 8.30 1.10 -23 2 1 1.60 1.20 23 2 -1 1.20 0.90 -23 2 1 0.40 1.10 -23 -2 -1 1.20 0.90 -23 -2 1 1.10 1.20 23 -2 -1 1.60 1.00 -23 2 -1 1.90 1.10 -23 2 2 127.39 5.50 23 2 -2 118.29 5.20 -23 -2 -2 115.29 5.10 -23 2 2 118.89 5.70 -23 -2 2 126.69 5.70 23 -2 -2 118.59 5.20 -23 2 -2 120.49 5.20 0 3 0 0.10 0.10 0 -3 0 0.00 0.10 0 3 1 32.50 1.20 0 3 -1 27.60 1.20 0 -3 1 28.30 1.20 0 3 -2 0.30 0.20 0 -3 2 0.10 0.10 0 -3 -3 11.00 0.60 0 -3 -3 11.60 0.60 0 3 3 11.50 0.60 0 3 -3 12.20 0.80 0 3 -3 11.90 0.60 0 -3 -4 0.00 0.10 0 -3 -4 -0.40 0.20 0 3 4 -0.10 0.30 0 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5 5 104.59 4.60 -13 -5 5 99.39 4.60 -13 5 -5 100.79 4.50 13 -5 -5 101.19 4.20 13 -5 -5 101.89 4.20 -13 -5 -6 -0.70 0.90 -13 5 6 -0.50 0.90 13 -5 -6 0.20 0.60 -13 5 -6 -0.60 0.90 13 -5 -6 -0.20 0.60 -13 5 7 16.10 1.80 -13 -5 -7 16.00 1.70 -13 5 -7 12.30 1.50 13 -5 -7 14.70 1.30 -14 5 0 2.00 0.70 -14 -5 0 2.90 0.60 14 5 0 2.50 0.50 -14 -5 0 2.10 0.70 14 -5 0 2.20 0.50 14 -5 1 61.99 2.60 14 5 -1 61.99 2.80 -14 -5 -1 62.29 2.90 -14 5 1 63.69 3.00 -14 -5 -1 66.29 2.80 -14 5 -1 63.59 3.00 -14 -5 1 57.39 3.00 14 5 1 65.39 2.70 14 -5 -1 65.99 2.70 -14 -5 -2 -0.30 0.50 -14 -5 -2 0.20 0.50 14 5 -2 -0.20 0.50 -14 5 2 -0.50 0.60 14 -5 -2 -0.20 0.40 14 -5 -2 0.30 0.50 -14 -5 2 0.00 0.60 -14 5 -2 -0.80 0.60 -14 -5 -3 90.09 3.70 14 5 -3 81.79 3.60 -14 5 3 88.79 3.80 -14 5 -3 87.49 3.90 14 -5 -3 85.79 3.50 14 -5 -3 85.49 3.60 -14 -5 3 77.19 3.90 -14 -5 -4 0.90 0.70 14 5 -4 1.30 0.70 -14 5 4 1.60 0.80 14 -5 -4 1.20 0.60 -14 -5 4 0.80 0.80 -14 5 -4 1.40 0.90 14 -5 -4 1.80 0.60 14 5 -5 12.30 1.20 -14 5 5 11.90 1.40 -14 -5 -5 17.20 1.50 -14 5 -5 16.50 1.60 14 -5 -5 13.80 1.20 14 -5 -5 14.40 1.20 -14 -5 5 11.60 1.50 -14 5 6 0.10 1.00 -14 -5 -6 0.20 0.90 14 -5 -6 0.00 0.70 -14 5 -6 -0.50 0.90 14 -5 -6 0.80 0.70 -14 -5 -7 49.40 2.90 -14 5 7 50.39 3.00 -14 5 -7 42.30 2.80 14 -5 -7 47.00 2.50 15 -5 0 585.44 20.90 -15 -5 0 587.54 21.10 15 5 0 564.44 21.00 -15 -5 0 563.74 21.30 -15 5 0 566.74 21.30 -15 -5 -1 0.50 0.50 15 5 -1 0.40 0.50 -15 -5 -1 0.70 0.70 -15 5 1 0.50 0.70 -15 -5 1 0.50 0.70 15 -5 -1 0.60 0.50 -15 5 -1 -0.40 0.70 15 5 1 0.90 0.50 -15 -5 -2 0.00 0.60 -15 5 2 0.40 0.80 -15 -5 -2 0.30 0.50 15 5 -2 0.00 0.60 -15 5 -2 0.90 0.80 15 -5 -2 0.30 0.50 -15 -5 2 0.90 0.70 -15 5 3 -0.30 0.70 -15 -5 -3 0.10 0.60 15 5 -3 0.30 0.60 -15 5 -3 1.20 0.80 15 -5 -3 0.00 0.50 -15 -5 3 -0.10 0.70 15 -5 -3 0.40 0.60 15 5 -4 319.17 12.80 -15 5 4 340.57 13.00 -15 -5 -4 363.16 12.80 -15 -5 4 314.77 13.10 15 -5 -4 342.77 12.70 15 -5 -4 345.97 12.70 -15 5 -4 348.57 13.00 15 5 -5 0.00 0.70 -15 -5 -5 0.70 0.80 -15 5 5 0.10 0.90 15 -5 -5 0.10 0.60 15 -5 -5 0.20 0.70 -15 5 -5 0.10 1.00 -15 -5 5 0.30 1.00 -15 -5 -6 0.40 0.90 -15 5 6 2.00 1.10 15 -5 -6 0.70 0.80 -15 5 -6 -0.20 1.00 15 -5 -6 0.10 0.70 16 5 0 15.80 1.10 16 -5 0 13.70 1.10 -16 -5 0 16.00 1.50 -16 5 0 13.50 1.40 -16 -5 0 13.30 1.20 -16 -5 -1 5.10 0.80 16 5 -1 5.90 0.80 -16 5 1 4.00 1.00 -16 -5 -1 4.60 0.90 -16 -5 1 9.50 1.20 16 -5 -1 6.60 0.80 16 5 1 5.00 0.70 -16 5 -1 5.10 1.00 -16 -5 -2 132.29 5.40 -16 -5 -2 138.99 5.30 16 5 -2 132.49 5.30 -16 5 2 134.39 5.60 -16 5 -2 129.59 5.60 16 -5 -2 137.59 5.30 -16 -5 2 119.69 5.60 16 5 -3 3.50 0.90 -16 -5 -3 4.60 0.80 -16 5 3 3.10 1.00 -16 -5 3 1.60 0.90 -16 5 -3 2.50 0.90 16 -5 -3 3.90 0.80 16 -5 -3 2.40 0.70 -16 5 4 8.30 1.30 -16 -5 -4 8.30 1.10 16 5 -4 6.90 1.00 -16 -5 4 9.20 1.40 16 -5 -4 9.30 1.00 16 -5 -4 8.70 1.00 -16 5 -4 10.10 1.30 -16 5 5 2.50 1.10 -16 -5 -5 2.90 1.00 16 5 -5 3.40 0.90 16 -5 -5 2.60 0.80 16 -5 -5 3.00 0.90 -16 5 -5 3.70 1.20 -16 -5 5 3.00 1.20 -16 -5 -6 58.19 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0 36.10 1.90 18 5 -1 1.40 0.70 -18 5 1 1.00 0.90 -18 -5 -1 1.60 0.80 -18 -5 -1 2.00 0.70 -18 5 -1 2.70 1.00 -18 -5 1 1.60 0.90 18 -5 -1 1.50 0.70 -18 -5 -2 1.40 0.70 18 5 -2 2.00 0.80 -18 5 2 1.10 1.00 -18 -5 -2 1.50 0.70 18 -5 -2 0.10 0.70 -18 5 -2 1.20 0.90 -18 -5 2 0.40 0.90 -18 -5 -3 0.50 0.70 18 5 -3 0.70 0.80 -18 5 3 0.60 1.00 -18 -5 3 0.90 1.00 18 -5 -3 0.70 0.80 -18 5 -3 2.10 1.00 -18 -5 -4 20.50 1.80 18 5 -4 19.90 1.70 -18 5 4 22.60 2.00 -18 -5 4 19.50 1.90 18 -5 -4 20.70 1.80 -18 5 -4 22.20 1.90 -18 -5 -5 5.40 1.10 18 5 -5 5.60 1.10 -18 5 5 5.20 1.30 -18 -5 5 6.80 1.40 -18 5 -5 6.40 1.40 18 -5 -5 4.90 1.10 18 -5 -5 5.90 1.10 -19 -5 0 63.89 3.20 -19 5 0 61.59 3.30 19 5 0 58.29 2.80 19 -5 0 62.19 2.90 -19 5 0 55.29 3.10 19 5 -1 27.50 1.80 -19 -5 -1 29.20 2.00 -19 5 1 25.30 2.20 19 -5 -1 27.90 1.80 -19 5 -1 27.80 2.20 -19 -5 1 27.90 2.10 19 5 -2 4.40 1.00 -19 -5 -2 4.70 0.90 -19 5 2 5.90 1.30 -19 -5 -2 4.60 1.00 19 -5 -2 6.30 1.00 -19 5 -2 4.30 1.10 -19 -5 2 7.60 1.30 19 5 -3 17.10 1.50 -19 -5 -3 17.60 1.40 -19 5 3 17.20 1.80 19 -5 -3 16.00 1.50 -19 -5 3 16.20 1.80 -19 5 -3 17.10 1.70 -19 -5 -4 49.90 2.60 19 5 -4 40.20 2.60 -19 5 4 45.90 3.00 -19 -5 4 46.00 3.00 -19 5 -4 47.30 2.70 19 -5 -4 46.70 2.60 -19 -5 -5 25.80 1.90 -19 5 5 27.10 2.40 19 5 -5 21.40 1.90 -19 -5 5 23.60 2.20 19 -5 -5 23.10 2.00 -19 5 -5 28.00 2.30 -20 5 0 2.20 1.00 -20 5 0 1.40 1.00 -20 -5 0 1.90 1.00 20 -5 0 1.10 0.80 20 5 0 2.20 0.80 -20 -5 -1 3.10 0.90 20 5 -1 2.50 0.80 -20 5 1 2.70 1.20 20 -5 -1 3.10 1.00 -20 -5 1 3.00 1.10 -20 5 -1 1.50 1.10 -20 5 2 1.50 1.20 20 5 -2 2.90 0.90 -20 -5 -2 1.90 0.90 -20 5 -2 2.10 1.00 20 -5 -2 1.30 0.90 -20 -5 2 1.90 1.10 -20 -5 -3 0.50 0.80 20 5 -3 0.60 0.90 -20 5 3 0.90 1.20 -20 -5 3 0.50 1.10 20 -5 -3 1.50 0.90 -20 5 -3 0.60 1.00 20 5 -4 1.60 1.00 -20 5 4 0.50 1.20 -20 -5 -4 0.70 0.90 -20 -5 4 1.20 1.10 20 -5 -4 3.00 1.10 -20 5 -4 1.20 1.10 21 5 0 36.50 2.10 -21 -5 0 36.70 2.50 -21 5 0 37.50 2.60 -21 -5 -1 18.20 1.60 -21 5 1 18.60 2.00 21 5 -1 19.30 1.70 -21 5 1 21.30 2.00 -21 -5 1 23.90 2.00 -21 5 -1 21.80 1.90 21 -5 -1 20.50 1.70 21 5 -2 158.98 6.30 -21 5 2 154.88 6.70 -21 5 -2 150.48 6.50 -21 -5 2 159.88 6.70 21 -5 -2 148.39 6.40 -21 5 3 14.90 1.80 21 5 -3 14.90 1.50 -21 -5 -3 13.50 1.30 -21 -5 3 14.00 1.80 -21 5 -3 15.20 1.60 21 -5 -3 15.40 1.60 -21 -5 -4 21.90 1.90 21 5 -4 26.30 2.30 -21 5 4 20.10 2.20 -21 5 -4 22.70 2.30 21 -5 -4 26.60 2.20 -21 -5 4 24.80 2.80 -22 -5 0 32.90 2.40 -22 5 0 35.40 2.70 22 5 -1 4.00 1.00 -22 5 1 3.10 1.30 -22 -5 -1 2.80 1.00 -22 5 1 4.80 1.40 -22 -5 1 4.00 1.20 22 -5 -1 3.20 1.10 -22 5 -1 1.90 1.10 22 5 -2 178.08 6.90 -22 5 2 164.38 7.50 -22 5 2 173.28 7.30 -22 -5 2 172.88 7.30 22 -5 -2 167.68 7.00 -22 5 -2 168.28 7.10 22 5 -3 2.90 1.10 -22 5 3 0.80 1.30 -22 -5 3 1.70 1.40 22 -5 -3 2.30 1.10 -22 5 -3 1.40 1.10 -23 5 0 4.50 1.30 -23 -5 0 1.90 1.10 23 5 -1 58.19 2.90 -23 5 1 52.99 3.40 -23 5 1 53.29 3.30 -23 -5 -1 50.79 2.90 -23 5 -1 48.60 3.10 23 -5 -1 52.09 2.90 -23 -5 1 56.29 3.20 0 6 0 0.20 0.10 0 -6 0 0.20 0.10 0 -6 1 0.10 0.10 0 6 1 0.00 0.10 0 6 -1 0.10 0.10 0 -6 2 176.98 6.40 0 6 2 173.18 6.50 0 6 -2 168.28 6.50 0 -6 3 0.30 0.20 0 -6 -3 0.20 0.10 0 -6 -3 0.50 0.20 0 6 -3 0.80 0.30 0 6 3 0.10 0.20 0 6 3 0.00 0.20 0 6 -3 0.10 0.10 0 6 4 0.90 0.30 0 6 -4 0.80 0.20 0 6 -4 1.30 0.30 0 -6 -4 0.00 0.20 0 -6 -4 0.30 0.20 0 -6 -4 0.40 0.20 0 6 5 0.60 0.40 0 6 -5 0.50 0.30 0 6 -5 0.20 0.20 0 -6 -5 0.60 0.30 0 -6 -5 0.00 0.30 0 -6 -5 -0.30 0.20 0 6 -6 40.70 1.90 0 -6 -6 43.20 1.90 0 6 6 41.50 2.10 0 -6 -6 42.80 2.00 0 -6 -7 0.70 0.50 0 6 7 0.40 0.60 0 6 -7 -0.30 0.40 0 6 8 1.20 0.90 0 -6 -8 1.80 0.70 0 -6 8 2.00 0.80 0 6 -8 2.40 0.70 -1 6 0 5.10 0.40 1 -6 0 5.40 0.40 -1 -6 0 5.90 0.40 1 6 0 5.40 0.40 1 -6 1 6.90 0.50 1 6 -1 6.10 0.40 -1 6 1 6.40 0.50 -1 6 -1 6.20 0.50 1 6 1 6.90 0.50 -1 -6 1 6.70 0.40 1 -6 -1 6.80 0.50 1 6 -2 125.89 4.80 1 6 -2 127.69 4.80 -1 6 2 129.19 4.90 1 -6 2 139.49 4.90 1 6 2 121.19 5.00 -1 6 -2 125.49 4.90 -1 -6 2 131.79 4.80 1 -6 3 6.10 0.50 -1 6 3 6.30 0.50 -1 -6 -3 6.50 0.40 1 6 -3 5.90 0.50 1 6 -3 6.30 0.40 -1 -6 -3 5.90 0.40 -1 6 3 6.00 0.50 -1 -6 3 6.40 0.40 -1 6 -3 8.80 0.70 1 -6 -3 6.00 0.40 1 6 3 5.90 0.50 1 6 3 4.90 0.60 1 -6 -3 8.00 0.50 -1 6 -3 6.70 0.40 -1 6 4 1.10 0.30 -1 -6 -4 2.20 0.30 -1 -6 -4 2.10 0.30 1 6 -4 1.70 0.30 1 6 -4 2.10 0.30 -1 -6 -4 1.70 0.30 1 6 4 2.60 0.40 -1 6 -4 2.20 0.30 -1 6 -4 2.20 0.30 1 -6 -4 1.40 0.30 1 -6 -4 2.10 0.30 1 -6 -4 1.50 0.30 1 6 -5 23.20 1.20 -1 -6 -5 25.10 1.20 -1 6 5 23.50 1.30 -1 -6 -5 23.30 1.20 1 6 -5 23.30 1.10 1 -6 -5 23.90 1.20 1 -6 -5 23.80 1.10 -1 6 -5 24.40 1.10 1 -6 -5 23.80 1.20 -1 6 -5 23.50 1.20 1 6 5 24.90 1.30 -1 6 6 30.40 1.60 -1 -6 -6 28.30 1.50 1 6 -6 28.40 1.40 1 6 6 26.60 1.60 1 -6 -6 29.30 1.50 -1 6 -6 27.10 1.40 1 -6 -6 27.10 1.50 -1 6 -6 26.20 1.30 -1 -6 -7 12.80 1.10 -1 6 7 9.90 1.10 1 6 -7 10.00 0.90 1 6 7 9.00 1.10 1 -6 -7 11.40 1.00 1 -6 8 0.50 0.70 1 6 -8 1.40 0.70 -1 -6 -8 0.70 0.60 -1 6 8 0.80 0.80 -1 6 -8 1.70 0.60 1 -6 -8 1.30 0.60 -1 -6 8 0.10 0.80 1 6 8 0.50 0.80 2 -6 0 50.99 2.10 -2 6 0 49.80 2.10 2 6 0 52.19 2.10 2 6 -1 0.20 0.20 2 -6 1 0.20 0.20 -2 6 1 0.20 0.20 2 -6 -1 0.20 0.20 -2 6 -1 0.30 0.20 2 6 -2 211.78 7.90 -2 6 2 218.18 8.10 2 6 -2 218.08 8.00 2 -6 2 226.18 8.10 2 -6 -2 219.48 7.90 -2 -6 2 222.78 8.00 2 6 2 215.48 8.00 -2 6 -2 215.08 8.20 2 6 -3 20.30 0.80 2 6 -3 16.80 0.90 -2 -6 -3 16.50 0.80 -2 -6 -3 17.30 0.80 -2 6 3 17.80 0.90 2 -6 3 16.30 0.90 -2 6 3 16.40 0.90 2 -6 -3 17.60 0.80 -2 -6 3 18.50 0.80 -2 6 -3 16.40 0.80 2 -6 -3 17.00 0.80 2 6 3 17.10 0.90 -2 6 -3 16.10 0.80 -2 -6 -4 18.70 1.00 -2 -6 -4 17.80 0.80 -2 6 4 17.80 1.00 2 6 -4 17.90 0.80 2 6 -4 19.00 0.90 -2 6 -4 18.10 0.90 2 -6 -4 18.60 0.90 2 -6 -4 19.50 0.90 -2 6 -4 18.50 0.90 2 6 4 19.10 1.00 2 -6 -4 18.70 0.90 2 6 -5 7.80 0.60 -2 6 5 7.80 0.70 -2 -6 -5 6.80 0.70 -2 -6 -5 8.20 0.70 -2 6 -5 6.80 0.60 2 -6 -5 6.50 0.60 2 -6 -5 8.10 0.70 -2 6 -5 6.20 0.60 2 -6 -5 7.60 0.70 2 6 5 7.80 0.70 -2 -6 -6 46.00 2.10 2 6 -6 45.10 2.00 -2 6 6 46.30 2.20 2 6 6 43.90 2.20 2 -6 -6 46.00 2.00 2 -6 -6 44.50 2.00 -2 6 -6 42.30 1.90 -2 6 -6 44.60 2.00 -2 6 7 14.20 1.30 2 6 -7 12.60 1.10 -2 -6 -7 12.20 1.10 -2 6 -7 13.60 1.10 2 6 7 13.70 1.20 2 -6 -7 12.30 1.10 2 -6 8 4.20 0.90 2 6 -8 3.50 0.70 -2 6 8 5.60 1.00 -2 -6 -8 5.30 0.90 2 -6 -8 4.60 0.80 -2 6 -8 4.70 0.80 -2 -6 8 3.30 0.90 2 6 8 4.50 1.00 -3 6 0 194.18 7.20 3 -6 0 189.18 7.10 3 -6 1 139.29 5.30 -3 6 1 141.69 5.30 3 6 -1 140.49 5.20 3 -6 -1 139.69 5.20 -3 6 -1 134.39 5.30 3 6 -2 267.47 10.20 -3 6 2 279.27 10.30 3 -6 2 279.47 10.40 3 6 -2 287.87 10.20 3 -6 -2 281.67 10.30 3 6 2 281.87 10.20 3 -6 -2 277.77 10.20 3 -6 -2 286.07 10.20 -3 6 -2 279.47 10.40 3 6 -3 59.69 2.40 -3 -6 -3 59.89 2.40 3 6 -3 64.39 2.40 -3 6 3 61.59 2.40 -3 -6 -3 61.59 2.40 -3 6 3 65.09 2.50 3 -6 -3 59.99 2.40 -3 6 -3 61.99 2.40 3 -6 -3 62.69 2.40 3 6 3 58.09 2.40 -3 6 -3 60.39 2.30 -3 6 4 68.79 2.80 3 6 -4 73.09 2.80 -3 -6 -4 69.39 2.80 3 6 4 69.39 2.80 3 -6 -4 70.49 2.70 3 -6 -4 70.09 2.70 3 -6 -4 69.29 2.70 -3 6 -4 67.39 2.70 -3 6 -4 69.99 2.70 3 6 -5 37.90 1.60 -3 6 5 36.20 1.70 -3 -6 -5 36.80 1.70 -3 6 -5 35.10 1.60 3 -6 -5 37.60 1.70 3 -6 -5 34.50 1.50 3 6 5 34.80 1.70 -3 6 -5 37.30 1.60 3 -6 -5 34.50 1.60 -3 6 6 60.79 2.80 -3 -6 -6 61.69 2.80 3 6 -6 59.69 2.60 3 -6 -6 67.39 2.70 3 -6 -6 59.19 2.70 3 6 6 64.89 2.80 -3 6 -6 61.49 2.60 -3 6 -6 66.19 2.60 3 6 -7 9.60 0.90 -3 6 7 10.20 1.10 -3 -6 -7 10.10 1.00 -3 6 -7 9.50 0.90 3 6 7 10.00 1.10 -3 6 -7 9.10 0.80 3 -6 -7 8.80 0.90 3 -6 8 20.40 1.60 -3 -6 -8 18.70 1.60 3 6 -8 20.90 1.50 -3 6 8 20.30 1.80 -3 -6 8 17.00 1.50 3 6 8 21.70 1.80 3 -6 -8 21.30 1.50 -3 6 -8 21.90 1.50 4 -6 0 343.97 12.30 -4 6 0 325.47 12.30 4 6 -1 208.48 7.80 -4 6 1 216.68 7.90 4 -6 1 217.58 7.90 -4 6 -1 205.58 7.90 4 -6 -1 207.28 7.80 -4 6 2 60.59 2.40 4 6 -2 56.99 2.30 -4 -6 -2 61.49 2.30 -4 -6 -2 56.49 2.40 4 6 -2 58.59 2.30 4 -6 2 59.19 2.50 4 -6 -2 59.99 2.40 4 -6 -2 59.39 2.20 -4 6 -2 58.09 2.60 4 -6 -2 58.79 2.30 -4 6 3 156.88 6.00 4 6 -3 154.58 5.90 -4 -6 -3 162.68 5.90 -4 -6 -3 157.08 6.00 -4 6 3 164.58 6.00 4 6 -3 162.38 5.90 -4 6 -3 159.38 5.90 -4 6 -3 154.88 6.00 4 -6 -3 165.18 5.90 4 -6 -3 163.98 5.90 4 6 3 163.88 6.00 -4 -6 -4 106.89 4.00 -4 -6 -4 105.69 4.20 4 6 -4 107.79 4.10 -4 6 4 106.29 4.20 -4 6 -4 108.39 4.10 4 -6 -4 109.49 4.10 4 -6 -4 105.69 4.10 4 -6 -4 110.09 4.10 -4 6 -4 106.99 4.10 4 6 4 108.69 4.20 -4 -6 -5 29.60 1.60 4 6 -5 33.00 1.50 -4 6 5 32.60 1.60 4 -6 -5 31.80 1.40 4 -6 -5 33.30 1.50 -4 6 -5 30.80 1.40 4 -6 -5 30.70 1.50 4 6 5 33.00 1.60 -4 6 -5 32.40 1.40 -4 -6 -6 13.70 1.10 4 6 -6 12.80 1.00 -4 6 6 12.90 1.10 -4 6 -6 13.50 0.90 -4 6 -6 12.60 0.90 4 -6 -6 13.00 1.00 4 6 6 14.10 1.20 -4 -6 -7 42.40 2.20 4 6 -7 41.80 2.10 -4 6 7 43.90 2.30 4 -6 7 43.70 2.20 -4 6 -7 43.80 2.00 4 -6 -7 43.10 2.10 -4 6 -7 44.40 2.10 4 6 7 42.80 2.30 4 -6 8 22.20 1.70 -4 6 8 22.40 1.90 4 6 -8 19.60 1.50 -4 -6 -8 18.30 1.70 -4 -6 8 19.90 1.70 4 -6 -8 23.20 1.50 -4 6 -8 22.10 1.50 4 6 8 22.50 1.80 5 -6 0 2.10 0.30 -5 6 0 1.70 0.30 -5 6 1 143.29 5.50 5 -6 1 140.79 5.50 5 -6 -1 144.09 5.20 5 -6 -1 139.19 5.40 -5 6 -1 142.09 5.50 5 -6 -1 147.89 5.30 -5 -6 -2 0.40 0.20 5 6 -2 0.50 0.20 5 -6 2 0.40 0.30 -5 -6 -2 0.70 0.20 5 6 -2 0.60 0.20 5 6 -2 0.20 0.20 -5 6 2 0.60 0.20 -5 6 -2 0.40 0.30 5 -6 -2 0.50 0.20 5 -6 -2 0.50 0.20 -5 6 -2 -0.10 0.30 -5 -6 2 1.00 0.30 5 6 2 0.20 0.20 -5 -6 -3 226.18 8.90 -5 6 3 242.48 8.90 5 6 -3 229.08 8.80 -5 6 3 241.78 8.80 5 6 -3 243.38 8.80 -5 -6 -3 245.18 8.80 5 6 3 236.78 8.80 5 -6 -3 243.98 8.80 -5 6 -3 236.78 8.90 5 -6 -3 250.57 8.80 -5 6 -3 239.68 8.70 -5 -6 -4 1.30 0.30 5 6 -4 1.20 0.30 -5 -6 -4 1.20 0.40 -5 6 4 1.10 0.40 5 -6 -4 1.10 0.30 -5 6 -4 1.10 0.30 5 -6 -4 1.30 0.30 -5 6 -4 1.30 0.30 5 6 4 1.50 0.40 -5 6 5 2.70 0.50 5 6 -5 3.60 0.50 -5 -6 -5 3.30 0.60 5 -6 -5 3.30 0.50 5 6 5 3.30 0.60 -5 6 -5 3.90 0.40 5 -6 -5 4.00 0.50 5 -6 -5 5.00 0.50 -5 6 -5 4.60 0.50 -5 6 6 -0.10 0.50 5 6 -6 0.20 0.40 -5 -6 -6 -0.10 0.50 5 -6 -6 0.00 0.40 -5 6 -6 0.10 0.40 5 6 6 0.10 0.50 -5 6 -6 0.50 0.40 -5 -6 -7 97.29 4.30 5 6 -7 96.89 4.10 -5 6 7 94.79 4.20 5 -6 7 98.59 4.10 -5 6 -7 98.79 4.00 5 6 7 99.69 4.20 5 -6 -7 99.59 4.00 -5 6 -7 99.49 4.00 -5 6 8 0.60 0.90 -5 -6 -8 0.30 0.80 5 -6 8 -0.20 0.70 5 6 -8 1.00 0.70 5 6 8 1.10 0.90 5 -6 -8 1.20 0.60 -5 -6 8 -0.80 0.70 -5 6 -8 0.80 0.60 6 -6 0 11.40 0.80 -6 6 0 11.20 0.80 6 6 0 8.50 0.60 -6 6 0 13.00 0.80 -6 -6 0 9.30 0.80 6 -6 0 12.20 0.60 6 6 -1 0.30 0.20 -6 6 1 1.30 0.30 -6 -6 -1 -0.10 0.30 6 -6 1 0.20 0.30 -6 6 1 0.70 0.30 6 -6 -1 0.40 0.20 -6 6 -1 -0.10 0.30 -6 -6 1 0.30 0.30 -6 6 -1 -0.10 0.20 6 -6 -1 0.00 0.20 6 -6 -1 0.10 0.10 6 -6 2 0.30 0.30 6 6 -2 0.20 0.20 6 6 -2 0.10 0.10 -6 -6 -2 -0.10 0.20 -6 -6 -2 0.90 0.30 6 6 -2 -0.10 0.20 -6 6 2 0.20 0.20 6 6 2 0.30 0.20 -6 -6 2 0.70 0.30 -6 6 -2 -0.20 0.30 6 -6 -2 0.30 0.20 -6 6 -2 0.30 0.30 6 -6 -2 0.40 0.20 -6 -6 -3 0.50 0.30 -6 6 3 0.70 0.30 -6 -6 -3 1.00 0.30 -6 6 -3 0.60 0.20 6 -6 -3 0.60 0.20 6 -6 -3 0.40 0.20 -6 6 -3 0.40 0.30 6 6 3 1.90 0.30 6 6 -4 5.50 0.50 -6 6 4 3.10 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18.50 1.20 8 -15 -2 19.00 1.10 8 15 -3 27.90 1.50 -8 15 3 23.40 1.80 -8 -15 -3 27.30 1.70 8 -15 -3 26.70 1.40 8 15 3 28.50 1.50 8 -15 -3 26.50 1.50 -8 -15 -4 0.00 0.60 8 15 -4 0.00 0.50 8 15 4 0.20 0.50 8 -15 -4 0.70 0.50 8 -15 -4 0.50 0.50 8 15 -5 19.70 1.50 -8 -15 -5 18.00 1.50 8 15 5 21.50 1.60 8 -15 -5 21.40 1.50 8 -15 -5 20.00 1.30 8 15 -6 8.60 1.10 -8 -15 -6 9.10 1.40 8 15 6 9.40 1.20 8 -15 -6 8.30 0.90 8 -15 -6 9.00 1.10 -8 -15 -7 10.60 1.40 8 15 -7 9.20 1.30 8 -15 -7 8.60 1.00 8 -15 -7 10.80 1.20 8 15 7 10.90 1.30 -9 15 0 120.99 5.40 9 15 0 128.39 5.00 9 -15 0 133.49 4.90 -9 -15 0 133.19 5.20 9 15 -1 34.90 1.60 -9 15 1 33.50 2.00 -9 -15 -1 33.00 1.90 9 -15 -1 33.80 1.50 9 15 1 32.30 1.60 -9 -15 1 35.50 1.80 9 -15 -1 35.40 1.80 -9 15 -1 30.40 2.00 -9 15 2 41.20 2.30 9 15 -2 44.50 2.00 -9 -15 -2 42.10 2.20 9 -15 -2 41.90 1.90 9 15 2 43.00 2.00 -9 -15 2 44.70 2.20 9 -15 -2 44.10 2.00 -9 15 3 60.89 3.20 -9 -15 -3 62.99 3.10 9 15 -3 69.39 2.90 9 -15 -3 66.19 2.70 9 15 3 63.59 2.80 9 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7.30 1.10 -1 28 -2 7.20 1.00 1 -28 -2 5.10 1.00 1 28 2 6.00 1.00 -1 28 3 3.60 1.10 1 -28 -3 4.00 1.50 1 28 3 3.80 1.30 -1 28 -3 2.40 1.20 -2 28 0 7.90 1.00 2 28 0 8.70 1.00 -2 -28 -1 2.80 0.90 -2 28 1 2.10 0.80 2 28 -1 4.50 0.90 -2 28 -1 2.70 0.80 2 28 1 3.20 0.80 2 28 -2 5.30 1.00 -2 28 2 6.20 1.00 2 -28 -2 5.80 1.00 -2 28 -2 5.60 1.00 -3 28 0 13.30 1.50 3 28 0 17.10 1.40 3 28 -1 2.50 0.80 -3 -28 -1 -0.40 0.80 3 28 1 1.30 0.70 -3 28 -1 1.30 0.70 -3 -28 -2 -0.80 0.80 3 28 -2 1.20 0.80 3 28 2 2.10 0.80 -3 28 -2 2.70 0.80 3 -28 -2 1.00 0.80 4 28 0 32.20 1.90 4 28 -1 4.70 0.90 -4 -28 -1 3.70 1.00 4 28 1 4.40 0.80 4 28 -2 159.08 6.10 -4 -28 -2 148.49 6.30 4 28 2 151.18 6.10 4 -28 -2 145.39 6.00 5 28 0 17.20 1.40 -5 -28 -1 9.40 1.30 5 28 -1 10.70 1.10 5 28 1 10.20 1.00 -5 -28 -2 -0.20 0.90 5 28 -2 1.20 0.80 5 28 2 2.10 0.80 5 -28 -2 0.30 0.70 -6 -28 0 3.70 1.00 6 28 0 5.00 0.80 6 28 -1 14.90 1.20 -6 -28 -1 11.20 1.40 6 28 1 12.80 1.20 6 -28 -2 213.98 8.60 -7 -28 0 17.60 1.60 7 28 0 16.70 1.40 -7 -28 -1 -0.30 0.90 7 28 -1 1.90 0.80 7 28 1 1.20 0.70 -8 -28 0 1.10 1.20 0 29 0 1.80 0.80 0 29 -1 4.60 1.00 0 29 1 4.20 0.90 0 29 2 0.20 1.10 1 29 0 21.90 1.70 -1 29 0 19.80 1.70 -1 29 1 19.60 1.60 -1 -29 -1 18.80 1.60 1 29 -1 18.50 1.60 1 29 1 22.40 1.70 -1 29 -1 19.70 1.60 -1 29 2 1.00 1.20 -2 29 0 1.00 0.80 2 29 0 0.20 0.70 2 29 -1 0.40 0.80 -2 -29 -1 -1.50 0.80 -2 29 1 0.80 0.80 2 29 1 -0.50 0.70 -2 29 -1 -0.30 0.70 3 29 0 2.40 0.80 -3 -29 -1 29.10 2.00 3 29 -1 31.20 1.90 3 29 1 30.30 1.90 4 29 0 10.00 1.10 -4 -29 -1 -0.90 0.90 4 29 -1 0.10 1.00 4 29 1 0.40 1.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 10738 _shelx_res_file ; TITL Mn2Co3Ge_10Mn_0ma_a.res in Pnnm Mn2Co3Ge_10Mn_0ma.res created by SHELXL-2018/3 at 21:04:19 on 19-Jan-2021 CELL 0.71073 12.6427 15.6725 4.8374 90.000 90.000 90.000 ZERR 2.00 0.0010 0.0012 0.0004 0.000 0.000 0.000 LATT 1 SYMM x+1/2, -y+1/2, -z+1/2 SYMM -x+1/2, y+1/2, -z+1/2 SYMM -x, -y, z SFAC MN CO GE UNIT 29.7886 30.9654 13.246 LIST 6 TEMP 23.000 acta omit 9 6 6 omit 0 21 3 omit 15 6 3 L.S. 4 FMAP 2 EADP CO2 GE22 EXYZ CO2 GE22 EADP CO1 MN11 EXYZ CO1 MN11 EADP CO3 MN33 EXYZ CO3 MN33 PLAN 5 BOND WGHT 0.016600 1.722500 FVAR 0.10100 0.87643 0.59425 MN1 1 0.026650 0.571152 0.000000 10.50000 0.00776 0.00632 = 0.00877 0.00000 0.00000 -0.00090 MN2 1 0.085858 0.734159 0.000000 10.50000 0.00568 0.00643 = 0.00831 0.00000 0.00000 -0.00049 MN3 1 0.101756 0.161466 0.000000 10.50000 0.00671 0.00690 = 0.00826 0.00000 0.00000 0.00025 MN4 1 0.220700 0.444397 0.000000 10.50000 0.00888 0.00681 = 0.00721 0.00000 0.00000 -0.00104 MN5 1 0.285179 0.264335 0.000000 10.50000 0.00615 0.00746 = 0.00771 0.00000 0.00000 0.00006 MN6 1 0.401475 0.549966 0.000000 10.50000 0.00600 0.00692 = 0.00728 0.00000 0.00000 0.00017 MN7 1 0.599500 0.027115 0.000000 10.50000 0.00517 0.00606 = 0.01029 0.00000 0.00000 -0.00008 CO1 2 0.100758 0.324111 0.234597 21.00000 0.00467 0.00666 = 0.00424 0.00053 0.00005 -0.00006 MN11 1 0.100758 0.324111 0.234597 -21.00000 0.00467 0.00666 = 0.00424 0.00053 0.00005 -0.00006 CO2 2 0.289210 0.102440 0.253731 31.00000 0.00573 0.00671 = 0.00560 -0.00113 0.00089 -0.00075 GE22 3 0.289210 0.102440 0.253731 -31.00000 0.00573 0.00671 = 0.00560 -0.00113 0.00089 -0.00075 CO3 2 0.412417 0.390785 0.240237 10.90000 0.00542 0.00591 = 0.00442 -0.00078 0.00076 0.00017 MN33 1 0.412417 0.390785 0.240237 10.10000 0.00542 0.00591 = 0.00442 -0.00078 0.00076 0.00017 CO4 2 0.190099 0.001393 0.000000 10.50000 0.00450 0.00521 = 0.00844 0.00000 0.00000 -0.00084 CO5 2 0.444393 0.136927 0.000000 10.50000 0.00448 0.00723 = 0.00807 0.00000 0.00000 -0.00127 CO6 2 0.697854 0.290907 0.000000 10.50000 0.00516 0.00540 = 0.00824 0.00000 0.00000 -0.00066 GE1 3 0.507656 0.285117 0.000000 10.50000 0.00568 0.00574 = 0.00735 0.00000 0.00000 0.00174 GE2 3 0.757892 0.146231 0.000000 10.50000 0.00424 0.00610 = 0.00838 0.00000 0.00000 0.00089 GE3 3 0.000000 0.000000 0.000000 10.25000 0.00428 0.00669 = 0.00750 0.00000 0.00000 0.00157 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM Mn2Co3Ge_10Mn_0ma_a.res in Pnnm REM wR2 = 0.051525, GooF = S = 1.10334, Restrained GooF = 1.10334 for all data REM R1 = 0.021855 for 3277 Fo > 4sig(Fo) and 0.026519 for all 3686 data REM 106 parameters refined using 0 restraints END WGHT 0.0166 1.7225 REM Highest difference peak 1.241, deepest hole -0.919, 1-sigma level 0.232 Q1 1 0.2208 0.0383 0.0000 10.50000 0.05 1.24 Q2 1 0.5828 0.2871 0.0000 10.50000 0.05 1.23 Q3 1 0.6162 0.2905 0.0000 10.50000 0.05 1.23 Q4 1 -0.0842 -0.0014 0.0000 10.50000 0.05 1.23 Q5 1 0.1648 -0.0395 0.0000 10.50000 0.05 1.22 ; _shelx_res_checksum 81663 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x+1/2, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x, -y, z' '-x, -y, -z' '-x-1/2, y-1/2, z-1/2' 'x-1/2, -y-1/2, z-1/2' 'x, y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Mn Mn1 0.02665(3) 0.57115(2) 0.000000 0.00762(5) Uani d 1 . . Mn Mn2 0.08586(3) 0.73416(2) 0.000000 0.00681(5) Uani d 1 . . Mn Mn3 0.10176(3) 0.16147(2) 0.000000 0.00729(5) Uani d 1 . . Mn Mn4 0.22070(3) 0.44440(2) 0.000000 0.00763(5) Uani d 1 . . Mn Mn5 0.28518(3) 0.26433(2) 0.000000 0.00710(5) Uani d 1 . . Mn Mn6 0.40147(3) 0.54997(2) 0.000000 0.00673(5) Uani d 1 . . Mn Mn7 0.59950(3) 0.02711(2) 0.000000 0.00717(5) Uani d 1 . . Co Co1 0.10076(2) 0.32411(2) 0.23460(4) 0.00519(4) Uani d 0.876(12) . . Mn Mn11 0.10076(2) 0.32411(2) 0.23460(4) 0.00519(4) Uani d 0.124(12) . . Co Co2 0.28921(2) 0.10244(2) 0.25373(4) 0.00601(5) Uani d 0.594(5) . . Ge Ge22 0.28921(2) 0.10244(2) 0.25373(4) 0.00601(5) Uani d 0.406(5) . . Co Co3 0.41242(2) 0.39078(2) 0.24024(4) 0.00525(4) Uani d 0.9 . . Mn Mn33 0.41242(2) 0.39078(2) 0.24024(4) 0.00525(4) Uani d 0.1 . . Co Co4 0.19010(2) 0.00139(2) 0.000000 0.00605(5) Uani d 1 . . Co Co5 0.44439(2) 0.13693(2) 0.000000 0.00660(5) Uani d 1 . . Co Co6 0.69785(2) 0.29091(2) 0.000000 0.00626(5) Uani d 1 . . Ge Ge1 0.50766(2) 0.28512(2) 0.000000 0.00626(4) Uani d 1 . . Ge Ge2 0.75789(2) 0.14623(2) 0.000000 0.00624(4) Uani d 1 . . Ge Ge3 0.000000 0.000000 0.000000 0.00616(5) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Mn1 0.00776(12) 0.00632(11) 0.00877(12) -0.00090(10) 0.000 0.000 Mn2 0.00568(11) 0.00643(11) 0.00831(12) -0.00049(9) 0.000 0.000 Mn3 0.00671(12) 0.00690(12) 0.00826(11) 0.00025(9) 0.000 0.000 Mn4 0.00888(13) 0.00681(11) 0.00721(12) -0.00104(10) 0.000 0.000 Mn5 0.00615(12) 0.00746(11) 0.00771(12) 0.00006(9) 0.000 0.000 Mn6 0.00600(11) 0.00692(12) 0.00728(11) 0.00017(9) 0.000 0.000 Mn7 0.00517(11) 0.00606(12) 0.01029(12) -0.00008(9) 0.000 0.000 Co1 0.00467(8) 0.00666(8) 0.00424(7) -0.00006(6) 0.00005(6) 0.00053(5) Mn11 0.00467(8) 0.00666(8) 0.00424(7) -0.00006(6) 0.00005(6) 0.00053(5) Co2 0.00573(8) 0.00671(8) 0.00560(7) -0.00075(5) 0.00089(5) -0.00113(5) Ge22 0.00573(8) 0.00671(8) 0.00560(7) -0.00075(5) 0.00089(5) -0.00113(5) Co3 0.00542(7) 0.00591(8) 0.00442(7) 0.00017(6) 0.00076(5) -0.00078(5) Mn33 0.00542(7) 0.00591(8) 0.00442(7) 0.00017(6) 0.00076(5) -0.00078(5) Co4 0.00450(10) 0.00521(10) 0.00844(11) -0.00084(8) 0.000 0.000 Co5 0.00448(10) 0.00723(11) 0.00807(11) -0.00127(8) 0.000 0.000 Co6 0.00516(10) 0.00540(10) 0.00824(11) -0.00066(8) 0.000 0.000 Ge1 0.00568(8) 0.00574(8) 0.00735(8) 0.00174(6) 0.000 0.000 Ge2 0.00424(8) 0.00610(8) 0.00838(8) 0.00089(6) 0.000 0.000 Ge3 0.00428(11) 0.00669(12) 0.00750(11) 0.00157(9) 0.000 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Mn Mn 0.3368 0.7283 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag Mn1 Mn1 Co1 5_565 4_565 115.53(2) ? Mn1 Mn1 Co1 5_565 5_565 115.53(2) ? Co1 Mn1 Co1 4_565 5_565 52.528(12) ? Mn1 Mn1 Co5 5_565 6_666 114.306(10) ? Co1 Mn1 Co5 4_565 6_666 55.589(9) ? Co1 Mn1 Co5 5_565 6_666 103.961(14) ? Mn1 Mn1 Co5 5_565 6_665 114.306(10) ? Co1 Mn1 Co5 4_565 6_665 103.961(14) ? Co1 Mn1 Co5 5_565 6_665 55.589(10) ? Co5 Mn1 Co5 6_666 6_665 131.329(19) ? Mn1 Mn1 Co2 5_565 3 115.43(2) ? Co1 Mn1 Co2 4_565 3 103.503(11) ? Co1 Mn1 Co2 5_565 3 129.031(15) ? Co5 Mn1 Co2 6_666 3 53.118(9) ? Co5 Mn1 Co2 6_665 3 102.459(14) ? Mn1 Mn1 Co2 5_565 6_665 115.43(2) ? Co1 Mn1 Co2 4_565 6_665 129.031(15) ? Co1 Mn1 Co2 5_565 6_665 103.503(11) ? Co5 Mn1 Co2 6_666 6_665 102.459(14) ? Co5 Mn1 Co2 6_665 6_665 53.118(9) ? Co2 Mn1 Co2 3 6_665 53.197(11) ? Mn1 Mn1 Mn2 5_565 . 179.52(3) ? Co1 Mn1 Mn2 4_565 . 64.048(12) ? Co1 Mn1 Mn2 5_565 . 64.048(12) ? Co5 Mn1 Mn2 6_666 . 65.706(10) ? Co5 Mn1 Mn2 6_665 . 65.706(10) ? Co2 Mn1 Mn2 3 . 64.983(11) ? Co2 Mn1 Mn2 6_665 . 64.983(11) ? Mn1 Mn1 Mn7 5_565 6_665 67.870(11) ? Co1 Mn1 Mn7 4_565 6_665 99.865(14) ? Co1 Mn1 Mn7 5_565 6_665 56.811(10) ? Co5 Mn1 Mn7 6_666 6_665 154.660(16) ? Co5 Mn1 Mn7 6_665 6_665 54.822(10) ? Co2 Mn1 Mn7 3 6_665 151.030(11) ? Co2 Mn1 Mn7 6_665 6_665 98.491(9) ? Mn2 Mn1 Mn7 . 6_665 111.899(11) ? Mn1 Mn1 Mn7 5_565 6_666 67.870(11) ? Co1 Mn1 Mn7 4_565 6_666 56.811(10) ? Co1 Mn1 Mn7 5_565 6_666 99.865(14) ? Co5 Mn1 Mn7 6_666 6_666 54.822(10) ? Co5 Mn1 Mn7 6_665 6_666 154.660(16) ? Co2 Mn1 Mn7 3 6_666 98.491(9) ? Co2 Mn1 Mn7 6_665 6_666 151.030(11) ? Mn2 Mn1 Mn7 . 6_666 111.899(11) ? Mn7 Mn1 Mn7 6_665 6_666 108.605(16) ? Mn1 Mn1 Mn7 5_565 2_454 66.355(11) ? Co1 Mn1 Mn7 4_565 2_454 151.018(12) ? Co1 Mn1 Mn7 5_565 2_454 99.440(9) ? Co5 Mn1 Mn7 6_666 2_454 152.641(16) ? Co5 Mn1 Mn7 6_665 2_454 54.876(10) ? Co2 Mn1 Mn7 3 2_454 100.733(13) ? Co2 Mn1 Mn7 6_665 2_454 57.797(9) ? Mn2 Mn1 Mn7 . 2_454 113.875(11) ? Mn7 Mn1 Mn7 6_665 2_454 52.632(12) ? Mn7 Mn1 Mn7 6_666 2_454 134.225(13) ? Mn1 Mn1 Mn7 5_565 2_455 66.355(12) ? Co1 Mn1 Mn7 4_565 2_455 99.440(9) ? Co1 Mn1 Mn7 5_565 2_455 151.018(12) ? Co5 Mn1 Mn7 6_666 2_455 54.876(10) ? Co5 Mn1 Mn7 6_665 2_455 152.641(16) ? Co2 Mn1 Mn7 3 2_455 57.797(9) ? Co2 Mn1 Mn7 6_665 2_455 100.733(13) ? Mn2 Mn1 Mn7 . 2_455 113.875(11) ? Mn7 Mn1 Mn7 6_665 2_455 134.225(13) ? Mn7 Mn1 Mn7 6_666 2_455 52.632(12) ? Mn7 Mn1 Mn7 2_454 2_455 106.855(16) ? Mn1 Mn2 Ge2 . 5_665 149.830(17) ? Mn1 Mn2 Co3 . 3 148.918(10) ? Ge2 Mn2 Co3 5_665 3 51.797(9) ? Mn1 Mn2 Co3 . 6_665 148.918(10) ? Ge2 Mn2 Co3 5_665 6_665 51.797(9) ? Co3 Mn2 Co3 3 6_665 54.215(12) ? Mn1 Mn2 Co6 . 5_665 98.155(15) ? Ge2 Mn2 Co6 5_665 5_665 51.675(11) ? Co3 Mn2 Co6 3 5_665 96.820(12) ? Co3 Mn2 Co6 6_665 5_665 96.820(12) ? Mn1 Mn2 Co1 . 5_565 56.266(10) ? Ge2 Mn2 Co1 5_665 5_565 147.559(11) ? Co3 Mn2 Co1 3 5_565 119.104(14) ? Co3 Mn2 Co1 6_665 5_565 96.513(10) ? Co6 Mn2 Co1 5_665 5_565 142.693(13) ? Mn1 Mn2 Co1 . 4_565 56.266(10) ? Ge2 Mn2 Co1 5_665 4_565 147.559(11) ? Co3 Mn2 Co1 3 4_565 96.513(10) ? Co3 Mn2 Co1 6_665 4_565 119.104(14) ? Co6 Mn2 Co1 5_665 4_565 142.693(12) ? Co1 Mn2 Co1 5_565 4_565 48.318(11) ? Mn1 Mn2 Ge1 . 6_665 98.890(10) ? Ge2 Mn2 Ge1 5_665 6_665 96.295(10) ? Co3 Mn2 Ge1 3 6_665 98.201(12) ? Co3 Mn2 Ge1 6_665 6_665 50.038(7) ? Co6 Mn2 Ge1 5_665 6_665 117.206(9) ? Co1 Mn2 Ge1 5_565 6_665 51.896(8) ? Co1 Mn2 Ge1 4_565 6_665 95.045(13) ? Mn1 Mn2 Ge1 . 6_666 98.890(10) ? Ge2 Mn2 Ge1 5_665 6_666 96.295(10) ? Co3 Mn2 Ge1 3 6_666 50.038(8) ? Co3 Mn2 Ge1 6_665 6_666 98.201(12) ? Co6 Mn2 Ge1 5_665 6_666 117.206(8) ? Co1 Mn2 Ge1 5_565 6_666 95.045(12) ? Co1 Mn2 Ge1 4_565 6_666 51.896(8) ? Ge1 Mn2 Ge1 6_665 6_666 118.928(16) ? Mn1 Mn2 Co2 . 6_665 57.485(11) ? Ge2 Mn2 Co2 5_665 6_665 95.523(13) ? Co3 Mn2 Co2 3 6_665 145.906(15) ? Co3 Mn2 Co2 6_665 6_665 116.643(10) ? Co6 Mn2 Co2 5_665 6_665 49.498(9) ? Co1 Mn2 Co2 5_565 6_665 93.539(11) ? Co1 Mn2 Co2 4_565 6_665 113.751(14) ? Ge1 Mn2 Co2 6_665 6_665 94.534(8) ? Ge1 Mn2 Co2 6_666 6_665 142.822(11) ? Mn1 Mn2 Co2 . 3 57.485(11) ? Ge2 Mn2 Co2 5_665 3 95.523(13) ? Co3 Mn2 Co2 3 3 116.643(10) ? Co3 Mn2 Co2 6_665 3 145.906(15) ? Co6 Mn2 Co2 5_665 3 49.498(9) ? Co1 Mn2 Co2 5_565 3 113.751(14) ? Co1 Mn2 Co2 4_565 3 93.539(11) ? Ge1 Mn2 Co2 6_665 3 142.822(11) ? Ge1 Mn2 Co2 6_666 3 94.534(8) ? Co2 Mn2 Co2 6_665 3 49.245(10) ? Mn1 Mn2 Mn3 . 5_565 108.261(16) ? Ge2 Mn2 Mn3 5_665 5_565 101.909(15) ? Co3 Mn2 Mn3 3 5_565 60.078(10) ? Co3 Mn2 Mn3 6_665 5_565 60.078(10) ? Co6 Mn2 Mn3 5_665 5_565 153.584(17) ? Co1 Mn2 Mn3 5_565 5_565 59.104(11) ? Co1 Mn2 Mn3 4_565 5_565 59.104(11) ? Ge1 Mn2 Mn3 6_665 5_565 59.466(8) ? Ge1 Mn2 Mn3 6_666 5_565 59.466(8) ? Co2 Mn2 Mn3 6_665 5_565 149.842(10) ? Co2 Mn2 Mn3 3 5_565 149.842(10) ? Co4 Mn3 Co1 . . 146.763(12) ? Co4 Mn3 Co1 . 8 146.763(12) ? Co1 Mn3 Co1 . 8 47.997(11) ? Co4 Mn3 Co6 . 2_455 93.834(11) ? Co1 Mn3 Co6 . 2_455 53.753(9) ? Co1 Mn3 Co6 8 2_455 96.284(13) ? Co4 Mn3 Co6 . 2_454 93.834(11) ? Co1 Mn3 Co6 . 2_454 96.284(13) ? Co1 Mn3 Co6 8 2_454 53.753(9) ? Co6 Mn3 Co6 2_455 2_454 118.959(17) ? Co4 Mn3 Ge1 . 2_454 116.257(9) ? Co1 Mn3 Ge1 . 2_454 94.339(12) ? Co1 Mn3 Ge1 8 2_454 51.582(8) ? Co6 Mn3 Ge1 2_455 2_454 147.326(16) ? Co6 Mn3 Ge1 2_454 2_454 50.603(9) ? Co4 Mn3 Ge1 . 2_455 116.257(8) ? Co1 Mn3 Ge1 . 2_455 51.581(8) ? Co1 Mn3 Ge1 8 2_455 94.339(12) ? Co6 Mn3 Ge1 2_455 2_455 50.603(9) ? Co6 Mn3 Ge1 2_454 2_455 147.326(16) ? Ge1 Mn3 Ge1 2_454 2_455 117.952(15) ? Co4 Mn3 Mn5 . . 100.809(15) ? Co1 Mn3 Mn5 . . 58.817(10) ? Co1 Mn3 Mn5 8 . 58.817(10) ? Co6 Mn3 Mn5 2_455 . 59.534(9) ? Co6 Mn3 Mn5 2_454 . 59.534(8) ? Ge1 Mn3 Mn5 2_454 . 100.181(10) ? Ge1 Mn3 Mn5 2_455 . 100.181(11) ? Co4 Mn3 Co2 . 8 50.176(9) ? Co1 Mn3 Co2 . 8 118.666(13) ? Co1 Mn3 Co2 8 8 97.253(10) ? Co6 Mn3 Co2 2_455 8 95.644(13) ? Co6 Mn3 Co2 2_454 8 49.435(8) ? Ge1 Mn3 Co2 2_454 8 94.497(8) ? Ge1 Mn3 Co2 2_455 8 145.401(11) ? Mn5 Mn3 Co2 . 8 59.872(11) ? Co4 Mn3 Co2 . . 50.176(9) ? Co1 Mn3 Co2 . . 97.253(10) ? Co1 Mn3 Co2 8 . 118.665(13) ? Co6 Mn3 Co2 2_455 . 49.435(8) ? Co6 Mn3 Co2 2_454 . 95.644(13) ? Ge1 Mn3 Co2 2_454 . 145.400(11) ? Ge1 Mn3 Co2 2_455 . 94.497(8) ? Mn5 Mn3 Co2 . . 59.872(11) ? Co2 Mn3 Co2 8 . 51.510(11) ? Co1 Mn4 Co1 8 . 50.260(12) ? Co1 Mn4 Co2 8 3 142.479(16) ? Co1 Mn4 Co2 . 3 115.174(11) ? Co1 Mn4 Co2 8 6_665 115.174(11) ? Co1 Mn4 Co2 . 6_665 142.478(16) ? Co2 Mn4 Co2 3 6_665 51.314(11) ? Co1 Mn4 Co4 8 6_666 144.716(12) ? Co1 Mn4 Co4 . 6_666 94.953(8) ? Co2 Mn4 Co4 3 6_666 50.234(8) ? Co2 Mn4 Co4 6_665 6_666 96.005(13) ? Co1 Mn4 Co4 8 6_665 94.952(9) ? Co1 Mn4 Co4 . 6_665 144.716(11) ? Co2 Mn4 Co4 3 6_665 96.005(13) ? Co2 Mn4 Co4 6_665 6_665 50.234(8) ? Co4 Mn4 Co4 6_666 6_665 118.511(17) ? Co1 Mn4 Co3 8 8 95.892(11) ? Co1 Mn4 Co3 . 8 116.945(14) ? Co2 Mn4 Co3 3 8 119.107(14) ? Co2 Mn4 Co3 6_665 8 97.418(10) ? Co4 Mn4 Co3 6_666 8 95.997(13) ? Co4 Mn4 Co3 6_665 8 52.784(9) ? Co1 Mn4 Co3 8 . 116.945(14) ? Co1 Mn4 Co3 . . 95.893(11) ? Co2 Mn4 Co3 3 . 97.418(10) ? Co2 Mn4 Co3 6_665 . 119.107(14) ? Co4 Mn4 Co3 6_666 . 52.784(9) ? Co4 Mn4 Co3 6_665 . 95.997(13) ? Co3 Mn4 Co3 8 . 48.742(11) ? Co1 Mn4 Mn6 8 . 150.846(10) ? Co1 Mn4 Mn6 . . 150.847(10) ? Co2 Mn4 Mn6 3 . 60.592(11) ? Co2 Mn4 Mn6 6_665 . 60.592(10) ? Co4 Mn4 Mn6 6_666 . 59.288(8) ? Co4 Mn4 Mn6 6_665 . 59.288(8) ? Co3 Mn4 Mn6 8 . 58.521(11) ? Co3 Mn4 Mn6 . . 58.521(11) ? Co1 Mn4 Ge2 8 2_454 51.708(8) ? Co1 Mn4 Ge2 . 2_454 95.891(12) ? Co2 Mn4 Ge2 3 2_454 145.625(11) ? Co2 Mn4 Ge2 6_665 2_454 95.101(8) ? Co4 Mn4 Ge2 6_666 2_454 145.407(16) ? Co4 Mn4 Ge2 6_665 2_454 50.310(8) ? Co3 Mn4 Ge2 8 2_454 50.043(8) ? Co3 Mn4 Ge2 . 2_454 93.420(12) ? Mn6 Mn4 Ge2 . 2_454 99.146(10) ? Co1 Mn5 Co1 8 . 48.611(11) ? Co1 Mn5 Co6 8 2_454 54.217(9) ? Co1 Mn5 Co6 . 2_454 97.317(13) ? Co1 Mn5 Co6 8 2_455 97.317(13) ? Co1 Mn5 Co6 . 2_455 54.217(9) ? Co6 Mn5 Co6 2_454 2_455 119.766(17) ? Co1 Mn5 Co3 8 8 94.265(11) ? Co1 Mn5 Co3 . 8 114.550(14) ? Co6 Mn5 Co3 2_454 8 94.982(9) ? Co6 Mn5 Co3 2_455 8 143.484(12) ? Co1 Mn5 Co3 8 . 114.550(14) ? Co1 Mn5 Co3 . . 94.266(11) ? Co6 Mn5 Co3 2_454 . 143.484(11) ? Co6 Mn5 Co3 2_455 . 94.982(9) ? Co3 Mn5 Co3 8 . 48.958(11) ? Co1 Mn5 Ge2 8 2_455 94.633(12) ? Co1 Mn5 Ge2 . 2_455 51.236(8) ? Co6 Mn5 Ge2 2_454 2_455 148.049(16) ? Co6 Mn5 Ge2 2_455 2_455 50.427(9) ? Co3 Mn5 Ge2 8 2_455 94.269(12) ? Co3 Mn5 Ge2 . 2_455 50.417(8) ? Co1 Mn5 Ge2 8 2_454 51.235(8) ? Co1 Mn5 Ge2 . 2_454 94.633(12) ? Co6 Mn5 Ge2 2_454 2_454 50.427(9) ? Co6 Mn5 Ge2 2_455 2_454 148.049(16) ? Co3 Mn5 Ge2 8 2_454 50.417(8) ? Co3 Mn5 Ge2 . 2_454 94.269(12) ? Ge2 Mn5 Ge2 2_455 2_454 118.343(15) ? Co1 Mn5 Co2 8 8 98.158(10) ? Co1 Mn5 Co2 . 8 120.021(14) ? Co6 Mn5 Co2 2_454 8 49.596(8) ? Co6 Mn5 Co2 2_455 8 96.031(13) ? Co3 Mn5 Co2 8 8 116.438(10) ? Co3 Mn5 Co2 . 8 143.712(15) ? Ge2 Mn5 Co2 2_455 8 145.485(11) ? Ge2 Mn5 Co2 2_454 8 94.371(8) ? Co1 Mn5 Co2 8 . 120.022(14) ? Co1 Mn5 Co2 . . 98.158(10) ? Co6 Mn5 Co2 2_454 . 96.031(13) ? Co6 Mn5 Co2 2_455 . 49.596(8) ? Co3 Mn5 Co2 8 . 143.712(15) ? Co3 Mn5 Co2 . . 116.437(10) ? Ge2 Mn5 Co2 2_455 . 94.372(8) ? Ge2 Mn5 Co2 2_454 . 145.485(11) ? Co2 Mn5 Co2 8 . 51.621(11) ? Co3 Mn6 Co3 8 . 49.887(11) ? Co3 Mn6 Co3 8 4_665 115.825(13) ? Co3 Mn6 Co3 . 4_665 94.790(11) ? Co3 Mn6 Co3 8 5_665 94.791(11) ? Co3 Mn6 Co3 . 5_665 115.825(13) ? Co3 Mn6 Co3 4_665 5_665 49.349(11) ? Co3 Mn6 Co4 8 6_665 53.679(8) ? Co3 Mn6 Co4 . 6_665 98.022(13) ? Co3 Mn6 Co4 4_665 6_665 143.553(11) ? Co3 Mn6 Co4 5_665 6_665 94.585(9) ? Co3 Mn6 Co4 8 6_666 98.022(13) ? Co3 Mn6 Co4 . 6_666 53.679(8) ? Co3 Mn6 Co4 4_665 6_666 94.585(9) ? Co3 Mn6 Co4 5_665 6_666 143.553(11) ? Co4 Mn6 Co4 6_665 6_666 120.386(17) ? Co3 Mn6 Co6 8 5_665 146.220(11) ? Co3 Mn6 Co6 . 5_665 146.221(11) ? Co3 Mn6 Co6 4_665 5_665 94.715(13) ? Co3 Mn6 Co6 5_665 5_665 94.715(13) ? Co4 Mn6 Co6 6_665 5_665 93.274(11) ? Co4 Mn6 Co6 6_666 5_665 93.274(11) ? Co3 Mn6 Co2 8 6_665 97.420(10) ? Co3 Mn6 Co2 . 6_665 119.110(13) ? Co3 Mn6 Co2 4_665 6_665 143.508(15) ? Co3 Mn6 Co2 5_665 6_665 116.758(10) ? Co4 Mn6 Co2 6_665 6_665 49.922(8) ? Co4 Mn6 Co2 6_666 6_665 95.244(13) ? Co6 Mn6 Co2 5_665 6_665 49.700(9) ? Co3 Mn6 Co2 8 3 119.109(13) ? Co3 Mn6 Co2 . 3 97.421(10) ? Co3 Mn6 Co2 4_665 3 116.758(10) ? Co3 Mn6 Co2 5_665 3 143.508(15) ? Co4 Mn6 Co2 6_665 3 95.243(13) ? Co4 Mn6 Co2 6_666 3 49.922(8) ? Co6 Mn6 Co2 5_665 3 49.700(9) ? Co2 Mn6 Co2 6_665 3 50.131(11) ? Co3 Mn6 Mn4 8 . 60.644(11) ? Co3 Mn6 Mn4 . . 60.645(11) ? Co3 Mn6 Mn4 4_665 . 151.676(9) ? Co3 Mn6 Mn4 5_665 . 151.676(9) ? Co4 Mn6 Mn4 6_665 . 60.226(8) ? Co4 Mn6 Mn4 6_666 . 60.226(9) ? Co6 Mn6 Mn4 5_665 . 99.175(15) ? Co2 Mn6 Mn4 6_665 . 58.470(11) ? Co2 Mn6 Mn4 3 . 58.470(11) ? Co3 Mn6 Ge1 8 5_665 143.795(12) ? Co3 Mn6 Ge1 . 5_665 143.795(12) ? Co3 Mn6 Ge1 4_665 5_665 49.600(8) ? Co3 Mn6 Ge1 5_665 5_665 49.600(8) ? Co4 Mn6 Ge1 6_665 5_665 114.724(9) ? Co4 Mn6 Ge1 6_666 5_665 114.724(9) ? Co6 Mn6 Ge1 5_665 5_665 50.690(11) ? Co2 Mn6 Ge1 6_665 5_665 94.643(12) ? Co2 Mn6 Ge1 3 5_665 94.643(12) ? Mn4 Mn6 Ge1 . 5_665 149.866(16) ? Co5 Mn7 Co5 . 5_655 119.090(15) ? Co5 Mn7 Mn7 . 5_655 59.937(15) ? Co5 Mn7 Mn7 5_655 5_655 59.153(14) ? Co5 Mn7 Co1 . 2 55.019(10) ? Co5 Mn7 Co1 5_655 2 149.038(8) ? Mn7 Mn7 Co1 5_655 2 106.620(16) ? Co5 Mn7 Co1 . 7_665 55.018(10) ? Co5 Mn7 Co1 5_655 7_665 149.038(8) ? Mn7 Mn7 Co1 5_655 7_665 106.620(16) ? Co1 Mn7 Co1 2 7_665 57.676(12) ? Co5 Mn7 Co4 . 5_655 148.264(17) ? Co5 Mn7 Co4 5_655 5_655 92.646(14) ? Mn7 Mn7 Co4 5_655 5_655 151.80(2) ? Co1 Mn7 Co4 2 5_655 98.002(12) ? Co1 Mn7 Co4 7_665 5_655 98.002(12) ? Co5 Mn7 Ge2 . . 95.736(15) ? Co5 Mn7 Ge2 5_655 . 145.174(16) ? Mn7 Mn7 Ge2 5_655 . 155.67(2) ? Co1 Mn7 Ge2 2 . 53.008(9) ? Co1 Mn7 Ge2 7_665 . 53.008(9) ? Co4 Mn7 Ge2 5_655 . 52.528(11) ? Co5 Mn7 Co2 . 5_655 150.333(9) ? Co5 Mn7 Co2 5_655 5_655 52.274(10) ? Mn7 Mn7 Co2 5_655 5_655 104.340(17) ? Co1 Mn7 Co2 2 5_655 148.909(15) ? Co1 Mn7 Co2 7_665 5_655 115.285(9) ? Co4 Mn7 Co2 5_655 5_655 51.319(9) ? Ge2 Mn7 Co2 . 5_655 97.402(13) ? Co5 Mn7 Co2 . 4_655 150.333(9) ? Co5 Mn7 Co2 5_655 4_655 52.274(10) ? Mn7 Mn7 Co2 5_655 4_655 104.340(17) ? Co1 Mn7 Co2 2 4_655 115.285(10) ? Co1 Mn7 Co2 7_665 4_655 148.909(15) ? Co4 Mn7 Co2 5_655 4_655 51.319(9) ? Ge2 Mn7 Co2 . 4_655 97.402(13) ? Co2 Mn7 Co2 5_655 4_655 52.842(11) ? Co5 Mn7 Mn4 . 2 107.205(11) ? Co5 Mn7 Mn4 5_655 2 105.200(11) ? Mn7 Mn7 Mn4 5_655 2 123.386(9) ? Co1 Mn7 Mn4 2 2 57.268(9) ? Co1 Mn7 Mn4 7_665 2 105.334(13) ? Co4 Mn7 Mn4 5_655 2 60.267(9) ? Ge2 Mn7 Mn4 . 2 60.538(9) ? Co2 Mn7 Mn4 5_655 2 102.420(13) ? Co2 Mn7 Mn4 4_655 2 58.150(10) ? Co5 Mn7 Mn4 . 2_554 107.205(11) ? Co5 Mn7 Mn4 5_655 2_554 105.200(11) ? Mn7 Mn7 Mn4 5_655 2_554 123.386(9) ? Co1 Mn7 Mn4 2 2_554 105.334(13) ? Co1 Mn7 Mn4 7_665 2_554 57.268(9) ? Co4 Mn7 Mn4 5_655 2_554 60.267(9) ? Ge2 Mn7 Mn4 . 2_554 60.538(9) ? Co2 Mn7 Mn4 5_655 2_554 58.150(9) ? Co2 Mn7 Mn4 4_655 2_554 102.420(13) ? Mn4 Mn7 Mn4 2 2_554 113.160(17) ? Co5 Mn7 Mn1 . 6_655 56.266(8) ? Co5 Mn7 Mn1 5_655 6_655 96.518(11) ? Mn7 Mn7 Mn1 5_655 6_655 64.331(10) ? Co1 Mn7 Mn1 2 6_655 101.065(13) ? Co1 Mn7 Mn1 7_665 6_655 53.737(9) ? Co4 Mn7 Mn1 5_655 6_655 124.506(8) ? Ge2 Mn7 Mn1 . 6_655 103.513(11) ? Co2 Mn7 Mn1 5_655 6_655 94.725(9) ? Co2 Mn7 Mn1 4_655 6_655 143.619(13) ? Mn4 Mn7 Mn1 2 6_655 157.713(16) ? Mn4 Mn7 Mn1 2_554 6_655 64.509(10) ? Co1 Co1 Ge2 8 2_455 122.180(6) ? Co1 Co1 Co5 8 2_455 121.821(7) ? Ge2 Co1 Co5 2_455 2_455 109.870(11) ? Co1 Co1 Ge1 8 2_455 121.716(6) ? Ge2 Co1 Ge1 2_455 2_455 104.617(10) ? Co5 Co1 Ge1 2_455 2_455 60.484(11) ? Co1 Co1 Co6 8 2_455 120.484(6) ? Ge2 Co1 Co6 2_455 2_455 57.820(10) ? Co5 Co1 Co6 2_455 2_455 107.755(11) ? Ge1 Co1 Co6 2_455 2_455 57.844(11) ? Co1 Co1 Mn1 8 5_565 63.736(6) ? Ge2 Co1 Mn1 2_455 5_565 129.042(13) ? Co5 Co1 Mn1 2_455 5_565 64.080(9) ? Ge1 Co1 Mn1 2_455 5_565 112.246(13) ? Co6 Co1 Mn1 2_455 5_565 170.084(13) ? Co1 Co1 Co1 8 8_556 180.0 ? Ge2 Co1 Co1 2_455 8_556 57.818(6) ? Co5 Co1 Co1 2_455 8_556 58.180(7) ? Ge1 Co1 Co1 2_455 8_556 58.285(6) ? Co6 Co1 Co1 2_455 8_556 59.515(6) ? Mn1 Co1 Co1 5_565 8_556 116.265(6) ? Co1 Co1 Mn7 8 2_455 118.837(6) ? Ge2 Co1 Mn7 2_455 2_455 65.110(10) ? Co5 Co1 Mn7 2_455 2_455 61.391(11) ? Ge1 Co1 Mn7 2_455 2_455 110.953(11) ? Co6 Co1 Mn7 2_455 2_455 112.468(11) ? Mn1 Co1 Mn7 5_565 2_455 69.452(10) ? Co1 Co1 Mn7 8_556 2_455 61.162(6) ? Co1 Co1 Mn4 8 . 64.869(6) ? Ge2 Co1 Mn4 2_455 . 67.822(9) ? Co5 Co1 Mn4 2_455 . 120.509(13) ? Ge1 Co1 Mn4 2_455 . 172.407(11) ? Co6 Co1 Mn4 2_455 . 116.276(13) ? Mn1 Co1 Mn4 5_565 . 73.558(13) ? Co1 Co1 Mn4 8_556 . 115.129(6) ? Mn7 Co1 Mn4 2_455 . 65.811(10) ? Co1 Co1 Mn5 8 . 65.694(6) ? Ge2 Co1 Mn5 2_455 . 65.659(9) ? Co5 Co1 Mn5 2_455 . 171.409(11) ? Ge1 Co1 Mn5 2_455 . 112.691(12) ? Co6 Co1 Mn5 2_455 . 63.679(9) ? Mn1 Co1 Mn5 5_565 . 124.506(11) ? Co1 Co1 Mn5 8_556 . 114.305(6) ? Mn7 Co1 Mn5 2_455 . 120.081(12) ? Mn4 Co1 Mn5 . . 65.484(12) ? Co1 Co1 Mn2 8 5_565 65.842(6) ? Ge2 Co1 Mn2 2_455 5_565 169.331(11) ? Co5 Co1 Mn2 2_455 5_565 66.896(11) ? Ge1 Co1 Mn2 2_455 5_565 64.798(9) ? Co6 Co1 Mn2 2_455 5_565 112.689(13) ? Mn1 Co1 Mn2 5_565 5_565 59.687(12) ? Co1 Co1 Mn2 8_556 5_565 114.160(5) ? Mn7 Co1 Mn2 2_455 5_565 118.741(12) ? Mn4 Co1 Mn2 . 5_565 122.778(11) ? Mn5 Co1 Mn2 . 5_565 116.052(11) ? Co1 Co1 Mn3 8 . 66.002(5) ? Ge2 Co1 Mn3 2_455 . 112.894(11) ? Co5 Co1 Mn3 2_455 . 116.565(13) ? Ge1 Co1 Mn3 2_455 . 64.889(9) ? Co6 Co1 Mn3 2_455 . 63.475(9) ? Mn1 Co1 Mn3 5_565 . 114.054(11) ? Co1 Co1 Mn3 8_556 . 113.999(5) ? Mn7 Co1 Mn3 2_455 . 175.160(9) ? Mn4 Co1 Mn3 . . 117.981(11) ? Mn5 Co1 Mn3 . . 61.207(11) ? Mn2 Co1 Mn3 5_565 . 62.387(11) ? Co6 Co2 Co4 2_455 . 118.573(14) ? Co6 Co2 Co5 2_455 . 120.310(13) ? Co4 Co2 Co5 . . 108.778(11) ? Co6 Co2 Co2 2_455 8_556 59.614(6) ? Co4 Co2 Co2 . 8_556 121.291(6) ? Co5 Co2 Co2 . 8_556 121.096(6) ? Co6 Co2 Co2 2_455 8 120.385(7) ? Co4 Co2 Co2 . 8 58.708(6) ? Co5 Co2 Co2 . 8 58.905(6) ? Co2 Co2 Co2 8_556 8 179.999(17) ? Co6 Co2 Mn1 2_455 6_656 109.476(11) ? Co4 Co2 Mn1 . 6_656 124.958(13) ? Co5 Co2 Mn1 . 6_656 63.309(10) ? Co2 Co2 Mn1 8_556 6_656 63.402(6) ? Co2 Co2 Mn1 8 6_656 116.599(6) ? Co6 Co2 Mn4 2_455 6_656 113.425(11) ? Co4 Co2 Mn4 . 6_656 66.261(9) ? Co5 Co2 Mn4 . 6_656 117.773(12) ? Co2 Co2 Mn4 8_556 6_656 64.343(5) ? Co2 Co2 Mn4 8 6_656 115.657(6) ? Mn1 Co2 Mn4 6_656 6_656 71.342(11) ? Co6 Co2 Mn7 2_455 5_655 176.035(10) ? Co4 Co2 Mn7 . 5_655 63.003(11) ? Co5 Co2 Mn7 . 5_655 61.087(11) ? Co2 Co2 Mn7 8_556 5_655 116.422(6) ? Co2 Co2 Mn7 8 5_655 63.579(5) ? Mn1 Co2 Mn7 6_656 5_655 67.497(10) ? Mn4 Co2 Mn7 6_656 5_655 63.463(9) ? Co6 Co2 Mn6 2_455 6_656 64.713(11) ? Co4 Co2 Mn6 . 6_656 64.499(9) ? Co5 Co2 Mn6 . 6_656 173.252(10) ? Co2 Co2 Mn6 8_556 6_656 64.934(5) ? Co2 Co2 Mn6 8 6_656 115.065(5) ? Mn1 Co2 Mn6 6_656 6_656 120.433(11) ? Mn4 Co2 Mn6 6_656 6_656 60.936(11) ? Mn7 Co2 Mn6 5_655 6_656 114.237(12) ? Co6 Co2 Mn5 2_455 . 64.697(9) ? Co4 Co2 Mn5 . . 111.558(11) ? Co5 Co2 Mn5 . . 65.503(11) ? Co2 Co2 Mn5 8_556 . 115.811(5) ? Co2 Co2 Mn5 8 . 64.189(5) ? Mn1 Co2 Mn5 6_656 . 112.126(12) ? Mn4 Co2 Mn5 6_656 . 176.351(13) ? Mn7 Co2 Mn5 5_655 . 118.556(10) ? Mn6 Co2 Mn5 6_656 . 115.607(12) ? Co6 Co2 Mn3 2_455 . 64.907(9) ? Co4 Co2 Mn3 . . 63.187(12) ? Co5 Co2 Mn3 . . 113.187(11) ? Co2 Co2 Mn3 8_556 . 115.754(5) ? Co2 Co2 Mn3 8 . 64.244(6) ? Mn1 Co2 Mn3 6_656 . 171.499(13) ? Mn4 Co2 Mn3 6_656 . 116.408(12) ? Mn7 Co2 Mn3 5_655 . 118.403(10) ? Mn6 Co2 Mn3 6_656 . 63.933(10) ? Mn5 Co2 Mn3 . . 60.058(10) ? Co6 Co2 Mn2 2_455 6_656 63.112(12) ? Co4 Co2 Mn2 . 6_656 173.281(9) ? Co5 Co2 Mn2 . 6_656 66.106(9) ? Co2 Co2 Mn2 8_556 6_656 65.378(5) ? Co2 Co2 Mn2 8 6_656 114.623(5) ? Mn1 Co2 Mn2 6_656 6_656 57.534(11) ? Mn4 Co2 Mn2 6_656 6_656 119.653(11) ? Mn7 Co2 Mn2 5_655 6_656 115.791(13) ? Mn6 Co2 Mn2 6_656 6_656 120.545(10) ? Mn5 Co2 Mn2 . 6_656 62.713(9) ? Mn3 Co2 Mn2 . 6_656 114.082(12) ? Co3 Co3 Ge1 8 . 60.422(6) ? Co3 Co3 Ge2 8 2_455 121.656(6) ? Ge1 Co3 Ge2 . 2_455 120.393(12) ? Co3 Co3 Ge3 8 2 121.650(6) ? Ge1 Co3 Ge3 . 2 121.689(12) ? Ge2 Co3 Ge3 2_455 2 105.968(10) ? Co3 Co3 Co4 8 6_666 120.136(6) ? Ge1 Co3 Co4 . 6_666 179.133(12) ? Ge2 Co3 Co4 2_455 6_666 58.786(10) ? Ge3 Co3 Co4 2 6_666 58.730(9) ? Co3 Co3 Co3 8 8_556 180.0 ? Ge1 Co3 Co3 . 8_556 119.578(6) ? Ge2 Co3 Co3 2_455 8_556 58.342(6) ? Ge3 Co3 Co3 2 8_556 58.351(5) ? Co4 Co3 Co3 6_666 8_556 59.863(6) ? Co3 Co3 Mn6 8 . 65.056(6) ? Ge1 Co3 Mn6 . . 117.022(11) ? Ge2 Co3 Mn6 2_455 . 113.562(12) ? Ge3 Co3 Mn6 2 . 66.260(8) ? Co4 Co3 Mn6 6_666 . 63.811(9) ? Co3 Co3 Mn6 8_556 . 114.944(6) ? Co3 Co3 Mn2 8 6_656 117.108(6) ? Ge1 Co3 Mn2 . 6_656 66.094(9) ? Ge2 Co3 Mn2 2_455 6_656 63.359(10) ? Ge3 Co3 Mn2 2 6_656 113.171(10) ? Co4 Co3 Mn2 6_666 6_656 113.070(11) ? Co3 Co3 Mn2 8_556 6_656 62.893(6) ? Mn6 Co3 Mn2 . 6_656 176.772(11) ? Co3 Co3 Mn6 8 5_665 65.326(6) ? Ge1 Co3 Mn6 . 5_665 66.190(11) ? Ge2 Co3 Mn6 2_455 5_665 171.747(11) ? Ge3 Co3 Mn6 2 5_665 65.783(8) ? Co4 Co3 Mn6 6_666 5_665 114.599(13) ? Co3 Co3 Mn6 8_556 5_665 114.676(5) ? Mn6 Co3 Mn6 . 5_665 64.175(13) ? Mn2 Co3 Mn6 6_656 5_665 118.717(12) ? Co3 Co3 Mn5 8 . 65.520(6) ? Ge1 Co3 Mn5 . . 65.905(11) ? Ge2 Co3 Mn5 2_455 . 65.053(9) ? Ge3 Co3 Mn5 2 . 171.003(10) ? Co4 Co3 Mn5 6_666 . 113.606(13) ? Co3 Co3 Mn5 8_556 . 114.479(5) ? Mn6 Co3 Mn5 . . 115.861(11) ? Mn2 Co3 Mn5 6_656 . 64.174(10) ? Mn6 Co3 Mn5 5_665 . 123.198(10) ? Co3 Co3 Mn4 8 . 65.628(6) ? Ge1 Co3 Mn4 . . 116.509(10) ? Ge2 Co3 Mn4 2_455 . 65.581(9) ? Ge3 Co3 Mn4 2 . 113.654(10) ? Co4 Co3 Mn4 6_666 . 63.566(9) ? Co3 Co3 Mn4 8_556 . 114.370(6) ? Mn6 Co3 Mn4 . . 60.834(11) ? Mn2 Co3 Mn4 6_656 . 117.412(12) ? Mn6 Co3 Mn4 5_665 . 117.108(11) ? Mn5 Co3 Mn4 . . 63.012(11) ? Co3 Co3 Mn3 8 2 116.414(6) ? Ge1 Co3 Mn3 . 2 65.309(9) ? Ge2 Co3 Mn3 2_455 2 112.814(11) ? Ge3 Co3 Mn3 2 2 65.291(9) ? Co4 Co3 Mn3 6_666 2 114.601(11) ? Co3 Co3 Mn3 8_556 2 63.588(6) ? Mn6 Co3 Mn3 . 2 119.512(12) ? Mn2 Co3 Mn3 6_656 2 62.132(11) ? Mn6 Co3 Mn3 5_665 2 64.289(10) ? Mn5 Co3 Mn3 . 2 117.743(12) ? Mn4 Co3 Mn3 . 2 177.948(9) ? Co2 Co4 Co2 8 . 62.582(12) ? Co2 Co4 Ge3 8 . 122.431(12) ? Co2 Co4 Ge3 . . 122.432(12) ? Co2 Co4 Ge2 8 5_655 119.978(13) ? Co2 Co4 Ge2 . 5_655 119.977(13) ? Ge3 Co4 Ge2 . 5_655 105.345(12) ? Co2 Co4 Co3 8 6_655 118.553(8) ? Co2 Co4 Co3 . 6_655 178.226(13) ? Ge3 Co4 Co3 . 6_655 58.391(8) ? Ge2 Co4 Co3 5_655 6_655 58.353(10) ? Co2 Co4 Co3 8 3_545 178.226(13) ? Co2 Co4 Co3 . 3_545 118.553(8) ? Ge3 Co4 Co3 . 3_545 58.391(8) ? Ge2 Co4 Co3 5_655 3_545 58.353(10) ? Co3 Co4 Co3 6_655 3_545 60.276(12) ? Co2 Co4 Mn7 8 5_655 65.676(11) ? Co2 Co4 Mn7 . 5_655 65.676(11) ? Ge3 Co4 Mn7 . 5_655 169.945(15) ? Ge2 Co4 Mn7 5_655 5_655 64.599(12) ? Co3 Co4 Mn7 6_655 5_655 113.326(13) ? Co3 Co4 Mn7 3_545 5_655 113.326(13) ? Co2 Co4 Mn3 8 . 66.636(11) ? Co2 Co4 Mn3 . . 66.637(11) ? Ge3 Co4 Mn3 . . 66.522(10) ? Ge2 Co4 Mn3 5_655 . 171.867(16) ? Co3 Co4 Mn3 6_655 . 114.970(13) ? Co3 Co4 Mn3 3_545 . 114.970(13) ? Mn7 Co4 Mn3 5_655 . 123.533(15) ? Co2 Co4 Mn6 8 6_655 65.577(10) ? Co2 Co4 Mn6 . 6_655 119.202(14) ? Ge3 Co4 Mn6 . 6_655 65.617(9) ? Ge2 Co4 Mn6 5_655 6_655 112.101(10) ? Co3 Co4 Mn6 6_655 6_655 62.511(10) ? Co3 Co4 Mn6 3_545 6_655 114.188(14) ? Mn7 Co4 Mn6 5_655 6_655 117.054(9) ? Mn3 Co4 Mn6 . 6_655 65.266(9) ? Co2 Co4 Mn6 8 6_656 119.201(14) ? Co2 Co4 Mn6 . 6_656 65.577(10) ? Ge3 Co4 Mn6 . 6_656 65.617(9) ? Ge2 Co4 Mn6 5_655 6_656 112.101(10) ? Co3 Co4 Mn6 6_655 6_656 114.188(13) ? Co3 Co4 Mn6 3_545 6_656 62.511(10) ? Mn7 Co4 Mn6 5_655 6_656 117.054(9) ? Mn3 Co4 Mn6 . 6_656 65.266(9) ? Mn6 Co4 Mn6 6_655 6_656 120.387(17) ? Co2 Co4 Mn4 8 6_656 116.529(14) ? Co2 Co4 Mn4 . 6_656 63.503(10) ? Ge3 Co4 Mn4 . 6_656 113.442(9) ? Ge2 Co4 Mn4 5_655 6_656 65.489(9) ? Co3 Co4 Mn4 6_655 6_656 114.783(13) ? Co3 Co4 Mn4 3_545 6_656 63.649(10) ? Mn7 Co4 Mn4 5_655 6_656 63.400(9) ? Mn3 Co4 Mn4 . 6_656 116.933(9) ? Mn6 Co4 Mn4 6_655 6_656 177.285(15) ? Mn6 Co4 Mn4 6_656 6_656 60.485(10) ? Co2 Co5 Co2 . 8 62.191(13) ? Co2 Co5 Co1 . 2 117.062(9) ? Co2 Co5 Co1 8 2 178.331(15) ? Co2 Co5 Co1 . 7_665 178.332(15) ? Co2 Co5 Co1 8 7_665 117.063(9) ? Co1 Co5 Co1 2 7_665 63.639(13) ? Co2 Co5 Ge1 . . 118.937(12) ? Co2 Co5 Ge1 8 . 118.937(12) ? Co1 Co5 Ge1 2 . 59.904(9) ? Co1 Co5 Ge1 7_665 . 59.904(9) ? Co2 Co5 Mn7 . . 118.064(13) ? Co2 Co5 Mn7 8 . 118.064(13) ? Co1 Co5 Mn7 2 . 63.591(11) ? Co1 Co5 Mn7 7_665 . 63.591(11) ? Ge1 Co5 Mn7 . . 112.269(15) ? Co2 Co5 Mn7 . 5_655 66.640(10) ? Co2 Co5 Mn7 8 5_655 66.640(10) ? Co1 Co5 Mn7 2 5_655 114.609(13) ? Co1 Co5 Mn7 7_665 5_655 114.609(13) ? Ge1 Co5 Mn7 . 5_655 173.179(16) ? Mn7 Co5 Mn7 . 5_655 60.909(15) ? Co2 Co5 Mn1 . 6_655 119.743(14) ? Co2 Co5 Mn1 8 6_655 63.575(10) ? Co1 Co5 Mn1 2 6_655 117.763(14) ? Co1 Co5 Mn1 7_665 6_655 60.331(10) ? Ge1 Co5 Mn1 . 6_655 108.800(10) ? Mn7 Co5 Mn1 . 6_655 68.911(10) ? Mn7 Co5 Mn1 5_655 6_655 69.483(10) ? Co2 Co5 Mn1 . 6_656 63.574(10) ? Co2 Co5 Mn1 8 6_656 119.743(14) ? Co1 Co5 Mn1 2 6_656 60.331(10) ? Co1 Co5 Mn1 7_665 6_656 117.763(14) ? Ge1 Co5 Mn1 . 6_656 108.800(10) ? Mn7 Co5 Mn1 . 6_656 68.911(10) ? Mn7 Co5 Mn1 5_655 6_656 69.483(10) ? Mn1 Co5 Mn1 6_655 6_656 131.327(19) ? Co2 Co5 Mn5 . . 64.791(11) ? Co2 Co5 Mn5 8 . 64.791(11) ? Co1 Co5 Mn5 2 . 113.564(13) ? Co1 Co5 Mn5 7_665 . 113.564(13) ? Ge1 Co5 Mn5 . . 64.232(12) ? Mn7 Co5 Mn5 . . 176.502(16) ? Mn7 Co5 Mn5 5_655 . 122.589(16) ? Mn1 Co5 Mn5 6_655 . 111.802(10) ? Mn1 Co5 Mn5 6_656 . 111.802(10) ? Co2 Co5 Mn2 . 6_656 65.012(10) ? Co2 Co5 Mn2 8 6_656 116.346(14) ? Co1 Co5 Mn2 2 6_656 62.162(10) ? Co1 Co5 Mn2 7_665 6_656 114.666(13) ? Ge1 Co5 Mn2 . 6_656 62.846(9) ? Mn7 Co5 Mn2 . 6_656 116.628(9) ? Mn7 Co5 Mn2 5_655 6_656 119.241(9) ? Mn1 Co5 Mn2 6_655 6_656 170.950(14) ? Mn1 Co5 Mn2 6_656 6_656 57.275(10) ? Mn5 Co5 Mn2 . 6_656 62.209(9) ? Co2 Co6 Co2 2 7_665 60.771(13) ? Co2 Co6 Ge2 2 . 121.153(13) ? Co2 Co6 Ge2 7_665 . 121.153(13) ? Co2 Co6 Ge1 2 . 121.118(13) ? Co2 Co6 Ge1 7_665 . 121.118(13) ? Ge2 Co6 Ge1 . . 106.347(14) ? Co2 Co6 Co1 2 7_665 179.649(16) ? Co2 Co6 Co1 7_665 7_665 119.129(8) ? Ge2 Co6 Co1 . 7_665 58.568(10) ? Ge1 Co6 Co1 . 7_665 59.232(9) ? Co2 Co6 Co1 2 2 119.129(8) ? Co2 Co6 Co1 7_665 2 179.649(16) ? Ge2 Co6 Co1 . 2 58.568(10) ? Ge1 Co6 Co1 . 2 59.232(9) ? Co1 Co6 Co1 7_665 2 60.970(12) ? Co2 Co6 Mn2 2 5_665 67.390(11) ? Co2 Co6 Mn2 7_665 5_665 67.390(11) ? Ge2 Co6 Mn2 . 5_665 63.315(11) ? Ge1 Co6 Mn2 . 5_665 169.662(16) ? Co1 Co6 Mn2 7_665 5_665 112.260(13) ? Co1 Co6 Mn2 2 5_665 112.260(13) ? Co2 Co6 Mn6 2 5_665 65.585(11) ? Co2 Co6 Mn6 7_665 5_665 65.585(11) ? Ge2 Co6 Mn6 . 5_665 171.782(16) ? Ge1 Co6 Mn6 . 5_665 65.435(12) ? Co1 Co6 Mn6 7_665 5_665 114.712(13) ? Co1 Co6 Mn6 2 5_665 114.712(13) ? Mn2 Co6 Mn6 5_665 5_665 124.903(15) ? Co2 Co6 Mn5 2 2 65.707(10) ? Co2 Co6 Mn5 7_665 2 117.623(14) ? Ge2 Co6 Mn5 . 2 65.231(9) ? Ge1 Co6 Mn5 . 2 112.512(10) ? Co1 Co6 Mn5 7_665 2 114.191(14) ? Co1 Co6 Mn5 2 2 62.104(10) ? Mn2 Co6 Mn5 5_665 2 64.224(9) ? Mn6 Co6 Mn5 5_665 2 117.008(9) ? Co2 Co6 Mn5 2 2_554 117.623(14) ? Co2 Co6 Mn5 7_665 2_554 65.707(10) ? Ge2 Co6 Mn5 . 2_554 65.231(9) ? Ge1 Co6 Mn5 . 2_554 112.512(10) ? Co1 Co6 Mn5 7_665 2_554 62.104(10) ? Co1 Co6 Mn5 2 2_554 114.191(14) ? Mn2 Co6 Mn5 5_665 2_554 64.224(9) ? Mn6 Co6 Mn5 5_665 2_554 117.008(9) ? Mn5 Co6 Mn5 2 2_554 119.767(17) ? Co2 Co6 Mn3 2 2_554 117.340(14) ? Co2 Co6 Mn3 7_665 2_554 65.657(10) ? Ge2 Co6 Mn3 . 2_554 112.920(10) ? Ge1 Co6 Mn3 . 2_554 65.014(9) ? Co1 Co6 Mn3 7_665 2_554 62.771(10) ? Co1 Co6 Mn3 2 2_554 114.613(14) ? Mn2 Co6 Mn3 5_665 2_554 117.784(9) ? Mn6 Co6 Mn3 5_665 2_554 64.403(9) ? Mn5 Co6 Mn3 2 2_554 176.675(16) ? Mn5 Co6 Mn3 2_554 2_554 60.529(10) ? Co2 Co6 Mn3 2 2 65.657(10) ? Co2 Co6 Mn3 7_665 2 117.340(14) ? Ge2 Co6 Mn3 . 2 112.920(10) ? Ge1 Co6 Mn3 . 2 65.014(9) ? Co1 Co6 Mn3 7_665 2 114.613(14) ? Co1 Co6 Mn3 2 2 62.771(10) ? Mn2 Co6 Mn3 5_665 2 117.784(9) ? Mn6 Co6 Mn3 5_665 2 64.403(9) ? Mn5 Co6 Mn3 2 2 60.529(10) ? Mn5 Co6 Mn3 2_554 2 176.675(16) ? Mn3 Co6 Mn3 2_554 2 118.958(17) ? Co3 Ge1 Co3 . 8 59.156(12) ? Co3 Ge1 Co6 . . 118.982(12) ? Co3 Ge1 Co6 8 . 118.983(12) ? Co3 Ge1 Co1 . 7_665 177.501(10) ? Co3 Ge1 Co1 8 7_665 118.691(8) ? Co6 Ge1 Co1 . 7_665 62.922(9) ? Co3 Ge1 Co1 . 2 118.690(8) ? Co3 Ge1 Co1 8 2 177.500(10) ? Co6 Ge1 Co1 . 2 62.922(10) ? Co1 Ge1 Co1 7_665 2 63.430(12) ? Co3 Ge1 Co5 . . 119.905(12) ? Co3 Ge1 Co5 8 . 119.904(12) ? Co6 Ge1 Co5 . . 111.164(13) ? Co1 Ge1 Co5 7_665 . 59.614(10) ? Co1 Ge1 Co5 2 . 59.614(10) ? Co3 Ge1 Mn2 . 6_655 114.197(12) ? Co3 Ge1 Mn2 8 6_655 63.868(10) ? Co6 Ge1 Mn2 . 6_655 115.560(9) ? Co1 Ge1 Mn2 7_665 6_655 63.308(10) ? Co1 Ge1 Mn2 2 6_655 117.153(12) ? Co5 Ge1 Mn2 . 6_655 66.048(8) ? Co3 Ge1 Mn2 . 6_656 63.868(10) ? Co3 Ge1 Mn2 8 6_656 114.196(13) ? Co6 Ge1 Mn2 . 6_656 115.560(9) ? Co1 Ge1 Mn2 7_665 6_656 117.153(12) ? Co1 Ge1 Mn2 2 6_656 63.308(10) ? Co5 Ge1 Mn2 . 6_656 66.048(9) ? Mn2 Ge1 Mn2 6_655 6_656 118.929(16) ? Co3 Ge1 Mn3 . 2 65.413(10) ? Co3 Ge1 Mn3 8 2 115.463(12) ? Co6 Ge1 Mn3 . 2 64.381(8) ? Co1 Ge1 Mn3 7_665 2 117.081(12) ? Co1 Ge1 Mn3 2 2 63.529(10) ? Co5 Ge1 Mn3 . 2 114.688(9) ? Mn2 Ge1 Mn3 6_655 2 179.256(13) ? Mn2 Ge1 Mn3 6_656 2 61.556(10) ? Co3 Ge1 Mn3 . 2_554 115.463(13) ? Co3 Ge1 Mn3 8 2_554 65.414(10) ? Co6 Ge1 Mn3 . 2_554 64.381(9) ? Co1 Ge1 Mn3 7_665 2_554 63.529(10) ? Co1 Ge1 Mn3 2 2_554 117.081(12) ? Co5 Ge1 Mn3 . 2_554 114.688(9) ? Mn2 Ge1 Mn3 6_655 2_554 61.556(10) ? Mn2 Ge1 Mn3 6_656 2_554 179.256(13) ? Mn3 Ge1 Mn3 2 2_554 117.953(16) ? Co3 Ge1 Mn6 . 5_665 64.211(10) ? Co3 Ge1 Mn6 8 5_665 64.212(10) ? Co6 Ge1 Mn6 . 5_665 63.874(12) ? Co1 Ge1 Mn6 7_665 5_665 116.408(12) ? Co1 Ge1 Mn6 2 5_665 116.408(12) ? Co5 Ge1 Mn6 . 5_665 175.038(14) ? Mn2 Ge1 Mn6 6_655 5_665 115.523(8) ? Mn2 Ge1 Mn6 6_656 5_665 115.523(9) ? Mn3 Ge1 Mn6 2 5_665 63.754(8) ? Mn3 Ge1 Mn6 2_554 5_665 63.754(8) ? Co6 Ge2 Co3 . 2 119.262(11) ? Co6 Ge2 Co3 . 7_665 119.262(11) ? Co3 Ge2 Co3 2 7_665 63.317(13) ? Co6 Ge2 Co4 . 5_655 177.355(15) ? Co3 Ge2 Co4 2 5_655 62.862(9) ? Co3 Ge2 Co4 7_665 5_655 62.862(9) ? Co6 Ge2 Co1 . 7_665 63.612(9) ? Co3 Ge2 Co1 2 7_665 177.092(13) ? Co3 Ge2 Co1 7_665 7_665 116.081(9) ? Co4 Ge2 Co1 5_655 7_665 114.252(11) ? Co6 Ge2 Co1 . 2 63.612(9) ? Co3 Ge2 Co1 2 2 116.081(9) ? Co3 Ge2 Co1 7_665 2 177.092(13) ? Co4 Ge2 Co1 5_655 2 114.252(11) ? Co1 Ge2 Co1 7_665 2 64.363(13) ? Co6 Ge2 Mn2 . 5_665 65.009(13) ? Co3 Ge2 Mn2 2 5_665 64.843(11) ? Co3 Ge2 Mn2 7_665 5_665 64.843(10) ? Co4 Ge2 Mn2 5_655 5_665 117.636(14) ? Co1 Ge2 Mn2 7_665 5_665 117.714(12) ? Co1 Ge2 Mn2 2 5_665 117.714(12) ? Co6 Ge2 Mn7 . . 114.484(14) ? Co3 Ge2 Mn7 2 . 115.570(12) ? Co3 Ge2 Mn7 7_665 . 115.570(12) ? Co4 Ge2 Mn7 5_655 . 62.872(12) ? Co1 Ge2 Mn7 7_665 . 61.881(10) ? Co1 Ge2 Mn7 2 . 61.881(10) ? Mn2 Ge2 Mn7 5_665 . 179.493(13) ? Co6 Ge2 Mn5 . 2 64.342(8) ? Co3 Ge2 Mn5 2 2 64.529(9) ? Co3 Ge2 Mn5 7_665 2 118.121(13) ? Co4 Ge2 Mn5 5_655 2 116.436(8) ? Co1 Ge2 Mn5 7_665 2 117.538(12) ? Co1 Ge2 Mn5 2 2 63.105(10) ? Mn2 Ge2 Mn5 5_665 2 64.445(8) ? Mn7 Ge2 Mn5 . 2 115.399(9) ? Co6 Ge2 Mn5 . 2_554 64.342(8) ? Co3 Ge2 Mn5 2 2_554 118.121(12) ? Co3 Ge2 Mn5 7_665 2_554 64.529(9) ? Co4 Ge2 Mn5 5_655 2_554 116.436(9) ? Co1 Ge2 Mn5 7_665 2_554 63.105(10) ? Co1 Ge2 Mn5 2 2_554 117.538(12) ? Mn2 Ge2 Mn5 5_665 2_554 64.445(9) ? Mn7 Ge2 Mn5 . 2_554 115.399(9) ? Mn5 Ge2 Mn5 2 2_554 118.342(15) ? Co6 Ge2 Mn4 . 2_554 114.905(9) ? Co3 Ge2 Mn4 2 2_554 117.402(12) ? Co3 Ge2 Mn4 7_665 2_554 64.375(10) ? Co4 Ge2 Mn4 5_655 2_554 64.201(9) ? Co1 Ge2 Mn4 7_665 2_554 60.469(9) ? Co1 Ge2 Mn4 2 2_554 114.394(13) ? Mn2 Ge2 Mn4 5_665 2_554 117.625(9) ? Mn7 Ge2 Mn4 . 2_554 62.518(9) ? Mn5 Ge2 Mn4 2 2_554 177.498(13) ? Mn5 Ge2 Mn4 2_554 2_554 62.516(10) ? Co6 Ge2 Mn4 . 2 114.905(9) ? Co3 Ge2 Mn4 2 2 64.375(10) ? Co3 Ge2 Mn4 7_665 2 117.402(12) ? Co4 Ge2 Mn4 5_655 2 64.201(8) ? Co1 Ge2 Mn4 7_665 2 114.394(13) ? Co1 Ge2 Mn4 2 2 60.469(9) ? Mn2 Ge2 Mn4 5_665 2 117.625(9) ? Mn7 Ge2 Mn4 . 2 62.518(8) ? Mn5 Ge2 Mn4 2 2 62.516(10) ? Mn5 Ge2 Mn4 2_554 2 177.498(13) ? Mn4 Ge2 Mn4 2_554 2 116.520(15) ? Co3 Ge3 Co3 6_655 2_455 180.000(11) ? Co3 Ge3 Co3 6_655 7_565 116.701(11) ? Co3 Ge3 Co3 2_455 7_565 63.299(11) ? Co3 Ge3 Co3 6_655 3_545 63.299(11) ? Co3 Ge3 Co3 2_455 3_545 116.701(11) ? Co3 Ge3 Co3 7_565 3_545 180.000(11) ? Co3 Ge3 Co4 6_655 . 62.879(8) ? Co3 Ge3 Co4 2_455 . 117.121(8) ? Co3 Ge3 Co4 7_565 . 117.121(8) ? Co3 Ge3 Co4 3_545 . 62.879(8) ? Co3 Ge3 Co4 6_655 5 117.120(8) ? Co3 Ge3 Co4 2_455 5 62.880(8) ? Co3 Ge3 Co4 7_565 5 62.880(8) ? Co3 Ge3 Co4 3_545 5 117.120(8) ? Co4 Ge3 Co4 . 5 180.0 ? Co3 Ge3 Mn6 6_655 2_454 63.733(9) ? Co3 Ge3 Mn6 2_455 2_454 116.267(9) ? Co3 Ge3 Mn6 7_565 2_454 62.997(9) ? Co3 Ge3 Mn6 3_545 2_454 117.003(9) ? Co4 Ge3 Mn6 . 2_454 116.262(7) ? Co4 Ge3 Mn6 5 2_454 63.737(7) ? Co3 Ge3 Mn6 6_655 6_656 116.267(9) ? Co3 Ge3 Mn6 2_455 6_656 63.733(9) ? Co3 Ge3 Mn6 7_565 6_656 117.003(9) ? Co3 Ge3 Mn6 3_545 6_656 62.997(9) ? Co4 Ge3 Mn6 . 6_656 63.738(7) ? Co4 Ge3 Mn6 5 6_656 116.263(7) ? Mn6 Ge3 Mn6 2_454 6_656 180.000(18) ? Co3 Ge3 Mn6 6_655 6_655 62.997(9) ? Co3 Ge3 Mn6 2_455 6_655 117.003(9) ? Co3 Ge3 Mn6 7_565 6_655 63.733(9) ? Co3 Ge3 Mn6 3_545 6_655 116.267(9) ? Co4 Ge3 Mn6 . 6_655 63.738(7) ? Co4 Ge3 Mn6 5 6_655 116.263(7) ? Mn6 Ge3 Mn6 2_454 6_655 62.626(13) ? Mn6 Ge3 Mn6 6_656 6_655 117.374(13) ? Co3 Ge3 Mn6 6_655 2_455 117.003(9) ? Co3 Ge3 Mn6 2_455 2_455 62.997(9) ? Co3 Ge3 Mn6 7_565 2_455 116.267(9) ? Co3 Ge3 Mn6 3_545 2_455 63.733(9) ? Co4 Ge3 Mn6 . 2_455 116.262(7) ? Co4 Ge3 Mn6 5 2_455 63.737(7) ? Mn6 Ge3 Mn6 2_454 2_455 117.374(13) ? Mn6 Ge3 Mn6 6_656 2_455 62.626(13) ? Mn6 Ge3 Mn6 6_655 2_455 180.000(18) ? Co3 Ge3 Mn3 6_655 . 115.316(9) ? Co3 Ge3 Mn3 2_455 . 64.684(9) ? Co3 Ge3 Mn3 7_565 . 64.684(9) ? Co3 Ge3 Mn3 3_545 . 115.316(9) ? Co4 Ge3 Mn3 . . 62.532(10) ? Co4 Ge3 Mn3 5 . 117.469(10) ? Mn6 Ge3 Mn3 2_454 . 116.485(7) ? Mn6 Ge3 Mn3 6_656 . 63.515(7) ? Mn6 Ge3 Mn3 6_655 . 63.515(7) ? Mn6 Ge3 Mn3 2_455 . 116.485(7) ? Co3 Ge3 Mn3 6_655 5 64.683(9) ? Co3 Ge3 Mn3 2_455 5 115.317(9) ? Co3 Ge3 Mn3 7_565 5 115.316(9) ? Co3 Ge3 Mn3 3_545 5 64.684(9) ? Co4 Ge3 Mn3 . 5 117.467(10) ? Co4 Ge3 Mn3 5 5 62.532(10) ? Mn6 Ge3 Mn3 2_454 5 63.516(7) ? Mn6 Ge3 Mn3 6_656 5 116.484(7) ? Mn6 Ge3 Mn3 6_655 5 116.484(7) ? Mn6 Ge3 Mn3 2_455 5 63.516(7) ? Mn3 Ge3 Mn3 . 5 180.0 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Mn1 Mn1 5_565 2.3298(7) ? Mn1 Co1 4_565 2.5646(4) ? Mn1 Co1 5_565 2.5646(4) ? Mn1 Co5 6_666 2.6546(3) ? Mn1 Co5 6_665 2.6546(3) ? Mn1 Co2 3 2.6607(4) ? Mn1 Co2 6_665 2.6607(4) ? Mn1 Mn2 . 2.6621(5) ? Mn1 Mn7 6_665 2.9783(3) ? Mn1 Mn7 6_666 2.9783(3) ? Mn1 Mn7 2_454 3.0117(3) ? Mn1 Mn7 2_455 3.0117(3) ? Mn2 Ge2 5_665 2.7233(4) ? Mn2 Co3 3 2.7577(4) ? Mn2 Co3 6_665 2.7577(4) ? Mn2 Co6 5_665 2.7626(5) ? Mn2 Co1 5_565 2.7728(4) ? Mn2 Co1 4_565 2.7728(4) ? Mn2 Ge1 6_665 2.8082(3) ? Mn2 Ge1 6_666 2.8082(3) ? Mn2 Co2 6_665 2.8593(4) ? Mn2 Co2 3 2.8593(4) ? Mn2 Mn3 5_565 2.8813(5) ? Mn3 Co4 . 2.7461(5) ? Mn3 Co1 . 2.7903(4) ? Mn3 Co1 8 2.7903(4) ? Mn3 Co6 2_455 2.8077(3) ? Mn3 Co6 2_454 2.8077(3) ? Mn3 Ge1 2_454 2.8224(3) ? Mn3 Ge1 2_455 2.8224(3) ? Mn3 Mn5 . 2.8243(5) ? Mn3 Co2 8 2.8247(4) ? Mn3 Co2 . 2.8247(4) ? Mn4 Co1 8 2.6723(4) ? Mn4 Co1 . 2.6723(4) ? Mn4 Co2 3 2.7514(4) ? Mn4 Co2 6_665 2.7514(4) ? Mn4 Co4 6_666 2.8142(3) ? Mn4 Co4 6_665 2.8142(3) ? Mn4 Co3 8 2.8162(4) ? Mn4 Co3 . 2.8163(4) ? Mn4 Mn6 . 2.8215(5) ? Mn4 Ge2 2_454 2.8441(3) ? Mn5 Co1 8 2.7571(4) ? Mn5 Co1 . 2.7571(4) ? Mn5 Co6 2_454 2.7962(3) ? Mn5 Co6 2_455 2.7962(3) ? Mn5 Co3 8 2.8046(4) ? Mn5 Co3 . 2.8046(4) ? Mn5 Ge2 2_455 2.8167(3) ? Mn5 Ge2 2_454 2.8167(3) ? Mn5 Co2 8 2.8190(4) ? Mn5 Co2 . 2.8190(4) ? Mn6 Co3 8 2.7556(4) ? Mn6 Co3 . 2.7556(4) ? Mn6 Co3 4_665 2.7837(4) ? Mn6 Co3 5_665 2.7837(4) ? Mn6 Co4 6_665 2.7875(3) ? Mn6 Co4 6_666 2.7875(3) ? Mn6 Co6 5_665 2.7922(5) ? Mn6 Co2 6_665 2.8120(4) ? Mn6 Co2 3 2.8120(4) ? Mn6 Ge1 5_665 2.8284(5) ? Mn7 Co5 . 2.6091(5) ? Mn7 Co5 5_655 2.6301(5) ? Mn7 Mn7 5_655 2.6556(7) ? Mn7 Co1 2 2.6618(4) ? Mn7 Co1 7_665 2.6618(4) ? Mn7 Co4 5_655 2.6973(5) ? Mn7 Ge2 . 2.7377(4) ? Mn7 Co2 5_655 2.7584(4) ? Mn7 Co2 4_655 2.7584(4) ? Co1 Co1 8 2.2697(4) ? Co1 Ge2 2_455 2.4105(3) ? Co1 Co5 2_455 2.4350(3) ? Co1 Ge1 2_455 2.4422(3) ? Co1 Co6 2_455 2.5307(3) ? Co1 Co1 8_556 2.5677(4) ? Co2 Co6 2_455 2.3552(3) ? Co2 Co4 . 2.3632(3) ? Co2 Co5 . 2.3765(3) ? Co2 Co2 8_556 2.3826(4) ? Co2 Co2 8 2.4548(4) ? Co3 Co3 8 2.3242(4) ? Co3 Ge1 . 2.3543(3) ? Co3 Ge2 2_455 2.3942(3) ? Co3 Ge3 2 2.3948(2) ? Co3 Co4 6_666 2.5028(3) ? Co3 Co3 8_556 2.5132(4) ? Co4 Ge3 . 2.4035(4) ? Co4 Ge2 5_655 2.4053(4) ? Co5 Ge1 . 2.4564(4) ? Co6 Ge2 . 2.3911(4) ? Co6 Ge1 . 2.4063(4) ? _cod_database_fobs_code 2022341