#------------------------------------------------------------------------------ #$Date: 2021-04-10 07:45:59 +0300 (Sat, 10 Apr 2021) $ #$Revision: 264028 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/23/2022350.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022350 loop_ _publ_author_name 'Linden, Anthony' 'Basu Baul, Tushar S.' _publ_section_title ; Structural diversity among some dialkyltin(IV) benzoate and related derivatives ; _journal_coeditor_code OV3150 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229621003545 _journal_volume 77 _journal_year 2021 _chemical_formula_iupac '[Sn (C4 H9)2 (C14 H11 N2 O3)2], 0.5C6 H12' _chemical_formula_moiety 'C36 H40 N4 O6 Sn, 0.5(C6 H12)' _chemical_formula_sum 'C39 H46 N4 O6 Sn' _chemical_formula_weight 785.49 _chemical_name_systematic ; Dibutylbis{(E)-2-hydroxy-5-[(3-methylphenyl)diazenyl]benzoato}tin(IV) cyclohexane hemisolvate ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 90 _cell_angle_beta 93.3046(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.40280(10) _cell_length_b 25.1718(2) _cell_length_c 15.50080(10) _cell_measurement_reflns_used 84811 _cell_measurement_temperature 160(2) _cell_measurement_theta_max 30.0 _cell_measurement_theta_min 2.0 _cell_volume 3662.71(5) _computing_cell_refinement ; DENZO-SMN (Otwinowski & Minor, 1997) ; _computing_data_collection ; COLLECT (Nonius, 2000) ; _computing_data_reduction ; DENZO-SMN and SCALEPACK (Otwinowski & Minor, 1997) ; _computing_molecular_graphics ; ORTEPII (Johnson, 1976) ; _computing_publication_material ; SHELXL2018 (Sheldrick, 2015), Mercury (Macrae et al., 2020) and PLATON (Spek, 2020) ; _computing_structure_refinement ; SHELXL2018 (Sheldrick, 2015) ; _computing_structure_solution ; SIR92 (Altomare et al., 1994) ; _diffrn_ambient_temperature 160(2) _diffrn_detector '65 mm CCD camera on \k goniostat' _diffrn_detector_area_resol_mean 9 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Nonius KappaCCD area detector' _diffrn_measurement_method '\f and \w scans with \k offsets' _diffrn_radiation_monochromator 'horizontally mounted graphite crystal' _diffrn_radiation_source 'Nonius FR590 sealed tube generator' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0657 _diffrn_reflns_av_unetI/netI 0.0445 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 35 _diffrn_reflns_limit_k_min -35 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 90950 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.029 _diffrn_reflns_theta_min 2.632 _diffrn_standards_decay_% 0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.749 _exptl_absorpt_correction_T_max 0.917 _exptl_absorpt_correction_T_min 0.854 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SORTAV; Blessing, 1995) ; _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.424 _exptl_crystal_description prism _exptl_crystal_F_000 1624 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.899 _refine_diff_density_min -0.630 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 623 _refine_ls_number_reflns 10702 _refine_ls_number_restraints 645 _refine_ls_restrained_S_all 1.032 _refine_ls_R_factor_all 0.0781 _refine_ls_R_factor_gt 0.0398 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0545P)^2^+1.0512P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0944 _refine_ls_wR_factor_ref 0.1101 _reflns_number_gt 7109 _reflns_number_total 10708 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ov3150sup1.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 2022350 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_hkl_file ; -13 0 1 3.46 7.48 -13 0 1 2.60 7.46 -13 0 2 33.81 7.25 -13 0 2 20.65 6.66 -13 0 2 30.05 8.70 13 0 -3 1.93 6.82 -13 0 3 8.69 5.31 -13 0 3 3.01 4.57 -13 0 4 29.75 8.13 13 0 -4 17.61 7.84 13 0 -5 2.27 7.15 -13 0 5 -0.78 5.12 -13 1 1 1.01 4.14 -13 -1 1 -0.11 6.25 13 -1 -1 2.14 4.95 13 -1 -1 1.48 6.83 -13 -1 1 5.31 7.68 -13 1 1 -5.43 6.90 -13 1 1 5.07 7.20 -13 1 2 -4.13 7.26 -13 -1 2 -2.68 4.79 13 1 -2 0.34 4.10 -13 1 2 -6.67 7.12 -13 1 2 0.23 5.08 -13 -1 2 -8.13 6.77 -13 1 3 0.45 5.20 -13 -1 3 0.78 7.80 13 1 -3 6.60 6.37 -13 1 3 1.12 5.13 -13 1 4 -0.45 6.25 -13 -1 4 12.47 6.01 13 1 -4 0.57 6.93 13 -1 -4 -4.09 8.07 -13 -1 5 19.91 8.34 -13 1 5 12.93 5.91 13 -1 -5 5.11 6.92 13 1 -5 6.47 7.94 -13 1 5 16.82 7.24 -13 2 1 -1.91 6.86 -13 2 1 15.16 8.26 13 2 -1 0.68 7.06 13 -2 -1 9.67 6.03 -13 2 1 7.39 7.16 13 -2 -1 15.53 6.64 -13 -2 1 12.92 4.46 13 -2 -2 12.97 7.10 13 2 -2 -3.76 4.78 -13 -2 2 11.02 7.35 -13 2 2 3.49 5.19 -13 2 2 8.28 5.70 -13 2 2 9.95 7.69 -13 -2 2 2.93 7.22 -13 -2 3 6.34 5.90 -13 2 3 2.26 4.86 -13 2 3 8.48 7.91 -13 2 3 10.84 7.71 13 2 -3 7.96 5.00 -13 2 4 -3.57 5.14 13 2 -4 0.34 6.59 -13 2 5 3.57 7.25 -13 -2 5 4.11 5.56 13 -2 -5 11.47 8.17 13 2 -5 -2.95 6.69 -13 2 5 8.25 6.36 -13 3 1 -6.79 7.81 13 -3 -1 5.57 5.46 -13 -3 1 10.46 7.12 -13 3 1 -1.01 7.40 13 3 -1 -1.71 4.79 -13 3 1 0.34 5.96 -13 -3 2 2.22 4.56 -13 3 2 4.19 5.20 13 -3 -2 -1.36 4.55 13 -3 -2 8.11 5.30 -13 3 2 3.36 5.26 -13 3 2 1.13 4.85 13 3 -2 3.07 4.55 -13 3 3 1.24 7.24 -13 3 3 -0.23 4.52 13 3 -3 -6.60 5.57 -13 3 3 -7.27 6.26 -13 3 4 13.41 5.92 13 3 -4 5.68 8.29 -13 3 4 4.18 5.65 -13 -4 1 10.03 8.23 -13 4 1 -3.60 5.06 13 -4 -1 3.18 5.91 13 4 -1 4.33 4.90 -13 4 1 5.95 5.05 -13 -4 1 12.45 7.45 -13 4 1 5.32 7.70 13 -4 -2 21.94 6.48 -13 4 2 21.85 8.67 13 4 -2 8.88 6.61 -13 4 2 17.48 7.62 -13 4 2 9.62 5.43 13 -4 -2 12.50 6.08 -13 -4 2 15.67 7.89 -13 4 3 -3.47 7.28 13 -4 -3 6.02 5.11 -13 -4 3 6.33 5.33 -13 4 3 6.11 7.01 -13 4 3 3.95 5.19 13 4 -3 6.03 5.46 -13 4 4 0.78 5.03 -13 4 4 4.30 6.90 13 4 -4 4.09 8.18 -13 -4 4 8.33 5.00 13 -4 -4 3.64 5.68 -13 5 1 1.68 5.73 -13 5 1 2.26 4.98 13 5 -1 -1.60 4.56 -13 5 1 4.72 6.29 -13 -5 1 1.00 4.56 -13 5 2 2.25 7.43 13 5 -2 7.18 5.92 -13 5 2 -2.92 7.07 -13 -5 2 5.77 4.89 13 -5 -2 -2.73 4.66 -13 5 2 4.30 7.24 -13 -5 3 0.67 6.88 -13 5 3 3.92 4.93 -13 5 3 3.96 6.56 13 5 -3 -3.07 5.00 -13 5 3 -4.74 7.33 13 -5 -3 -0.23 5.79 -13 6 1 -2.47 5.17 -13 6 1 8.09 6.96 13 6 -1 2.05 5.02 -13 -6 1 -5.77 6.22 -13 6 1 2.49 5.10 -13 6 2 26.89 7.20 13 -6 -2 28.36 6.30 13 -6 -2 34.76 8.18 -13 6 2 39.52 9.21 -13 6 2 25.47 7.70 -13 -6 2 8.21 8.21 13 6 -2 18.79 6.61 13 -6 -3 1.25 5.23 13 6 -3 3.87 5.35 -13 -6 3 -1.66 5.10 -13 6 3 0.79 5.72 -13 6 3 -3.38 7.44 12 0 -1 8.46 6.54 -12 0 1 -5.07 3.72 -12 0 1 -7.93 3.96 -12 0 1 -3.24 3.58 12 0 -2 12.77 5.65 12 0 -2 3.87 4.44 -12 0 2 0.45 5.77 -12 0 2 2.60 5.65 -12 0 2 8.04 5.81 12 0 -3 2.61 5.78 -12 0 3 -1.02 4.30 -12 0 3 1.45 4.35 -12 0 4 38.57 7.14 12 0 -4 35.26 6.71 -12 0 5 0.33 5.68 12 0 -5 0.34 5.93 12 0 -5 -0.68 3.74 -12 0 5 -3.01 3.23 12 0 -6 5.67 5.55 12 0 -6 5.38 4.47 -12 0 6 11.24 5.90 -12 0 7 -4.67 4.67 12 0 -7 -0.69 3.45 -12 0 7 -1.22 4.89 12 0 -7 2.15 5.32 12 0 -8 4.41 5.66 -12 0 8 5.79 4.78 -12 0 8 8.89 6.00 12 0 -8 11.40 5.07 -12 0 9 -1.11 5.56 12 0 -9 -1.36 6.11 -12 0 9 3.11 5.77 12 0 -9 -2.88 4.85 -12 0 10 31.71 7.68 -12 0 10 37.95 8.10 -12 -1 1 12.97 5.19 12 1 -1 16.36 6.66 -12 1 1 12.76 5.71 12 1 -1 13.33 3.99 -12 1 1 9.52 3.97 -12 -1 1 16.19 6.03 -12 -1 1 16.63 4.64 12 -1 -1 17.02 5.75 -12 1 1 23.67 5.18 -12 1 2 3.24 5.14 -12 -1 2 4.24 3.79 -12 1 2 7.46 6.33 12 1 -2 6.60 4.67 -12 -1 2 6.90 6.22 -12 1 2 4.08 5.55 12 1 -2 3.17 4.30 12 -1 -2 3.73 4.07 -12 1 3 2.15 4.30 -12 1 3 9.05 6.37 12 1 -3 -4.08 5.44 -12 -1 3 2.94 4.29 12 1 -3 3.07 3.98 12 -1 -3 4.08 5.67 -12 -1 3 3.12 6.13 12 1 -4 0.00 4.66 -12 -1 4 0.33 3.34 12 -1 -4 2.96 4.55 -12 1 4 3.57 5.58 -12 1 4 1.13 5.43 -12 -1 4 0.00 4.45 12 -1 -4 -0.11 3.52 12 -1 -5 -1.36 3.74 12 1 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2.83 12 2 -2 -0.68 3.87 -12 -2 2 7.35 6.33 -12 2 2 -3.73 5.76 12 -2 -2 -2.84 3.75 -12 2 2 2.61 5.78 12 -2 -2 -2.03 4.18 12 2 -3 22.18 5.35 -12 2 3 36.44 6.11 12 2 -3 29.16 5.90 -12 2 3 25.17 7.83 12 -2 -3 31.93 7.27 -12 -2 3 31.17 6.35 12 -2 -3 30.13 7.14 -12 -2 3 29.46 6.32 -12 -2 3 27.50 6.46 12 2 -4 -1.70 5.11 -12 2 4 -4.36 4.02 12 2 -4 7.63 4.10 -12 -2 4 -2.67 4.56 -12 -2 4 -4.12 4.90 12 -2 -4 3.63 4.54 -12 2 4 1.47 3.51 12 -2 -4 1.59 3.98 -12 -2 5 27.67 6.22 12 2 -5 16.67 7.26 -12 2 5 18.64 5.25 12 -2 -5 17.79 6.04 -12 -2 5 20.68 6.23 12 2 -5 33.12 8.11 -12 2 6 2.45 3.79 -12 -2 6 6.55 5.00 -12 -2 6 -1.44 4.45 12 -2 -6 4.65 5.10 12 2 -6 11.78 6.23 12 2 -6 11.00 6.76 12 -2 -6 4.01 4.01 -12 2 6 3.57 4.46 -12 -2 7 1.55 5.11 12 -2 -7 2.30 4.48 -12 2 7 -6.13 5.57 12 2 -7 7.81 6.20 12 -2 -7 2.83 6.01 12 2 -7 -0.57 6.22 -12 2 8 7.91 6.80 -12 -2 8 3.44 6.33 12 -2 -8 -1.15 4.72 -12 2 8 -6.90 6.12 -12 -2 8 -1.44 5.77 12 2 -8 7.80 5.88 12 2 -8 8.18 6.22 12 -2 -8 5.33 6.12 12 -2 -9 10.73 5.19 -12 2 9 9.03 7.69 12 -2 -9 7.48 7.48 12 2 -9 12.66 6.67 -12 -2 9 9.54 6.88 -12 2 9 12.46 7.12 12 -2 -10 -3.85 5.90 -12 2 10 -3.12 6.80 -12 -2 10 5.21 6.54 -12 2 10 4.22 6.11 -12 -2 10 2.33 5.22 -12 -3 1 4.34 5.35 -12 3 1 6.12 3.74 12 -3 -1 0.00 4.09 -12 3 1 8.31 4.71 -12 3 1 1.46 4.50 12 -3 -1 9.23 4.73 -12 -3 1 2.82 4.40 12 3 -1 13.91 6.39 12 3 -1 4.29 5.87 12 3 -2 10.37 6.27 -12 -3 2 13.13 6.90 -12 -3 2 14.58 4.68 12 -3 -2 6.77 4.51 12 3 -2 13.69 5.09 12 -3 -2 14.89 5.23 -12 3 2 14.00 6.43 -12 3 2 19.17 6.95 -12 3 2 16.66 6.69 -12 -3 2 7.34 5.76 12 -3 -3 -0.57 3.75 -12 3 3 -0.22 4.03 12 3 -3 -12.26 5.56 12 -3 -3 -3.85 5.77 -12 3 3 -2.94 3.74 12 3 -3 -0.91 3.53 -12 -3 3 7.68 5.67 12 3 -4 1.02 3.41 -12 -3 4 5.89 4.56 -12 3 4 3.36 3.80 12 3 -4 2.85 5.12 12 -3 -4 5.56 4.43 12 -3 -4 10.00 4.66 -12 3 4 -0.11 4.07 -12 -3 4 6.45 4.89 -12 -3 5 6.00 5.22 12 -3 -5 3.31 5.59 12 3 -5 -2.86 4.23 12 3 -5 -0.79 6.01 -12 3 5 4.81 6.26 -12 -3 6 21.10 6.33 12 -3 -6 28.60 7.67 12 3 -6 20.71 6.34 12 -3 -6 6.69 4.42 -12 -3 6 25.44 7.22 12 3 -6 27.50 7.79 -12 3 6 23.45 7.26 12 -3 -7 2.16 5.44 -12 3 7 -0.22 4.80 12 -3 -7 1.15 4.13 -12 -3 7 15.32 6.22 12 3 -7 -0.68 5.88 -12 -3 7 3.89 5.00 12 3 -7 1.49 6.66 12 3 -8 10.02 7.14 -12 -3 8 14.21 5.66 -12 3 8 26.08 7.13 -12 3 8 40.61 9.59 12 -3 -8 9.19 7.94 -12 -3 8 23.52 5.88 12 3 -8 13.89 7.00 12 -3 -8 18.76 6.21 12 -3 -9 8.51 6.46 -12 3 9 2.67 6.68 12 -3 -9 1.38 6.92 -12 3 9 -1.56 6.69 -12 -3 9 -0.33 6.77 -12 3 10 -11.15 8.37 12 -3 -10 2.95 6.47 -12 3 10 -0.11 6.12 -12 -3 10 -4.77 5.21 -12 -4 1 -8.24 5.87 12 4 -1 4.56 6.16 -12 -4 1 0.11 5.34 -12 -4 1 0.34 3.73 12 -4 -1 3.29 5.22 -12 4 1 5.28 5.96 -12 4 1 3.63 4.65 -12 4 1 3.49 5.63 12 4 -1 4.29 4.52 12 -4 -1 -1.35 3.49 -12 -4 2 5.23 5.23 -12 -4 2 10.60 5.86 -12 4 2 9.76 6.28 12 -4 -2 23.92 6.77 -12 4 2 12.36 5.67 12 4 -2 16.30 5.93 12 4 -2 13.93 4.98 -12 4 2 12.41 6.20 -12 -4 2 20.72 6.91 12 4 -3 2.38 5.45 -12 -4 3 0.89 3.89 12 -4 -3 7.69 6.11 12 4 -3 -4.78 5.58 -12 4 3 3.25 4.60 -12 4 3 11.56 6.46 12 4 -4 21.69 6.47 12 -4 -4 33.84 6.70 -12 4 4 27.88 7.39 12 4 -4 33.60 7.74 -12 4 4 23.21 5.89 -12 -4 4 42.77 7.11 12 -4 -5 16.75 6.38 -12 4 5 14.14 5.21 -12 4 5 19.35 7.50 12 4 -5 13.15 6.91 -12 -4 5 13.10 4.77 12 4 -5 10.40 5.03 -12 -4 5 14.99 5.33 -12 -4 6 10.77 5.00 12 -4 -6 2.52 5.95 -12 4 6 7.27 6.93 12 4 -6 -7.02 5.54 12 -4 -6 -4.99 4.54 -12 -4 6 3.11 4.33 12 4 -6 1.83 4.58 12 -4 -7 -6.20 6.31 12 -4 -7 1.36 5.56 -12 4 7 -3.46 5.70 -12 -4 7 -1.78 5.55 12 4 -7 -6.32 6.21 -12 -4 7 -1.55 6.22 12 4 -7 1.69 6.21 12 -4 -8 11.62 7.13 -12 -4 8 9.77 5.77 -12 4 8 -6.48 7.48 12 -4 -8 -5.22 6.01 12 4 -8 4.26 6.68 -12 4 8 5.24 5.13 12 4 -8 -9.71 5.64 -12 -4 8 4.33 4.55 12 -4 -9 14.64 7.15 -12 4 9 12.95 7.82 12 -4 -9 8.40 6.47 -12 -4 9 5.44 5.33 -12 -4 9 5.55 4.33 -12 4 9 17.28 5.24 -12 4 10 13.92 7.69 -12 -4 10 18.76 6.99 12 -4 -10 2.16 7.26 -12 4 10 13.73 8.15 -12 -5 1 20.07 6.88 -12 5 1 19.97 5.79 12 -5 -1 30.04 6.41 -12 5 1 17.21 7.87 -12 -5 1 23.62 7.01 -12 -5 1 24.13 5.34 -12 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8.55 4.55 -12 5 9 6.47 5.69 -12 -5 9 7.54 4.77 -12 5 9 7.49 6.15 -12 -6 1 1.44 3.56 12 6 -1 0.90 5.54 12 -6 -1 2.36 5.28 12 -6 -1 4.31 4.65 -12 6 1 2.38 5.33 12 6 -1 2.28 5.59 -12 6 1 7.98 4.61 -12 -6 1 0.00 6.10 -12 6 1 1.69 6.19 -12 -6 1 2.48 4.95 12 6 -2 -1.03 6.16 -12 -6 2 2.44 4.00 12 -6 -2 6.01 4.99 -12 6 2 15.31 6.35 -12 6 2 18.03 6.87 12 -6 -2 10.26 4.17 -12 6 2 3.94 4.72 -12 -6 2 5.66 4.53 12 6 -2 0.79 6.23 12 -6 -3 7.01 5.09 12 6 -3 2.84 4.32 -12 6 3 -1.93 4.87 12 6 -3 7.28 6.15 12 6 -3 4.72 4.94 -12 6 3 -5.84 5.50 12 -6 -3 -4.88 4.43 -12 -6 3 9.77 5.77 12 6 -4 15.33 5.68 12 6 -4 17.32 5.81 12 -6 -4 29.04 7.15 -12 6 4 20.39 6.57 -12 6 4 23.11 7.07 -12 -6 4 19.76 5.55 12 -6 -4 17.94 6.58 -12 -6 5 1.78 5.44 12 6 -5 -4.00 6.52 -12 6 5 2.80 7.29 12 -6 -5 0.79 4.20 -12 6 5 2.38 5.89 12 -6 -5 2.16 7.06 12 6 -5 -7.03 5.21 -12 -6 6 -0.67 4.99 12 -6 -6 4.11 3.89 12 6 -6 8.25 5.77 12 6 -6 18.69 6.99 -12 6 7 -5.71 6.60 12 -6 -7 -7.61 4.77 12 6 -7 -0.11 6.78 12 6 -7 -3.39 5.75 12 -6 -7 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0.34 1.81 9 -7 -4 18.81 3.44 9 7 -4 20.40 4.28 -9 7 4 27.51 4.06 -9 7 4 18.44 3.41 9 7 -4 24.90 4.55 9 7 -4 23.44 3.91 -9 -7 4 21.91 4.45 9 -7 -4 19.15 4.19 -9 -7 4 25.21 3.57 9 -7 -4 17.75 3.64 -9 7 5 25.01 3.98 9 -7 -5 19.39 4.08 -9 -7 5 29.35 5.34 9 7 -5 25.88 4.05 9 7 -5 21.30 3.85 9 -7 -5 30.51 4.03 9 -7 -5 26.81 3.73 -9 -7 5 24.89 3.68 9 7 -5 20.40 3.69 9 7 -6 128.78 9.79 -9 7 6 111.30 8.77 -9 -7 6 113.58 9.45 -9 -7 6 118.77 9.38 9 -7 -6 107.20 9.94 9 7 -6 108.24 7.57 9 7 -6 108.84 7.51 9 -7 -6 119.30 9.99 -9 7 6 107.89 9.19 9 7 -7 28.58 4.39 9 -7 -7 22.95 4.43 9 7 -7 17.81 3.38 -9 7 7 21.00 5.39 9 7 -7 23.03 4.63 -9 -7 7 27.91 4.02 -9 -7 7 26.34 4.67 9 -7 -7 24.54 3.70 -9 -7 8 35.00 5.33 9 7 -8 23.42 4.28 -9 7 8 27.93 5.50 9 7 -8 34.75 4.87 -9 -7 8 30.38 4.91 9 7 -8 30.06 5.18 9 -7 -8 32.67 5.21 9 -7 -8 27.40 4.89 -9 -7 9 0.67 3.13 9 7 -9 4.40 4.75 9 -7 -9 0.93 4.17 9 7 -9 8.33 3.38 -9 -7 9 3.89 3.44 -9 7 9 2.02 3.59 9 -7 -9 4.55 4.32 9 7 -9 4.73 2.48 9 -7 -10 9.72 4.98 9 7 -10 4.73 2.59 9 -7 -10 10.12 4.55 -9 7 10 3.14 3.02 -9 -7 10 2.33 3.33 -9 -7 10 8.15 4.24 -9 7 10 7.39 3.13 9 7 -10 12.85 4.86 9 7 -11 16.09 5.18 9 -7 -11 9.13 5.66 -9 -7 11 17.88 5.11 -9 -7 11 12.06 4.36 9 7 -11 7.52 4.86 9 -7 -11 13.42 3.98 -9 7 11 16.32 3.13 -9 7 11 2.46 4.48 9 7 -12 29.68 7.04 -9 7 12 34.06 6.92 9 7 -12 36.87 5.96 -9 -7 12 42.77 7.15 9 -7 -12 29.06 5.88 -9 7 12 39.72 6.94 9 -7 -12 21.48 6.59 -9 -7 12 39.42 6.89 -9 -7 13 20.65 5.69 9 -7 -13 22.66 6.67 -9 -7 13 14.77 4.66 9 7 -13 16.25 6.45 9 -7 -13 14.20 5.00 9 7 -13 18.29 4.94 -9 7 13 16.29 4.80 -9 7 13 23.04 5.48 9 7 -14 11.31 5.38 -9 -7 14 6.92 4.80 -9 7 14 -0.67 6.58 -9 -7 14 12.21 5.00 -9 7 14 0.00 3.91 9 7 -14 2.99 5.87 9 -7 -14 5.05 4.70 9 -7 -14 10.89 4.88 -9 7 15 6.35 4.79 -9 7 15 -0.22 4.81 -9 -7 15 2.90 5.47 9 -7 -15 4.81 4.69 9 7 -15 -6.60 4.92 9 7 -15 -1.03 6.20 -9 7 16 0.67 4.70 -9 -7 16 6.14 7.36 -9 7 16 1.78 6.90 -9 -7 16 -2.55 4.22 9 7 -16 4.02 6.03 -9 -8 1 57.77 4.68 -9 -8 1 54.04 4.36 9 -8 -1 56.54 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9.81 3.46 8 6 -1 9.46 1.94 8 -6 -2 9.02 2.51 -8 -6 2 11.59 2.12 -8 -6 2 12.92 3.34 8 -6 -2 12.13 1.47 8 -6 -2 14.60 3.19 -8 6 2 16.74 3.30 8 -6 -2 15.15 3.28 -8 6 2 4.52 2.60 8 6 -2 12.81 3.32 -8 -6 2 14.88 3.49 8 -6 -2 13.35 2.24 -8 6 3 24.49 3.19 8 6 -3 27.46 3.99 8 -6 -3 25.33 3.67 -8 -6 3 23.38 3.79 8 -6 -3 23.52 2.26 -8 -6 3 26.08 3.23 8 -6 -3 24.10 3.85 -8 6 3 26.32 4.18 8 -6 -3 25.75 2.04 8 6 -3 30.08 4.13 8 -6 -3 23.49 3.31 -8 6 4 76.04 6.03 8 -6 -4 80.71 5.44 -8 6 4 72.39 4.85 8 6 -4 64.85 6.02 -8 -6 4 73.58 5.02 8 6 -4 62.19 6.80 8 -6 -4 66.64 5.30 8 6 -4 73.91 5.87 8 -6 -4 72.70 6.12 -8 -6 4 77.57 6.23 8 -6 -4 74.09 6.15 -8 6 5 25.22 3.30 8 6 -5 23.90 4.04 8 6 -5 24.10 4.51 8 -6 -5 29.70 4.53 -8 6 5 27.24 4.73 -8 -6 5 26.70 3.89 -8 -6 5 28.32 3.23 8 -6 -5 23.01 2.14 8 -6 -5 26.55 4.04 8 6 -5 26.61 3.74 8 -6 -6 125.59 10.29 -8 -6 6 128.02 8.45 -8 -6 6 132.50 9.48 8 6 -6 151.89 10.02 8 -6 -6 130.62 8.51 8 6 -6 126.98 10.18 8 -6 -6 135.34 7.96 -8 6 6 133.12 7.71 8 6 -6 129.31 8.92 -8 6 6 135.86 8.99 8 6 -7 -0.93 1.97 8 6 -7 0.34 2.48 -8 -6 7 2.90 2.34 -8 -6 7 3.34 2.34 8 6 -7 -0.68 2.48 8 -6 -7 2.04 2.61 8 -6 -7 1.79 1.34 8 -6 -7 -1.62 1.74 -8 6 7 -1.23 2.02 8 6 -8 2.82 2.25 8 -6 -8 0.00 2.77 -8 -6 8 -1.67 2.22 8 6 -8 -0.45 1.58 8 6 -8 4.86 3.47 -8 6 8 2.02 2.47 -8 -6 8 2.34 2.34 8 -6 -9 1.02 2.39 8 6 -9 5.07 2.37 8 -6 -9 -1.04 2.42 -8 -6 9 -1.79 1.79 8 6 -9 0.11 2.93 8 6 -9 3.01 3.24 -8 6 9 4.14 2.35 -8 -6 9 2.78 2.89 -8 6 10 147.04 13.20 8 6 -10 167.67 10.03 8 6 -10 127.85 9.37 -8 -6 10 140.94 11.72 8 6 -10 144.15 9.12 -8 6 10 149.77 11.29 -8 -6 10 173.76 11.90 8 -6 -10 149.78 9.10 8 -6 -10 142.35 10.37 -8 -6 11 23.23 5.00 8 6 -11 18.89 4.95 -8 6 11 25.59 4.47 -8 6 11 7.48 4.02 8 -6 -11 32.28 5.40 8 6 -11 27.92 4.84 8 -6 -11 20.24 4.32 -8 -6 11 28.79 4.80 8 6 -12 50.35 5.62 8 6 -12 48.15 5.17 -8 6 12 40.92 5.80 -8 -6 12 54.69 7.23 -8 -6 12 37.71 6.14 8 -6 -12 62.88 7.90 -8 6 12 42.44 6.14 8 -6 -12 48.17 5.34 8 -6 -13 14.16 5.37 -8 6 13 7.58 4.34 8 6 -13 4.47 4.70 -8 6 13 3.24 4.69 8 6 -13 8.30 4.37 8 -6 -13 6.36 3.86 -8 -6 13 0.78 4.35 -8 -6 13 0.00 5.00 8 -6 -14 5.47 4.10 8 6 -14 7.55 5.72 -8 6 14 -0.56 4.90 8 -6 -14 0.11 4.31 8 6 -14 3.36 3.13 -8 -6 14 4.01 4.01 -8 6 14 5.91 5.02 8 -6 -15 0.34 3.86 -8 6 15 -1.00 4.69 -8 6 15 -1.89 4.00 8 6 -15 3.88 5.48 8 6 -15 0.22 4.47 -8 -6 15 -1.23 3.23 -8 -6 15 -2.67 4.33 -8 -6 16 1.78 6.35 8 6 -16 4.90 4.22 8 -6 -16 -0.57 5.44 8 6 -16 16.06 5.58 -8 -6 16 4.67 4.67 -8 6 16 4.57 6.47 -8 6 16 10.00 6.56 -8 6 17 4.22 5.11 8 -6 -17 5.55 4.19 8 6 -17 -1.71 4.55 -8 -6 17 -0.33 4.12 -8 6 17 0.45 6.36 8 6 -17 0.78 5.35 8 -7 -1 1.37 2.40 8 -7 -1 1.36 1.81 8 -7 -1 -1.25 1.82 -8 7 1 4.19 2.95 -8 7 1 2.73 2.84 -8 -7 1 4.46 2.90 8 7 -1 3.42 2.96 -8 -7 1 3.61 2.14 8 -7 -1 4.21 0.68 8 7 -1 4.12 1.03 -8 -7 1 2.34 1.67 8 -7 -2 33.94 3.29 -8 -7 2 39.28 4.50 -8 -7 2 45.33 4.12 8 -7 -2 49.00 4.11 8 -7 -2 41.86 4.56 -8 7 2 53.55 5.21 -8 7 2 51.82 4.67 -8 -7 2 44.07 4.80 8 -7 -2 43.74 4.41 8 7 -2 48.51 4.58 8 -7 -3 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21.49 4.62 8 7 -9 23.77 4.06 -8 7 9 31.37 5.60 8 7 -9 20.95 3.15 -8 -7 9 25.91 4.45 -8 -7 9 24.59 3.80 8 7 -9 16.66 3.01 -8 7 10 21.38 4.37 -8 -7 10 22.01 4.45 8 7 -10 15.59 5.08 -8 -7 10 23.14 3.47 8 -7 -10 24.46 4.32 -8 7 10 6.94 3.25 8 7 -10 26.69 4.28 8 -7 -10 15.44 4.96 8 7 -10 17.70 3.16 8 -7 -11 -0.34 2.27 -8 7 11 -1.01 4.14 -8 -7 11 4.36 4.25 8 -7 -11 4.25 4.14 8 7 -11 3.60 3.49 8 7 -11 3.46 3.11 -8 7 11 1.23 4.13 -8 -7 11 6.34 3.00 -8 7 12 -0.11 4.02 8 7 -12 6.41 3.37 -8 -7 12 8.05 4.36 -8 -7 12 4.33 3.45 8 -7 -12 5.45 4.09 -8 7 12 1.79 5.02 8 7 -12 -2.88 4.37 8 -7 -12 2.64 2.98 -8 -7 13 13.97 3.80 8 -7 -13 8.63 4.54 -8 -7 13 15.23 3.89 8 7 -13 14.25 4.82 -8 7 13 13.83 4.35 8 7 -13 14.00 4.71 8 -7 -13 21.03 5.71 -8 7 13 13.29 4.69 8 -7 -14 37.18 6.69 -8 7 14 46.90 8.36 8 7 -14 51.63 7.84 -8 -7 14 46.03 6.37 -8 -7 14 36.67 6.33 -8 7 14 39.42 6.81 8 7 -14 44.54 7.44 8 -7 -14 52.32 7.75 8 7 -15 16.80 4.68 -8 -7 15 22.23 6.70 -8 -7 15 30.56 5.45 -8 7 15 19.48 4.45 8 7 -15 24.03 5.37 8 -7 -15 18.08 6.25 -8 7 15 24.11 6.25 8 -7 -15 12.56 4.30 8 7 -16 18.13 7.07 -8 -7 16 8.04 3.68 8 7 -16 11.16 4.24 8 -7 -16 12.03 6.24 -8 7 16 17.35 6.79 -8 7 16 9.26 6.92 8 -7 -17 0.00 4.19 8 7 -17 10.70 7.52 8 7 -17 3.23 4.68 -8 7 17 4.35 6.81 -8 7 17 6.34 5.56 8 -8 -1 0.68 2.16 -8 8 1 -1.13 2.95 -8 -8 1 0.00 1.45 -8 -8 1 1.67 2.01 -8 8 1 0.23 2.39 8 -8 -1 2.29 1.72 8 -8 -1 0.68 0.68 8 8 -1 0.11 1.71 8 -8 -1 0.45 1.92 -8 -8 1 2.48 2.93 -8 8 2 8.65 2.05 8 -8 -2 8.06 1.25 -8 -8 2 10.51 2.35 8 8 -2 9.61 3.09 8 -8 -2 8.79 2.51 8 -8 -2 8.18 1.25 8 -8 -2 9.95 3.16 -8 -8 2 14.03 3.23 -8 8 2 7.14 2.61 8 -8 -2 9.35 2.96 8 -8 -3 105.80 4.87 8 -8 -3 101.01 6.01 -8 -8 3 105.87 7.24 8 -8 -3 89.27 6.61 8 -8 -3 114.34 6.53 -8 8 3 108.40 8.94 -8 8 3 93.68 7.52 -8 -8 3 103.15 7.83 8 -8 -3 108.19 9.05 8 8 -3 91.73 10.22 -8 -8 4 3.47 2.01 -8 8 4 4.86 3.28 8 -8 -4 5.01 2.39 8 -8 -4 5.89 3.29 -8 8 4 4.44 2.28 -8 -8 4 2.78 2.67 8 8 -4 2.14 2.03 8 -8 -4 1.13 1.70 8 8 -4 5.53 3.22 8 8 -4 3.75 2.39 8 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79.04 8.23 8 8 -11 92.81 8.44 -8 8 11 89.06 9.40 -8 -8 11 89.84 7.28 8 -8 -11 76.21 8.42 8 8 -12 -0.69 2.76 8 -8 -12 -1.49 2.64 -8 -8 12 -5.89 4.78 8 8 -12 1.12 2.36 -8 8 12 -4.47 4.47 8 -8 -12 0.57 3.98 -8 -8 12 -1.68 3.70 -8 8 12 -9.05 4.36 -8 -8 13 20.83 4.70 -8 8 13 24.37 5.70 8 -8 -13 34.09 5.95 8 -8 -13 26.68 5.22 8 8 -13 33.33 5.61 8 8 -13 25.50 5.51 -8 8 13 24.22 4.58 8 8 -14 3.32 5.16 8 -8 -14 5.48 4.91 8 -8 -14 1.02 4.31 8 8 -14 0.22 4.59 -8 8 14 4.92 5.03 -8 8 14 8.03 6.13 -8 -8 14 1.46 4.81 8 8 -15 -0.91 5.38 8 -8 -15 13.31 5.92 8 8 -15 -2.12 3.13 -8 -8 15 2.91 4.14 8 -8 -15 -6.79 4.75 -8 8 15 -6.14 3.91 -8 8 15 0.11 5.90 8 -8 -16 -1.14 5.90 -8 8 16 2.46 4.24 8 8 -16 -3.65 3.77 -8 -8 16 -0.56 6.26 -8 8 16 3.01 6.35 8 8 -16 4.58 4.35 -8 8 17 13.84 5.80 8 8 -17 13.71 5.13 8 -8 -17 11.11 5.44 -8 8 17 12.35 6.12 -8 -8 17 18.68 6.26 8 8 -17 12.42 6.61 8 9 -1 45.62 5.93 8 -9 -1 64.72 4.65 8 -9 -1 63.77 3.98 -8 9 1 59.20 5.91 8 -9 -1 66.34 5.26 -8 -9 1 62.56 5.38 8 -9 -1 55.99 7.23 -8 -9 1 70.52 5.46 -8 9 1 61.23 6.24 8 -9 -2 81.22 6.27 -8 -9 2 96.11 7.91 8 -9 -2 90.33 6.62 8 -9 -2 83.55 5.23 8 -9 -2 101.73 7.91 -8 9 2 95.60 6.49 -8 9 2 93.49 6.46 8 9 -2 73.68 7.67 -8 -9 2 93.78 5.95 8 -9 -3 81.16 6.11 8 -9 -3 71.73 5.56 -8 9 3 72.46 6.57 8 -9 -3 77.98 5.59 8 -9 -3 76.04 5.73 8 9 -3 68.77 6.31 -8 -9 3 79.46 6.40 -8 9 3 81.71 6.15 -8 -9 3 70.48 6.68 8 -9 -4 33.14 4.49 8 -9 -4 35.25 3.17 8 9 -4 34.55 3.92 -8 9 4 27.36 3.99 8 9 -4 29.22 3.95 -8 -9 4 37.29 4.56 -8 9 4 31.44 4.18 -8 -9 4 35.81 3.71 8 -9 -4 33.92 3.53 8 -9 -4 42.74 4.87 -8 9 5 0.79 2.71 8 9 -5 3.00 2.19 8 -9 -5 2.38 1.81 -8 -9 5 -3.59 2.13 8 -9 -5 1.27 2.89 -8 -9 5 4.79 2.56 8 9 -5 2.14 2.36 8 9 -5 4.76 2.95 -8 9 5 -0.91 2.16 8 -9 -5 -0.11 2.38 8 -9 -6 40.86 3.74 8 9 -6 41.48 5.06 8 -9 -6 42.03 4.40 8 -9 -6 26.25 3.86 8 9 -6 44.32 4.63 -8 9 6 35.87 5.19 -8 9 6 38.85 4.32 -8 -9 6 37.39 4.01 8 9 -6 35.58 4.29 -8 -9 6 45.04 4.83 8 9 -7 26.24 3.49 8 -9 -7 31.18 4.87 8 9 -7 29.19 3.48 -8 -9 7 35.38 4.67 -8 9 7 22.30 4.17 8 -9 -7 23.21 4.10 8 9 -7 33.61 4.83 -8 -9 7 26.62 3.37 -8 -9 8 82.43 6.56 8 -9 -8 70.58 5.81 8 9 -8 79.95 7.42 8 9 -8 64.67 6.86 8 -9 -8 88.99 7.65 8 9 -8 82.60 6.26 -8 9 8 84.12 8.10 -8 -9 8 67.41 5.73 -8 -9 9 12.69 3.26 8 -9 -9 14.92 4.33 -8 -9 9 15.13 4.78 -8 9 9 13.03 4.60 8 -9 -9 11.46 3.59 8 9 -9 15.97 3.04 8 9 -9 12.48 2.81 8 9 -9 17.60 5.09 8 -9 -10 24.02 5.01 8 9 -10 26.32 4.27 8 9 -10 22.90 5.32 -8 9 10 24.34 5.27 -8 -9 10 21.90 4.61 -8 -9 10 13.68 4.56 8 -9 -10 25.52 3.93 -8 -9 11 14.37 3.59 8 -9 -11 13.99 3.41 8 -9 -11 16.35 3.57 -8 -9 11 10.45 4.34 8 9 -11 22.05 5.20 -8 9 11 18.60 5.15 -8 9 11 16.25 4.71 8 9 -11 20.69 4.84 -8 -9 12 13.36 4.94 8 9 -12 3.80 2.77 8 -9 -12 10.34 4.55 -8 -9 12 17.34 4.56 -8 9 12 8.51 4.25 -8 9 12 12.08 5.26 8 9 -12 10.79 3.71 8 -9 -12 19.18 4.59 -8 9 13 6.03 3.46 -8 -9 13 9.32 3.70 8 -9 -13 3.43 3.66 -8 -9 13 7.33 4.00 8 9 -13 13.13 5.27 8 -9 -13 5.11 5.22 -8 9 13 10.18 4.92 8 9 -13 4.83 5.29 8 9 -14 10.19 4.93 -8 9 14 9.73 4.36 8 -9 -14 13.36 5.25 8 -9 -14 7.60 3.74 -8 9 14 11.05 5.25 -8 -9 14 8.98 5.05 8 9 -14 11.36 5.39 -8 9 15 4.36 4.25 8 -9 -15 14.58 4.56 8 9 -15 10.42 6.07 -8 -9 15 9.87 6.17 8 9 -15 17.45 4.70 -8 9 15 11.93 6.36 8 -9 -15 10.75 4.98 8 9 -16 1.83 6.06 8 9 -16 9.16 4.91 8 -9 -16 -0.57 3.75 -8 9 16 6.24 4.79 -8 9 16 5.47 5.14 -8 -9 16 6.73 5.38 8 9 -17 -3.90 3.79 -8 -9 17 12.66 7.73 -8 9 17 0.45 8.02 8 -9 -17 -2.61 6.81 -8 9 17 4.13 6.14 8 10 -1 4.56 2.96 -8 10 1 5.56 2.49 8 -10 -1 6.68 2.49 8 -10 -1 4.09 1.14 8 -10 -1 3.05 2.37 -8 -10 1 8.91 2.56 -8 -10 1 6.19 1.58 8 -10 -1 3.32 2.06 -8 10 1 0.11 2.27 8 10 -2 18.53 3.89 -8 -10 2 19.93 2.37 8 -10 -2 22.63 2.39 -8 10 2 16.84 2.96 8 -10 -2 19.75 3.54 -8 -10 2 17.49 3.57 8 -10 -2 15.26 3.39 -8 10 2 20.63 4.65 8 -10 -2 13.32 2.39 -8 10 3 -0.34 2.72 -8 10 3 -0.91 2.16 8 -10 -3 -2.17 2.62 8 -10 -3 -5.55 2.94 -8 -10 3 0.67 2.78 -8 -10 3 -1.69 1.69 8 -10 -3 0.23 2.17 8 -10 -3 0.45 1.25 8 10 -3 -0.57 1.95 8 -10 -4 73.29 5.52 -8 10 4 78.55 7.13 -8 10 4 75.61 7.19 8 -10 -4 81.69 7.04 8 -10 -4 80.18 7.15 8 -10 -4 71.02 7.17 8 10 -4 76.47 5.99 -8 -10 4 88.67 5.52 -8 -10 4 71.16 6.68 8 10 -4 98.58 6.54 8 10 -5 52.66 5.18 8 -10 -5 44.89 4.31 -8 -10 5 52.17 5.18 -8 10 5 47.26 5.88 8 -10 -5 51.56 5.22 -8 10 5 48.21 4.67 8 10 -5 51.50 5.54 8 10 -5 52.63 5.45 8 -10 -5 49.45 5.43 -8 -10 5 52.66 5.90 -8 -10 6 115.62 9.13 8 10 -6 105.17 7.12 8 -10 -6 101.42 7.73 8 -10 -6 107.49 5.67 8 -10 -6 103.92 8.46 -8 -10 6 96.40 8.24 -8 10 6 109.07 9.37 8 10 -6 114.85 7.98 -8 10 6 92.65 8.64 8 10 -6 107.04 8.56 8 -10 -7 10.67 3.71 8 -10 -7 13.47 2.83 8 10 -7 11.35 2.90 8 10 -7 11.48 3.04 -8 10 7 4.87 2.26 8 10 -7 9.10 3.82 -8 -10 7 14.02 4.45 8 -10 -7 9.45 3.76 -8 10 7 7.78 3.16 -8 -10 7 4.85 2.25 8 10 -8 13.04 2.81 8 10 -8 13.82 3.71 8 -10 -8 7.86 4.55 -8 10 8 12.16 3.15 -8 -10 8 11.46 4.12 -8 -10 8 13.75 3.94 8 -10 -8 15.66 3.36 8 -10 -8 13.01 2.60 8 10 -8 15.99 4.29 8 10 -9 0.22 2.14 8 -10 -9 2.96 4.33 8 10 -9 -0.90 3.71 -8 -10 9 -2.59 3.15 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6.16 5.38 -8 -14 13 2.17 4.90 8 -14 -13 4.76 5.55 8 -14 -13 5.54 5.31 -8 14 13 9.55 5.95 -8 14 13 8.65 5.84 -8 -14 14 1.59 5.81 -8 14 14 1.46 3.25 -8 14 14 6.73 4.37 8 -14 -14 7.59 4.37 8 14 -14 9.74 6.16 8 -14 -14 3.40 4.19 8 14 -14 -3.11 5.30 8 -14 -14 7.81 4.53 8 14 -15 -1.79 6.37 8 -14 -15 -3.21 4.36 8 14 -15 -3.45 4.94 8 -14 -15 2.04 6.22 8 -14 -15 -2.71 4.18 -8 14 15 -5.04 7.28 -8 -14 15 -1.25 5.92 -8 14 15 -3.47 5.72 -8 15 1 44.66 4.64 8 -15 -1 43.00 4.73 -8 15 1 59.22 6.00 -8 -15 1 46.82 5.92 -8 15 1 43.34 5.52 8 -15 -1 49.93 4.97 8 -15 -1 49.13 4.80 8 15 -1 43.75 5.58 -8 -15 1 53.86 5.70 8 -15 -2 11.03 2.27 -8 15 2 9.07 2.72 8 -15 -2 13.01 2.72 -8 -15 2 15.98 3.35 8 -15 -2 16.30 3.28 -8 15 2 11.33 3.51 8 -15 -2 13.69 4.11 8 15 -2 12.22 3.31 -8 15 3 66.27 6.25 8 -15 -3 82.76 8.28 -8 -15 3 97.83 7.26 8 -15 -3 81.30 6.83 8 15 -3 78.39 7.91 -8 15 3 80.15 8.05 8 -15 -3 69.84 7.29 8 -15 -4 5.16 3.32 8 -15 -4 4.89 2.84 8 15 -4 5.06 3.68 -8 -15 4 4.91 3.13 8 15 -4 1.92 3.27 8 -15 -4 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5.17 -7 -9 17 7.18 4.49 -7 9 17 21.41 4.91 -7 -9 18 12.33 5.72 -7 9 18 7.36 6.69 7 9 -18 0.00 7.01 7 9 -18 1.25 4.54 -7 9 18 4.00 7.11 7 -9 -18 10.59 4.84 7 -10 -1 2.92 0.67 -7 10 1 2.04 1.47 7 -10 -1 4.06 2.82 -7 10 1 0.11 2.50 7 10 -1 5.49 2.63 -7 -10 1 1.34 2.12 7 -10 -1 3.07 2.39 -7 -10 1 2.37 1.13 7 -10 -1 3.53 1.37 7 -10 -1 -1.03 1.83 7 -10 -2 108.12 8.26 7 10 -2 113.08 7.46 7 -10 -2 106.59 6.63 7 -10 -2 104.25 8.23 -7 -10 2 108.77 6.58 7 -10 -2 107.66 7.62 -7 10 2 115.16 7.26 -7 -10 2 118.00 6.20 -7 10 2 111.34 6.70 7 10 -3 71.00 5.18 7 -10 -3 79.34 7.30 7 -10 -3 83.62 6.57 -7 10 3 88.84 5.24 -7 -10 3 79.58 5.98 7 -10 -3 78.20 6.47 -7 10 3 75.54 6.24 -7 -10 3 87.80 5.80 7 -10 -3 82.89 5.86 7 -10 -4 53.91 5.12 7 -10 -4 54.07 4.08 7 10 -4 67.26 5.08 7 10 -4 59.31 5.19 7 -10 -4 54.96 4.27 -7 -10 4 49.80 4.35 -7 10 4 58.07 4.56 -7 -10 4 64.03 4.96 7 -10 -4 55.84 5.45 -7 10 4 58.14 5.44 -7 10 5 45.26 4.10 -7 -10 5 51.07 4.51 7 10 -5 55.37 4.84 -7 -10 5 47.00 4.79 7 -10 -5 45.96 4.52 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6 -4 -4 178.14 8.28 6 -4 -4 163.89 7.47 6 4 -4 155.99 7.93 6 4 -4 165.18 7.68 -6 -4 4 174.91 7.81 -6 4 4 174.51 9.13 -6 -4 4 185.56 8.93 -6 -4 4 159.23 6.74 -6 4 4 160.76 7.95 6 4 -4 161.39 7.85 6 -4 -4 163.22 7.38 6 -4 -4 159.24 8.65 -6 4 5 -0.22 1.35 6 4 -5 2.26 1.69 -6 -4 5 1.34 1.34 6 4 -5 -0.46 1.50 6 4 -5 3.27 1.92 -6 -4 5 3.34 2.12 -6 4 5 -3.05 1.58 6 -4 -5 2.38 1.93 6 -4 -5 3.69 1.84 6 -4 -5 2.94 1.02 -6 -4 5 1.49 0.92 -6 -4 6 2.34 1.56 -6 -4 6 2.79 1.90 6 -4 -6 3.18 1.82 6 -4 -6 6.08 1.35 -6 -4 6 2.99 1.04 6 -4 -6 0.34 2.07 6 4 -6 5.53 2.65 6 4 -6 4.51 1.69 -6 4 6 3.36 1.79 6 4 -6 2.59 1.47 -6 -4 7 148.74 8.14 6 4 -7 141.58 7.93 6 -4 -7 151.25 8.60 -6 4 7 165.32 7.73 6 4 -7 139.87 6.66 6 4 -7 153.67 6.66 -6 -4 7 143.93 8.52 -6 -4 7 145.68 6.81 6 -4 -7 132.45 6.93 6 -4 -7 147.95 6.95 -6 -4 8 106.73 6.13 -6 -4 8 99.25 5.41 6 -4 -8 93.54 6.25 6 -4 -8 104.91 6.26 6 4 -8 105.57 6.19 6 4 -8 109.64 7.23 -6 -4 8 103.52 5.24 6 4 -8 98.49 5.87 -6 4 8 104.93 6.93 6 -4 -8 103.82 6.40 -6 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23.31 5.27 6 9 -18 58.60 8.50 6 9 -18 50.00 8.82 6 9 -18 50.32 8.24 6 -9 -18 49.33 8.18 -6 9 18 53.25 8.65 -6 -9 19 14.02 6.28 6 9 -19 18.24 6.45 -6 9 19 -0.78 7.10 6 10 -1 5.04 2.18 -6 -10 1 1.47 1.01 -6 -10 1 -3.01 1.67 6 -10 -1 0.11 0.80 6 -10 -1 1.60 1.60 6 -10 -1 2.49 1.81 6 -10 -1 0.46 1.48 -6 10 1 1.13 2.16 -6 10 1 2.03 1.58 6 -10 -2 279.87 11.78 6 10 -2 268.21 11.85 -6 -10 2 264.58 11.73 6 -10 -2 255.10 10.80 6 -10 -2 252.03 12.34 -6 -10 2 263.85 12.82 -6 10 2 257.85 11.57 -6 10 2 242.70 11.81 6 -10 -2 245.26 15.12 6 -10 -3 13.04 1.96 6 10 -3 14.88 2.54 6 -10 -3 14.52 2.16 6 -10 -3 9.42 2.84 -6 -10 3 17.92 1.92 -6 -10 3 13.37 2.45 -6 10 3 15.70 2.27 -6 10 3 14.87 2.72 6 -10 -3 11.16 1.94 -6 -10 4 139.09 7.44 6 -10 -4 144.14 8.22 6 -10 -4 132.31 6.59 6 -10 -4 132.54 7.82 6 -10 -4 145.92 8.75 -6 10 4 138.24 7.64 6 10 -4 129.53 7.97 6 10 -4 152.65 8.69 -6 10 4 137.86 7.49 -6 -10 4 145.81 7.02 -6 -10 5 8.35 2.00 6 10 -5 8.55 2.14 6 -10 -5 13.32 3.19 6 -10 -5 6.82 1.90 6 -10 -5 7.81 2.04 6 -10 -5 8.56 2.55 -6 10 5 10.49 1.94 -6 10 5 7.14 2.15 6 10 -5 6.71 1.85 -6 -10 5 8.11 2.03 -6 10 6 17.76 3.51 -6 10 6 19.84 2.04 6 10 -6 16.42 3.01 6 -10 -6 19.02 2.24 6 -10 -6 14.36 2.62 6 10 -6 11.85 2.03 6 10 -6 14.39 2.81 -6 -10 6 21.16 3.01 -6 -10 6 15.33 2.48 6 -10 -6 14.90 3.00 6 -10 -6 20.49 2.83 6 10 -7 1.27 1.73 6 -10 -7 -1.68 1.12 6 10 -7 -1.24 1.91 6 -10 -7 -0.68 1.71 -6 -10 7 5.46 2.78 -6 10 7 2.60 1.92 -6 -10 7 0.90 2.03 6 10 -7 1.13 1.24 6 -10 -7 -3.80 2.53 6 10 -8 223.33 11.07 -6 -10 8 225.23 12.51 6 -10 -8 216.32 9.70 -6 -10 8 208.45 10.03 6 -10 -8 199.38 10.56 6 -10 -8 198.34 8.06 6 10 -8 206.41 13.38 -6 10 8 198.33 13.28 6 10 -8 227.91 10.80 6 10 -9 3.37 2.70 -6 -10 9 3.23 2.34 6 -10 -9 3.95 1.02 6 -10 -9 3.20 2.06 -6 10 9 3.14 2.36 6 10 -9 1.01 1.12 -6 -10 9 4.70 0.92 -6 -10 9 4.51 2.25 6 10 -9 4.49 2.99 6 -10 -9 3.42 2.28 -6 -10 10 192.07 11.97 -6 -10 10 196.87 12.36 -6 10 10 230.77 12.89 6 10 -10 218.52 10.92 6 10 -10 211.17 11.71 -6 -10 10 188.32 13.07 6 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6.22 -6 10 17 -1.89 5.35 -6 -10 17 -1.24 3.82 6 10 -17 0.00 4.15 6 10 -18 10.30 4.87 -6 10 18 -0.67 4.44 -6 -10 18 4.94 4.50 6 -10 -18 -2.69 5.38 6 10 -18 1.67 4.12 6 10 -18 1.68 3.91 -6 -11 1 48.20 2.83 6 11 -1 45.92 3.78 6 -11 -1 40.88 3.19 6 -11 -1 40.32 3.65 -6 11 1 39.40 3.50 6 -11 -1 40.31 3.44 6 -11 -1 38.89 3.84 -6 11 1 44.34 4.54 -6 -11 1 39.44 3.12 -6 11 2 -2.15 1.58 6 -11 -2 1.72 1.84 6 -11 -2 -0.46 2.17 -6 -11 2 1.13 1.13 6 -11 -2 0.80 1.14 6 -11 -2 -1.59 2.27 6 11 -2 3.22 2.07 -6 11 2 0.34 1.25 -6 -11 2 3.56 2.23 6 -11 -3 31.45 3.18 6 -11 -3 36.21 3.97 -6 -11 3 37.54 2.94 -6 11 3 32.27 2.73 -6 11 3 35.43 3.75 6 -11 -3 33.00 3.23 -6 -11 3 30.63 3.79 6 11 -3 27.09 3.00 6 -11 -3 30.64 3.19 -6 -11 4 97.11 5.43 -6 11 4 85.04 6.02 6 -11 -4 98.97 5.90 -6 11 4 91.90 6.61 -6 -11 4 94.89 6.13 6 -11 -4 92.45 6.14 6 11 -4 106.72 6.54 6 11 -4 89.44 6.36 6 -11 -4 88.70 5.23 6 -11 -4 88.34 5.67 -6 11 5 112.39 5.71 6 11 -5 121.50 7.88 -6 11 5 119.55 6.92 6 -11 -5 115.34 5.89 6 -11 -5 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2.48 1.01 6 13 -7 -1.12 2.69 6 -13 -7 -1.50 1.97 -6 -13 7 2.84 1.59 -6 -13 7 1.78 1.78 6 -13 -8 20.18 3.40 6 -13 -8 15.33 2.88 6 13 -8 18.07 3.82 6 -13 -8 11.75 2.85 -6 -13 8 22.04 3.86 -6 13 8 17.06 3.16 6 13 -8 16.49 2.47 6 13 -8 13.98 3.58 6 13 -9 -0.45 2.02 -6 -13 9 1.25 2.61 6 -13 -9 0.00 2.72 6 -13 -9 -0.23 2.05 6 -13 -9 0.92 1.72 -6 13 9 0.34 2.48 6 13 -9 -0.12 1.85 -6 -13 10 20.89 4.20 6 -13 -10 13.84 3.89 6 13 -10 12.55 3.91 6 13 -10 18.30 3.82 -6 13 10 18.99 3.93 6 -13 -10 15.64 3.17 6 -13 -10 12.08 2.74 -6 13 11 10.43 3.48 6 -13 -11 7.51 2.96 6 -13 -11 16.86 4.33 -6 -13 11 13.05 3.86 6 13 -11 15.71 4.49 6 13 -11 10.80 4.02 6 13 -12 117.09 8.82 -6 13 12 92.96 13.98 6 13 -12 121.39 10.66 -6 -13 12 127.32 12.26 6 -13 -12 113.56 9.77 -6 13 12 115.09 10.63 6 -13 -12 121.52 8.53 -6 13 13 5.81 2.57 -6 -13 13 11.00 4.65 -6 13 13 3.57 3.46 6 -13 -13 3.52 3.18 6 13 -13 3.54 4.46 6 -13 -13 10.87 4.53 6 13 -13 9.42 3.14 -6 -13 14 19.05 5.56 6 -13 -14 17.28 4.97 6 -13 -14 13.70 4.98 -6 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2.22 3.55 5 -5 -17 0.56 3.35 5 5 -17 0.45 4.28 5 -5 -17 -3.02 3.13 5 5 -17 1.22 3.78 -5 5 17 -1.01 3.80 -5 -5 18 0.11 3.24 5 -5 -18 3.36 3.92 5 5 -18 -4.23 3.34 5 5 -18 -0.45 5.07 -5 5 18 -1.89 6.10 5 -5 -18 -0.34 3.13 5 5 -19 29.28 7.54 5 5 -19 18.45 5.89 5 -5 -19 22.39 5.71 5 -5 -19 26.16 6.15 -5 5 19 26.18 7.99 -5 5 20 7.65 4.77 5 5 -20 0.68 6.31 5 5 -20 11.89 6.78 5 -6 -1 6.77 1.92 -5 6 1 4.42 1.47 5 -6 -1 6.24 0.91 5 6 -1 6.09 0.69 5 6 -1 4.71 1.38 -5 6 1 5.03 2.06 -5 -6 1 1.47 1.69 -5 -6 1 7.15 1.01 5 6 -1 4.47 1.15 -5 -6 1 5.14 1.34 -5 6 1 5.56 1.36 5 -6 -1 7.58 1.49 5 -6 -1 5.93 0.78 5 -6 -1 4.93 1.61 5 -6 -2 194.90 8.60 -5 6 2 191.30 8.40 5 6 -2 190.75 10.21 -5 6 2 171.38 14.65 5 6 -2 180.37 8.65 -5 -6 2 181.03 8.37 5 -6 -2 189.24 8.42 5 -6 -2 188.44 8.57 -5 6 2 179.65 7.05 5 -6 -2 181.45 7.46 5 -6 -2 186.40 7.30 5 -6 -2 179.33 10.21 -5 -6 2 191.35 7.16 -5 6 3 78.87 4.53 -5 6 3 71.42 5.89 -5 6 3 74.50 3.99 5 -6 -3 77.02 3.38 5 -6 -3 70.31 4.10 -5 -6 3 75.91 3.91 -5 -6 3 85.45 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2.69 -5 -9 9 8.13 2.79 -5 -9 9 7.86 2.47 5 -9 -9 5.63 1.35 5 -9 -10 1.60 2.51 -5 9 10 0.00 1.79 5 -9 -10 1.34 0.78 5 -9 -10 1.68 0.67 5 -9 -10 2.93 1.46 -5 -9 10 2.25 2.70 -5 -9 10 -0.22 1.78 5 9 -10 3.60 2.48 5 9 -10 1.47 1.02 5 9 -10 2.74 2.05 5 -9 -10 -2.26 1.47 -5 -9 10 3.13 1.74 -5 9 11 7.92 2.01 -5 -9 11 4.27 2.47 5 -9 -11 2.48 2.70 5 -9 -11 3.76 2.28 5 -9 -11 3.71 2.03 5 9 -11 2.81 1.80 5 9 -11 3.87 2.28 -5 -9 11 6.26 2.09 -5 -9 12 79.15 6.27 5 -9 -12 83.82 5.63 5 -9 -12 90.56 6.71 -5 -9 12 79.94 7.07 5 -9 -12 82.56 6.63 -5 9 12 90.57 7.58 5 9 -12 75.41 6.82 -5 9 12 80.30 7.24 5 9 -12 86.45 8.20 5 9 -13 15.08 4.20 5 9 -13 15.02 3.14 -5 -9 13 13.81 2.79 5 -9 -13 16.20 2.81 -5 -9 13 14.03 3.26 -5 9 13 10.46 3.00 -5 9 13 17.37 3.56 5 -9 -13 12.79 2.69 5 -9 -13 12.27 3.29 5 -9 -14 70.96 7.94 -5 9 14 81.30 7.46 -5 9 14 101.49 9.45 5 -9 -14 88.29 7.96 5 9 -14 86.42 9.40 -5 -9 14 95.94 7.55 5 -9 -14 80.32 7.09 -5 -9 14 96.31 8.76 5 9 -14 92.85 7.36 5 9 -14 83.54 7.66 -5 9 15 15.15 3.23 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7 2.78 1.78 -5 -10 7 2.41 0.57 5 -10 -7 1.59 0.57 5 -10 -7 0.46 1.37 5 10 -7 2.14 1.12 5 -10 -8 135.96 7.36 5 -10 -8 126.82 7.65 -5 -10 8 135.45 7.46 -5 -10 8 148.31 8.02 5 10 -8 133.49 6.75 5 10 -8 145.27 7.12 5 10 -8 140.90 9.11 -5 10 8 143.70 7.87 5 -10 -8 134.59 7.73 5 -10 -8 134.30 6.91 -5 -10 8 154.42 7.88 5 10 -9 24.84 3.09 5 10 -9 19.80 1.80 -5 10 9 25.00 2.69 -5 -10 9 24.53 3.49 5 -10 -9 22.43 3.85 -5 -10 9 20.61 2.30 5 -10 -9 21.34 2.15 5 -10 -9 19.55 1.33 -5 10 9 16.37 2.00 -5 -10 9 28.40 4.01 5 -10 -9 20.08 3.20 5 10 -9 22.50 3.82 5 10 -10 187.58 9.56 5 -10 -10 171.19 8.14 -5 10 10 184.13 9.95 5 10 -10 167.39 9.14 -5 -10 10 184.99 10.24 -5 -10 10 169.05 9.37 5 -10 -10 182.23 9.26 5 -10 -10 182.35 10.95 5 10 -10 164.67 7.37 -5 -10 11 1.69 2.93 5 -10 -11 0.11 2.82 5 -10 -11 -0.57 2.62 5 10 -11 1.91 2.02 5 10 -11 1.59 1.94 -5 -10 11 1.85 1.74 5 -10 -11 2.82 1.47 -5 10 11 1.45 2.68 -5 10 12 91.91 6.69 -5 10 12 80.33 6.91 5 -10 -12 82.49 8.19 -5 -10 12 98.55 7.88 5 10 -12 87.43 6.82 5 10 -12 83.86 7.64 -5 -10 12 84.66 7.31 5 -10 -12 83.84 6.18 5 -10 -12 90.10 8.24 5 10 -13 -0.91 3.29 5 -10 -13 10.77 3.70 5 10 -13 10.99 3.14 5 -10 -13 8.34 2.82 -5 -10 13 4.87 2.09 -5 10 13 2.11 3.12 -5 10 13 9.02 2.56 5 -10 -13 0.80 3.52 -5 -10 13 8.77 2.81 -5 -10 14 3.02 2.44 5 10 -14 -1.12 2.46 5 -10 -14 -0.67 3.59 5 -10 -14 -1.02 2.61 -5 10 14 -4.45 2.89 -5 -10 14 1.01 2.14 5 10 -14 -1.59 3.06 -5 10 14 -2.56 2.78 5 -10 -14 -1.01 2.25 5 10 -14 -0.45 2.25 5 -10 -15 3.25 2.58 5 10 -15 -1.79 3.24 5 -10 -15 2.71 3.51 -5 10 15 2.00 2.00 -5 -10 15 6.63 4.50 5 10 -15 0.91 3.85 5 10 -15 1.01 2.36 -5 10 15 0.33 4.22 5 10 -16 62.78 7.92 -5 10 16 70.81 7.99 5 10 -16 63.41 7.17 5 -10 -16 58.09 6.83 -5 10 16 49.59 7.24 -5 -10 16 80.73 7.87 5 10 -16 71.34 7.70 -5 10 17 3.44 4.21 5 10 -17 -1.02 3.84 5 10 -17 -6.26 4.36 5 10 -17 6.47 5.35 5 -10 -17 6.04 4.48 -5 -10 17 1.01 4.83 5 10 -18 29.69 7.03 -5 -10 18 37.77 6.63 5 10 -18 18.65 6.78 -5 10 18 29.82 6.65 5 -10 -18 38.16 7.50 5 10 -18 41.31 8.02 -5 10 19 -9.86 5.98 5 10 -19 -1.11 4.23 5 10 -19 -9.49 6.22 5 10 -19 -0.89 5.02 5 -10 -19 -5.04 3.69 -5 11 1 190.42 10.12 5 -11 -1 186.51 9.28 5 -11 -1 181.74 9.23 5 -11 -1 189.59 8.27 5 11 -1 178.89 8.38 5 -11 -1 194.72 8.69 -5 11 1 184.58 8.50 -5 11 1 193.31 7.99 -5 -11 1 190.68 8.68 -5 -11 1 197.15 8.60 5 11 -2 17.97 2.42 -5 11 2 18.84 1.92 5 -11 -2 20.43 3.06 -5 -11 2 21.81 1.81 5 -11 -2 22.30 2.28 5 -11 -2 22.99 2.44 -5 11 2 14.64 2.72 -5 11 2 19.86 2.16 5 -11 -2 21.78 2.07 -5 -11 2 22.25 2.45 5 -11 -2 21.68 2.97 -5 -11 3 67.44 3.73 5 11 -3 65.25 4.27 5 -11 -3 57.43 4.45 -5 11 3 70.33 4.55 5 -11 -3 66.08 4.32 -5 11 3 51.39 5.12 5 -11 -3 71.61 4.05 -5 -11 3 75.75 4.34 -5 11 3 64.34 3.85 5 -11 -3 61.98 4.78 5 -11 -3 72.77 5.00 5 -11 -4 -1.03 2.05 5 11 -4 -0.35 1.27 -5 -11 4 0.79 1.36 5 -11 -4 2.83 1.70 -5 11 4 0.80 1.14 -5 11 4 1.60 2.17 -5 11 4 4.32 2.27 5 11 -4 3.16 2.14 -5 -11 4 2.00 2.00 5 -11 -4 1.27 1.27 5 -11 -4 0.00 1.11 5 -11 -4 2.95 2.04 -5 -11 5 81.28 4.29 -5 -11 5 66.30 4.56 5 -11 -5 72.40 3.78 -5 11 5 71.63 4.88 5 11 -5 70.14 5.43 5 -11 -5 68.85 4.27 5 11 -5 83.64 6.18 -5 11 5 74.71 3.65 5 -11 -5 68.42 4.87 5 -11 -5 71.28 5.59 5 11 -6 56.78 4.50 -5 11 6 50.19 3.85 5 -11 -6 56.38 3.33 -5 -11 6 53.63 4.45 5 11 -6 53.01 4.04 -5 11 6 51.15 3.28 -5 -11 6 63.31 4.40 5 -11 -6 56.39 4.68 5 -11 -6 49.14 3.51 5 -11 -6 54.09 4.02 -5 11 7 150.14 8.70 5 -11 -7 172.18 6.66 5 11 -7 175.79 9.44 -5 -11 7 158.31 8.81 -5 -11 7 165.36 7.90 5 -11 -7 170.44 8.23 5 11 -7 155.35 8.18 -5 -11 7 165.09 6.57 5 -11 -7 142.56 8.83 5 -11 -7 160.77 9.48 5 11 -7 150.92 10.13 5 11 -8 231.14 13.56 5 -11 -8 250.01 11.54 -5 -11 8 255.00 12.84 5 11 -8 248.14 11.02 -5 -11 8 272.02 12.81 5 -11 -8 271.98 12.45 5 11 -8 280.02 11.92 -5 11 8 260.89 12.84 -5 -11 8 267.48 12.87 5 -11 -8 251.32 12.30 5 -11 -8 268.19 10.65 -5 11 9 138.94 7.97 -5 -11 9 130.44 7.00 5 -11 -9 138.67 8.28 5 -11 -9 139.55 7.27 5 11 -9 138.93 7.53 5 11 -9 121.59 6.99 5 11 -9 122.67 7.20 -5 -11 9 132.98 9.59 5 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-11 15 45.19 7.44 5 -11 -15 59.35 6.56 5 11 -15 72.67 6.82 5 11 -16 0.79 2.83 -5 -11 16 -1.46 3.38 -5 11 16 -0.78 4.77 5 11 -16 1.34 3.02 -5 11 16 -1.67 3.56 5 -11 -16 1.68 2.57 5 11 -16 1.12 3.57 -5 11 17 3.33 5.55 5 11 -17 0.45 3.79 5 -11 -17 -2.46 3.02 5 11 -17 3.39 5.43 -5 -11 17 4.62 6.76 5 11 -17 0.22 3.02 -5 11 18 5.54 4.43 5 11 -18 3.01 3.79 5 11 -18 3.01 5.90 5 -11 -18 5.37 4.14 -5 -11 18 8.56 7.55 5 11 -18 2.49 5.65 5 -11 -19 9.40 5.49 5 11 -19 21.29 5.69 5 11 -19 30.87 7.24 -5 11 19 14.96 8.86 5 11 -19 15.91 6.34 5 -12 -1 39.71 3.09 -5 12 1 34.88 3.75 -5 -12 1 38.34 2.27 5 -12 -1 41.71 3.29 5 12 -1 39.79 3.10 5 -12 -1 44.52 3.20 5 -12 -1 32.14 2.51 -5 12 1 39.30 3.28 -5 -12 1 41.25 3.34 -5 12 1 36.20 3.15 -5 -12 2 23.01 1.70 5 -12 -2 20.88 2.28 5 12 -2 23.95 2.42 5 -12 -2 23.14 2.42 -5 12 2 16.81 2.84 5 -12 -2 23.51 3.29 -5 12 2 18.95 2.61 -5 -12 2 24.68 2.67 -5 12 2 18.82 2.25 5 -12 -2 20.15 2.16 -5 12 3 170.67 9.05 5 -12 -3 174.29 9.54 5 -12 -3 175.65 8.76 -5 -12 3 190.00 8.28 5 -12 -3 181.34 9.38 -5 -12 3 181.44 7.90 -5 12 3 146.21 14.46 -5 12 3 173.97 9.55 5 12 -3 192.59 9.70 5 -12 -3 178.54 8.53 5 -12 -3 207.58 8.77 -5 12 4 118.28 6.14 5 12 -4 125.92 6.48 -5 -12 4 133.20 6.79 -5 -12 4 133.28 6.69 5 -12 -4 125.72 7.18 -5 12 4 106.99 6.97 -5 12 4 123.01 6.94 5 -12 -4 126.77 6.02 5 -12 -4 116.42 7.43 5 -12 -4 116.74 6.26 5 -12 -4 115.67 6.35 5 12 -4 125.86 6.20 -5 12 5 125.67 7.39 5 12 -5 112.85 7.52 5 -12 -5 120.73 7.16 5 -12 -5 121.03 8.09 -5 12 5 122.00 6.62 -5 -12 5 128.98 6.90 -5 -12 5 131.19 6.57 5 -12 -5 123.24 6.46 5 -12 -5 132.59 6.39 5 12 -5 135.43 7.20 5 -12 -6 41.42 3.68 5 -12 -6 33.46 4.23 5 -12 -6 38.08 2.66 -5 -12 6 42.43 2.83 -5 -12 6 34.14 3.56 5 12 -6 32.68 3.35 -5 12 6 37.87 2.49 5 12 -6 39.52 3.93 5 -12 -6 42.38 3.63 -5 12 6 37.43 3.06 5 12 -7 2.92 1.24 -5 -12 7 1.67 1.67 5 -12 -7 3.55 2.29 5 12 -7 4.15 2.31 -5 12 7 8.15 2.49 5 -12 -7 3.29 1.59 5 -12 -7 3.10 0.78 5 12 -7 4.38 2.69 -5 -12 7 0.68 1.47 5 -12 -7 5.14 2.74 5 12 -8 43.23 4.38 -5 12 8 51.64 4.29 -5 -12 8 45.11 2.53 5 -12 -8 43.28 3.51 5 -12 -8 41.04 4.33 5 12 -8 32.66 4.03 5 12 -8 41.78 2.70 -5 -12 8 49.09 4.64 5 -12 -8 47.28 4.80 5 -12 -9 3.20 2.17 5 12 -9 6.20 2.52 5 12 -9 3.93 0.90 -5 -12 9 4.30 2.26 5 12 -9 4.83 3.03 -5 12 9 5.96 2.70 -5 -12 9 6.64 1.37 5 -12 -9 4.12 1.14 5 -12 -9 6.81 2.38 -5 12 10 67.65 5.38 5 -12 -10 64.22 6.62 -5 -12 10 70.90 5.51 5 -12 -10 69.76 4.10 5 12 -10 68.66 5.61 5 12 -10 65.49 5.62 -5 -12 10 64.89 5.43 5 -12 -10 71.39 6.00 -5 -12 11 88.23 7.02 5 12 -11 75.58 6.85 5 12 -11 87.81 7.64 -5 12 11 88.46 7.04 -5 -12 11 85.34 8.37 5 -12 -11 85.28 6.88 5 -12 -11 68.24 8.89 5 -12 -11 80.37 6.59 5 -12 -12 29.59 3.29 5 12 -12 29.29 5.05 -5 -12 12 28.83 3.00 -5 12 12 28.98 4.57 5 -12 -12 37.92 4.73 -5 12 12 43.93 6.02 5 -12 -12 28.10 3.98 -5 -12 12 33.56 4.63 5 12 -12 33.95 4.90 5 12 -13 10.01 3.87 -5 -12 13 10.06 3.39 5 -12 -13 12.49 4.20 -5 12 13 9.35 2.67 5 12 -13 9.64 3.81 -5 12 13 6.57 2.89 5 -12 -13 13.59 3.37 5 12 -14 0.45 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13 -7 23.19 3.81 5 13 -7 25.92 3.70 5 -13 -7 22.73 2.97 5 -13 -7 20.41 3.17 -5 13 7 31.83 3.85 -5 -13 7 28.02 3.40 -5 13 8 180.55 8.81 -5 -13 8 175.67 9.87 5 13 -8 178.11 11.11 -5 -13 8 164.70 8.75 5 -13 -8 169.05 8.34 5 -13 -8 152.56 9.82 5 -13 -8 180.93 8.62 5 13 -8 163.94 8.41 5 13 -8 156.68 8.87 -5 -13 9 1.03 1.15 5 -13 -9 5.23 2.73 5 -13 -9 5.25 1.94 -5 -13 9 -4.08 2.49 5 13 -9 2.25 2.36 -5 13 9 0.79 1.69 5 -13 -9 7.94 2.83 5 13 -9 1.49 2.99 5 13 -10 18.52 3.70 5 -13 -10 14.14 3.54 5 -13 -10 12.57 2.72 -5 13 10 14.80 3.25 -5 -13 10 13.97 2.06 5 -13 -10 14.85 2.95 5 13 -10 21.19 3.44 -5 -13 10 17.34 3.06 5 13 -11 0.91 3.20 -5 -13 11 0.45 3.29 -5 -13 11 -0.34 1.38 5 13 -11 -1.23 2.13 5 -13 -11 1.13 2.48 5 -13 -11 -1.94 2.05 -5 13 11 -2.46 2.79 -5 13 12 55.77 7.14 5 -13 -12 64.88 5.86 5 13 -12 57.47 5.70 5 13 -12 71.45 6.62 -5 -13 12 67.18 5.67 5 -13 -12 58.35 5.92 -5 13 12 56.98 6.13 -5 13 13 3.90 2.12 5 13 -13 5.80 3.76 -5 13 13 0.33 2.67 -5 -13 13 2.27 3.51 5 -13 -13 2.04 2.72 5 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14 2 25.98 2.47 5 -14 -2 34.07 2.96 5 -14 -2 31.11 2.64 5 -14 -2 35.03 3.87 -5 14 2 25.74 2.85 -5 14 2 31.64 3.40 -5 -14 2 33.59 2.28 5 -14 -2 30.90 3.76 -5 14 3 79.87 5.80 -5 14 3 80.54 4.29 5 -14 -3 75.57 5.34 5 -14 -3 73.93 6.31 5 -14 -3 79.46 4.90 -5 14 3 62.15 5.14 5 14 -3 80.06 6.12 -5 -14 3 82.90 5.13 5 -14 -3 66.30 4.90 5 -14 -3 80.53 4.63 -5 14 4 90.66 5.58 5 -14 -4 87.40 5.65 5 -14 -4 77.48 5.55 5 -14 -4 84.39 5.57 5 -14 -4 81.41 5.91 -5 14 4 71.79 5.67 5 14 -4 80.36 6.36 5 14 -4 89.33 5.97 -5 -14 4 90.52 5.13 5 -14 -4 85.33 5.25 -5 14 4 63.96 6.07 5 -14 -5 169.05 9.28 5 -14 -5 174.46 7.67 5 14 -5 185.95 9.67 -5 -14 5 162.67 7.75 -5 14 5 165.34 10.04 5 14 -5 168.12 9.14 -5 14 5 168.72 10.24 5 -14 -5 166.74 8.29 5 -14 -5 176.06 9.25 5 -14 -6 29.97 3.97 5 14 -6 25.58 3.82 -5 -14 6 29.70 3.64 -5 14 6 27.62 3.75 5 -14 -6 24.72 2.89 -5 14 6 27.08 2.16 5 14 -6 25.79 3.47 5 -14 -6 29.28 2.12 -5 -14 7 21.16 2.84 5 -14 -7 24.61 3.33 -5 14 7 25.86 3.18 5 -14 -7 23.19 3.54 5 14 -7 21.59 2.66 5 14 -7 25.46 3.14 5 -14 -7 22.46 3.52 5 -14 -8 41.63 3.52 -5 -14 8 43.33 3.53 -5 -14 8 41.71 2.77 5 -14 -8 41.76 4.12 -5 14 8 51.56 4.86 5 14 -8 41.17 4.38 5 14 -8 49.55 4.61 5 14 -8 42.85 2.92 5 -14 -8 34.27 3.54 5 -14 -9 45.26 5.22 5 -14 -9 45.22 4.33 -5 -14 9 52.87 5.23 -5 -14 9 44.44 3.56 5 14 -9 48.69 5.39 5 -14 -9 39.27 5.82 5 14 -9 43.34 4.94 -5 14 9 50.13 4.73 -5 14 10 19.08 3.37 -5 -14 10 12.16 3.30 5 -14 -10 9.64 2.61 5 -14 -10 14.40 3.29 5 -14 -10 19.96 4.22 5 14 -10 13.91 2.69 5 14 -10 7.22 3.90 5 14 -11 127.21 8.70 -5 -14 11 148.06 9.89 5 -14 -11 132.76 10.29 5 -14 -11 132.01 9.42 5 14 -11 155.70 9.32 -5 14 11 130.65 11.41 5 -14 -11 128.94 8.66 -5 -14 12 35.90 4.20 5 14 -12 39.80 5.38 -5 14 12 31.02 4.35 5 14 -12 33.56 4.57 5 -14 -12 36.99 4.85 5 -14 -12 33.21 5.46 -5 14 12 28.33 4.13 5 -14 -12 37.65 5.67 -5 14 13 4.01 4.23 5 14 -13 2.51 4.10 5 -14 -13 1.48 4.09 -5 14 13 4.34 2.45 -5 -14 13 3.29 4.09 5 14 -13 6.05 3.02 5 -14 -13 -1.46 3.04 -5 14 14 -1.56 4.67 -5 -14 14 0.79 4.43 5 -14 -14 -1.24 3.03 5 -14 -14 2.49 3.17 5 14 -14 -5.18 3.94 5 14 -14 -3.53 4.09 -5 14 14 4.78 3.34 5 14 -14 -1.57 2.91 -5 -14 15 8.85 4.99 5 14 -15 10.33 5.22 5 -14 -15 7.80 3.39 5 -14 -15 7.41 3.82 -5 14 15 5.11 5.11 5 14 -15 8.76 3.59 5 14 -15 5.81 4.14 -5 14 15 8.90 3.23 5 -14 -16 13.91 5.72 5 14 -16 14.63 4.47 -5 -14 16 12.82 5.67 5 14 -16 19.83 5.15 5 14 -16 11.80 4.88 -5 14 16 12.43 5.88 5 14 -17 9.75 6.69 -5 -14 17 19.40 5.78 5 14 -17 16.32 4.70 5 14 -17 13.50 6.13 -5 14 17 21.85 6.54 5 -14 -17 22.42 6.39 -5 -14 18 0.91 5.22 5 14 -18 6.81 6.36 5 -14 -18 0.22 3.92 5 14 -18 2.04 5.10 5 14 -18 2.45 7.02 -5 14 18 -1.22 4.43 5 -15 -1 179.49 10.54 5 15 -1 183.87 10.53 -5 15 1 193.00 10.75 5 -15 -1 165.47 9.43 -5 15 1 197.29 7.97 5 15 -1 177.61 7.27 -5 15 1 169.92 11.60 -5 -15 1 202.82 11.95 5 15 -2 2.53 1.49 -5 15 2 3.19 1.94 -5 15 2 4.49 1.69 -5 -15 2 5.70 1.25 5 -15 -2 2.96 1.82 5 -15 -2 4.35 1.37 5 -15 -2 1.37 2.16 5 -15 -2 1.82 1.60 -5 15 2 4.08 2.04 5 -15 -3 39.77 4.20 5 -15 -3 35.10 3.53 -5 15 3 39.19 3.29 -5 15 3 26.65 3.20 -5 15 3 44.28 3.04 5 15 -3 38.51 3.34 5 -15 -3 40.81 3.70 5 -15 -3 39.64 3.42 -5 -15 3 40.16 3.19 5 -15 -3 35.26 3.22 -5 15 4 1.83 2.06 -5 -15 4 3.99 1.71 5 -15 -4 7.20 1.97 -5 15 4 8.04 1.59 -5 15 4 6.60 2.28 5 -15 -4 9.10 2.28 5 -15 -4 8.44 2.74 5 -15 -4 7.02 3.28 5 -15 -4 6.11 1.78 5 15 -4 6.76 2.25 5 15 -4 3.70 1.50 5 -15 -5 56.05 4.43 5 -15 -5 58.19 4.30 5 15 -5 54.71 4.05 -5 15 5 56.12 5.01 5 15 -5 59.02 4.17 -5 15 5 53.82 3.99 5 -15 -5 53.79 5.60 5 -15 -5 59.10 3.91 -5 -15 5 67.45 4.22 5 15 -6 45.21 4.60 -5 -15 6 41.08 3.99 5 15 -6 45.70 4.28 -5 15 6 41.75 4.89 5 -15 -6 41.12 4.20 -5 15 6 41.71 2.39 5 -15 -6 46.66 4.05 5 15 -7 115.09 6.24 5 15 -7 117.84 8.08 -5 15 7 114.90 8.06 -5 -15 7 113.40 6.17 5 -15 -7 116.38 8.29 5 -15 -7 126.32 7.26 5 -15 -7 121.68 7.54 5 -15 -8 11.35 2.64 5 15 -8 8.86 3.14 -5 15 8 5.09 2.49 5 15 -8 10.03 2.65 -5 -15 8 7.87 2.17 5 -15 -8 6.17 2.97 5 15 -8 5.16 1.23 5 -15 -8 10.67 3.18 5 -15 -9 1.13 2.50 5 15 -9 2.88 2.76 5 -15 -9 -0.57 2.28 -5 -15 9 1.94 2.51 5 -15 -9 0.34 1.71 5 15 -9 3.48 3.25 -5 15 9 0.79 2.82 -5 15 10 -1.46 2.92 5 15 -10 2.30 2.18 5 -15 -10 2.16 2.16 5 -15 -10 1.48 2.38 -5 -15 10 1.94 3.08 5 15 -10 -1.35 2.24 5 -15 -10 2.85 3.31 5 15 -11 4.81 2.29 -5 -15 11 1.94 2.28 -5 15 11 4.81 2.02 5 15 -11 1.46 3.48 5 -15 -11 -2.94 2.72 5 -15 -11 6.61 3.64 5 -15 -11 2.95 3.18 5 -15 -12 16.11 3.97 -5 -15 12 17.20 4.56 5 15 -12 6.40 4.00 -5 15 12 18.86 4.13 5 15 -12 16.47 4.71 -5 15 12 21.10 5.36 5 -15 -12 15.58 3.73 5 -15 -12 19.10 3.87 -5 -15 13 80.06 8.54 5 15 -13 73.30 7.18 -5 15 13 62.92 6.35 5 -15 -13 74.25 8.56 5 -15 -13 69.43 7.49 5 -15 -13 65.48 6.70 5 15 -13 67.65 7.95 -5 15 13 65.07 9.03 5 15 -14 13.09 5.48 5 -15 -14 21.17 6.11 5 -15 -14 11.81 3.82 5 -15 -14 13.61 4.76 -5 15 14 8.79 3.89 -5 -15 14 12.98 4.44 5 15 -14 14.22 4.44 5 15 -14 11.02 4.72 -5 15 14 11.46 3.67 5 15 -15 35.66 7.82 5 15 -15 34.90 6.85 5 15 -15 28.40 6.48 -5 -15 15 32.78 5.80 5 -15 -15 25.07 4.88 -5 15 15 39.78 5.33 5 -15 -15 36.39 5.73 5 15 -16 -3.74 3.18 -5 -15 16 2.28 3.64 -5 15 16 2.22 3.88 5 -15 -16 0.34 3.03 5 15 -16 4.91 5.02 5 15 -16 -0.67 3.47 5 -15 -16 2.27 5.78 5 15 -17 1.47 5.90 -5 -15 17 13.99 7.85 5 15 -17 6.47 4.68 5 15 -17 5.59 3.91 -5 15 17 -1.11 6.21 5 -15 -17 12.45 4.60 5 -15 -17 8.73 6.24 5 15 -18 1.81 6.57 5 -15 -18 0.57 4.53 5 15 -18 3.68 6.59 5 15 -18 2.23 4.79 -5 -15 18 3.52 6.71 5 -15 -18 1.46 6.28 5 16 -1 -1.13 0.68 -5 16 1 -1.24 1.47 -5 16 1 1.12 1.23 -5 -16 1 -0.23 0.80 5 -16 -1 1.83 2.40 5 -16 -1 0.56 1.24 5 -16 -1 1.82 2.39 5 16 -1 1.94 2.06 5 -16 -1 -0.68 1.25 -5 16 1 1.37 1.59 5 16 -2 78.51 5.17 -5 16 2 68.94 4.72 -5 16 2 77.19 5.78 5 -16 -2 71.26 5.13 5 -16 -2 77.28 5.92 5 -16 -2 74.00 4.34 -5 16 2 50.85 4.69 -5 -16 2 75.82 5.82 5 -16 -2 89.32 6.27 -5 -16 3 1.71 1.37 -5 16 3 5.29 1.58 5 16 -3 2.19 2.19 5 -16 -3 4.43 2.95 -5 16 3 2.61 1.70 5 -16 -3 5.81 1.37 5 -16 -3 5.24 2.05 5 -16 -3 5.31 1.73 -5 16 3 1.60 1.72 5 -16 -4 112.06 6.93 5 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144.77 8.09 -5 16 10 138.12 8.21 5 16 -10 159.61 11.10 5 -16 -11 14.07 3.40 -5 16 11 10.53 2.69 -5 -16 11 12.69 2.97 5 16 -11 10.20 2.91 5 16 -11 10.54 3.67 5 -16 -11 13.17 3.86 5 -16 -11 11.27 4.33 5 16 -12 38.98 5.72 -5 16 12 49.47 6.37 5 -16 -12 36.76 4.30 5 16 -12 38.20 5.71 5 -16 -12 46.15 6.37 -5 16 12 36.74 4.69 -5 -16 12 50.73 5.37 5 -16 -12 48.70 6.02 5 -16 -13 3.86 4.20 5 16 -13 6.84 3.42 5 16 -13 2.58 4.37 5 -16 -13 3.61 3.61 -5 16 13 6.91 4.01 -5 16 13 3.34 3.34 -5 -16 13 10.39 4.00 5 -16 -13 3.97 3.40 5 16 -14 -4.59 4.59 -5 16 14 3.12 3.34 -5 -16 14 -4.79 4.57 5 -16 -14 1.02 3.06 5 -16 -14 1.69 2.82 5 16 -14 0.34 2.70 5 -16 -14 -1.82 4.31 5 16 -14 0.57 2.85 5 16 -15 2.81 4.94 -5 -16 15 -2.51 4.34 5 16 -15 -0.23 2.96 5 16 -15 3.58 4.14 -5 16 15 6.33 5.11 5 -16 -15 -1.24 3.04 5 -16 -15 -0.34 3.86 5 -16 -16 4.72 5.39 5 16 -16 7.37 4.47 -5 -16 16 28.74 7.07 -5 16 16 5.11 6.22 5 16 -16 14.53 6.47 5 16 -16 14.78 5.26 5 -16 -16 24.84 7.26 5 -16 -17 5.39 5.95 5 -16 -17 -0.23 5.67 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2.05 5 -17 -5 15.76 3.43 5 -17 -5 14.79 2.56 5 17 -5 16.96 3.59 -5 17 5 19.14 3.08 5 -17 -5 12.64 3.19 5 -17 -6 23.73 2.91 5 -17 -6 24.56 4.34 -5 17 6 21.41 3.64 -5 17 6 18.62 1.94 5 17 -6 20.63 4.04 5 17 -6 23.26 3.70 -5 -17 6 24.99 3.21 5 -17 -6 25.03 3.53 -5 -17 7 86.93 7.46 5 -17 -7 82.35 5.83 5 17 -7 65.58 5.78 5 -17 -7 81.22 7.18 -5 17 7 70.87 6.37 5 17 -7 79.34 6.16 5 -17 -7 79.37 6.03 5 17 -8 105.67 7.16 -5 17 8 120.15 7.49 5 17 -8 122.23 8.63 5 -17 -8 104.92 9.13 5 -17 -8 100.48 7.28 -5 -17 8 114.22 8.38 5 -17 -8 109.75 9.11 5 17 -9 2.88 2.54 5 -17 -9 0.80 1.70 -5 17 9 5.77 2.49 5 17 -9 1.01 2.46 5 -17 -9 5.59 3.88 5 -17 -9 0.11 1.61 -5 -17 9 1.61 2.98 5 -17 -10 19.87 3.31 5 17 -10 22.41 4.82 5 17 -10 10.92 2.87 5 -17 -10 15.00 4.09 5 -17 -10 18.24 4.22 -5 -17 10 15.59 4.36 -5 17 10 17.11 4.05 -5 -17 11 1.26 3.32 5 17 -11 2.29 2.64 5 -17 -11 -0.11 3.07 5 -17 -11 0.68 2.61 -5 17 11 -0.78 2.92 5 17 -11 -2.80 3.25 5 -17 -11 -1.02 2.85 5 17 -12 23.29 5.15 -5 17 12 18.43 3.58 5 -17 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37.75 3.42 4 -4 -11 33.82 2.60 -4 -4 12 148.37 9.18 4 4 -12 154.71 10.41 -4 4 12 163.38 8.49 -4 4 12 173.13 9.36 -4 -4 12 160.02 8.82 4 -4 -12 145.98 8.87 4 -4 -12 148.97 8.48 4 -4 -12 167.80 8.49 4 -4 -12 138.41 7.52 4 -4 -12 142.73 9.71 4 4 -12 144.84 9.59 4 4 -13 98.19 8.01 4 4 -13 111.99 7.83 -4 4 13 108.98 7.94 -4 4 13 107.39 7.68 -4 -4 13 103.10 6.81 4 -4 -13 113.98 7.25 4 -4 -13 104.70 5.68 4 -4 -13 97.97 7.96 4 -4 -13 109.68 7.18 4 4 -13 112.41 7.53 4 -4 -14 40.50 4.57 4 4 -14 34.14 4.51 4 4 -14 39.85 4.24 4 4 -14 43.70 4.26 -4 4 14 32.26 4.56 -4 -4 14 23.10 4.13 4 -4 -14 32.52 4.60 4 -4 -14 43.22 4.00 -4 4 14 41.74 4.70 4 4 -15 -0.45 2.59 4 4 -15 -0.67 3.23 -4 4 15 -2.35 2.02 -4 -4 15 1.12 2.57 4 -4 -15 6.95 3.48 4 -4 -15 1.56 2.01 4 4 -15 5.48 2.79 4 4 -16 0.33 3.23 4 4 -16 -0.22 2.01 -4 4 16 2.22 2.89 -4 -4 16 3.24 4.35 4 -4 -16 -5.16 3.59 4 -4 -16 0.78 3.13 4 4 -16 -0.11 2.48 4 -4 -17 11.88 4.71 4 4 -17 12.13 5.34 -4 4 17 10.45 4.22 4 4 -17 12.50 3.72 4 4 -17 14.59 3.79 4 -4 -17 13.73 4.35 4 4 -18 21.52 5.18 4 4 -18 19.80 5.12 -4 4 18 29.11 7.89 -4 -4 18 11.16 4.35 4 -4 -18 14.24 4.37 4 -4 -18 18.20 4.80 4 4 -18 22.03 5.34 4 4 -19 11.38 6.42 4 -4 -19 7.29 5.61 4 4 -19 12.35 5.78 4 -4 -19 13.74 5.70 -4 4 19 4.22 5.56 4 4 -20 19.46 6.00 4 -4 -20 22.45 7.04 4 4 -20 14.31 5.86 -4 4 20 30.67 6.11 4 -4 -20 26.70 6.17 -4 -4 21 1.79 4.69 4 -4 -21 -0.34 6.03 4 4 -21 0.78 5.00 -4 -5 1 1090.87 39.49 -4 5 1 1053.77 41.78 -4 5 1 1048.82 43.62 -4 -5 1 1065.88 55.91 -4 -5 1 1018.51 46.78 4 -5 -1 1022.07 38.79 -4 -5 1 1058.01 39.94 -4 5 1 1119.81 42.10 4 -5 -1 972.33 43.10 -4 5 1 1020.11 39.03 4 5 -1 1095.31 45.16 4 5 -1 1055.01 58.40 4 5 -1 1080.37 45.88 4 5 -1 1011.18 44.03 4 -5 -1 1022.76 41.09 4 -5 -1 1036.43 40.46 4 -5 -1 1043.66 55.70 4 -5 -1 1086.63 40.80 4 -5 -1 1032.59 41.68 -4 5 1 1080.53 47.86 -4 -5 2 73.99 3.47 -4 -5 2 75.05 4.02 4 -5 -2 82.63 4.04 -4 5 2 69.78 4.70 4 5 -2 73.70 3.92 -4 5 2 77.80 4.65 -4 -5 2 76.54 4.10 4 -5 -2 76.71 3.04 4 -5 -2 81.30 3.29 4 5 -2 71.83 4.29 -4 5 2 80.62 3.52 4 5 -2 67.69 5.00 -4 5 2 77.94 4.20 4 5 -2 80.50 3.78 4 -5 -2 77.03 3.85 4 -5 -2 76.21 4.27 4 -5 -2 66.98 3.99 -4 5 3 159.96 12.55 -4 -5 3 181.25 7.48 -4 5 3 184.98 9.64 -4 -5 3 200.28 8.13 -4 -5 3 195.34 8.16 -4 5 3 189.11 8.20 -4 -5 3 52.77 6.51 4 -5 -3 196.56 7.23 4 -5 -3 185.81 8.22 4 -5 -3 181.26 7.83 4 -5 -3 190.66 8.50 4 -5 -3 203.28 8.04 4 5 -3 205.26 10.59 -4 5 3 194.48 8.95 -4 5 4 54.91 3.29 4 -5 -4 60.07 3.98 4 5 -4 61.74 3.38 4 5 -4 56.80 3.90 -4 5 4 54.46 3.85 -4 -5 4 54.87 3.35 4 -5 -4 54.58 3.31 4 -5 -4 54.99 2.94 4 -5 -4 61.53 2.57 -4 -5 4 58.02 2.29 -4 5 4 49.36 3.73 -4 -5 4 51.37 3.49 -4 -5 4 58.35 3.46 -4 5 4 53.07 3.91 -4 5 5 105.75 4.84 4 5 -5 107.17 4.74 -4 -5 5 111.40 4.69 4 -5 -5 107.28 4.78 -4 -5 5 103.13 4.46 4 5 -5 107.95 5.38 -4 -5 5 106.41 5.36 -4 5 5 107.40 5.86 4 -5 -5 108.75 4.80 4 -5 -5 101.55 5.35 -4 5 5 93.71 5.91 -4 -5 5 94.32 6.63 4 -5 -5 108.14 4.42 4 5 -5 122.15 5.41 4 5 -6 30.92 2.03 4 -5 -6 33.92 2.96 -4 -5 6 35.14 2.45 4 -5 -6 33.86 2.60 4 -5 -6 31.32 2.01 -4 5 6 32.99 3.25 4 5 -6 32.15 2.59 -4 5 6 31.78 2.02 4 -5 -6 28.33 2.05 -4 -5 6 31.51 2.68 4 5 -6 27.93 2.74 4 -5 -7 48.67 3.28 4 -5 -7 49.16 3.23 4 -5 -7 52.01 2.74 4 5 -7 55.86 3.72 4 5 -7 49.36 3.30 -4 5 7 47.68 3.47 -4 -5 7 52.44 4.02 -4 -5 7 53.96 3.46 4 5 -7 43.45 2.82 -4 5 7 49.70 3.35 4 -5 -7 51.27 3.42 4 -5 -8 1.46 2.03 -4 -5 8 2.90 1.90 -4 -5 8 -1.90 1.45 4 5 -8 -0.23 1.14 4 5 -8 0.45 1.80 4 -5 -8 1.03 0.80 4 -5 -8 1.14 1.14 4 -5 -8 -1.00 0.78 -4 5 8 0.56 1.23 4 5 -8 0.79 1.02 -4 5 8 2.01 1.79 4 -5 -9 272.48 13.06 4 5 -9 291.55 11.05 4 5 -9 266.28 12.70 -4 5 9 281.29 12.06 4 -5 -9 284.57 13.46 4 5 -9 265.20 12.84 -4 -5 9 287.48 11.28 4 -5 -9 266.11 13.17 4 -5 -9 265.27 11.30 -4 -5 9 287.51 12.18 -4 5 9 282.58 12.50 4 5 -10 7.75 1.14 4 -5 -10 7.59 1.56 -4 -5 10 5.70 1.90 4 -5 -10 6.85 1.91 4 -5 -10 9.79 1.48 -4 5 10 4.24 1.45 -4 5 10 9.03 2.34 4 5 -10 7.98 2.02 -4 -5 10 6.93 2.12 4 5 -10 7.69 2.15 4 -5 -10 6.50 1.94 4 5 -11 209.78 12.01 4 -5 -11 197.09 10.61 -4 5 11 197.88 9.93 -4 5 11 201.05 11.81 -4 -5 11 218.22 9.28 -4 -5 11 200.00 9.94 4 -5 -11 201.25 11.90 4 -5 -11 180.72 10.79 4 -5 -11 220.54 11.75 4 -5 -11 195.62 10.84 4 5 -11 202.06 9.84 4 5 -11 193.29 9.55 -4 5 12 2.23 1.90 4 5 -12 4.85 2.71 -4 5 12 -0.45 1.56 -4 -5 12 2.23 2.68 4 -5 -12 0.45 1.57 4 -5 -12 1.56 1.11 4 -5 -12 -0.68 1.94 4 -5 -12 1.25 1.25 4 -5 -12 2.57 2.01 4 5 -12 -2.91 2.13 4 5 -13 7.78 3.61 4 5 -13 15.55 3.13 4 5 -13 11.47 2.70 -4 5 13 8.49 2.68 -4 -5 13 12.95 2.79 4 -5 -13 6.95 2.58 4 -5 -13 10.05 2.57 4 -5 -13 10.23 2.96 4 -5 -13 11.77 2.00 -4 5 13 5.79 2.23 -4 -5 14 11.05 2.90 4 5 -14 10.49 2.82 4 5 -14 12.29 3.91 4 5 -14 11.43 3.03 -4 5 14 11.41 3.91 4 -5 -14 7.73 3.14 4 -5 -14 6.93 2.01 4 -5 -14 9.77 1.89 -4 5 15 120.92 10.41 4 5 -15 128.06 9.02 4 5 -15 127.28 11.05 -4 -5 15 138.47 9.72 4 -5 -15 137.61 9.98 4 -5 -15 127.37 8.83 4 5 -15 132.14 8.27 -4 5 16 2.47 3.36 4 -5 -16 0.11 3.13 4 5 -16 2.48 4.06 4 5 -16 0.33 2.34 -4 5 16 2.44 3.78 -4 -5 16 2.01 3.13 4 -5 -16 3.92 3.81 4 5 -16 0.67 2.23 4 5 -17 51.22 7.24 4 5 -17 53.13 6.13 -4 5 17 61.10 7.78 4 -5 -17 48.30 7.40 4 -5 -17 50.97 6.04 4 5 -17 56.13 6.88 4 5 -18 -3.61 4.62 4 5 -18 -1.78 4.23 4 5 -18 1.56 3.90 4 -5 -18 1.12 3.36 4 -5 -18 -0.11 4.47 -4 5 18 -0.56 5.00 4 5 -19 -0.78 3.45 4 5 -19 1.35 3.61 -4 5 19 2.67 4.44 -4 -5 19 -1.68 3.46 4 -5 -19 -5.49 5.38 4 -5 -19 5.81 4.14 4 5 -20 13.42 7.67 4 5 -20 17.12 6.89 4 -5 -20 7.40 5.16 4 -5 -20 7.49 5.82 -4 -6 1 299.69 12.07 -4 -6 1 297.44 11.52 -4 6 1 287.14 15.11 -4 6 1 293.50 12.14 -4 6 1 302.48 14.85 -4 -6 1 306.64 12.06 4 -6 -1 301.33 12.76 4 6 -1 298.93 15.15 -4 6 1 282.02 11.18 4 6 -1 282.69 13.83 4 6 -1 296.68 13.43 4 -6 -1 300.17 12.56 4 -6 -1 285.67 11.69 4 -6 -1 289.91 11.87 4 -6 -1 295.69 12.27 -4 -6 1 302.12 14.96 4 -6 -1 287.85 10.73 4 -6 -2 1.58 0.90 4 6 -2 1.62 0.92 4 -6 -2 1.46 1.01 4 -6 -2 2.24 0.34 4 -6 -2 1.71 1.14 4 6 -2 1.83 0.80 4 6 -2 4.05 1.24 -4 6 2 2.27 1.47 -4 6 2 1.93 1.02 -4 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185.94 9.36 4 -6 -6 165.30 6.26 4 -6 -6 155.98 7.41 4 6 -6 179.68 8.11 4 6 -6 164.06 7.45 -4 6 6 168.81 7.76 -4 -6 6 172.36 7.38 4 -6 -7 28.46 2.94 -4 6 7 30.25 2.69 -4 -6 7 31.11 3.12 -4 6 7 28.76 2.23 4 6 -7 28.47 2.62 4 6 -7 35.86 2.93 -4 -6 7 31.97 2.79 4 -6 -7 31.15 2.01 4 -6 -7 29.65 1.82 4 6 -7 30.56 1.92 4 -6 -7 32.73 3.08 4 6 -8 141.63 5.53 4 -6 -8 142.40 6.96 -4 -6 8 141.50 6.93 -4 -6 8 152.95 7.25 4 6 -8 144.09 7.16 4 6 -8 152.67 6.99 -4 6 8 141.55 9.45 -4 6 8 145.07 7.38 4 -6 -8 141.97 6.99 4 -6 -8 142.98 5.81 4 -6 -8 151.01 5.70 4 6 -9 -0.11 2.04 4 -6 -9 1.01 2.02 4 -6 -9 -0.89 1.01 4 6 -9 -2.03 2.03 4 6 -9 0.23 0.79 -4 6 9 1.44 1.33 -4 6 9 0.00 1.67 -4 6 9 2.79 2.01 -4 -6 9 -0.89 1.45 4 -6 -9 0.23 0.91 4 -6 -9 1.37 1.83 -4 -6 9 0.11 2.23 4 6 -10 11.86 1.14 4 6 -10 10.76 2.72 -4 6 10 13.04 2.68 -4 -6 10 14.19 2.91 4 -6 -10 13.03 1.35 4 6 -10 15.07 2.92 -4 6 10 12.93 2.68 -4 -6 10 5.47 2.68 4 -6 -10 14.38 2.47 4 -6 -10 14.26 1.71 4 -6 -10 12.44 2.51 4 -6 -10 17.66 2.24 4 -6 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4.48 3.47 4 6 -17 -0.45 2.56 4 6 -17 10.36 4.23 4 -6 -17 1.79 4.71 4 6 -17 -0.68 2.93 -4 6 17 -1.33 3.22 4 -6 -17 -1.23 3.13 -4 -6 17 -1.90 3.02 4 -6 -18 33.95 6.16 4 6 -18 40.07 6.23 4 -6 -18 40.86 6.16 -4 6 18 23.20 6.77 4 6 -18 33.61 6.34 4 6 -18 37.56 6.09 4 6 -19 6.45 4.89 -4 -6 19 4.70 3.80 4 6 -19 4.74 5.19 4 6 -19 3.56 3.00 4 -6 -19 5.71 3.81 -4 6 19 5.33 4.88 4 -6 -19 -7.85 5.60 4 -6 -20 18.59 5.94 -4 -6 20 24.75 5.73 4 6 -20 15.12 5.56 4 6 -20 18.96 5.42 4 -6 -20 24.89 6.50 -4 6 20 16.99 7.22 4 7 -1 595.71 31.63 -4 7 1 620.07 26.01 4 -7 -1 583.99 21.83 4 7 -1 566.21 27.08 4 7 -1 621.82 24.34 -4 -7 1 622.93 27.27 -4 -7 1 600.04 22.86 -4 -7 1 619.75 22.50 4 -7 -1 592.29 26.50 -4 7 1 598.21 24.12 -4 7 1 622.94 24.62 4 -7 -1 613.06 26.38 4 -7 -1 598.67 22.97 4 -7 -1 588.95 24.31 4 -7 -1 632.66 22.87 -4 7 2 312.67 11.99 4 7 -2 310.51 15.48 -4 -7 2 335.73 13.38 -4 7 2 323.22 13.40 -4 7 2 339.52 14.17 -4 -7 2 333.40 16.97 -4 -7 2 327.34 11.87 4 -7 -2 328.81 13.49 4 -7 -2 291.69 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2.14 4 -11 -5 25.03 2.95 4 11 -6 8.31 2.58 -4 11 6 9.18 1.93 -4 -11 6 8.68 1.69 -4 -11 6 8.86 0.92 4 -11 -6 9.78 2.05 4 -11 -6 7.67 0.78 4 11 -6 7.58 1.61 4 -11 -6 8.60 2.15 -4 11 6 6.99 0.78 -4 11 6 7.41 0.90 4 11 -7 67.50 4.58 4 11 -7 67.57 3.83 -4 11 7 65.80 4.85 -4 -11 7 60.87 3.44 4 -11 -7 78.01 4.42 4 -11 -7 65.98 4.35 4 11 -7 72.55 4.49 -4 -11 7 68.26 3.83 -4 11 7 69.92 3.32 4 11 -8 38.52 3.20 4 11 -8 41.01 3.93 4 11 -8 35.95 1.91 -4 11 8 39.11 3.15 -4 -11 8 37.65 3.21 4 -11 -8 38.44 2.84 4 -11 -8 39.90 4.35 -4 11 8 36.12 2.65 -4 -11 8 46.85 3.72 4 -11 -8 41.53 3.61 4 11 -9 230.95 9.90 -4 -11 9 212.19 10.37 4 -11 -9 215.60 12.25 4 11 -9 219.55 10.95 -4 11 9 200.32 13.05 -4 11 9 226.13 11.65 -4 -11 9 239.60 11.38 4 -11 -9 227.61 11.37 4 -11 -9 220.81 10.98 4 11 -10 43.71 3.98 -4 11 10 37.41 3.32 -4 11 10 49.21 4.13 -4 -11 10 51.00 4.39 4 -11 -10 46.06 4.27 4 -11 -10 45.56 4.23 4 11 -10 52.58 4.72 -4 -11 10 49.78 3.58 4 -11 -10 45.61 3.85 -4 -11 11 44.46 3.82 -4 11 11 48.22 4.46 4 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86.02 6.69 -4 13 4 96.03 5.35 -4 13 4 95.63 4.41 -4 -13 4 91.76 6.18 4 -13 -4 100.82 4.97 4 -13 -4 97.25 6.02 4 -13 -4 110.19 5.35 -4 13 4 94.55 5.27 4 -13 -5 3.43 2.52 4 13 -5 8.31 2.58 -4 13 5 7.08 2.17 -4 -13 5 6.12 1.70 4 13 -5 6.47 1.96 -4 13 5 3.75 1.48 -4 13 5 3.99 0.91 -4 -13 5 4.23 0.69 4 -13 -5 5.28 1.61 4 -13 -5 5.11 1.82 4 -13 -5 4.49 0.79 4 13 -6 -0.46 1.27 -4 -13 6 1.61 0.69 -4 13 6 0.44 0.33 -4 13 6 1.24 0.56 4 13 -6 0.90 1.57 -4 13 6 3.07 2.39 -4 13 6 0.80 1.36 -4 -13 6 2.38 1.81 4 -13 -6 2.51 1.48 4 -13 -6 1.93 2.04 4 -13 -7 4.31 1.93 -4 -13 7 5.89 1.81 4 13 -7 4.51 1.13 4 -13 -7 2.04 2.38 4 13 -7 3.45 1.38 4 13 -7 5.05 2.69 -4 -13 7 3.45 1.03 -4 13 7 3.74 1.92 -4 13 7 1.87 0.99 4 13 -8 108.04 7.22 -4 13 8 101.70 5.08 4 -13 -8 103.13 6.11 4 13 -8 128.37 6.96 4 13 -8 105.16 4.22 4 13 -8 101.15 4.27 -4 13 8 105.39 6.20 -4 -13 8 106.62 6.91 -4 -13 8 114.78 5.39 4 -13 -8 93.86 5.56 4 -13 -8 109.33 6.86 4 13 -9 2.36 3.03 -4 -13 9 1.83 1.26 4 13 -9 -1.71 1.60 -4 13 9 0.88 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8.67 0 -1 11 195.89 9.44 0 -1 11 183.34 8.89 0 1 11 206.84 9.00 0 1 -11 193.40 8.51 0 1 -11 198.47 8.04 0 1 -11 196.26 9.31 0 -1 -11 173.26 9.18 0 -1 -11 196.89 8.60 0 1 -12 92.94 5.32 0 -1 -12 85.51 6.35 0 -1 -12 91.11 5.56 0 -1 12 79.99 6.94 0 -1 12 99.90 5.67 0 1 -12 70.57 5.22 0 1 -12 96.61 5.91 0 -1 -12 87.00 5.58 0 1 12 77.40 5.45 0 1 13 19.15 3.67 0 1 -13 19.87 2.84 0 1 -13 17.40 3.68 0 -1 -13 21.56 3.75 0 -1 -13 21.78 3.24 0 1 -13 26.09 3.00 0 -1 -13 19.93 2.67 0 -1 13 21.39 3.12 0 1 14 77.16 6.91 0 1 -14 76.13 7.39 0 1 -14 75.32 6.89 0 -1 -14 85.00 6.80 0 -1 14 71.05 6.25 0 1 -14 81.56 5.91 0 -1 -14 78.25 7.61 0 -1 -14 81.75 6.25 0 1 -15 155.19 9.15 0 1 -15 150.77 10.34 0 -1 -15 139.65 9.55 0 -1 -15 159.69 10.05 0 -1 15 138.17 9.27 0 1 -15 145.07 10.35 0 -1 -15 159.62 9.25 0 1 16 42.72 4.92 0 1 -16 45.74 5.91 0 -1 -16 45.92 5.68 0 -1 -16 49.52 4.68 0 1 -16 48.68 5.01 0 1 -16 41.06 5.45 0 -1 -16 51.03 5.81 0 -1 -17 67.45 6.48 0 -1 -17 73.88 6.70 0 -1 17 62.85 7.62 0 1 -17 55.29 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3.16 0.45 0 2 -2 0.67 0.45 0 2 -2 1.34 0.45 0 2 -2 3.03 0.45 0 -2 -2 4.27 0.56 0 -2 -2 2.69 0.45 0 -2 -2 3.50 0.34 0 -2 -2 3.15 0.34 0 -2 2 1.91 0.45 0 -2 2 2.92 0.45 0 -2 2 2.02 0.45 0 2 3 170.69 6.18 0 2 3 160.36 7.94 0 2 3 165.19 8.48 0 2 3 161.96 7.37 0 2 3 161.89 7.36 0 2 3 167.33 7.36 0 2 -3 163.22 7.33 0 2 -3 166.27 8.06 0 2 -3 167.76 7.22 0 2 -3 162.19 7.15 0 -2 -3 167.82 6.98 0 -2 -3 158.01 6.83 0 -2 -3 158.66 7.13 0 -2 -3 157.73 9.18 0 -2 -3 161.29 7.26 0 -2 3 164.04 6.52 0 -2 3 169.67 7.86 0 -2 3 172.12 8.64 0 -2 3 162.71 8.02 0 2 4 21.64 1.68 0 2 4 20.80 1.57 0 2 4 19.45 1.23 0 2 4 21.18 1.56 0 2 4 19.68 1.24 0 2 4 19.78 1.44 0 2 -4 20.96 1.58 0 2 -4 19.55 1.45 0 -2 -4 19.92 1.57 0 2 -4 17.06 1.44 0 -2 -4 21.09 1.23 0 2 -4 21.98 1.67 0 -2 -4 22.71 1.45 0 -2 4 21.78 1.35 0 -2 4 23.32 1.68 0 -2 4 21.19 1.68 0 -2 4 21.77 1.44 0 -2 -4 21.05 1.58 0 -2 -4 20.87 1.11 0 -2 5 323.85 15.83 0 2 5 322.40 11.45 0 2 5 307.69 17.45 0 2 5 331.27 14.17 0 2 5 302.90 11.33 0 2 5 308.25 11.44 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396.00 16.77 0 5 -1 365.87 17.45 0 5 -1 372.36 18.34 0 -5 -1 374.43 15.67 0 -5 -1 370.06 15.41 0 -5 1 375.20 16.30 0 -5 1 379.43 16.66 0 -5 1 368.14 15.09 0 -5 1 362.41 15.88 0 5 1 385.76 15.44 0 5 1 355.88 15.30 0 5 1 365.56 15.98 0 5 -1 364.05 17.18 0 5 -1 378.33 28.00 0 5 -1 368.64 15.51 0 -5 -1 354.25 14.76 0 -5 1 366.62 15.78 0 5 2 121.82 4.63 0 5 2 103.59 5.10 0 5 2 110.60 5.80 0 5 2 115.65 5.99 0 5 2 110.25 4.74 0 5 2 108.40 5.25 0 5 -2 117.09 5.01 0 5 -2 108.10 6.31 0 5 -2 120.74 5.18 0 5 -2 115.90 5.32 0 -5 -2 115.96 5.18 0 -5 -2 106.56 5.11 0 -5 -2 113.23 4.74 0 -5 -2 109.19 5.59 0 -5 2 115.13 4.95 0 -5 2 119.03 4.99 0 -5 2 109.36 5.01 0 5 -2 108.51 4.50 0 5 -2 108.91 5.23 0 -5 2 114.12 5.56 0 -5 2 111.52 4.71 0 5 3 179.87 7.65 0 5 3 173.71 7.76 0 5 3 180.91 7.70 0 5 3 173.62 7.12 0 5 -3 177.58 7.65 0 5 -3 183.39 7.72 0 5 -3 189.85 8.80 0 5 -3 178.74 9.66 0 -5 -3 178.56 7.43 0 -5 -3 162.48 7.80 0 -5 -3 176.20 7.26 0 -5 -3 177.89 7.42 0 -5 -3 177.95 7.05 0 -5 3 180.25 7.20 0 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0 5 -6 3.48 1.46 0 -5 -6 5.08 1.13 0 -5 -6 6.54 0.79 0 -5 6 5.28 1.57 0 -5 6 5.29 1.46 0 -5 6 6.26 1.56 0 -5 6 7.47 1.03 0 5 6 4.77 1.25 0 5 6 8.03 1.12 0 5 7 -0.34 1.12 0 5 -7 3.28 1.36 0 5 -7 0.00 1.12 0 5 -7 1.44 0.77 0 5 7 1.78 1.00 0 -5 -7 1.35 1.23 0 -5 -7 1.58 0.56 0 -5 7 6.74 3.82 0 5 7 0.34 0.78 0 5 7 1.12 0.67 0 5 7 0.45 1.25 0 -5 -7 2.60 1.47 0 -5 -7 0.23 0.56 0 -5 7 2.79 1.00 0 5 -8 21.40 2.60 0 5 -8 24.22 2.46 0 5 8 14.48 2.81 0 5 8 19.53 2.16 0 5 8 22.14 2.23 0 5 -8 21.43 2.21 0 -5 -8 18.76 2.15 0 -5 -8 21.20 1.91 0 -5 -8 22.35 1.69 0 -5 -8 21.92 1.57 0 -5 8 18.43 2.92 0 -5 8 18.72 2.45 0 5 8 21.61 1.57 0 5 -9 307.33 13.27 0 -5 -9 320.13 13.47 0 5 9 334.84 13.69 0 5 9 316.21 13.24 0 5 -9 314.39 15.85 0 5 -9 327.96 13.59 0 -5 -9 305.44 13.80 0 -5 -9 312.52 12.03 0 -5 9 326.44 13.27 0 -5 -9 297.32 12.90 0 -5 -10 5.77 2.04 0 -5 -10 7.97 1.46 0 -5 10 5.22 0.91 0 -5 10 6.57 2.23 0 5 10 5.73 1.35 0 5 10 7.34 1.89 0 5 -10 6.58 2.04 0 5 -10 6.80 1.78 0 5 -10 6.96 1.44 0 -5 -10 5.05 1.57 0 -5 -10 6.05 1.35 0 5 11 164.64 8.01 0 5 -11 155.29 8.06 0 5 -11 172.04 9.04 0 5 11 156.57 10.15 0 5 -11 167.99 7.73 0 -5 -11 161.64 8.50 0 -5 -11 151.89 6.84 0 -5 -11 160.02 8.41 0 -5 -11 156.61 6.74 0 -5 11 155.72 6.14 0 -5 11 165.42 7.58 0 5 -12 28.84 3.43 0 5 12 32.94 3.45 0 5 -12 36.92 3.86 0 5 -12 37.57 4.79 0 -5 -12 32.87 3.74 0 -5 -12 24.77 3.81 0 -5 -12 29.75 2.92 0 -5 12 27.66 2.50 0 -5 12 38.93 3.46 0 -5 -12 23.34 2.92 0 5 -13 1.02 2.39 0 -5 13 -0.46 1.48 0 5 13 2.90 2.34 0 5 -13 1.67 2.68 0 5 -13 -3.10 1.99 0 -5 -13 -0.91 2.61 0 -5 -13 -0.22 1.68 0 -5 -13 -0.11 1.35 0 -5 13 0.56 2.01 0 5 14 15.39 3.57 0 5 -14 8.88 2.62 0 -5 -14 15.91 3.36 0 -5 -14 16.06 2.47 0 -5 14 10.62 3.02 0 -5 -14 15.32 3.06 0 5 -14 11.40 2.66 0 5 -14 7.47 2.23 0 5 -15 58.07 5.24 0 5 -15 51.27 5.13 0 5 -15 59.48 6.20 0 -5 -15 45.71 4.93 0 -5 -15 52.12 4.27 0 -5 -15 52.68 5.00 0 5 -16 0.68 2.85 0 5 16 0.78 3.35 0 5 -16 2.34 2.79 0 5 -16 3.99 2.55 0 -5 -16 -2.73 3.29 0 -5 -16 0.11 3.25 0 -5 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1.47 0.34 0 -6 1 2.29 0.57 0 -6 1 1.93 0.57 0 -6 1 1.72 0.46 0 6 1 1.03 0.57 0 -6 1 1.60 0.68 0 6 2 41.72 2.40 0 -6 2 37.87 1.71 0 -6 2 39.29 2.27 0 6 2 39.50 1.91 0 6 -2 40.02 2.25 0 6 -2 37.65 1.69 0 6 -2 39.93 2.38 0 -6 2 40.17 2.38 0 -6 2 40.11 2.18 0 6 2 38.78 1.81 0 6 2 37.05 2.39 0 6 2 35.19 2.51 0 6 2 36.24 2.26 0 6 -2 38.11 1.71 0 6 -2 35.15 2.07 0 6 -2 36.86 2.39 0 -6 -2 38.13 1.91 0 -6 -2 36.16 2.39 0 -6 -2 39.61 2.06 0 -6 2 40.06 1.80 0 -6 -3 123.41 4.72 0 6 3 119.24 5.64 0 6 3 120.93 5.56 0 6 -3 115.05 5.79 0 -6 -3 105.77 5.21 0 -6 -3 119.29 5.25 0 6 3 119.69 6.31 0 6 3 119.05 4.99 0 6 3 116.21 4.90 0 6 -3 119.77 5.00 0 6 -3 123.62 5.40 0 6 -3 123.51 5.60 0 6 -3 120.18 5.53 0 6 -3 122.81 5.98 0 -6 -3 124.67 5.29 0 -6 -3 111.42 5.14 0 -6 3 123.17 5.17 0 -6 3 122.45 5.67 0 -6 3 118.40 4.89 0 -6 3 120.40 5.44 0 -6 3 119.53 5.62 0 6 -4 41.45 2.25 0 6 4 38.08 2.62 0 6 4 33.42 2.36 0 6 4 38.00 1.80 0 6 -4 39.33 1.93 0 6 -4 40.63 2.36 0 6 4 42.14 2.36 0 6 -4 40.70 2.57 0 6 4 38.83 1.80 0 -6 -4 35.69 2.25 0 -6 -4 41.67 2.49 0 -6 -4 41.44 1.91 0 -6 -4 38.45 1.82 0 -6 4 41.44 2.25 0 -6 4 44.30 2.71 0 -6 4 39.49 1.81 0 -6 4 41.86 2.37 0 -6 4 37.56 2.41 0 6 5 116.52 4.61 0 6 5 105.43 6.27 0 6 5 107.54 4.48 0 6 5 110.00 5.15 0 6 5 105.63 5.00 0 6 5 107.08 4.93 0 6 -5 103.27 4.87 0 6 -5 105.65 5.94 0 6 -5 109.69 5.34 0 6 -5 115.59 4.84 0 -6 -5 117.08 5.64 0 -6 -5 103.06 5.19 0 -6 -5 111.60 4.55 0 -6 -5 104.33 4.34 0 -6 5 111.51 4.72 0 -6 5 115.70 5.19 0 -6 5 103.93 4.40 0 -6 5 107.01 5.17 0 -6 5 104.47 5.29 0 6 6 838.49 29.66 0 6 6 794.99 32.90 0 6 6 803.31 29.51 0 6 6 815.47 35.84 0 6 6 791.32 34.09 0 6 6 801.87 28.74 0 6 -6 787.17 35.23 0 6 -6 827.47 34.36 0 6 -6 816.75 33.28 0 6 -6 816.63 32.04 0 -6 -6 780.24 30.13 0 -6 -6 756.86 32.76 0 -6 -6 825.30 32.72 0 -6 -6 756.85 31.52 0 -6 6 861.08 26.43 0 -6 6 824.20 39.88 0 -6 6 772.73 29.49 0 -6 6 807.40 32.74 0 -6 6 750.35 32.72 0 6 7 353.53 15.72 0 6 7 318.61 14.88 0 6 7 343.83 12.38 0 6 7 337.58 14.44 0 6 7 326.84 13.52 0 6 7 324.44 16.18 0 6 -7 324.56 14.39 0 6 -7 342.30 13.31 0 6 -7 352.86 15.17 0 -6 -7 345.09 13.33 0 -6 -7 330.00 13.95 0 -6 -7 339.36 12.62 0 -6 -7 324.64 12.47 0 -6 7 339.31 25.17 0 -6 7 317.56 12.08 0 -6 7 361.38 14.10 0 -6 7 321.55 13.83 0 6 8 95.50 7.41 0 6 8 93.67 4.03 0 6 8 90.79 4.57 0 6 -8 97.67 4.99 0 6 -8 92.68 4.58 0 6 -8 89.52 4.64 0 -6 -8 79.99 4.52 0 -6 -8 86.63 4.61 0 -6 -8 94.67 3.85 0 -6 -8 82.49 3.84 0 -6 8 99.21 5.73 0 -6 8 91.03 5.14 0 -6 8 87.73 4.26 0 6 9 66.93 3.25 0 6 9 75.59 4.45 0 6 -9 61.68 3.86 0 6 -9 70.86 4.24 0 6 -9 71.34 4.20 0 -6 -9 71.02 4.07 0 -6 -9 66.04 4.49 0 -6 -9 69.13 3.39 0 -6 -9 66.46 3.16 0 -6 9 69.65 4.80 0 -6 9 66.28 5.06 0 6 10 2.70 1.35 0 6 10 3.90 1.78 0 6 -10 4.09 1.48 0 6 -10 6.80 1.67 0 6 -10 8.72 1.88 0 -6 -10 8.04 2.26 0 -6 -10 5.39 1.91 0 -6 -10 5.86 1.58 0 -6 -10 6.43 1.24 0 -6 10 5.22 1.13 0 -6 10 5.91 2.23 0 -6 10 11.39 1.96 0 6 11 8.79 2.03 0 6 11 8.68 2.11 0 6 -11 13.29 2.50 0 6 -11 4.01 2.34 0 6 -11 11.26 2.21 0 -6 -11 13.82 2.49 0 -6 -11 12.57 2.13 0 -6 -11 11.27 1.58 0 -6 -11 12.28 1.46 0 -6 11 12.39 1.36 0 -6 11 8.71 2.12 0 6 12 10.02 2.56 0 6 -12 6.59 2.61 0 6 -12 8.03 2.90 0 6 -12 6.18 1.99 0 -6 -12 6.12 2.38 0 -6 -12 8.42 2.02 0 -6 -12 6.54 1.69 0 -6 -12 6.08 1.58 0 -6 12 8.65 1.25 0 -6 12 8.04 2.23 0 6 13 9.69 2.45 0 6 -13 5.69 2.96 0 6 -13 10.28 2.87 0 -6 -13 6.12 2.84 0 -6 -13 8.08 2.58 0 -6 -13 7.44 1.92 0 -6 -13 6.31 1.46 0 -6 13 5.24 1.48 0 -6 13 5.81 3.13 0 -6 13 6.66 2.30 0 6 14 151.52 11.71 0 6 -14 141.26 11.16 0 6 -14 175.94 9.51 0 -6 -14 161.02 10.10 0 -6 -14 145.83 8.30 0 -6 -14 149.05 9.69 0 -6 14 148.87 9.06 0 -6 14 134.12 8.96 0 6 15 48.11 6.03 0 6 -15 48.07 5.70 0 6 -15 58.22 4.65 0 -6 -15 51.42 5.45 0 -6 -15 44.75 5.38 0 -6 -15 48.91 4.62 0 -6 15 47.47 5.04 0 -6 15 46.60 5.51 0 6 16 5.14 3.13 0 6 -16 6.38 4.10 0 6 -16 12.19 3.43 0 -6 -16 6.93 3.75 0 -6 -16 8.86 3.03 0 -6 -16 6.43 2.25 0 -6 16 5.94 3.25 0 -6 16 4.59 3.44 0 6 17 6.71 4.36 0 6 -17 3.08 3.08 0 6 -17 6.57 3.23 0 6 -17 5.65 3.44 0 -6 -17 -1.70 3.41 0 -6 -17 6.28 4.37 0 -6 17 6.96 3.14 0 -6 17 1.15 3.21 0 6 18 3.36 4.71 0 6 -18 3.88 2.96 0 6 -18 4.57 3.34 0 6 -18 5.10 4.44 0 -6 -18 9.88 5.34 0 -6 -18 10.43 4.71 0 -6 18 4.16 3.48 0 -6 18 6.99 4.93 0 6 19 1.68 3.70 0 6 -19 2.96 6.16 0 6 -19 10.03 5.24 0 6 -19 2.55 2.89 0 -6 -19 -6.70 5.11 0 -6 -19 1.01 5.38 0 -6 19 -2.36 3.26 0 -6 19 3.44 5.16 0 6 20 35.18 6.74 0 6 -20 46.18 8.55 0 6 -20 45.22 8.91 0 6 -20 47.46 8.00 0 -6 -20 45.96 6.81 0 -6 -20 42.29 8.64 0 -6 20 43.27 7.44 0 -6 20 51.07 7.56 0 6 -21 -0.68 4.56 0 6 -21 -3.45 4.01 0 6 -21 6.56 5.56 0 -6 -21 5.39 5.95 0 -6 21 -3.27 4.85 0 -6 21 5.04 8.35 0 7 0 0.00 0.46 0 7 0 0.00 0.57 0 7 0 -0.23 0.34 0 7 0 -1.03 0.80 0 -7 0 0.23 0.11 0 -7 0 0.11 0.11 0 -7 0 1.03 1.26 0 -7 0 -0.11 1.03 0 -7 0 -0.68 0.46 0 7 1 174.40 6.67 0 7 1 174.19 8.47 0 7 1 174.24 6.92 0 7 1 168.91 7.76 0 7 1 162.12 8.13 0 7 -1 171.74 6.95 0 7 -1 173.00 8.84 0 7 -1 186.94 8.21 0 7 -1 167.08 8.61 0 7 -1 162.19 7.58 0 7 -1 172.59 7.92 0 -7 -1 164.98 8.34 0 -7 -1 161.94 7.43 0 -7 -1 153.78 7.22 0 -7 1 178.52 6.68 0 -7 1 166.69 8.55 0 -7 1 176.61 7.09 0 -7 1 162.64 7.72 0 -7 1 170.57 7.58 0 7 2 86.75 4.31 0 7 2 78.69 3.76 0 7 2 81.56 3.50 0 7 2 86.97 3.54 0 7 2 80.05 4.34 0 7 -2 80.62 3.43 0 7 -2 83.54 4.48 0 7 -2 90.41 4.04 0 7 -2 79.93 4.39 0 7 -2 83.14 4.07 0 7 -2 76.87 4.10 0 -7 -2 83.34 3.49 0 -7 -2 78.23 3.76 0 -7 -2 82.88 3.77 0 -7 2 86.40 3.38 0 -7 2 83.83 4.09 0 -7 2 83.92 3.31 0 -7 2 85.21 3.98 0 -7 2 79.62 3.91 0 7 3 55.83 3.95 0 7 3 57.20 3.06 0 7 3 60.17 2.83 0 7 3 56.33 2.60 0 7 3 57.15 3.19 0 7 -3 58.00 2.74 0 7 -3 48.38 3.33 0 7 -3 59.08 2.92 0 7 -3 61.08 3.14 0 7 -3 58.91 2.59 0 7 -3 59.64 3.50 0 7 -3 56.69 3.18 0 -7 -3 56.82 2.48 0 -7 -3 51.74 2.84 0 -7 -3 61.79 2.71 0 -7 -3 58.82 3.08 0 -7 3 59.44 2.59 0 -7 3 57.16 3.52 0 -7 3 53.32 2.39 0 -7 3 55.03 3.06 0 -7 3 57.63 2.87 0 7 4 13.49 1.46 0 7 -4 10.83 1.56 0 7 -4 13.35 1.46 0 7 -4 14.65 1.25 0 7 4 19.24 1.46 0 7 4 14.57 1.02 0 7 4 13.09 0.79 0 7 4 12.96 1.59 0 7 -4 13.20 0.90 0 7 -4 13.64 1.58 0 7 -4 14.74 1.59 0 -7 -4 12.27 1.24 0 -7 -4 14.71 1.58 0 -7 -4 12.42 1.25 0 -7 -4 14.37 0.90 0 -7 4 15.61 1.35 0 -7 4 14.26 1.81 0 -7 4 14.42 1.02 0 -7 4 15.84 1.70 0 -7 4 15.04 1.72 0 -7 5 529.73 19.43 0 7 5 491.35 21.70 0 7 5 470.05 20.51 0 7 5 479.91 17.93 0 7 5 474.96 21.97 0 7 5 480.12 16.95 0 7 -5 483.31 17.37 0 7 -5 495.14 19.29 0 7 -5 520.93 19.37 0 7 -5 495.53 18.93 0 -7 -5 498.10 17.93 0 -7 -5 449.06 20.05 0 -7 -5 478.96 18.71 0 -7 -5 477.35 17.65 0 -7 5 504.05 19.11 0 -7 5 469.17 19.36 0 -7 5 481.38 20.53 0 -7 5 453.94 19.56 0 7 6 38.39 2.69 0 7 6 32.68 2.57 0 7 6 34.49 1.79 0 7 6 32.27 1.91 0 7 6 31.57 2.95 0 7 6 31.85 2.46 0 7 -6 33.89 2.27 0 7 -6 34.47 2.69 0 7 -6 34.61 2.33 0 -7 -6 35.64 2.48 0 -7 -6 32.73 2.37 0 -7 -6 35.77 1.82 0 -7 -6 32.43 1.71 0 -7 6 34.36 2.36 0 -7 6 30.33 2.82 0 -7 6 31.24 1.58 0 -7 6 35.97 2.81 0 -7 6 32.60 2.42 0 7 7 23.23 2.69 0 7 7 19.91 2.13 0 7 7 22.58 1.46 0 7 7 23.62 1.68 0 7 7 22.66 2.01 0 7 -7 23.58 2.04 0 7 -7 24.37 2.68 0 7 -7 26.90 2.44 0 -7 -7 21.79 2.37 0 -7 -7 22.09 2.14 0 -7 -7 25.42 1.60 0 -7 -7 25.77 1.48 0 -7 7 17.86 2.13 0 -7 7 23.72 1.35 0 -7 7 27.25 2.13 0 -7 7 23.75 2.31 0 7 8 592.22 37.16 0 7 8 628.20 27.43 0 7 8 645.58 23.99 0 7 -8 585.82 22.35 0 7 -8 608.48 24.81 0 7 -8 597.44 24.34 0 -7 -8 598.82 23.85 0 -7 -8 589.00 24.10 0 -7 -8 609.93 21.33 0 -7 -8 601.53 21.86 0 -7 8 636.65 30.02 0 -7 8 584.29 25.18 0 -7 8 589.67 21.29 0 -7 8 595.63 25.62 0 -7 -9 188.92 7.38 0 -7 9 191.60 8.11 0 7 9 201.48 8.07 0 7 9 194.96 8.36 0 7 -9 194.59 9.42 0 7 -9 204.80 10.16 0 7 -9 204.22 8.62 0 -7 -9 205.47 8.60 0 -7 -9 174.61 8.78 0 -7 -9 195.01 7.97 0 -7 9 187.44 8.95 0 -7 9 180.93 8.77 0 -7 10 347.24 15.35 0 7 10 387.81 22.02 0 7 10 407.44 17.16 0 7 -10 365.95 16.59 0 7 -10 402.91 14.74 0 7 -10 387.04 15.69 0 -7 -10 364.99 15.29 0 -7 -10 385.48 15.87 0 -7 -10 375.25 15.23 0 -7 -10 373.33 16.21 0 -7 10 367.81 13.96 0 -7 10 384.76 17.11 0 -7 -11 56.48 3.28 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86.97 4.08 0 8 1 90.27 4.90 0 8 1 88.75 4.36 0 8 -1 88.49 3.80 0 8 -1 85.99 4.13 0 8 -1 89.23 4.05 0 8 -1 87.65 6.57 0 -8 -1 85.80 4.34 0 -8 -1 90.26 3.95 0 -8 1 93.35 4.56 0 -8 1 84.68 3.43 0 -8 1 90.61 4.09 0 -8 1 83.41 4.13 0 -8 2 70.28 3.15 0 -8 2 68.64 3.20 0 -8 2 68.98 3.86 0 8 2 63.58 4.76 0 8 2 60.10 3.88 0 8 2 70.99 2.83 0 8 2 70.42 3.88 0 8 2 70.25 4.35 0 8 -2 70.24 3.08 0 8 -2 72.88 3.45 0 8 -2 72.82 3.37 0 8 -2 69.72 3.71 0 8 -2 70.34 3.85 0 8 -2 68.27 3.88 0 -8 -2 72.76 3.04 0 -8 -2 70.55 3.65 0 -8 -2 67.24 3.54 0 -8 2 73.43 3.22 0 8 3 69.32 3.30 0 8 3 68.26 3.16 0 8 -3 67.02 2.86 0 8 -3 73.89 3.59 0 8 -3 67.88 3.59 0 8 3 71.63 3.62 0 8 3 71.40 4.09 0 8 3 68.62 2.72 0 8 -3 71.65 3.91 0 8 -3 71.37 3.37 0 8 -3 68.59 3.62 0 8 -3 64.73 3.18 0 -8 -3 75.73 3.27 0 -8 -3 65.68 3.75 0 -8 -3 66.70 4.11 0 -8 3 71.89 3.60 0 -8 3 73.35 3.75 0 -8 3 69.35 3.31 0 -8 3 77.70 3.64 0 -8 3 67.80 3.91 0 8 -4 1.01 0.78 0 8 -4 0.23 0.90 0 -8 4 2.13 0.79 0 -8 4 0.68 0.79 0 8 4 1.13 0.79 0 8 4 2.14 1.13 0 8 4 0.57 0.45 0 8 4 0.79 0.45 0 8 4 1.59 1.59 0 8 -4 0.11 0.68 0 8 -4 -0.22 0.67 0 8 -4 1.01 0.45 0 8 -4 2.15 1.13 0 -8 -4 0.68 0.79 0 -8 -4 1.70 0.79 0 -8 -4 1.35 0.56 0 -8 4 0.00 0.46 0 -8 4 0.91 1.02 0 -8 4 1.72 1.03 0 -8 5 864.23 34.49 0 8 5 829.80 34.55 0 8 5 812.58 42.77 0 8 5 803.44 30.86 0 8 5 770.97 34.15 0 8 5 795.32 30.82 0 8 -5 835.47 31.16 0 8 -5 868.40 31.96 0 8 -5 833.13 33.42 0 8 -5 836.15 36.41 0 -8 -5 822.11 27.97 0 -8 -5 738.72 31.12 0 -8 -5 778.29 32.11 0 -8 -5 832.77 34.34 0 -8 -5 801.24 30.31 0 -8 5 857.60 31.79 0 -8 5 804.98 29.33 0 -8 5 825.39 31.66 0 -8 5 787.96 30.13 0 -8 -6 93.64 4.09 0 -8 6 106.21 4.72 0 -8 6 93.33 4.42 0 -8 6 106.61 5.75 0 8 6 102.89 4.83 0 8 6 89.71 5.38 0 8 6 100.11 4.14 0 8 6 96.96 3.93 0 8 6 102.62 4.70 0 8 -6 90.93 4.88 0 8 -6 96.38 5.37 0 8 -6 100.25 5.66 0 -8 -6 104.33 5.08 0 -8 -6 92.45 4.53 0 -8 -6 101.47 4.17 0 -8 6 85.55 4.72 0 8 7 503.82 21.90 0 8 7 508.66 23.59 0 8 7 474.14 18.70 0 8 7 490.65 19.51 0 8 7 490.43 18.67 0 8 -7 485.39 19.87 0 8 -7 477.77 20.70 0 8 -7 494.62 17.85 0 -8 -7 477.52 17.40 0 -8 -7 458.14 18.09 0 -8 -7 480.13 18.83 0 -8 -7 467.57 17.02 0 -8 7 488.37 19.67 0 -8 7 478.56 19.21 0 -8 7 472.06 20.58 0 -8 7 465.82 19.15 0 8 8 66.39 3.36 0 8 8 68.94 3.35 0 -8 -8 68.13 3.73 0 -8 -8 67.93 4.18 0 -8 -8 72.10 3.19 0 -8 -8 65.09 3.09 0 8 -8 60.27 4.20 0 -8 8 70.47 3.15 0 -8 8 73.17 4.16 0 8 8 70.08 3.27 0 8 -8 68.92 3.91 0 8 -8 73.88 4.09 0 -8 8 67.85 4.94 0 -8 8 68.23 4.60 0 8 -9 173.62 9.77 0 8 -9 192.00 8.18 0 -8 9 176.96 7.96 0 8 9 184.96 7.29 0 8 9 193.72 8.03 0 8 -9 175.13 9.38 0 -8 -9 179.35 7.69 0 -8 -9 171.35 8.35 0 -8 -9 174.03 6.85 0 -8 -9 176.21 6.97 0 -8 9 173.40 7.42 0 -8 9 172.03 8.32 0 -8 10 20.21 2.54 0 -8 -10 20.84 2.82 0 -8 -10 21.89 1.94 0 -8 -10 20.27 1.59 0 -8 10 19.50 1.02 0 -8 10 20.64 1.35 0 -8 10 18.59 2.69 0 8 10 15.60 1.68 0 8 10 23.06 2.56 0 8 -10 22.27 2.84 0 8 -10 16.84 2.68 0 8 -10 26.27 3.20 0 -8 -10 22.41 2.60 0 8 11 17.00 2.03 0 8 11 18.93 2.67 0 8 -11 16.11 2.43 0 -8 -11 19.37 2.49 0 -8 -11 23.87 2.59 0 -8 -11 20.16 1.94 0 -8 -11 20.36 1.82 0 -8 11 18.77 1.37 0 -8 11 20.75 1.35 0 -8 11 17.69 2.91 0 -8 11 11.89 2.54 0 8 -11 21.83 2.73 0 8 -11 19.18 3.57 0 8 12 5.12 2.23 0 8 -12 3.41 2.39 0 8 -12 3.90 2.45 0 8 -12 7.73 2.21 0 -8 -12 13.37 2.95 0 -8 -12 10.92 2.59 0 -8 -12 3.87 1.59 0 -8 -12 6.48 1.48 0 -8 12 6.27 1.03 0 -8 12 5.50 0.90 0 -8 12 4.81 2.46 0 -8 12 8.31 2.54 0 8 13 208.13 11.93 0 8 -13 188.87 11.27 0 8 -13 192.56 11.59 0 8 -13 219.25 13.25 0 -8 -13 206.94 12.93 0 -8 13 188.35 9.32 0 -8 13 192.23 11.43 0 -8 -13 195.17 10.23 0 -8 13 206.40 11.09 0 -8 -13 205.01 10.69 0 8 -14 -0.11 2.51 0 8 -14 1.45 1.78 0 8 -14 2.65 1.99 0 -8 -14 0.68 1.82 0 -8 -14 -0.11 2.81 0 -8 -14 1.02 1.25 0 -8 14 -0.67 2.69 0 -8 14 1.04 2.08 0 8 14 -1.00 2.56 0 8 15 58.25 5.80 0 8 -15 58.13 5.47 0 8 -15 67.28 7.02 0 8 -15 57.70 6.19 0 -8 -15 60.37 6.24 0 -8 -15 52.07 5.74 0 -8 -15 54.85 4.88 0 -8 15 66.28 7.29 0 -8 15 55.11 5.30 0 8 -16 3.19 3.19 0 8 -16 5.46 3.12 0 8 -16 4.76 3.65 0 -8 -16 1.82 2.50 0 -8 -16 1.80 2.70 0 -8 16 2.65 3.57 0 8 16 8.15 3.80 0 8 17 3.47 4.25 0 8 -17 2.51 3.99 0 8 -17 -2.12 2.45 0 -8 -17 7.26 3.18 0 -8 -17 3.82 3.71 0 -8 17 4.61 3.34 0 8 -17 2.88 4.32 0 8 18 2.80 4.37 0 8 -18 0.57 4.22 0 8 -18 0.67 2.90 0 8 -18 3.21 3.88 0 -8 -18 -1.13 4.31 0 -8 -18 0.22 2.81 0 -8 18 -3.60 3.04 0 -8 18 10.24 5.41 0 8 -19 27.73 6.62 0 8 -19 46.32 8.02 0 8 -19 40.71 6.54 0 -8 -19 31.20 6.35 0 -8 -19 41.83 6.97 0 -8 19 33.68 6.65 0 -8 19 30.36 6.33 0 8 -20 2.05 3.99 0 -8 -20 3.60 5.96 0 -8 20 -4.85 4.96 0 -8 20 3.79 2.99 0 8 -20 -1.11 5.46 0 8 -20 2.44 5.00 0 -8 -20 2.61 3.97 0 8 21 2.92 7.09 0 8 -21 13.80 5.82 0 8 -21 9.91 5.12 0 8 -21 13.44 5.00 0 -8 21 9.03 5.76 0 -8 21 3.90 5.05 0 -8 -21 29.14 7.20 0 9 0 5.62 1.26 0 9 0 0.91 0.91 0 9 0 0.34 0.45 0 9 0 -0.34 0.57 0 -9 0 0.11 0.11 0 -9 0 0.23 0.11 0 -9 0 0.00 0.57 0 -9 0 -0.34 0.57 0 9 1 47.14 1.92 0 9 1 44.31 2.98 0 9 1 50.46 2.38 0 9 1 49.31 2.73 0 9 1 48.23 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4.83 0 -9 6 99.92 4.44 0 9 7 5.71 1.68 0 9 7 7.06 0.78 0 9 7 4.82 0.78 0 9 7 8.37 1.79 0 9 -7 6.48 1.70 0 9 -7 8.61 1.68 0 9 -7 8.09 1.44 0 -9 -7 5.42 1.58 0 -9 -7 6.69 1.47 0 -9 -7 5.96 0.79 0 -9 -7 6.01 0.79 0 -9 7 5.73 1.46 0 -9 7 5.56 0.68 0 -9 7 4.62 1.46 0 -9 7 3.92 1.27 0 9 7 6.18 1.80 0 9 8 56.23 2.80 0 9 8 52.77 3.68 0 9 -8 49.65 3.41 0 9 -8 50.56 3.54 0 -9 -8 49.94 3.73 0 -9 -8 49.11 3.28 0 -9 -8 50.79 2.60 0 -9 -8 49.21 2.51 0 -9 8 48.97 3.93 0 -9 8 48.92 2.27 0 -9 8 50.61 3.82 0 -9 8 38.89 3.35 0 9 8 50.21 2.37 0 9 -8 54.74 3.69 0 9 9 128.37 5.72 0 9 9 129.55 6.36 0 9 -9 120.12 6.71 0 9 -9 129.82 6.70 0 9 -9 129.39 6.63 0 -9 -9 117.60 6.56 0 -9 9 117.30 5.09 0 -9 9 122.86 6.07 0 -9 9 123.94 7.17 0 -9 -9 123.74 6.33 0 -9 -9 129.00 5.46 0 -9 -9 127.17 5.03 0 9 10 270.63 11.23 0 9 10 264.31 11.71 0 9 -10 275.76 11.27 0 9 -10 259.23 11.49 0 -9 -10 266.62 13.02 0 -9 -10 263.43 10.95 0 -9 -10 258.65 10.75 0 -9 10 260.56 9.31 0 -9 10 249.02 10.95 0 -9 10 268.37 10.89 0 -9 10 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4.42 0 -25 8 17.31 3.65 0 25 -9 25.59 4.52 0 25 -9 23.75 5.44 0 -25 9 26.73 4.21 0 -25 9 37.43 5.74 0 -25 -9 32.94 5.60 0 25 -10 12.43 5.33 0 25 -10 17.31 5.07 0 -25 -10 9.26 4.11 0 -25 10 18.83 4.13 0 -25 10 19.77 4.32 0 25 -11 17.53 5.55 0 -25 11 16.19 4.82 0 25 -11 18.84 4.63 0 -25 -11 13.48 5.14 0 -25 11 13.28 4.43 0 25 -12 0.89 3.77 0 25 -12 4.63 4.63 0 -25 -12 -9.47 5.71 0 -25 12 2.18 3.67 0 -25 12 -0.45 2.72 0 -25 -13 5.82 6.50 0 25 -13 2.75 3.85 0 -25 13 -2.52 3.67 0 -25 13 8.16 5.21 0 25 -14 -6.98 6.10 0 25 -14 3.63 5.95 0 -25 -14 4.44 7.18 0 -25 14 -4.13 5.85 0 -25 14 -7.59 5.32 0 25 -15 2.33 5.10 0 25 -15 3.08 4.52 0 -25 -15 -2.62 4.67 0 -25 15 -1.84 5.96 0 -25 15 -3.40 3.62 0 26 0 63.07 5.16 0 26 0 65.91 6.33 0 26 0 68.94 5.77 0 -26 0 65.91 6.60 0 26 -1 39.32 4.52 0 26 1 51.92 4.84 0 26 1 39.48 4.41 0 26 1 46.32 4.67 0 26 -1 45.33 5.15 0 -26 -1 44.48 5.59 0 -26 1 47.47 5.79 0 26 -1 40.71 4.99 0 26 2 20.02 3.73 0 26 -2 23.94 3.44 0 -26 -2 21.13 4.46 0 -26 2 26.07 3.76 0 26 2 23.79 3.34 0 26 -2 24.46 3.80 0 26 -2 23.49 4.52 0 26 2 21.51 3.28 0 26 3 -1.36 2.50 0 26 -3 1.00 2.99 0 -26 -3 -0.23 2.63 0 26 3 0.78 2.45 0 26 -3 -2.34 2.90 0 26 -3 -3.84 3.05 0 -26 3 -1.37 2.51 0 -26 -4 2.40 2.86 0 -26 4 5.02 3.31 0 26 4 5.69 2.73 0 26 4 5.68 2.45 0 26 -4 -3.90 3.12 0 26 -4 5.19 2.71 0 26 -4 7.19 3.87 0 -26 5 1.60 2.05 0 26 -5 -2.56 3.11 0 26 -5 3.54 3.76 0 -26 -5 1.72 3.44 0 26 -6 85.93 7.89 0 26 -6 72.71 7.18 0 -26 -6 74.45 7.33 0 -26 6 71.42 6.85 0 26 -7 1.33 4.22 0 26 -7 0.22 3.09 0 -26 -7 -0.23 2.98 0 -26 7 -1.26 3.56 0 -26 7 -0.68 3.19 0 26 -8 47.97 6.55 0 26 -8 42.37 6.51 0 -26 -8 46.94 6.53 0 -26 8 51.11 6.66 0 -26 8 46.55 5.92 0 26 -9 -0.22 4.22 0 26 -9 -3.86 4.52 0 -26 -9 7.09 5.03 0 -26 9 -1.26 2.87 0 -26 9 1.59 3.98 0 26 -10 -4.55 4.66 0 26 -10 1.32 2.87 0 -26 -10 -1.49 4.69 0 -26 10 -2.99 4.83 0 -26 10 1.70 3.06 0 26 -11 2.44 4.77 0 26 -11 7.71 4.52 0 -26 -11 4.11 5.03 0 -26 11 -4.94 5.17 0 -26 11 4.99 3.51 0 -26 12 37.92 6.68 0 26 -12 34.04 6.21 0 26 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5.47 0 -28 1 9.08 4.43 0 28 2 5.19 2.82 0 28 2 -0.91 3.28 0 28 2 4.33 3.00 0 28 -2 5.13 3.35 0 28 -2 1.35 2.60 0 28 -2 2.54 3.43 0 -28 -2 3.77 3.08 0 -28 2 10.36 3.30 0 -28 -3 5.49 3.66 0 28 -3 5.75 3.38 0 28 3 5.21 3.51 0 28 3 5.56 3.18 0 28 3 6.33 3.11 0 28 -3 -0.33 3.34 0 28 -3 9.07 4.20 0 -28 3 7.52 3.76 0 28 -4 0.22 3.23 0 28 -4 -0.68 2.93 0 28 -4 -0.77 4.20 0 -28 -4 6.53 4.69 0 -28 4 2.62 3.65 0 28 -5 18.68 4.67 0 28 -5 13.40 3.83 0 28 -5 9.83 4.64 0 -28 -5 24.40 4.58 0 -28 5 28.16 4.90 0 28 -6 11.56 4.67 0 28 -6 6.07 4.95 0 28 -6 6.07 3.86 0 -28 -6 4.01 3.44 0 -28 6 16.30 4.67 0 -28 7 12.52 3.53 0 28 -7 9.22 3.55 0 28 -7 14.27 3.93 0 28 -7 12.68 4.41 0 -28 -7 24.07 5.04 0 28 -8 17.65 5.77 0 28 -8 12.68 5.51 0 -28 -8 6.87 4.01 0 -28 8 16.82 5.46 0 28 -9 5.33 3.77 0 -28 -9 1.49 5.38 0 -28 9 3.34 4.14 0 -28 9 3.63 4.54 0 28 -10 1.44 4.99 0 28 -10 -2.09 3.19 0 -28 -10 2.52 6.07 0 -28 10 -6.33 5.52 0 -28 10 -1.13 3.51 0 28 -11 1.88 4.32 0 28 -11 -0.22 4.29 0 -28 -11 6.98 7.21 0 -28 11 1.61 5.87 0 -28 11 5.09 5.20 0 28 -12 2.33 6.43 0 28 -12 5.61 6.94 0 -28 -12 8.69 5.60 0 -28 12 9.10 7.02 0 28 -13 -8.42 6.21 0 28 -13 2.20 5.17 0 -28 -13 7.65 6.40 0 -28 13 10.13 7.14 0 -29 0 -4.55 3.98 0 29 0 1.01 3.25 0 29 0 1.02 2.26 0 29 0 0.66 3.76 0 29 1 -3.51 3.73 0 -29 1 3.63 3.63 0 29 1 -0.45 3.71 0 29 1 0.22 3.43 0 29 -1 7.27 3.47 0 29 -1 1.36 3.84 0 29 -1 -0.88 2.54 0 -29 -1 8.67 4.56 0 29 2 6.23 3.40 0 29 2 2.55 3.77 0 29 2 6.76 4.39 0 29 -2 7.70 3.68 0 29 -2 5.64 3.27 0 29 -2 11.16 4.31 0 -29 -2 3.43 2.74 0 29 -3 1.45 4.12 0 29 -3 -2.54 3.76 0 29 3 2.83 3.73 0 29 -3 0.90 2.71 0 -29 -3 1.60 4.46 0 -29 3 2.39 3.53 0 29 -4 26.27 5.57 0 29 -4 12.51 4.85 0 29 4 34.50 5.79 0 29 -4 14.24 4.64 0 -29 -4 28.63 5.95 0 -29 4 34.19 5.70 0 29 -5 5.12 3.11 0 -29 5 4.44 2.85 0 29 -5 3.04 2.93 0 29 -5 0.66 2.87 0 -29 -5 1.60 4.70 0 29 -6 4.56 3.33 0 29 -6 -0.22 3.60 0 29 -6 0.44 3.86 0 -29 -6 4.59 4.13 0 -29 6 5.01 4.56 0 29 -7 -0.66 3.86 0 29 -7 -6.11 4.78 0 29 -7 2.47 3.15 0 -29 -7 4.36 5.39 0 -29 7 -1.59 4.21 0 29 -8 27.28 5.28 0 29 -8 21.42 4.88 0 29 -8 23.69 5.40 0 -29 -8 28.08 7.34 0 -29 8 28.62 5.79 0 29 -9 2.88 5.44 0 29 -9 0.77 3.97 0 -29 -9 -3.44 5.73 0 -29 9 5.44 4.76 0 29 -10 38.37 6.88 0 -29 -10 43.29 6.53 0 -29 10 46.53 7.95 0 29 -10 31.27 8.26 0 -29 10 37.12 5.66 0 29 -11 -10.53 5.21 0 29 -11 1.65 7.05 0 -29 -11 1.37 4.12 0 -29 11 3.46 4.49 0 29 -12 3.21 6.87 0 29 -12 -1.21 5.39 0 -29 -12 0.69 7.32 0 -29 12 2.88 5.07 0 30 0 19.44 5.09 0 30 0 10.97 4.70 0 30 0 12.94 5.42 0 -30 0 21.05 5.35 0 30 1 24.24 5.05 0 30 1 31.10 5.20 0 30 1 22.14 5.42 0 30 -1 33.07 5.36 0 30 -1 27.45 5.76 0 30 -1 29.29 4.75 0 -30 -1 24.86 6.73 0 -30 1 27.02 4.88 0 30 2 1.70 3.74 0 30 2 6.75 4.05 0 30 2 -0.22 3.43 0 30 -2 1.23 4.24 0 30 -2 3.05 4.85 0 30 -2 7.62 4.86 0 -30 -2 2.63 4.00 0 30 -3 2.45 4.23 0 30 3 1.58 4.29 0 30 -3 -6.09 4.17 0 30 -3 -2.43 3.86 0 -30 -3 -4.46 4.58 0 -30 3 -0.80 2.73 0 30 4 -2.15 2.38 0 30 -4 1.11 3.23 0 30 -4 -2.82 4.40 0 30 -4 0.55 2.98 0 -30 -4 0.57 3.66 0 -30 4 -5.13 3.53 0 30 5 13.30 3.75 0 30 -5 17.57 5.12 0 30 -5 7.77 3.94 0 30 -5 4.96 4.52 0 -30 -5 5.50 5.39 0 -30 5 17.77 5.35 0 30 -6 4.67 4.89 0 30 -6 17.33 4.61 0 30 -6 21.60 6.50 0 -30 -6 8.71 6.31 0 -30 6 16.73 3.64 0 30 -7 15.88 4.89 0 30 -7 19.44 6.07 0 30 -7 19.39 6.61 0 -30 -7 19.49 6.42 0 -30 7 15.23 5.80 0 30 -8 0.89 4.88 0 30 -8 9.88 6.29 0 30 -8 1.32 6.17 0 -30 -8 -3.55 4.24 0 -30 8 4.99 4.54 0 30 -9 3.33 4.66 0 30 -9 8.08 6.39 0 30 -9 2.20 4.51 0 -30 -9 -5.50 4.58 0 -30 9 1.47 3.40 0 30 -10 -0.67 4.32 0 30 -10 3.25 6.28 0 30 -10 -0.11 4.62 0 -30 -10 4.70 5.73 0 30 -11 5.49 5.15 0 30 -11 0.33 4.40 0 30 -11 0.55 5.88 0 -30 -11 8.13 7.79 0 -30 11 2.42 6.57 0 31 0 -2.69 2.57 0 31 0 3.73 4.07 0 31 0 2.65 2.65 0 -31 0 3.19 3.98 0 31 -1 2.87 4.97 0 31 1 -0.34 2.91 0 31 1 1.70 3.96 0 31 1 2.65 2.77 0 31 -1 -1.90 3.80 0 31 -1 -2.03 5.31 0 -31 -1 5.47 5.82 0 31 2 0.22 4.61 0 31 -2 -1.23 4.35 0 31 -2 -6.32 4.40 0 31 -2 5.08 4.64 0 -31 -2 1.03 3.88 0 31 3 11.04 5.30 0 31 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5.49 0 32 -4 -5.90 5.34 0 32 -4 3.38 3.72 0 32 -4 2.42 5.73 0 -32 -4 0.69 4.47 0 -32 4 -1.93 4.10 0 32 -5 3.11 3.45 0 32 -5 -0.34 6.08 0 32 -5 2.97 5.40 0 -32 -5 6.42 4.36 0 -32 5 0.80 4.78 0 32 -6 13.00 6.11 0 32 -6 10.81 6.19 0 32 -6 3.96 5.72 0 -32 -6 12.84 5.62 0 -32 6 16.26 5.68 0 32 -7 2.11 4.22 0 32 -7 -2.59 6.07 0 32 -7 -4.84 4.29 0 -32 -7 0.80 4.70 0 32 -8 10.76 6.77 0 -32 -8 9.75 7.46 0 32 -8 8.99 6.52 0 32 -8 10.45 4.84 0 32 -9 -8.10 6.32 0 32 -9 5.05 5.16 0 32 -9 5.28 5.17 0 -32 -9 7.34 4.93 0 33 0 -4.55 3.75 0 33 -1 3.61 3.84 0 33 -1 -3.35 4.91 0 33 -1 1.32 5.30 0 -33 -1 -5.93 5.47 0 33 -2 -0.79 5.53 0 33 -2 7.39 5.62 0 -33 -2 6.62 4.45 0 33 -3 0.45 3.61 0 33 -3 -0.89 3.56 0 33 -3 8.92 4.19 0 -33 -3 2.06 6.18 0 33 -4 9.47 5.84 0 33 -4 1.78 5.67 0 33 -4 11.39 5.53 0 -33 -4 0.11 5.84 0 33 -5 -1.92 6.31 0 33 -5 4.33 4.33 0 33 -5 12.88 6.38 0 -33 -5 5.85 5.85 0 33 -6 -0.23 7.54 0 33 -6 -1.11 5.78 0 33 -6 -2.97 4.84 0 -33 -6 9.41 7.34 0 33 -7 -4.77 5.66 0 33 -7 1.46 6.53 0 33 -7 0.11 4.73 0 -33 -7 -12.05 6.77 0 34 1 7.52 4.22 0 34 -2 3.27 4.29 0 34 -2 -1.65 5.84 0 -34 -2 0.80 4.80 0 34 -3 1.47 4.51 0 34 -3 0.00 4.07 0 -34 -3 2.97 6.52 0 34 -4 -3.84 6.77 0 34 -4 1.54 6.16 0 -34 -4 0.23 6.87 0 34 -5 12.22 6.67 0 34 -5 2.37 5.07 0 34 -5 7.70 6.49 0 -34 -5 3.78 7.22 0 34 -6 -5.18 7.10 0 34 -6 -3.11 4.00 0 34 -6 -0.66 4.73 0 -34 -6 0.11 7.23 0 35 1 4.22 4.45 0 35 2 7.65 5.60 0 35 -3 2.97 7.27 0 35 -3 -2.14 5.42 0 -35 -3 0.46 6.63 1 0 0 7.16 1.39 1 0 0 0.91 0.57 1 0 0 8.83 2.72 1 0 0 0.23 0.11 -1 0 0 0.00 0.23 -1 0 0 0.11 0.23 -1 0 0 0.00 0.23 -1 0 0 0.00 0.11 1 0 1 -0.23 0.34 1 0 1 0.45 0.22 1 0 1 0.00 0.23 1 0 1 0.00 0.22 1 0 1 0.23 0.23 1 0 1 0.00 0.23 -1 0 -1 0.23 0.23 -1 0 -1 -0.11 0.34 -1 0 -1 0.11 0.23 -1 0 -1 0.34 0.34 -1 0 -1 0.11 0.23 1 0 3 0.57 0.68 1 0 3 0.45 0.67 1 0 3 1.01 0.56 1 0 3 0.11 0.34 -1 0 -3 0.00 0.45 -1 0 -3 1.57 0.67 -1 0 -3 0.22 0.45 -1 0 -3 -0.11 0.45 1 0 4 176.05 6.92 1 0 4 170.36 6.48 1 0 4 171.28 7.15 1 0 4 169.67 7.27 -1 0 -4 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564.52 25.54 2 -6 6 541.15 22.73 2 -6 6 518.03 23.25 2 6 7 0.34 1.36 2 6 7 1.23 1.23 2 6 7 0.00 0.89 -2 6 -7 1.13 0.90 -2 6 -7 0.00 1.00 -2 6 -7 -1.33 1.33 -2 -6 -7 -0.11 1.02 -2 -6 -7 0.23 1.02 -2 -6 -7 1.22 0.33 -2 -6 -7 0.23 0.34 -2 -6 -7 -0.68 1.14 -2 -6 -7 2.12 1.00 2 -6 7 -1.13 1.59 2 -6 7 1.13 1.47 2 -6 7 1.15 1.04 2 6 8 132.85 8.29 2 6 8 144.47 6.55 -2 6 -8 140.84 6.42 -2 6 -8 147.13 6.90 -2 6 -8 152.93 6.19 -2 -6 -8 138.24 7.01 -2 -6 -8 149.07 6.55 -2 -6 -8 149.50 6.23 -2 -6 -8 149.66 5.83 -2 -6 -8 152.46 7.84 -2 -6 -8 145.74 8.71 2 -6 8 150.50 7.02 2 -6 8 148.63 7.70 -2 6 -9 57.65 4.23 2 6 9 55.82 4.82 2 6 9 54.04 3.55 -2 6 -9 58.91 4.06 -2 6 -9 57.90 3.87 -2 -6 -9 49.90 4.52 -2 -6 -9 61.20 4.73 -2 -6 -9 60.35 2.56 -2 -6 -9 63.94 2.91 -2 -6 -9 61.47 3.97 -2 -6 -9 57.53 4.13 2 -6 9 63.36 4.29 2 -6 9 63.28 4.71 2 6 10 342.78 16.45 -2 6 -10 344.84 13.76 -2 6 -10 343.11 15.59 -2 6 -10 332.87 14.37 -2 -6 -10 333.46 15.92 -2 -6 -10 344.71 13.97 -2 -6 -10 350.46 13.94 -2 -6 -10 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6.52 6 0 0 636.19 22.95 6 0 0 630.15 25.12 6 0 0 606.22 27.66 6 0 0 590.28 32.05 -6 0 0 613.87 24.08 -6 0 0 629.85 25.05 -6 0 0 617.12 25.63 6 0 1 0.11 1.36 6 0 1 2.64 1.49 -6 0 -1 -0.91 1.81 -6 0 -1 0.23 1.37 -6 0 -1 0.79 1.36 6 0 2 16.67 2.49 6 0 2 18.50 2.53 -6 0 -2 19.05 2.61 -6 0 -2 18.15 2.61 -6 0 -2 19.90 2.84 6 0 3 1.04 1.04 -6 0 -3 0.79 1.36 -6 0 -3 0.68 1.25 -6 0 -3 -1.14 1.25 6 0 4 166.57 7.71 -6 0 -4 162.98 8.16 -6 0 -4 163.36 8.41 -6 0 -4 177.55 7.49 6 0 5 0.11 1.15 -6 0 -5 -2.38 1.82 -6 0 -5 0.46 0.46 -6 0 -5 0.46 1.14 -6 0 -5 2.84 1.70 -6 0 -5 -0.34 1.93 6 0 6 120.42 6.88 -6 0 -6 110.25 6.47 -6 0 -6 111.48 4.33 -6 0 -6 117.61 6.48 -6 0 -6 124.50 7.15 -6 0 -6 125.70 6.92 6 0 7 -0.92 2.06 -6 0 -7 -1.48 2.50 -6 0 -7 -0.57 0.79 -6 0 -7 -4.08 2.38 -6 0 -7 1.02 1.70 -6 0 -7 -1.81 1.70 6 0 8 5.47 1.94 -6 0 -8 11.92 3.07 -6 0 -8 6.44 1.47 -6 0 -8 8.03 2.49 -6 0 -8 8.03 1.92 -6 0 -8 7.70 2.26 6 0 9 3.41 2.84 -6 0 -9 0.23 1.81 -6 0 -9 -0.79 1.35 -6 0 -9 4.06 2.93 -6 0 -9 1.24 1.92 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-12 -7 -1 15.99 5.41 12 -7 1 5.44 6.45 12 7 2 3.08 6.04 -12 7 -2 -2.36 4.04 -12 7 -2 3.73 6.66 -12 7 -2 -7.27 4.20 -12 -7 -2 -1.47 4.17 -12 -7 -2 5.67 5.34 12 -7 2 -4.07 3.62 12 -7 2 0.00 5.36 -12 7 -3 -2.36 3.93 -12 7 -3 -4.97 5.88 -12 7 -3 -8.85 6.36 -12 -7 -3 4.74 6.65 -12 -7 -3 1.11 5.00 -12 -7 -3 0.23 4.51 12 -7 3 3.84 5.20 12 -7 3 0.69 5.26 -12 7 -4 5.28 4.50 -12 7 -4 1.02 4.52 -12 7 -4 3.52 6.81 -12 -7 -4 8.69 6.32 -12 -7 -4 -7.11 6.55 12 -7 4 3.61 6.89 12 -7 4 -2.52 5.50 -12 7 -5 2.59 4.39 -12 7 -5 -7.69 4.98 -12 7 -5 9.53 6.58 -12 -7 -5 2.15 4.52 -12 -7 -5 5.42 5.76 12 -7 5 0.34 5.64 12 -7 5 -1.95 5.97 -12 7 -6 15.66 7.21 -12 7 -6 6.56 4.86 -12 7 -6 11.56 7.48 -12 -7 -6 5.09 5.09 12 -7 6 6.08 5.07 12 -7 6 1.95 6.21 -12 7 -7 0.00 6.54 -12 7 -7 -2.03 4.18 -12 7 -7 -2.60 7.59 12 -7 7 0.67 5.85 12 8 0 -2.86 6.97 -12 8 0 -2.13 5.27 -12 8 0 4.74 5.53 -12 8 0 9.30 4.09 -12 -8 0 0.11 4.29 -12 -8 0 -0.89 5.11 -12 -8 0 2.47 4.95 12 8 1 12.56 6.51 -12 8 -1 2.58 5.38 -12 8 -1 12.31 5.42 -12 8 -1 2.27 3.86 -12 -8 -1 13.20 7.00 -12 -8 -1 7.55 5.33 12 -8 1 10.86 5.09 12 -8 1 8.08 5.35 -12 8 -2 5.27 6.50 -12 8 -2 1.24 6.55 -12 8 -2 -2.95 4.65 -12 -8 -2 3.61 4.74 -12 -8 -2 -4.67 5.56 -12 -8 -2 4.39 5.40 12 -8 2 -0.34 5.77 12 -8 2 -3.53 3.31 -12 8 -3 5.84 6.51 -12 8 -3 10.29 7.01 -12 8 -3 -0.57 6.24 -12 -8 -3 14.55 5.87 -12 -8 -3 12.00 4.56 -12 -8 -3 15.09 5.86 12 -8 3 14.91 5.76 12 -8 3 -1.14 3.88 -12 8 -4 2.92 6.18 -12 8 -4 -3.39 4.75 -12 8 -4 -3.06 4.54 -12 -8 -4 -12.87 6.32 -12 -8 -4 -0.56 3.83 12 -8 4 -5.87 4.62 12 -8 4 -8.36 5.73 -12 8 -5 4.95 7.20 -12 8 -5 -1.13 4.18 -12 8 -5 -6.23 7.25 -12 -8 -5 10.26 7.33 12 -8 5 5.52 5.30 12 -8 5 -1.84 4.70 -12 8 -6 -11.15 6.98 -12 8 -6 6.10 5.09 -12 8 -6 -15.17 8.83 12 -8 6 9.90 7.31 12 -8 6 -3.56 6.67 12 9 0 6.39 6.62 -12 9 0 10.99 6.28 -12 9 0 12.86 7.79 -12 9 0 16.00 6.01 -12 -9 0 7.80 4.86 -12 -9 0 11.44 6.11 12 -9 0 7.05 4.20 -12 9 -1 3.59 4.15 -12 9 -1 2.26 4.40 -12 9 -1 -5.67 4.08 -12 -9 -1 -1.02 3.95 -12 -9 -1 -5.44 5.55 12 -9 1 3.17 4.64 12 -9 1 -3.41 5.23 -12 9 -2 -2.58 3.92 -12 9 -2 4.97 6.89 -12 9 -2 1.47 6.80 -12 -9 -2 2.37 7.22 -12 -9 -2 6.89 4.56 -12 -9 -2 3.48 4.61 12 -9 2 1.69 4.18 12 -9 2 -1.60 5.93 -12 9 -3 9.20 4.38 -12 9 -3 2.26 6.78 -12 9 -3 -3.97 5.90 -12 -9 -3 4.06 4.40 -12 -9 -3 -9.45 6.86 12 -9 3 1.35 6.77 12 -9 3 1.71 5.37 -12 9 -4 5.17 4.61 -12 9 -4 -0.79 4.86 -12 9 -4 -3.29 4.76 -12 -9 -4 -5.31 4.85 -12 -9 -4 8.22 5.63 12 -9 4 0.23 6.20 12 -9 4 -5.15 3.78 -12 9 -5 8.44 5.17 -12 9 -5 11.87 5.76 -12 9 -5 -2.38 7.02 -12 -9 -5 0.23 5.52 12 -9 5 4.28 7.20 12 -9 5 9.29 6.65 -12 9 -6 -1.46 4.84 -12 9 -6 -3.84 4.97 -12 9 -6 15.95 7.58 12 -9 6 2.81 5.96 12 -9 6 13.45 7.36 12 10 0 1.48 6.05 -12 10 0 0.67 4.48 -12 10 0 10.61 6.66 -12 10 0 1.13 5.56 -12 -10 0 -1.13 5.99 -12 -10 0 12.55 5.89 12 -10 0 5.88 4.64 12 -10 0 0.34 5.00 -12 10 -1 -5.60 4.15 -12 10 -1 -0.23 3.84 -12 10 -1 8.39 6.58 -12 -10 -1 -0.90 6.32 -12 -10 -1 11.67 5.89 12 -10 1 2.03 7.01 12 -10 1 -1.48 3.87 -12 10 -2 12.89 6.39 -12 10 -2 17.29 7.46 -12 10 -2 14.85 7.14 -12 -10 -2 9.48 5.98 -12 -10 -2 7.67 4.56 12 -10 2 15.24 7.00 12 -10 2 3.65 4.67 -12 10 -3 1.35 5.95 -12 10 -3 13.22 6.78 -12 10 -3 -3.51 6.91 -12 -10 -3 6.32 6.21 -12 -10 -3 0.45 5.50 12 -10 3 0.11 4.73 12 -10 3 2.86 6.51 -12 10 -4 -1.35 6.29 -12 10 -4 4.18 5.31 -12 10 -4 0.34 7.02 -12 -10 -4 13.71 7.19 12 -10 4 8.78 4.39 12 -10 4 4.01 5.84 -12 10 -5 10.57 6.97 -12 10 -5 -2.94 5.42 -12 10 -5 -1.70 5.43 -12 -10 -5 0.67 4.95 12 -10 5 -2.14 4.05 12 -10 5 -2.52 6.54 -12 11 0 -9.97 6.39 -12 11 0 1.69 5.19 -12 11 0 3.97 6.12 -12 -11 0 3.84 4.75 -12 -11 0 -4.11 5.67 12 -11 0 4.30 6.44 12 -11 0 3.64 5.00 -12 11 -1 1.01 6.27 -12 11 -1 6.77 6.55 -12 11 -1 -2.04 5.78 -12 -11 -1 10.95 6.32 -12 -11 -1 6.56 4.56 12 -11 1 6.55 6.21 12 -11 1 1.14 5.92 -12 11 -2 2.35 7.40 -12 11 -2 1.47 4.40 -12 11 -2 -10.42 6.23 -12 -11 -2 -4.97 7.11 12 -11 2 -3.04 4.40 12 -11 2 -1.48 5.59 -12 11 -3 2.13 6.51 -12 11 -3 0.45 7.57 -12 11 -3 -5.09 4.08 -12 -11 -3 1.13 3.95 -12 -11 -3 8.29 5.49 12 -11 3 -1.13 6.19 12 -11 3 3.43 6.97 -12 11 -4 10.22 7.19 -12 11 -4 -3.95 6.89 -12 11 -4 -5.32 7.69 -12 -11 -4 -6.39 5.50 12 -11 4 -10.35 7.42 12 -11 4 -5.27 6.18 -12 11 -5 11.69 7.19 -12 11 -5 3.27 5.42 -12 11 -5 10.06 5.54 12 -11 5 0.11 7.41 12 -11 5 4.13 5.39 -12 12 0 -0.34 5.94 -12 12 0 -1.81 5.08 -12 12 0 1.59 4.76 -12 -12 0 -1.81 7.01 -12 -12 0 4.34 4.56 12 -12 0 1.02 3.95 12 -12 0 0.23 6.59 -12 12 -1 9.18 7.06 -12 12 -1 21.79 7.68 -12 12 -1 0.79 4.30 -12 -12 -1 0.90 6.78 12 -12 1 4.51 6.54 12 -12 1 4.10 4.55 -12 12 -2 3.81 7.17 -12 12 -2 9.26 5.53 -12 12 -2 0.79 3.96 -12 -12 -2 3.84 5.19 12 -12 2 15.10 6.87 12 -12 2 2.17 4.67 -12 12 -3 12.90 6.84 -12 12 -3 16.48 8.92 -12 12 -3 10.63 7.81 12 -12 3 15.75 6.30 12 -12 3 6.63 7.31 -12 12 -4 2.58 6.40 -12 12 -4 4.74 7.34 -12 12 -4 4.75 6.10 -12 -12 -4 7.95 5.37 12 -12 4 8.65 6.52 12 -12 4 8.59 5.72 -12 13 0 7.84 5.37 -12 13 0 12.41 7.56 -12 13 0 6.57 6.00 -12 -13 0 15.61 5.65 -12 -13 0 12.36 5.01 12 -13 0 16.49 7.91 12 -13 0 7.84 5.91 -12 13 -1 5.60 5.26 -12 13 -1 1.69 4.97 -12 13 -1 3.40 6.68 -12 -13 -1 5.31 4.74 12 -13 1 -0.23 4.96 12 -13 1 3.87 6.94 -12 13 -2 -0.34 4.15 -12 13 -2 4.85 7.90 -12 13 -2 -2.38 6.67 12 -13 2 5.18 5.97 12 -13 2 11.17 7.53 -12 13 -3 1.69 4.96 -12 13 -3 -3.62 7.23 12 -13 3 3.60 7.53 12 -13 3 -2.74 4.68 -12 14 0 1.57 4.70 -12 14 0 1.24 6.99 -12 14 0 7.13 6.57 -12 -14 0 1.81 5.43 12 -14 0 5.19 5.19 12 -14 0 -0.91 5.80 -12 14 -1 5.60 6.04 -12 14 -1 4.17 5.41 -12 14 -1 -3.28 5.88 12 -14 1 -3.16 7.66 12 -14 1 6.94 5.35 -12 14 -2 0.22 4.70 -12 14 -2 13.87 7.44 -12 14 -2 6.22 6.67 12 -14 2 -10.24 6.53 12 -14 2 9.35 7.87 13 0 0 7.29 5.35 -13 0 0 -0.34 5.29 -13 0 0 15.09 4.58 -13 0 0 11.20 8.15 13 0 1 5.26 7.05 13 0 2 -2.84 5.23 -13 0 -2 1.57 6.83 -13 0 -2 -9.40 8.04 13 1 0 12.07 8.09 -13 1 0 0.56 5.17 -13 1 0 11.08 7.72 -13 1 0 9.62 7.13 -13 -1 0 10.94 6.36 13 -1 0 0.91 4.67 13 1 1 -3.99 4.21 -13 1 -1 -9.07 7.06 -13 -1 -1 0.56 6.59 -13 -1 -1 1.02 8.03 13 1 2 -0.91 4.89 -13 1 -2 5.49 7.29 -13 1 -2 12.47 7.82 -13 -1 -2 -0.89 4.25 -13 -1 -2 -1.25 6.91 13 -1 2 3.64 4.43 13 2 0 -13.79 6.61 -13 2 0 -0.22 5.28 -13 2 0 0.56 7.17 -13 2 0 -6.57 6.79 -13 -2 0 1.00 4.46 13 -2 0 -6.48 4.78 13 2 1 -5.35 4.33 -13 2 -1 -2.13 6.29 -13 2 -1 2.58 5.16 -13 2 -1 7.93 7.59 -13 -2 -1 4.69 5.69 -13 2 -2 4.04 4.83 -13 2 -2 0.00 8.28 -13 -2 -2 1.56 6.25 13 3 0 12.54 7.41 -13 3 0 16.06 7.53 -13 3 0 3.93 5.05 -13 3 0 7.82 8.50 -13 -3 0 10.91 7.02 13 3 1 5.47 5.70 -13 3 -1 8.08 5.61 -13 3 -1 5.95 7.19 -13 3 -1 3.97 7.03 -13 -3 -1 7.02 5.91 13 -3 1 1.82 4.43 -13 3 -2 2.92 8.09 -13 3 -2 9.87 6.80 -13 -3 -2 8.47 6.58 -13 -3 -2 4.30 5.54 13 4 0 -0.80 7.64 -13 4 0 -9.99 6.74 -13 4 0 0.56 4.38 -13 4 0 4.76 8.27 -13 -4 0 8.68 4.67 13 4 1 0.11 5.01 -13 4 -1 0.34 5.16 -13 4 -1 -0.34 7.87 -13 4 -1 5.89 6.69 -13 -4 -1 -0.11 4.23 13 -4 1 -2.27 5.00 13 4 2 -0.34 8.09 -13 4 -2 2.03 7.76 -13 4 -2 1.93 5.33 -13 -4 -2 1.34 5.01 -13 -4 -2 4.86 5.42 13 -4 2 6.69 5.56 13 5 0 11.40 7.64 -13 5 0 3.93 6.06 -13 5 0 9.67 7.64 -13 5 0 7.93 7.59 -13 -5 0 5.22 6.45 13 -5 0 -1.02 5.00 13 5 1 11.63 6.84 -13 5 -1 5.16 6.73 -13 5 -1 23.51 7.88 -13 5 -1 6.35 7.71 -13 -5 -1 16.01 6.23 13 -5 1 8.96 8.06 13 6 0 -5.82 6.84 -13 6 0 11.56 5.50 -13 6 0 -0.22 7.65 -13 6 0 1.13 5.44 -13 -6 0 9.00 6.66 -13 -6 0 9.00 6.66 ; _shelx_hkl_checksum 74271 _shelx_res_file ; TITL TSBB-2 (L0218) l0218.res created by SHELXL-2018/3 at 17:22:06 on 19-Jan-2021 CELL 0.71073 9.4028 25.1718 15.5008 90.000 93.3046 90.000 ZERR 4 0.0001 0.0002 0.0001 0.000 0.0003 0.000 LATT 1 SYMM -X, .50+Y, .50-Z SFAC C H N O SN UNIT 156 184 16 24 4 MERG 2 OMIT 1 0 0 OMIT 0 2 1 OMIT 1 1 0 OMIT -1 1 1 OMIT 1 1 1 OMIT 1 2 0 TEMP -113 L.S. 12 BOND $H BIND SN1 O2 BIND SN1 O5A BIND SN1 O5B CONF ACTA SIMU 0.01 0.01 1.7 O6A > C28B SADI 0.005 O2 C1 C14A O5A C14B O5B SADI 0.005 O1 C1 O4 C14A O4 C14B DFIX 1.52 0.01 C37 C38 C38 C39 C37 C39_$2 HTAB O3 O2 HTAB O3 O2_$1 HTAB O6A O5A HTAB O6B O5B EQIV $1 2-x,1-y,-z EQIV $2 2-x, 1-y, 1-z FMAP 2 PLAN 10 WGHT 0.054500 1.051200 FVAR 0.19996 0.43714 SN1 5 1.143550 0.404581 0.175237 11.00000 0.03821 0.04234 = 0.03366 0.00012 0.00971 0.00372 O1 4 0.994558 0.454906 0.228896 11.00000 0.04861 0.04407 = 0.03492 0.00263 0.01111 0.01261 O2 4 1.010813 0.484306 0.096703 11.00000 0.04681 0.06038 = 0.03156 0.00055 0.01072 0.00753 O3 4 0.874224 0.570691 0.045910 11.00000 0.05483 0.05124 = 0.03074 0.00616 0.01197 0.00749 H3 2 0.921711 0.545539 0.044804 11.00000 0.06869 N1 3 0.641423 0.570791 0.367880 11.00000 0.04252 0.03964 = 0.03544 -0.00339 0.00966 0.00012 N2 3 0.557223 0.607652 0.382963 11.00000 0.03897 0.04060 = 0.03677 -0.00269 0.00980 -0.00047 C1 1 0.957258 0.488392 0.168602 11.00000 0.03873 0.04417 = 0.02978 -0.00012 0.00397 0.00045 C2 1 0.855978 0.530781 0.186956 11.00000 0.03513 0.04073 = 0.03048 -0.00332 0.00426 -0.00137 C3 1 0.820395 0.569980 0.124805 11.00000 0.03991 0.03887 = 0.03081 0.00151 0.00547 -0.00329 C4 1 0.727073 0.610622 0.144133 11.00000 0.05063 0.03870 = 0.03516 0.00458 0.00452 0.00129 AFIX 43 H4 2 0.704542 0.637386 0.102346 11.00000 -1.20000 AFIX 0 C5 1 0.667225 0.612565 0.222626 11.00000 0.04622 0.03526 = 0.03926 -0.00220 0.00691 0.00127 AFIX 43 H5 2 0.604374 0.640728 0.235119 11.00000 -1.20000 AFIX 0 C6 1 0.698738 0.572971 0.284568 11.00000 0.03761 0.03739 = 0.03336 -0.00284 0.00838 -0.00390 C7 1 0.792389 0.532841 0.266347 11.00000 0.04053 0.03582 = 0.03136 0.00245 0.00453 -0.00037 AFIX 43 H7 2 0.814077 0.506154 0.308404 11.00000 -1.20000 AFIX 0 C8 1 0.499253 0.604285 0.466254 11.00000 0.03677 0.04036 = 0.03425 -0.00510 0.00648 -0.00399 C9 1 0.398899 0.642564 0.483591 11.00000 0.04273 0.04123 = 0.03796 -0.00254 0.00800 -0.00187 AFIX 43 H9 2 0.374403 0.668761 0.441186 11.00000 -1.20000 AFIX 0 C10 1 0.333006 0.643470 0.562024 11.00000 0.04229 0.05047 = 0.04064 -0.00890 0.00871 -0.00293 C11 1 0.372559 0.604742 0.622576 11.00000 0.05353 0.05530 = 0.03461 -0.00653 0.01110 -0.00566 AFIX 43 H11 2 0.330706 0.604756 0.676913 11.00000 -1.20000 AFIX 0 C12 1 0.471622 0.566189 0.605300 11.00000 0.05776 0.04896 = 0.03605 0.00228 0.00696 -0.00131 AFIX 43 H12 2 0.495179 0.539636 0.647273 11.00000 -1.20000 AFIX 0 C13 1 0.536830 0.565837 0.527596 11.00000 0.04391 0.04245 = 0.03966 -0.00342 0.00519 0.00051 AFIX 43 H13 2 0.606252 0.539696 0.516368 11.00000 -1.20000 AFIX 0 C27 1 0.223513 0.685184 0.578848 11.00000 0.05978 0.06321 = 0.05405 -0.00476 0.01938 0.01088 AFIX 137 H271 2 0.184768 0.678779 0.635272 11.00000 -1.50000 H272 2 0.146349 0.683583 0.533646 11.00000 -1.50000 H273 2 0.268068 0.720375 0.578592 11.00000 -1.50000 AFIX 0 O4 4 1.161306 0.373752 0.300962 11.00000 0.04452 0.04743 = 0.03687 0.00125 0.00568 0.00822 PART 1 O5A 4 1.334911 0.326171 0.237996 21.00000 0.03059 0.05531 = 0.02834 0.00593 0.00842 0.00965 SAME O3 > C27 O6A 4 1.450287 0.249504 0.332762 21.00000 0.05097 0.05076 = 0.03722 0.01149 0.01661 0.00509 AFIX 83 H6A 2 1.426681 0.265078 0.286191 21.00000 -1.50000 AFIX 0 N3A 3 1.117100 0.317417 0.594436 21.00000 0.03503 0.04135 = 0.03349 0.00128 0.00700 -0.00001 N4A 3 1.124406 0.292715 0.663272 21.00000 0.04404 0.04360 = 0.03413 0.00254 0.00928 -0.00404 C14A 1 1.263084 0.339333 0.300235 21.00000 0.03625 0.03865 = 0.03175 0.00169 0.00567 -0.00307 C15A 1 1.275682 0.310454 0.383830 21.00000 0.03147 0.03490 = 0.03487 -0.00213 0.00449 -0.00096 C16A 1 1.371077 0.267751 0.395490 21.00000 0.03420 0.04218 = 0.03325 -0.00225 0.01464 -0.00445 C17A 1 1.387931 0.241818 0.475408 21.00000 0.03484 0.03615 = 0.03746 0.00161 0.01125 0.00308 AFIX 43 H171 2 1.455009 0.213821 0.483992 21.00000 -1.20000 AFIX 0 C18A 1 1.306095 0.257567 0.540677 21.00000 0.02949 0.02963 = 0.02928 -0.00150 0.00917 -0.00034 AFIX 43 H181 2 1.316526 0.239976 0.594895 21.00000 -1.20000 AFIX 0 C19A 1 1.207717 0.298728 0.529938 21.00000 0.03203 0.02918 = 0.03154 -0.00139 0.00343 0.00094 C20A 1 1.193742 0.325435 0.452031 21.00000 0.02981 0.03275 = 0.02882 0.00144 0.00461 0.00360 AFIX 43 H201 2 1.128234 0.354046 0.444884 21.00000 -1.20000 AFIX 0 C21A 1 1.028370 0.312953 0.725421 21.00000 0.03694 0.04502 = 0.03670 -0.00101 0.00691 -0.00162 C22A 1 0.937969 0.355101 0.708527 21.00000 0.04531 0.05342 = 0.04346 -0.00861 0.00229 -0.00295 AFIX 43 H221 2 0.938030 0.372809 0.654406 21.00000 -1.20000 AFIX 0 C23A 1 0.845780 0.372016 0.770860 21.00000 0.04654 0.06107 = 0.05003 -0.01659 0.01033 -0.00549 C24A 1 0.855086 0.346518 0.850211 21.00000 0.04894 0.06266 = 0.05662 -0.01504 0.01552 -0.00613 AFIX 43 H241 2 0.795821 0.358344 0.893955 21.00000 -1.20000 AFIX 0 C25A 1 0.946409 0.304850 0.868308 21.00000 0.05760 0.05812 = 0.05219 -0.00917 0.02336 -0.00811 AFIX 43 H25A 2 0.948616 0.288099 0.923288 21.00000 -1.20000 AFIX 0 C26A 1 1.035543 0.287357 0.805686 21.00000 0.04743 0.04881 = 0.03866 0.00048 0.00926 0.00152 AFIX 43 H261 2 1.099738 0.258732 0.817100 21.00000 -1.20000 AFIX 0 C28A 1 0.753151 0.420614 0.758138 21.00000 0.04955 0.06286 = 0.06689 -0.01018 0.02049 0.00658 AFIX 137 H281 2 0.665835 0.411168 0.724009 21.00000 -1.50000 H282 2 0.804899 0.447936 0.727597 21.00000 -1.50000 H283 2 0.728524 0.434321 0.814542 21.00000 -1.50000 AFIX 0 PART 2 O5B 4 1.309626 0.328209 0.232073 -21.00000 0.03675 0.04693 = 0.03134 -0.00094 0.00447 0.00225 SAME O3 > C27 O6B 4 1.463042 0.251744 0.308066 -21.00000 0.04643 0.04950 = 0.03470 0.00866 0.01762 0.01193 AFIX 83 H6B 2 1.437641 0.272918 0.268220 -21.00000 -1.50000 AFIX 0 N3B 3 1.185118 0.285802 0.608448 -21.00000 0.03941 0.04127 = 0.03478 0.00363 0.00872 -0.00030 N4B 3 1.089403 0.320008 0.609152 -21.00000 0.04254 0.04270 = 0.03372 0.00000 0.00633 -0.00297 C14B 1 1.252734 0.335460 0.302276 -21.00000 0.03439 0.03656 = 0.03293 -0.00416 0.00540 -0.00461 C15B 1 1.291598 0.303975 0.380719 -21.00000 0.03316 0.03666 = 0.02826 0.00045 0.00692 -0.00098 C16B 1 1.393528 0.263124 0.378525 -21.00000 0.03209 0.03776 = 0.03162 -0.00102 0.01148 -0.00100 C17B 1 1.423501 0.232233 0.451563 -21.00000 0.03623 0.03573 = 0.04116 0.00059 0.00542 -0.00038 AFIX 43 H172 2 1.493150 0.204936 0.450500 -21.00000 -1.20000 AFIX 0 C18B 1 1.353160 0.240978 0.524899 -21.00000 0.03452 0.03400 = 0.03685 0.00261 0.00526 0.00507 AFIX 43 H182 2 1.373890 0.219341 0.574244 -21.00000 -1.20000 AFIX 0 C19B 1 1.250702 0.281396 0.528678 -21.00000 0.03015 0.03255 = 0.03174 0.00207 0.00430 0.00081 C20B 1 1.222769 0.313188 0.456892 -21.00000 0.02952 0.03303 = 0.03600 -0.00376 0.00297 0.00218 AFIX 43 H202 2 1.156312 0.341497 0.459372 -21.00000 -1.20000 AFIX 0 C21B 1 1.024454 0.322744 0.691210 -21.00000 0.04183 0.04221 = 0.03761 -0.00746 0.00700 -0.00833 C22B 1 0.917403 0.359753 0.696392 -21.00000 0.04362 0.05334 = 0.04534 -0.01258 0.00393 0.00188 AFIX 43 H222 2 0.890803 0.380898 0.647321 -21.00000 -1.20000 AFIX 0 C23B 1 0.847284 0.366706 0.772644 -21.00000 0.04529 0.06476 = 0.04988 -0.01772 0.00730 -0.00158 C24B 1 0.882357 0.334103 0.842284 -21.00000 0.05353 0.06196 = 0.05168 -0.01294 0.01016 -0.00671 AFIX 43 H242 2 0.833196 0.337597 0.893834 -21.00000 -1.20000 AFIX 0 C25B 1 0.987276 0.296857 0.837546 -21.00000 0.05698 0.05850 = 0.04796 0.00279 0.01403 -0.00234 AFIX 43 H252 2 1.011694 0.275187 0.886349 -21.00000 -1.20000 AFIX 0 C26B 1 1.059337 0.290192 0.761677 -21.00000 0.04829 0.05058 = 0.04153 0.00181 0.01046 -0.00503 AFIX 43 H263 2 1.131037 0.263793 0.758446 -21.00000 -1.20000 AFIX 0 C28B 1 0.728813 0.406808 0.772838 -21.00000 0.06582 0.08568 = 0.06412 -0.01347 0.01696 0.00684 AFIX 137 H284 2 0.754429 0.434989 0.814503 -21.00000 -1.50000 H285 2 0.641172 0.389335 0.789138 -21.00000 -1.50000 H286 2 0.713613 0.422241 0.714997 -21.00000 -1.50000 AFIX 0 PART 0 C29 1 1.016279 0.347483 0.107603 11.00000 0.04459 0.04705 = 0.03252 -0.00242 0.00798 0.00514 AFIX 23 H291 2 0.978564 0.362721 0.052015 11.00000 -1.20000 H292 2 1.075319 0.316216 0.094748 11.00000 -1.20000 AFIX 0 C30 1 0.892272 0.329991 0.160578 11.00000 0.04545 0.04929 = 0.03451 -0.00121 0.00770 0.00064 AFIX 23 H301 2 0.930799 0.315112 0.216247 11.00000 -1.20000 H302 2 0.834154 0.361491 0.173503 11.00000 -1.20000 AFIX 0 C31 1 0.796981 0.288669 0.114657 11.00000 0.04348 0.04813 = 0.04143 -0.00333 0.00075 0.00492 AFIX 23 H311 2 0.757029 0.303476 0.059265 11.00000 -1.20000 H312 2 0.854462 0.257036 0.101545 11.00000 -1.20000 AFIX 0 C32 1 0.675879 0.272221 0.169924 11.00000 0.04630 0.06770 = 0.06630 -0.01340 0.00661 -0.00947 AFIX 137 H321 2 0.715235 0.256159 0.223728 11.00000 -1.50000 H322 2 0.614986 0.246356 0.138249 11.00000 -1.50000 H323 2 0.619406 0.303553 0.183397 11.00000 -1.50000 AFIX 0 C33 1 1.335539 0.446078 0.160235 11.00000 0.04746 0.04614 = 0.04908 -0.00295 0.00798 -0.00550 AFIX 23 H331 2 1.312307 0.483083 0.142993 11.00000 -1.20000 H332 2 1.389692 0.447418 0.216890 11.00000 -1.20000 AFIX 0 C34 1 1.430953 0.422135 0.093903 11.00000 0.03932 0.04867 = 0.04725 -0.00050 0.00433 -0.00243 AFIX 23 H341 2 1.447514 0.384176 0.107854 11.00000 -1.20000 H342 2 1.380992 0.424035 0.035994 11.00000 -1.20000 AFIX 0 C35 1 1.572428 0.449797 0.091027 11.00000 0.04385 0.06352 = 0.05392 0.00338 0.00587 -0.00319 AFIX 23 H351 2 1.626598 0.444800 0.147116 11.00000 -1.20000 H352 2 1.556030 0.488363 0.082824 11.00000 -1.20000 AFIX 0 C36 1 1.660623 0.429356 0.019211 11.00000 0.04525 0.08071 = 0.06699 0.01171 0.01310 0.00529 AFIX 137 H361 2 1.679330 0.391364 0.027768 11.00000 -1.50000 H362 2 1.751182 0.448674 0.020065 11.00000 -1.50000 H363 2 1.608370 0.434816 -0.036627 11.00000 -1.50000 AFIX 0 C37 1 0.906113 0.511918 0.572577 11.00000 0.11326 0.20999 = 0.11856 -0.07286 -0.03579 0.06314 AFIX 23 H371 2 0.948957 0.493958 0.624624 11.00000 -1.20000 H372 2 0.822029 0.532405 0.589114 11.00000 -1.20000 AFIX 0 C38 1 1.015980 0.549004 0.532833 11.00000 0.08143 0.06885 = 0.10878 0.00306 0.02217 0.00685 AFIX 23 H381 2 0.963940 0.572510 0.490655 11.00000 -1.20000 H382 2 1.057966 0.571923 0.579548 11.00000 -1.20000 AFIX 0 C39 1 1.132085 0.524290 0.489677 11.00000 0.09781 0.12489 = 0.08961 -0.00066 0.01104 0.03164 AFIX 23 H391 2 1.188027 0.552653 0.463175 11.00000 -1.20000 H392 2 1.195644 0.506552 0.533944 11.00000 -1.20000 AFIX 0 HKLF 4 REM TSBB-2 (L0218) REM wR2 = 0.1101, GooF = S = 1.038, Restrained GooF = 1.032 for all data REM R1 = 0.0398 for 7109 Fo > 4sig(Fo) and 0.0781 for all 10702 data REM 623 parameters refined using 645 restraints END WGHT 0.0545 1.0512 REM Highest difference peak 0.899, deepest hole -0.630, 1-sigma level 0.080 Q1 1 0.1435 0.7126 0.6758 11.00000 0.05 0.90 Q2 1 0.4289 0.5960 0.5241 11.00000 0.05 0.84 Q3 1 0.8183 0.4855 0.5969 11.00000 0.05 0.71 Q4 1 1.0879 0.4907 0.4989 11.00000 0.05 0.65 Q5 1 0.8895 0.5402 0.5222 11.00000 0.05 0.50 Q6 1 1.0703 0.5302 0.4430 11.00000 0.05 0.37 Q7 1 1.1382 0.4605 0.5427 11.00000 0.05 0.37 Q8 1 0.4013 0.5460 0.4934 11.00000 0.05 0.30 Q9 1 0.8802 0.6206 0.0404 11.00000 0.05 0.28 Q10 1 0.9817 0.4806 0.0816 11.00000 0.05 0.27 ; _shelx_res_checksum 74413 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Sn Sn1 1.14355(2) 0.40458(2) 0.17524(2) 0.03777(7) Uani d 1 . . O O1 0.99456(19) 0.45491(7) 0.22890(10) 0.0422(4) Uani d 1 . . O O2 1.01081(19) 0.48431(7) 0.09670(11) 0.0459(4) Uani d 1 . . O O3 0.8742(2) 0.57069(8) 0.04591(11) 0.0452(4) Uani d 1 . . H H3 0.922(4) 0.5455(14) 0.045(2) 0.069(12) Uiso d 1 . . N N1 0.6414(2) 0.57079(8) 0.36788(13) 0.0389(5) Uani d 1 . . N N2 0.5572(2) 0.60765(8) 0.38296(13) 0.0385(5) Uani d 1 . . C C1 0.9573(3) 0.48839(10) 0.16860(14) 0.0375(5) Uani d 1 . . C C2 0.8560(2) 0.53078(9) 0.18696(14) 0.0354(5) Uani d 1 . . C C3 0.8204(3) 0.56998(10) 0.12480(15) 0.0364(5) Uani d 1 . . C C4 0.7271(3) 0.61062(10) 0.14413(16) 0.0414(6) Uani d 1 . . H H4 0.704542 0.637386 0.102346 0.050 Uiso calc 1 . . C C5 0.6672(3) 0.61257(10) 0.22263(16) 0.0401(6) Uani d 1 . . H H5 0.604374 0.640728 0.235119 0.048 Uiso calc 1 . . C C6 0.6987(3) 0.57297(10) 0.28457(15) 0.0359(5) Uani d 1 . . C C7 0.7924(3) 0.53284(9) 0.26635(15) 0.0358(5) Uani d 1 . . H H7 0.814077 0.506154 0.308404 0.043 Uiso calc 1 . . C C8 0.4993(3) 0.60429(9) 0.46625(15) 0.0370(5) Uani d 1 . . C C9 0.3989(3) 0.64256(10) 0.48359(16) 0.0404(6) Uani d 1 . . H H9 0.374403 0.668761 0.441186 0.049 Uiso calc 1 . . C C10 0.3330(3) 0.64347(11) 0.56202(17) 0.0442(6) Uani d 1 . . C C11 0.3726(3) 0.60474(11) 0.62258(17) 0.0475(7) Uani d 1 . . H H11 0.330706 0.604756 0.676913 0.057 Uiso calc 1 . . C C12 0.4716(3) 0.56619(11) 0.60530(17) 0.0474(6) Uani d 1 . . H H12 0.495179 0.539636 0.647273 0.057 Uiso calc 1 . . C C13 0.5368(3) 0.56584(10) 0.52760(16) 0.0419(6) Uani d 1 . . H H13 0.606252 0.539696 0.516368 0.050 Uiso calc 1 . . C C27 0.2235(3) 0.68518(13) 0.5788(2) 0.0584(8) Uani d 1 . . H H271 0.184768 0.678779 0.635272 0.088 Uiso calc 1 . . H H272 0.146349 0.683583 0.533646 0.088 Uiso calc 1 . . H H273 0.268068 0.720375 0.578592 0.088 Uiso calc 1 . . O O4 1.16131(18) 0.37375(7) 0.30096(11) 0.0428(4) Uani d 1 . . O O5A 1.335(2) 0.3262(13) 0.2380(11) 0.038(3) Uani d 0.437(5) A 1 O O6A 1.4503(15) 0.2495(6) 0.3328(6) 0.0458(18) Uani d 0.437(5) A 1 H H6A 1.426681 0.265078 0.286191 0.069 Uiso calc 0.437(5) A 1 N N3A 1.1171(13) 0.3174(6) 0.5944(7) 0.0364(18) Uani d 0.437(5) A 1 N N4A 1.1244(5) 0.2927(2) 0.6633(3) 0.0403(12) Uani d 0.437(5) A 1 C C14A 1.263(3) 0.3393(10) 0.3002(11) 0.035(2) Uani d 0.437(5) A 1 C C15A 1.276(2) 0.3105(7) 0.3838(9) 0.0336(17) Uani d 0.437(5) A 1 C C16A 1.3711(14) 0.2678(5) 0.3955(6) 0.0361(17) Uani d 0.437(5) A 1 C C17A 1.3879(9) 0.2418(3) 0.4754(5) 0.0358(15) Uani d 0.437(5) A 1 H H171 1.455009 0.213821 0.483992 0.043 Uiso calc 0.437(5) A 1 C C18A 1.3061(8) 0.2576(3) 0.5407(4) 0.0292(13) Uani d 0.437(5) A 1 H H181 1.316526 0.239976 0.594895 0.035 Uiso calc 0.437(5) A 1 C C19A 1.2077(8) 0.2987(3) 0.5299(4) 0.0309(14) Uani d 0.437(5) A 1 C C20A 1.1937(12) 0.3254(4) 0.4520(6) 0.0303(16) Uani d 0.437(5) A 1 H H201 1.128234 0.354046 0.444884 0.036 Uiso calc 0.437(5) A 1 C C21A 1.0284(8) 0.3130(3) 0.7254(5) 0.0394(15) Uani d 0.437(5) A 1 C C22A 0.9380(17) 0.3551(7) 0.7085(9) 0.047(2) Uani d 0.437(5) A 1 H H221 0.938030 0.372809 0.654406 0.057 Uiso calc 0.437(5) A 1 C C23A 0.846(3) 0.3720(12) 0.7709(13) 0.0523(19) Uani d 0.437(5) A 1 C C24A 0.8551(14) 0.3465(5) 0.8502(8) 0.056(2) Uani d 0.437(5) A 1 H H241 0.795821 0.358344 0.893955 0.067 Uiso calc 0.437(5) A 1 C C25A 0.9464(10) 0.3049(4) 0.8683(6) 0.0552(18) Uani d 0.437(5) A 1 H H25A 0.948616 0.288099 0.923288 0.066 Uiso calc 0.437(5) A 1 C C26A 1.0355(8) 0.2874(3) 0.8057(6) 0.0447(16) Uani d 0.437(5) A 1 H H261 1.099738 0.258732 0.817100 0.054 Uiso calc 0.437(5) A 1 C C28A 0.7532(13) 0.4206(5) 0.7581(10) 0.059(2) Uani d 0.437(5) A 1 H H281 0.665835 0.411168 0.724009 0.089 Uiso calc 0.437(5) A 1 H H282 0.804899 0.447936 0.727597 0.089 Uiso calc 0.437(5) A 1 H H283 0.728524 0.434321 0.814542 0.089 Uiso calc 0.437(5) A 1 O O5B 1.3096(18) 0.3282(9) 0.2321(9) 0.038(2) Uani d 0.563(5) A 2 O O6B 1.4630(12) 0.2517(4) 0.3081(5) 0.0430(13) Uani d 0.563(5) A 2 H H6B 1.437641 0.272918 0.268220 0.064 Uiso calc 0.563(5) A 2 N N3B 1.1851(4) 0.28580(16) 0.6084(2) 0.0382(10) Uani d 0.563(5) A 2 N N4B 1.0894(10) 0.3200(5) 0.6092(5) 0.0395(15) Uani d 0.563(5) A 2 C C14B 1.253(2) 0.3355(7) 0.3023(9) 0.034(2) Uani d 0.563(5) A 2 C C15B 1.2916(16) 0.3040(5) 0.3807(7) 0.0325(14) Uani d 0.563(5) A 2 C C16B 1.3935(10) 0.2631(4) 0.3785(5) 0.0335(14) Uani d 0.563(5) A 2 C C17B 1.4235(7) 0.2322(3) 0.4516(4) 0.0376(13) Uani d 0.563(5) A 2 H H172 1.493150 0.204936 0.450500 0.045 Uiso calc 0.563(5) A 2 C C18B 1.3532(6) 0.2410(2) 0.5249(4) 0.0350(11) Uani d 0.563(5) A 2 H H182 1.373890 0.219341 0.574244 0.042 Uiso calc 0.563(5) A 2 C C19B 1.2507(6) 0.2814(3) 0.5287(3) 0.0314(12) Uani d 0.563(5) A 2 C C20B 1.2228(9) 0.3132(3) 0.4569(5) 0.0328(14) Uani d 0.563(5) A 2 H H202 1.156312 0.341497 0.459372 0.039 Uiso calc 0.563(5) A 2 C C21B 1.0245(7) 0.3227(3) 0.6912(4) 0.0404(13) Uani d 0.563(5) A 2 C C22B 0.9174(13) 0.3598(5) 0.6964(7) 0.0474(17) Uani d 0.563(5) A 2 H H222 0.890803 0.380898 0.647321 0.057 Uiso calc 0.563(5) A 2 C C23B 0.847(3) 0.3667(9) 0.7726(10) 0.0531(17) Uani d 0.563(5) A 2 C C24B 0.8824(11) 0.3341(4) 0.8423(6) 0.0554(18) Uani d 0.563(5) A 2 H H242 0.833196 0.337597 0.893834 0.067 Uiso calc 0.563(5) A 2 C C25B 0.9873(8) 0.2969(3) 0.8375(5) 0.0541(15) Uani d 0.563(5) A 2 H H252 1.011694 0.275187 0.886349 0.065 Uiso calc 0.563(5) A 2 C C26B 1.0593(6) 0.2902(2) 0.7617(5) 0.0465(12) Uani d 0.563(5) A 2 H H263 1.131037 0.263793 0.758446 0.056 Uiso calc 0.563(5) A 2 C C28B 0.7288(11) 0.4068(4) 0.7728(8) 0.071(2) Uani d 0.563(5) A 2 H H284 0.754429 0.434989 0.814503 0.107 Uiso calc 0.563(5) A 2 H H285 0.641172 0.389335 0.789138 0.107 Uiso calc 0.563(5) A 2 H H286 0.713613 0.422241 0.714997 0.107 Uiso calc 0.563(5) A 2 C C29 1.0163(3) 0.34748(10) 0.10760(16) 0.0412(6) Uani d 1 . . H H291 0.978564 0.362721 0.052015 0.049 Uiso calc 1 . . H H292 1.075319 0.316216 0.094748 0.049 Uiso calc 1 . . C C30 0.8923(3) 0.32999(11) 0.16058(16) 0.0429(6) Uani d 1 . . H H301 0.930799 0.315112 0.216247 0.051 Uiso calc 1 . . H H302 0.834154 0.361491 0.173503 0.051 Uiso calc 1 . . C C31 0.7970(3) 0.28867(11) 0.11466(17) 0.0444(6) Uani d 1 . . H H311 0.757029 0.303476 0.059265 0.053 Uiso calc 1 . . H H312 0.854462 0.257036 0.101545 0.053 Uiso calc 1 . . C C32 0.6759(3) 0.27222(14) 0.1699(2) 0.0600(8) Uani d 1 . . H H321 0.715235 0.256159 0.223728 0.090 Uiso calc 1 . . H H322 0.614986 0.246356 0.138249 0.090 Uiso calc 1 . . H H323 0.619406 0.303553 0.183397 0.090 Uiso calc 1 . . C C33 1.3355(3) 0.44608(11) 0.16023(18) 0.0474(6) Uani d 1 . . H H331 1.312307 0.483083 0.142993 0.057 Uiso calc 1 . . H H332 1.389692 0.447418 0.216890 0.057 Uiso calc 1 . . C C34 1.4310(3) 0.42214(11) 0.09390(18) 0.0450(6) Uani d 1 . . H H341 1.447514 0.384176 0.107854 0.054 Uiso calc 1 . . H H342 1.380992 0.424035 0.035994 0.054 Uiso calc 1 . . C C35 1.5724(3) 0.44980(13) 0.0910(2) 0.0536(7) Uani d 1 . . H H351 1.626598 0.444800 0.147116 0.064 Uiso calc 1 . . H H352 1.556030 0.488363 0.082824 0.064 Uiso calc 1 . . C C36 1.6606(3) 0.42936(15) 0.0192(2) 0.0639(8) Uani d 1 . . H H361 1.679330 0.391364 0.027768 0.096 Uiso calc 1 . . H H362 1.751182 0.448674 0.020065 0.096 Uiso calc 1 . . H H363 1.608370 0.434816 -0.036627 0.096 Uiso calc 1 . . C C37 0.9061(6) 0.5119(2) 0.5726(4) 0.149(3) Uani d 1 . . H H371 0.948957 0.493958 0.624624 0.179 Uiso calc 1 . . H H372 0.822029 0.532405 0.589114 0.179 Uiso calc 1 . . C C38 1.0160(4) 0.54900(15) 0.5328(3) 0.0857(12) Uani d 1 . . H H381 0.963940 0.572510 0.490655 0.103 Uiso calc 1 . . H H382 1.057966 0.571923 0.579548 0.103 Uiso calc 1 . . C C39 1.1321(5) 0.5243(2) 0.4897(3) 0.1039(15) Uani d 1 . . H H391 1.188027 0.552653 0.463175 0.125 Uiso calc 1 . . H H392 1.195644 0.506552 0.533944 0.125 Uiso calc 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Sn1 0.03821(10) 0.04234(12) 0.03366(10) 0.00372(7) 0.00971(7) 0.00012(7) O1 0.0486(10) 0.0441(10) 0.0349(9) 0.0126(8) 0.0111(8) 0.0026(8) O2 0.0468(10) 0.0604(12) 0.0316(9) 0.0075(9) 0.0107(8) 0.0006(8) O3 0.0548(12) 0.0512(12) 0.0307(9) 0.0075(10) 0.0120(8) 0.0062(8) N1 0.0425(12) 0.0396(12) 0.0354(11) 0.0001(9) 0.0097(9) -0.0034(9) N2 0.0390(11) 0.0406(12) 0.0368(11) -0.0005(9) 0.0098(9) -0.0027(9) C1 0.0387(13) 0.0442(14) 0.0298(12) 0.0005(11) 0.0040(10) -0.0001(10) C2 0.0351(12) 0.0407(13) 0.0305(12) -0.0014(10) 0.0043(9) -0.0033(10) C3 0.0399(13) 0.0389(13) 0.0308(12) -0.0033(10) 0.0055(10) 0.0015(10) C4 0.0506(15) 0.0387(13) 0.0352(13) 0.0013(11) 0.0045(11) 0.0046(10) C5 0.0462(15) 0.0353(13) 0.0393(14) 0.0013(11) 0.0069(11) -0.0022(11) C6 0.0376(13) 0.0374(13) 0.0334(12) -0.0039(10) 0.0084(10) -0.0028(10) C7 0.0405(13) 0.0358(13) 0.0314(12) -0.0004(10) 0.0045(10) 0.0025(9) C8 0.0368(13) 0.0404(14) 0.0342(12) -0.0040(10) 0.0065(10) -0.0051(10) C9 0.0427(14) 0.0412(14) 0.0380(13) -0.0019(11) 0.0080(11) -0.0025(11) C10 0.0423(14) 0.0505(16) 0.0406(14) -0.0029(12) 0.0087(11) -0.0089(12) C11 0.0535(17) 0.0553(17) 0.0346(13) -0.0057(13) 0.0111(12) -0.0065(12) C12 0.0578(17) 0.0490(16) 0.0360(14) -0.0013(13) 0.0070(12) 0.0023(12) C13 0.0439(14) 0.0425(15) 0.0397(14) 0.0005(11) 0.0052(11) -0.0034(11) C27 0.0598(18) 0.0632(19) 0.0541(18) 0.0109(15) 0.0194(14) -0.0048(15) O4 0.0445(10) 0.0474(11) 0.0369(9) 0.0082(8) 0.0057(8) 0.0012(8) O5A 0.031(6) 0.055(5) 0.028(4) 0.010(4) 0.008(4) 0.006(3) O6A 0.051(4) 0.051(3) 0.037(5) 0.005(3) 0.017(4) 0.011(4) N3A 0.035(4) 0.041(3) 0.033(3) 0.000(3) 0.007(3) 0.001(3) N4A 0.044(2) 0.044(2) 0.034(2) -0.004(2) 0.009(2) 0.0025(19) C14A 0.036(4) 0.039(4) 0.032(4) -0.003(4) 0.006(3) 0.002(3) C15A 0.031(4) 0.035(4) 0.035(3) -0.001(3) 0.004(3) -0.002(3) C16A 0.034(4) 0.042(3) 0.033(3) -0.004(3) 0.015(3) -0.002(3) C17A 0.035(3) 0.036(3) 0.037(4) 0.003(3) 0.011(3) 0.002(3) C18A 0.029(3) 0.030(4) 0.029(3) 0.000(3) 0.009(3) -0.002(3) C19A 0.032(3) 0.029(3) 0.032(2) 0.001(2) 0.003(2) -0.001(2) C20A 0.030(4) 0.033(4) 0.029(3) 0.004(3) 0.005(2) 0.001(2) C21A 0.037(3) 0.045(3) 0.037(4) -0.002(3) 0.007(3) -0.001(3) C22A 0.045(4) 0.053(4) 0.043(4) -0.003(3) 0.002(3) -0.009(3) C23A 0.047(3) 0.061(4) 0.050(3) -0.005(3) 0.010(3) -0.017(3) C24A 0.049(4) 0.063(5) 0.057(4) -0.006(3) 0.016(3) -0.015(4) C25A 0.058(4) 0.058(4) 0.052(4) -0.008(3) 0.023(3) -0.009(3) C26A 0.047(4) 0.049(3) 0.039(4) 0.002(3) 0.009(3) 0.000(3) C28A 0.050(4) 0.063(5) 0.067(5) 0.007(4) 0.020(3) -0.010(4) O5B 0.037(5) 0.047(4) 0.031(3) 0.002(4) 0.004(3) -0.001(3) O6B 0.046(3) 0.050(2) 0.035(3) 0.0119(19) 0.018(3) 0.009(3) N3B 0.039(2) 0.041(2) 0.0348(19) -0.0003(16) 0.0087(15) 0.0036(16) N4B 0.043(4) 0.043(3) 0.034(3) -0.003(3) 0.006(2) 0.000(2) C14B 0.034(3) 0.037(3) 0.033(3) -0.005(3) 0.005(3) -0.004(3) C15B 0.033(3) 0.037(3) 0.028(2) -0.001(2) 0.007(2) 0.000(2) C16B 0.032(3) 0.038(3) 0.032(3) -0.001(2) 0.011(2) -0.001(2) C17B 0.036(3) 0.036(3) 0.041(3) 0.000(2) 0.005(2) 0.001(2) C18B 0.035(3) 0.034(3) 0.037(3) 0.005(2) 0.005(2) 0.003(2) C19B 0.030(3) 0.033(3) 0.032(2) 0.001(2) 0.004(2) 0.002(2) C20B 0.030(3) 0.033(3) 0.036(2) 0.002(2) 0.003(2) -0.004(2) C21B 0.042(2) 0.042(3) 0.038(3) -0.008(2) 0.007(2) -0.007(2) C22B 0.044(4) 0.053(3) 0.045(3) 0.002(3) 0.004(3) -0.013(3) C23B 0.045(3) 0.065(4) 0.050(3) -0.002(3) 0.007(3) -0.018(3) C24B 0.054(4) 0.062(4) 0.052(3) -0.007(3) 0.010(3) -0.013(3) C25B 0.057(4) 0.059(3) 0.048(4) -0.002(3) 0.014(3) 0.003(3) C26B 0.048(3) 0.051(3) 0.042(3) -0.005(2) 0.010(2) 0.002(3) C28B 0.066(4) 0.086(5) 0.064(4) 0.007(4) 0.017(3) -0.013(4) C29 0.0446(14) 0.0470(15) 0.0325(12) 0.0051(11) 0.0080(10) -0.0024(11) C30 0.0454(15) 0.0493(15) 0.0345(13) 0.0006(12) 0.0077(11) -0.0012(11) C31 0.0435(14) 0.0481(15) 0.0414(14) 0.0049(12) 0.0008(11) -0.0033(12) C32 0.0463(16) 0.068(2) 0.066(2) -0.0095(14) 0.0066(14) -0.0134(16) C33 0.0475(15) 0.0461(15) 0.0491(15) -0.0055(12) 0.0080(12) -0.0029(12) C34 0.0393(14) 0.0487(15) 0.0473(15) -0.0024(12) 0.0043(11) -0.0005(12) C35 0.0438(15) 0.0635(19) 0.0539(17) -0.0032(13) 0.0059(13) 0.0034(14) C36 0.0453(17) 0.081(2) 0.067(2) 0.0053(16) 0.0131(15) 0.0117(18) C37 0.113(4) 0.210(7) 0.119(4) 0.063(5) -0.036(4) -0.073(5) C38 0.081(3) 0.069(2) 0.109(3) 0.007(2) 0.022(2) 0.003(2) C39 0.098(3) 0.125(4) 0.090(3) 0.032(3) 0.011(3) -0.001(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Sn1 O2 . . 53.93(5) y O1 Sn1 O4 . . 82.76(6) y O1 Sn1 O5A . . 135.8(3) y O1 Sn1 O5B . . 135.6(2) y O1 Sn1 C29 . . 103.65(9) y O1 Sn1 C33 . . 109.89(9) y O2 Sn1 O4 . . 136.44(6) y O2 Sn1 O5A . . 167.5(4) y O2 Sn1 O5B . . 169.5(3) y O2 Sn1 C29 . . 92.83(8) y O2 Sn1 C33 . . 87.56(9) y O4 Sn1 O5A . . 53.3(3) y O4 Sn1 O5B . . 52.9(2) y O4 Sn1 C29 . . 102.85(9) y O4 Sn1 C33 . . 105.25(9) y O5A Sn1 C29 . . 91.6(6) y O5A Sn1 C33 . . 81.4(6) y O5B Sn1 C29 . . 88.7(5) y O5B Sn1 C33 . . 84.4(5) y C29 Sn1 C33 . . 138.31(10) y C1 O1 Sn1 . . 105.49(14) ? C1 O2 Sn1 . . 81.66(14) ? C3 O3 H3 . . 105(3) ? N2 N1 C6 . . 114.6(2) ? N1 N2 C8 . . 113.7(2) ? O2 C1 O1 . . 118.9(2) ? O2 C1 C2 . . 122.0(2) ? O1 C1 C2 . . 119.07(19) ? C7 C2 C3 . . 118.7(2) ? C7 C2 C1 . . 120.8(2) ? C3 C2 C1 . . 120.6(2) ? O3 C3 C4 . . 117.3(2) ? O3 C3 C2 . . 122.9(2) ? C4 C3 C2 . . 119.8(2) ? C5 C4 C3 . . 120.9(2) ? C5 C4 H4 . . 119.5 ? C3 C4 H4 . . 119.5 ? C4 C5 C6 . . 120.0(2) ? C4 C5 H5 . . 120.0 ? C6 C5 H5 . . 120.0 ? C7 C6 C5 . . 119.5(2) ? C7 C6 N1 . . 115.8(2) ? C5 C6 N1 . . 124.7(2) ? C6 C7 C2 . . 121.1(2) ? C6 C7 H7 . . 119.4 ? C2 C7 H7 . . 119.4 ? C9 C8 C13 . . 120.1(2) ? C9 C8 N2 . . 115.6(2) ? C13 C8 N2 . . 124.3(2) ? C8 C9 C10 . . 121.4(2) ? C8 C9 H9 . . 119.3 ? C10 C9 H9 . . 119.3 ? C11 C10 C9 . . 117.5(2) ? C11 C10 C27 . . 122.2(2) ? C9 C10 C27 . . 120.3(3) ? C12 C11 C10 . . 121.3(2) ? C12 C11 H11 . . 119.4 ? C10 C11 H11 . . 119.4 ? C11 C12 C13 . . 120.7(3) ? C11 C12 H12 . . 119.6 ? C13 C12 H12 . . 119.6 ? C12 C13 C8 . . 119.0(2) ? C12 C13 H13 . . 120.5 ? C8 C13 H13 . . 120.5 ? C10 C27 H271 . . 109.5 ? C10 C27 H272 . . 109.5 ? H271 C27 H272 . . 109.5 ? C10 C27 H273 . . 109.5 ? H271 C27 H273 . . 109.5 ? H272 C27 H273 . . 109.5 ? C14B O4 Sn1 . . 108.0(5) ? C14A O4 Sn1 . . 105.1(6) ? C14A O5A Sn1 . . 73.6(12) ? C16A O6A H6A . . 109.5 ? N4A N3A C19A . . 115.7(9) ? N3A N4A C21A . . 113.1(7) ? O5A C14A O4 . . 128.0(15) ? O5A C14A C15A . . 121.5(13) ? O4 C14A C15A . . 110.0(9) ? C20A C15A C16A . . 119.0(9) ? C20A C15A C14A . . 120.6(9) ? C16A C15A C14A . . 120.3(8) ? O6A C16A C17A . . 116.3(8) ? O6A C16A C15A . . 123.1(9) ? C17A C16A C15A . . 120.6(8) ? C18A C17A C16A . . 118.7(7) ? C18A C17A H171 . . 120.6 ? C16A C17A H171 . . 120.7 ? C17A C18A C19A . . 121.8(6) ? C17A C18A H181 . . 119.1 ? C19A C18A H181 . . 119.1 ? C20A C19A C18A . . 119.7(6) ? C20A C19A N3A . . 114.9(7) ? C18A C19A N3A . . 125.4(7) ? C19A C20A C15A . . 120.1(8) ? C19A C20A H201 . . 119.9 ? C15A C20A H201 . . 119.9 ? C22A C21A C26A . . 121.5(8) ? C22A C21A N4A . . 123.1(8) ? C26A C21A N4A . . 115.4(7) ? C21A C22A C23A . . 120.2(11) ? C21A C22A H221 . . 119.9 ? C23A C22A H221 . . 119.9 ? C24A C23A C22A . . 117.5(10) ? C24A C23A C28A . . 119.9(10) ? C22A C23A C28A . . 122.1(11) ? C25A C24A C23A . . 122.8(10) ? C25A C24A H241 . . 118.6 ? C23A C24A H241 . . 118.6 ? C24A C25A C26A . . 119.6(9) ? C24A C25A H25A . . 120.2 ? C26A C25A H25A . . 120.2 ? C25A C26A C21A . . 118.4(8) ? C25A C26A H261 . . 120.8 ? C21A C26A H261 . . 120.8 ? C23A C28A H281 . . 109.5 ? C23A C28A H282 . . 109.5 ? H281 C28A H282 . . 109.5 ? C23A C28A H283 . . 109.5 ? H281 C28A H283 . . 109.5 ? H282 C28A H283 . . 109.5 ? C14B O5B Sn1 . . 84.7(9) ? C16B O6B H6B . . 109.5 ? N4B N3B C19B . . 114.4(5) ? N3B N4B C21B . . 112.5(7) ? O5B C14B O4 . . 114.3(11) ? O5B C14B C15B . . 122.5(10) ? O4 C14B C15B . . 123.1(8) ? C20B C15B C16B . . 119.4(7) ? C20B C15B C14B . . 120.1(7) ? C16B C15B C14B . . 120.5(6) ? O6B C16B C17B . . 117.4(6) ? O6B C16B C15B . . 122.8(7) ? C17B C16B C15B . . 119.7(6) ? C18B C17B C16B . . 120.2(5) ? C18B C17B H172 . . 119.9 ? C16B C17B H172 . . 119.9 ? C17B C18B C19B . . 121.2(5) ? C17B C18B H182 . . 119.4 ? C19B C18B H182 . . 119.4 ? C20B C19B C18B . . 119.0(5) ? C20B C19B N3B . . 125.8(6) ? C18B C19B N3B . . 115.3(5) ? C19B C20B C15B . . 120.5(6) ? C19B C20B H202 . . 119.7 ? C15B C20B H202 . . 119.7 ? C22B C21B C26B . . 119.6(6) ? C22B C21B N4B . . 115.5(7) ? C26B C21B N4B . . 124.9(6) ? C21B C22B C23B . . 121.1(8) ? C21B C22B H222 . . 119.5 ? C23B C22B H222 . . 119.5 ? C24B C23B C22B . . 118.9(8) ? C24B C23B C28B . . 122.8(8) ? C22B C23B C28B . . 118.1(9) ? C25B C24B C23B . . 120.4(8) ? C25B C24B H242 . . 119.8 ? C23B C24B H242 . . 119.8 ? C24B C25B C26B . . 120.9(7) ? C24B C25B H252 . . 119.6 ? C26B C25B H252 . . 119.6 ? C21B C26B C25B . . 119.1(6) ? C21B C26B H263 . . 120.5 ? C25B C26B H263 . . 120.5 ? C23B C28B H284 . . 109.5 ? C23B C28B H285 . . 109.5 ? H284 C28B H285 . . 109.5 ? C23B C28B H286 . . 109.5 ? H284 C28B H286 . . 109.5 ? H285 C28B H286 . . 109.5 ? C30 C29 Sn1 . . 110.95(16) ? C30 C29 H291 . . 109.4 ? Sn1 C29 H291 . . 109.4 ? C30 C29 H292 . . 109.4 ? Sn1 C29 H292 . . 109.4 ? H291 C29 H292 . . 108.0 ? C31 C30 C29 . . 113.1(2) ? C31 C30 H301 . . 109.0 ? C29 C30 H301 . . 109.0 ? C31 C30 H302 . . 109.0 ? C29 C30 H302 . . 109.0 ? H301 C30 H302 . . 107.8 ? C32 C31 C30 . . 111.2(2) ? C32 C31 H311 . . 109.4 ? C30 C31 H311 . . 109.4 ? C32 C31 H312 . . 109.4 ? C30 C31 H312 . . 109.4 ? H311 C31 H312 . . 108.0 ? C31 C32 H321 . . 109.5 ? C31 C32 H322 . . 109.5 ? H321 C32 H322 . . 109.5 ? C31 C32 H323 . . 109.5 ? H321 C32 H323 . . 109.5 ? H322 C32 H323 . . 109.5 ? C34 C33 Sn1 . . 114.74(18) ? C34 C33 H331 . . 108.6 ? Sn1 C33 H331 . . 108.6 ? C34 C33 H332 . . 108.6 ? Sn1 C33 H332 . . 108.6 ? H331 C33 H332 . . 107.6 ? C35 C34 C33 . . 113.1(2) ? C35 C34 H341 . . 109.0 ? C33 C34 H341 . . 109.0 ? C35 C34 H342 . . 109.0 ? C33 C34 H342 . . 109.0 ? H341 C34 H342 . . 107.8 ? C34 C35 C36 . . 112.8(3) ? C34 C35 H351 . . 109.0 ? C36 C35 H351 . . 109.0 ? C34 C35 H352 . . 109.0 ? C36 C35 H352 . . 109.0 ? H351 C35 H352 . . 107.8 ? C35 C36 H361 . . 109.5 ? C35 C36 H362 . . 109.5 ? H361 C36 H362 . . 109.5 ? C35 C36 H363 . . 109.5 ? H361 C36 H363 . . 109.5 ? H362 C36 H363 . . 109.5 ? C39 C37 C38 3_766 . 106.1(5) ? C39 C37 H371 3_766 . 110.5 ? C38 C37 H371 . . 110.5 ? C39 C37 H372 3_766 . 110.5 ? C38 C37 H372 . . 110.5 ? H371 C37 H372 . . 108.7 ? C39 C38 C37 . . 117.5(4) ? C39 C38 H381 . . 107.9 ? C37 C38 H381 . . 107.9 ? C39 C38 H382 . . 107.9 ? C37 C38 H382 . . 107.9 ? H381 C38 H382 . . 107.2 ? C37 C39 C38 3_766 . 116.0(4) ? C37 C39 H391 3_766 . 108.3 ? C38 C39 H391 . . 108.3 ? C37 C39 H392 3_766 . 108.3 ? C38 C39 H392 . . 108.3 ? H391 C39 H392 . . 107.4 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Sn1 O1 . 2.0961(16) y Sn1 O2 . 2.6252(18) y Sn1 O4 . 2.0954(17) y Sn1 O5A . 2.81(3) y Sn1 O5B . 2.60(2) y Sn1 C29 . 2.110(3) y Sn1 C33 . 2.110(3) y Sn1 O3 3_765 3.4786(17) y O1 C1 . 1.292(3) ? O2 C1 . 1.253(2) ? O3 C3 . 1.350(3) ? O3 H3 . 0.78(3) ? N1 N2 . 1.250(3) y N1 C6 . 1.429(3) ? N2 C8 . 1.433(3) ? C1 C2 . 1.469(3) ? C2 C7 . 1.400(3) ? C2 C3 . 1.406(3) ? C3 C4 . 1.392(4) ? C4 C5 . 1.371(3) ? C4 H4 . 0.9500 ? C5 C6 . 1.404(3) ? C5 H5 . 0.9500 ? C6 C7 . 1.380(3) ? C7 H7 . 0.9500 ? C8 C9 . 1.386(3) ? C8 C13 . 1.388(3) ? C9 C10 . 1.396(3) ? C9 H9 . 0.9500 ? C10 C11 . 1.389(4) ? C10 C27 . 1.504(4) ? C11 C12 . 1.382(4) ? C11 H11 . 0.9500 ? C12 C13 . 1.383(3) ? C12 H12 . 0.9500 ? C13 H13 . 0.9500 ? C27 H271 . 0.9800 ? C27 H272 . 0.9800 ? C27 H273 . 0.9800 ? O4 C14B . 1.291(4) ? O4 C14A . 1.291(4) ? O5A C14A . 1.254(4) ? O6A C16A . 1.340(9) ? O6A H6A . 0.8400 ? N3A N4A . 1.233(10) ? N3A C19A . 1.430(10) ? N4A C21A . 1.450(8) ? C14A C15A . 1.485(11) ? C15A C20A . 1.395(10) ? C15A C16A . 1.405(10) ? C16A C17A . 1.401(10) ? C17A C18A . 1.365(8) ? C17A H171 . 0.9500 ? C18A C19A . 1.393(8) ? C18A H181 . 0.9500 ? C19A C20A . 1.382(9) ? C20A H201 . 0.9500 ? C21A C22A . 1.375(10) ? C21A C26A . 1.399(9) ? C22A C23A . 1.401(11) ? C22A H221 . 0.9500 ? C23A C24A . 1.386(11) ? C23A C28A . 1.508(11) ? C24A C25A . 1.374(11) ? C24A H241 . 0.9500 ? C25A C26A . 1.390(9) ? C25A H25A . 0.9500 ? C26A H261 . 0.9500 ? C28A H281 . 0.9800 ? C28A H282 . 0.9800 ? C28A H283 . 0.9800 ? O5B C14B . 1.253(4) ? O6B C16B . 1.336(6) ? O6B H6B . 0.8400 ? N3B N4B . 1.246(8) ? N3B C19B . 1.418(6) ? N4B C21B . 1.444(8) ? C14B C15B . 1.480(8) ? C15B C20B . 1.398(8) ? C15B C16B . 1.407(8) ? C16B C17B . 1.389(8) ? C17B C18B . 1.366(7) ? C17B H172 . 0.9500 ? C18B C19B . 1.405(7) ? C18B H182 . 0.9500 ? C19B C20B . 1.383(7) ? C20B H202 . 0.9500 ? C21B C22B . 1.377(8) ? C21B C26B . 1.390(7) ? C22B C23B . 1.397(9) ? C22B H222 . 0.9500 ? C23B C24B . 1.381(9) ? C23B C28B . 1.503(10) ? C24B C25B . 1.366(9) ? C24B H242 . 0.9500 ? C25B C26B . 1.401(8) ? C25B H252 . 0.9500 ? C26B H263 . 0.9500 ? C28B H284 . 0.9800 ? C28B H285 . 0.9800 ? C28B H286 . 0.9800 ? C29 C30 . 1.529(3) ? C29 H291 . 0.9900 ? C29 H292 . 0.9900 ? C30 C31 . 1.522(4) ? C30 H301 . 0.9900 ? C30 H302 . 0.9900 ? C31 C32 . 1.521(4) ? C31 H311 . 0.9900 ? C31 H312 . 0.9900 ? C32 H321 . 0.9800 ? C32 H322 . 0.9800 ? C32 H323 . 0.9800 ? C33 C34 . 1.527(4) ? C33 H331 . 0.9900 ? C33 H332 . 0.9900 ? C34 C35 . 1.504(4) ? C34 H341 . 0.9900 ? C34 H342 . 0.9900 ? C35 C36 . 1.516(4) ? C35 H351 . 0.9900 ? C35 H352 . 0.9900 ? C36 H361 . 0.9800 ? C36 H362 . 0.9800 ? C36 H363 . 0.9800 ? C37 C39 3_766 1.360(5) ? C37 C38 . 1.546(6) ? C37 H371 . 0.9900 ? C37 H372 . 0.9900 ? C38 C39 . 1.453(5) ? C38 H381 . 0.9900 ? C38 H382 . 0.9900 ? C39 H391 . 0.9900 ? C39 H392 . 0.9900 ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag O3 H3 O2 . 0.78(3) 1.91(3) 2.623(3) 153(3) yes O3 H3 O2 3_765 0.78(3) 2.44(3) 2.872(3) 117(3) yes O6A H6A O5A . 0.84 1.90 2.62(3) 144 yes O6B H6B O5B . 0.84 1.90 2.64(2) 146 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag C6 N1 N2 C8 . . . . 179.1(2) ? Sn1 O2 C1 O1 . . . . -0.6(2) ? Sn1 O2 C1 C2 . . . . 178.0(2) ? Sn1 O1 C1 O2 . . . . 0.7(3) ? Sn1 O1 C1 C2 . . . . -177.90(18) ? O2 C1 C2 C7 . . . . 176.8(2) ? O1 C1 C2 C7 . . . . -4.6(4) ? O2 C1 C2 C3 . . . . -2.9(4) ? O1 C1 C2 C3 . . . . 175.7(2) ? C7 C2 C3 O3 . . . . -178.8(2) ? C1 C2 C3 O3 . . . . 0.9(4) ? C7 C2 C3 C4 . . . . 2.0(4) ? C1 C2 C3 C4 . . . . -178.3(2) ? O3 C3 C4 C5 . . . . 179.6(2) ? C2 C3 C4 C5 . . . . -1.1(4) ? C3 C4 C5 C6 . . . . -0.6(4) ? C4 C5 C6 C7 . . . . 1.3(4) ? C4 C5 C6 N1 . . . . -179.3(2) ? N2 N1 C6 C7 . . . . 179.8(2) ? N2 N1 C6 C5 . . . . 0.4(4) ? C5 C6 C7 C2 . . . . -0.3(4) ? N1 C6 C7 C2 . . . . -179.8(2) ? C3 C2 C7 C6 . . . . -1.3(4) ? C1 C2 C7 C6 . . . . 179.0(2) ? N1 N2 C8 C9 . . . . -176.3(2) ? N1 N2 C8 C13 . . . . 3.3(4) ? C13 C8 C9 C10 . . . . -0.3(4) ? N2 C8 C9 C10 . . . . 179.3(2) ? C8 C9 C10 C11 . . . . 0.5(4) ? C8 C9 C10 C27 . . . . -179.5(3) ? C9 C10 C11 C12 . . . . -1.1(4) ? C27 C10 C11 C12 . . . . 178.9(3) ? C10 C11 C12 C13 . . . . 1.5(4) ? C11 C12 C13 C8 . . . . -1.2(4) ? C9 C8 C13 C12 . . . . 0.6(4) ? N2 C8 C13 C12 . . . . -178.9(2) ? C19A N3A N4A C21A . . . . -179.0(10) ? Sn1 O5A C14A O4 . . . . 1(3) ? Sn1 O5A C14A C15A . . . . 173(3) ? Sn1 O4 C14A O5A . . . . -1(4) ? Sn1 O4 C14A C15A . . . . -174.0(19) ? O5A C14A C15A C20A . . . . -179(3) ? O4 C14A C15A C20A . . . . -6(4) ? O5A C14A C15A C16A . . . . 1(4) ? O4 C14A C15A C16A . . . . 174(2) ? C20A C15A C16A O6A . . . . 177.7(15) ? C14A C15A C16A O6A . . . . -3(3) ? C20A C15A C16A C17A . . . . -2(2) ? C14A C15A C16A C17A . . . . 177(2) ? O6A C16A C17A C18A . . . . -177.7(10) ? C15A C16A C17A C18A . . . . 2.4(18) ? C16A C17A C18A C19A . . . . -0.4(12) ? C17A C18A C19A C20A . . . . -1.4(11) ? C17A C18A C19A N3A . . . . 179.4(11) ? N4A N3A C19A C20A . . . . 177.4(11) ? N4A N3A C19A C18A . . . . -3.5(19) ? C18A C19A C20A C15A . . . . 1.4(16) ? N3A C19A C20A C15A . . . . -179.4(15) ? C16A C15A C20A C19A . . . . 1(2) ? C14A C15A C20A C19A . . . . -179(2) ? N3A N4A C21A C22A . . . . 0.5(16) ? N3A N4A C21A C26A . . . . -178.1(10) ? C26A C21A C22A C23A . . . . -3(3) ? N4A C21A C22A C23A . . . . 179(2) ? C21A C22A C23A C24A . . . . 3(5) ? C21A C22A C23A C28A . . . . 175(2) ? C22A C23A C24A C25A . . . . -2(4) ? C28A C23A C24A C25A . . . . -174(2) ? C23A C24A C25A C26A . . . . 1(2) ? C24A C25A C26A C21A . . . . -0.3(14) ? C22A C21A C26A C25A . . . . 1.3(15) ? N4A C21A C26A C25A . . . . 179.9(7) ? C19B N3B N4B C21B . . . . 179.3(7) ? Sn1 O5B C14B O4 . . . . -2.1(19) ? Sn1 O5B C14B C15B . . . . -180(2) ? Sn1 O4 C14B O5B . . . . 3(2) ? Sn1 O4 C14B C15B . . . . -179.5(19) ? O5B C14B C15B C20B . . . . -179(2) ? O4 C14B C15B C20B . . . . 4(3) ? O5B C14B C15B C16B . . . . -2(3) ? O4 C14B C15B C16B . . . . -179.1(18) ? C20B C15B C16B O6B . . . . 179.6(12) ? C14B C15B C16B O6B . . . . 2(2) ? C20B C15B C16B C17B . . . . 0.6(18) ? C14B C15B C16B C17B . . . . -176.8(16) ? O6B C16B C17B C18B . . . . -178.2(8) ? C15B C16B C17B C18B . . . . 0.8(13) ? C16B C17B C18B C19B . . . . -0.7(9) ? C17B C18B C19B C20B . . . . -0.9(9) ? C17B C18B C19B N3B . . . . 179.5(5) ? N4B N3B C19B C20B . . . . 4.0(10) ? N4B N3B C19B C18B . . . . -176.5(8) ? C18B C19B C20B C15B . . . . 2.3(12) ? N3B C19B C20B C15B . . . . -178.1(9) ? C16B C15B C20B C19B . . . . -2.2(17) ? C14B C15B C20B C19B . . . . 175.2(16) ? N3B N4B C21B C22B . . . . -179.9(10) ? N3B N4B C21B C26B . . . . -2.0(14) ? C26B C21B C22B C23B . . . . 3(2) ? N4B C21B C22B C23B . . . . -179(2) ? C21B C22B C23B C24B . . . . -3(4) ? C21B C22B C23B C28B . . . . -178.4(15) ? C22B C23B C24B C25B . . . . 2(3) ? C28B C23B C24B C25B . . . . 177.4(18) ? C23B C24B C25B C26B . . . . -1.3(19) ? C22B C21B C26B C25B . . . . -1.8(11) ? N4B C21B C26B C25B . . . . -179.6(8) ? C24B C25B C26B C21B . . . . 1.1(11) ? Sn1 C29 C30 C31 . . . . -179.94(18) ? C29 C30 C31 C32 . . . . 179.6(2) ? Sn1 C33 C34 C35 . . . . -174.66(19) ? C33 C34 C35 C36 . . . . -174.4(2) ? C39 C37 C38 C39 3_766 . . . -48.3(6) ? C37 C38 C39 C37 . . . 3_766 53.0(7) ? _cod_database_fobs_code 2022350