#------------------------------------------------------------------------------ #$Date: 2021-04-10 07:45:59 +0300 (Sat, 10 Apr 2021) $ #$Revision: 264028 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/23/2022350.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022350 _cell_angle_alpha 90.000 _cell_angle_beta 93.305 _cell_angle_gamma 90.000 _cell_length_a 9.4028 _cell_length_b 25.1718 _cell_length_c 15.5008 _exptl_crystal_F_000 1624.00 _reflns_d_resolution_high 0.7101 _cod_data_source_file ov3150Isup2.hkl _cod_data_source_block I _shelx_title ' TSBB-2 (L0218)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 265.89 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 745.81 854.54 16.69 o 3 0 0 6301.33 5909.13 92.38 o 4 0 0 19942.78 20132.41 253.45 o 5 0 0 9.29 -7.23 9.55 o 6 0 0 14778.31 15515.09 242.86 o 7 0 0 11271.72 10924.34 190.50 o 8 0 0 1726.00 1746.44 61.49 o 9 0 0 93.09 71.99 28.74 o 10 0 0 1577.61 1625.99 91.45 o 11 0 0 793.84 927.60 84.49 o 12 0 0 10.94 3.21 58.82 o 13 0 0 91.29 213.07 69.81 o 2 1 0 1676.62 1627.55 18.32 o 3 1 0 3279.42 3101.01 33.33 o 4 1 0 2242.34 2095.02 24.30 o 5 1 0 1380.92 1269.23 19.17 o 6 1 0 4219.02 4287.61 52.83 o 7 1 0 380.08 345.74 15.81 o 8 1 0 1548.15 1489.98 33.22 o 9 1 0 1140.96 1129.60 48.21 o 10 1 0 43.70 45.10 21.65 o 11 1 0 30.66 -23.34 30.87 o 12 1 0 42.51 94.59 38.50 o 13 1 0 90.20 164.43 62.58 o 2 2 0 6171.90 5857.24 60.83 o 3 2 0 2487.90 2532.13 26.94 o 4 2 0 1153.09 1099.43 16.76 o 5 2 0 44.90 40.09 8.75 o 6 2 0 3294.63 3370.03 42.29 o 7 2 0 2454.97 2332.84 43.41 o 8 2 0 521.45 471.07 29.38 o 9 2 0 0.38 -5.66 16.77 o 10 2 0 415.87 373.92 31.57 o 11 2 0 63.88 81.15 28.57 o 12 2 0 7.20 -14.00 36.60 o 13 2 0 17.88 -56.79 56.79 o 1 3 0 24093.76 22446.32 887.59 o 2 3 0 41944.27 42301.53 519.40 o 3 3 0 339.15 333.44 6.78 o 4 3 0 4802.82 5045.42 52.59 o 5 3 0 19753.35 20068.85 208.47 o 6 3 0 8380.61 8914.98 115.35 o 7 3 0 393.82 395.00 24.74 o 8 3 0 2093.21 2058.75 50.77 o 9 3 0 1609.45 1685.71 53.70 o 10 3 0 475.12 455.99 32.75 o 11 3 0 350.33 328.64 37.87 o 12 3 0 406.50 406.92 64.26 o 13 3 0 273.02 243.85 75.69 o 0 4 0 19817.37 17047.72 1708.87 o 1 4 0 257.48 336.06 5.05 o 2 4 0 8202.53 7804.21 69.46 o 3 4 0 14203.13 14231.44 127.86 o 4 4 0 15010.08 15670.74 146.45 o 5 4 0 3422.13 3660.40 43.59 o 6 4 0 2198.44 2202.90 44.92 o 7 4 0 3523.71 3567.81 62.47 o 8 4 0 906.23 931.93 28.52 o 9 4 0 347.85 299.24 23.89 o 10 4 0 1121.16 1253.35 53.25 o 11 4 0 347.80 346.51 34.00 o 12 4 0 39.18 -40.90 43.48 o 13 4 0 50.47 28.94 64.20 o 1 5 0 12654.52 13609.22 127.44 o 2 5 0 329.63 315.75 5.44 o 3 5 0 10556.25 10553.47 89.80 o 4 5 0 2010.61 2139.00 24.82 o 5 5 0 2806.59 3400.86 43.56 o 6 5 0 140.57 171.98 9.92 o 7 5 0 87.62 66.04 11.95 o 8 5 0 12.05 21.93 15.70 o 9 5 0 17.39 10.69 16.20 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7.61 o 4 8 0 1425.85 1465.49 19.94 o 5 8 0 4.30 15.51 7.08 o 6 8 0 28.94 37.76 7.68 o 7 8 0 211.32 195.77 11.80 o 8 8 0 18.98 9.51 12.81 o 9 8 0 403.68 451.31 26.60 o 10 8 0 103.08 62.19 24.99 o 11 8 0 27.87 42.19 35.07 o 12 8 0 10.49 48.01 47.05 o 1 9 0 13455.33 13863.95 124.43 o 2 9 0 16266.06 16086.58 141.64 o 3 9 0 5145.28 5005.04 44.57 o 4 9 0 107.83 97.57 6.56 o 5 9 0 6744.15 6651.20 75.12 o 6 9 0 3943.88 3984.48 65.03 o 7 9 0 31.34 38.19 8.54 o 8 9 0 1771.38 1978.44 46.29 o 9 9 0 502.20 549.61 28.29 o 10 9 0 186.99 199.46 31.41 o 11 9 0 143.17 158.59 35.15 o 12 9 0 219.57 251.30 53.55 o 0 10 0 6626.03 5694.67 418.22 o 1 10 0 13269.88 12841.44 117.19 o 2 10 0 3884.56 3974.44 37.48 o 3 10 0 14921.99 14784.77 135.22 o 4 10 0 2746.14 2407.57 32.09 o 5 10 0 986.48 926.21 16.91 o 6 10 0 879.85 886.40 21.57 o 7 10 0 2133.41 2136.85 37.91 o 8 10 0 771.22 731.26 28.07 o 9 10 0 365.31 293.02 28.48 o 10 10 0 776.10 772.76 43.85 o 11 10 0 599.44 530.01 62.64 o 12 10 0 111.72 92.98 47.68 o 1 11 0 640.79 563.86 10.87 o 2 11 0 6694.47 6764.32 60.63 o 3 11 0 0.51 -4.64 4.64 o 4 11 0 99.06 85.39 6.96 o 5 11 0 385.92 362.58 11.61 o 6 11 0 685.78 634.48 21.05 o 7 11 0 34.54 33.57 10.39 o 8 11 0 163.00 144.12 18.43 o 9 11 0 80.04 42.95 25.47 o 10 11 0 124.36 136.87 31.18 o 11 11 0 38.92 28.02 42.22 o 12 11 0 49.75 17.81 52.39 o 0 12 0 7959.26 7700.86 125.66 o 1 12 0 29.76 26.65 6.68 o 2 12 0 110.35 82.98 5.40 o 3 12 0 1647.34 1552.31 19.94 o 4 12 0 4571.32 4425.36 51.97 o 5 12 0 1928.49 1902.55 30.35 o 6 12 0 130.11 112.36 9.77 o 7 12 0 1139.33 1210.54 27.92 o 8 12 0 453.99 430.94 26.60 o 9 12 0 4.57 15.81 22.41 o 10 12 0 319.85 286.15 38.11 o 11 12 0 101.48 10.82 36.51 o 12 12 0 19.51 16.90 48.42 o 1 13 0 11921.87 12147.76 131.74 o 2 13 0 4136.56 3810.75 43.09 o 3 13 0 2947.03 2821.44 31.54 o 4 13 0 1759.05 1566.24 24.39 o 5 13 0 2929.27 2889.51 45.92 o 6 13 0 2631.83 2699.20 72.61 o 7 13 0 196.63 162.40 15.59 o 8 13 0 1231.90 1212.21 44.35 o 9 13 0 1002.36 979.25 44.86 o 10 13 0 356.02 306.69 44.94 o 11 13 0 127.35 70.35 42.83 o 12 13 0 358.86 277.41 56.53 o 0 14 0 3368.63 3572.20 81.33 o 1 14 0 250.57 250.28 10.28 o 2 14 0 53.10 42.38 5.53 o 3 14 0 1854.72 1837.26 25.12 o 4 14 0 484.40 496.14 13.97 o 5 14 0 354.82 354.00 12.02 o 6 14 0 196.96 157.80 8.58 o 7 14 0 1006.60 1103.53 30.08 o 8 14 0 597.02 589.96 41.72 o 9 14 0 17.33 67.02 29.30 o 10 14 0 42.98 77.07 38.06 o 11 14 0 111.46 95.23 43.76 o 12 14 0 23.24 65.60 57.43 o 1 15 0 4.48 26.29 8.36 o 2 15 0 4039.40 4165.89 66.05 o 3 15 0 140.97 135.84 8.43 o 4 15 0 1018.67 871.67 17.72 o 5 15 0 430.13 378.07 22.47 o 6 15 0 67.48 57.84 7.65 o 7 15 0 45.50 37.63 18.45 o 8 15 0 701.17 657.90 36.90 o 9 15 0 272.37 182.70 34.11 o 10 15 0 15.62 -16.76 38.45 o 11 15 0 27.55 28.08 47.13 o 0 16 0 2100.99 2323.37 64.61 o 1 16 0 5970.18 6302.98 86.93 o 2 16 0 733.00 786.79 23.57 o 3 16 0 4878.22 4895.07 66.50 o 4 16 0 2831.69 2883.21 42.57 o 5 16 0 0.38 -2.62 8.18 o 6 16 0 881.23 903.76 42.63 o 7 16 0 2279.00 2568.76 66.97 o 8 16 0 1093.80 1167.80 48.29 o 9 16 0 93.45 52.72 36.55 o 10 16 0 418.48 386.23 47.55 o 11 16 0 433.01 373.89 70.02 o 1 17 0 936.05 901.11 19.44 o 2 17 0 3176.77 3086.99 48.67 o 3 17 0 13.62 -5.96 5.96 o 4 17 0 130.24 159.20 15.52 o 5 17 0 693.65 710.11 31.75 o 6 17 0 353.13 324.75 28.76 o 7 17 0 13.99 8.12 19.27 o 8 17 0 360.88 357.27 35.35 o 9 17 0 637.67 669.04 49.96 o 10 17 0 78.88 48.87 37.85 o 11 17 0 258.23 202.98 62.38 o 0 18 0 69.80 86.95 21.24 o 1 18 0 539.28 550.28 15.57 o 2 18 0 62.44 51.28 11.80 o 3 18 0 827.66 886.99 28.04 o 4 18 0 353.99 336.16 15.01 o 5 18 0 88.59 78.05 14.05 o 6 18 0 8.71 0.06 20.80 o 7 18 0 137.30 160.02 26.91 o 8 18 0 0.44 -10.14 31.76 o 9 18 0 84.90 102.13 60.27 o 10 18 0 11.46 -16.05 48.50 o 11 18 0 35.73 141.56 79.96 o 1 19 0 642.27 661.30 18.76 o 2 19 0 5400.03 5649.85 88.90 o 3 19 0 584.41 468.13 20.40 o 4 19 0 963.67 970.54 29.13 o 5 19 0 1757.15 1909.25 46.36 o 6 19 0 1244.40 1317.40 50.02 o 7 19 0 0.48 27.94 24.23 o 8 19 0 381.04 547.84 52.75 o 9 19 0 636.85 786.31 92.34 o 10 19 0 107.14 26.19 52.76 o 11 19 0 2.71 -39.94 57.60 o 0 20 0 1964.07 1925.88 55.70 o 1 20 0 529.16 467.95 24.74 o 2 20 0 399.27 458.50 20.11 o 3 20 0 664.32 672.94 25.93 o 4 20 0 365.03 352.94 18.18 o 5 20 0 3.82 7.99 17.06 o 6 20 0 326.23 314.32 31.18 o 7 20 0 936.35 885.17 50.36 o 8 20 0 415.33 406.16 68.83 o 9 20 0 45.44 11.66 42.03 o 10 20 0 172.94 106.62 76.11 o 1 21 0 0.60 8.68 16.56 o 2 21 0 153.01 100.92 19.39 o 3 21 0 21.24 11.07 16.37 o 4 21 0 25.89 18.38 17.59 o 5 21 0 20.40 14.85 21.66 o 6 21 0 229.28 239.59 34.50 o 7 21 0 1.71 8.40 31.78 o 8 21 0 44.68 5.54 42.70 o 9 21 0 11.05 -27.85 72.09 o 10 21 0 0.52 -11.73 92.88 o 0 22 0 438.27 367.39 27.91 o 1 22 0 1999.41 2038.83 50.96 o 2 22 0 63.83 31.14 14.45 o 3 22 0 704.37 739.69 33.11 o 4 22 0 1316.25 1401.63 49.64 o 5 22 0 15.16 34.37 28.37 o 6 22 0 143.98 137.68 30.55 o 7 22 0 611.13 549.80 45.06 o 8 22 0 154.57 154.90 50.02 o 9 22 0 33.53 69.96 67.01 o 10 22 0 104.79 34.14 83.88 o 1 23 0 91.53 85.57 18.68 o 2 23 0 2679.18 3113.43 68.74 o 3 23 0 197.16 213.81 27.52 o 4 23 0 214.57 197.98 27.83 o 5 23 0 1373.78 1469.05 63.57 o 6 23 0 669.85 793.51 50.45 o 7 23 0 68.28 37.62 40.92 o 8 23 0 215.91 255.55 67.14 o 9 23 0 428.52 344.53 74.45 o 10 23 0 57.19 -81.48 81.48 o 0 24 0 639.89 656.24 46.39 o 1 24 0 120.38 91.25 18.89 o 2 24 0 26.41 45.16 20.43 o 3 24 0 0.37 9.78 27.24 o 4 24 0 132.89 115.19 26.62 o 5 24 0 95.78 -3.03 26.71 o 6 24 0 5.84 -20.32 32.06 o 7 24 0 0.68 78.13 41.02 o 8 24 0 67.92 36.96 68.08 o 9 24 0 0.43 -6.72 64.34 o 1 25 0 67.89 67.12 20.59 o 2 25 0 441.72 562.08 35.28 o 3 25 0 27.00 20.81 22.92 o 4 25 0 48.00 57.69 28.20 o 5 25 0 707.57 854.33 59.93 o 6 25 0 135.49 155.70 38.50 o 7 25 0 24.40 -72.76 72.76 o 8 25 0 50.74 9.21 76.25 o 9 25 0 118.37 282.25 83.51 o 0 26 0 1483.72 1646.90 73.59 o 1 26 0 991.58 990.76 44.62 o 2 26 0 0.25 10.71 22.18 o 3 26 0 1733.90 2002.02 70.91 o 4 26 0 1051.16 1038.94 77.25 o 5 26 0 74.57 -9.49 38.17 o 6 26 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2 31 0 141.90 100.29 48.11 o 3 31 0 19.20 22.34 49.07 o 4 31 0 0.09 14.46 49.88 o 5 31 0 11.79 9.66 59.83 o 6 31 0 0.65 -56.97 75.12 o 0 32 0 112.05 125.12 53.12 o 1 32 0 292.16 208.33 56.22 o 2 32 0 128.97 85.55 53.79 o 3 32 0 1045.30 1068.11 107.16 o 4 32 0 137.81 210.50 66.36 o 5 32 0 7.50 45.61 70.75 o 1 33 0 258.48 183.54 67.15 o 2 33 0 401.14 409.49 106.67 o 3 33 0 32.89 -33.99 77.87 o 4 33 0 82.20 69.82 81.83 o 1 34 0 2.25 89.53 128.80 o 2 34 0 5.95 -59.69 69.86 o 3 34 0 1.64 29.40 60.32 o 2 35 0 326.95 246.85 171.07 o -13 1 1 23.78 31.88 55.45 o -12 1 1 348.12 389.22 41.80 o -11 1 1 1097.80 1225.77 52.08 o -10 1 1 92.70 101.96 27.28 o -9 1 1 1702.54 1537.14 44.78 o -8 1 1 3129.77 3176.99 52.91 o -7 1 1 2362.87 2515.63 37.25 o -6 1 1 1428.06 1297.89 24.90 o -5 1 1 6039.65 5439.00 65.36 o -4 1 1 8465.88 8386.80 84.42 o -3 1 1 449.46 455.74 8.98 o -2 1 1 12808.04 13433.85 148.17 o 2 1 1 29178.99 27128.32 266.36 o 3 1 1 653.50 536.71 9.00 o 4 1 1 197.04 178.84 7.33 o 5 1 1 8009.34 8400.85 94.30 o 6 1 1 8649.12 8821.34 108.08 o 7 1 1 4167.13 4401.90 76.50 o 8 1 1 1167.55 1051.52 32.01 o 9 1 1 1127.81 1111.76 37.08 o 10 1 1 589.74 542.21 34.13 o 11 1 1 43.55 -14.32 39.24 o 12 1 1 490.51 407.81 57.91 o 13 1 1 39.97 -73.74 73.74 o -13 2 1 188.61 218.78 59.63 o -12 2 1 212.19 184.09 36.57 o -11 2 1 271.83 242.54 36.79 o -10 2 1 1455.61 1469.28 56.71 o -9 2 1 685.00 729.94 30.89 o -8 2 1 16.13 23.84 10.27 o -7 2 1 5080.38 5150.22 66.99 o -6 2 1 8341.14 7973.49 94.85 o -5 2 1 3718.26 3545.30 43.19 o -4 2 1 5222.72 5296.54 52.26 o -3 2 1 18119.04 17697.95 177.00 o -2 2 1 4102.67 3825.60 40.13 o -1 2 1 22.71 13.31 2.13 o 1 2 1 8036.49 6203.40 481.38 o 2 2 1 170.14 134.79 3.70 o 3 2 1 1899.36 1756.09 19.14 o 4 2 1 8799.04 8279.94 83.83 o 5 2 1 3039.98 2995.25 40.26 o 6 2 1 1794.58 1641.78 30.96 o 7 2 1 3955.17 4252.19 66.95 o 8 2 1 4242.92 4712.76 84.21 o 9 2 1 363.40 380.25 27.03 o 10 2 1 342.46 319.75 27.92 o 11 2 1 754.74 754.60 62.78 o 12 2 1 161.87 110.74 48.86 o 13 2 1 68.58 22.31 61.68 o -13 3 1 13.62 30.72 62.59 o -12 3 1 202.38 132.19 39.03 o -11 3 1 53.99 -2.85 32.55 o -10 3 1 56.34 30.50 23.60 o -9 3 1 187.80 188.95 23.79 o -8 3 1 1169.37 1083.03 43.73 o -7 3 1 430.92 418.57 15.65 o -6 3 1 150.33 182.25 11.09 o -5 3 1 2999.72 3072.81 38.72 o -4 3 1 1824.45 1803.13 21.31 o -3 3 1 585.63 554.42 9.04 o -2 3 1 11122.22 10642.79 105.56 o -1 3 1 19122.85 17138.72 188.97 o 0 3 1 5626.74 2753.14 415.65 o 1 3 1 503.78 800.22 8.50 o 2 3 1 519.19 616.61 9.92 o 3 3 1 295.69 311.35 7.08 o 4 3 1 102.11 83.13 6.30 o 5 3 1 28.48 30.17 7.62 o 6 3 1 976.55 924.71 23.04 o 7 3 1 0.71 0.09 11.58 o 8 3 1 534.46 612.11 31.97 o 9 3 1 237.64 230.48 23.15 o 10 3 1 8.39 -4.17 21.12 o 11 3 1 52.88 71.58 29.57 o 12 3 1 64.07 63.76 44.78 o 13 3 1 56.02 130.90 58.67 o -13 4 1 149.50 118.48 56.18 o -12 4 1 26.46 35.75 37.88 o -11 4 1 412.19 358.45 33.83 o -10 4 1 956.34 1010.55 47.73 o -9 4 1 439.65 464.03 27.77 o -8 4 1 34.91 44.62 17.45 o -7 4 1 3798.60 3734.07 60.13 o 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