#------------------------------------------------------------------------------
#$Date: 2021-04-10 07:45:59 +0300 (Sat, 10 Apr 2021) $
#$Revision: 264028 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/23/2022352.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022352
loop_
_publ_author_name
'Linden, Anthony'
'Basu Baul, Tushar S.'
_publ_section_title
;
Structural diversity among some dialkyltin(IV) benzoate and related
derivatives
;
_journal_coeditor_code OV3150
_journal_issue 5
_journal_name_full 'Acta Crystallographica Section C'
_journal_page_first
;
;
_journal_paper_doi 10.1107/S2053229621003545
_journal_volume 77
_journal_year 2021
_chemical_formula_iupac
'[Sn (C7 H7)2 (C12 H12 N O3)2 (H2 O)], 2C6 H6'
_chemical_formula_moiety 'C38 H40 N2 O7 Sn, 2(C6 H6)'
_chemical_formula_sum 'C50 H52 N2 O7 Sn'
_chemical_formula_weight 911.62
_chemical_name_systematic
'Aquadibenzylbis(4-{(E)-[(Z)-4-hydroxypent-3-en-2-ylidene]amino}benzoato)tin(IV) benzene disolvate'
_space_group_crystal_system monoclinic
_space_group_IT_number 15
_space_group_name_Hall '-C 2yc'
_space_group_name_H-M_alt 'C 1 2/c 1'
_atom_sites_solution_hydrogens mixed
_atom_sites_solution_primary heavy
_atom_sites_solution_secondary difmap
_audit_creation_method SHELXL-2018/3
_cell_angle_alpha 90
_cell_angle_beta 115.0715(12)
_cell_angle_gamma 90
_cell_formula_units_Z 4
_cell_length_a 23.6530(5)
_cell_length_b 10.1034(2)
_cell_length_c 20.5952(4)
_cell_measurement_reflns_used 125492
_cell_measurement_temperature 160(2)
_cell_measurement_theta_max 30.0
_cell_measurement_theta_min 2.0
_cell_volume 4458.02(16)
_computing_cell_refinement
;
DENZO-SMN (Otwinowski & Minor, 1997)
;
_computing_data_collection
;
COLLECT (Nonius, 2000)
;
_computing_data_reduction
;
DENZO-SMN and SCALEPACK (Otwinowski & Minor, 1997)
;
_computing_molecular_graphics
;
ORTEPII (Johnson, 1976)
;
_computing_publication_material
;
SHELXL2018 (Sheldrick, 2015), Mercury (Macrae et al.,
2020) and PLATON
(Spek, 2020)
;
_computing_structure_refinement
;
SHELXL2018 (Sheldrick, 2015)
;
_computing_structure_solution
;
PATTY and DIRDIF94 (Beurskens et al., 1992, 1994)
;
_diffrn_ambient_temperature 160(2)
_diffrn_detector '65 mm CCD camera on \k goniostat'
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type 'Nonius KappaCCD area detector'
_diffrn_measurement_method '\w scans with \k offsets'
_diffrn_radiation_monochromator 'horizontally mounted graphite crystal'
_diffrn_radiation_source 'Nonius FR590 sealed tube generator'
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.1006
_diffrn_reflns_av_unetI/netI 0.0547
_diffrn_reflns_limit_h_max 32
_diffrn_reflns_limit_h_min -32
_diffrn_reflns_limit_k_max 14
_diffrn_reflns_limit_k_min -14
_diffrn_reflns_limit_l_max 29
_diffrn_reflns_limit_l_min -28
_diffrn_reflns_number 58583
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 30.032
_diffrn_reflns_theta_min 2.183
_diffrn_standards_decay_% 0
_diffrn_standards_number 0
_exptl_absorpt_coefficient_mu 0.627
_exptl_absorpt_correction_T_max 0.943
_exptl_absorpt_correction_T_min 0.753
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SORTAV; Blessing, 1995)
;
_exptl_crystal_colour colorless
_exptl_crystal_density_diffrn 1.358
_exptl_crystal_description tablet
_exptl_crystal_F_000 1888
_exptl_crystal_size_max 0.25
_exptl_crystal_size_mid 0.22
_exptl_crystal_size_min 0.10
_platon_squeeze_details 'see _refine_special_details'
_refine_diff_density_max 1.063
_refine_diff_density_min -2.173
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.047
_refine_ls_hydrogen_treatment mixed
_refine_ls_matrix_type full
_refine_ls_number_parameters 228
_refine_ls_number_reflns 6506
_refine_ls_number_restraints 2
_refine_ls_restrained_S_all 1.047
_refine_ls_R_factor_all 0.0765
_refine_ls_R_factor_gt 0.0559
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0943P)^2^+4.7027P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1370
_refine_ls_wR_factor_ref 0.1483
_reflns_number_gt 5193
_reflns_number_total 6506
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file ov3150sup1.cif
_cod_data_source_block III
_cod_original_sg_symbol_H-M 'C 2/c'
_cod_database_code 2022352
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
-32 0 8 32.03 8.40
-32 0 9 2.79 6.79
-32 0 9 -5.11 5.84
-32 0 10 28.24 6.94
-32 0 10 25.82 7.27
-32 0 11 5.23 5.72
-32 0 11 -8.48 8.00
-32 0 12 28.59 8.97
-32 0 12 25.91 7.66
-32 0 13 -0.48 6.42
-32 0 13 9.97 6.69
-32 0 14 37.46 7.30
-32 0 14 17.21 7.40
-32 0 15 10.82 5.35
-32 0 15 -3.15 6.55
-32 0 16 30.17 6.33
-32 0 17 0.97 6.08
-32 0 18 17.53 5.84
-32 0 19 6.34 5.97
-32 2 6 21.39 8.07
-32 2 6 14.50 6.36
-32 2 7 8.26 5.97
-32 2 7 11.36 6.60
-32 2 8 24.58 6.21
-32 2 8 23.31 8.42
-32 -2 9 -0.24 6.85
-32 2 9 1.01 5.42
-32 2 9 0.00 6.70
-32 2 10 14.53 5.39
-32 2 10 6.69 6.33
-32 -2 10 19.95 6.24
-32 2 10 10.35 6.33
-32 2 11 17.50 6.68
-32 -2 11 7.22 5.39
-32 2 11 12.16 6.93
-32 -2 12 20.21 5.88
-32 2 12 9.46 6.07
-32 2 12 7.41 6.20
-32 2 13 -4.00 5.94
-32 -2 13 1.84 4.90
-32 2 13 6.44 6.19
-32 2 14 21.50 7.77
-32 -2 14 15.69 5.76
-32 2 14 8.35 6.17
-32 -2 15 0.98 6.25
-32 2 15 3.02 5.80
-32 -2 16 7.85 6.01
-32 2 16 16.77 6.51
-32 2 17 28.11 6.14
-32 2 18 0.98 4.54
-31 1 3 27.22 7.67
-31 1 4 -1.41 5.75
-31 1 4 -3.41 5.97
-31 1 5 30.14 6.90
-31 1 5 35.34 7.43
-31 -1 5 31.65 7.30
-31 1 6 -1.34 6.09
-31 -1 6 -0.97 5.84
-31 1 6 0.89 5.22
-31 1 6 2.80 7.05
-31 1 7 19.32 6.81
-31 -1 7 23.25 6.82
-31 1 7 18.75 6.94
-31 1 7 27.93 5.97
-31 1 8 2.55 5.83
-31 -1 8 0.00 5.72
-31 1 8 -17.03 6.81
-31 1 9 26.13 6.44
-31 1 9 24.40 6.92
-31 -1 9 39.81 7.18
-31 -1 10 -5.84 5.11
-31 1 10 3.64 5.59
-31 1 10 -2.06 5.70
-31 -1 11 7.06 5.36
-31 -1 11 16.42 6.52
-31 1 11 14.44 6.31
-31 1 11 8.98 6.55
-31 1 12 8.85 5.70
-31 -1 12 2.80 6.33
-31 1 12 14.80 6.55
-31 -1 12 5.55 6.28
-31 -1 13 51.76 7.80
-31 -1 13 66.44 8.70
-31 1 13 39.24 7.39
-31 1 13 69.77 8.98
-31 1 14 1.09 6.31
-31 -1 14 7.55 4.87
-31 1 14 5.57 5.08
-31 -1 14 -3.63 6.29
-31 1 15 28.07 7.29
-31 -1 15 48.02 6.95
-31 1 15 22.13 5.81
-31 -1 15 33.39 7.86
-31 1 16 13.02 6.81
-31 -1 16 8.11 6.66
-31 1 16 13.18 5.68
-31 -1 16 3.90 5.73
-31 1 17 -1.46 6.46
-31 1 17 12.81 6.28
-31 -1 17 5.61 4.51
-31 -1 17 3.03 6.43
-31 1 18 -2.66 4.83
-31 1 18 -9.28 6.47
-31 -1 18 3.91 5.25
-31 -1 18 -0.61 6.07
-31 -1 19 8.80 5.62
-31 1 19 -12.21 4.71
-31 1 20 4.23 6.17
-31 -1 20 2.81 5.14
-31 3 4 2.67 6.35
-31 3 4 3.93 6.87
-31 3 5 -3.31 5.86
-31 3 5 11.04 6.62
-31 3 6 35.29 7.47
-31 3 6 32.10 8.21
-31 -3 6 39.90 8.59
-31 3 7 6.00 6.73
-31 3 7 6.13 5.75
-31 3 7 14.19 6.36
-31 -3 7 3.07 5.53
-31 3 8 9.28 6.35
-31 3 8 12.09 6.47
-31 -3 8 9.09 5.28
-31 -3 9 29.86 6.64
-31 3 9 30.48 7.31
-31 3 9 32.19 7.44
-31 3 10 18.77 6.09
-31 3 10 13.99 6.33
-31 -3 10 23.11 6.51
-31 3 10 9.37 6.82
-31 3 11 15.41 7.77
-31 3 11 14.35 7.05
-31 -3 11 11.31 5.29
-31 -3 12 11.68 6.64
-31 3 12 10.81 6.56
-31 3 12 5.81 5.93
-31 3 13 59.19 8.82
-31 -3 13 47.12 7.14
-31 3 13 42.12 8.13
-31 -3 14 25.10 6.65
-31 3 14 25.43 6.63
-31 3 14 17.72 8.13
-31 3 15 3.37 5.29
-31 -3 15 5.91 5.29
-31 3 15 2.43 6.44
-31 3 16 2.52 5.64
-31 -3 16 2.46 5.54
-31 3 16 -1.82 6.32
-31 -3 17 8.49 5.17
-31 3 17 11.49 5.86
-31 3 18 8.37 5.17
-31 3 19 -2.83 4.43
-31 5 9 0.61 7.82
-31 5 9 5.88 6.39
-31 5 10 11.90 5.50
-31 -5 10 13.15 5.89
-31 5 10 17.30 8.40
-31 5 11 6.56 7.77
-31 -5 11 14.27 5.76
-31 5 12 22.78 6.26
-31 5 13 -1.13 4.88
-31 5 14 31.00 6.88
-30 0 0 40.96 8.99
-30 0 1 -11.95 6.43
-30 0 1 1.46 6.80
-30 0 2 85.90 10.45
-30 0 3 -7.41 6.07
-30 0 4 5.59 5.83
-30 0 5 -1.21 5.34
-30 0 6 -1.82 5.83
-30 0 7 -0.36 5.22
-30 0 7 1.33 5.93
-30 0 8 36.29 6.80
-30 0 8 9.79 7.38
-30 0 9 -4.37 4.73
-30 0 9 -7.38 5.80
-30 0 10 58.40 8.46
-30 0 10 73.01 8.49
-30 0 11 8.24 6.43
-30 0 11 4.60 5.80
-30 0 12 29.82 6.67
-30 0 12 26.38 6.65
-30 0 13 -7.63 5.57
-30 0 13 -1.58 5.94
-30 0 14 32.71 6.42
-30 0 14 31.26 6.91
-30 0 15 7.89 6.07
-30 0 15 0.97 4.48
-30 0 16 74.47 9.72
-30 0 16 80.10 8.24
-30 0 17 3.03 5.45
-30 0 17 5.96 6.21
-30 0 18 -5.61 6.22
-30 0 18 1.58 4.49
-30 0 19 4.64 6.23
-30 0 19 -1.09 5.22
-30 0 20 24.78 5.34
-30 0 20 26.53 7.95
-30 0 21 4.13 5.11
-30 0 22 7.91 5.23
-30 2 1 0.51 6.61
-30 2 1 18.94 7.58
-30 2 2 7.14 7.01
-30 -2 2 18.75 6.94
-30 2 2 9.65 7.09
-30 -2 3 2.07 5.85
-30 2 3 7.07 5.49
-30 2 3 15.46 6.01
-30 2 3 10.99 6.72
-30 2 4 36.86 7.17
-30 -2 4 22.18 8.29
-30 2 4 31.50 7.69
-30 2 4 40.85 7.07
-30 2 5 6.22 5.36
-30 2 5 4.76 5.86
-30 -2 5 5.24 5.85
-30 2 6 20.35 7.19
-30 2 6 32.92 6.53
-30 -2 6 16.82 6.34
-30 2 6 35.10 8.29
-30 2 7 6.33 5.72
-30 2 7 -4.99 4.99
-30 -2 7 2.93 5.49
-30 2 7 4.99 5.24
-30 2 8 22.26 6.33
-30 2 8 11.73 6.25
-30 -2 8 11.10 6.58
-30 2 8 16.78 6.32
-30 -2 9 14.03 6.71
-30 2 9 21.31 6.09
-30 2 9 5.83 5.59
-30 2 9 10.57 7.04
-30 2 10 48.83 8.02
-30 -2 10 50.62 7.20
-30 2 10 41.23 6.79
-30 -2 11 0.00 4.76
-30 2 11 7.36 4.37
-30 2 11 4.24 5.45
-30 2 11 -0.85 5.46
-30 2 12 9.10 6.31
-30 -2 12 15.38 5.13
-30 2 12 19.82 6.16
-30 2 13 0.24 5.95
-30 2 13 6.76 5.55
-30 -2 13 2.93 5.25
-30 2 14 21.44 7.11
-30 2 14 27.33 7.41
-30 -2 14 34.67 7.10
-30 -2 14 14.78 4.76
-30 -2 15 5.42 7.83
-30 2 15 8.06 6.61
-30 2 15 22.62 6.93
-30 -2 15 11.24 5.38
-30 2 16 12.91 6.94
-30 2 16 1.56 6.37
-30 -2 16 -1.09 6.39
-30 -2 16 -0.24 3.91
-30 -2 17 -1.69 7.48
-30 -2 17 3.55 4.89
-30 2 17 3.42 6.59
-30 2 17 2.16 5.04
-30 2 18 10.03 6.48
-30 -2 18 3.14 6.52
-30 -2 18 9.06 5.02
-30 2 18 5.27 5.39
-30 -2 19 6.53 6.53
-30 2 19 -1.84 6.50
-30 2 19 1.32 4.55
-30 -2 19 4.65 4.65
-30 2 20 14.60 6.46
-30 -2 20 15.79 4.90
-30 -2 21 3.92 4.77
-30 2 21 9.34 5.51
-30 4 3 21.93 7.15
-30 4 3 25.36 7.70
-30 4 3 21.57 8.50
-30 4 4 -4.80 6.77
-30 4 4 -9.97 6.53
-30 4 4 -12.92 5.95
-30 4 5 2.09 8.24
-30 4 5 -10.82 6.52
-30 4 5 4.70 5.85
-30 -4 5 1.11 6.06
-30 4 6 7.37 6.88
-30 4 6 4.42 6.02
-30 -4 6 -9.40 7.17
-30 4 6 7.01 5.74
-30 4 7 12.62 8.09
-30 -4 7 24.86 6.19
-30 4 7 18.67 7.29
-30 4 7 38.10 7.11
-30 4 8 13.07 5.25
-30 4 8 12.71 5.99
-30 4 8 0.86 6.11
-30 -4 8 3.71 5.07
-30 4 9 38.30 7.56
-30 -4 9 40.10 7.67
-30 4 9 25.24 7.92
-30 4 10 10.63 6.02
-30 4 10 -0.61 6.20
-30 4 10 9.85 6.93
-30 -4 10 6.19 5.32
-30 4 11 40.87 7.76
-30 -4 11 41.22 6.32
-30 4 11 29.38 7.16
-30 4 12 9.58 7.15
-30 4 12 2.41 4.31
-30 4 12 -0.97 6.05
-30 -4 12 -0.99 5.57
-30 4 13 15.39 6.30
-30 4 13 0.60 5.54
-30 -4 13 5.32 5.20
-30 -4 14 23.39 5.08
-30 4 14 18.50 7.21
-30 4 14 9.33 6.30
-30 -4 15 11.01 5.20
-30 4 15 4.37 7.40
-30 4 15 9.46 7.30
-30 4 16 0.84 6.45
-30 4 16 2.67 6.07
-30 -4 16 8.04 4.95
-30 -4 17 6.18 4.45
-30 4 17 18.80 6.90
-30 -4 18 -0.49 4.20
-30 4 18 2.85 5.70
-30 4 19 13.43 4.31
-30 6 9 18.29 7.32
-30 -6 9 18.49 7.22
-30 6 9 18.61 5.86
-30 -6 10 6.58 6.33
-30 6 10 11.90 5.25
-30 6 10 10.45 6.56
-30 -6 11 18.73 6.45
-30 6 11 14.41 6.78
-30 -6 12 1.90 4.68
-30 6 12 -6.40 6.40
-30 6 13 16.03 6.06
-29 1 -2 10.44 7.16
-29 -1 -1 27.14 7.51
-29 1 -1 39.96 7.90
-29 1 -1 45.38 8.82
-29 1 0 14.99 6.92
-29 1 0 21.99 7.05
-29 -1 0 24.61 7.27
-29 1 1 50.43 8.39
-29 1 1 29.52 7.83
-29 -1 1 32.62 8.00
-29 -1 2 5.34 6.06
-29 1 2 2.43 5.95
-29 1 2 -1.16 5.78
-29 1 3 27.15 6.82
-29 1 3 26.00 6.80
-29 -1 3 27.78 6.79
-29 1 4 -2.79 5.22
-29 1 4 5.27 5.53
-29 -1 4 9.10 7.04
-29 1 4 -0.73 4.97
-29 1 5 15.51 5.57
-29 1 5 10.81 5.71
-29 -1 5 9.83 5.94
-29 1 6 -1.21 5.10
-29 -1 6 1.58 5.22
-29 1 6 8.00 6.54
-29 1 6 2.56 4.61
-29 -1 7 14.80 5.46
-29 1 7 10.30 5.57
-29 1 7 13.10 5.82
-29 1 7 15.83 5.23
-29 1 8 5.57 6.18
-29 1 8 -1.02 3.93
-29 -1 8 4.25 5.09
-29 1 8 -3.51 4.85
-29 -1 9 47.31 6.98
-29 -1 9 33.84 6.19
-29 1 9 39.48 6.66
-29 1 9 30.86 5.42
-29 1 9 28.45 7.27
-29 -1 10 3.25 5.30
-29 -1 10 3.15 4.73
-29 1 10 3.99 4.84
-29 1 10 -3.63 4.72
-29 1 11 44.60 7.01
-29 -1 11 46.46 6.43
-29 -1 11 37.35 6.75
-29 1 11 49.79 6.66
-29 1 12 4.11 4.47
-29 -1 12 -4.61 4.12
-29 -1 12 9.40 5.79
-29 1 12 -3.15 5.58
-29 1 13 144.51 10.38
-29 -1 13 142.14 11.47
-29 1 13 123.37 11.16
-29 -1 13 153.12 10.68
-29 1 14 25.79 5.54
-29 -1 14 21.50 6.40
-29 -1 14 26.94 4.98
-29 1 14 8.14 5.95
-29 1 15 14.93 5.18
-29 1 15 20.31 6.32
-29 -1 15 5.46 5.22
-29 -1 15 8.59 7.14
-29 1 16 -1.71 5.36
-29 1 16 4.57 4.21
-29 -1 16 1.58 3.77
-29 -1 16 -0.97 5.57
-29 1 17 12.45 5.86
-29 1 17 3.85 4.45
-29 -1 17 -3.40 4.74
-29 -1 17 5.09 6.18
-29 1 18 15.04 6.85
-29 -1 18 6.57 4.01
-29 1 18 -2.29 5.17
-29 -1 18 -0.36 6.19
-29 1 19 17.03 6.74
-29 -1 19 11.19 6.32
-29 1 19 19.73 6.13
-29 -1 19 8.16 4.63
-29 -1 20 4.50 5.96
-29 1 20 -2.46 6.02
-29 1 20 6.62 4.33
-29 -1 20 4.75 4.51
-29 1 21 32.51 6.50
-29 -1 21 39.62 5.97
-29 1 21 26.08 7.63
-29 -1 21 34.36 7.80
-29 -1 22 16.46 7.07
-29 1 22 0.84 5.42
-29 1 22 3.45 6.41
-29 -1 22 3.66 4.27
-29 -1 23 15.13 4.76
-29 1 23 23.41 5.07
-29 3 0 8.21 7.11
-29 3 0 9.59 7.19
-29 3 1 21.52 7.09
-29 -3 1 9.41 6.36
-29 3 1 15.39 6.60
-29 3 1 0.37 6.74
-29 3 2 2.08 6.37
-29 3 2 21.59 6.86
-29 -3 2 17.73 6.60
-29 3 2 10.15 5.01
-29 3 3 -7.26 5.61
-29 -3 3 5.63 5.75
-29 3 3 1.35 6.24
-29 3 3 6.24 5.14
-29 3 4 30.22 7.59
-29 3 4 39.74 7.41
-29 3 4 29.85 6.48
-29 -3 4 33.77 7.10
-29 3 5 3.18 5.99
-29 -3 5 -3.55 5.14
-29 3 5 -11.40 5.38
-29 3 5 -4.52 5.13
-29 3 6 9.04 5.37
-29 -3 6 18.73 5.88
-29 3 6 14.65 5.98
-29 3 7 33.03 7.07
-29 -3 7 34.29 6.37
-29 3 7 24.40 6.04
-29 3 7 14.76 6.10
-29 3 8 21.07 5.97
-29 3 8 17.28 6.45
-29 -3 8 13.96 5.88
-29 3 9 31.81 6.68
-29 3 9 32.28 6.53
-29 -3 9 34.92 6.98
-29 3 9 17.64 6.32
-29 -3 10 12.01 4.78
-29 3 10 19.02 6.30
-29 3 10 23.81 6.20
-29 3 10 5.87 5.48
-29 3 11 40.06 7.16
-29 3 11 56.08 8.10
-29 3 11 38.00 5.57
-29 -3 11 29.42 6.50
-29 3 12 20.27 6.07
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3 -9 1 68.00 6.05
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3 9 2 54.20 5.11
3 -9 2 49.57 4.24
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3 9 5 33.13 5.18
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3 -9 7 19.30 2.93
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3 -9 8 73.52 4.89
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3 9 9 22.93 4.91
3 -9 9 33.39 3.80
3 9 10 12.59 4.44
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3 9 11 8.14 4.31
3 9 11 16.82 5.16
3 9 12 48.32 6.82
3 9 12 45.05 6.88
3 9 13 41.34 6.45
3 9 13 30.07 6.01
3 9 14 21.60 6.09
3 9 14 19.50 7.36
3 9 15 10.97 5.84
3 9 15 14.26 7.01
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3 9 16 9.53 7.27
3 9 16 20.98 6.13
3 9 16 8.45 6.73
3 9 17 9.04 6.07
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3 9 17 0.37 6.85
3 9 18 -0.12 6.06
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4 0 1 3.03 1.17
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4 0 6 941.68 34.20
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10 0 2 579.55 24.03
10 0 2 537.80 23.44
10 0 2 585.10 21.27
10 0 3 -2.82 1.69
10 0 3 -4.18 2.39
10 0 3 -4.59 1.69
10 0 3 -1.86 1.28
10 0 4 606.22 22.36
10 0 4 585.35 26.22
10 0 4 580.99 22.50
10 0 4 574.51 20.84
10 0 5 0.34 1.93
10 0 5 3.62 2.53
10 0 5 4.81 2.76
10 0 5 -1.16 1.28
10 0 6 169.07 8.76
10 0 6 150.26 9.24
10 0 6 183.07 7.92
10 0 7 -5.23 2.05
10 0 7 3.46 2.51
10 0 7 -0.58 1.40
10 0 7 2.68 2.56
10 0 8 82.37 5.81
10 0 8 100.78 6.68
10 0 8 68.10 3.85
10 0 8 62.51 5.36
10 0 9 -0.91 2.39
10 0 9 0.12 2.97
10 0 9 1.98 1.40
10 0 9 1.46 3.28
10 0 10 270.17 12.99
10 0 10 195.97 14.22
10 0 10 266.95 11.11
10 0 10 267.90 11.88
10 0 11 0.68 2.84
10 0 11 6.37 3.42
10 0 11 -0.82 1.28
10 0 11 -1.69 2.29
10 0 12 31.70 4.32
10 0 12 30.40 3.77
10 0 12 24.36 4.71
10 0 12 33.91 2.34
10 0 12 29.47 3.83
10 0 13 -4.54 3.97
10 0 13 -1.88 2.58
10 0 13 1.30 1.30
10 0 13 -2.81 1.05
10 0 13 0.71 2.62
10 0 14 144.34 9.31
10 0 14 111.67 8.67
10 0 14 132.96 8.53
10 0 15 1.70 3.85
10 0 15 -0.82 3.85
10 0 15 -3.18 3.06
10 0 16 17.23 4.45
10 0 16 25.68 6.00
10 0 16 23.97 4.31
10 0 16 24.34 5.03
10 0 17 3.75 3.75
10 0 17 -0.35 3.71
10 0 17 4.89 4.42
10 0 18 14.66 5.39
10 0 18 17.71 5.90
10 0 18 18.65 5.10
10 0 19 -8.21 5.28
10 0 19 -3.35 4.39
10 0 19 1.27 4.84
10 0 20 65.61 8.80
10 0 20 52.00 7.50
10 0 20 68.81 7.81
10 0 21 7.75 6.22
10 0 21 4.49 7.25
10 2 -23 3.18 3.30
10 2 -22 32.13 2.59
10 2 -22 25.07 4.50
10 -2 -22 34.54 4.79
10 2 -21 4.11 3.15
10 -2 -21 5.60 3.54
10 2 -20 77.17 4.96
10 2 -20 115.07 7.58
10 2 -20 109.95 8.63
10 -2 -20 106.40 7.12
10 2 -19 5.06 1.41
10 2 -19 9.56 2.99
10 2 -19 9.79 3.63
10 -2 -19 4.12 2.86
10 -2 -19 10.36 2.53
10 2 -18 41.92 5.08
10 2 -18 45.12 4.39
10 2 -18 38.22 4.81
10 -2 -18 40.54 4.56
10 -2 -18 32.22 3.81
10 -2 -18 40.48 5.51
10 2 -17 9.06 3.53
10 2 -17 13.85 1.51
10 2 -17 12.27 2.48
10 2 -17 12.19 3.23
10 -2 -17 19.31 3.18
10 -2 -17 13.22 2.55
10 -2 -17 16.72 3.58
10 -2 -17 16.69 3.94
10 2 -16 17.56 3.40
10 2 -16 14.95 1.62
10 2 -16 8.43 2.58
10 2 -16 9.39 2.85
10 -2 -16 12.70 2.72
10 -2 -16 14.79 2.68
10 -2 -16 15.84 3.10
10 -2 -16 18.28 3.68
10 2 -15 27.79 3.43
10 2 -15 28.21 3.85
10 2 -15 20.62 1.85
10 2 -15 14.77 2.91
10 2 -15 25.88 3.55
10 -2 -15 26.63 3.40
10 -2 -15 26.18 2.92
10 -2 -15 22.22 3.33
10 -2 -15 21.04 3.78
10 2 -14 61.45 5.15
10 2 -14 74.26 6.27
10 2 -14 60.68 3.38
10 2 -14 72.60 5.20
10 2 -14 90.71 5.88
10 -2 -14 82.24 5.22
10 -2 -14 63.91 5.28
10 -2 -14 84.81 5.93
10 -2 -14 64.62 5.89
10 2 -13 16.72 1.38
10 2 -13 16.12 2.74
10 2 -13 18.25 3.00
10 2 -13 19.23 1.63
10 2 -13 19.71 2.29
10 2 -13 13.44 2.80
10 -2 -13 17.10 2.61
10 -2 -13 18.70 2.35
10 -2 -13 19.79 2.96
10 -2 -13 21.34 3.17
10 2 -12 42.65 2.43
10 2 -12 56.04 3.76
10 2 -12 52.86 4.37
10 2 -12 41.36 2.67
10 2 -12 46.12 4.10
10 2 -12 39.60 4.65
10 -2 -12 57.85 4.08
10 -2 -12 45.83 3.65
10 -2 -12 47.60 4.62
10 -2 -12 56.88 4.21
10 2 -11 87.11 4.05
10 2 -11 85.94 5.11
10 2 -11 100.01 6.18
10 2 -11 92.64 5.56
10 2 -11 79.14 6.46
10 -2 -11 82.95 6.01
10 -2 -11 77.60 5.43
10 -2 -11 89.86 6.16
10 -2 -11 96.86 6.52
10 2 -10 307.63 12.60
10 2 -10 296.22 11.96
10 2 -10 314.38 12.98
10 2 -10 216.91 13.10
10 2 -10 281.53 14.67
10 -2 -10 240.70 13.15
10 -2 -10 304.99 13.82
10 -2 -10 298.17 15.53
10 -2 -10 289.90 12.92
10 -2 -10 290.74 13.49
10 2 -9 16.68 1.36
10 2 -9 16.37 2.12
10 2 -9 17.28 2.37
10 2 -9 12.38 2.03
10 2 -9 14.30 2.16
10 -2 -9 20.81 2.38
10 -2 -9 14.38 2.12
10 -2 -9 20.41 2.54
10 -2 -9 20.14 2.49
10 -2 -9 18.77 2.43
10 2 -8 255.64 10.81
10 2 -8 289.52 10.44
10 2 -8 256.60 10.78
10 2 -8 246.30 10.70
10 2 -8 230.10 12.04
10 -2 -8 233.39 12.25
10 -2 -8 236.74 11.18
10 -2 -8 248.84 12.58
10 -2 -8 289.64 11.36
10 2 -7 87.85 4.12
10 2 -7 79.31 4.74
10 2 -7 99.12 5.01
10 2 -7 73.22 5.07
10 2 -7 75.46 5.35
10 -2 -7 66.27 5.45
10 -2 -7 77.03 5.71
10 -2 -7 78.37 5.11
10 -2 -7 87.99 5.21
10 2 -6 73.13 3.76
10 2 -6 80.47 4.86
10 2 -6 75.43 4.75
10 2 -6 71.47 4.32
10 2 -6 76.15 4.74
10 -2 -6 71.45 4.78
10 -2 -6 71.47 4.52
10 -2 -6 79.40 3.92
10 -2 -6 80.36 4.64
10 -2 -6 75.37 4.63
10 2 -5 6.41 1.33
10 2 -5 2.78 1.56
10 2 -5 6.14 1.42
10 2 -5 10.28 1.92
10 -2 -5 7.41 2.05
10 -2 -5 7.42 1.75
10 -2 -5 3.70 1.27
10 -2 -5 9.28 2.02
10 -2 -5 6.70 1.62
10 2 -4 76.73 3.90
10 2 -4 78.29 4.51
10 2 -4 51.00 4.17
10 2 -4 69.75 4.65
10 -2 -4 58.36 4.23
10 -2 -4 70.73 4.37
10 -2 -4 68.28 4.07
10 -2 -4 76.86 4.53
10 -2 -4 69.76 4.39
10 2 -3 40.88 3.03
10 2 -3 33.72 2.85
10 2 -3 28.11 3.00
10 2 -3 47.23 3.52
10 -2 -3 33.12 3.20
10 -2 -3 41.04 3.09
10 -2 -3 42.44 2.80
10 -2 -3 42.71 3.22
10 -2 -3 34.13 2.77
10 2 -2 474.51 17.51
10 2 -2 483.19 20.36
10 2 -2 436.88 19.73
10 2 -2 494.50 18.24
10 -2 -2 473.55 18.17
10 -2 -2 467.51 21.17
10 -2 -2 443.38 18.41
10 -2 -2 479.79 18.44
10 -2 -2 449.09 18.75
10 2 -1 16.44 2.15
10 2 -1 13.88 2.22
10 2 -1 17.79 2.05
10 -2 -1 14.12 2.05
10 -2 -1 15.55 2.40
10 -2 -1 13.74 2.00
10 -2 -1 12.55 1.79
10 -2 -1 15.86 1.71
10 2 0 195.52 8.89
10 2 0 226.44 8.73
10 2 0 178.66 9.51
10 2 0 195.48 8.80
10 -2 0 197.16 8.99
10 -2 0 192.08 9.89
10 -2 0 188.73 8.74
10 -2 0 203.86 9.11
10 -2 0 189.08 8.95
10 2 1 18.60 2.40
10 2 1 16.84 2.37
10 2 1 15.01 2.20
10 2 1 17.03 1.94
10 -2 1 16.22 2.16
10 -2 1 18.45 2.23
10 -2 1 10.16 2.24
10 -2 1 15.79 1.67
10 2 2 55.42 4.23
10 2 2 56.82 4.54
10 2 2 50.81 4.40
10 2 2 57.03 3.89
10 -2 2 50.64 4.08
10 -2 2 45.07 3.80
10 -2 2 51.58 2.22
10 -2 2 48.61 3.91
10 -2 2 49.39 3.35
10 2 3 56.84 4.92
10 2 3 50.28 4.80
10 2 3 51.91 4.77
10 2 3 67.19 4.12
10 -2 3 61.36 4.53
10 -2 3 51.96 4.66
10 -2 3 57.57 2.83
10 -2 3 66.06 4.50
10 -2 3 61.67 3.59
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10 2 4 89.77 6.51
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10 -2 4 116.92 6.69
10 -2 4 110.37 6.61
10 -2 4 119.37 5.08
10 -2 4 106.24 6.64
10 -2 4 109.01 5.74
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10 2 5 48.50 3.31
10 -2 5 33.73 3.51
10 -2 5 45.12 3.86
10 -2 5 32.08 2.48
10 -2 5 43.94 3.79
10 -2 5 35.63 2.62
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10 2 6 71.91 5.36
10 2 6 68.97 4.34
10 -2 6 55.03 4.76
10 -2 6 48.77 4.72
10 -2 6 51.66 3.42
10 -2 6 75.75 5.09
10 -2 6 55.25 3.09
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10 2 7 59.91 3.88
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10 -2 7 52.45 4.65
10 -2 7 43.14 3.19
10 -2 7 52.02 4.61
10 -2 7 34.08 2.60
10 -2 7 38.52 3.50
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10 2 8 75.91 4.90
10 2 8 71.10 6.00
10 -2 8 59.61 5.33
10 -2 8 59.21 4.12
10 -2 8 82.42 6.03
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10 2 10 12.05 3.98
10 2 10 8.87 2.27
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10 2 11 62.10 6.25
10 2 11 74.66 5.00
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10 2 12 112.99 6.60
10 2 12 129.79 8.65
10 -2 12 129.42 7.83
10 -2 12 87.18 6.78
10 -2 12 84.68 6.62
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10 2 13 17.46 4.20
10 2 13 13.99 2.73
10 2 13 4.61 3.52
10 -2 13 22.09 3.97
10 -2 13 12.83 3.15
10 -2 13 9.81 2.66
10 2 14 74.06 6.95
10 2 14 63.75 6.80
10 2 14 78.18 5.02
10 2 14 83.55 7.74
10 -2 14 65.56 6.57
10 -2 14 74.46 6.05
10 -2 14 69.52 5.40
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10 2 15 0.45 4.64
10 2 15 10.23 4.33
10 -2 15 5.66 3.85
10 -2 15 2.90 3.25
10 -2 15 5.72 2.75
10 2 16 33.99 5.18
10 2 16 29.11 3.45
10 2 16 34.64 6.11
10 -2 16 38.10 5.10
10 -2 16 32.53 4.00
10 2 17 1.53 4.47
10 2 17 1.30 5.31
10 2 17 6.80 4.65
10 -2 17 -13.06 4.04
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10 2 18 26.58 6.47
10 2 18 27.91 5.70
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10 -2 18 13.76 4.44
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10 2 19 22.77 7.04
10 2 19 11.47 6.62
10 -2 19 18.76 5.75
10 -2 19 20.25 5.29
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10 4 -20 60.59 6.83
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10 4 -19 51.87 5.45
10 4 -19 64.06 4.55
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10 4 -19 63.64 5.94
10 -4 -19 71.18 6.16
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10 4 -18 2.92 2.69
10 4 -18 -0.60 3.49
10 -4 -18 7.46 3.15
10 4 -17 61.23 4.80
10 4 -17 53.54 4.24
10 4 -17 63.32 4.85
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10 -4 -17 64.52 5.74
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10 -4 -15 60.60 5.79
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10 4 -14 51.16 4.45
10 4 -14 57.86 4.84
10 4 -14 49.89 3.88
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10 4 -14 55.21 5.16
10 -4 -14 56.50 5.39
10 -4 -14 52.20 5.22
10 -4 -14 60.05 5.43
10 4 -13 78.02 5.46
10 4 -13 90.39 7.34
10 4 -13 69.95 5.14
10 4 -13 70.65 5.90
10 4 -13 82.89 6.86
10 -4 -13 106.99 7.63
10 -4 -13 67.39 6.19
10 -4 -13 92.30 7.18
10 4 -12 26.11 2.60
10 4 -12 26.52 3.53
10 4 -12 24.40 3.00
10 4 -12 20.73 2.88
10 -4 -12 29.68 3.70
10 -4 -12 26.63 3.58
10 -4 -12 28.48 3.75
10 4 -11 56.99 3.83
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10 4 -11 51.55 4.66
10 4 -11 50.39 4.56
10 -4 -11 59.58 5.04
10 -4 -11 55.64 4.91
10 -4 -11 46.04 4.61
10 -4 -11 55.15 5.26
10 4 -10 184.49 6.33
10 4 -10 161.68 6.26
10 4 -10 173.83 8.86
10 4 -10 164.56 9.88
10 4 -10 182.01 9.45
10 4 -10 139.40 9.48
10 -4 -10 154.82 9.42
10 -4 -10 155.83 9.11
10 -4 -10 133.79 9.56
10 -4 -10 138.53 8.86
10 4 -9 207.06 7.99
10 4 -9 195.54 7.66
10 4 -9 193.23 8.62
10 4 -9 197.27 10.59
10 4 -9 194.31 9.93
10 4 -9 170.82 11.06
10 -4 -9 141.97 9.77
10 -4 -9 181.67 9.71
10 -4 -9 189.05 8.89
10 -4 -9 188.49 9.80
10 -4 -9 188.51 9.66
10 4 -8 68.46 3.43
10 4 -8 68.26 3.31
10 4 -8 64.09 4.25
10 4 -8 70.28 5.20
10 4 -8 55.60 5.04
10 -4 -8 60.10 5.17
10 -4 -8 61.23 5.15
10 -4 -8 60.49 4.84
10 -4 -8 77.49 4.96
10 -4 -8 67.49 4.64
10 4 -7 57.08 3.09
10 4 -7 59.87 3.22
10 4 -7 45.54 3.48
10 4 -7 67.53 4.95
10 -4 -7 62.18 4.40
10 -4 -7 54.06 4.54
10 -4 -7 52.46 4.08
10 -4 -7 63.58 4.60
10 -4 -7 41.44 3.82
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10 -4 -6 53.47 4.19
10 -4 -6 42.55 3.56
10 -4 -6 44.95 4.25
10 -4 -6 50.28 3.36
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10 4 -5 294.32 12.03
10 4 -5 285.33 13.04
10 -4 -5 285.24 12.97
10 -4 -5 268.66 13.97
10 -4 -5 279.34 12.65
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10 4 -4 111.77 5.78
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10 -4 -3 130.40 7.69
10 -4 -3 137.91 7.07
10 -4 -3 122.49 7.68
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10 -4 -2 5.38 1.57
10 -4 -2 7.62 1.85
10 -4 -2 8.49 2.36
10 -4 -2 6.12 1.39
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10 4 -1 280.39 11.62
10 4 -1 265.85 11.97
10 -4 -1 242.98 11.94
10 -4 -1 263.01 14.00
10 -4 -1 274.86 11.73
10 -4 -1 240.83 12.27
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10 4 0 123.00 7.50
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10 -4 0 133.76 8.41
10 -4 0 147.32 7.33
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10 4 1 160.87 8.33
10 4 1 156.88 8.14
10 4 1 149.32 8.29
10 -4 1 144.49 8.62
10 -4 1 172.97 8.76
10 -4 1 173.37 8.76
10 -4 1 147.35 7.77
10 -4 1 165.40 6.64
10 4 2 63.64 5.47
10 4 2 59.77 5.04
10 4 2 69.16 5.54
10 -4 2 50.79 4.66
10 -4 2 62.80 4.53
10 -4 2 62.72 5.26
10 -4 2 68.93 3.04
10 4 3 97.87 6.49
10 4 3 88.28 6.90
10 -4 3 91.17 6.54
10 -4 3 94.69 5.88
10 -4 3 90.71 6.33
10 -4 3 94.33 3.99
10 4 4 28.75 3.48
10 4 4 31.10 3.52
10 4 4 30.56 4.20
10 -4 4 24.95 3.38
10 -4 4 28.17 2.77
10 -4 4 29.31 3.28
10 -4 4 21.71 1.53
10 4 5 85.47 6.23
10 4 5 82.26 6.46
10 4 5 90.30 7.25
10 -4 5 67.26 5.95
10 -4 5 77.73 5.19
10 -4 5 91.70 6.82
10 -4 5 82.77 3.56
10 -4 5 87.82 3.43
10 4 6 68.41 5.74
10 4 6 104.53 6.23
10 4 6 85.37 6.57
10 4 6 75.77 6.22
10 -4 6 83.18 5.48
10 -4 6 77.56 6.59
10 -4 6 71.47 3.14
10 -4 6 69.45 2.95
10 4 7 99.65 7.17
10 4 7 112.60 7.80
10 4 7 137.49 9.29
10 4 7 86.22 7.46
10 -4 7 103.73 7.00
10 -4 7 118.04 7.89
10 -4 7 108.08 4.27
10 -4 7 95.85 4.09
10 4 8 67.32 5.97
10 4 8 80.28 5.76
10 4 8 61.08 5.88
10 4 8 62.47 6.49
10 -4 8 70.85 5.71
10 -4 8 53.65 3.79
10 -4 8 72.42 5.77
10 -4 8 57.44 2.88
10 4 9 37.56 4.17
10 4 9 32.53 4.62
10 4 9 27.24 4.79
10 4 9 30.66 4.29
10 -4 9 35.57 4.19
10 -4 9 33.04 3.00
10 -4 9 19.98 4.23
10 -4 9 32.59 2.08
10 4 10 3.33 3.10
10 4 10 6.07 3.60
10 4 10 -10.93 3.69
10 4 10 -5.89 3.68
10 -4 10 0.70 2.56
10 -4 10 1.62 1.85
10 -4 10 -0.12 1.16
10 4 11 79.82 6.90
10 4 11 75.98 6.18
10 4 11 84.63 7.12
10 -4 11 75.56 6.63
10 -4 11 69.03 4.87
10 -4 11 62.33 3.25
10 4 12 54.42 5.71
10 4 12 57.48 6.37
10 -4 12 43.84 4.99
10 -4 12 48.38 4.17
10 -4 12 50.77 2.91
10 4 13 76.21 7.24
10 4 13 110.51 8.45
10 -4 13 78.93 6.96
10 -4 13 90.29 5.57
10 -4 13 74.42 4.20
10 4 14 6.64 4.15
10 4 14 10.02 4.52
10 -4 14 10.30 3.47
10 -4 14 7.00 1.87
10 4 15 43.95 5.92
10 4 15 37.78 6.46
10 -4 15 55.27 4.98
10 4 16 3.67 4.62
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13 -3 -10 50.43 4.74
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13 -3 -9 66.59 5.16
13 -3 -9 83.09 5.68
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30 0 -15 -5.57 5.68
30 0 -14 41.39 7.39
30 0 -13 -15.71 5.69
30 0 -12 14.94 6.73
30 0 -11 9.27 6.29
30 0 -10 66.12 9.07
30 0 -9 10.72 7.84
30 0 -8 20.97 7.18
30 0 -7 -10.84 5.71
30 0 -6 12.19 6.68
30 0 -5 14.39 6.96
30 0 -4 -11.04 6.89
30 0 -3 -4.90 6.81
30 0 -2 54.15 9.63
30 2 -20 21.58 7.38
30 2 -19 4.21 6.94
30 -2 -19 19.55 8.80
30 2 -18 -0.23 6.49
30 -2 -18 9.94 7.08
30 2 -17 2.05 7.63
30 -2 -17 -6.05 6.39
30 2 -16 7.07 6.16
30 -2 -16 23.59 6.84
30 2 -15 4.80 6.63
30 -2 -15 20.38 7.40
30 2 -14 23.81 6.75
30 -2 -14 13.20 6.03
30 2 -13 -5.81 5.58
30 2 -12 8.20 6.15
30 2 -11 6.01 6.35
30 -2 -11 17.81 6.51
30 2 -10 39.90 7.54
30 -2 -10 41.78 7.67
30 2 -9 9.21 6.64
30 -2 -9 16.43 7.93
30 2 -8 5.86 6.79
30 -2 -8 17.09 6.47
30 2 -7 0.94 6.83
30 -2 -7 5.92 6.15
30 2 -6 21.79 7.70
30 -2 -6 25.93 8.88
30 2 -5 9.05 6.79
30 -2 -5 1.65 6.47
30 2 -4 30.54 8.02
30 -2 -4 26.87 7.70
30 2 -3 5.42 8.67
30 -2 -3 0.48 6.68
30 2 -2 15.00 7.80
30 2 -1 21.51 7.73
30 4 -19 9.62 6.98
30 4 -18 -7.23 6.20
30 4 -17 0.69 6.21
30 -4 -17 7.02 7.02
30 4 -16 13.60 6.92
30 -4 -16 12.17 7.01
30 4 -15 -1.85 6.12
30 -4 -15 8.72 7.34
30 4 -14 11.82 8.23
30 -4 -14 13.41 6.99
30 4 -13 7.21 6.74
30 -4 -13 9.28 6.76
30 4 -12 3.50 6.53
30 -4 -12 13.87 6.88
30 4 -11 15.82 7.50
30 -4 -11 21.81 7.23
30 4 -10 12.47 6.94
30 -4 -10 7.59 8.17
30 4 -9 29.54 8.04
30 -4 -9 41.57 7.39
30 4 -8 -4.27 7.00
30 -4 -8 5.68 6.38
30 4 -7 17.65 7.51
30 -4 -7 24.95 8.51
30 4 -6 6.23 6.59
30 -4 -6 12.20 7.27
30 4 -5 -11.67 6.50
30 -4 -5 -8.74 7.44
30 4 -4 3.45 6.42
30 4 -3 33.50 9.45
30 6 -13 16.61 7.07
30 -6 -13 19.46 6.95
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30 -6 -12 -0.70 8.00
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30 -6 -11 11.73 6.85
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30 6 -9 15.17 7.41
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31 1 -18 -7.52 6.95
31 -1 -18 -2.40 6.97
31 1 -17 -6.61 6.39
31 -1 -17 11.30 8.56
31 1 -16 10.04 7.08
31 -1 -16 0.23 6.50
31 1 -15 37.70 7.77
31 -1 -15 36.38 7.98
31 1 -14 -4.23 6.06
31 -1 -14 -7.19 6.84
31 1 -13 32.78 8.14
31 -1 -13 35.84 8.22
31 1 -12 4.25 7.01
31 -1 -12 3.54 6.63
31 1 -11 14.29 6.57
31 -1 -11 21.88 7.10
31 1 -10 -3.12 6.13
31 -1 -10 -10.11 6.32
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31 -1 -9 21.80 7.27
31 1 -8 -12.49 7.94
31 -1 -8 6.95 6.61
31 1 -7 13.61 7.16
31 -1 -7 24.23 7.34
31 1 -6 4.01 6.96
31 -1 -6 2.34 7.97
31 1 -5 5.34 7.60
31 -1 -5 14.97 7.66
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31 3 -18 1.26 7.10
31 3 -17 8.38 7.46
31 3 -16 5.52 6.67
31 -3 -16 11.70 7.34
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31 -3 -8 -2.32 6.61
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31 -3 -7 15.50 7.23
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31 -5 -12 19.08 7.51
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_shelx_res_file
;
TITL TSBB-192 (L0711)
y_sq.res
created by SHELXL-2018/3 at 16:32:08 on 20-Jan-2021
CELL 0.71073 23.653 10.1034 20.5952 90 115.0715 90
ZERR 4 0.0005 0.0002 0.0004 0 0.0012 0
LATT 7
SYMM -X,+Y,0.5-Z
SFAC C H N O Sn
UNIT 200 208 8 28 4
DFIX 0.84 0.01 O3 H3
L.S. 5 0 48
PLAN 12
TEMP -113
CONF
HTAB N1 O10
BOND $H
FMAP 2
ACTA
DFIX 0.84 0.01 O3 H3
HTAB N1 O10
HTAB O3 O10_$1
EQIV $1 0.5+x, 0.5-y, 0.5+z
ABIN
WGHT 0.094300 4.702700
FVAR 0.11042
SN1 5 0.000000 0.209439 0.250000 10.50000 0.01201 0.02281 =
0.01816 0.00000 0.00244 0.00000
O1 4 -0.062484 0.037027 0.194562 11.00000 0.01328 0.02478 =
0.02820 -0.00121 0.00084 -0.00070
O2 4 -0.102422 0.236628 0.161879 11.00000 0.01829 0.02200 =
0.02923 -0.00125 0.00572 -0.00093
O3 4 0.000000 0.440785 0.250000 10.50000 0.03902 0.01598 =
0.03251 0.00000 -0.00252 0.00000
H3 2 0.030054 0.475979 0.284114 11.00000 0.05076
O10 4 -0.435382 -0.117004 -0.145459 11.00000 0.02285 0.03445 =
0.02594 0.00223 0.00304 -0.00220
N1 3 -0.343382 -0.120494 -0.016107 11.00000 0.01527 0.03174 =
0.02151 0.00343 0.00020 -0.00030
H1 2 -0.358063 -0.083729 -0.055190 11.00000 0.03329
C1 1 -0.108494 0.111284 0.157720 11.00000 0.01564 0.02288 =
0.02363 -0.00149 0.00672 -0.00097
C2 1 -0.169370 0.048662 0.111661 11.00000 0.01608 0.02835 =
0.01980 -0.00171 0.00516 -0.00086
C3 1 -0.176584 -0.087907 0.112044 11.00000 0.01413 0.02860 =
0.02404 -0.00209 0.00327 0.00373
AFIX 43
H3A 2 -0.142047 -0.141854 0.140536 11.00000 -1.20000
AFIX 0
C4 1 -0.233716 -0.145563 0.071206 11.00000 0.02035 0.02283 =
0.03036 -0.00573 0.00606 -0.00190
AFIX 43
H4 2 -0.238480 -0.238854 0.071822 11.00000 -1.20000
AFIX 0
C5 1 -0.284193 -0.066779 0.029229 11.00000 0.01578 0.03095 =
0.02114 -0.00202 0.00497 -0.00267
C6 1 -0.277034 0.070298 0.028108 11.00000 0.01391 0.03111 =
0.02939 0.00908 0.00343 0.00160
AFIX 43
H6 2 -0.311396 0.124213 -0.000880 11.00000 -1.20000
AFIX 0
C7 1 -0.219684 0.127388 0.069387 11.00000 0.02119 0.02694 =
0.02940 0.00515 0.00545 -0.00117
AFIX 43
H7 2 -0.214750 0.220631 0.068782 11.00000 -1.20000
AFIX 0
C8 1 -0.377629 -0.207244 -0.000031 11.00000 0.02045 0.03759 =
0.02711 0.00094 0.00789 -0.00125
C9 1 -0.434760 -0.247988 -0.051138 11.00000 0.02092 0.02761 =
0.02881 0.00017 0.00894 -0.00217
AFIX 43
H9 2 -0.457607 -0.310895 -0.037549 11.00000 -1.20000
AFIX 0
C10 1 -0.461562 -0.201230 -0.123201 11.00000 0.01901 0.02573 =
0.02819 -0.00399 0.00569 0.00124
C11 1 -0.523133 -0.258853 -0.173864 11.00000 0.02061 0.04185 =
0.02775 -0.00313 0.00395 -0.00370
AFIX 137
H11A 2 -0.547018 -0.285054 -0.146995 11.00000 -1.50000
H11B 2 -0.515815 -0.336583 -0.197729 11.00000 -1.50000
H11C 2 -0.546698 -0.192478 -0.209889 11.00000 -1.50000
AFIX 0
C12 1 -0.354077 -0.259384 0.075328 11.00000 0.03183 0.09088 =
0.03058 0.01657 0.00440 -0.02066
AFIX 137
H12A 2 -0.323563 -0.329840 0.082306 11.00000 -1.50000
H12B 2 -0.389126 -0.294807 0.083429 11.00000 -1.50000
H12C 2 -0.334203 -0.187465 0.109331 11.00000 -1.50000
AFIX 0
C13 1 0.040321 0.219283 0.174124 11.00000 0.02128 0.04587 =
0.02871 -0.00150 0.01155 -0.00115
AFIX 23
H13A 2 0.069539 0.295146 0.187002 11.00000 -1.20000
H13B 2 0.065092 0.137904 0.178904 11.00000 -1.20000
AFIX 0
C14 1 -0.005167 0.233656 0.097212 11.00000 0.02185 0.02905 =
0.02652 -0.00111 0.01181 0.00100
C15 1 -0.034355 0.123790 0.057485 11.00000 0.04456 0.03177 =
0.03830 -0.00070 0.02059 -0.00373
AFIX 43
H15 2 -0.024141 0.038632 0.078874 11.00000 -1.20000
AFIX 0
C16 1 -0.078290 0.134854 -0.013002 11.00000 0.04637 0.06164 =
0.03143 -0.01171 0.01387 -0.01631
AFIX 43
H16 2 -0.097970 0.058061 -0.039592 11.00000 -1.20000
AFIX 0
C17 1 -0.093138 0.258110 -0.044111 11.00000 0.03375 0.08602 =
0.02440 0.00304 0.00856 0.00775
AFIX 43
H17 2 -0.124052 0.267139 -0.091927 11.00000 -1.20000
AFIX 0
C18 1 -0.062946 0.368533 -0.005578 11.00000 0.04678 0.04983 =
0.04195 0.01996 0.02636 0.02431
AFIX 43
H18 2 -0.071962 0.453215 -0.027685 11.00000 -1.20000
AFIX 0
C19 1 -0.019887 0.356934 0.064610 11.00000 0.04269 0.03181 =
0.03891 0.00312 0.02655 0.00506
AFIX 43
H19 2 -0.000091 0.433880 0.090941 11.00000 -1.20000
AFIX 0
HKLF 4
REM TSBB-192 (L0711)
REM wR2 = 0.1483, GooF = S = 1.047, Restrained GooF = 1.047 for all data
REM R1 = 0.0559 for 5193 Fo > 4sig(Fo) and 0.0765 for all 6506 data
REM 228 parameters refined using 2 restraints
END
WGHT 0.0943 4.7027
REM Highest difference peak 1.063, deepest hole -2.173, 1-sigma level 0.129
Q1 1 0.0291 0.3144 0.2627 11.00000 0.05 1.06
Q2 1 0.0109 0.1999 0.1983 11.00000 0.05 1.05
Q3 1 0.0209 0.0981 0.2528 11.00000 0.05 0.87
Q4 1 0.0091 0.3071 0.2182 11.00000 0.05 0.81
Q5 1 0.0377 0.1680 0.2321 11.00000 0.05 0.81
Q6 1 0.0456 0.2115 0.3066 11.00000 0.05 0.73
Q7 1 0.0074 0.2617 0.1583 11.00000 0.05 0.61
Q8 1 0.0097 0.2838 0.0767 11.00000 0.05 0.61
Q9 1 -0.0848 0.3107 0.2069 11.00000 0.05 0.56
Q10 1 0.0375 0.3972 0.2610 11.00000 0.05 0.55
Q11 1 -0.1268 0.2570 0.1699 11.00000 0.05 0.54
Q12 1 -0.0703 0.2028 0.1467 11.00000 0.05 0.54
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-13 5 25 -0.26 0.00
-11 5 25 0.51 0.00
-9 5 25 1.15 0.00
-7 5 25 -1.86 0.00
-5 5 25 0.19 0.00
-3 5 25 1.80 0.00
-20 6 25 0.72 0.00
-18 6 25 -1.00 0.00
-16 6 25 1.57 0.00
-14 6 25 -0.90 0.00
-12 6 25 -0.01 0.00
-10 6 25 -0.11 0.00
-8 6 25 -0.64 0.00
-6 6 25 1.28 0.00
-15 7 25 3.09 0.00
-13 7 25 -1.69 0.00
-9 7 25 5.90 0.00
-26 0 26 0.57 0.00
-24 0 26 2.59 0.00
-22 0 26 -4.70 0.00
-20 0 26 3.73 0.00
-18 0 26 -2.58 0.00
-16 0 26 2.99 0.00
-14 0 26 -1.33 0.00
-12 0 26 0.41 0.00
-10 0 26 -1.95 0.00
-8 0 26 0.54 0.00
-6 0 26 0.64 0.00
-4 0 26 0.29 0.00
-2 0 26 0.98 0.00
0 0 26 -1.47 0.00
-25 1 26 -2.21 0.00
-23 1 26 -0.07 0.00
-21 1 26 2.86 0.00
-19 1 26 -1.18 0.00
-17 1 26 -3.44 0.00
-15 1 26 4.05 0.00
-13 1 26 -2.98 0.00
-11 1 26 3.93 0.00
-9 1 26 -5.96 0.00
-7 1 26 9.23 0.00
-5 1 26 -8.01 0.00
-3 1 26 1.34 0.00
-1 1 26 1.71 0.00
-24 2 26 1.06 0.00
-22 2 26 -1.04 0.00
-20 2 26 -1.56 0.00
-18 2 26 3.47 0.00
-16 2 26 -1.67 0.00
-14 2 26 1.14 0.00
-12 2 26 -0.67 0.00
-10 2 26 -1.85 0.00
-8 2 26 1.30 0.00
-6 2 26 -0.30 0.00
-4 2 26 1.04 0.00
-2 2 26 -0.11 0.00
0 2 26 -0.04 0.00
-23 3 26 0.34 0.00
-21 3 26 -0.95 0.00
-19 3 26 1.17 0.00
-17 3 26 -0.92 0.00
-15 3 26 -0.82 0.00
-13 3 26 -0.87 0.00
-11 3 26 4.48 0.00
-9 3 26 -3.93 0.00
-7 3 26 2.60 0.00
-5 3 26 -0.92 0.00
-3 3 26 -1.88 0.00
-1 3 26 1.14 0.00
-22 4 26 -1.91 0.00
-20 4 26 2.46 0.00
-18 4 26 -0.44 0.00
-16 4 26 -1.44 0.00
-14 4 26 4.36 0.00
-12 4 26 -3.87 0.00
-10 4 26 -1.02 0.00
-8 4 26 1.24 0.00
-6 4 26 1.63 0.00
-4 4 26 -1.84 0.00
-19 5 26 3.34 0.00
-17 5 26 -4.14 0.00
-15 5 26 1.02 0.00
-13 5 26 -0.09 0.00
-11 5 26 1.88 0.00
-9 5 26 -0.50 0.00
-7 5 26 -0.44 0.00
-16 6 26 1.10 0.00
-14 6 26 1.11 0.00
-12 6 26 -1.23 0.00
-10 6 26 -1.33 0.00
-23 1 27 -2.03 0.00
-21 1 27 1.56 0.00
-19 1 27 -0.69 0.00
-17 1 27 -0.07 0.00
-15 1 27 -0.49 0.00
-13 1 27 0.84 0.00
-11 1 27 -0.22 0.00
-9 1 27 0.19 0.00
-7 1 27 -0.57 0.00
-5 1 27 0.18 0.00
-3 1 27 0.59 0.00
-22 2 27 -1.70 0.00
-20 2 27 1.85 0.00
-18 2 27 -0.78 0.00
-16 2 27 1.00 0.00
-14 2 27 -2.35 0.00
-12 2 27 4.47 0.00
-10 2 27 -5.32 0.00
-8 2 27 1.88 0.00
-6 2 27 3.00 0.00
-4 2 27 -4.18 0.00
-21 3 27 2.34 0.00
-19 3 27 -2.35 0.00
-17 3 27 0.03 0.00
-15 3 27 0.82 0.00
-13 3 27 -0.11 0.00
-11 3 27 0.01 0.00
-9 3 27 0.36 0.00
-7 3 27 -0.97 0.00
-5 3 27 0.36 0.00
-20 4 27 -0.05 0.00
-18 4 27 0.98 0.00
-16 4 27 0.05 0.00
-14 4 27 -0.84 0.00
-12 4 27 0.38 0.00
-10 4 27 -0.57 0.00
-8 4 27 0.87 0.00
-15 5 27 1.35 0.00
-13 5 27 0.98 0.00
-11 5 27 -2.11 0.00
-20 0 28 -3.07 0.00
-18 0 28 1.21 0.00
-16 0 28 -1.35 0.00
-14 0 28 -0.70 0.00
-12 0 28 1.29 0.00
-10 0 28 -1.25 0.00
-8 0 28 4.62 0.00
-6 0 28 -4.86 0.00
-21 1 28 -3.20 0.00
-19 1 28 1.78 0.00
-17 1 28 1.81 0.00
-15 1 28 -2.11 0.00
-13 1 28 3.41 0.00
-11 1 28 -5.68 0.00
-9 1 28 6.33 0.00
-7 1 28 -6.88 0.00
-20 2 28 1.61 0.00
-18 2 28 -2.15 0.00
-16 2 28 0.38 0.00
-14 2 28 -1.28 0.00
-12 2 28 0.27 0.00
-10 2 28 1.56 0.00
-8 2 28 0.56 0.00
-17 3 28 -2.65 0.00
-15 3 28 2.95 0.00
-13 3 28 1.56 0.00
-11 3 28 -4.25 0.00
-9 3 28 2.05 0.00
2 0 0 -295.38 0.00
30 2 0 -0.97 0.00
6 14 0 0.49 0.00
29 3 1 1.23 0.00
-28 6 1 -1.78 0.00
23 9 1 2.67 0.00
-22 10 1 -0.92 0.00
16 12 1 -3.05 0.00
-13 13 1 3.03 0.00
-6 14 1 -5.02 0.00
-31 1 2 2.99 0.00
-30 4 2 3.07 0.00
28 4 2 1.47 0.00
-26 8 2 2.50 0.00
24 8 2 -0.44 0.00
-6 14 2 1.46 0.00
4 14 2 3.14 0.00
-31 3 3 -4.35 0.00
20 10 3 -0.46 0.00
-6 14 3 3.57 0.00
-2 14 3 3.77 0.00
0 14 3 -0.10 0.00
4 14 3 1.71 0.00
-32 0 4 9.84 0.00
28 0 4 2.32 0.00
-25 9 4 -1.21 0.00
17 11 4 0.30 0.00
-18 12 4 -2.47 0.00
14 12 4 0.75 0.00
-6 14 4 -3.30 0.00
-2 14 4 -2.75 0.00
2 14 4 5.73 0.00
-32 2 5 0.12 0.00
22 8 5 -2.59 0.00
-21 11 5 -1.59 0.00
-18 12 5 2.14 0.00
9 13 5 3.64 0.00
-6 14 5 -1.43 0.00
-4 14 5 2.97 0.00
-2 14 5 -1.02 0.00
0 14 5 -1.08 0.00
-32 0 6 -11.27 0.00
-18 12 6 4.59 0.00
-4 14 6 -5.64 0.00
-2 14 6 0.97 0.00
-30 6 7 -1.16 0.00
19 9 7 0.08 0.00
-18 12 7 -4.76 0.00
7 13 7 2.50 0.00
-33 1 8 -0.50 0.00
24 4 8 0.13 0.00
-31 5 8 2.60 0.00
-30 6 8 -3.61 0.00
-29 7 8 -2.49 0.00
-24 10 8 2.14 0.00
16 10 8 -0.68 0.00
-18 12 8 -3.05 0.00
-13 13 8 3.38 0.00
-33 1 9 -0.52 0.00
24 2 9 -6.38 0.00
-32 4 9 1.64 0.00
-29 7 9 5.90 0.00
17 9 9 0.43 0.00
-24 10 9 2.63 0.00
-18 12 9 4.28 0.00
-13 13 9 -0.14 0.00
-33 1 10 1.30 0.00
-32 4 10 -1.09 0.00
-29 7 10 1.53 0.00
18 8 10 1.34 0.00
14 10 10 -1.04 0.00
-21 11 10 -1.33 0.00
8 12 10 0.87 0.00
-33 1 11 2.34 0.00
-32 4 11 -3.27 0.00
15 9 11 1.43 0.00
-21 11 11 0.78 0.00
-11 13 11 0.08 0.00
-33 1 12 -3.47 0.00
21 3 12 1.41 0.00
-32 4 12 2.73 0.00
-29 7 12 -1.05 0.00
16 8 12 -1.69 0.00
9 11 12 -1.06 0.00
-7 13 12 -2.21 0.00
-5 13 12 6.25 0.00
-33 1 13 -2.05 0.00
-32 4 13 0.82 0.00
-29 7 13 0.28 0.00
13 9 13 4.42 0.00
-33 1 14 1.73 0.00
19 3 14 2.69 0.00
-32 4 14 -1.68 0.00
-30 6 14 1.95 0.00
-14 12 14 1.67 0.00
-33 1 15 0.34 0.00
-31 5 15 -1.75 0.00
-30 6 15 -1.16 0.00
-25 9 15 1.74 0.00
-12 12 15 -1.29 0.00
-2 12 15 -5.09 0.00
-33 1 16 -0.63 0.00
16 4 16 2.14 0.00
14 6 16 -0.54 0.00
9 9 16 0.63 0.00
6 10 16 0.51 0.00
16 2 17 1.76 0.00
-26 8 17 1.21 0.00
7 9 17 0.32 0.00
4 10 17 -2.25 0.00
15 1 18 -2.33 0.00
8 8 18 -2.24 0.00
-23 9 18 -1.94 0.00
2 10 18 1.72 0.00
-13 11 18 -0.17 0.00
12 4 19 1.02 0.00
11 5 19 1.90 0.00
10 6 19 1.86 0.00
6 8 19 0.00 0.00
-18 10 19 0.01 0.00
12 2 20 -1.15 0.00
-30 4 20 -0.72 0.00
-29 5 20 -2.80 0.00
1 9 20 2.16 0.00
-16 10 20 -0.10 0.00
-4 10 20 1.53 0.00
-31 1 21 0.93 0.00
-25 7 21 1.12 0.00
2 8 21 2.10 0.00
-19 9 21 2.96 0.00
9 1 22 -2.45 0.00
-30 2 22 -0.25 0.00
-26 6 22 1.74 0.00
-5 9 22 -1.58 0.00
-4 8 23 -4.12 0.00
-25 5 24 -1.66 0.00
0 6 24 1.50 0.00
-3 7 24 -1.12 0.00
-14 8 24 1.49 0.00
-12 8 24 -1.00 0.00
-10 8 24 1.34 0.00
3 1 25 -0.62 0.00
-1 5 25 -2.72 0.00
-4 6 25 -0.34 0.00
-17 7 25 -1.88 0.00
-11 7 25 -1.96 0.00
-7 7 25 -5.70 0.00
1 1 26 -0.69 0.00
-2 4 26 1.23 0.00
-21 5 26 -1.31 0.00
-5 5 26 -1.20 0.00
-18 6 26 -2.35 0.00
-8 6 26 0.85 0.00
-6 4 27 -0.23 0.00
-17 5 27 -1.52 0.00
-9 5 27 1.01 0.00
-22 0 28 4.67 0.00
-19 3 28 1.76 0.00
-14 4 28 -4.39 0.00
-12 4 28 2.75 0.00
-17 1 29 -0.02 0.00
-15 1 29 1.12 0.00
-13 1 29 -0.75 0.00
0 0 0 0.00 0.00
# SQUEEZE RESULTS (Version = 111220)
# Note: Data are Listed for all Voids in the P1 Unit Cell
# i.e. Centre of Gravity, Solvent Accessible Volume,
# Recovered number of Electrons in the Void and
# Details about the Squeezed Material
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.250 -0.056 0.250 324 85 ' '
2 0.750 0.016 0.250 324 85 ' '
3 0.250 -0.003 0.750 325 85 ' '
4 0.750 -0.073 0.750 325 85 ' '
# Missing Reflections Below sin(th)/lambda = 0.25
loop_
_platon_missing_refln_index_h
_platon_missing_refln_index_k
_platon_missing_refln_index_l
_platon_missing_refln_theta
2 0 0 1.901
_platon_squeeze_void_probe_radius 1.20
_platon_squeeze_details
)
TITL x C 1 2/c 1 R = 0.06
CELL 23.6530 10.1034 20.5952 90.00 115.07 90.00
SPGR C2/c
# Solvent Accessible Volume = 1299
# Electrons Found in S.A.V. = 338
# Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others
C101 0.273 0.507 0.253 ! 4.65 eA-3
C102 0.803 0.484 0.172 ! 4.48 eA-3
C103 0.789 0.018 0.808 ! 3.72 eA-3
C104 0.749 0.491 0.271 ! 3.69 eA-3
C105 0.165 0.505 0.268 ! 3.62 eA-3
C106 0.243 0.121 0.243 ! 3.30 eA-3
C107 0.749 0.462 0.153 ! 3.27 eA-3
C108 0.314 0.083 0.197 ! 2.99 eA-3
C109 0.203 0.365 0.762 ! 2.89 eA-3
C110 0.711 0.090 0.796 ! 2.78 eA-3
C111 0.735 0.416 0.214 ! 2.72 eA-3
C112 0.180 0.493 0.229 ! 2.53 eA-3
C113 0.258 0.397 0.318 ! 2.06 eA-3
C114 0.711 0.048 0.201 ! 2.01 eA-3
Q115 0.969 0.317 0.216 ! 1.36 eA-3
Q116 0.992 0.157 0.303 ! 1.13 eA-3
Q117 0.985 0.221 0.292 ! 1.13 eA-3
Q118 0.983 0.318 0.265 ! 1.12 eA-3
C119 0.790 0.496 0.731 ! 1.09 eA-3
Q120 1.000 0.250 0.250 ! 1.02 eA-3
Q121 0.008 0.093 0.265 ! 0.95 eA-3
Q122 0.955 0.181 0.265 ! 0.94 eA-3
C123 0.673 0.497 0.167 ! 0.93 eA-3
Q124 0.961 0.127 0.236 ! 0.92 eA-3
Q125 0.554 0.276 0.794 ! 0.90 eA-3
Q126 0.507 0.217 0.797 ! 0.84 eA-3
C127 0.280 0.349 0.339 ! 0.84 eA-3
Q128 0.461 0.098 0.736 ! 0.83 eA-3
C129 0.730 0.041 0.309 ! 0.80 eA-3
Q130 0.626 0.249 0.833 ! 0.79 eA-3
Q131 0.539 0.351 0.792 ! 0.78 eA-3
Q132 0.968 0.200 0.185 ! 0.78 eA-3
Q133 0.828 0.375 0.197 ! 0.78 eA-3
C134 0.210 0.431 0.192 ! 0.77 eA-3
Q135 0.189 0.093 0.199 ! 0.76 eA-3
Q136 0.491 0.313 0.765 ! 0.75 eA-3
Q137 0.213 0.039 0.277 ! 0.74 eA-3
Q138 0.713 0.413 0.786 ! 0.74 eA-3
C139 0.288 0.048 0.761 ! 0.73 eA-3
Q140 0.304 0.119 0.006 ! 0.73 eA-3
Q141 1.002 0.248 0.155 ! 0.71 eA-3
Q142 0.102 0.041 0.286 ! 0.71 eA-3
C143 0.249 0.036 0.099 ! 0.70 eA-3
Q144 0.984 0.408 0.200 ! 0.69 eA-3
C145 0.719 0.303 0.256 ! 0.69 eA-3
Q146 0.929 0.176 0.158 ! 0.69 eA-3
Q147 0.749 0.506 0.564 ! 0.68 eA-3
C148 0.233 0.359 0.817 ! 0.68 eA-3
C149 0.667 0.130 0.757 ! 0.67 eA-3
Q150 0.076 0.252 0.920 ! 0.66 eA-3
Q151 0.493 0.302 0.857 ! 0.65 eA-3
Q152 0.548 0.468 0.296 ! 0.65 eA-3
Q153 0.978 0.376 0.290 ! 0.65 eA-3
Q154 0.375 0.087 0.672 ! 0.64 eA-3
Q155 0.765 0.165 0.579 ! 0.63 eA-3
Q156 0.765 0.462 0.341 ! 0.63 eA-3
Q157 0.203 0.508 0.651 ! 0.63 eA-3
Q158 0.267 0.442 0.854 ! 0.62 eA-3
Q159 0.962 0.184 0.092 ! 0.61 eA-3
Q160 0.008 0.278 0.084 ! 0.61 eA-3
C161 0.384 0.025 0.283 ! 0.60 eA-3
Q162 0.242 0.411 0.170 ! 0.60 eA-3
C163 0.268 0.312 0.723 ! 0.59 eA-3
Q164 0.906 0.186 0.172 ! 0.59 eA-3
Q165 0.937 0.491 0.138 ! 0.59 eA-3
Q166 0.539 0.186 0.920 ! 0.59 eA-3
Q167 0.333 0.490 0.372 ! 0.58 eA-3
Q168 0.359 0.442 0.985 ! 0.58 eA-3
Q169 0.742 0.124 0.359 ! 0.58 eA-3
Q170 0.180 0.401 0.874 ! 0.58 eA-3
Q171 0.226 0.030 0.832 ! 0.58 eA-3
C172 0.344 0.461 0.265 ! 0.58 eA-3
Q173 0.944 0.381 0.587 ! 0.57 eA-3
Q174 0.807 0.046 0.714 ! 0.57 eA-3
Q175 0.243 0.446 0.677 ! 0.57 eA-3
Q176 0.343 0.253 0.734 ! 0.57 eA-3
Q177 0.616 0.343 0.842 ! 0.57 eA-3
Q178 0.406 0.435 0.204 ! 0.56 eA-3
C179 0.311 0.313 0.738 ! 0.56 eA-3
Q180 0.624 0.129 0.497 ! 0.56 eA-3
Q181 0.689 0.466 0.090 ! 0.56 eA-3
Q182 0.311 0.382 0.064 ! 0.55 eA-3
Q183 0.147 0.375 0.109 ! 0.55 eA-3
Q184 0.248 0.160 0.062 ! 0.55 eA-3
Q185 0.087 0.316 0.424 ! 0.55 eA-3
Q186 0.109 0.191 0.079 ! 0.55 eA-3
Q187 0.753 0.092 0.114 ! 0.55 eA-3
Q188 0.149 0.337 0.356 ! 0.55 eA-3
Q189 0.673 0.157 0.109 ! 0.55 eA-3
Q190 0.180 0.427 0.430 ! 0.55 eA-3
Q191 0.158 0.317 0.283 ! 0.55 eA-3
Q192 0.046 0.421 0.406 ! 0.55 eA-3
Q193 0.483 0.439 0.808 ! 0.54 eA-3
Q194 0.351 0.339 0.751 ! 0.54 eA-3
Q195 0.501 0.213 0.356 ! 0.54 eA-3
Q196 0.186 0.101 0.380 ! 0.54 eA-3
Q197 0.031 0.302 0.186 ! 0.54 eA-3
Q198 0.930 0.292 0.159 ! 0.54 eA-3
Q199 0.040 0.218 0.432 ! 0.54 eA-3
)
;
_shelx_fab_checksum 3315
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn Sn1 0.000000 0.20944(3) 0.250000 0.01902(10) Uani d 1 . .
O O1 -0.06248(9) 0.0370(2) 0.19456(11) 0.0248(4) Uani d 1 . .
O O2 -0.10242(10) 0.2366(2) 0.16188(12) 0.0247(4) Uani d 1 . .
O O3 0.000000 0.4408(3) 0.250000 0.0353(8) Uani d 1 . .
H H3 0.0301(14) 0.476(4) 0.2841(16) 0.051(13) Uiso d 1 . .
O O10 -0.43538(10) -0.1170(2) -0.14546(12) 0.0303(5) Uani d 1 . .
N N1 -0.34338(12) -0.1205(3) -0.01611(14) 0.0255(5) Uani d 1 . .
H H1 -0.3581(18) -0.084(4) -0.055(2) 0.033(10) Uiso d 1 . .
C C1 -0.10849(13) 0.1113(3) 0.15772(15) 0.0213(6) Uani d 1 . .
C C2 -0.16937(13) 0.0487(3) 0.11166(15) 0.0222(6) Uani d 1 . .
C C3 -0.17658(13) -0.0879(3) 0.11204(16) 0.0239(6) Uani d 1 . .
H H3A -0.142047 -0.141854 0.140536 0.029 Uiso calc 1 . .
C C4 -0.23372(14) -0.1456(3) 0.07121(17) 0.0261(6) Uani d 1 . .
H H4 -0.238480 -0.238854 0.071822 0.031 Uiso calc 1 . .
C C5 -0.28419(13) -0.0668(3) 0.02923(15) 0.0236(6) Uani d 1 . .
C C6 -0.27703(14) 0.0703(3) 0.02811(17) 0.0268(6) Uani d 1 . .
H H6 -0.311396 0.124213 -0.000880 0.032 Uiso calc 1 . .
C C7 -0.21968(14) 0.1274(3) 0.06939(17) 0.0277(6) Uani d 1 . .
H H7 -0.214750 0.220631 0.068782 0.033 Uiso calc 1 . .
C C8 -0.37763(15) -0.2072(3) -0.00003(18) 0.0291(7) Uani d 1 . .
C C9 -0.43476(15) -0.2480(3) -0.05114(18) 0.0263(6) Uani d 1 . .
H H9 -0.457607 -0.310895 -0.037549 0.032 Uiso calc 1 . .
C C10 -0.46156(15) -0.2012(3) -0.12320(18) 0.0258(6) Uani d 1 . .
C C11 -0.52313(16) -0.2589(4) -0.17386(18) 0.0322(7) Uani d 1 . .
H H11A -0.547018 -0.285054 -0.146995 0.048 Uiso calc 1 . .
H H11B -0.515815 -0.336583 -0.197729 0.048 Uiso calc 1 . .
H H11C -0.546698 -0.192478 -0.209889 0.048 Uiso calc 1 . .
C C12 -0.3541(2) -0.2594(6) 0.0753(2) 0.0541(12) Uani d 1 . .
H H12A -0.323563 -0.329840 0.082306 0.081 Uiso calc 1 . .
H H12B -0.389126 -0.294807 0.083429 0.081 Uiso calc 1 . .
H H12C -0.334203 -0.187465 0.109331 0.081 Uiso calc 1 . .
C C13 0.04032(16) 0.2193(4) 0.17412(18) 0.0316(7) Uani d 1 . .
H H13A 0.069539 0.295146 0.187002 0.038 Uiso calc 1 . .
H H13B 0.065092 0.137904 0.178904 0.038 Uiso calc 1 . .
C C14 -0.00517(15) 0.2337(3) 0.09721(17) 0.0253(6) Uani d 1 . .
C C15 -0.03435(18) 0.1238(4) 0.0575(2) 0.0372(8) Uani d 1 . .
H H15 -0.024141 0.038632 0.078874 0.045 Uiso calc 1 . .
C C16 -0.0783(2) 0.1349(5) -0.0130(2) 0.0474(10) Uani d 1 . .
H H16 -0.097970 0.058061 -0.039592 0.057 Uiso calc 1 . .
C C17 -0.0931(2) 0.2581(6) -0.0441(2) 0.0494(11) Uani d 1 . .
H H17 -0.124052 0.267139 -0.091927 0.059 Uiso calc 1 . .
C C18 -0.06295(19) 0.3685(4) -0.0056(2) 0.0436(10) Uani d 1 . .
H H18 -0.071962 0.453215 -0.027685 0.052 Uiso calc 1 . .
C C19 -0.01989(18) 0.3569(4) 0.06461(19) 0.0346(8) Uani d 1 . .
H H19 -0.000091 0.433880 0.090941 0.042 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Sn1 0.01201(14) 0.02281(16) 0.01816(14) 0.000 0.00244(10) 0.000
O1 0.0133(10) 0.0248(11) 0.0282(10) -0.0007(8) 0.0008(8) -0.0012(9)
O2 0.0183(10) 0.0220(11) 0.0292(11) -0.0009(8) 0.0057(9) -0.0012(9)
O3 0.039(2) 0.0160(15) 0.0325(18) 0.000 -0.0025(16) 0.000
O10 0.0229(11) 0.0344(13) 0.0259(11) -0.0022(10) 0.0030(9) 0.0022(10)
N1 0.0153(12) 0.0317(14) 0.0215(12) -0.0003(10) 0.0002(10) 0.0034(11)
C1 0.0156(13) 0.0229(14) 0.0236(13) -0.0010(11) 0.0067(11) -0.0015(11)
C2 0.0161(13) 0.0283(15) 0.0198(12) -0.0009(11) 0.0052(11) -0.0017(11)
C3 0.0141(13) 0.0286(15) 0.0240(13) 0.0037(11) 0.0033(11) -0.0021(12)
C4 0.0204(14) 0.0228(15) 0.0304(15) -0.0019(12) 0.0061(12) -0.0057(13)
C5 0.0158(13) 0.0309(16) 0.0211(13) -0.0027(11) 0.0050(11) -0.0020(12)
C6 0.0139(13) 0.0311(16) 0.0294(15) 0.0016(12) 0.0034(12) 0.0091(13)
C7 0.0212(15) 0.0269(15) 0.0294(15) -0.0012(12) 0.0055(12) 0.0051(13)
C8 0.0205(15) 0.0376(18) 0.0271(15) -0.0012(13) 0.0079(12) 0.0009(13)
C9 0.0209(15) 0.0276(14) 0.0288(15) -0.0022(12) 0.0089(12) 0.0002(13)
C10 0.0190(14) 0.0257(15) 0.0282(15) 0.0012(12) 0.0057(12) -0.0040(12)
C11 0.0206(16) 0.0419(19) 0.0277(16) -0.0037(14) 0.0039(13) -0.0031(14)
C12 0.032(2) 0.091(3) 0.0306(19) -0.021(2) 0.0044(16) 0.017(2)
C13 0.0213(15) 0.046(2) 0.0287(16) -0.0012(14) 0.0116(13) -0.0015(14)
C14 0.0218(15) 0.0290(17) 0.0265(15) 0.0010(12) 0.0118(12) -0.0011(12)
C15 0.045(2) 0.0318(18) 0.0383(18) -0.0037(16) 0.0206(17) -0.0007(16)
C16 0.046(2) 0.062(3) 0.0314(18) -0.016(2) 0.0139(17) -0.0117(19)
C17 0.034(2) 0.086(3) 0.0244(17) 0.008(2) 0.0086(15) 0.003(2)
C18 0.047(2) 0.050(2) 0.042(2) 0.0243(19) 0.0264(18) 0.0200(19)
C19 0.043(2) 0.0318(19) 0.0389(18) 0.0051(15) 0.0266(17) 0.0031(15)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 Sn1 O1 . 2 78.94(11) y
O1 Sn1 O2 . . 57.26(8) y
O1 Sn1 O2 . 2 136.18(8) y
O1 Sn1 O3 . . 140.53(5) y
O1 Sn1 C13 . . 93.73(11) y
O1 Sn1 C13 . 2 90.36(11) y
O2 Sn1 O2 . 2 166.56(11) y
O2 Sn1 O3 . . 83.28(6) y
O2 Sn1 C13 . . 93.61(11) y
O2 Sn1 C13 . 2 85.77(11) y
O3 Sn1 C13 . . 87.35(10) y
C13 Sn1 C13 . 2 174.7(2) y
C1 O1 Sn1 . . 93.31(18) ?
C1 O2 Sn1 . . 89.18(17) ?
Sn1 O3 H3 . . 115(3) ?
Sn1 O3 H3 . 2 115(3) ?
H3 O3 H3 . 2 130(7) ?
C8 N1 C5 . . 128.6(3) ?
C8 N1 H1 . . 120(3) ?
C5 N1 H1 . . 111(3) ?
O2 C1 O1 . . 120.1(3) ?
O2 C1 C2 . . 121.1(3) ?
O1 C1 C2 . . 118.7(3) ?
C7 C2 C3 . . 119.8(3) ?
C7 C2 C1 . . 119.8(3) ?
C3 C2 C1 . . 120.4(3) ?
C4 C3 C2 . . 120.4(3) ?
C4 C3 H3A . . 119.8 ?
C2 C3 H3A . . 119.8 ?
C3 C4 C5 . . 119.9(3) ?
C3 C4 H4 . . 120.1 ?
C5 C4 H4 . . 120.1 ?
C4 C5 C6 . . 120.0(3) ?
C4 C5 N1 . . 122.5(3) ?
C6 C5 N1 . . 117.4(3) ?
C7 C6 C5 . . 119.8(3) ?
C7 C6 H6 . . 120.1 ?
C5 C6 H6 . . 120.1 ?
C6 C7 C2 . . 120.2(3) ?
C6 C7 H7 . . 119.9 ?
C2 C7 H7 . . 119.9 ?
N1 C8 C9 . . 120.8(3) ?
N1 C8 C12 . . 119.4(3) ?
C9 C8 C12 . . 119.9(3) ?
C8 C9 C10 . . 123.8(3) ?
C8 C9 H9 . . 118.1 ?
C10 C9 H9 . . 118.1 ?
O10 C10 C9 . . 122.5(3) ?
O10 C10 C11 . . 119.6(3) ?
C9 C10 C11 . . 117.8(3) ?
C10 C11 H11A . . 109.5 ?
C10 C11 H11B . . 109.5 ?
H11A C11 H11B . . 109.5 ?
C10 C11 H11C . . 109.5 ?
H11A C11 H11C . . 109.5 ?
H11B C11 H11C . . 109.5 ?
C8 C12 H12A . . 109.5 ?
C8 C12 H12B . . 109.5 ?
H12A C12 H12B . . 109.5 ?
C8 C12 H12C . . 109.5 ?
H12A C12 H12C . . 109.5 ?
H12B C12 H12C . . 109.5 ?
C14 C13 Sn1 . . 115.6(2) ?
C14 C13 H13A . . 108.4 ?
Sn1 C13 H13A . . 108.4 ?
C14 C13 H13B . . 108.4 ?
Sn1 C13 H13B . . 108.4 ?
H13A C13 H13B . . 107.4 ?
C15 C14 C19 . . 118.4(3) ?
C15 C14 C13 . . 120.3(3) ?
C19 C14 C13 . . 121.3(3) ?
C14 C15 C16 . . 121.4(4) ?
C14 C15 H15 . . 119.3 ?
C16 C15 H15 . . 119.3 ?
C17 C16 C15 . . 119.4(4) ?
C17 C16 H16 . . 120.3 ?
C15 C16 H16 . . 120.3 ?
C16 C17 C18 . . 119.7(4) ?
C16 C17 H17 . . 120.1 ?
C18 C17 H17 . . 120.1 ?
C19 C18 C17 . . 120.5(4) ?
C19 C18 H18 . . 119.7 ?
C17 C18 H18 . . 119.7 ?
C18 C19 C14 . . 120.5(4) ?
C18 C19 H19 . . 119.8 ?
C14 C19 H19 . . 119.8 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Sn1 O1 . 2.257(2) y
Sn1 O2 . 2.348(2) y
Sn1 O3 . 2.337(3) y
Sn1 C13 . 2.150(3) y
O1 C1 . 1.274(4) ?
O2 C1 . 1.273(4) ?
O3 H3 . 0.838(7) ?
O10 C10 . 1.248(4) y
N1 C5 . 1.421(4) y
N1 C8 . 1.327(4) y
N1 H1 . 0.82(4) ?
C1 C2 . 1.489(4) ?
C2 C7 . 1.389(4) ?
C2 C3 . 1.391(4) ?
C3 C4 . 1.382(4) ?
C3 H3A . 0.9500 ?
C4 C5 . 1.390(4) ?
C4 H4 . 0.9500 ?
C5 C6 . 1.397(5) ?
C6 C7 . 1.385(4) ?
C6 H6 . 0.9500 ?
C7 H7 . 0.9500 ?
C8 C9 . 1.378(5) y
C8 C12 . 1.505(5) ?
C9 C10 . 1.425(5) y
C9 H9 . 0.9500 ?
C10 C11 . 1.504(4) ?
C11 H11A . 0.9800 ?
C11 H11B . 0.9800 ?
C11 H11C . 0.9800 ?
C12 H12A . 0.9800 ?
C12 H12B . 0.9800 ?
C12 H12C . 0.9800 ?
C13 C14 . 1.498(5) ?
C13 H13A . 0.9900 ?
C13 H13B . 0.9900 ?
C14 C15 . 1.378(5) ?
C14 C19 . 1.388(5) ?
C15 C16 . 1.386(5) ?
C15 H15 . 0.9500 ?
C16 C17 . 1.376(7) ?
C16 H16 . 0.9500 ?
C17 C18 . 1.380(7) ?
C17 H17 . 0.9500 ?
C18 C19 . 1.376(5) ?
C18 H18 . 0.9500 ?
C19 H19 . 0.9500 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
N1 H1 O10 . 0.82(4) 2.01(4) 2.631(3) 132(4) yes
O3 H3 O10 8_556 0.838(7) 1.95(2) 2.712(3) 151(4) yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Sn1 O2 C1 O1 . . . . -3.3(3) ?
Sn1 O2 C1 C2 . . . . 175.1(2) ?
Sn1 O1 C1 O2 . . . . 3.4(3) ?
Sn1 O1 C1 C2 . . . . -175.0(2) ?
O2 C1 C2 C7 . . . . 3.5(4) ?
O1 C1 C2 C7 . . . . -178.1(3) ?
O2 C1 C2 C3 . . . . -174.9(3) ?
O1 C1 C2 C3 . . . . 3.5(4) ?
C7 C2 C3 C4 . . . . -0.7(5) ?
C1 C2 C3 C4 . . . . 177.7(3) ?
C2 C3 C4 C5 . . . . 0.3(5) ?
C3 C4 C5 C6 . . . . 0.3(5) ?
C3 C4 C5 N1 . . . . 177.4(3) ?
C8 N1 C5 C4 . . . . 51.0(5) ?
C8 N1 C5 C6 . . . . -131.8(4) ?
C4 C5 C6 C7 . . . . -0.6(5) ?
N1 C5 C6 C7 . . . . -177.8(3) ?
C5 C6 C7 C2 . . . . 0.2(5) ?
C3 C2 C7 C6 . . . . 0.5(5) ?
C1 C2 C7 C6 . . . . -177.9(3) ?
C5 N1 C8 C9 . . . . 179.5(3) ?
C5 N1 C8 C12 . . . . 0.6(6) ?
N1 C8 C9 C10 . . . . -0.6(5) ?
C12 C8 C9 C10 . . . . 178.2(4) ?
C8 C9 C10 O10 . . . . -1.2(5) ?
C8 C9 C10 C11 . . . . 177.5(3) ?
Sn1 C13 C14 C15 . . . . -83.5(4) ?
Sn1 C13 C14 C19 . . . . 95.3(3) ?
C19 C14 C15 C16 . . . . -1.2(5) ?
C13 C14 C15 C16 . . . . 177.7(3) ?
C14 C15 C16 C17 . . . . 0.0(6) ?
C15 C16 C17 C18 . . . . 1.8(6) ?
C16 C17 C18 C19 . . . . -2.6(6) ?
C17 C18 C19 C14 . . . . 1.4(5) ?
C15 C14 C19 C18 . . . . 0.4(5) ?
C13 C14 C19 C18 . . . . -178.4(3) ?
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.250 -0.056 0.250 324 85 ' '
2 0.750 0.016 0.250 324 85 ' '
3 0.250 -0.003 0.750 325 85 ' '
4 0.750 -0.073 0.750 325 85 ' '
_cod_database_fobs_code 2022352