#------------------------------------------------------------------------------ #$Date: 2021-04-10 07:45:59 +0300 (Sat, 10 Apr 2021) $ #$Revision: 264028 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/23/2022354.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022354 _cell_angle_alpha 76.371 _cell_angle_beta 75.521 _cell_angle_gamma 88.161 _cell_length_a 12.0054 _cell_length_b 14.7309 _cell_length_c 23.9132 _exptl_crystal_F_000 1768.00 _reflns_d_resolution_high 0.8396 _cod_data_source_file ov3150Vsup6.hkl _cod_data_source_block V _shelx_title ' TSBB-71 (L0403)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 570.10 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1651.57 1314.16 149.46 o 3 0 0 1455.58 1417.62 54.83 o 4 0 0 30424.34 26837.16 383.84 o 5 0 0 63098.83 63215.89 927.68 o 6 0 0 11392.56 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