#------------------------------------------------------------------------------ #$Date: 2021-04-10 07:47:18 +0300 (Sat, 10 Apr 2021) $ #$Revision: 264029 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/23/2022355.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022355 _cell_angle_alpha 89.116 _cell_angle_beta 87.262 _cell_angle_gamma 89.258 _cell_length_a 9.4872 _cell_length_b 10.7297 _cell_length_c 25.9197 _exptl_crystal_F_000 1336.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file ov31461sup2.hkl _cod_data_source_block 1 _shelx_title ' p-1_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 373.21 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 3646.56 4133.53 19.38 o 2 0 0 54.62 126.52 14.92 o 3 0 0 114.44 126.16 9.55 o 4 0 0 17375.57 18567.35 440.28 o 5 0 0 2711.92 2793.10 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235.77 107.66 o 1 -1 28 5.60 17.23 105.50 o 3 -1 28 86.95 100.12 106.58 o 4 -1 28 9.95 1.81 65.38 o 5 -1 28 249.35 161.49 107.66 o 6 -1 28 227.98 366.04 127.57 o -5 0 28 410.86 438.56 114.66 o -4 0 28 6.89 -32.58 91.93 o -3 0 28 1072.10 1093.95 96.39 o -2 0 28 77.72 118.99 87.46 o -1 0 28 1121.68 1134.44 93.48 o 0 0 28 2.50 111.68 86.00 o 2 0 28 53.55 44.14 98.51 o 3 0 28 2137.89 2371.71 132.42 o 4 0 28 1102.32 1105.11 119.50 o 5 0 28 599.37 662.10 125.42 o 6 0 28 37.35 135.11 117.35 o -5 1 28 247.86 369.84 103.87 o -4 1 28 249.48 213.02 91.21 o -3 1 28 175.54 227.41 90.78 o -2 1 28 131.24 122.01 85.72 o -1 1 28 1196.80 1253.14 149.11 o 0 1 28 486.02 563.50 151.53 o 1 1 28 516.07 553.36 107.66 o 2 1 28 65.88 129.19 105.50 o 3 1 28 298.68 421.48 108.73 o 4 1 28 56.70 103.35 110.35 o 5 1 28 711.66 693.32 122.73 o 6 1 28 37.22 90.43 122.19 o -4 2 28 608.96 673.52 97.78 o -3 2 28 505.95 575.96 90.92 o -2 2 28 231.23 327.43 89.20 o -1 2 28 101.15 206.52 82.75 o 0 2 28 587.84 556.33 84.19 o 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