#------------------------------------------------------------------------------ #$Date: 2021-04-23 12:55:31 +0300 (Fri, 23 Apr 2021) $ #$Revision: 264474 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/23/2022362.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022362 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 3.7738 _cell_length_b 5.6349 _cell_length_c 32.9787 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.7862 _cod_data_source_file fm30636sup5.hkl _cod_data_source_block 6 _shelx_title ' a_1961_1_a.res in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 81.21 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1217.07 1218.68 19.31 o 4 0 0 748.83 746.95 27.59 o 1 1 0 1537.38 1590.56 16.99 o 2 1 0 2892.48 2865.32 25.52 o 3 1 0 25.07 26.64 1.00 o 4 1 0 226.34 228.21 8.38 o 0 2 0 1333.28 1308.24 15.78 o 1 2 0 54.47 71.26 1.54 o 2 2 0 38.40 32.53 0.98 o 3 2 0 47.34 53.38 1.98 o 4 2 0 300.67 291.88 8.81 o 1 3 0 156.71 143.83 1.82 o 2 3 0 538.81 502.63 4.84 o 3 3 0 115.88 120.46 4.15 o 4 3 0 272.22 262.39 8.14 o 0 4 0 1530.26 1561.95 14.36 o 1 4 0 53.92 55.45 1.13 o 2 4 0 8.05 11.02 0.64 o 3 4 0 1.13 1.12 0.40 o 1 5 0 1.23 1.10 0.34 o 2 5 0 78.96 94.42 2.12 o 3 5 0 122.99 116.54 3.29 o 0 6 0 387.20 389.78 7.11 o 1 6 0 110.64 112.27 2.26 o 2 6 0 76.83 77.59 4.14 o 1 0 1 3117.75 2848.98 58.02 o 2 0 1 60.78 55.44 1.37 o 3 0 1 41.72 42.34 1.41 o 4 0 1 32.18 31.99 1.66 o -4 1 1 18.82 21.41 1.51 o -3 1 1 383.50 361.45 4.45 o -2 1 1 247.10 263.03 3.90 o -1 1 1 4048.12 3881.97 45.10 o 0 1 1 195.42 185.03 2.07 o 1 1 1 3706.08 3581.53 38.11 o 2 1 1 234.64 244.13 3.26 o 3 1 1 350.65 337.73 4.59 o 4 1 1 18.01 19.03 1.69 o -4 2 1 89.88 89.98 3.57 o -3 2 1 12.65 14.59 0.91 o -2 2 1 225.85 250.61 3.89 o -1 2 1 203.22 180.00 2.53 o 0 2 1 82.26 83.06 1.39 o 1 2 1 268.35 245.04 3.87 o 2 2 1 233.58 258.16 3.23 o 3 2 1 9.76 10.57 0.89 o 4 2 1 94.21 94.59 4.33 o -4 3 1 101.25 91.11 3.88 o -3 3 1 464.63 455.34 8.53 o -2 3 1 23.50 21.25 0.77 o -1 3 1 273.43 294.42 2.88 o 0 3 1 1.26 0.54 0.17 o 1 3 1 358.95 382.89 3.71 o 2 3 1 25.34 22.58 0.76 o 3 3 1 388.10 388.25 6.55 o 4 3 1 109.35 94.84 4.05 o -3 4 1 155.55 147.52 3.30 o -2 4 1 109.47 106.87 1.92 o -1 4 1 373.80 355.42 3.38 o 0 4 1 132.08 138.19 1.63 o 1 4 1 415.71 390.60 3.53 o 2 4 1 115.94 117.35 1.98 o 3 4 1 145.86 138.48 2.90 o -3 5 1 140.54 140.96 4.19 o -2 5 1 4.43 3.84 0.50 o -1 5 1 186.72 182.77 2.70 o 0 5 1 14.13 15.50 0.62 o 1 5 1 203.01 196.48 2.55 o 2 5 1 3.29 3.05 0.51 o 3 5 1 153.01 155.02 3.94 o -2 6 1 44.06 47.99 1.56 o -1 6 1 323.72 327.34 4.32 o 0 6 1 1.58 1.44 0.42 o 1 6 1 322.80 338.44 5.29 o 2 6 1 46.37 49.68 2.04 o 0 7 1 0.87 1.02 0.76 o 1 0 2 5235.71 4930.03 103.19 o 2 0 2 7.26 16.78 0.81 o 3 0 2 764.30 729.10 7.68 o 4 0 2 157.45 152.82 3.98 o -4 1 2 235.94 224.11 6.43 o -3 1 2 208.44 212.65 3.13 o -2 1 2 2492.72 2445.50 30.23 o -1 1 2 5889.30 5729.68 54.32 o 0 1 2 5051.23 4869.81 46.24 o 1 1 2 5821.76 5577.49 64.07 o 2 1 2 2470.27 2394.33 24.63 o 3 1 2 209.98 222.78 3.59 o 4 1 2 246.52 240.72 7.87 o -4 2 2 109.81 105.29 3.15 o -3 2 2 209.54 211.46 3.93 o -2 2 2 1231.72 1265.12 12.22 o -1 2 2 262.29 284.46 3.77 o 0 2 2 5064.78 4937.02 39.38 o 1 2 2 298.26 318.86 4.49 o 2 2 2 1295.56 1344.79 11.29 o 3 2 2 186.23 187.18 3.51 o 4 2 2 120.30 117.08 4.16 o -4 3 2 115.70 115.36 4.58 o -3 3 2 55.57 53.81 2.22 o -2 3 2 369.50 358.20 3.53 o -1 3 2 260.37 251.63 2.63 o 0 3 2 152.95 153.48 1.76 o 1 3 2 280.67 264.07 3.07 o 2 3 2 360.02 352.82 3.53 o 3 3 2 55.95 54.28 1.85 o 4 3 2 122.64 120.24 4.45 o -3 4 2 3.45 6.03 0.72 o -2 4 2 110.73 102.51 2.41 o -1 4 2 60.23 61.42 1.13 o 0 4 2 171.36 150.27 1.73 o 1 4 2 63.86 63.91 1.21 o 2 4 2 126.72 116.83 2.61 o 3 4 2 0.84 2.29 0.45 o -3 5 2 13.24 14.84 1.70 o -2 5 2 412.12 380.28 6.63 o -1 5 2 36.89 40.98 1.22 o 0 5 2 155.28 148.77 2.01 o 1 5 2 42.45 45.92 1.22 o 2 5 2 471.01 448.18 7.76 o 3 5 2 15.10 17.20 1.18 o -2 6 2 14.08 11.73 0.79 o -1 6 2 26.42 28.00 1.15 o 0 6 2 180.74 190.04 3.10 o 1 6 2 22.49 24.16 1.03 o 2 6 2 7.18 5.73 0.68 o 0 7 2 34.41 37.04 2.55 o 1 0 3 295.00 330.68 4.66 o 2 0 3 999.68 965.94 14.37 o 3 0 3 34.71 37.30 1.33 o 4 0 3 10.39 12.03 0.98 o -4 1 3 33.53 31.66 2.83 o -3 1 3 542.59 530.66 6.26 o -2 1 3 553.34 558.77 6.40 o -1 1 3 2785.26 2732.23 27.78 o 0 1 3 59.79 67.24 1.55 o 1 1 3 2844.37 2752.61 29.76 o 2 1 3 603.20 611.35 6.78 o 3 1 3 595.99 595.17 6.93 o 4 1 3 22.80 20.74 1.65 o -4 2 3 99.08 93.66 3.18 o -3 2 3 45.82 43.22 1.65 o -2 2 3 132.33 139.01 2.62 o -1 2 3 2049.63 2082.54 21.11 o 0 2 3 4.00 6.35 0.37 o 1 2 3 2100.67 2153.84 30.31 o 2 2 3 89.76 99.17 1.95 o 3 2 3 39.91 38.66 1.46 o 4 2 3 94.13 91.53 4.48 o -4 3 3 69.27 68.02 2.92 o -3 3 3 550.65 554.49 10.98 o -2 3 3 47.00 47.61 1.11 o -1 3 3 905.53 922.40 6.81 o 0 3 3 62.02 86.28 1.24 o 1 3 3 846.13 853.92 7.34 o 2 3 3 57.58 54.36 1.16 o 3 3 3 497.09 500.19 7.08 o 4 3 3 57.44 59.90 3.75 o -3 4 3 2.39 3.99 0.58 o -2 4 3 334.61 319.15 4.61 o -1 4 3 698.22 662.00 4.74 o 0 4 3 11.00 13.85 0.49 o 1 4 3 635.49 606.28 4.66 o 2 4 3 334.80 310.78 4.22 o 3 4 3 2.04 1.99 0.50 o -3 5 3 295.30 288.56 6.80 o -2 5 3 28.98 30.03 1.74 o -1 5 3 406.80 391.38 4.64 o 0 5 3 189.42 193.03 2.45 o 1 5 3 395.29 382.26 4.51 o 2 5 3 38.05 43.71 1.37 o 3 5 3 270.37 281.73 7.55 o -2 6 3 52.07 48.85 1.58 o -1 6 3 87.54 99.20 2.43 o 0 6 3 102.52 101.71 2.31 o 1 6 3 95.59 104.48 2.15 o 2 6 3 35.63 33.13 1.37 o 0 7 3 205.71 231.87 10.05 o 0 0 4 120.58 108.64 3.40 o 1 0 4 3720.63 3556.95 78.44 o 2 0 4 302.30 306.43 5.64 o 3 0 4 574.17 560.29 7.35 o 4 0 4 3.17 3.78 0.61 o -4 1 4 85.30 92.43 3.79 o -3 1 4 97.15 102.40 2.12 o -2 1 4 501.77 506.04 5.79 o -1 1 4 2973.14 2913.06 28.20 o 0 1 4 20.17 22.76 0.66 o 1 1 4 3201.28 3205.08 36.09 o 2 1 4 635.19 646.01 6.65 o 3 1 4 88.61 91.68 1.91 o 4 1 4 112.84 111.29 4.30 o -4 2 4 26.78 28.74 2.17 o -3 2 4 1029.02 1006.45 10.44 o -2 2 4 116.81 128.42 2.32 o -1 2 4 1097.39 1106.19 12.41 o 0 2 4 7.35 10.16 0.47 o 1 2 4 1044.18 1081.10 16.16 o 2 2 4 143.21 151.38 2.46 o 3 2 4 1032.74 1011.48 11.59 o 4 2 4 31.32 32.56 2.23 o -4 3 4 253.53 238.57 6.55 o -3 3 4 150.71 143.06 3.87 o -2 3 4 313.40 301.88 3.54 o -1 3 4 172.26 178.93 1.92 o 0 3 4 594.11 658.33 5.50 o 1 3 4 132.41 140.29 1.74 o 2 3 4 301.03 287.06 3.13 o 3 3 4 152.74 148.55 2.94 o 4 3 4 278.00 299.52 15.44 o -3 4 4 188.50 187.25 3.60 o -2 4 4 351.95 341.87 4.91 o -1 4 4 70.44 72.27 1.17 o 0 4 4 372.12 348.22 2.95 o 1 4 4 91.23 92.95 1.47 o 2 4 4 333.16 320.39 4.81 o 3 4 4 220.73 211.65 3.80 o -3 5 4 8.89 10.26 0.87 o -2 5 4 158.12 150.34 5.01 o -1 5 4 109.78 103.14 1.96 o 0 5 4 12.78 12.01 0.58 o 1 5 4 143.82 138.37 2.23 o 2 5 4 135.82 127.59 2.55 o 3 5 4 8.15 8.70 0.75 o -2 6 4 130.00 137.61 6.00 o -1 6 4 83.88 77.78 2.19 o 0 6 4 150.12 147.09 2.77 o 1 6 4 103.93 98.12 2.45 o 2 6 4 117.91 127.43 3.11 o 0 7 4 69.97 66.65 3.99 o 1 0 5 4738.95 4518.78 100.09 o 2 0 5 300.20 274.69 5.56 o 3 0 5 70.99 71.33 2.11 o 4 0 5 8.09 9.68 0.84 o -4 1 5 73.65 74.51 4.18 o -3 1 5 89.52 92.81 2.11 o -2 1 5 3.86 5.43 0.74 o -1 1 5 11.12 10.45 0.43 o 0 1 5 1124.77 1121.32 18.26 o 1 1 5 3.95 3.65 0.37 o 2 1 5 12.89 13.46 0.61 o 3 1 5 88.45 93.26 1.92 o 4 1 5 91.02 90.53 3.77 o -4 2 5 74.61 78.49 3.28 o -3 2 5 436.49 437.25 6.38 o -2 2 5 2400.61 2411.36 20.52 o -1 2 5 638.97 621.28 7.98 o 0 2 5 1499.59 1532.04 14.41 o 1 2 5 606.09 614.66 12.79 o 2 2 5 2352.92 2319.05 19.51 o 3 2 5 440.41 446.82 7.01 o 4 2 5 86.73 93.25 3.26 o -4 3 5 185.00 171.86 5.22 o -3 3 5 278.00 254.16 5.99 o -2 3 5 317.73 320.55 3.82 o -1 3 5 444.52 454.27 3.86 o 0 3 5 1489.54 1483.28 11.55 o 1 3 5 460.73 486.77 7.95 o 2 3 5 312.92 312.66 3.13 o 3 3 5 286.30 274.70 4.86 o 4 3 5 148.98 148.23 9.49 o -3 4 5 22.51 25.60 1.21 o -2 4 5 400.47 390.74 5.65 o -1 4 5 421.48 438.75 3.70 o 0 4 5 34.45 32.85 0.81 o 1 4 5 397.26 416.45 3.67 o 2 4 5 359.17 335.40 3.66 o 3 4 5 21.08 24.11 1.18 o -3 5 5 106.76 97.95 15.31 o -2 5 5 5.16 5.79 0.66 o -1 5 5 48.34 47.53 1.57 o 0 5 5 1151.31 1103.75 9.34 o 1 5 5 37.31 38.79 1.10 o 2 5 5 2.16 1.90 0.40 o 3 5 5 106.58 110.65 4.57 o -2 6 5 767.44 801.52 18.62 o -1 6 5 268.99 263.14 5.05 o 0 6 5 28.48 28.52 1.11 o 1 6 5 288.33 276.95 6.08 o 2 6 5 772.95 794.30 13.48 o 0 7 5 100.25 120.89 4.88 o 0 0 6 318.25 341.27 5.75 o 1 0 6 2.49 2.19 0.35 o 2 0 6 0.17 0.59 0.28 o 3 0 6 403.37 374.38 5.29 o 4 0 6 1.50 1.65 0.51 o -4 1 6 94.22 103.50 4.74 o -3 1 6 113.13 117.42 2.59 o -2 1 6 385.79 398.95 4.83 o -1 1 6 658.29 588.36 6.85 o 0 1 6 169.25 169.99 4.42 o 1 1 6 614.07 554.47 6.41 o 2 1 6 351.85 363.75 4.04 o 3 1 6 124.01 129.47 2.33 o 4 1 6 80.96 77.04 4.00 o -4 2 6 137.61 139.97 4.65 o -3 2 6 489.02 486.32 7.31 o -2 2 6 56.47 62.20 1.58 o -1 2 6 128.83 131.65 2.41 o 0 2 6 1327.01 1288.71 12.33 o 1 2 6 98.26 103.33 2.47 o 2 2 6 51.31 55.17 1.35 o 3 2 6 596.82 594.88 10.66 o 4 2 6 144.24 147.37 4.27 o -4 3 6 37.56 32.21 2.76 o -3 3 6 94.80 92.06 2.98 o -2 3 6 79.44 76.24 1.68 o -1 3 6 1058.25 1003.65 7.32 o 0 3 6 30.44 31.81 0.65 o 1 3 6 1096.78 1051.88 8.63 o 2 3 6 82.10 80.11 1.34 o 3 3 6 84.98 82.09 2.27 o 4 3 6 39.32 28.44 3.83 o -3 4 6 304.08 301.83 5.02 o -2 4 6 18.98 19.71 0.87 o -1 4 6 47.68 50.58 0.99 o 0 4 6 294.79 303.34 3.27 o 1 4 6 25.68 27.37 0.77 o 2 4 6 21.18 23.99 0.85 o 3 4 6 273.22 274.79 6.26 o -3 5 6 115.63 94.92 7.47 o -2 5 6 101.27 103.09 2.64 o -1 5 6 582.53 574.56 5.81 o 0 5 6 185.91 172.04 2.35 o 1 5 6 496.87 491.73 7.01 o 2 5 6 96.43 101.03 1.91 o 3 5 6 125.89 129.25 5.04 o -2 6 6 98.69 94.42 6.36 o -1 6 6 137.48 146.05 4.61 o 0 6 6 200.82 196.99 3.15 o 1 6 6 151.71 154.27 3.20 o 2 6 6 104.75 102.26 4.03 o 0 7 6 56.91 55.48 3.00 o 1 0 7 8.56 8.93 0.59 o 2 0 7 664.67 638.39 10.45 o 3 0 7 24.13 21.89 1.12 o 4 0 7 412.56 433.69 7.65 o -4 1 7 148.87 158.14 5.17 o -3 1 7 270.26 271.43 4.33 o -2 1 7 272.29 268.00 3.40 o -1 1 7 499.78 486.08 6.20 o 0 1 7 6595.40 6073.82 68.00 o 1 1 7 512.85 514.15 6.78 o 2 1 7 259.01 256.81 3.73 o 3 1 7 262.08 261.76 3.60 o 4 1 7 135.63 141.94 5.15 o -4 2 7 118.79 124.00 4.29 o -3 2 7 186.89 185.16 4.64 o -2 2 7 283.11 291.88 3.96 o -1 2 7 79.21 74.03 1.49 o 0 2 7 114.59 133.42 2.27 o 1 2 7 77.44 74.75 1.89 o 2 2 7 371.15 374.81 4.18 o 3 2 7 190.60 191.07 3.87 o 4 2 7 106.95 113.52 4.95 o -4 3 7 422.09 402.39 13.90 o -3 3 7 15.56 15.36 1.25 o -2 3 7 56.03 53.33 1.31 o -1 3 7 200.23 201.75 2.28 o 0 3 7 3010.40 3023.15 20.07 o 1 3 7 207.07 208.20 2.74 o 2 3 7 59.93 60.09 1.18 o 3 3 7 16.44 15.13 0.94 o 4 3 7 429.83 406.81 17.94 o -3 4 7 57.57 50.89 1.68 o -2 4 7 1223.02 1246.61 13.92 o -1 4 7 3.64 4.29 0.37 o 0 4 7 7.07 9.78 0.46 o 1 4 7 4.35 5.85 0.41 o 2 4 7 1155.43 1181.60 13.79 o 3 4 7 59.68 54.32 1.89 o -3 5 7 12.07 10.50 2.03 o -2 5 7 192.52 200.78 4.80 o -1 5 7 386.72 367.72 4.34 o 0 5 7 1310.93 1319.33 9.86 o 1 5 7 399.45 380.44 4.21 o 2 5 7 183.10 191.23 4.04 o 3 5 7 13.08 11.39 1.57 o -2 6 7 169.69 205.24 10.64 o -1 6 7 182.42 189.68 3.09 o 0 6 7 137.50 129.84 2.44 o 1 6 7 184.21 188.68 3.07 o 2 6 7 195.16 178.77 10.01 o 0 7 7 141.21 137.25 5.08 o 0 0 8 245.96 248.18 5.12 o 1 0 8 289.38 278.12 4.19 o 2 0 8 16.28 18.20 0.90 o 3 0 8 127.73 125.57 3.08 o 4 0 8 46.86 45.73 2.40 o -4 1 8 2.89 3.38 0.95 o -3 1 8 87.26 87.53 2.09 o -2 1 8 148.71 142.88 2.44 o -1 1 8 1668.03 1565.48 18.82 o 0 1 8 227.09 228.95 2.91 o 1 1 8 1852.55 1827.57 22.62 o 2 1 8 142.71 140.88 2.25 o 3 1 8 79.52 82.10 1.84 o 4 1 8 2.16 3.32 0.68 o -4 2 8 232.70 239.15 7.77 o -3 2 8 270.44 264.27 5.17 o -2 2 8 0.91 1.38 0.35 o -1 2 8 371.20 333.35 4.89 o 0 2 8 304.94 262.47 6.88 o 1 2 8 363.68 333.55 6.72 o 2 2 8 1.16 1.48 0.32 o 3 2 8 278.04 279.94 4.45 o 4 2 8 237.21 227.39 7.78 o -4 3 8 135.43 123.28 4.07 o -3 3 8 334.36 340.96 6.73 o -2 3 8 130.46 136.85 3.10 o -1 3 8 449.69 413.12 3.71 o 0 3 8 43.77 47.73 0.84 o 1 3 8 467.54 434.56 4.66 o 2 3 8 129.42 139.98 2.21 o 3 3 8 332.40 323.13 5.86 o 4 3 8 137.66 132.18 8.10 o -3 4 8 555.80 566.39 8.42 o -2 4 8 23.38 24.98 1.12 o -1 4 8 621.64 622.45 5.16 o 0 4 8 128.79 132.87 1.74 o 1 4 8 654.19 647.97 5.31 o 2 4 8 21.26 22.68 0.91 o 3 4 8 525.59 527.20 8.89 o -3 5 8 64.42 66.07 4.86 o -2 5 8 13.46 13.82 0.87 o -1 5 8 679.90 698.26 7.19 o 0 5 8 223.91 234.17 3.00 o 1 5 8 687.85 707.09 7.00 o 2 5 8 16.26 16.70 0.93 o 3 5 8 57.33 50.50 3.12 o -2 6 8 83.65 79.35 5.80 o -1 6 8 45.62 47.45 1.42 o 0 6 8 198.26 190.89 3.31 o 1 6 8 45.82 46.09 1.48 o 2 6 8 79.97 74.47 4.15 o 0 7 8 0.48 1.64 0.67 o 1 0 9 41.15 39.54 1.21 o 2 0 9 628.17 647.08 7.35 o 3 0 9 10.02 8.75 0.81 o 4 0 9 146.47 160.54 5.88 o -4 1 9 137.03 137.82 4.76 o -3 1 9 186.34 189.10 3.43 o -2 1 9 701.13 697.40 7.34 o -1 1 9 32.36 32.37 1.10 o 0 1 9 756.70 759.54 10.30 o 1 1 9 31.50 33.46 1.08 o 2 1 9 673.01 688.70 6.98 o 3 1 9 154.95 155.63 2.69 o 4 1 9 171.11 171.00 5.81 o -4 2 9 756.65 733.42 18.28 o -3 2 9 0.60 0.76 0.51 o -2 2 9 1426.56 1376.92 11.53 o -1 2 9 452.60 437.66 4.46 o 0 2 9 314.34 324.92 6.23 o 1 2 9 483.65 480.50 6.52 o 2 2 9 1415.66 1382.06 15.79 o 3 2 9 0.96 1.02 0.44 o 4 2 9 704.47 690.09 18.75 o -4 3 9 30.89 28.94 1.76 o -3 3 9 79.28 81.98 3.00 o -2 3 9 317.61 316.68 4.65 o -1 3 9 113.62 112.34 1.63 o 0 3 9 694.43 680.13 4.89 o 1 3 9 98.68 98.38 1.56 o 2 3 9 281.63 282.40 4.17 o 3 3 9 86.84 86.93 2.32 o 4 3 9 50.29 47.89 4.37 o -3 4 9 64.41 61.77 1.81 o -2 4 9 394.53 402.68 6.99 o -1 4 9 490.55 483.35 4.26 o 0 4 9 877.18 871.79 6.10 o 1 4 9 486.09 475.15 4.44 o 2 4 9 460.04 471.89 5.46 o 3 4 9 64.10 60.79 2.10 o -3 5 9 173.96 193.03 9.51 o -2 5 9 197.90 194.97 5.26 o -1 5 9 276.72 282.70 3.97 o 0 5 9 75.60 73.86 1.64 o 1 5 9 293.16 295.24 3.69 o 2 5 9 213.37 215.84 5.20 o 3 5 9 167.22 163.42 9.06 o -2 6 9 40.73 39.64 3.95 o -1 6 9 226.97 218.55 4.73 o 0 6 9 16.47 19.21 0.92 o 1 6 9 248.02 247.37 5.85 o 2 6 9 39.10 31.85 5.28 o 0 7 9 154.98 142.17 6.95 o 0 0 10 730.85 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