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Information card for entry 2022366
Preview
| Coordinates | 2022366.cif |
|---|---|
| Structure factors | 2022366.hkl |
| Original IUCr paper | HTML |
| Chemical name | [1,1'-Bis(dicyclohexylphosphanyl)ferrocene-\ κ^2^<i>P</i>,<i>P</i>'][chlorido/cyanido(0.25/1.75)]zinc(II) |
|---|---|
| Formula | C35.75 H52 Cl0.25 Fe N1.75 P2 Zn |
| Calculated formula | C35.718 H52 Cl0.282 Fe N1.718 P2 Zn |
| Title of publication | Transition-metal complexes of group 12 with 1,1'-bis(phosphanyl)ferrocene ligands |
| Authors of publication | Chaudhary, Karan; Trivedi, Manoj; Masram, Dhanraj T.; Rath, Nigam P. |
| Journal of publication | Acta Crystallographica Section C |
| Year of publication | 2021 |
| Journal volume | 77 |
| Journal issue | 5 |
| Pages of publication | 240 - 248 |
| a | 8.2992 ± 0.0006 Å |
| b | 21.6504 ± 0.0018 Å |
| c | 9.9175 ± 0.0007 Å |
| α | 90° |
| β | 112.451 ± 0.004° |
| γ | 90° |
| Cell volume | 1646.9 ± 0.2 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 11 |
| Hermann-Mauguin space group symbol | P 1 21/m 1 |
| Hall space group symbol | -P 2yb |
| Residual factor for all reflections | 0.0591 |
| Residual factor for significantly intense reflections | 0.0397 |
| Weighted residual factors for significantly intense reflections | 0.0852 |
| Weighted residual factors for all reflections included in the refinement | 0.0926 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 266202 (current) | 2021-06-06 | cif/ Updating files of 2022363, 2022364, 2022365, 2022366 Original log message: Adding full bibliography for 2022363--2022366.cif. |
2022366.cif 2022366.hkl |
| 264571 | 2021-04-27 | cif/ hkl/ Adding structures of 2022363, 2022364, 2022365, 2022366 via cif-deposit CGI script. |
2022366.cif 2022366.hkl |
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Users of the data should acknowledge the original authors of the
structural data.