#------------------------------------------------------------------------------ #$Date: 2021-05-07 08:37:56 +0300 (Fri, 07 May 2021) $ #$Revision: 265039 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/23/2022371.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022371 loop_ _publ_author_name 'Roy, Monalisa' 'Li, Keyao' 'Nisar, Madiha' 'Wong, Lawrence W.-Y.' 'Sung, Herman H.-Y.' 'Haynes, Richard K.' 'Williams, Ian D.' _publ_section_title ; Varying degrees of homostructurality in a series of cocrystals of antimalarial drug 11-azaartemisinin with salicylic acids ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first ; ; _journal_paper_doi 10.1107/S2053229621004460 _journal_volume 77 _journal_year 2021 _chemical_formula_moiety 'C7 H5 Br O3' _chemical_formula_sum 'C7 H5 Br O3' _chemical_formula_weight 217.02 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_date 2020-04-29 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 81.959(10) _cell_angle_beta 73.812(10) _cell_angle_gamma 71.352(10) _cell_formula_units_Z 2 _cell_length_a 6.9581(7) _cell_length_b 7.1413(8) _cell_length_c 8.0284(9) _cell_measurement_reflns_used 1508 _cell_measurement_temperature 100.01(10) _cell_measurement_theta_max 72.2100 _cell_measurement_theta_min 6.5420 _cell_volume 362.44(7) _computing_cell_refinement 'CrysAlisPro 1.171.40.69a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.40.69a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.69a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.01(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.1788 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 0.981 _diffrn_measured_fraction_theta_max 0.943 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -3.00 33.00 1.00 1.00 -- -39.95 37.00 60.00 36 2 \w -64.00 -7.00 1.00 1.00 -- -39.95 37.00 60.00 57 3 \w -19.00 73.00 1.00 1.00 -- 39.95 -77.00 120.00 92 4 \w -36.00 60.00 1.00 1.00 -- 39.95 -37.00-150.00 96 5 \w 75.00 109.00 1.00 2.00 -- 104.18-111.00 60.00 34 6 \w 120.00 178.00 1.00 2.00 -- 104.18 77.00 90.00 58 7 \w 110.00 166.00 1.00 2.00 -- 104.18 30.00 150.00 56 8 \w 65.00 99.00 1.00 2.00 -- 104.18 -61.00 60.00 34 9 \w 64.00 145.00 1.00 2.00 -- 104.18 178.00 -60.00 81 10 \w 102.00 135.00 1.00 2.00 -- 104.18 -61.00 60.00 33 11 \w 81.00 170.00 1.00 2.00 -- 104.18 30.00 60.00 89 12 \w 78.00 107.00 1.00 2.00 -- 104.18 30.00 150.00 29 13 \w 36.00 133.00 1.00 2.00 -- 104.18 -61.00 -30.00 97 14 \w 20.00 105.00 1.00 2.00 -- 104.18 -94.00 -90.00 85 ; _diffrn_measurement_device 'kappa diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0260723000 _diffrn_orient_matrix_UB_12 -0.1542351000 _diffrn_orient_matrix_UB_13 0.1525991000 _diffrn_orient_matrix_UB_21 0.0002208000 _diffrn_orient_matrix_UB_22 0.1450881000 _diffrn_orient_matrix_UB_23 0.1249950000 _diffrn_orient_matrix_UB_31 -0.2398903000 _diffrn_orient_matrix_UB_32 0.0846204000 _diffrn_orient_matrix_UB_33 0.0337530000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0248 _diffrn_reflns_av_unetI/netI 0.0312 _diffrn_reflns_Laue_measured_fraction_full 0.981 _diffrn_reflns_Laue_measured_fraction_max 0.943 _diffrn_reflns_limit_h_max 4 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 7 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 1946 _diffrn_reflns_point_group_measured_fraction_full 0.981 _diffrn_reflns_point_group_measured_fraction_max 0.943 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.204 _diffrn_reflns_theta_min 6.552 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_current 0.80 _diffrn_source_power 0.040 _diffrn_source_target Cu _diffrn_source_type 'SuperNova (Cu) X-ray Source' _diffrn_source_voltage 50 _exptl_absorpt_coefficient_mu 7.364 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.94584 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.69a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_colour_primary colorless _exptl_crystal_density_diffrn 1.989 _exptl_crystal_description block _exptl_crystal_F_000 212 _exptl_crystal_size_max 0.06 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.03 _refine_diff_density_max 0.451 _refine_diff_density_min -0.753 _refine_diff_density_rms 0.097 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.019 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 108 _refine_ls_number_reflns 1347 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.019 _refine_ls_R_factor_all 0.0279 _refine_ls_R_factor_gt 0.0261 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0477P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0667 _refine_ls_wR_factor_ref 0.0678 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1275 _reflns_number_total 1347 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file dv3004sup8.txt _cod_data_source_block mona38cult _cod_original_cell_volume 362.43(8) _cod_database_code 2022371 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.809 _shelx_estimated_absorpt_t_min 0.666 _diffrn_oxdiff_digest_frames ; 01a958403cdb6a7be16caa1a06563f8f0900031d8f7 ; _diffrn_oxdiff_digest_hkl ; 012498c4f8cc137c3778ac295847ef588e53ea ; _reflns_odcompleteness_completeness 98.39 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C3(H3A), C4(H4), C6(H6) ; _shelx_res_file ; mona38cult.res created by SHELXL-2014/7 TITL mona38CuLT in P-1 #2 REM reset to P-1 #2 CELL 1.54184 6.95813 7.14128 8.02837 81.9588 73.8115 71.3518 ZERR 2 0.00071 0.00084 0.00093 0.0097 0.0095 0.0099 LATT 1 SFAC C H Br O UNIT 14 10 2 6 EQIV $1 -X,-Y,2-Z L.S. 10 PLAN 20 SIZE 0.03 0.03 0.06 TEMP -173 HTAB O3 O1 HTAB O2 O1_$1 BOND $H fmap 2 acta OMIT -2 6 3 OMIT -7 -5 1 REM REM REM WGHT 0.047700 FVAR 9.23049 BR1 3 0.345537 0.339804 0.134253 11.00000 0.01547 0.02772 = 0.01727 -0.00003 -0.00064 -0.00857 O1 4 -0.174238 0.093363 0.890133 11.00000 0.01365 0.02205 = 0.02003 0.00065 -0.00114 -0.00476 O2 4 0.158603 0.099838 0.805469 11.00000 0.01479 0.02986 = 0.01961 0.00411 -0.00618 -0.00996 H2 2 0.171711 0.035441 0.896737 11.00000 0.04755 O3 4 -0.413352 0.226991 0.672178 11.00000 0.01139 0.02756 = 0.02645 0.00185 -0.00185 -0.00565 H3 2 -0.378900 0.163259 0.763995 11.00000 0.05733 C1 1 -0.045596 0.211104 0.602584 11.00000 0.01349 0.01387 = 0.01906 -0.00339 -0.00275 -0.00291 C2 1 -0.239333 0.254510 0.561219 11.00000 0.01175 0.01381 = 0.02256 -0.00262 -0.00235 -0.00335 C3 1 -0.255577 0.331330 0.394140 11.00000 0.01277 0.02211 = 0.02430 -0.00267 -0.00678 -0.00336 AFIX 43 H3A 2 -0.386768 0.364499 0.365953 11.00000 -1.20000 AFIX 0 C4 1 -0.084538 0.359527 0.270162 11.00000 0.01775 0.01864 = 0.01925 -0.00059 -0.00720 -0.00293 AFIX 43 H4 2 -0.097479 0.412368 0.157095 11.00000 -1.20000 AFIX 0 C5 1 0.108959 0.309994 0.311285 11.00000 0.01336 0.01661 = 0.01725 -0.00312 -0.00032 -0.00444 C6 1 0.129813 0.238618 0.475388 11.00000 0.00896 0.01511 = 0.01927 -0.00317 -0.00119 -0.00196 AFIX 43 H6 2 0.261306 0.208236 0.502506 11.00000 -1.20000 AFIX 0 C7 1 -0.026157 0.130344 0.777646 11.00000 0.01153 0.01582 = 0.02105 -0.00274 -0.00263 -0.00289 HKLF 4 REM mona38CuLT in P-1 #2 REM R1 = 0.0261 for 1275 Fo > 4sig(Fo) and 0.0279 for all 1347 data REM 108 parameters refined using 0 restraints END WGHT 0.0467 0.0000 REM Highest difference peak 0.451, deepest hole -0.753, 1-sigma level 0.097 Q1 1 -0.0332 0.1685 0.6809 11.00000 0.05 0.45 Q2 1 0.2307 0.3520 0.0545 11.00000 0.05 0.36 Q3 1 0.3105 0.1877 0.0939 11.00000 0.05 0.36 Q4 1 0.1238 0.2823 0.3892 11.00000 0.05 0.33 Q5 1 0.3517 0.4021 0.0201 11.00000 0.05 0.33 Q6 1 0.4737 0.3206 0.2213 11.00000 0.05 0.33 Q7 1 0.3026 0.2249 0.5014 11.00000 0.05 0.32 Q8 1 0.3108 0.5778 0.2187 11.00000 0.05 0.30 Q9 1 -0.1175 0.2209 0.5814 11.00000 0.05 0.29 Q10 1 0.4446 0.2858 0.2347 11.00000 0.05 0.28 Q11 1 0.3758 0.4512 0.1695 11.00000 0.05 0.28 Q12 1 0.4950 0.5453 0.1202 11.00000 0.05 0.27 Q13 1 0.2154 0.2341 0.1505 11.00000 0.05 0.25 Q14 1 0.3217 0.2885 0.2623 11.00000 0.05 0.25 Q15 1 0.0357 0.2112 0.5384 11.00000 0.05 0.25 Q16 1 -0.2424 0.2998 0.4807 11.00000 0.05 0.25 Q17 1 0.0008 0.3463 0.2959 11.00000 0.05 0.25 Q18 1 0.1848 0.2796 0.8367 11.00000 0.05 0.25 Q19 1 0.5079 0.4188 0.0478 11.00000 0.05 0.24 Q20 1 0.0858 0.1563 1.0275 11.00000 0.05 0.24 ; _shelx_res_checksum 13883 _shelx_hkl_file ; -8 -5 -3 17263.3 597.488 14 -8 -4 -5 1712.89 267.749 14 -8 -4 -4 8048.72 564.137 14 -8 -4 -3 58448.7 1493.48 14 -8 -4 -2 7535.45 554.926 14 -8 -4 -1 843.620 227.318 14 -8 -3 -6 22296.1 725.087 14 -8 -3 -5 33246.7 1083.43 14 -8 -3 -4 10396.4 694.110 14 -8 -3 -3 4238.51 490.801 14 -8 -3 -2 28505.3 1148.58 14 -8 -3 -1 38100.3 1246.40 14 -8 -3 0 1810.59 288.486 14 -8 -2 -5 10146.3 564.587 14 -8 -2 -4 30256.1 1070.28 14 -8 -2 -3 17568.3 880.174 14 -8 -2 -2 19533.6 929.217 14 -8 -2 -1 14562.1 779.973 14 -8 -2 0 37785.1 1097.68 14 -8 -1 -4 20269.5 666.366 14 -8 -1 -3 33864.8 987.943 14 -8 -1 -2 14810.4 692.371 14 -8 -1 -1 1131.66 236.182 14 -7 -6 -3 7777.37 483.006 6 -7 -6 -2 3737.14 411.894 6 -7 -6 -1 35641.6 1189.73 6 -7 -6 0 50867.1 1331.55 6 -7 -5 -6 24265.5 875.724 14 -7 -5 -5 1326.16 300.570 14 -7 -5 -4 6693.28 582.234 14 -7 -5 -3 23076.1 1035.97 14 -7 -5 -2 5186.63 510.495 14 -7 -5 -2 6120.36 568.993 6 -7 -5 -1 2244.20 320.918 14 -7 -5 -1 1278.89 334.189 6 -7 -5 0 12667.7 823.316 6 -7 -5 1 26918.3 787.251 13 -7 -4 -7 750.468 221.438 14 -7 -4 -6 18598.4 981.345 14 -7 -4 -5 83460.0 2212.36 14 -7 -4 -4 6521.87 701.782 14 -7 -4 -3 26861.7 1346.86 14 -7 -4 -2 41601.8 1385.04 6 -7 -4 -2 45661.5 1704.05 14 -7 -4 -1 66639.1 1904.69 6 -7 -4 -1 70231.1 2037.16 14 -7 -4 0 1754.14 366.633 14 -7 -4 1 31091.7 1145.25 14 -7 -4 2 37737.5 925.504 13 -7 -3 -7 8837.52 599.658 14 -7 -3 -6 828.582 328.989 14 -7 -3 -5 33087.3 1513.25 14 -7 -3 -4 12298.0 1020.78 14 -7 -3 -3 17199.7 1172.57 14 -7 -3 -2 30.0202 351.198 14 -7 -3 -1 22116.2 1293.11 14 -7 -3 0 51418.8 1852.96 14 -7 -3 1 9455.03 784.048 14 -7 -2 -7 20746.3 838.368 14 -7 -2 -6 20515.2 1041.66 14 -7 -2 -5 2343.24 481.293 14 -7 -2 -4 56515.3 1988.10 14 -7 -2 -3 67354.7 2260.57 14 -7 -2 -2 14820.6 1096.44 14 -7 -2 -1 2010.50 540.555 14 -7 -2 0 49736.1 1880.34 14 -7 -2 1 55087.3 1849.98 14 -7 -2 2 6146.97 438.662 5 -7 -1 -6 13732.1 726.966 14 -7 -1 -5 52268.4 1599.90 14 -7 -1 -4 631.774 312.490 14 -7 -1 -3 196.810 264.083 14 -7 -1 -2 33789.9 1503.48 14 -7 -1 -2 36280.7 1302.94 9 -7 -1 -1 59983.9 1973.79 14 -7 -1 -1 61144.6 1709.82 5 -7 -1 0 3321.12 540.920 14 -7 -1 0 3290.30 470.351 5 -7 -1 1 22922.3 1141.00 14 -7 -1 1 22166.6 1012.03 5 -7 -1 2 48371.3 1324.25 5 -7 0 -5 20468.6 863.621 9 -7 0 -4 39402.7 1336.06 9 -7 0 -4 37350.1 1142.84 14 -7 0 -3 1340.13 302.011 14 -7 0 -3 1742.40 382.291 9 -7 0 -2 13307.3 875.957 9 -7 0 -2 14839.8 840.794 14 -7 0 -1 46717.0 1483.53 14 -7 0 -1 48830.8 1607.51 5 -7 0 0 16256.7 868.039 14 -7 0 0 17674.9 980.747 5 -7 0 1 1590.07 338.313 5 -7 0 2 15948.1 745.897 5 -7 1 -5 2345.14 333.353 9 -7 1 -4 30244.3 1122.60 9 -7 1 -3 24110.9 1086.45 9 -7 1 -2 31876.2 1284.57 9 -7 1 -1 638.169 331.602 5 -7 1 0 36143.7 1285.83 5 -7 1 1 40236.3 1211.51 5 -7 1 2 5672.17 384.317 5 -7 2 -4 293.457 178.534 9 -7 2 -3 9600.26 581.936 9 -6 -7 -4 33793.0 1007.51 6 -6 -7 -3 54123.1 1479.06 6 -6 -7 -2 35109.4 1289.70 6 -6 -7 -1 24139.9 1068.08 6 -6 -7 0 29218.8 1079.68 6 -6 -7 1 6313.44 438.313 6 -6 -6 -4 11758.3 717.313 6 -6 -6 -3 35110.4 1391.27 6 -6 -6 -2 6648.77 693.098 6 -6 -6 -1 6399.95 715.570 6 -6 -6 0 10215.2 836.636 6 -6 -6 1 27893.4 1224.94 6 -6 -6 2 19820.6 855.420 13 -6 -5 -7 182.657 198.519 14 -6 -5 -6 22285.2 1036.73 14 -6 -5 -5 41181.8 1493.02 14 -6 -5 -4 7867.84 710.988 14 -6 -5 -3 12598.0 883.928 6 -6 -5 -3 12777.9 871.737 14 -6 -5 -2 200543. 3614.40 6 -6 -5 -2 201812. 3173.28 14 -6 -5 -1 1187.64 416.819 6 -6 -5 0 439.056 337.907 6 -6 -5 1 22035.5 1259.24 6 -6 -5 2 50858.1 1649.84 13 -6 -5 2 53337.3 1737.06 6 -6 -5 3 9571.11 626.268 13 -6 -4 -8 27662.1 959.325 14 -6 -4 -7 7526.41 688.685 14 -6 -4 -6 72.6770 320.877 14 -6 -4 -5 15836.1 1108.61 14 -6 -4 -4 73072.3 2302.21 14 -6 -4 -3 24703.2 1331.84 14 -6 -4 -2 5191.62 606.529 6 -6 -4 -2 4646.69 617.275 14 -6 -4 -1 10421.5 854.771 14 -6 -4 -1 11134.8 920.949 6 -6 -4 0 102146. 2786.56 6 -6 -4 0 103475. 2516.43 14 -6 -4 1 25524.8 1237.22 14 -6 -4 1 24078.4 1415.28 6 -6 -4 2 8783.85 789.647 13 -6 -4 3 58684.5 1734.74 13 -6 -4 4 29970.9 966.649 13 -6 -3 -8 1050.58 282.733 14 -6 -3 -7 29610.6 1385.61 14 -6 -3 -6 37230.8 1727.55 14 -6 -3 -5 72.6889 390.296 14 -6 -3 -4 41419.2 1838.25 14 -6 -3 -3 75502.6 2395.02 14 -6 -3 -2 39098.6 1727.49 14 -6 -3 -2 36514.1 1377.05 6 -6 -3 -1 93025.8 2609.92 14 -6 -3 -1 91560.9 2380.64 6 -6 -3 0 13637.1 1029.63 6 -6 -3 0 14259.7 1062.91 14 -6 -3 1 31081.3 1602.94 6 -6 -3 1 31398.3 1385.58 13 -6 -3 1 32245.6 1565.64 14 -6 -3 2 8360.64 767.012 13 -6 -3 2 9069.00 842.113 14 -6 -3 3 8804.62 736.371 13 -6 -3 4 35925.4 1194.76 13 -6 -2 -8 1526.79 306.658 14 -6 -2 -7 10629.9 852.893 14 -6 -2 -6 27393.3 1468.66 14 -6 -2 -5 40168.7 1805.78 14 -6 -2 -4 28533.9 1533.54 14 -6 -2 -3 31424.6 1583.50 14 -6 -2 -2 119403. 2981.15 14 -6 -2 -1 38260.1 1712.45 14 -6 -2 -1 38657.4 1446.20 6 -6 -2 0 34685.8 1677.67 14 -6 -2 1 57368.8 2145.56 14 -6 -2 1 60418.4 1779.92 13 -6 -2 2 127273. 3104.70 14 -6 -2 2 121120. 2658.79 13 -6 -2 3 26712.5 1244.52 13 -6 -2 4 4907.56 493.508 13 -6 -1 -8 15776.7 622.347 14 -6 -1 -7 31737.0 1221.93 14 -6 -1 -6 1085.02 386.363 14 -6 -1 -5 43630.4 1766.86 14 -6 -1 -4 54953.5 1987.32 14 -6 -1 -3 1659.60 480.330 14 -6 -1 -3 1997.41 389.622 9 -6 -1 -2 12079.5 967.449 14 -6 -1 -2 11252.0 800.194 5 -6 -1 -2 10379.0 780.313 9 -6 -1 -1 85222.3 2470.40 14 -6 -1 -1 84043.9 2173.94 9 -6 -1 -1 88166.4 2258.07 5 -6 -1 0 309.358 349.500 5 -6 -1 0 406.360 358.923 14 -6 -1 1 7250.88 819.453 14 -6 -1 2 6345.17 792.052 14 -6 -1 2 6148.30 617.277 13 -6 -1 3 41997.4 1469.51 13 -6 -1 4 23326.0 946.188 13 -6 0 -7 28744.7 989.022 9 -6 0 -6 9409.90 629.812 14 -6 0 -6 9603.30 733.336 9 -6 0 -5 66.4221 342.597 9 -6 0 -5 913.846 338.822 14 -6 0 -4 19347.9 1090.33 14 -6 0 -4 18800.9 1142.58 9 -6 0 -3 144272. 3065.62 9 -6 0 -3 142440. 2925.29 14 -6 0 -2 21635.2 1233.54 9 -6 0 -2 22683.6 1213.35 14 -6 0 -2 23804.6 1291.16 5 -6 0 -1 20136.9 1191.87 9 -6 0 -1 20491.6 1229.36 5 -6 0 -1 18737.3 1105.17 14 -6 0 0 37194.3 1578.10 14 -6 0 0 35701.3 1645.45 5 -6 0 1 141144. 3104.24 14 -6 0 1 139831. 3271.53 5 -6 0 2 8044.08 829.090 5 -6 0 3 33687.4 1449.74 5 -6 0 3 31578.3 1138.66 13 -6 0 4 52278.3 1452.90 5 -6 0 4 49694.3 1180.30 13 -6 1 -7 245.599 194.257 9 -6 1 -6 55068.1 1674.53 9 -6 1 -5 23897.2 1248.50 9 -6 1 -4 518.080 375.135 9 -6 1 -3 27654.8 1468.07 9 -6 1 -2 19582.5 1267.53 5 -6 1 -2 19074.0 1234.33 9 -6 1 -1 23803.5 1369.98 9 -6 1 -1 24286.1 1411.88 5 -6 1 0 1501.66 487.110 9 -6 1 0 2112.33 563.413 5 -6 1 0 2305.45 394.290 14 -6 1 1 2316.61 531.955 5 -6 1 2 35713.6 1558.22 5 -6 1 3 21502.9 1066.26 5 -6 1 4 1695.55 276.400 5 -6 2 -6 6411.60 512.775 9 -6 2 -5 16568.1 959.359 9 -6 2 -4 30423.3 1407.85 9 -6 2 -3 15779.6 1093.74 9 -6 2 -2 49497.0 1892.57 9 -6 2 -1 57416.9 2086.10 5 -6 2 -1 58615.1 2047.16 9 -6 2 0 11473.7 941.727 5 -6 2 1 1773.18 436.039 5 -6 2 2 48005.8 1534.37 5 -6 2 3 41985.8 1131.00 5 -6 3 -5 3696.60 361.762 9 -6 3 -4 12898.8 738.539 9 -6 3 -3 32157.1 1246.05 9 -6 3 -2 1105.39 330.522 9 -6 3 -1 187.748 261.660 9 -5 -8 -4 21030.4 746.957 6 -5 -8 -3 8068.72 545.048 6 -5 -8 -2 1756.97 327.239 6 -5 -8 -1 25578.7 933.761 6 -5 -8 0 24619.0 790.823 6 -5 -7 -5 131.397 174.144 6 -5 -7 -4 7654.72 638.802 6 -5 -7 -3 29620.0 1340.37 6 -5 -7 -2 32298.3 1468.06 6 -5 -7 -1 113.002 260.272 6 -5 -7 0 12193.3 866.619 6 -5 -7 1 45485.9 1405.60 6 -5 -7 2 14405.8 599.318 6 -5 -6 -7 1453.26 293.520 11 -5 -6 -6 23005.3 1162.52 11 -5 -6 -5 28949.4 1129.14 6 -5 -6 -4 8124.23 744.152 6 -5 -6 -3 12013.3 954.050 6 -5 -6 -2 44888.8 1853.24 6 -5 -6 -1 37981.2 1754.31 6 -5 -6 0 1116.95 424.903 6 -5 -6 1 46318.0 1780.49 6 -5 -6 2 7360.28 659.551 6 -5 -5 -8 59802.7 1194.62 14 -5 -5 -8 61036.1 1362.01 11 -5 -5 -7 132.729 209.315 14 -5 -5 -7-39.4512 231.658 11 -5 -5 -6 6256.37 627.601 14 -5 -5 -6 5966.00 670.786 11 -5 -5 -5 22382.4 1156.25 14 -5 -5 -5 25714.7 1376.64 11 -5 -5 -4 31377.7 1281.11 14 -5 -5 -4 32043.7 1533.75 11 -5 -5 -4 31534.0 1331.32 6 -5 -5 -3 23661.7 1223.38 6 -5 -5 -2 444.013 323.052 6 -5 -5 -1 124268. 3045.71 6 -5 -5 0 51955.2 2025.89 6 -5 -5 1 16087.5 1159.92 6 -5 -5 2 19841.0 1212.70 6 -5 -5 3 82955.7 2126.86 6 -5 -5 4 35056.2 1277.44 13 -5 -4 -8 484.793 265.335 14 -5 -4 -8 633.564 218.402 11 -5 -4 -7 68569.8 2148.86 14 -5 -4 -7 69119.8 1882.21 11 -5 -4 -6 41113.5 1581.57 11 -5 -4 -6 41303.6 1759.73 14 -5 -4 -5 1913.82 514.780 14 -5 -4 -5 1415.15 412.603 11 -5 -4 -4 38419.6 1529.25 11 -5 -4 -4 39051.7 1604.97 14 -5 -4 -3 87404.9 2208.62 11 -5 -4 -3 88488.9 3362.84 4 -5 -4 -3 87654.5 2076.63 6 -5 -4 -3 89954.4 2290.23 14 -5 -4 -2 24703.3 1155.25 14 -5 -4 -2 24478.8 1769.28 4 -5 -4 -2 22305.2 1167.19 6 -5 -4 -1 1361.15 379.848 6 -5 -4 -1 1359.08 346.658 14 -5 -4 0 63740.5 2116.02 6 -5 -4 0 65330.9 1821.51 14 -5 -4 1 45806.4 1890.25 6 -5 -4 1 46653.7 1588.36 14 -5 -4 2 260.442 263.203 14 -5 -4 2 70.7369 321.234 6 -5 -4 3 82.0834 313.262 6 -5 -4 4 34377.9 1491.34 13 -5 -4 5 25074.5 964.032 13 -5 -3 -9 10782.8 594.972 14 -5 -3 -8 10719.6 834.002 14 -5 -3 -7 45318.3 1420.12 11 -5 -3 -7 47080.0 1951.07 14 -5 -3 -6 18740.4 1300.27 14 -5 -3 -6 17862.4 958.183 11 -5 -3 -5 19436.1 1257.34 14 -5 -3 -4 4636.31 622.736 14 -5 -3 -4 4905.40 859.978 4 -5 -3 -3 8250.62 762.310 14 -5 -3 -3 7805.63 993.036 4 -5 -3 -2 121367. 2629.56 14 -5 -3 -2 118514. 2220.76 6 -5 -3 -2 120626. 3621.43 4 -5 -3 -1 170473. 3092.95 14 -5 -3 -1 173030. 3005.80 6 -5 -3 0 28516.3 1313.86 14 -5 -3 0 28612.3 1348.85 6 -5 -3 1 51063.4 1809.80 14 -5 -3 1 52005.0 1928.25 6 -5 -3 1 51873.2 2443.35 2 -5 -3 2 116141. 3034.43 6 -5 -3 2 114660. 2766.59 14 -5 -3 3 36685.8 1729.87 13 -5 -3 4 15412.6 1097.30 13 -5 -3 5 62472.9 1755.25 13 -5 -2 -9 17524.3 746.399 14 -5 -2 -8 61827.9 1916.82 14 -5 -2 -7 41822.4 1831.57 14 -5 -2 -6 9013.38 942.696 14 -5 -2 -5 74735.5 2380.02 14 -5 -2 -5 71399.9 2836.86 4 -5 -2 -4 108044. 2682.36 14 -5 -2 -4 100031. 3300.58 4 -5 -2 -3 11188.9 863.909 14 -5 -2 -3 9614.59 1010.14 4 -5 -2 -2 27416.2 1530.49 4 -5 -2 -2 25281.1 1208.36 14 -5 -2 -1 68673.7 1975.59 14 -5 -2 -1 68104.2 1694.76 6 -5 -2 0 66244.8 1919.37 6 -5 -2 0 63354.0 1948.47 14 -5 -2 1 4808.86 639.921 6 -5 -2 1 5161.38 665.205 14 -5 -2 2 21104.6 1204.03 13 -5 -2 2 20295.7 1263.13 14 -5 -2 3 24628.3 1426.71 13 -5 -2 4 57974.0 2113.86 13 -5 -2 5 888.164 327.580 13 -5 -2 6 23421.0 793.075 13 -5 -1 -8 4504.35 505.986 14 -5 -1 -7 53973.4 1911.35 14 -5 -1 -6 1573.92 470.331 14 -5 -1 -5 736.061 356.832 14 -5 -1 -4 20061.5 1162.98 14 -5 -1 -3 82564.7 1798.10 9 -5 -1 -3 83879.4 2223.20 14 -5 -1 -2 69195.6 1955.00 14 -5 -1 -1 6345.75 559.532 9 -5 -1 -1 5883.77 540.210 5 -5 -1 -1 7165.17 671.648 14 -5 -1 0 342769. 4478.13 14 -5 -1 0 343201. 4051.69 6 -5 -1 0 340852. 3906.16 9 -5 -1 1 17187.1 1095.36 14 -5 -1 1 16360.1 904.800 13 -5 -1 2 5260.80 717.785 14 -5 -1 2 5141.03 658.256 13 -5 -1 3 32317.2 1581.90 13 -5 -1 4 98402.2 2677.28 13 -5 -1 5 20372.8 1086.94 13 -5 -1 6 1473.84 259.855 13 -5 0 -8 3437.44 393.541 9 -5 0 -7 28622.4 1181.39 14 -5 0 -7 29281.0 1288.12 9 -5 0 -6 87478.1 2266.69 14 -5 0 -6 83421.2 2327.23 9 -5 0 -5 31738.9 1427.36 14 -5 0 -5 33060.8 1479.55 9 -5 0 -4 337.318 317.074 14 -5 0 -4 197.829 329.504 9 -5 0 -3 56683.6 1733.76 14 -5 0 -3 57621.5 1847.92 9 -5 0 -3 57621.9 1785.42 5 -5 0 -2 96107.1 2308.21 9 -5 0 -2 94536.0 2257.51 5 -5 0 -2 96166.4 2219.45 14 -5 0 -1 37737.0 1436.96 14 -5 0 -1 39555.0 1518.62 9 -5 0 -1 38968.8 1529.65 5 -5 0 0 33.2281 285.105 14 -5 0 0-115.315 345.993 9 -5 0 1 32066.4 1461.28 14 -5 0 2 94877.0 2429.34 13 -5 0 2 91948.9 2574.79 14 -5 0 3 26342.5 1392.30 13 -5 0 4 263.365 307.286 13 -5 0 5 53133.6 1643.56 13 -5 0 6 43000.5 999.831 13 -5 1 -8 15229.8 723.129 9 -5 1 -7 14803.8 947.602 9 -5 1 -6 3312.38 589.977 9 -5 1 -6 2570.75 404.261 10 -5 1 -5 16177.8 1152.33 9 -5 1 -4 54595.1 2073.26 9 -5 1 -3 14218.1 1051.85 9 -5 1 -2 14470.3 1039.70 9 -5 1 -2 14828.5 1059.61 5 -5 1 -1 117917. 2841.07 9 -5 1 -1 118873. 3315.30 3 -5 1 -1 120403. 2278.60 14 -5 1 -1 119452. 2905.56 5 -5 1 0 85430.6 2563.96 5 -5 1 0 88426.4 2102.46 14 -5 1 0 88831.6 2511.68 9 -5 1 1 80188.2 2559.09 5 -5 1 1 79611.1 2158.89 14 -5 1 1 75184.1 2407.20 9 -5 1 2 9109.69 765.951 13 -5 1 3 39749.9 1582.09 13 -5 1 4 14048.6 914.449 13 -5 1 5 7815.50 604.180 5 -5 1 5 7176.22 562.230 13 -5 2 -7 39036.9 1336.35 9 -5 2 -6 2224.18 478.694 9 -5 2 -6 3223.40 423.110 10 -5 2 -5 11284.5 794.161 10 -5 2 -5 11941.4 1036.15 9 -5 2 -4 33391.6 1329.99 10 -5 2 -4 35283.6 1730.49 9 -5 2 -3 45654.5 1559.30 8 -5 2 -3 46071.4 1950.07 9 -5 2 -2 14411.3 1156.44 5 -5 2 -2 13316.2 1083.17 9 -5 2 -1 12061.7 1029.30 9 -5 2 -1 12395.4 1063.14 5 -5 2 0 60447.5 2196.14 9 -5 2 0 59340.2 2261.21 5 -5 2 1 42277.0 1891.50 5 -5 2 2 23196.2 1404.85 5 -5 2 3 19713.4 991.797 13 -5 2 3 19212.0 1183.19 5 -5 2 4 52096.5 1574.04 5 -5 2 4 50978.0 1413.53 13 -5 2 5 31315.4 815.051 13 -5 3 -6 22983.5 836.039 10 -5 3 -6 24688.7 1042.76 9 -5 3 -5 27669.0 1097.17 10 -5 3 -5 29219.9 1334.79 9 -5 3 -4 2172.26 507.110 9 -5 3 -4 1875.52 399.389 10 -5 3 -3 22855.9 1330.08 9 -5 3 -2 52216.4 1716.66 8 -5 3 -2 50878.0 1960.52 9 -5 3 -1 18054.5 1030.21 8 -5 3 -1 15589.5 1194.86 5 -5 3 -1 17061.2 1154.17 9 -5 3 0 4304.32 519.805 8 -5 3 0 5550.36 735.587 9 -5 3 0 5679.92 755.442 5 -5 3 1 81411.9 1925.41 8 -5 3 1 83636.0 2402.52 5 -5 3 2 1454.91 403.119 5 -5 3 3 9750.60 661.633 5 -5 4 -5 12925.9 548.289 10 -5 4 -5 12934.4 613.869 9 -5 4 -4 5712.49 507.731 9 -5 4 -4 6490.90 496.448 10 -5 4 -3 657.052 297.290 9 -5 4 -3 264.898 208.163 10 -5 4 -2 5987.19 552.149 8 -5 4 -2 7163.25 620.383 9 -5 4 -1 49580.8 1481.30 8 -5 4 -1 54827.1 1613.02 9 -5 4 0 14625.9 794.733 8 -5 4 1 924.706 212.196 8 -4 -8 -5 1445.77 221.561 6 -4 -8 -4 8368.10 570.907 6 -4 -8 -3 16692.2 876.112 6 -4 -8 -2 24203.9 1076.29 6 -4 -8 -2 20536.6 764.804 7 -4 -8 -1 7486.55 591.077 6 -4 -8 -1 7012.89 484.183 7 -4 -8 0 16049.8 755.141 6 -4 -8 0 14673.9 646.334 7 -4 -8 1 15005.6 572.587 7 -4 -7 -6 13030.5 567.051 6 -4 -7 -5 60809.8 1669.54 6 -4 -7 -4 1951.77 437.049 6 -4 -7 -3 6772.66 759.821 6 -4 -7 -3 5665.57 529.220 12 -4 -7 -2 50526.2 1943.92 6 -4 -7 -1 17063.0 944.281 7 -4 -7 -1 18481.2 1169.93 6 -4 -7 0 3280.63 530.304 6 -4 -7 0 2359.17 408.248 7 -4 -7 1 10949.3 772.388 6 -4 -7 1 9677.64 693.545 7 -4 -7 2 32925.1 1145.33 7 -4 -7 2 32163.6 1028.34 6 -4 -7 3 8604.04 493.609 7 -4 -6 -8 1776.66 257.464 11 -4 -6 -7 14520.6 875.791 11 -4 -6 -6 1479.72 441.431 11 -4 -6 -5 37130.3 1718.86 11 -4 -6 -4 12558.0 1042.55 11 -4 -6 -2 2663.96 550.446 6 -4 -6 -1 76403.7 1941.55 7 -4 -6 -1 76827.9 2446.09 6 -4 -6 0 24357.7 1174.75 7 -4 -6 0 22442.1 1333.73 6 -4 -6 1 1102.51 374.373 7 -4 -6 1 1492.28 424.512 6 -4 -6 2 19236.4 1070.63 6 -4 -6 2 19622.5 1054.04 7 -4 -6 3 38950.3 1350.66 7 -4 -6 3 38933.3 1236.81 6 -4 -6 4 24517.8 910.194 7 -4 -5 -8 2807.25 322.567 14 -4 -5 -8 2693.07 399.176 11 -4 -5 -7 68049.2 2120.43 11 -4 -5 -7 60333.5 1685.81 14 -4 -5 -6 35980.2 1396.43 14 -4 -5 -6 35315.5 1673.30 11 -4 -5 -5 1588.26 512.233 11 -4 -5 -4 90779.1 2567.72 11 -4 -5 -3 94024.2 3532.21 4 -4 -5 -3 90802.6 2496.32 11 -4 -5 -2 39672.4 1585.03 6 -4 -5 -1 13007.4 961.568 6 -4 -5 0 39237.6 1643.88 6 -4 -5 1 83770.6 2426.06 6 -4 -5 1 80978.4 1975.63 7 -4 -5 2 25568.8 1340.33 6 -4 -5 2 26808.1 1259.09 7 -4 -5 3 14867.2 969.514 6 -4 -5 3 12615.2 877.133 7 -4 -5 4 32891.9 1275.14 7 -4 -5 5 30157.9 1078.54 13 -4 -4 -9 11556.7 576.652 11 -4 -4 -9 12019.6 606.167 14 -4 -4 -8 582.956 298.498 11 -4 -4 -8 464.295 306.349 14 -4 -4 -7 3241.73 564.228 11 -4 -4 -6 56076.2 2011.09 11 -4 -4 -5 45170.5 2462.53 4 -4 -4 -5 41972.0 1672.24 11 -4 -4 -4 1160.39 518.210 4 -4 -4 -4 703.338 302.872 14 -4 -4 -4 196.436 295.639 11 -4 -4 -3 4406.51 822.812 4 -4 -4 -3 4070.79 534.870 11 -4 -4 -3 3398.87 382.243 14 -4 -4 -2 57804.6 2645.18 4 -4 -4 -2 54314.7 1628.66 11 -4 -4 -2 56945.3 1624.85 6 -4 -4 -1 74971.4 1945.51 6 -4 -4 0 816.521 277.818 6 -4 -4 1 58858.0 1910.20 6 -4 -4 1 60083.7 2896.67 2 -4 -4 2 81334.2 2316.32 6 -4 -4 2 79398.6 3387.03 2 -4 -4 2 79351.1 1865.72 7 -4 -4 3 6113.16 702.254 6 -4 -4 3 5934.94 630.131 7 -4 -4 4 2827.03 476.999 7 -4 -4 5 59273.3 1871.57 13 -4 -4 6 30191.3 884.035 13 -4 -3 -9 13135.2 772.223 14 -4 -3 -9 12216.1 615.307 11 -4 -3 -8 37984.5 1406.57 11 -4 -3 -7 49073.1 1748.31 11 -4 -3 -6 37611.8 1527.98 11 -4 -3 -5 105140. 3663.21 4 -4 -3 -5 107550. 2374.66 11 -4 -3 -4 133151. 4026.16 4 -4 -3 -4 123671. 2249.55 11 -4 -3 -3 122.259 324.530 4 -4 -3 -2 58951.2 2476.97 4 -4 -3 -1 162011. 3993.54 4 -4 -3 0 61750.7 2583.09 2 -4 -3 1 6720.19 962.857 2 -4 -3 1 8188.32 691.322 6 -4 -3 2 33536.2 1291.85 14 -4 -3 2 33164.6 2135.26 2 -4 -3 2 35660.9 1483.65 6 -4 -3 3 145040. 2566.41 7 -4 -3 3 146995. 3149.88 6 -4 -3 4 35189.4 1712.74 13 -4 -3 5 321.351 353.706 13 -4 -3 6 36616.7 1251.48 13 -4 -2 -9 179.005 226.635 14 -4 -2 -8 12910.8 784.888 11 -4 -2 -7 6773.58 643.642 11 -4 -2 -6 109217. 2267.26 11 -4 -2 -6 115606. 3835.61 4 -4 -2 -5 16.1186 318.790 4 -4 -2 -4 60849.3 2572.04 4 -4 -2 -3 57754.5 2347.11 4 -4 -2 -2 81163.0 2610.45 4 -4 -2 -1 386.062 276.815 4 -4 -2 0 121472. 3161.69 2 -4 -2 1 133267. 3594.78 2 -4 -2 2 2716.92 455.498 14 -4 -2 2 2310.04 424.262 6 -4 -2 2 2322.83 623.545 2 -4 -2 3 48894.8 2447.36 2 -4 -2 3 46646.4 1788.60 6 -4 -2 3 43281.7 1715.44 14 -4 -2 4 33991.2 1680.42 13 -4 -2 5 46776.0 1918.77 13 -4 -2 6 700.986 301.323 13 -4 -1 -9 15521.7 763.439 14 -4 -1 -7 11781.2 836.403 9 -4 -1 -6 191627. 3053.30 9 -4 -1 -6 190961. 4741.28 4 -4 -1 -5 10097.7 1092.27 4 -4 -1 -4 11307.9 1083.93 4 -4 -1 -3 101123. 2826.01 4 -4 -1 -2 85713.6 2373.16 4 -4 -1 -1 37390.2 1462.76 4 -4 -1 0 9856.26 807.191 2 -4 -1 1 97677.4 2702.36 2 -4 -1 2 128517. 3383.63 2 -4 -1 2 127798. 2559.00 13 -4 -1 2 125458. 2656.74 6 -4 -1 2 127059. 2651.79 14 -4 -1 3 42229.6 2054.56 2 -4 -1 3 45853.8 1792.82 13 -4 -1 3 45812.3 1808.11 14 -4 -1 4 25938.5 1461.63 13 -4 -1 5 74014.6 2430.36 13 -4 -1 6 58214.9 1868.48 13 -4 -1 7 483.867 155.993 13 -4 0 -9 11753.9 549.075 9 -4 0 -8 31476.3 1279.61 9 -4 0 -8 29729.9 1176.57 14 -4 0 -7 10831.0 877.244 9 -4 0 -6 12103.1 926.881 9 -4 0 -6 11405.3 843.695 10 -4 0 -5 152644. 2966.63 9 -4 0 -5 150256. 3805.64 4 -4 0 -5 145728. 2819.52 14 -4 0 -5 149980. 2465.70 10 -4 0 -4 133360. 2448.51 9 -4 0 -4 133910. 3337.16 4 -4 0 -3 13442.0 956.118 4 -4 0 -2 16730.4 1257.86 3 -4 0 -1 155694. 3470.41 3 -4 0 0 126407. 2839.60 3 -4 0 2 99946.4 2265.67 13 -4 0 2 102176. 2428.35 14 -4 0 3 65168.0 2164.11 14 -4 0 3 70252.7 2179.75 13 -4 0 4 3540.45 642.210 13 -4 0 5 1721.32 538.772 13 -4 0 6 38977.7 1507.51 13 -4 0 7 24248.3 759.555 13 -4 1 -9 1866.02 256.996 9 -4 1 -8 12921.3 848.381 9 -4 1 -7 36717.5 1625.33 9 -4 1 -6 34966.4 1671.45 9 -4 1 -6 36072.0 1516.75 10 -4 1 -5 82431.7 2435.10 9 -4 1 -5 79203.6 2122.74 10 -4 1 -4 32382.0 1435.16 9 -4 1 -4 31781.7 1179.99 10 -4 1 -3 21445.9 1618.43 3 -4 1 -3 23335.2 1151.61 5 -4 1 -3 24611.5 1186.50 9 -4 1 -2 3624.69 666.688 3 -4 1 -1 6806.89 834.566 3 -4 1 0 94099.7 2831.85 3 -4 1 0 93952.3 2156.83 9 -4 1 1 105970. 2098.63 14 -4 1 1 107865. 2470.24 9 -4 1 2 209.156 296.940 13 -4 1 2 539.764 314.301 14 -4 1 3 33627.9 1548.45 13 -4 1 4 110192. 2965.85 13 -4 1 5 26487.5 1448.22 13 -4 1 6 1334.22 374.097 13 -4 2 -8 6504.64 554.239 9 -4 2 -7 12579.4 957.149 9 -4 2 -6 49456.0 2020.54 9 -4 2 -6 46182.4 1772.06 10 -4 2 -5 119637. 3118.48 9 -4 2 -5 122765. 2820.38 10 -4 2 -4 2583.53 559.196 9 -4 2 -3 81125.2 2120.57 8 -4 2 -3 80270.3 3208.86 3 -4 2 -3 80772.3 2376.34 9 -4 2 -2 116584. 2381.07 8 -4 2 -2 116648. 3734.01 3 -4 2 -2 115172. 2741.08 5 -4 2 -2 116377. 2696.79 9 -4 2 -1 37650.9 1323.01 8 -4 2 -1 37704.8 2047.86 3 -4 2 -1 38769.7 1534.63 9 -4 2 -1 38007.4 1576.40 5 -4 2 0 6223.01 702.943 5 -4 2 0 6024.43 663.917 9 -4 2 0 5220.58 814.589 3 -4 2 1 73312.6 2291.66 5 -4 2 1 75507.8 2224.72 9 -4 2 2 97645.8 2403.40 13 -4 2 3 2036.92 500.202 13 -4 2 4 11205.5 961.078 13 -4 2 5 8506.58 766.364 13 -4 2 6 37157.0 929.865 5 -4 2 6 44170.4 1262.03 13 -4 3 -7 2645.54 417.227 9 -4 3 -6 2209.57 494.785 9 -4 3 -6 3014.06 495.380 10 -4 3 -5 72647.3 2236.46 10 -4 3 -5 72405.0 2354.23 9 -4 3 -4 59.5103 423.189 9 -4 3 -3 833.769 434.304 9 -4 3 -3 1615.61 462.817 8 -4 3 -2 3302.62 586.172 9 -4 3 -2 3743.85 588.655 8 -4 3 -1 42873.5 1694.68 8 -4 3 -1 43713.3 1753.73 9 -4 3 -1 40381.5 1801.04 5 -4 3 0 40790.4 1674.40 9 -4 3 0 46254.9 1868.66 5 -4 3 1-135.857 353.338 9 -4 3 1-71.5073 378.227 5 -4 3 2 103079. 2738.63 5 -4 3 2 99585.6 2367.43 13 -4 3 3 21349.6 1213.31 5 -4 3 3 20082.3 1145.80 13 -4 3 4 8984.71 709.929 5 -4 3 4 9712.50 773.908 13 -4 3 5 9786.48 661.618 13 -4 4 -6 7932.64 578.466 10 -4 4 -6 6745.69 505.791 9 -4 4 -5 2799.64 445.267 9 -4 4 -5 2677.27 440.872 10 -4 4 -4 88520.0 2386.07 10 -4 4 -4 87811.5 2298.99 9 -4 4 -3 34101.3 1614.59 8 -4 4 -3 32606.3 1471.30 9 -4 4 -2 904.902 390.797 9 -4 4 -2 130.844 372.016 8 -4 4 -1 24491.5 1379.67 8 -4 4 -1 24172.0 1246.04 9 -4 4 0 49951.9 1907.10 8 -4 4 0 53462.5 1779.94 9 -4 4 0 48269.7 1853.78 5 -4 4 1 27383.1 1403.88 8 -4 4 1 29160.1 1376.50 5 -4 4 2 322.824 282.214 5 -4 4 3 23929.6 1003.17 13 -4 4 3 22908.2 917.900 5 -4 4 4 21150.0 841.705 13 -4 5 -5 13495.7 616.329 10 -4 5 -4 6496.24 532.741 10 -4 5 -4 5907.97 394.519 9 -4 5 -3 305.876 189.571 9 -4 5 -3 603.694 283.929 10 -4 5 -2 18261.6 1053.65 8 -4 5 -2 17011.8 766.229 9 -4 5 -1 13786.6 930.227 8 -4 5 0 319.291 262.959 8 -4 5 1 29037.5 1227.40 8 -4 5 2 39905.7 1274.95 8 -4 5 3 9685.74 528.257 8 -4 6 -2 12815.5 538.802 10 -4 6 0 3424.21 301.855 8 -3 -8 -5 11010.9 548.143 6 -3 -8 -4 1255.70 245.785 12 -3 -8 -4 743.134 256.707 6 -3 -8 -3 4830.15 454.465 12 -3 -8 -3 5324.63 551.634 6 -3 -8 -2 23689.6 1082.15 6 -3 -8 -1 44686.4 1411.32 6 -3 -8 -1 45338.7 1461.36 7 -3 -8 0 464.675 252.261 7 -3 -8 0 312.453 204.585 6 -3 -8 1 16035.9 798.399 7 -3 -8 2 26170.2 861.898 7 -3 -7 -6 620.686 172.271 12 -3 -7 -5 8342.14 635.392 12 -3 -7 -4 42735.7 1516.91 12 -3 -7 -3 2159.38 465.659 12 -3 -7 -2 2866.27 505.192 12 -3 -7 -1 19270.9 1158.22 12 -3 -7 -1 20528.4 1256.85 6 -3 -7 0 24761.5 1324.95 7 -3 -7 0 25304.8 1276.77 6 -3 -7 1 1723.25 433.672 7 -3 -7 1 2815.27 440.879 6 -3 -7 2 23691.4 1197.06 7 -3 -7 3 1407.97 324.230 7 -3 -7 4 22245.5 802.622 7 -3 -6 -8 4470.16 349.703 11 -3 -6 -7 29151.6 1182.60 11 -3 -6 -6 12290.3 936.787 11 -3 -6 -5 1715.56 483.056 11 -3 -6 -4 33234.9 1597.32 11 -3 -6 -4 35927.7 1458.23 12 -3 -6 -3 62630.1 1923.62 12 -3 -6 -3 56659.8 2055.49 11 -3 -6 -2 23000.1 1200.46 12 -3 -6 -1 814.343 343.706 12 -3 -6 0 155054. 3258.78 6 -3 -6 1 42798.2 1725.20 7 -3 -6 1 42767.2 1659.97 6 -3 -6 2 2039.04 472.543 7 -3 -6 2 1878.01 405.483 6 -3 -6 3 10642.6 898.832 7 -3 -6 4 48568.3 1647.06 7 -3 -6 5 22708.3 897.003 7 -3 -5 -8 3593.20 465.822 11 -3 -5 -7 7483.49 775.361 11 -3 -5 -6 37493.8 1733.53 11 -3 -5 -5 31612.9 1571.32 11 -3 -5 -4 27768.9 1772.24 4 -3 -5 -4 27529.8 1390.31 11 -3 -5 -3 52102.1 2484.10 4 -3 -5 -3 52268.5 1796.71 11 -3 -5 -2 56105.0 2573.80 4 -3 -5 -2 57420.9 1849.57 11 -3 -5 -2 53500.3 1464.37 12 -3 -5 -1 49912.3 1450.25 12 -3 -5 0 2916.72 441.589 12 -3 -5 0 2916.36 482.068 6 -3 -5 1 30332.7 1329.95 7 -3 -5 1 27876.0 1292.11 6 -3 -5 2 81692.2 2272.42 7 -3 -5 2 78991.6 2155.61 6 -3 -5 3 5076.50 679.303 7 -3 -5 3 6774.25 631.895 6 -3 -5 4 2073.18 516.459 7 -3 -5 5 37632.4 1478.19 7 -3 -5 5 32451.0 1240.24 13 -3 -4 -9 18207.2 800.874 11 -3 -4 -8 24992.5 1267.69 11 -3 -4 -7 8440.60 870.847 11 -3 -4 -6 6644.28 796.084 11 -3 -4 -5 74293.4 3006.69 4 -3 -4 -5 78689.7 2259.95 11 -3 -4 -4 59632.6 2638.97 4 -3 -4 -4 60909.9 1829.20 11 -3 -4 -3 1354.57 465.685 4 -3 -4 -2 42796.5 2150.18 4 -3 -4 -1 127710. 3721.51 4 -3 -4 0 150362. 4211.91 2 -3 -4 1 55637.3 2663.03 2 -3 -4 2 60314.2 1708.29 7 -3 -4 2 57567.0 1694.88 6 -3 -4 3 59936.0 2961.85 2 -3 -4 3 59127.0 1899.67 7 -3 -4 3 58849.4 1776.17 6 -3 -4 4 36742.9 1626.61 7 -3 -4 5 4476.19 630.203 7 -3 -4 5 4260.89 602.967 13 -3 -4 6 36519.3 1182.56 13 -3 -3 -9 648.105 252.885 11 -3 -3 -8 21317.5 1207.21 11 -3 -3 -7 62565.4 2127.54 11 -3 -3 -6 25603.0 1828.33 4 -3 -3 -6 30006.5 1405.91 11 -3 -3 -5-142.233 348.345 4 -3 -3 -5-560.723 308.632 11 -3 -3 -4 34672.1 1970.40 4 -3 -3 -3 362715. 5959.87 4 -3 -3 -2 27098.4 1588.22 4 -3 -3 -1 3813.10 651.677 4 -3 -3 0 128480. 3501.63 2 -3 -3 1 159001. 4117.36 2 -3 -3 2 42803.5 2291.79 2 -3 -3 3 34498.0 2192.92 2 -3 -3 3 34316.8 1297.28 7 -3 -3 3 33965.5 1287.11 6 -3 -3 4 75912.3 2184.91 7 -3 -3 4 72798.4 1983.50 6 -3 -3 5 68793.8 2219.57 7 -3 -3 5 70465.4 2274.34 13 -3 -3 6 707.275 294.761 13 -3 -2 -9 35108.3 1197.14 11 -3 -2 -8 768.935 383.047 11 -3 -2 -7 21290.2 1208.30 11 -3 -2 -6 39117.1 2239.08 4 -3 -2 -6 38236.9 1476.16 11 -3 -2 -5 68231.8 2845.21 4 -3 -2 -4 5064.91 768.796 4 -3 -2 -3 107594. 3044.93 4 -3 -2 -2 53761.5 1996.01 4 -3 -2 -1 22863.1 1274.43 4 -3 -2 0 5134.37 686.117 2 -3 -2 1 293958. 5037.08 2 -3 -2 2 15242.4 1294.94 2 -3 -2 3 5347.41 868.018 2 -3 -2 4 9796.70 786.039 7 -3 -2 4 8673.68 1174.66 2 -3 -2 5 86726.4 2576.43 13 -3 -2 6 46303.1 1769.52 13 -3 -2 7-14.0626 192.485 13 -3 -1 -9 28837.6 972.585 11 -3 -1 -8 31332.6 1282.85 9 -3 -1 -8 31637.7 1295.36 11 -3 -1 -7 12003.5 859.347 11 -3 -1 -6 17839.6 1483.15 4 -3 -1 -6 18211.8 924.260 11 -3 -1 -5 100147. 3280.23 4 -3 -1 -4 146273. 3612.40 4 -3 -1 -3 77989.1 2367.10 4 -3 -1 -2 275608. 3991.47 4 -3 -1 -1 259730. 3565.41 4 -3 -1 0 168396. 2931.36 2 -3 -1 1 314.205 332.698 2 -3 -1 2 82784.5 2649.72 2 -3 -1 3 237408. 4935.96 2 -3 -1 4 53516.5 1875.24 13 -3 -1 4 51312.7 2556.57 2 -3 -1 5 6065.90 770.354 13 -3 -1 6 59156.5 2071.92 13 -3 -1 7 53685.1 1551.28 13 -3 0 -9-67.2337 211.297 9 -3 0 -8 42810.5 1634.34 9 -3 0 -7 52838.0 1893.02 9 -3 0 -6 6025.36 889.277 4 -3 0 -6 5516.90 653.995 10 -3 0 -5 3668.48 680.836 4 -3 0 -4 127438. 3221.42 4 -3 0 -3 82821.4 2271.02 4 -3 0 -2 75.5879 291.087 3 -3 0 -2 372.293 273.101 4 -3 0 -1 277.047 290.062 3 -3 0 -1 1817.86 294.678 4 -3 0 0 71763.4 1497.67 2 -3 0 0 70032.5 1851.50 3 -3 0 1 140559. 2608.39 2 -3 0 1 143591. 2379.97 3 -3 0 2 13122.0 976.740 2 -3 0 3 15547.4 1222.40 2 -3 0 4 65186.5 2109.53 13 -3 0 4 64904.3 2638.33 2 -3 0 5 36093.8 1732.55 13 -3 0 6 752.197 412.237 13 -3 0 7 37092.8 1340.63 13 -3 1 -9 11815.7 660.228 9 -3 1 -8 310.081 331.921 9 -3 1 -7 19189.4 1263.35 9 -3 1 -6 81303.3 2437.66 9 -3 1 -6 78979.9 2833.55 4 -3 1 -6 78117.6 2295.29 10 -3 1 -5 58339.9 1897.35 9 -3 1 -5 58899.2 2383.20 4 -3 1 -5 56136.1 1751.95 10 -3 1 -4 4843.15 652.279 4 -3 1 -3 127514. 2702.29 4 -3 1 -3 122863. 3447.56 3 -3 1 -2 369347. 3657.90 4 -3 1 -2 378718. 5674.16 3 -3 1 -1 1550.83 439.553 3 -3 1 0 53156.8 1929.24 3 -3 1 1 186846. 3427.17 3 -3 1 3 25729.6 1225.85 13 -3 1 4 43756.0 1824.60 13 -3 1 5 112034. 3051.25 13 -3 1 6 32376.3 1562.35 13 -3 1 7 1248.49 341.709 13 -3 2 -9 34242.3 896.900 9 -3 2 -8 33762.6 1371.90 9 -3 2 -7 400.072 418.600 9 -3 2 -7 359.714 384.093 10 -3 2 -6 18228.7 1263.30 9 -3 2 -6 16083.7 1155.25 10 -3 2 -5 11815.8 1011.62 9 -3 2 -5 10002.9 860.211 10 -3 2 -4 163802. 3156.36 9 -3 2 -4 164620. 4324.46 3 -3 2 -3 468.940 396.713 3 -3 2 -2 47425.5 2233.14 3 -3 2 -1 32120.6 1811.33 3 -3 2 0 96013.0 3002.74 3 -3 2 1 6066.16 761.247 3 -3 2 2 88001.3 2654.67 3 -3 2 2 88045.6 2029.47 13 -3 2 2 85119.4 2082.29 9 -3 2 3 51375.4 1830.19 13 -3 2 4 19739.1 1284.90 13 -3 2 5 6196.76 795.438 13 -3 2 6 27045.2 1357.73 13 -3 2 7 26225.6 981.908 13 -3 3 -8 13782.7 696.933 9 -3 3 -7 23142.3 1198.32 9 -3 3 -7 24121.5 1228.92 10 -3 3 -6 10922.0 967.825 9 -3 3 -6 10193.9 943.573 10 -3 3 -5 6574.26 775.613 9 -3 3 -5 6315.20 790.805 10 -3 3 -4 110433. 2806.48 9 -3 3 -4 112488. 3449.35 3 -3 3 -3 39052.9 1608.47 8 -3 3 -3 43066.4 2297.57 3 -3 3 -3 38820.9 1578.75 9 -3 3 -2 1095.69 401.945 9 -3 3 -2 976.906 347.239 8 -3 3 -2 878.081 461.521 3 -3 3 -1 109580. 2502.68 8 -3 3 -1 111053. 3643.84 3 -3 3 -1 112820. 2532.60 5 -3 3 -1 110619. 2352.72 9 -3 3 0 69595.0 1856.01 9 -3 3 0 67546.1 2789.37 3 -3 3 0 66477.5 1913.03 5 -3 3 1 29243.3 1317.72 5 -3 3 1 26548.7 1073.72 13 -3 3 1 29531.0 1247.50 9 -3 3 1 29284.8 1816.24 3 -3 3 2 1940.57 466.712 5 -3 3 2 2489.19 468.300 13 -3 3 2 2855.34 536.733 3 -3 3 3 36700.4 1626.26 13 -3 3 4 82645.1 2576.28 13 -3 3 5 16001.2 881.625 5 -3 3 5 18468.8 1194.58 13 -3 3 6 10264.1 780.192 13 -3 4 -7 16233.2 731.369 9 -3 4 -6 20150.8 1122.72 10 -3 4 -6 18377.3 988.521 9 -3 4 -5 6098.01 745.825 10 -3 4 -5 5636.71 669.687 9 -3 4 -4 20828.5 1211.56 9 -3 4 -3 95528.6 2798.38 8 -3 4 -3 92852.9 2444.84 9 -3 4 -2 62208.2 2206.63 8 -3 4 -2 63564.2 1970.36 9 -3 4 -1 8054.24 850.716 8 -3 4 -1 9401.86 782.812 9 -3 4 0 202.230 323.484 5 -3 4 0 139.436 278.475 9 -3 4 1 63523.8 1836.07 9 -3 4 1 63872.4 1968.41 5 -3 4 2 72070.5 2125.38 13 -3 4 2 70579.2 2004.19 5 -3 4 3 2359.86 505.292 13 -3 4 4 12479.2 959.684 13 -3 4 5 30816.3 1290.09 13 -3 4 6 6141.92 451.645 13 -3 5 -6 4151.98 389.146 10 -3 5 -5 23936.9 1107.33 10 -3 5 -5 22584.2 812.529 9 -3 5 -4 23371.3 1254.10 10 -3 5 -4 21485.1 932.935 9 -3 5 -3 14812.6 1110.08 8 -3 5 -3 15048.1 838.862 9 -3 5 -2 16367.1 1202.42 8 -3 5 -1 27596.9 1541.62 8 -3 5 0 503.254 417.586 8 -3 5 1 1918.07 529.443 8 -3 5 2 22318.2 1071.48 13 -3 5 3 25108.1 1109.61 13 -3 5 4 2269.37 359.196 13 -3 5 5 8468.38 466.263 13 -3 6 -4 6921.08 481.619 10 -3 6 -3 69062.4 1699.43 10 -3 6 -2 819.299 319.974 8 -3 6 -1 16921.7 1011.75 8 -3 6 0 24402.1 1191.28 8 -3 6 1 21163.6 1074.98 8 -3 6 2 49.4399 196.456 8 -3 6 3 19149.5 785.477 8 -2 -8 -4 47020.2 1261.95 12 -2 -8 -3 43.3378 219.225 12 -2 -8 -2 4312.95 517.807 12 -2 -8 -2 4152.93 477.417 6 -2 -8 -1 12937.4 734.087 6 -2 -8 0 13716.2 858.161 7 -2 -8 1 2441.40 393.267 7 -2 -8 2 459.734 220.521 7 -2 -7 -6 14982.4 720.167 12 -2 -7 -5 707.082 302.659 12 -2 -7 -4 29007.7 1370.91 12 -2 -7 -3 17071.0 1144.14 12 -2 -7 -2 9526.51 893.328 12 -2 -7 -1 1823.28 515.093 12 -2 -7 0 34025.3 1403.29 6 -2 -7 1 40886.0 1773.96 7 -2 -7 2 2928.11 524.707 7 -2 -7 3 56722.7 1772.60 7 -2 -7 4 4562.56 457.295 7 -2 -6 -7 3792.35 411.319 11 -2 -6 -6 56772.4 1747.41 11 -2 -6 -5 20691.2 1170.95 11 -2 -6 -4 46.6537 323.086 11 -2 -6 -3 50577.6 1765.77 11 -2 -6 -2 43606.3 1752.06 12 -2 -6 -1 24480.6 1336.27 12 -2 -6 0 653.031 382.233 12 -2 -6 1 29274.9 1301.91 6 -2 -6 2 63510.2 2243.76 7 -2 -6 3 47449.1 1938.17 7 -2 -6 4 9571.48 852.894 7 -2 -6 5 25851.1 1136.58 7 -2 -5 -8 21646.0 933.400 11 -2 -5 -7 2933.79 510.645 11 -2 -5 -6 1337.89 440.231 11 -2 -5 -5 48179.7 1834.88 11 -2 -5 -4 83320.9 2254.19 11 -2 -5 -3 2340.81 541.163 4 -2 -5 -3 2055.51 426.938 11 -2 -5 -2 18787.7 967.842 11 -2 -5 -1 69472.6 1811.29 12 -2 -5 0 44282.1 1505.32 12 -2 -5 1 710.161 282.963 6 -2 -5 2 55280.0 1904.69 7 -2 -5 2 55741.3 2554.72 2 -2 -5 3 88037.6 2552.80 7 -2 -5 4 8798.07 906.080 7 -2 -5 5 2034.74 462.499 7 -2 -5 6 15058.8 896.506 7 -2 -4 -9 338.625 182.527 11 -2 -4 -8 28106.8 1309.11 11 -2 -4 -7 32397.9 1568.08 11 -2 -4 -6 32019.3 1561.33 11 -2 -4 -5 26040.4 1617.22 4 -2 -4 -5 29360.2 1366.21 11 -2 -4 -4 82749.5 2850.21 4 -2 -4 -4 81560.6 2002.55 11 -2 -4 -3 61713.7 2388.65 4 -2 -4 -2 13150.0 1111.21 4 -2 -4 -1 13358.9 1130.07 4 -2 -4 1 180695. 4388.46 2 -2 -4 2 12702.7 1264.33 2 -2 -4 3 34617.2 2137.99 2 -2 -4 3 37363.3 1488.94 7 -2 -4 4 181133. 3591.28 7 -2 -4 5 36121.1 1711.26 7 -2 -4 6 290.325 326.653 7 -2 -3 -9 44615.4 1410.22 11 -2 -3 -8 4034.75 629.362 11 -2 -3 -7 20578.6 1290.78 11 -2 -3 -6 44896.0 2187.85 4 -2 -3 -6 50942.9 1830.35 11 -2 -3 -5 113547. 3455.49 4 -2 -3 -5 117456. 2436.71 11 -2 -3 -4 1327.94 424.169 4 -2 -3 -3 92561.1 2749.01 4 -2 -3 -2 177559. 3632.02 4 -2 -3 -1 26121.2 1384.70 4 -2 -3 0 1990.02 507.284 2 -2 -3 1 52730.4 2170.18 2 -2 -3 2 126958. 3583.87 2 -2 -3 3 8561.25 1082.62 2 -2 -3 4 57459.9 2854.78 2 -2 -3 4 60934.7 1924.87 7 -2 -3 5 449.105 371.938 7 -2 -3 6 62877.1 1832.59 13 -2 -2 -9 13087.7 816.904 11 -2 -2 -8 34879.3 1582.78 11 -2 -2 -7 1360.22 453.810 11 -2 -2 -6 9839.42 1108.94 4 -2 -2 -6 6752.67 689.904 11 -2 -2 -5 154614. 3972.22 4 -2 -2 -4 31969.9 1664.36 4 -2 -2 -3 2587.48 504.597 4 -2 -2 -2 31417.8 1387.52 4 -2 -2 -1 237345. 3587.77 4 -2 -2 0 149296. 2866.22 4 -2 -2 0 152939. 2941.66 2 -2 -2 1 1201.16 430.141 2 -2 -2 2 344344. 5373.27 2 -2 -2 3 193550. 4532.95 2 -2 -2 4 38546.2 1399.27 7 -2 -2 4 38171.5 2246.72 2 -2 -2 5 39813.3 1653.54 7 -2 -2 5 44356.1 1660.05 13 -2 -2 5 42494.3 2520.55 2 -2 -2 6 92313.1 2382.72 13 -2 -1 -9 1481.09 298.336 9 -2 -1 -9 1631.49 352.369 11 -2 -1 -8 60213.4 1982.13 11 -2 -1 -7 100381. 2537.71 11 -2 -1 -6 24669.2 1685.48 4 -2 -1 -6 24178.5 1155.48 11 -2 -1 -5 5141.61 755.532 4 -2 -1 -4 186552. 3819.93 4 -2 -1 -3 211466. 3612.99 4 -2 -1 -2 69926.3 1801.23 4 -2 -1 -1 129217. 2201.77 4 -2 -1 0 106263. 1938.02 4 -2 -1 0 105234. 2003.94 2 -2 -1 1 131741. 2592.63 2 -2 -1 2 54376.0 1987.85 2 -2 -1 3 57891.1 2332.03 2 -2 -1 4 118635. 3801.31 2 -2 -1 5 4626.20 617.649 13 -2 -1 5 4027.47 838.094 2 -2 -1 6 36887.7 1559.96 13 -2 -1 7 36130.2 1364.72 13 -2 0 -9 16958.4 860.343 9 -2 0 -9 15138.4 744.117 11 -2 0 -8 1826.36 430.973 11 -2 0 -7 24894.1 1200.24 11 -2 0 -6 50637.8 2397.73 4 -2 0 -6 47241.3 1477.61 11 -2 0 -5 77927.0 2774.01 4 -2 0 -4 15929.6 1144.43 4 -2 0 -3 85740.3 2225.27 4 -2 0 -2 102028. 1963.54 4 -2 0 -2 100394. 2279.37 3 -2 0 -1 88404.8 1493.28 4 -2 0 -1 91740.9 1908.32 3 -2 0 0 51453.7 986.292 4 -2 0 0 52592.7 1060.98 2 -2 0 0 53178.7 1288.43 3 -2 0 1 286729. 3226.55 2 -2 0 1 285001. 2698.79 3 -2 0 2 332607. 2641.12 3 -2 0 2 334401. 4344.49 1 -2 0 3 31195.8 1616.72 1 -2 0 4 75654.2 2813.64 1 -2 0 5 118726. 2735.79 13 -2 0 6 28029.1 1440.73 13 -2 0 7 2577.61 452.323 13 -2 1 -9 32755.5 1170.38 9 -2 1 -8 67419.4 1659.83 11 -2 1 -7 1117.38 318.045 11 -2 1 -6 64253.6 2724.34 4 -2 1 -6 59434.5 2007.90 10 -2 1 -5 134295. 3628.80 4 -2 1 -5 133836. 2557.66 10 -2 1 -4 76421.3 2463.23 4 -2 1 -3 629.904 342.608 3 -2 1 -3 694.040 319.823 4 -2 1 -2 82196.4 1728.38 4 -2 1 -2 79825.8 2254.78 3 -2 1 -1 491780. 3014.82 4 -2 1 -1 487063. 5261.04 3 -2 1 0 32453.3 1317.44 3 -2 1 1 3038.80 329.832 1 -2 1 1 2669.23 415.037 3 -2 1 2 78956.8 1933.67 3 -2 1 2 79446.2 1971.26 1 -2 1 3 249035. 4246.55 1 -2 1 4 44357.1 2100.77 1 -2 1 4 48068.2 1622.59 13 -2 1 5 15251.6 1069.75 13 -2 1 5 17628.3 1425.62 1 -2 1 6 16721.5 1159.69 13 -2 1 7 100688. 2453.40 13 -2 1 8 4911.23 363.267 13 -2 2 -9-25.6245 179.765 9 -2 2 -8 22774.0 1220.37 9 -2 2 -7 59933.0 2194.34 9 -2 2 -6 13769.8 1063.73 10 -2 2 -5 2796.09 574.928 4 -2 2 -5 2851.76 480.517 10 -2 2 -4 97565.4 2763.33 4 -2 2 -4 91663.3 2892.09 3 -2 2 -3 80552.2 2155.99 4 -2 2 -3 78337.1 2578.96 3 -2 2 -2 2363.16 501.034 3 -2 2 -2 2416.65 347.937 4 -2 2 -1 29319.8 1539.19 3 -2 2 0 160251. 3490.69 3 -2 2 1 65029.5 2200.30 3 -2 2 2 1873.19 435.093 3 -2 2 3 211594. 3918.03 3 -2 2 4 21660.4 1196.97 13 -2 2 5 8291.67 864.951 13 -2 2 6 5428.75 749.495 13 -2 2 7 34117.7 1398.18 13 -2 3 -8 439.244 270.269 9 -2 3 -7 44643.7 1743.22 9 -2 3 -6 54164.3 2049.27 9 -2 3 -6 52099.4 2053.63 10 -2 3 -5 8245.14 821.525 9 -2 3 -5 9297.08 888.680 10 -2 3 -4 16782.1 1043.96 9 -2 3 -4 16526.9 1303.38 3 -2 3 -3 65253.5 1880.54 8 -2 3 -3 64063.9 2547.38 3 -2 3 -2 119764. 3501.41 3 -2 3 -1 57266.3 2440.61 3 -2 3 0 124887. 3552.23 3 -2 3 1 91227.2 3044.97 3 -2 3 2 115070. 3368.94 3 -2 3 3 13821.5 1172.62 3 -2 3 3 11773.6 895.566 13 -2 3 4 43394.1 1828.96 13 -2 3 5 95272.9 2823.98 13 -2 3 6 20594.7 1291.96 13 -2 3 7 2614.18 413.529 13 -2 4 -7 1509.89 319.107 9 -2 4 -6 20499.4 1122.01 9 -2 4 -6 20683.0 1221.88 10 -2 4 -5 40844.6 1646.58 9 -2 4 -5 43702.4 1855.25 10 -2 4 -4 27367.9 1323.45 9 -2 4 -3 638.386 294.921 9 -2 4 -3 935.633 383.052 8 -2 4 -2 48674.3 1801.31 8 -2 4 -2 50361.7 2442.62 3 -2 4 -2 48393.1 1465.79 9 -2 4 -1 60977.9 1974.67 8 -2 4 -1 65961.6 2820.79 3 -2 4 0 17959.2 1501.86 3 -2 4 0 19399.3 933.961 5 -2 4 1 3936.91 510.877 13 -2 4 1 3214.40 697.908 3 -2 4 2 52169.0 2514.39 3 -2 4 2 46974.1 1743.47 13 -2 4 3 66553.9 2216.60 13 -2 4 4 4858.33 739.837 13 -2 4 5 1150.40 519.863 13 -2 4 6 19435.3 1088.78 13 -2 4 7 12682.8 616.664 13 -2 5 -6 68.8735 211.228 10 -2 5 -5 9242.83 802.209 10 -2 5 -5 8683.19 599.973 9 -2 5 -4 30330.5 1513.53 10 -2 5 -3 17576.4 1253.58 8 -2 5 -2 668.643 369.665 8 -2 5 -1 33380.7 1668.82 8 -2 5 0 129800. 3244.67 8 -2 5 1 2023.67 441.893 13 -2 5 2 918.361 428.777 13 -2 5 3 44672.8 1816.66 13 -2 5 4 48771.9 1881.75 13 -2 5 5 9451.53 771.000 13 -2 5 6 7294.95 516.657 13 -2 6 -5 1381.54 255.270 10 -2 6 -4 3035.55 429.225 10 -2 6 -3 10550.9 821.419 10 -2 6 -2 48861.5 1841.37 8 -2 6 -1 1245.50 449.705 8 -2 6 0 7893.87 808.316 8 -2 6 1 23341.3 1344.77 8 -2 6 2 22285.3 1268.48 8 -2 6 3 574.977 263.224 13 -2 6 4 20783.0 915.563 13 -2 7 -2 11329.7 596.413 10 -2 7 -1 16807.0 794.721 8 -2 7 0 2683.52 377.656 8 -2 7 1 22872.7 921.465 8 -2 7 2 6625.71 478.368 8 -1 -8 -4 905.872 221.471 12 -1 -8 -3 77384.2 1696.30 12 -1 -8 -2 4633.39 496.637 12 -1 -8 -1 2646.68 305.393 6 -1 -8 0 13964.9 819.809 7 -1 -8 1 15539.4 798.320 7 -1 -8 2 603.917 225.976 7 -1 -7 -6 11944.5 604.270 12 -1 -7 -5 10053.0 722.847 12 -1 -7 -4 195.835 287.070 12 -1 -7 -3 26074.7 1390.25 12 -1 -7 -2 19589.6 1258.55 12 -1 -7 -1 6845.12 801.397 12 -1 -7 0 3761.75 638.828 12 -1 -7 1 14074.9 1052.69 7 -1 -7 2 29603.7 1415.92 7 -1 -7 3 13671.3 894.197 7 -1 -7 4 4871.14 462.230 7 -1 -6 -2 92536.8 2648.81 12 -1 -6 -1 77286.9 2387.40 12 -1 -6 0 24418.8 1366.19 12 -1 -6 1-43.2836 349.919 12 -1 -6 2 20620.4 1303.97 7 -1 -6 3 27130.7 1464.13 7 -1 -6 4 15658.3 1063.82 7 -1 -6 5 2318.60 402.042 7 -1 -5 -8 17213.1 611.751 11 -1 -5 -7 26131.3 1106.35 11 -1 -5 -6 37.6599 341.503 11 -1 -5 -5 192.534 282.596 11 -1 -5 -4 31292.5 1296.48 11 -1 -5 -3 48540.8 1454.59 11 -1 -5 0 45341.6 1552.04 12 -1 -5 1 58508.2 1846.15 12 -1 -5 2 5667.91 666.598 7 -1 -5 3 29880.5 1498.15 7 -1 -5 4 106158. 2861.25 7 -1 -5 5 18724.5 1208.44 7 -1 -5 6 2824.55 469.019 7 -1 -4 -8 2238.16 386.348 11 -1 -4 -7 16978.7 1058.36 11 -1 -4 -6 70321.9 2166.81 11 -1 -4 -5 57507.9 1836.52 11 -1 -4 -4 594.777 230.361 11 -1 -4 -3 51099.4 1889.75 4 -1 -4 -2 604988. 6337.38 4 -1 -4 1 90260.5 2707.38 2 -1 -4 2 72277.8 2573.64 2 -1 -4 3 18601.6 1406.91 2 -1 -4 3 19029.2 1056.59 7 -1 -4 4 1224.75 405.060 7 -1 -4 4 3346.49 622.355 2 -1 -4 5 83856.7 2522.35 7 -1 -4 6 22125.0 1311.65 7 -1 -3 -9 20831.0 867.281 11 -1 -3 -8 36336.6 1529.30 11 -1 -3 -7 1182.85 457.848 11 -1 -3 -6 19575.5 1172.57 11 -1 -3 -5 7009.50 632.153 11 -1 -3 -5 7185.91 812.788 4 -1 -3 -4 94169.3 2674.43 4 -1 -3 -3 16410.2 1053.85 4 -1 -3 -2 88324.8 2248.65 4 -1 -3 -1 31135.9 1309.79 4 -1 -3 0 91195.1 2349.03 2 -1 -3 1 5620.72 685.461 2 -1 -3 2 110162. 3003.87 2 -1 -3 3 148247. 3786.93 2 -1 -3 4 22515.6 1678.54 2 -1 -3 4 23924.3 1162.98 7 -1 -3 5 66170.2 2851.09 2 -1 -3 5 63945.8 2141.73 7 -1 -3 6 49038.3 2023.64 7 -1 -2 -9 4225.68 488.489 11 -1 -2 -8 17196.9 1159.03 11 -1 -2 -7 79331.5 2441.72 11 -1 -2 -6 17076.0 1311.49 4 -1 -2 -6 19000.6 1100.10 11 -1 -2 -5 32690.1 1685.04 4 -1 -2 -4 259907. 4297.87 4 -1 -2 -3 135349. 2750.87 4 -1 -2 -2 39753.6 1360.72 4 -1 -2 -1 643582. 4954.04 4 -1 -2 0 174418. 2643.63 4 -1 -2 0 172664. 2646.50 2 -1 -2 1 52656.6 1644.07 2 -1 -2 2 1036.42 390.672 2 -1 -2 3 29616.2 1649.01 2 -1 -2 4 150130. 4008.54 2 -1 -2 5 138513. 2867.37 7 -1 -2 5 138496. 4199.72 2 -1 -2 6 9774.07 917.407 7 -1 -1 -9 20168.9 998.923 11 -1 -1 -8 1620.34 494.956 11 -1 -1 -7 35039.2 1615.03 11 -1 -1 -6 72521.9 2758.11 4 -1 -1 -6 69818.0 1991.11 11 -1 -1 -5 14882.6 1173.40 4 -1 -1 -4 82588.5 2404.19 4 -1 -1 -3 122313. 2525.39 4 -1 -1 -2 431102. 3853.19 4 -1 -1 0 4824.11 386.914 2 -1 -1 1 177868. 2521.34 2 -1 -1 2 285614. 3894.57 1 -1 -1 3 5663.56 709.072 1 -1 -1 4 90093.5 3049.95 1 -1 -1 5 150578. 2930.30 7 -1 0 -9 38325.0 1278.97 11 -1 0 -8 16249.1 1095.30 11 -1 0 -7 6201.70 713.835 11 -1 0 -6 63884.8 2635.29 4 -1 0 -6 65774.4 1876.39 11 -1 0 -5 131299. 3544.16 4 -1 0 -4 75483.9 2337.51 4 -1 0 -3 91577.8 2180.38 4 -1 0 -2 183861. 2439.82 4 -1 0 -1 404470. 2545.33 4 -1 0 0 11781.5 344.387 4 -1 0 0 12028.2 430.220 3 -1 0 0 12622.0 372.475 2 -1 0 1 30382.5 624.426 3 -1 0 1 29445.7 885.135 1 -1 0 2 116370. 1358.06 3 -1 0 2 117410. 2315.13 1 -1 0 3 180894. 3574.57 1 -1 0 3 187151. 1940.18 3 -1 0 4 81496.4 2813.02 1 -1 0 5 16077.1 1438.39 1 -1 0 6 223363. 3452.80 13 -1 0 6 229706. 5538.63 1 -1 1 -9 2266.54 305.860 11 -1 1 -8 30329.4 1293.77 11 -1 1 -7 95418.7 2400.69 11 -1 1 -6 19966.0 1514.02 4 -1 1 -6 18002.8 1000.81 11 -1 1 -5 16312.6 1292.87 4 -1 1 -3 567567. 5320.87 3 -1 1 -2 38566.8 1264.28 3 -1 1 -1 233740. 2870.49 3 -1 1 0 233917. 1096.69 1 -1 1 0 231520. 2680.16 3 -1 1 1 251285. 2840.56 3 -1 1 2 3660.85 448.639 1 -1 1 2 3759.20 415.871 3 -1 1 3 130808. 2329.33 3 -1 1 3 122026. 2898.81 1 -1 1 4 157743. 3851.62 1 -1 1 5 18088.3 1493.62 1 -1 1 5 16711.9 949.046 13 -1 1 6 39690.2 1601.57 13 -1 1 7 42.9655 240.659 13 -1 2 -9 14795.9 692.500 9 -1 2 -8 3996.33 427.333 11 -1 2 -7 17884.4 993.758 11 -1 2 -6 74194.2 2919.79 4 -1 2 -6 76119.9 1924.63 11 -1 2 -6 77532.5 2372.82 10 -1 2 -5 7395.41 692.496 10 -1 2 -3 168515. 3184.10 3 -1 2 -2 16574.5 1012.61 3 -1 2 -1 1167.28 354.916 3 -1 2 0 52320.8 1718.97 3 -1 2 1 107478. 2480.33 3 -1 2 2 88350.7 2338.85 3 -1 2 3 11428.6 917.336 1 -1 2 3 10910.0 875.323 3 -1 2 4 72096.3 2273.60 3 -1 2 4 71694.9 2580.76 1 -1 2 5 161758. 3150.02 13 -1 2 5 159901. 4301.28 1 -1 2 6 58388.6 2017.45 13 -1 2 7 23732.9 1225.35 13 -1 3 -8 22071.4 1008.12 9 -1 3 -7 8020.09 776.315 9 -1 3 -6 51775.4 1996.34 10 -1 3 -5 111386. 2702.41 10 -1 3 -4 43462.9 1518.10 10 -1 3 -3 13891.7 1062.90 3 -1 3 -2 225593. 4197.16 3 -1 3 -1 264894. 4611.22 3 -1 3 0 28617.8 1544.39 3 -1 3 1 19269.9 1300.19 3 -1 3 2 121650. 3273.36 3 -1 3 3 120582. 2872.60 1 -1 3 3 115548. 3245.87 3 -1 3 4 15126.9 999.241 13 -1 3 4 15286.6 1234.88 3 -1 3 4 15978.7 1234.44 1 -1 3 5 27074.8 1465.51 13 -1 3 6 54969.3 2039.31 13 -1 3 7 652.099 322.600 13 -1 3 8 16819.5 640.227 13 -1 4 -7 12699.8 757.668 9 -1 4 -6 8881.80 791.026 9 -1 4 -6 10164.4 880.883 10 -1 4 -5 14429.0 989.594 9 -1 4 -5 16991.9 1143.23 10 -1 4 -4 34143.4 1353.45 9 -1 4 -4 37068.4 1560.17 10 -1 4 -3 45616.0 1348.46 9 -1 4 -3 48483.2 1722.27 8 -1 4 -3 46940.8 1984.57 3 -1 4 -2 7521.44 665.474 8 -1 4 -2 7372.29 869.495 3 -1 4 -1 11850.4 1121.56 3 -1 4 0 51502.1 2366.51 3 -1 4 1 48258.5 2335.24 3 -1 4 2 1806.02 409.401 13 -1 4 2 1685.22 503.525 3 -1 4 3 53517.6 2498.20 3 -1 4 3 52230.4 1827.54 13 -1 4 4 102287. 3264.86 3 -1 4 4 105132. 2842.43 13 -1 4 5 3891.02 684.464 13 -1 4 6 14450.2 1061.94 13 -1 4 7 50498.7 1547.55 13 -1 5 -6 55132.3 1558.33 10 -1 5 -5 3082.19 507.618 10 -1 5 -4 17693.9 1122.47 10 -1 5 -3 48575.0 1870.34 8 -1 5 -2 91843.9 2504.74 8 -1 5 -2 90716.5 2921.82 3 -1 5 -1-45.1476 345.519 8 -1 5 -1-191.153 223.733 3 -1 5 0 51309.6 2547.68 3 -1 5 1 104232. 3662.27 3 -1 5 1 99089.4 2491.37 13 -1 5 2 29914.1 1979.10 3 -1 5 2 26366.7 1392.70 13 -1 5 3 300.286 416.120 13 -1 5 4 22833.4 1442.69 13 -1 5 5 53696.3 2061.75 13 -1 5 6 9826.15 782.743 13 -1 5 7 3239.51 336.581 13 -1 6 -5 26827.3 944.640 10 -1 6 -4 7246.07 627.470 10 -1 6 -3-75.3627 268.361 10 -1 6 -2 34561.1 1541.14 8 -1 6 -1 14197.9 1038.68 8 -1 6 0 10045.4 917.585 8 -1 6 1 1042.06 415.578 8 -1 6 2 41553.1 1754.29 13 -1 6 3 24842.6 1384.07 13 -1 6 4 2608.93 523.772 13 -1 6 5 29521.0 1241.86 13 -1 6 6 11442.1 585.019 13 -1 7 -3 3413.34 332.276 10 -1 7 -2 750.789 249.477 10 -1 7 -1 24957.4 1081.31 8 -1 7 0 24402.9 1115.09 8 -1 7 1 6983.34 634.037 8 -1 7 2 12221.6 771.362 8 -1 7 3 13220.8 739.090 8 -1 7 4 18305.0 698.678 8 0 -8 -3 1309.98 218.697 12 0 -8 -1 1722.99 284.759 7 0 -8 0-27.5653 166.214 7 0 -8 1 10536.2 522.146 7 0 -7 -5 24293.1 906.455 12 0 -7 -4 29937.4 1216.08 12 0 -7 -3 116.834 260.738 12 0 -7 -2 10127.3 840.206 12 0 -7 -1 51660.6 1847.13 12 0 -7 0 39077.0 1603.23 12 0 -7 1 15055.4 990.777 7 0 -7 2 12634.7 841.343 7 0 -7 3 22150.7 963.294 7 0 -7 4 9562.53 511.508 7 0 -6 -2 41626.2 1779.07 12 0 -6 -1 8130.12 824.633 12 0 -6 0 19868.3 1223.19 12 0 -6 1 38044.4 1657.91 12 0 -6 2 3157.82 569.258 7 0 -6 3 10071.5 848.312 7 0 -6 4 46938.0 1638.80 7 0 -6 5 2639.07 388.365 7 0 -5 0 24512.2 1186.77 12 0 -5 1 156375. 3006.36 12 0 -5 3 3342.31 550.048 7 0 -5 4 9224.21 841.589 7 0 -5 5 43062.2 1668.32 7 0 -5 6 29045.2 1172.04 7 0 -4 -8 40726.8 980.944 11 0 -4 -7 921.548 291.536 11 0 -4 -6 20064.1 1073.64 11 0 -4 -5 46554.3 1538.89 11 0 -4 3 108818. 2376.16 7 0 -4 4 25392.0 1282.21 7 0 -4 5 20396.4 1212.21 7 0 -4 6 24150.7 1289.48 7 0 -3 -8 7639.28 639.768 11 0 -3 -7 66742.0 2055.22 11 0 -3 -6 10990.3 856.410 11 0 -3 -5 18346.6 952.349 11 0 -3 -2 18083.9 831.153 4 0 -3 1 56277.0 1606.49 2 0 -3 2 57616.3 1827.68 2 0 -3 3 24164.7 1364.69 2 0 -3 4 75331.9 2613.32 2 0 -3 4 76684.9 1899.31 7 0 -3 5 42918.5 1644.03 7 0 -3 6 1866.22 486.940 7 0 -2 -9 8272.84 530.399 11 0 -2 -8 598.201 349.986 11 0 -2 -7 53197.9 1981.32 11 0 -2 -6 74270.1 2142.54 11 0 -2 -5 32855.5 1215.78 11 0 -2 -4 2809.71 466.368 4 0 -2 -3 52678.5 1496.93 4 0 -2 -2 161747. 2226.52 4 0 -2 -1 999999. 4884.36 4 0 -2 1 321939. 3251.61 2 0 -2 2 206055. 3130.23 2 0 -2 3 24178.1 1301.70 2 0 -2 4 59014.9 2257.78 2 0 -2 5 129868. 2585.93 7 0 -2 5 135706. 3860.76 2 0 -2 6 24562.2 1311.44 7 0 -1 -9 24505.2 992.935 11 0 -1 -8 55553.3 1945.14 11 0 -1 -7 9125.22 896.390 11 0 -1 -6 53766.9 2171.53 4 0 -1 -6 57397.1 1848.55 11 0 -1 -5 101204. 2884.02 4 0 -1 -4 31242.4 1398.79 4 0 -1 -3 12382.3 772.871 4 0 -1 -2 135113. 1871.94 4 0 -1 -1 50458.7 847.316 4 0 -1 0 15503.9 450.071 2 0 -1 2 132001. 2254.23 1 0 -1 3 41338.0 1585.81 1 0 -1 4 30580.5 1626.44 1 0 -1 5 11429.7 1160.36 1 0 0 -9 5872.31 504.474 11 0 0 -8 31285.5 1456.93 11 0 0 -7 60394.5 2125.37 11 0 0 -6 7748.16 941.912 4 0 0 -6 7182.85 714.770 11 0 0 -5 27960.8 1578.68 4 0 0 2 55722.7 1400.52 1 0 0 3 188084. 3322.96 1 0 0 4 215237. 4302.13 1 0 0 5 33932.9 1984.22 1 0 0 6 9075.19 1196.59 1 0 1 -9 41151.9 1141.61 11 0 1 -8 308.268 293.679 11 0 1 -7 69992.9 2231.10 11 0 1 -6 119412. 3680.17 4 0 1 -2 138440. 1718.91 3 0 1 -1 22192.3 634.400 3 0 1 0 14911.4 495.280 3 0 1 4 33585.5 1738.22 1 0 1 5 129047. 3856.89 1 0 1 6 63702.8 2943.13 1 0 2 -9 16165.8 666.755 9 0 2 -8 17114.0 923.133 11 0 2 -7-21.6753 307.847 11 0 2 -5 141391. 2693.48 10 0 2 -3 26537.2 996.229 3 0 2 -2 205818. 2708.52 3 0 2 -1 345303. 3479.53 3 0 2 0 386442. 3766.68 3 0 2 5 34375.8 1993.53 1 0 2 6 84742.9 2073.35 13 0 2 6 87006.1 3379.46 1 0 3 -8 55007.4 1502.67 9 0 3 -8 57883.1 1277.31 11 0 3 -7 57094.1 1700.97 11 0 3 -5 47488.3 1684.64 10 0 3 -4 81679.6 1854.38 10 0 3 -2 59741.7 1780.43 3 0 3 -1 52061.2 1742.20 3 0 3 0 179823. 3311.62 3 0 3 1 66603.1 2141.77 3 0 3 2 20147.9 1256.44 3 0 3 3 79234.4 2614.28 3 0 3 4 148016. 3669.98 3 0 3 5 20740.5 1584.60 1 0 3 5 22428.4 1166.38 13 0 3 5 21359.8 1433.50 3 0 3 6 12344.9 936.114 13 0 3 7 76573.3 2076.29 13 0 4 -7 23246.1 992.318 9 0 4 -6 24597.7 1190.13 9 0 4 -5 19525.7 1114.87 10 0 4 -4 25491.2 1205.34 10 0 4 -2 51284.6 1936.10 3 0 4 -1 2369.52 512.382 3 0 4 0 73220.7 2539.14 3 0 4 1 372593. 5961.39 3 0 4 2 11883.5 1129.95 3 0 4 3 8311.36 692.239 13 0 4 3 7213.62 945.777 3 0 4 4 31037.5 1414.34 13 0 4 4 28345.5 1813.52 3 0 4 5 56803.3 2050.81 13 0 4 5 54939.9 2390.93 3 0 4 6 22224.9 1287.81 13 0 4 7 653.349 302.260 13 0 5 -5 44894.9 1530.78 10 0 5 -4 9231.16 762.333 10 0 5 -3 3425.12 485.201 10 0 5 -2 13625.3 874.440 8 0 5 -1 173124. 4092.56 3 0 5 -1 182448. 2899.60 8 0 5 0 25540.8 1709.70 3 0 5 0 26735.4 1127.17 8 0 5 1 20457.1 1570.40 3 0 5 1 22424.8 1163.18 13 0 5 2 60820.9 1980.39 13 0 5 2 61362.9 2749.11 3 0 5 3 102899. 2736.52 13 0 5 3 108068. 3709.48 3 0 5 4 4250.14 669.556 13 0 5 5 27942.9 1544.13 13 0 5 6 44480.7 1740.62 13 0 5 7 14377.8 788.250 13 0 6 -4 46787.1 1380.65 10 0 6 -3 10730.3 758.439 10 0 6 -2 4219.80 537.404 8 0 6 -1 43183.0 1604.41 8 0 6 0 23660.6 1233.39 8 0 6 1 7895.85 771.585 8 0 6 2 46111.4 1935.44 13 0 6 3 7459.66 878.782 13 0 6 4 15447.4 1187.58 13 0 6 5 5467.49 681.407 13 0 6 6 5486.10 537.478 13 0 7 0 37515.1 1308.89 8 0 7 1 53586.9 1611.69 8 0 7 2 10592.3 744.249 8 0 7 3 440.594 250.829 8 0 7 5 22924.9 678.448 8 1 -7 -4 16508.1 632.320 12 1 -7 -3 13435.7 699.787 12 1 -7 -2 12176.0 723.988 12 1 -7 -1 7158.78 591.929 12 1 -7 1 25528.5 1000.00 7 1 -7 2 796.686 224.149 7 1 -6 -2 39238.6 1594.03 12 1 -6 -1 921.978 372.105 12 1 -6 0 10544.6 839.603 12 1 -6 2 31915.3 1346.57 7 1 -6 3-123.794 237.472 7 1 -6 4 7882.97 566.412 7 1 -5 0 43399.4 1552.87 12 1 -5 1 255.790 270.665 12 1 -5 3 51064.8 1738.45 7 1 -5 4 19331.1 1063.35 7 1 -5 5 3250.41 447.034 7 1 -4 3 45809.4 1425.61 7 1 -4 4 33662.6 1329.28 7 1 -4 5 14249.5 928.938 7 1 -4 6 8575.61 684.877 7 1 -3 -7 671.055 281.565 11 1 -3 -6 48162.0 1559.66 11 1 -3 4 43267.3 1295.82 7 1 -3 5 106857. 2317.72 7 1 -3 6 54923.9 1789.43 7 1 -2 -8 22908.5 954.782 11 1 -2 -7 20099.5 1104.20 11 1 -2 -6 55705.0 1800.61 11 1 -2 -5 136926. 2444.00 11 1 -2 2 17809.9 725.571 2 1 -2 3 177239. 2884.62 2 1 -2 4 14596.8 1028.08 2 1 -2 5 7093.48 588.182 7 1 -2 6 76013.5 2082.94 7 1 -1 -9 3278.96 284.728 11 1 -1 -8 34426.5 1351.11 11 1 -1 -7 509.801 372.418 11 1 -1 -6 36821.9 1527.53 11 1 -1 -5 13347.5 807.227 11 1 -1 -4 125282. 2558.06 4 1 -1 -3 106117. 1987.38 4 1 -1 -2 2830.91 266.700 4 1 -1 -1 211836. 970.582 4 1 -1 1 226417. 1264.41 2 1 -1 2 41914.9 1022.99 1 1 -1 3 572492. 5053.98 1 1 -1 4 36650.1 1638.84 1 1 -1 5 18368.1 1324.17 1 1 -1 6 17727.1 1396.94 1 1 0 -9 11347.6 545.200 11 1 0 -8 4069.42 547.115 11 1 0 -7 35315.0 1619.04 11 1 0 -6 194221. 3566.57 11 1 0 -5 11960.2 1005.33 4 1 0 4 72545.0 2322.77 1 1 0 5 149216. 3853.83 1 1 0 6 67003.1 2871.10 1 1 1 -9 11059.7 515.600 11 1 1 -8 22022.6 1121.21 11 1 1 -7 259.570 340.740 11 1 1 -6-392.214 384.289 4 1 1 5 15214.1 1315.65 1 1 1 6 76081.3 3096.05 1 1 2 -8 44119.6 1458.73 11 1 2 -7 24216.8 1341.88 11 1 2 -1 53701.7 1000.80 3 1 2 6 22155.8 1748.81 1 1 3 -8 1769.63 273.983 11 1 3 -7 29954.5 1328.92 11 1 3 -1 6679.04 527.363 3 1 3 0 94057.4 2070.79 3 1 3 5 6146.48 529.254 13 1 3 6 22638.2 1753.97 1 1 4 -7 3976.62 395.072 9 1 4 -7 3601.17 409.441 11 1 4 -1 88821.6 2317.57 3 1 4 0 45672.3 1782.75 3 1 4 1 1024.99 391.298 3 1 4 2 633635. 7562.55 3 1 4 4 30.0737 266.360 13 1 4 5 69218.5 2036.14 13 1 4 5 63336.4 2702.66 3 1 4 6 84801.5 2269.06 13 1 5 0 46201.7 2050.13 3 1 5 1 6182.08 824.301 3 1 5 2 383.554 268.640 13 1 5 2-223.538 381.352 3 1 5 3 60756.6 1981.85 13 1 5 3 60262.7 2685.91 3 1 5 4 34580.4 1590.88 13 1 5 4 37899.5 2191.73 3 1 5 5 265.894 364.923 13 1 5 6 545.538 351.925 13 1 5 7 27551.8 1095.84 13 1 6 1 81004.4 2880.11 3 1 6 3 97294.5 2820.27 13 1 6 4 38613.7 1816.02 13 1 6 5 32507.0 1571.11 13 1 6 6 2365.43 443.772 13 2 -6 -4 20172.9 694.046 12 2 -6 -3 578.829 211.047 12 2 -6 -2 22759.2 960.393 12 2 -5 -1 2200.77 408.816 12 2 -1 -8 3915.33 335.755 11 2 -1 -7 90336.5 2095.81 11 2 -1 -6 15471.1 962.307 11 2 -1 -5 14001.3 831.727 11 2 -1 3 596.976 217.526 1 2 -1 4 76982.0 1987.64 1 2 0 -8 24102.6 925.842 11 2 0 -7 2283.42 459.376 11 2 0 -6 26238.8 1340.09 11 2 0 4 14078.6 970.800 1 2 0 5 68723.0 2429.69 1 2 0 6 53213.3 2336.30 1 2 1 -8 55633.5 1464.16 11 2 1 -7 33452.9 1501.99 11 2 1 6 26426.5 1791.61 1 2 2 -8 2211.31 325.492 11 2 2 -7 44098.2 1688.04 11 2 3 -8 12245.9 544.707 11 2 3 -7 5722.24 610.504 11 2 4 -7 22496.7 907.059 11 2 4 0 114310. 2467.48 3 2 4 5 30738.9 1166.24 13 2 5 1 70113.3 2478.74 3 2 5 2 19696.6 1415.98 3 2 5 3 3152.35 494.979 13 2 5 3 2221.11 578.101 3 2 5 4 90871.1 2375.48 13 2 5 4 90244.6 3324.93 3 2 5 5 54337.0 1848.77 13 2 5 6 1711.39 359.625 13 2 6 2 47682.8 2190.75 3 3 0 -7 33109.2 1027.52 11 3 0 -6 520.546 312.044 11 3 0 -5 31672.7 1295.05 11 3 1 -7 51882.5 1460.44 11 3 1 -6 48060.2 1698.11 11 3 1 6 17433.6 1338.35 1 3 2 -7 1076.84 297.499 11 3 3 -7 31822.9 1091.94 11 3 4 -7 27820.3 803.560 11 4 2 -6 705.160 252.936 11 0 0 0 0.00 0.00 0 TITL mona38CuLT in P1 REM P1 (#1 in standard setting) CELL 1.54184 6.958134 7.141281 8.028370 81.9588 73.8115 71.3518 ZERR 2.00 0.000708 0.000844 0.000930 0.0097 0.0095 0.0099 LATT -1 SFAC C H O Br UNIT 14.00 10.00 6.00 2.00 TREF HKLF 4 END ; _shelx_hkl_checksum 91182 _olex2_date_sample_data_collection 2020-04-29 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.129 _oxdiff_exptl_absorpt_empirical_full_min 0.912 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br1 Br 0.34554(4) 0.33980(4) 0.13425(3) 0.02047(12) Uani 1 1 d . . . . . O1 O -0.1742(3) 0.0934(3) 0.8901(3) 0.0195(4) Uani 1 1 d . . . . . O2 O 0.1586(3) 0.0998(3) 0.8055(3) 0.0208(4) Uani 1 1 d . . . . . H2 H 0.172(7) 0.035(7) 0.897(7) 0.048(13) Uiso 1 1 d . . . . . O3 O -0.4134(3) 0.2270(3) 0.6722(3) 0.0228(4) Uani 1 1 d . . . . . H3 H -0.379(8) 0.163(8) 0.764(7) 0.057(14) Uiso 1 1 d . . . . . C1 C -0.0456(4) 0.2111(4) 0.6026(3) 0.0158(5) Uani 1 1 d . . . . . C2 C -0.2393(4) 0.2545(4) 0.5612(4) 0.0164(5) Uani 1 1 d . . . . . C3 C -0.2556(4) 0.3313(4) 0.3941(4) 0.0196(5) Uani 1 1 d . . . . . H3A H -0.3868 0.3645 0.3660 0.023 Uiso 1 1 calc R . . . . C4 C -0.0845(4) 0.3595(4) 0.2702(4) 0.0187(5) Uani 1 1 d . . . . . H4 H -0.0975 0.4124 0.1571 0.022 Uiso 1 1 calc R . . . . C5 C 0.1090(4) 0.3100(4) 0.3113(3) 0.0163(5) Uani 1 1 d . . . . . C6 C 0.1298(4) 0.2386(4) 0.4754(3) 0.0151(5) Uani 1 1 d . . . . . H6 H 0.2613 0.2082 0.5025 0.018 Uiso 1 1 calc R . . . . C7 C -0.0262(4) 0.1303(4) 0.7776(4) 0.0165(5) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Br1 0.01547(17) 0.02772(18) 0.01727(17) -0.00003(11) -0.00064(11) -0.00857(12) O1 0.0137(9) 0.0220(9) 0.0200(10) 0.0007(7) -0.0011(7) -0.0048(7) O2 0.0148(9) 0.0299(10) 0.0196(10) 0.0041(8) -0.0062(8) -0.0100(8) O3 0.0114(9) 0.0276(10) 0.0265(11) 0.0019(8) -0.0018(8) -0.0057(8) C1 0.0135(12) 0.0139(11) 0.0191(13) -0.0034(9) -0.0027(10) -0.0029(9) C2 0.0118(11) 0.0138(11) 0.0226(13) -0.0026(9) -0.0024(10) -0.0033(9) C3 0.0128(12) 0.0221(12) 0.0243(14) -0.0027(10) -0.0068(10) -0.0034(10) C4 0.0178(13) 0.0186(12) 0.0193(13) -0.0006(10) -0.0072(10) -0.0029(10) C5 0.0134(12) 0.0166(11) 0.0173(12) -0.0031(9) -0.0003(9) -0.0044(9) C6 0.0090(11) 0.0151(11) 0.0193(12) -0.0032(9) -0.0012(9) -0.0020(9) C7 0.0115(12) 0.0158(11) 0.0211(13) -0.0027(9) -0.0026(10) -0.0029(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.6763 1.2805 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C7 O2 H2 113(3) . . ? C2 O3 H3 108(3) . . ? C2 C1 C7 119.6(2) . . ? C6 C1 C2 120.1(2) . . ? C6 C1 C7 120.3(2) . . ? O3 C2 C1 124.4(2) . . ? O3 C2 C3 116.7(2) . . ? C3 C2 C1 119.0(2) . . ? C2 C3 H3A 119.6 . . ? C4 C3 C2 120.9(2) . . ? C4 C3 H3A 119.6 . . ? C3 C4 H4 120.2 . . ? C3 C4 C5 119.6(2) . . ? C5 C4 H4 120.2 . . ? C4 C5 Br1 118.7(2) . . ? C6 C5 Br1 120.2(2) . . ? C6 C5 C4 121.1(2) . . ? C1 C6 H6 120.4 . . ? C5 C6 C1 119.2(2) . . ? C5 C6 H6 120.4 . . ? O1 C7 O2 122.7(2) . . ? O1 C7 C1 122.1(2) . . ? O2 C7 C1 115.2(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Br1 C5 1.900(3) . ? O1 C7 1.239(3) . ? O2 H2 0.82(5) . ? O2 C7 1.311(3) . ? O3 H3 0.86(5) . ? O3 C2 1.342(3) . ? C1 C2 1.406(4) . ? C1 C6 1.405(4) . ? C1 C7 1.468(4) . ? C2 C3 1.397(4) . ? C3 H3A 0.9500 . ? C3 C4 1.373(4) . ? C4 H4 0.9500 . ? C4 C5 1.399(4) . ? C5 C6 1.374(4) . ? C6 H6 0.9500 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O2 H2 O1 0.82(5) 1.83(5) 2.645(3) 174(5) 2_557 O3 H3 O1 0.86(5) 1.87(5) 2.623(3) 144(5) .