#------------------------------------------------------------------------------ #$Date: 2021-12-21 04:59:12 +0200 (Tue, 21 Dec 2021) $ #$Revision: 271558 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/24/2022489.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022489 _cell_angle_alpha 90.000 _cell_angle_beta 96.296 _cell_angle_gamma 90.000 _cell_length_a 18.7299 _cell_length_b 11.1592 _cell_length_c 21.6646 _exptl_crystal_F_000 1912.00 _reflns_d_resolution_high 0.6547 _cod_data_source_file yd30223sup4.hkl _cod_data_source_block 3 _shelx_title ' jpl-351_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 403.57 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 11716.38 11304.18 233.99 o 5 0 0 62935.20 59192.23 601.98 o 6 0 0 24.43 37.25 29.76 o 7 0 0 2328.24 2376.08 147.93 o 8 0 0 60.61 28.18 36.48 o 9 0 0 195.04 55.75 34.40 o 10 0 0 897.37 1096.43 122.12 o 11 0 0 4608.27 4608.46 253.68 o 12 0 0 2073.16 1849.20 170.15 o 13 0 0 1759.78 1524.87 154.39 o 14 0 0 8255.51 9067.96 402.98 o 15 0 0 1058.23 1276.93 159.59 o 16 0 0 1560.53 1609.74 185.82 o 17 0 0 4284.59 4051.12 317.09 o 18 0 0 2195.33 2016.45 231.34 o 19 0 0 126.22 131.00 79.81 o 20 0 0 2015.59 2058.50 255.00 o 21 0 0 892.37 983.29 185.10 o 22 0 0 351.71 112.11 90.98 o 23 0 0 968.49 968.10 190.36 o 24 0 0 1134.96 1309.83 229.90 o 25 0 0 391.43 629.34 172.34 o 26 0 0 757.34 1018.87 213.36 o 27 0 0 0.82 24.72 80.19 o 3 1 0 6654.71 6217.14 107.16 o 4 1 0 7564.66 7108.21 106.64 o 5 1 0 5199.74 4775.77 97.92 o 6 1 0 2074.60 1774.74 80.93 o 7 1 0 4.91 38.26 81.35 o 8 1 0 367.50 364.62 42.71 o 9 1 0 103.93 98.82 26.64 o 10 1 0 221.83 94.36 27.11 o 11 1 0 784.38 1442.43 117.22 o 12 1 0 2318.50 2700.75 142.13 o 13 1 0 67.65 649.29 82.18 o 14 1 0 60.79 339.84 61.72 o 15 1 0 821.78 1885.68 134.31 o 16 1 0 151.73 325.45 96.07 o 17 1 0 30.27 363.02 121.39 o 18 1 0 134.74 196.23 62.84 o 19 1 0 305.62 1472.18 148.12 o 20 1 0 488.80 344.89 81.99 o 21 1 0 0.05 656.85 111.99 o 22 1 0 435.25 1057.89 137.35 o 23 1 0 10.42 425.24 97.72 o 24 1 0 232.87 834.02 132.01 o 25 1 0 2.32 683.21 123.43 o 26 1 0 10.53 218.25 80.95 o 27 1 0 1.66 389.74 103.19 o 0 2 0 11691.16 12365.54 224.46 o 1 2 0 113.53 173.63 17.22 o 2 2 0 23652.26 24644.67 424.09 o 3 2 0 162870.17 170806.89 1256.04 o 4 2 0 352.20 329.20 23.51 o 5 2 0 17831.54 16612.53 275.73 o 6 2 0 2367.20 2468.66 88.93 o 7 2 0 2906.39 2600.95 108.00 o 8 2 0 1219.20 1302.99 83.20 o 9 2 0 8920.56 8414.09 222.56 o 10 2 0 425.47 185.71 48.73 o 11 2 0 6704.97 6806.92 366.26 o 12 2 0 556.88 312.98 50.34 o 13 2 0 250.33 383.00 167.29 o 14 2 0 3359.90 3566.07 186.77 o 15 2 0 27.64 99.15 120.32 o 16 2 0 708.10 680.69 276.12 o 17 2 0 14.86 -65.67 65.67 o 18 2 0 1152.89 642.38 223.67 o 19 2 0 652.06 332.38 73.46 o 20 2 0 1923.10 2199.29 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779.62 537.02 45.04 o 9 5 0 330.10 169.68 28.28 o 10 5 0 771.37 483.24 51.94 o 11 5 0 2044.11 2004.58 116.58 o 12 5 0 345.03 115.95 177.79 o 13 5 0 206.05 436.55 237.24 o 14 5 0 781.31 585.83 71.70 o 15 5 0 1703.48 2058.05 530.35 o 16 5 0 54.51 56.57 64.29 o 17 5 0 1837.97 1645.62 141.59 o 18 5 0 1.80 -45.80 45.80 o 19 5 0 1271.96 1209.38 131.69 o 20 5 0 92.62 510.70 94.31 o 21 5 0 273.33 502.07 97.02 o 22 5 0 892.72 1271.11 146.79 o 23 5 0 90.80 156.73 104.79 o 24 5 0 446.26 861.46 199.66 o 25 5 0 852.03 1332.67 254.07 o 0 6 0 5631.20 5750.93 77.20 o 1 6 0 407.95 430.76 22.96 o 2 6 0 4287.40 4156.69 103.74 o 3 6 0 4954.44 5269.52 94.97 o 4 6 0 405.84 230.12 17.34 o 5 6 0 673.76 552.73 38.28 o 6 6 0 18.83 12.71 15.43 o 7 6 0 501.30 475.45 26.82 o 8 6 0 100.03 -0.66 19.81 o 9 6 0 1856.06 1914.94 93.46 o 10 6 0 2171.16 2107.30 108.60 o 11 6 0 2240.41 1933.71 146.94 o 12 6 0 3376.43 3790.54 309.65 o 13 6 0 1605.94 1623.90 113.55 o 14 6 0 3338.78 3215.51 165.22 o 15 6 0 8.37 -44.01 44.01 o 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711.71 668.55 31.58 o 2 8 0 773.08 753.37 47.84 o 3 8 0 872.80 807.43 68.06 o 4 8 0 8.93 -9.97 38.77 o 5 8 0 7.99 -3.58 51.52 o 6 8 0 1156.76 1061.46 118.09 o 7 8 0 48.98 -8.99 60.02 o 8 8 0 120.61 -59.33 66.93 o 9 8 0 490.55 413.44 114.59 o 10 8 0 624.38 303.17 86.01 o 11 8 0 1.70 390.36 125.05 o 12 8 0 660.03 715.81 143.98 o 13 8 0 232.13 554.04 124.10 o 14 8 0 647.18 1224.27 194.93 o 15 8 0 144.11 -60.54 82.58 o 16 8 0 628.80 472.83 123.88 o 17 8 0 585.18 372.92 112.45 o 18 8 0 0.86 -112.24 112.24 o 19 8 0 40.93 -95.00 95.00 o 20 8 0 43.21 -11.27 67.78 o 21 8 0 15.66 768.70 198.66 o 22 8 0 98.05 325.19 141.65 o 23 8 0 115.39 1144.26 236.28 o 1 9 0 483.60 433.26 36.22 o 2 9 0 3777.43 3692.50 83.84 o 3 9 0 938.81 878.05 60.07 o 4 9 0 2829.70 2936.08 144.52 o 5 9 0 520.63 386.64 50.09 o 6 9 0 3068.62 3132.25 218.65 o 7 9 0 1983.61 1749.27 168.24 o 8 9 0 2528.32 2024.68 180.92 o 9 9 0 150.76 24.93 63.71 o 10 9 0 2235.66 2061.66 205.01 o 11 9 0 330.49 106.98 54.34 o 12 9 0 401.12 389.43 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