#------------------------------------------------------------------------------ #$Date: 2022-02-10 04:57:23 +0200 (Thu, 10 Feb 2022) $ #$Revision: 272899 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/25/2022538.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2022538 _cell_angle_alpha 74.992 _cell_angle_beta 84.667 _cell_angle_gamma 71.815 _cell_length_a 9.6431 _cell_length_b 14.4883 _cell_length_c 20.8044 _exptl_crystal_F_000 1072.00 _reflns_d_resolution_high 0.8393 _cod_data_source_file zo30166sup5.hkl _cod_data_source_block 6 _shelx_title ' 06010 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.40 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 4086.83 4162.70 62.62 o 2 0 0 360.86 323.73 9.92 o 3 0 0 9786.14 9694.06 117.62 o 4 0 0 1714.08 1684.90 28.99 o 5 0 0 1927.65 1851.63 39.82 o 6 0 0 462.10 438.23 15.58 o 7 0 0 692.53 774.58 21.38 o 8 0 0 1005.74 986.02 30.81 o 9 0 0 2.10 9.16 16.45 o 10 0 0 17.52 13.64 23.30 o -10 1 0 157.70 155.31 37.91 o -9 1 0 27.88 77.97 17.20 o -8 1 0 395.47 421.25 18.44 o -7 1 0 606.54 562.24 19.45 o -6 1 0 169.42 161.14 13.11 o -5 1 0 16.94 13.65 7.86 o -4 1 0 2084.97 2039.38 47.08 o -3 1 0 194.16 251.86 11.13 o -2 1 0 218.37 158.24 14.97 o -1 1 0 7687.77 7242.78 97.76 o 0 1 0 367.30 487.90 7.96 o 1 1 0 210.74 160.79 5.70 o 2 1 0 3135.38 3493.44 44.84 o 3 1 0 2228.71 2300.43 33.40 o 4 1 0 301.91 392.45 16.01 o 5 1 0 88.73 54.28 12.48 o 6 1 0 0.53 4.52 8.59 o 7 1 0 366.03 335.51 15.66 o 8 1 0 10.53 6.92 14.61 o 9 1 0 218.60 238.36 19.94 o 10 1 0 66.14 43.73 24.10 o 11 1 0 140.72 159.30 31.29 o -10 2 0 318.16 293.70 28.22 o -9 2 0 0.31 14.40 18.02 o -8 2 0 22.35 19.07 11.82 o -7 2 0 1540.12 1409.05 37.20 o -6 2 0 45.32 34.33 11.54 o -5 2 0 27.94 23.98 9.02 o -4 2 0 3475.76 3394.19 58.56 o -3 2 0 5.23 16.39 7.65 o -2 2 0 5342.64 5635.28 72.09 o -1 2 0 4061.92 4090.79 52.67 o 0 2 0 3591.91 3839.93 43.32 o 1 2 0 8051.61 8759.73 93.52 o 2 2 0 11892.42 12886.87 135.71 o 3 2 0 1387.05 1343.42 22.45 o 4 2 0 257.45 189.98 14.46 o 5 2 0 3876.17 4033.31 50.96 o 6 2 0 625.65 603.52 17.00 o 7 2 0 1123.19 1060.35 23.90 o 8 2 0 129.73 144.06 17.32 o 9 2 0 403.26 387.37 32.69 o 10 2 0 120.46 78.58 61.29 o 11 2 0 165.72 184.39 31.97 o -10 3 0 4.27 32.61 21.42 o -9 3 0 72.61 111.38 22.59 o -8 3 0 429.71 436.34 40.80 o -7 3 0 124.55 138.21 16.44 o -6 3 0 204.30 176.22 15.54 o -5 3 0 894.48 851.98 23.72 o -4 3 0 1667.79 1510.45 30.29 o -3 3 0 7863.01 7423.74 95.82 o -2 3 0 94.05 91.67 9.22 o -1 3 0 13.14 17.87 7.92 o 0 3 0 174.34 189.86 13.39 o 1 3 0 10450.16 11352.51 141.62 o 2 3 0 23799.30 25785.95 474.36 o 3 3 0 723.05 706.01 27.75 o 4 3 0 109.44 177.03 9.12 o 5 3 0 745.54 752.15 17.09 o 6 3 0 1220.96 1201.34 23.34 o 7 3 0 202.30 193.17 13.18 o 8 3 0 319.21 297.91 18.99 o 9 3 0 105.60 112.95 24.96 o 10 3 0 62.32 53.27 37.57 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251.76 238.38 43.95 o 3 7 23 131.77 108.90 39.51 o -1 8 23 134.58 134.22 34.12 o 0 8 23 97.36 118.61 31.96 o 2 8 23 59.48 3.19 36.83 o 3 8 23 24.09 60.21 38.82 o 4 8 23 37.92 -13.03 37.01 o 0 9 23 4.19 38.77 28.16 o 3 9 23 39.31 66.51 40.46 o 4 9 23 0.16 7.63 38.86 o 3 10 23 57.35 62.37 40.93 o -1 1 24 75.99 40.64 26.05 o 0 1 24 15.80 12.93 23.25 o 1 1 24 56.55 97.65 34.16 o -1 2 24 214.44 218.92 29.98 o 0 2 24 0.06 92.94 34.37 o 1 2 24 176.50 152.64 38.30 o -1 3 24 76.30 45.72 24.09 o 0 3 24 26.89 34.46 30.41 o 1 3 24 0.48 79.23 31.57 o 3 3 24 10.81 34.48 28.64 o -1 4 24 1.73 19.68 25.68 o 0 4 24 2.91 48.22 29.67 o 1 4 24 4.99 9.36 28.77 o 2 4 24 377.53 512.81 47.05 o 3 4 24 31.89 17.42 34.46 o -1 5 24 44.17 46.71 28.68 o 0 5 24 72.74 122.32 34.37 o 1 5 24 104.59 112.18 32.74 o 2 5 24 67.08 73.02 31.70 o 3 5 24 146.29 140.34 40.76 o -1 6 24 28.35 134.22 35.37 o 0 6 24 399.46 446.26 43.69 o 1 6 24 92.28 117.27 33.08 o 3 6 24 62.44 36.70 40.02 o 0 7 24 203.61 316.83 40.15 o 1 7 24 5.48 75.61 30.92 o 3 7 24 179.86 136.76 43.52 o