#------------------------------------------------------------------------------
#$Date: 2022-08-23 04:39:56 +0300 (Tue, 23 Aug 2022) $
#$Revision: 277355 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/26/2022652.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2022652
_cell_angle_alpha                90.000
_cell_angle_beta                 93.710
_cell_angle_gamma                90.000
_cell_length_a                   16.8354
_cell_length_b                   6.7870
_cell_length_c                   10.1499
_exptl_crystal_F_000             944.00
_reflns_d_resolution_high        0.7701
_cod_data_source_file            wp3029Isup2.hkl
_cod_data_source_block           I
_shelx_title                     ' AJC_Li4CdGe2S7_141_2_0m in Cc'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            565.76
_shelx_f_squared_multiplier      1.000
loop_
_space_group_symop_operation_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
-1 1 -13 6277.24 6298.27 117.97 o
1 1 -13 6403.95 6541.73 120.50 o
3 1 -13 3471.96 3303.29 82.01 o
-6 0 -12 432.92 572.83 73.65 o
-4 0 -12 9742.71 9532.30 262.88 o
-2 0 -12 19508.85 19416.56 439.97 o
0 0 -12 6502.79 6533.62 207.85 o
2 0 -12 440.21 403.71 62.74 o
4 0 -12 8286.21 8173.19 290.11 o
6 0 -12 1087.97 1081.33 57.50 o
8 0 -12 8519.61 8734.11 171.72 o
10 0 -12 11526.81 11566.96 208.81 o
-7 1 -12 814.89 837.46 54.95 o
-5 1 -12 244.58 286.13 39.50 o
-3 1 -12 2352.27 2293.72 65.46 o
-1 1 -12 1471.69 1451.15 53.69 o
1 1 -12 1458.50 1517.01 53.38 o
3 1 -12 1417.23 1432.18 51.64 o
5 1 -12 4453.30 4377.79 92.98 o
7 1 -12 196.04 176.45 24.30 o
9 1 -12 563.72 552.27 37.69 o
-6 2 -12 165.07 180.74 38.10 o
-4 2 -12 1958.32 1971.77 87.75 o
-2 2 -12 3664.15 3588.96 82.51 o
0 2 -12 3467.12 3481.33 81.84 o
2 2 -12 478.57 462.23 34.04 o
4 2 -12 790.99 813.93 61.95 o
6 2 -12 151.21 160.96 24.87 o
8 2 -12 2087.50 2071.58 64.37 o
-3 3 -12 6616.92 6585.03 119.61 o
-1 3 -12 1713.57 1807.50 59.02 o
1 3 -12 2187.68 2197.37 64.66 o
3 3 -12 2855.88 2740.45 71.92 o
5 3 -12 10493.91 10697.24 163.68 o
-9 1 -11 2450.80 2402.08 80.09 o
-7 1 -11 7631.42 7735.71 358.43 o
-5 1 -11 2682.58 2690.53 67.52 o
-3 1 -11 234.66 306.27 29.65 o
-1 1 -11 44849.92 45137.65 564.43 o
1 1 -11 1486.82 1497.19 55.70 o
3 1 -11 3207.36 3213.34 73.66 o
5 1 -11 11577.97 11698.41 167.20 o
7 1 -11 9067.98 9238.62 143.37 o
9 1 -11 5853.92 5986.32 124.70 o
11 1 -11 1131.86 1148.17 43.79 o
-8 2 -11 18158.41 18210.46 232.53 o
-6 2 -11 1604.75 1643.34 53.99 o
-4 2 -11 5666.95 5720.62 104.35 o
-2 2 -11 10360.72 10304.73 152.78 o
0 2 -11 6579.16 6606.12 113.97 o
2 2 -11 900.25 882.01 40.15 o
4 2 -11 2328.39 2343.23 63.51 o
6 2 -11 24253.98 25035.66 301.05 o
8 2 -11 1921.02 1959.40 59.03 o
10 2 -11 956.56 894.43 42.91 o
12 2 -11 2416.37 2650.54 120.37 o
-7 3 -11 1377.98 1350.03 51.19 o
-5 3 -11 1182.53 1108.24 46.39 o
-3 3 -11 830.91 863.69 42.15 o
-1 3 -11 1410.26 1491.36 58.85 o
1 3 -11 638.90 642.18 36.92 o
3 3 -11 216.74 257.36 26.87 o
5 3 -11 380.59 363.35 29.76 o
7 3 -11 610.84 669.91 37.95 o
9 3 -11 2155.63 2150.57 61.79 o
-4 4 -11 7194.49 7263.23 123.97 o
-2 4 -11 2164.75 2072.67 60.65 o
0 4 -11 1304.78 1212.86 47.64 o
2 4 -11 272.81 286.01 28.01 o
4 4 -11 588.45 608.13 35.73 o
6 4 -11 11685.99 11857.23 169.36 o
-10 0 -10 1807.15 1886.00 92.80 o
-8 0 -10 780.87 761.17 62.75 o
-6 0 -10 18123.70 17840.60 387.78 o
-4 0 -10 4785.03 4794.64 158.55 o
-2 0 -10 4228.46 4126.75 144.85 o
0 0 -10 8325.17 8193.25 150.45 o
2 0 -10 25062.85 25151.11 363.10 o
4 0 -10 4022.15 4064.52 96.88 o
6 0 -10 1565.32 1582.23 59.46 o
8 0 -10 53862.67 54808.05 853.89 o
10 0 -10 1176.61 1181.53 53.61 o
12 0 -10 8195.93 8209.54 157.29 o
14 0 -10 17924.91 17712.16 381.88 o
-11 1 -10 1017.11 946.76 70.94 o
-9 1 -10 284.68 306.91 43.64 o
-7 1 -10 3424.56 3257.53 88.85 o
-5 1 -10 7156.74 7025.60 115.17 o
-3 1 -10 1696.19 1696.71 50.52 o
-1 1 -10 811.02 822.52 36.85 o
1 1 -10 3904.72 4027.23 79.83 o
3 1 -10 1632.59 1662.28 49.75 o
5 1 -10 3201.02 3113.28 69.82 o
7 1 -10 5827.64 5879.41 102.61 o
9 1 -10 3534.92 3596.87 65.85 o
11 1 -10 274.09 280.28 22.67 o
13 1 -10 1554.94 1534.16 49.98 o
15 1 -10 8380.57 8368.39 133.36 o
-12 2 -10 2083.64 2099.03 106.45 o
-10 2 -10 8.03 -7.32 18.24 o
-8 2 -10 16.20 17.02 14.64 o
-6 2 -10 4072.79 4144.55 82.92 o
-4 2 -10 68.83 77.30 17.65 o
-2 2 -10 1919.04 1911.09 54.38 o
0 2 -10 886.46 852.89 49.14 o
2 2 -10 2767.21 2823.25 105.45 o
4 2 -10 4619.61 4697.34 99.48 o
6 2 -10 141.77 108.20 19.11 o
8 2 -10 8872.07 9121.20 138.19 o
10 2 -10 25.03 15.65 15.60 o
12 2 -10 2436.88 2385.73 92.82 o
14 2 -10 1994.02 2081.51 77.79 o
-11 3 -10 1250.33 1131.06 56.89 o
-9 3 -10 191.27 251.86 39.55 o
-7 3 -10 9025.39 8786.28 134.58 o
-5 3 -10 20106.87 20111.47 247.01 o
-3 3 -10 5742.83 5669.83 100.31 o
-1 3 -10 441.28 408.61 36.52 o
1 3 -10 8214.88 8339.45 129.76 o
3 3 -10 1240.30 1301.73 45.37 o
5 3 -10 8791.23 8898.69 135.20 o
7 3 -10 11473.65 11589.74 163.55 o
9 3 -10 6852.73 7094.34 120.17 o
11 3 -10 193.17 236.26 24.81 o
13 3 -10 2687.60 2882.83 81.20 o
-8 4 -10 663.28 700.06 47.19 o
-6 4 -10 1582.05 1541.05 50.51 o
-4 4 -10 3023.91 3069.76 71.09 o
-2 4 -10 3576.28 3531.52 77.17 o
0 4 -10 3801.94 3762.06 95.38 o
2 4 -10 8888.52 8931.98 136.14 o
4 4 -10 1718.61 1756.81 51.95 o
6 4 -10 1871.28 1924.13 52.98 o
8 4 -10 11471.40 11648.23 162.10 o
10 4 -10 1698.84 1719.43 49.63 o
-5 5 -10 2704.07 2682.07 67.10 o
-3 5 -10 7625.51 7685.43 123.20 o
-1 5 -10 2235.32 2239.62 58.58 o
1 5 -10 130.33 205.71 30.49 o
3 5 -10 2253.92 2260.71 72.61 o
5 5 -10 4856.26 4782.40 92.14 o
7 5 -10 5.40 32.93 25.98 o
-13 1 -9 1423.63 1533.64 95.51 o
-11 1 -9 16363.35 16516.95 354.35 o
-9 1 -9 999.29 949.40 39.90 o
-7 1 -9 8499.82 8701.06 126.43 o
-5 1 -9 8933.20 9149.15 162.73 o
-3 1 -9 8373.70 8603.80 141.99 o
-1 1 -9 363.95 364.90 27.15 o
1 1 -9 2224.41 2149.61 54.15 o
3 1 -9 54236.40 54576.09 1051.52 o
5 1 -9 1957.61 1974.57 43.65 o
7 1 -9 65.52 65.58 12.65 o
9 1 -9 4962.92 5200.66 92.34 o
11 1 -9 11921.12 11996.28 140.90 o
13 1 -9 4892.03 4962.50 78.92 o
15 1 -9 113.81 100.73 19.24 o
-14 2 -9 2885.15 2814.69 91.33 o
-12 2 -9 5528.23 5595.32 218.69 o
-10 2 -9 13467.93 13409.44 217.25 o
-8 2 -9 1828.38 1788.50 50.33 o
-6 2 -9 750.15 735.56 33.27 o
-4 2 -9 72417.05 72391.20 736.53 o
-2 2 -9 2998.44 3011.64 65.30 o
0 2 -9 3110.12 3201.51 66.64 o
2 2 -9 19066.75 19317.40 232.71 o
4 2 -9 16868.68 17282.48 213.34 o
6 2 -9 3950.24 3814.04 75.06 o
8 2 -9 1849.93 1913.26 60.54 o
10 2 -9 5236.53 5226.13 92.35 o
12 2 -9 3059.08 3073.78 68.72 o
14 2 -9 4150.60 4242.51 99.76 o
16 2 -9 6241.44 6217.34 166.78 o
-13 3 -9 1037.10 993.14 73.67 o
-11 3 -9 1793.60 1647.49 62.70 o
-9 3 -9 1816.78 1746.21 116.00 o
-7 3 -9 1479.27 1492.59 49.59 o
-5 3 -9 2215.35 2245.40 57.08 o
-3 3 -9 2432.14 2436.57 64.77 o
-1 3 -9 348.88 379.73 27.24 o
1 3 -9 483.57 495.22 29.12 o
3 3 -9 317.91 319.21 24.43 o
5 3 -9 1601.11 1623.37 47.78 o
7 3 -9 3108.43 3098.83 66.70 o
9 3 -9 391.23 439.66 29.28 o
11 3 -9 1323.89 1333.57 37.86 o
13 3 -9 3966.21 4091.18 94.93 o
15 3 -9 637.97 628.72 37.55 o
-10 4 -9 3755.74 3744.27 96.34 o
-8 4 -9 4952.89 4909.97 110.51 o
-6 4 -9 452.69 460.21 32.33 o
-4 4 -9 32485.65 32404.46 361.72 o
-2 4 -9 227.82 201.06 21.03 o
0 4 -9 4931.40 4959.75 89.81 o
2 4 -9 6212.29 6224.64 102.22 o
4 4 -9 6838.78 6724.62 107.74 o
6 4 -9 9436.42 9357.81 180.37 o
8 4 -9 1050.99 991.32 34.91 o
10 4 -9 1409.13 1581.95 296.09 o
12 4 -9 44.48 49.93 11.72 o
-9 5 -9 2745.61 2698.19 79.27 o
-7 5 -9 2724.63 2569.87 76.07 o
-5 5 -9 6252.69 6267.29 105.09 o
-3 5 -9 4622.41 4559.13 84.83 o
-1 5 -9 124.46 117.99 16.97 o
1 5 -9 404.61 413.70 25.42 o
3 5 -9 20721.76 20690.94 242.56 o
5 5 -9 1382.06 1449.49 65.52 o
7 5 -9 1456.77 1445.47 65.52 o
9 5 -9 3675.96 3586.62 104.08 o
11 5 -9 9327.57 9351.12 271.01 o
-4 6 -9 2934.80 2871.79 57.92 o
-2 6 -9 1590.58 1520.15 105.07 o
0 6 -9 558.76 596.23 53.02 o
2 6 -9 957.71 933.42 57.78 o
4 6 -9 1558.82 1618.56 72.34 o
6 6 -9 5415.29 5385.21 183.13 o
-16 0 -8 31921.66 31361.38 635.35 o
-14 0 -8 2345.31 2276.83 106.47 o
-12 0 -8 376.55 204.58 35.46 o
-10 0 -8 17092.19 16795.96 346.48 o
-8 0 -8 35221.91 36538.76 677.47 o
-6 0 -8 7197.00 7162.62 131.65 o
-4 0 -8 2829.46 2798.88 69.22 o
-2 0 -8 13237.83 13053.20 250.14 o
0 0 -8 3576.64 3526.98 139.39 o
2 0 -8 11735.71 11774.90 315.87 o
4 0 -8 26683.42 27454.42 369.84 o
6 0 -8 21033.65 21238.17 299.18 o
8 0 -8 334.95 320.84 28.75 o
10 0 -8 7274.24 7270.63 135.12 o
14 0 -8 233.74 238.86 26.80 o
16 0 -8 2940.02 3036.52 114.69 o
18 0 -8 6277.99 6351.45 180.45 o
-15 1 -8 2544.97 2459.86 120.13 o
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-11 1 -8 675.90 678.74 32.87 o
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-3 1 -8 5374.85 5248.31 86.03 o
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1 1 -8 637.37 614.58 23.34 o
3 1 -8 1587.69 1585.83 36.11 o
5 1 -8 27962.11 28602.16 272.02 o
7 1 -8 1222.75 1158.83 32.66 o
9 1 -8 2499.86 2567.48 49.45 o
11 1 -8 9352.94 9134.58 127.82 o
13 1 -8 3373.16 3344.95 59.58 o
15 1 -8 1081.76 1094.81 43.11 o
17 1 -8 1253.43 1291.80 53.61 o
-14 2 -8 169.34 189.83 34.09 o
-12 2 -8 204.24 188.76 25.98 o
-10 2 -8 3199.92 3149.10 80.13 o
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-6 2 -8 3698.21 3844.34 89.83 o
-4 2 -8 636.45 656.63 29.84 o
-2 2 -8 808.04 830.81 32.37 o
0 2 -8 298.51 328.87 22.80 o
2 2 -8 4995.06 5026.62 128.83 o
4 2 -8 1911.25 1982.42 49.76 o
6 2 -8 1825.77 1819.17 47.00 o
8 2 -8 185.52 218.79 21.65 o
10 2 -8 574.90 607.86 36.77 o
12 2 -8 11932.43 12223.86 245.81 o
14 2 -8 243.44 236.80 23.16 o
16 2 -8 1713.64 1743.98 79.15 o
-13 3 -8 563.62 555.55 35.61 o
-11 3 -8 565.73 576.15 72.29 o
-9 3 -8 17231.72 16616.52 249.64 o
-7 3 -8 2757.22 2727.02 59.79 o
-5 3 -8 2583.32 2436.09 55.51 o
-3 3 -8 11135.31 11225.71 149.15 o
-1 3 -8 28654.93 29197.85 322.52 o
1 3 -8 5699.21 5661.66 91.69 o
3 3 -8 899.96 915.97 33.65 o
5 3 -8 68467.23 68831.73 698.38 o
7 3 -8 1013.12 1002.70 34.75 o
9 3 -8 10413.83 10393.90 121.79 o
11 3 -8 18487.44 18501.60 192.12 o
13 3 -8 6005.15 6155.61 114.18 o
15 3 -8 4984.75 4837.75 95.87 o
-12 4 -8 672.89 608.35 62.74 o
-10 4 -8 2292.79 2227.44 69.41 o
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-6 4 -8 3140.52 3144.69 66.43 o
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0 4 -8 7497.29 7429.06 126.36 o
2 4 -8 5852.23 5759.41 92.59 o
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8 4 -8 794.37 791.06 27.87 o
10 4 -8 1818.52 1852.64 38.75 o
12 4 -8 14303.50 14364.34 239.48 o
14 4 -8 429.91 446.82 43.11 o
-11 5 -8 855.69 816.04 47.82 o
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-7 5 -8 880.79 860.98 42.61 o
-5 5 -8 7739.97 7867.85 118.69 o
-3 5 -8 1002.18 1015.63 35.74 o
-1 5 -8 702.82 708.76 49.64 o
1 5 -8 12709.84 12690.68 159.43 o
3 5 -8 1973.57 1942.74 70.43 o
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7 5 -8 1183.77 1176.38 56.70 o
11 5 -8 30.66 58.80 24.05 o
13 5 -8 316.40 285.21 36.65 o
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2 6 -8 5420.90 5274.24 124.66 o
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1 1 -7 26344.99 26440.30 247.46 o
3 1 -7 7081.76 6998.80 85.23 o
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11 1 -7 2111.83 2131.08 38.05 o
13 1 -7 10742.46 10762.10 110.18 o
15 1 -7 9522.45 9208.21 341.64 o
17 1 -7 163.26 191.51 24.05 o
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1 5 -7 10162.25 9759.02 172.45 o
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7 5 -7 4589.34 4637.88 106.24 o
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6 6 -7 653.34 642.15 48.11 o
10 6 -7 10317.44 10665.08 282.10 o
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