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Information card for entry 2023040
Preview
| Coordinates | 2023040.cif |
|---|---|
| Structure factors | 2023040.hkl |
| Original IUCr paper | HTML |
| Common name | Bis[1-oxopyridin-2-olato(1-)]bis(2,4,6-trimethylphenyl)silicon(IV) |
|---|---|
| Chemical name | Dimesitylbis[1-oxopyridin-2-olato(1-)]silicon(IV) |
| Formula | C28 H30 N2 O4 Si |
| Calculated formula | C28 H30 N2 O4 Si |
| Title of publication | Synthesis and crystal structures of bis-[1-oxopyridin-2-olato(1-)]bis-(penta-fluoro-phen-yl)silicon(IV)-tetra-hydro-furan-pentane (2/1/1), bis-[1-oxopyridin-2-olato(1-)]bis-(<i>p</i>-tol-yl)silicon(IV), and dimesitylbis[1-oxopyridin-2-olato(1-)]silicon(IV). |
| Authors of publication | Kraft, Bradley M.; Brennessel, William W.; Andrews, Jordan W.; Viggiani, Michael T.; Kittrell, Nathan F.; Heckman, Matthew T. |
| Journal of publication | Acta crystallographica. Section E, Crystallographic communications |
| Year of publication | 2024 |
| Journal volume | 80 |
| Journal issue | Pt 3 |
| Pages of publication | 318 - 324 |
| a | 12.571 ± 0.0002 Å |
| b | 12.68898 ± 0.00019 Å |
| c | 15.358 ± 0.0002 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2449.8 ± 0.06 Å3 |
| Cell temperature | 100 ± 0.1 K |
| Ambient diffraction temperature | 100 ± 0.1 K |
| Number of distinct elements | 5 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0342 |
| Residual factor for significantly intense reflections | 0.0316 |
| Weighted residual factors for significantly intense reflections | 0.0775 |
| Weighted residual factors for all reflections included in the refinement | 0.0787 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.045 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 291115 (current) | 2024-04-06 | cif/ Updating files of 2023038, 2023039, 2023040 Original log message: Adding full bibliography for 2023038--2023040.cif. |
2023040.cif 2023040.hkl |
| 289908 | 2024-02-21 | cif/ hkl/ Adding structures of 2023038, 2023039, 2023040 via cif-deposit CGI script. |
2023040.cif 2023040.hkl |
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Users of the data should acknowledge the original authors of the
structural data.