#------------------------------------------------------------------------------
#$Date: 2024-04-19 07:40:14 +0300 (Fri, 19 Apr 2024) $
#$Revision: 291291 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/30/2023089.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023089
loop_
_publ_author_name
'N\"ather, Christian'
'Jess, Inke'
_publ_section_title
;
 Synthesis, crystal structure and thermal properties of the dinuclear
 complex bis(\m-4-methylpyridine N-oxide-\k2
 O:O)bis[(methanol-\kO)(4-methylpyridine
 N-oxide-\kO)bis(thiocyanato-\kN)cobalt(II)]
;
_journal_coeditor_code           JP2005
_journal_issue                   5
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi               10.1107/S2056989024003128
_journal_volume                  80
_journal_year                    2024
_chemical_formula_iupac          '[Co2 (N C S)4 (C6 H7 N1 O1)4 (C1 H4 O1)2]'
_chemical_formula_moiety         'C30 H36 Co2 N8 O6 S4'
_chemical_formula_sum            'C30 H36 Co2 N8 O6 S4'
_chemical_formula_weight         850.77
_chemical_name_systematic
;Bis(\m-4-methylpyridine
<i>N</i>-oxide-\k^2^<i>O</i>:<i>O</i>)bis[(methanol-\k<i>O</i>)(4-methylpyridine <i>N</i>-oxide-\k<i>O</i>)bis(thiocyanato-\k<i>N</i>)cobalt(II)]
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_creation_method
;
Olex2 1.3-ac4
(compiled 2020.11.27 svn.r5f609507 for Rigaku Oxford Diffraction, GUI svn.r6214)
;
_cell_angle_alpha                90
_cell_angle_beta                 97.0894(11)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   11.46665(13)
_cell_length_b                   12.37103(15)
_cell_length_c                   13.58185(17)
_cell_measurement_reflns_used    9687
_cell_measurement_temperature    100.00(10)
_cell_measurement_theta_max      80.1060
_cell_measurement_theta_min      4.7590
_cell_volume                     1911.91(4)
_computing_cell_refinement
;
CrysAlisPro 1.171.42.90a (Rigaku OD, 2023)
;
_computing_data_collection
;
CrysAlisPro 1.171.42.90a (Rigaku OD, 2023)
;
_computing_data_reduction
;
CrysAlisPro 1.171.42.90a (Rigaku OD, 2023)
;
_computing_molecular_graphics
;
DIAMOND (Brandenburg & Putz, 1999) and XP in SHELXTL-PC (Sheldrick,
2008)
;
_computing_publication_material
;
Publcif (Westrip, 2010)
;
_computing_structure_refinement
;
<i>SHELXL2016/6</i> (Sheldrick, 2015b)
;
_computing_structure_solution
;
<i>SHELXT2014/5</i> (Sheldrick, 2015a)
;
_diffrn_ambient_temperature      100.00(10)
_diffrn_detector                 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.979
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB Synergy, Dualflex, HyPix'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0239
_diffrn_reflns_av_unetI/netI     0.0181
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            13370
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         80.567
_diffrn_reflns_theta_min         4.767
_diffrn_source                   'micro-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu    9.269
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.52882
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2023)
;
_exptl_crystal_colour            violet
_exptl_crystal_density_diffrn    1.478
_exptl_crystal_description       block
_exptl_crystal_F_000             876
_exptl_crystal_size_max          0.21
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.1
_refine_diff_density_max         0.666
_refine_diff_density_min         -0.570
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.087
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     231
_refine_ls_number_reflns         4111
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.087
_refine_ls_R_factor_all          0.0385
_refine_ls_R_factor_gt           0.0376
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0563P)^2^+1.4735P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1024
_refine_ls_wR_factor_ref         0.1030
_reflns_number_gt                3945
_reflns_number_total             4111
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            jp2005.cif
_cod_data_source_block           1
_cod_database_code               2023089
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
   0   0  -1 36.5097 9.31519   6
   0   0  -2 229110. 3307.24   6
   0   0  -3 105.176 28.7645   6
   0   0   3 26.7983 21.9766   9
   0   0  -4 298493. 4359.26   6
   0   0   4 310949. 4385.02   2
   0   0   4 300445. 4354.69   9
   0   0  -5 84.4491 41.0042   6
   0   0   5 82.4936 32.1377   9
   0   0   5 88.9708 98.5085   2
   0   0   6 57547.2 880.412   9
   0   0   6 70912.1 955.124   2
   0   0   7 66.9621 149.755   2
   0   0   8 540.808 90.4672  12
   0   0   8 501.073 178.857   2
   0   0   9-29.9607 105.710  12
   0   0   9 198.547 200.666   2
   0   0  10 53800.9 927.548   2
   0   0  10 53291.3 819.270  12
   0   0  11 200.681 146.256   5
   0   0  11 172.752 235.638   2
   0   0  11 81.7127 155.001  12
   0   0  12 55094.6 855.354   5
   0   0  13 153.305 202.994  37
   0   0  14 6503.29 238.532  37
   0   0  15 88.4793 163.577  37
   0   0  16 2907.13 127.419  37
   0   1   0 7.98557 13.1870   8
   0   1   1 302848. 4364.06   6
   0   1  -1 308284. 4377.85   6
   0   1   1 305087. 4370.81   2
   0  -1   1 296431. 4370.00   2
   0   1   1 305231. 4370.14  10
   0   1  -2 69989.7 1028.92   6
   0  -1   2 69282.6 1026.94   2
   0   1   2 69385.0 1027.97   2
   0   1   2 70199.5 1022.36   9
   0   1  -3 8534.46 155.287   6
   0  -1   3 8224.82 159.846   2
   0   1   3 8226.47 144.588   9
   0   1  -4 234954. 3374.25   6
   0  -1   4 237709. 3384.18   2
   0   1   4 226531. 3362.49   9
   0   1  -5 9033.86 179.370   6
   0  -1   5 9143.28 207.092   2
   0   1   5 8829.80 163.797   9
   0   1  -6 4899.43 126.231   6
   0   1   6 4823.01 109.247   9
   0  -1   7 3691.41 186.396   2
   0  -1   8 147728. 2178.86   2
   0  -1   8 142917. 2097.42  12
   0   1   8 142987. 2095.68  12
   0  -1   9 3269.39 230.218   2
   0  -1   9 3013.66 128.758  12
   0   1   9 2912.38 127.899  12
   0   1  10 12261.1 252.009  12
   0  -1  10 12609.7 255.013  12
   0  -1  11 63160.3 915.240  30
   0  -1  11 57567.5 896.362   5
   0   1  11 57622.2 898.971   5
   0   1  11 54428.5 1012.46   2
   0  -1  11 54441.8 1006.58   2
   0  -1  11 60267.8 905.280  12
   0  -1  12 16916.1 330.797   5
   0   1  12 17454.6 335.788   5
   0  -1  12 16518.4 347.221  30
   0  -1  13 2946.53 193.831  37
   0   1  13 3239.00 238.103  37
   0  -1  14 3094.97 189.033  37
   0   1  14 3629.07 233.669  37
   0  -1  15 3834.43 165.090  37
   0   1  15 4516.45 209.134  37
   0   1  16 4875.60 161.820  37
   0  -1  17 742.279 73.3682  25
   0   1  17 738.017 73.9496  25
   0   2   0 425.954 36.4285   6
   0   2   0 689.980 35.8661   8
   0   2   1 58431.5 833.994   6
   0   2  -1 57561.0 847.809   6
   0  -2   1 54175.7 826.311   2
   0   2   1 56195.1 827.668   2
   0   2   1 57200.2 831.802  10
   0   2   1 60872.1 849.311   8
   0   2  -2 245910. 3511.80   6
   0   2   2 244686. 3481.61   6
   0  -2   2 236883. 3494.62   2
   0   2   2 241366. 3496.58   2
   0   2   2 233436. 3495.60  10
   0   2   2 244122. 3503.80   9
   0   2  -3 72026.4 1074.37   6
   0  -2   3 71041.0 1063.40   2
   0   2   3 70986.1 1064.65   2
   0   2   3 71621.3 1062.69   9
   0   2  -4 99537.5 1486.05   6
   0  -2   4 101283. 1482.31   2
   0   2   4 101049. 1485.50   2
   0   2   4 97327.6 1472.28   9
   0   2  -5 3319.79 123.596   6
   0  -2   5 3548.16 134.616   2
   0   2   5 3634.97 139.535   2
   0   2   5 3084.91 98.6199   9
   0   2   5 3405.09 140.674   7
   0   2   6 682.988 131.809   2
   0  -2   6 705.788 126.378   2
   0   2  -6 706.114 92.2817   6
   0   2   7 7715.72 234.947   2
   0  -2   7 7474.21 225.722   2
   0   2   8 25634.2 497.364   2
   0  -2   8 26355.3 491.512   2
   0  -2   8 24725.7 404.144  12
   0   2   9 33560.2 646.022   2
   0  -2   9 34055.4 635.076   2
   0  -2   9 35017.9 544.620  12
   0   2  10 27112.3 571.049   2
   0  -2  10 27433.4 560.642   2
   0  -2  10 28129.3 460.083  12
   0   2  11 21112.3 408.161  34
   0   2  11 22305.3 387.886   5
   0  -2  11 21669.1 381.923   5
   0  -2  11 21082.0 408.129  30
   0  -2  11 23388.8 390.749  12
   0   2  11 22383.5 508.741   2
   0  -2  11 21798.3 494.975   2
   0   2  12 78.4150 226.102  37
   0   2  12 92.0511 178.115   5
   0  -2  12 71.3770 160.839   5
   0  -2  12 243.610 201.378  30
   0  -2  12 158.774 162.614  12
   0   2 -12 288.327 153.490  31
   0   2  13 6842.26 278.845  37
   0   2 -13 6551.94 204.057  31
   0  -2  13 7087.40 255.530  30
   0   2  14 1702.59 238.376  37
   0   2  15 2070.77 206.268  37
   0   2  16 1068.60 145.059  25
   0   2  16 882.599 146.646  37
   0  -2  17 90.1616 55.1826  25
   0   3   0 307.651 51.6659   6
   0   3   0-9.63795 46.0200   8
   0   3   1 26982.9 402.875   6
   0   3  -1 28070.0 398.507   8
   0   3   1 27780.0 417.019   8
   0   3   1 26216.0 394.515  10
   0  -3   1 24202.1 380.594   2
   0   3   1 25560.2 382.697   2
   0   3   2 101160. 1485.63  10
   0   3   2 104266. 1511.46   8
   0   3  -2 100340. 1474.30   8
   0   3  -2 104350. 1512.84   6
   0   3   2 103642. 1480.75   6
   0   3   2 102742. 1500.54   7
   0   3   2 100594. 1483.50   2
   0  -3   2 98324.7 1481.08   2
   0   3   3 62055.5 870.870   7
   0   3  -3 63727.0 884.007   6
   0   3   3 62420.6 856.441   2
   0  -3   3 61564.6 852.834   2
   0   3   3 61063.6 880.657   8
   0   3   3 60968.7 854.894  10
   0  -3   4 150233. 2198.26   2
   0   3   4 147839. 2200.59   2
   0   3  -4 150738. 2221.02   6
   0   3   5 2041.72 125.950   2
   0  -3   5 1959.18 122.558   2
   0   3  -5 1970.63 127.342   6
   0  -3   6 11338.3 255.317   2
   0   3   6 11233.7 262.175   2
   0   3  -6 10809.8 253.738   6
   0   3   7 2418.03 177.940   2
   0  -3   7 2447.36 167.187   2
   0   3  -7 2402.91 142.401   6
   0  -3   8 46029.7 759.233   2
   0   3   8 44798.9 768.449   2
   0  -3   8 43961.6 678.846  12
   0   3   9 4535.31 250.993   2
   0  -3   9 4491.72 230.521   2
   0  -3   9 4866.96 151.135  12
   0   3  10 13086.3 377.454   2
   0  -3  10 13170.1 362.023   2
   0  -3  10 13328.4 263.993  12
   0  -3  11 8275.22 216.983  24
   0  -3  11 7869.66 210.603  12
   0  -3  11 9134.92 252.666  30
   0  -3  11 7031.16 200.578   5
   0   3  11 7223.36 213.560   5
   0  -3  11 6033.68 280.290   2
   0   3  11 6278.55 302.910   2
   0   3  11 9315.40 243.834  34
   0   3  12 1998.40 249.139  37
   0  -3  12 2242.51 225.768  30
   0  -3  12 2311.90 166.547  12
   0   3 -12 2180.68 177.329  31
   0  -3  12 2053.14 169.573  24
   0   3  13 20471.8 440.299  37
   0   3 -13 19736.0 376.075  31
   0   3  14 11300.2 320.805  37
   0   3 -14 9547.37 232.644  31
   0   3  15 3654.78 231.969  37
   0   3  15 4261.32 200.559  25
   0   3  16 176.493 145.227  37
   0   4   0 144829. 2153.80   6
   0   4   0 147338. 2146.76   8
   0   4  -1 18003.6 321.312   6
   0   4   1 18816.4 309.677   6
   0   4   1 17915.1 313.686   8
   0   4   1 17346.5 290.029  10
   0   4  -1 18245.3 295.831   8
   0   4   2 706.697 81.8492   7
   0   4   2 703.828 57.4292   6
   0   4   2 724.791 55.4477  10
   0   4  -2 946.510 45.6292   8
   0   4   2 704.229 86.0981   8
   0  -4   2 607.624 47.0952   2
   0   4   2 956.436 53.8535   2
   0   4   3 296380. 4334.98   2
   0   4  -3 307273. 4375.17   6
   0   4   3 304518. 4358.91   7
   0   4   3 299991. 4338.34  10
   0  -4   3 293296. 4331.32   2
   0   4   4 114315. 1688.05   7
   0  -4   4 110314. 1658.24   2
   0   4   4 109862. 1663.60   2
   0   4  -4 116605. 1705.14   6
   0   4   5 52708.1 844.718   7
   0   4   5 52506.3 829.511   2
   0  -4   5 52229.9 821.148   2
   0   4  -5 53996.4 863.844   6
   0   4   6 167444. 2450.45   7
   0   4  -6 163515. 2450.91   6
   0  -4   6 162369. 2420.86   2
   0   4   6 159940. 2428.10   2
   0   4   7 19304.1 388.272   2
   0  -4   7 19273.9 375.548   2
   0  -4   8 5170.51 215.696   2
   0   4   8 5096.37 228.829   2
   0   4   8 4939.44 121.319  11
   0  -4   9 2095.64 200.483   2
   0   4   9 1934.65 212.959   2
   0  -4   9 2104.58 124.923  12
   0  -4  10 753.263 125.460   5
   0   4  10 879.945 133.800   5
   0  -4  10 755.289 151.876  24
   0  -4  10 993.146 143.491  19
   0  -4  10 887.459 130.481  12
   0  -4  10 781.745 191.112   2
   0   4  10 607.371 210.323   2
   0  -4  10 783.030 178.844  30
   0  -4  11 3468.39 189.592  24
   0   4  11 3252.90 236.998   2
   0  -4  11 3492.50 174.237  19
   0  -4  11 3400.83 221.420  30
   0   4  11 3479.54 208.375  34
   0  -4  11 3673.60 159.866  12
   0   4 -11 3664.70 190.921  31
   0   4 -12 6297.57 219.124  31
   0  -4  12 5690.78 198.046  19
   0  -4  12 5348.21 188.601  12
   0   4  12 6974.72 269.912  34
   0  -4  12 6564.97 263.616  30
   0  -4  12 6126.63 216.565  24
   0   4 -13 1846.64 180.947  31
   0   4  13 1468.36 261.169  37
   0  -4  13 1966.35 231.940  30
   0  -4  13 1863.37 175.067  24
   0   4  14 5117.86 214.536  25
   0   4  14 5462.69 278.468  37
   0  -4  14 5372.66 233.541  30
   0   4 -14 4952.14 185.955  31
   0   4  15 3733.17 230.101  37
   0   4  16 7869.44 178.597  37
   0   4 -16 4716.68 100.979  23
   0   5   0 84.5209 68.5594   8
   0   5   0 0.98316 88.1038   6
   0   5   1 37550.8 589.835  10
   0   5   1 38408.5 618.144   8
   0   5  -1 37786.5 597.274   8
   0   5  -1 39477.0 636.125   6
   0   5   1 39758.7 615.707   6
   0   5   2 1406.19 69.6068  10
   0   5  -2 1364.36 61.1678   8
   0   5   2 1505.77 82.4506   6
   0   5   2 1434.90 107.290   7
   0   5   3 14432.0 244.764  10
   0   5   3 12855.9 230.222   2
   0  -5   3 12627.9 226.888   2
   0   5  -3 15652.1 313.457   6
   0   5   3 14936.3 279.806   7
   0  -5   4 91635.4 1410.97   2
   0   5   4 93581.6 1417.01   2
   0   5  -4 101133. 1482.41   6
   0   5   4 99913.5 1456.54   7
   0   5   5 131024. 1954.02   7
   0   5   5 127444. 1921.80   2
   0  -5   5 128403. 1914.91   2
   0   5  -5 130790. 1974.01   6
   0   5   6 28461.8 520.425   7
   0   5  -6 27069.0 525.849   6
   0  -5   6 27555.3 477.727   2
   0   5   6 27244.0 487.957   2
   0   5  -7 37216.1 674.959   6
   0   5   7 36599.3 562.024  11
   0  -5   7 37172.2 626.325   2
   0   5   7 36892.8 637.281   2
   0  -5   8 6949.23 234.203   2
   0   5   8 7186.71 255.101   2
   0  -5   9 28463.4 441.996  12
   0   5   9 23631.5 518.840   2
   0   5  10 1917.98 204.867   2
   0  -5  10 2297.05 182.468  24
   0  -5  10 2380.69 168.125  19
   0  -5  10 2250.91 200.410  30
   0   5 -10 2609.15 179.717  31
   0  -5  10 2581.47 134.879  12
   0   5  10 2485.49 217.922  37
   0   5  10 2354.06 183.176  34
   0   5  11 14785.2 360.663  37
   0  -5  11 14891.4 306.060  19
   0  -5  11 14622.7 319.699  24
   0   5 -11 15121.7 321.107  31
   0  -5  11 14314.8 279.694  12
   0  -5  11 15051.9 336.844  30
   0   5  12 2998.20 267.653  37
   0  -5  12 3437.85 184.739  19
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   2  12   3 2381.55 157.928  14
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   2 -12   5 34.8743 141.828  19
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   2 -12   6 3341.77 163.703  19
   2 -12   7 19288.4 340.658  19
   2 -12   8 339.577 129.928  19
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   2  13  -5 1890.20 135.927  27
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   2 -13   6 11612.9 211.138  19
   2 -13   7 1869.15 96.8140  19
   2 -13   8 1463.35 78.1584  19
   2  14  -7 1848.60 59.2147  14
   2  14  -6 115.197 63.8365  14
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   2  14  -5 6432.58 139.933  27
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   2  14   2 164.625 96.2532  14
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   2  14   3 7750.92 190.884  27
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   2 -14   5 304.905 65.6267  17
   2 -14   6 1261.56 62.1224  17
   2  15  -5 449.790 31.0803  14
   2  15  -3 58.0348 54.3814  27
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   2  15  -2 5208.86 102.917  14
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   2  15  -1 3344.90 97.7038  27
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   2  15   0 6739.77 140.786  27
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  -3   0   8 101.041 179.035   2
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  -3   0   2 161.920 57.7795  10
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   3   0   0 60.4963 72.0402   1
   3   0   1 143715. 2124.01   1
   3   0   2 59.2195 91.0234   1
   3   0   3 5263.38 171.812   1
   3   0   4 185.450 131.725   1
   3   0   5 520796. 7641.87   8
   3   0   5 535764. 7671.05   2
   3   0   6 63.3374 77.9859   8
   3   0   6 37.6084 170.363   2
   3   0   7 120063. 1857.54   9
   3   0   7 124813. 1886.25   2
   3   0   8-49.8198 195.603   2
   3   0   9 10595.2 241.243  12
   3   0   9 11181.2 338.600   2
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   3   0  10 69.7715 153.969  37
   3   0  11 76556.9 1172.23  37
   3   0  12-56.9091 189.026  37
   3   0  13 2004.63 189.745  37
   3   0  14 127.744 148.664  37
   3   0  15 4776.53 178.177  25
   3   0  16 25.9729 83.0931  25
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   3   1 -15 17560.1 317.061  31
  -3  -1  14 46.0277 164.173   5
  -3  -1  13 20326.8 368.076   5
  -3   1  13 20662.9 372.560   5
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  -3  -1   7 1020.20 161.629   2
  -3  -1   6 197384. 2922.41   2
  -3   1   6 197053. 2915.55   7
  -3   1   5 30791.3 514.486   7
  -3   1   5 30673.6 531.162  10
  -3   1   4 568.520 92.2856  10
   3   1  -4 519.490 34.0746   9
  -3   1   4 606.160 74.0230   7
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   3  -1   0 437609. 6229.78   1
   3   1   0 421532. 6231.34   1
   3  -1   1 98340.6 1423.94   1
   3   1   1 91730.3 1423.82   1
   3  -1   2 34058.2 533.183   1
   3   1   2 30720.6 531.111   1
   3   1   3 253898. 3921.94   1
   3  -1   3 282137. 3926.85   1
   3  -1   4 128641. 1844.47   1
   3   1   4 115854. 1838.50   1
   3  -1   5 41272.9 654.362   2
   3   1   5 39285.1 642.555   9
   3   1   5 39673.8 632.620   8
   3  -1   6 34378.7 601.073   2
   3   1   6 32876.8 571.198   8
   3   1   6 34316.9 586.919   9
   3  -1   7 47082.3 791.705   2
   3   1   7 45099.1 763.454   9
   3  -1   8 23788.3 481.220   2
   3   1   8 22768.7 378.861  12
   3   1   9 21272.3 373.248  12
   3  -1  10 16175.8 331.792  12
   3   1  10 16183.9 325.358  12
   3   1  10 17279.8 340.744  37
   3  -1  10 17615.0 352.897  30
   3  -1  11 7045.15 233.327  12
   3   1  11 6856.27 221.147  12
   3  -1  11 6370.36 261.327  30
   3   1  12 877.438 186.414  12
   3  -1  12 725.788 199.431  12
   3   1  12 856.177 208.194  37
   3  -1  13 15923.7 318.436  12
   3   1  13 14310.1 332.475  37
   3   1  14 1824.12 179.119  37
   3   1  14 2063.90 202.314  29
   3   1  14 2229.00 204.502  25
   3   1  15 606.934 120.389  37
   3  -1  15 835.779 152.775  29
   3  -1  15 828.279 139.755  25
   3   1  15 956.938 154.618  25
   3   1  16 3143.21 107.338  25
   3  -1  16 2667.79 91.4673  25
  -3   2  17 236.260 73.2403  37
   3   2 -16 628.641 90.9252  31
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   3   2 -15 535.906 143.332  31
  -3   2  15 892.077 230.405  37
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  -3  -2  14 23128.6 407.121   5
  -3   2  14 24544.5 419.912   5
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  -3  -2  12 1386.99 153.988   5
  -3   2  12 1533.28 169.315   5
  -3  -2  12 1381.75 142.356  15
  -3   2  12 1767.37 177.880  34
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  -3  -2  11 13997.4 271.417  15
  -3  -2  11 14106.1 271.730   5
  -3   2  11 14315.9 279.009   5
  -3  -2  11 14302.0 380.108   2
  -3   2  11 14495.2 392.351   2
  -3   2  11 13704.3 291.840  34
  -3  -2  10 1093.09 202.684   2
  -3   2  10 1012.41 216.891   2
  -3   2   9 63354.0 1052.58   2
  -3  -2   9 63453.5 1036.85   2
  -3   2   8 80219.8 1294.17   2
  -3  -2   8 82193.8 1282.84   2
  -3   2   7 1457.67 165.847   2
  -3  -2   7 1238.63 154.476   2
  -3   2   7 978.986 145.216   7
  -3   2   6 19983.3 394.364   2
  -3  -2   6 20420.0 384.813   2
  -3   2   6 19780.8 379.090   7
  -3  -2   5 78190.4 1183.33   2
  -3   2   5 77099.9 1190.45   2
  -3   2   5 76454.5 1184.95   7
   3   2  -4 135306. 2005.52   9
  -3   2   4 145086. 2048.05   7
   3   2  -3 14416.4 243.618   9
  -3   2   3 14507.3 276.204  10
  -3   2   2 2080.53 98.3389  10
   3   2  -2 2017.37 76.1837   9
   3   2  -1 8164.30 166.092   9
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   3   2   0 52525.6 817.638   1
   3  -2   0 53471.5 811.784   1
   3   2   0 53032.1 817.975   9
  -3  -2   0 52685.4 776.315  10
   3  -2   1 3096.64 114.813   1
   3   2   1 3085.34 122.212   1
   3  -2   2 24331.7 405.790   1
   3   2   2 22690.6 407.585   1
   3  -2   3 352546. 5036.00   1
   3   2   3 339222. 5038.67   1
   3   2   3 343507. 5041.56   9
   3   2   4 7472.33 205.709   1
   3  -2   4 7648.37 202.943   1
   3   2   4 7501.47 196.445   9
   3   2   5 354.764 122.297   8
   3   2   5 287.441 107.026   9
   3   2   6 48169.1 804.102   8
   3   2   6 49028.8 802.163   9
   3   2   7 92528.7 1388.00   2
   3   2   7 88267.1 1363.86   9
   3   2   7 88424.5 1289.45  12
   3   2   8 7067.33 226.787   9
   3   2   8 7494.43 175.306  12
   3   2   9 6821.06 184.394  12
   3   2  10 927.886 187.605  37
   3  -2  10 943.551 206.277  30
   3  -2  10 462.054 171.531  12
   3   2  10 594.173 151.661  12
   3   2  11 485.724 216.917  37
   3  -2  11 330.123 228.108  30
   3  -2  11 460.744 181.204  12
   3   2  11 466.220 167.704  12
   3   2  12 18710.9 392.138  29
   3  -2  12 18084.2 358.440  12
   3  -2  12 18444.6 399.289  30
   3   2  13 179.276 216.828  37
   3   2  13 299.224 219.512  25
   3  -2  13 64.5829 166.438  12
   3   2  13 77.4343 209.095  29
   3   2  14 922.976 192.147  37
   3   2  14 1076.60 214.834  25
   3  -2  15 3009.99 135.217  25
   3   2  15 3327.38 172.116  25
   3   2  16 739.289 83.2464  25
  -3   3  16 888.423 162.317  37
   3   3 -16 616.130 93.1658  31
  -3   3  15 15009.8 345.213  37
   3   3 -15 13410.8 274.447  31
  -3  -3  14 381.731 147.765   5
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   3 -12   5 21135.3 365.599  19
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   3 -12   8 673.055 119.599  19
   3 -12   9 771.533 96.7163  19
   3 -12  10 2193.24 69.8430  19
   3  13  -8 595.233 73.8307  27
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   3  13  -7 585.376 97.8935  27
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   3  13  -4 204.275 143.369  27
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   4   0  -1 132.332 101.876   1
   4   0   0 206951. 3046.18   1
   4   0   1 89.0337 105.739   1
   4   0   2 34382.0 576.198   1
   4   0   3 22.6227 141.014   1
   4   0   4 101856. 1566.80   1
   4   0   5 33.7081 90.7853   8
   4   0   5-10.5642 159.638   1
   4   0   6 1469.53 103.087   3
   4   0   6 988.477 103.510   8
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   4   0   8 46846.7 807.625   9
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   4   0  10 62229.5 926.838  12
   4   0  10 56821.9 925.679  37
   4   0  11 46.7998 182.879  12
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   4  -1  -1 18624.1 335.079   1
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   4   1   0 243.320 109.450   1
   4  -1   1 55383.5 843.998   1
   4   1   1 51422.6 844.451   1
   4  -1   2 147551. 2112.46   1
   4   1   2 135411. 2112.67   1
   4   1   3 41223.8 717.765   1
   4  -1   3 45568.8 720.850   1
   4   1   4 88.1316 151.422   1
   4  -1   4 156.824 147.752   1
   4  -1   5 42661.9 690.279   8
   4   1   5 45733.6 732.068   8
   4  -1   5 46400.2 753.791   1
   4   1   5 43337.5 750.820   1
   4   1   6 457.652 98.3290   3
   4  -1   6 547.450 99.8422   3
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   4   1   7 174.362 147.541   9
   4   1   7 306.048 112.748   8
   4   1   8 54531.7 839.472  12
   4   1   8 55845.6 929.718   9
   4   1   9 11606.9 265.279  12
   4  -1   9 14324.5 302.788  30
   4  -1  10 41801.4 669.318  30
   4   1  10 40384.2 658.396  37
   4   1  11 4235.64 229.592  37
   4   1  11 4534.66 201.871  12
   4   1  12 9000.99 270.138  37
   4   1  12 9085.48 242.915  12
   4   1  13 1392.98 189.661  37
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   4   2   0 88654.0 1372.15   1
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   4  -2   1 2823.18 134.421   1
   4  -2   2 17296.4 326.406   1
   4   2   2 16202.8 333.387   1
   4   2   3 288584. 4260.84   9
   4   2   3 280907. 4255.41   1
   4   2   4 24552.4 468.530   9
   4   2   4 23874.9 470.761   1
   4   2   5 43654.0 746.940   9
   4   2   5 44016.8 744.975   8
   4   2   6 603.045 138.833   9
   4   2   6 750.027 145.372   8
   4  -2   6 851.180 96.2784   3
   4   2   6 813.564 102.742   3
   4   2   7 27829.6 442.287  12
   4   2   7 27396.6 520.116   8
   4   2   7 28762.8 542.044   9
   4   2   8 3469.48 145.841  12
   4   2   8 3764.67 202.983   9
   4   2   9 10073.1 229.282  12
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   4   2   9 9968.38 270.782  37
   4  -2  10 4522.34 250.963  30
   4   2  10 4478.98 233.699  37
   4   2  10 4207.23 201.103  35
   4  -2  11 12670.0 331.901  30
   4   2  11 11570.6 305.326  25
   4   2  11 10934.8 265.642  12
   4  -2  11 11149.8 287.661  12
   4   2  11 11856.8 285.268  35
   4   2  11 12288.3 317.602  37
   4  -2  12 1305.09 183.617  12
   4   2  12 956.078 221.915  37
   4   2  12 1394.52 226.723  25
   4   2  12 1218.26 234.887  29
   4  -2  13 1144.94 154.384  12
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   4   2  13 1433.06 219.674  25
   4   2  13 1349.78 213.740  29
   4   2  14 10461.3 259.506  37
   4   2  14 13300.0 275.559  25
   4  -2  14 10994.9 239.655  25
   4   2  14 12456.5 266.954  29
   4   2  15 1313.67 121.775  25
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   4   3  -4 21565.6 362.805   9
   4   3  -3 133497. 1977.67   9
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   4  -3  -1 49451.6 794.193   1
   4   3  -1 50547.3 806.961   1
   4  -3   0 34234.1 560.314   1
   4   3   0 33775.2 573.145   1
   4   3   0 34009.8 570.491   9
   4  -3   1 94540.3 1427.85   1
   4   3   1 89125.3 1435.67   1
   4  -3   2 17489.6 330.884   1
   4   3   2 17096.5 343.344   1
   4   3   2 16945.1 348.747   9
   4  -3   3 21826.7 399.224   1
   4   3   3 20494.7 405.224   1
   4  -3   4 1081.88 144.403   1
   4   3   4 1220.46 156.279   1
   4   3   4 1169.70 142.785   9
   4   3   5 8920.33 265.617   8
   4   3   5 8339.08 247.338   9
   4   3   6 71214.6 1172.41   9
   4   3   6 76949.3 1195.16   8
   4  -3   6 76466.3 1077.53   3
   4   3   6 71713.6 1078.74   3
   4   3   6 69186.2 1069.20  12
   4   3   7 12082.7 226.200  12
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   4   3   7 13197.4 336.840   8
   4   3   7 12600.8 327.769   9
   4   3   8 9770.10 206.376  12
   4   3   8 9603.92 300.261   9
   4  -3   9 11812.6 266.190  19
   4   3   9 12238.6 287.259  25
   4   3   9 12573.1 290.007  29
   4   3   9 13136.9 282.309  35
   4   3   9 13693.3 307.584  37
   4  -3  10 312.723 189.327  32
  -4   3 -10 8.10518 128.380  23
   4  -3  10 198.088 159.760  19
   4   3  10 289.322 199.908  25
   4  -3  10 13.6953 233.276  30
   4   3  10 271.506 196.333  29
   4   3  10 152.056 140.162  12
   4   3  10 300.622 222.597  37
   4   3  10 19.7194 166.880  35
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   4  -3  11 738.656 158.770  19
   4  -3  11 756.242 255.233  30
   4   3  11 843.990 226.901  29
   4  -3  11 835.858 183.753  12
   4   3  11 547.987 197.685  36
   4   3  11 490.884 242.057  37
   4   3  11 710.178 224.645  25
   4   3  12 17480.5 366.453  25
   4   3  12 16761.2 356.477  29
   4  -3  12 15004.4 312.659  12
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   4   3  12 16328.0 369.233  37
   4   3  13 8490.37 253.311  29
   4   3  13 8454.25 266.150  25
   4   3  13 8310.64 268.338  37
   4   3  14 558.296 169.914  37
   4   3  14 595.029 176.221  25
   4  -3  14 443.240 108.889  25
   4   3  15 5404.17 145.319  25
   4  -3  15 4996.62 145.489  29
   4   4 -16 970.986 86.6727  31
   4   4 -15 13460.0 266.896  31
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  -4  -4  13 4441.40 189.584  24
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  -4   4  12 5348.58 191.316   5
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  -4   4  11 28579.1 487.364  34
  -4  -4  11 27131.7 448.041   5
  -4   4  11 26995.8 460.283   5
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  -4   4  10 9699.87 219.701   5
  -4   4  10 9538.08 327.287   2
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  -4  -4   9 1088.55 177.540   2
  -4   4   9 1158.94 199.640   2
  -4  -4   8 4562.32 206.285   2
  -4   4   8 4354.56 231.722   2
  -4   4   8 4936.21 241.967   7
  -4   4   7 32614.5 600.256   7
  -4  -4   7 32822.4 568.920   2
  -4   4   7 32983.0 613.621  10
  -4   4   6 17695.3 387.555   7
  -4   4   6 17056.6 392.160  10
  -4   4   6 17633.6 379.405   2
  -4   4   5 106929. 1682.21   2
  -4   4   5 109059. 1701.86  10
  -4   4   5 109953. 1699.24   7
  -4   4   4 41606.1 705.562  10
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   4   4  -2 30557.9 531.995   1
   4  -4  -2 31223.5 520.760   1
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   4  -4  -1 7179.22 179.836   1
   4   4  -1 6971.03 195.448   1
   4  -4   0 74814.5 1157.36   1
   4   4   0 75281.3 1172.33   1
   4   4   1 243176. 3481.85   9
   4  -4   1 238070. 3446.82   1
   4   4   2 6293.79 204.732   9
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   4   4   2 6760.94 196.863   1
   4  -4   3 587.621 123.867   1
   4   4   3 557.802 135.207   1
   4   4   4 38199.8 682.231   8
   4   4   4 36875.6 658.853   9
   4   4   5 54111.4 925.641   9
   4   4   5 53275.6 826.547   3
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   4   4   6 10616.1 303.637   9
   4   4   6 10934.4 331.053   8
   4   4   7 46618.5 716.010  12
   4   4   7 48672.1 839.189   9
   4   4   7 48562.4 857.952   8
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   4   4   9 8249.98 236.939  36
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   4   4   9 8279.70 256.911  29
   4  -4   9 8824.32 277.111  30
   4   4  10 13717.0 309.766  36
   4   4  10 13771.7 305.941  35
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   4   4  12 4040.47 271.541  37
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   4   4  12 4303.30 227.089  29
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   4   5 -14 2606.89 192.513  31
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   4   5  -3 16317.5 323.622   1
   4  -5  -3 16527.4 310.992   1
   4   5  -3 16545.7 319.284   9
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   4  -5  -2 574.652 97.3873   1
   4   5  -2 621.190 112.323   1
   4   5  -2 588.596 117.368   9
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   4  -5  -1 89951.3 1366.77   1
   4   5  -1 88614.9 1377.46   1
   4  -5   0 758.081 92.5046   1
   4   5   0 869.369 102.592   1
   4   5   0 878.421 137.036   9
   4  -5   1 9280.86 207.785   1
   4   5   1 9003.55 210.969   1
   4   5   1 9609.62 250.240   9
   4  -5   2 64071.1 977.140   1
   4   5   2 62464.2 980.282   1
   4   5   2 62703.1 1023.04   9
   4  -5   3 47476.2 759.151   1
   4   5   4 610.848 164.327   9
   4   5   5 47179.8 854.702   9
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   4   5   6 8464.29 281.572   9
   4   5   6 8327.54 322.618   8
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   4   5   7 6833.92 283.579   9
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   4   5   8 11136.9 271.256  29
   4   5   8 11460.7 270.747  25
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   4  -5   8 12171.5 272.102  19
   4  -5   8 11240.2 289.251  30
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   4   5   8 10856.8 260.655  35
   4   5   8 10429.1 253.390  36
   4   5   8 10616.5 325.125   9
  -4   5  -9 42933.2 678.561  23
   4  -5   9 42769.7 690.283  19
   4   5   9 42259.5 702.243  25
   4   5   9 43406.9 700.622  29
   4  -5   9 42407.7 710.409  30
   4   5   9 42120.9 691.906  35
   4  -5  10 188.741 187.246  19
   4   5  10 80.6710 210.942  25
   4   5  10-13.5888 202.370  29
   4  -5  10 216.334 241.933  30
   4   5  10-62.7768 167.672  35
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   4  -5  11 26268.6 464.120  19
   4   5  11 27949.5 495.585  25
   4   5  11 28041.5 525.240  37
   4   5  11 27045.1 482.703  29
   4  -5  11 26448.4 454.155  12
   4  -5  12 8873.78 211.730  12
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   4   5  12 10051.6 277.702  25
   4   5  12 9695.78 254.133  29
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   4  -5  13 441.452 106.495  12
   4   5  13 558.549 173.989  25
   4   5  13 507.182 218.754  37
   4   5  14 3626.53 141.081  25
   4   5  14 3435.81 170.132  37
   4   6 -15 1176.05 115.681  31
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   4   6 -14 87.5031 161.575  31
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  -4   6   2 233449. 3326.48  10
  -4   6   2 219494. 3225.42  11
  -4   6   1 20935.7 425.053  10
   4   6  -1 20825.9 399.787   9
   4   6   0 64446.1 1044.15   9
   4   6   1 50007.4 813.144   9
  -4   6  -1 46674.0 712.113  13
   4   6   2 5022.30 239.867   8
   4   6   2 5528.03 223.316   9
   4   6   3 1466.12 196.039   8
   4   6   4 62918.0 1055.73   9
  -4   6  -4 62777.4 1074.44   6
   4   6   5 1819.16 202.661   9
   4   6   5 2095.16 247.524   8
  -4   6  -5 1930.04 231.873   6
   4   6   6 16738.7 452.459   8
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   4   6   7 1944.49 144.629  26
   4   6   7 1751.40 174.913  25
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   4   6   7 1626.05 140.071  22
   4   6   7 1681.98 204.201  37
   4   6   7 1749.16 153.155  36
   4   6   7 1683.25 158.805  35
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   4   6   7 1497.75 207.682   9
   4   6   7 1741.79 178.556  29
   4  -6   7 1609.84 190.370  30
   4   6   8 3422.38 163.550  26
   4   6   8 3277.80 201.510  25
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   4  -6   8 3607.32 207.219  19
   4   6   8 3234.45 199.814  29
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   4  -6   8 3320.28 226.623  30
   4   6   8 3532.27 234.221  37
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   4  -6   9 2239.49 204.567  19
   4   6   9 1937.20 208.606  25
   4   6   9 1926.62 198.891  29
   4  -6   9 1726.61 238.656  30
   4   6   9 1987.63 246.523  37
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   4  -6  10 12385.4 302.041  19
   4   6  10 12936.2 312.632  25
   4   6  10 13317.4 302.794  29
   4  -6  10 13208.7 340.225  30
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   4  -6  11 1959.09 184.637  19
   4   6  11 2052.08 186.279  29
   4  -6  11 2009.41 254.612  30
   4   6  11 2132.83 210.525  25
   4  -6  11 1747.55 142.209  12
   4   6  12 2991.04 198.341  25
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   4  -6  12 3188.44 130.360  12
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   4  -6  13 4480.13 120.840  12
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   4   6  14 11305.3 169.458  25
   4   7 -15 1968.00 87.9724  31
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   4   7 -12 1075.45 206.294  31
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   4   7   0 62127.8 1051.80   8
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   4   7   1 18395.3 412.591   8
   4   7   1 19383.0 410.725   9
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   4   7   2 5712.61 260.474   8
   4   7   2 5623.66 242.186   9
   4   7   3 1511.71 238.188   8
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   4   7   4 1699.31 209.159   9
   4   7   4 1649.54 238.656   8
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   4   7   5 1190.15 206.614   9
   4   7   6 95183.9 1424.23  21
   4   7   6 97554.9 1431.17  22
   4  -7   6 95493.7 1428.34  19
   4   7   6 94457.6 1409.74  18
   4   7   6 91132.7 1414.34  27
   4   7   6 95497.7 1423.63  29
   4  -7   6 90208.0 1422.98  30
   4   7   6 95560.2 1423.61  25
   4   7   6 97320.9 1426.46  26
   4   7   6 94190.2 1438.79  37
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   4   7   7 6088.64 198.526  22
   4   7   7 5944.03 181.004  21
   4  -7   7 5839.43 228.974  19
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   4   7   7 7612.86 255.062  37
   4   7   7 6513.12 217.815  25
   4   7   7 6682.41 205.081  26
   4   7   7 6681.48 214.021  29
   4   7   7 6257.79 180.141  27
   4  -7   7 6824.54 238.039  30
   4   7   8 980.790 153.799  26
   4   7   8 683.021 184.025  25
   4   7   8 778.802 176.622  29
   4  -7   8 898.013 220.286  30
   4   7   8 828.166 230.521  37
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   4   7   8 615.652 140.182  22
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   4  -7   9 40863.5 657.539  19
   4   7   9 39493.6 652.760  25
   4   7   9 38327.8 643.482  29
   4  -7   9 38722.5 668.643  30
   4   7   9 38545.7 680.228  37
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   4  -7  10 24063.0 426.177  19
   4   7  10 23343.0 423.791  25
   4  -7  10 22714.8 449.436  30
   4   7  10 22668.4 462.923  37
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   4  -7  11 9205.57 242.347  19
   4   7  11 9896.25 248.326  25
   4  -7  11 9602.65 293.430  30
   4   7  11 10239.4 306.744  37
   4  -7  12 26846.0 433.380  19
   4   7  12 26780.0 439.735  25
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   4   8 -14 797.097 100.381  31
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   4   8 -13 1244.46 153.090  31
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   4   8 -12 1669.76 184.565  31
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   4   8 -11 10657.7 278.297  31
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   4   8 -10 623.741 195.583  31
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   4   8  -9 6659.29 227.617  31
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   4   8  -8 269.377 171.708  31
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  -4   8   8 323.458 178.669  28
  -4   8   7 1649.28 256.969   7
  -4   8   7 1912.40 156.161  13
  -4  -8   7 1618.84 143.460  15
  -4   8   7 1618.81 176.337  28
  -4   8   6 177.159 190.397  10
  -4   8   6 140.896 229.109   7
  -4   8   6 263.627 140.762  13
  -4  -8   6 221.213 120.249  15
  -4   8   6 264.379 152.079  28
  -4   8   5 34480.3 696.773   7
  -4   8   5 34334.9 571.790  28
  -4   8   5 33642.2 668.185  10
  -4   8   5 35205.9 561.296  11
  -4   8   4 9937.96 316.075  10
  -4   8   3 3139.45 222.415  10
  -4   8   3 3083.72 154.945  13
  -4   8   2 416.651 193.513  10
   4   8  -2 282.176 137.521   8
  -4   8   2 324.053 130.175  13
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  -4   8   1 806.850 199.043  10
   4   8  -1 462.967 151.800   8
  -4   8   1 505.054 125.778  13
  -4   8   1 625.642 188.848   6
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   4   8   0 4401.03 226.307   8
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  -4   8   0 4615.79 250.940   6
   4   8   1 61366.4 1045.37   8
  -4   8  -1 59824.8 918.169  13
   4   8   2 448.981 205.448   8
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   4   8   3 4952.45 278.417   8
   4   8   4 1357.36 160.572  33
   4   8   4 1387.25 148.491  29
   4   8   4 1083.52 140.381  26
   4   8   4 1098.83 144.431  27
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   4   8   4 1287.56 148.284  22
   4  -8   4 1236.92 163.801  19
   4   8   4 1186.13 157.772  21
   4   8   4 1045.87 233.633   8
   4   8   4 1201.91 122.542  16
   4   8   5 11096.3 252.088  29
   4   8   5 10842.2 243.862  27
   4   8   5 11814.3 257.521  26
   4   8   5 10454.9 241.364  25
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   4   8   5 11066.4 266.294  21
   4   8   5 11280.7 258.010  22
   4  -8   5 10585.9 269.392  19
   4   8   5 11729.1 263.031  33
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   4   8   5 11736.8 272.347  37
   4  -8   6 9364.55 262.824  19
   4   8   6 9095.21 233.138  25
   4   8   6 9758.77 241.169  26
   4   8   6 8967.48 227.220  27
   4  -8   6 9104.01 252.252  30
   4   8   6 9516.86 247.899  29
   4   8   6 9508.26 266.793  37
   4   8   6 9232.51 236.214  21
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  -5   0   4 77.3331 111.708  10
  -5   0   4 20.2017 66.0347   7
  -5   0   3 48406.5 755.465  10
  -5   0   3 46673.1 719.365   7
  -5   0   2 241.930 89.8602  10
   5   0  -1 131924. 2003.96   1
  -5   0   1 134708. 1985.11  10
   5   0   0 4.90908 136.743   1
   5   0   1 27633.4 496.910   1
   5   0   2 57.5537 141.435   1
   5   0   3 79331.7 1253.92   1
   5   0   4 19.0847 169.461   1
   5   0   5 41045.8 732.178   1
   5   0   5 41772.1 635.820   3
   5   0   6 7.36209 109.933   3
   5   0   7 344.932 131.879   3
   5   0   7 353.900 182.178   9
   5   0   8-117.049 167.700   9
   5   0   9 28361.4 496.726  37
   5   0   9 29851.1 508.139  32
   5   0  10-8.80989 175.039  37
   5   0  10 117.526 174.723  12
   5   0  11 1125.40 199.491  25
   5   0  11 943.616 182.036  37
   5   0  11 857.896 183.296  12
   5   0  12 196.414 189.273  25
   5   0  12-18.3888 163.185  37
   5   0  12-105.240 158.833  12
   5   0  13 5679.26 251.956  29
   5   0  13 5309.56 204.250  25
   5   0  14 63.9062 158.731  29
   5   0  14-125.894 128.438  25
   5   0  15 14253.9 213.720  29
   5   0  15 10504.8 195.822  25
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   5   1 -16 3203.62 106.181  31
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   5   1  -1 1678.43 147.694   1
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   5  -1   0 126927. 1870.58   1
   5   1   0 122641. 1873.53   1
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   5  -1   1 64629.8 998.751   1
   5   1   1 60982.8 1000.84   1
   5   1   2 48156.4 808.700   1
   5  -1   2 50639.4 805.870   1
   5  -1   3 564.304 162.595   1
   5   1   3 546.634 163.645   1
   5  -1   4 52568.5 857.581   1
   5   1   4 49875.5 859.193   1
   5   1   5 3768.60 223.574   1
   5  -1   5 3946.71 216.132   1
   5   1   5 3928.60 125.933   3
   5  -1   5 4201.90 122.580   3
   5  -1   6 10570.2 210.641   3
   5   1   6 10013.3 212.278   3
   5   1   6 9795.49 311.627   9
   5   1   6 9713.84 269.786   8
   5   1   7 36603.3 591.693   3
   5   1   7 35660.3 695.935   9
   5   1   8 21445.7 479.993   9
   5   1   9 8537.83 246.585  37
   5  -1   9 8963.79 255.118  32
   5   1   9 8075.64 241.250  25
   5   1  10 4426.52 222.307  37
   5  -1  10 4313.40 214.723  32
   5   1  10 4080.05 219.047  25
   5  -1  10 3799.74 207.352  12
   5   1  10 3792.91 188.379  12
   5   1  11 1052.44 209.853  25
   5  -1  11 975.580 183.163  25
   5   1  11 1325.07 206.384  37
   5   1  11 982.527 207.612  35
   5  -1  11 1100.51 187.168  12
   5   1  11 1093.32 167.289  12
   5   1  12 1181.71 193.535  37
   5   1  12 1456.96 160.880  12
   5  -1  12 1571.99 176.537  12
   5  -1  12 1267.03 181.477  25
   5   1  12 1285.94 204.556  25
   5   1  12 1332.48 239.424  29
   5   1  13 1341.51 161.119  37
   5  -1  13 1746.59 145.920  12
   5   1  13 2033.99 213.479  29
   5  -1  13 1520.12 159.450  25
   5   1  13 1811.04 181.473  25
   5   1  14 24930.1 412.264  29
   5  -1  14 25185.1 412.725  29
   5   1  14 24094.4 396.130  25
   5  -1  15 53.4371 84.2961  29
   5   1  15 137.499 71.9048  25
  -5  -2  16 2094.49 88.6540  37
   5   2 -16 2725.00 102.740  31
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  -5   2  15 2742.53 150.878   5
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  -5  -2  12 4570.22 169.896  15
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  -5   2  11 17929.4 327.875   5
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  -5  -2  10 21383.1 354.855  15
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  -5  -2  10 20154.8 452.978   2
  -5  -2  10 19541.2 347.422   5
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  -5  -2   9 323.966 204.517   2
  -5   2   9 244.363 222.480   2
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  -5   2   8 69566.4 1163.17   2
  -5   2   7 1292.84 186.013  10
  -5   2   7 1480.68 153.623   7
  -5   2   7 1314.53 200.576   2
  -5  -2   7 1481.22 182.115   2
  -5   2   6 58725.1 975.807  10
  -5   2   6 59793.1 968.667   2
  -5  -2   6 60529.5 955.764   2
  -5   2   6 57541.0 942.938   7
  -5   2   5 5749.01 180.514   7
  -5   2   5 6078.10 217.315  10
  -5   2   4 32868.0 539.843   7
  -5   2   4 32936.7 563.730  10
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   5   2  -3 593.721 92.4523   9
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   5   2  -2 66189.4 1031.50   1
   5  -2  -2 65340.2 1020.34   1
  -5  -2   2 65899.1 987.173  10
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   5   2  -2 62893.5 1013.52   9
   5  -2  -1 15193.6 307.814   1
   5   2  -1 14825.3 320.181   1
  -5  -2   1 15219.5 262.847  10
   5  -2   0 138360. 2040.21   1
   5   2   0 141529. 2055.77   1
   5  -2   1 815.168 139.529   1
   5   2   1 874.726 154.759   1
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   5  -2   2 9342.05 241.623   1
   5   2   2 8942.39 253.442   1
   5  -2   3 8431.41 241.958   1
   5   2   3 7503.61 250.615   1
   5  -2   4 62250.1 978.889   1
   5   2   4 58374.0 985.097   1
   5   2   4 57027.7 895.270   3
   5  -2   4 61703.6 893.788   3
   5   2   4 64887.4 1005.57   9
   5   2   5 1154.84 187.518   1
   5  -2   5 1150.72 177.684   1
   5   2   5 1478.57 178.228   9
   5   2   5 1146.43 156.625   8
   5  -2   5 1318.32 96.0336   3
   5   2   5 1224.76 101.418   3
   5   2   6 105080. 1614.86   8
   5   2   6 100181. 1622.40   9
   5  -2   6 106053. 1510.36   3
   5   2   6 97894.8 1511.33   3
   5   2   7 74.7965 106.869  12
   5  -2   7 62.7129 127.927   3
   5   2   7 38.8577 179.622   9
   5   2   7-14.8506 147.446   8
   5   2   8 6972.68 275.401   9
   5   2   8 6902.88 183.924  12
   5   2   8 7073.64 223.472  25
   5   2   8 6438.09 228.145  37
   5  -2   9 3641.41 177.207  19
   5   2   9 3216.53 217.535  37
   5   2   9 3354.94 206.636  25
   5   2   9 3520.02 165.745  12
   5  -2   9 3043.60 240.806  30
   5  -2   9 3172.39 214.809  32
   5  -2  10 2379.82 210.813  32
   5   2  10 2200.82 213.106  35
   5   2  10 2437.41 226.132  37
   5   2  10 2184.35 215.834  25
   5   2  10 1957.81 168.312  12
   5   2  10 2174.28 233.413  29
   5   2  11 0.94886 199.243  35
   5   2  11 287.421 224.557  37
   5   2  11 130.555 215.725  25
   5   2  11 127.670 157.335  12
   5   2  11 148.493 236.529  29
   5   2  12 2861.12 241.535  29
   5  -2  12 2176.54 171.300  25
   5   2  12 2613.57 225.471  25
   5   2  12 2505.33 221.316  37
   5   2  13 5042.35 225.661  29
   5  -2  13 3943.68 160.326  25
   5   2  13 5091.09 213.308  25
   5   2  13 4269.38 199.253  37
   5   2  14 885.061 141.253  25
   5  -2  14 665.653 94.7104  25
   5   2  14 699.811 147.213  29
   5   2  15 1933.25 84.7681  25
   5  -2  15 2254.50 92.6911  29
   5   3 -16 148.225 81.9429  31
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  -5   3  15 5404.98 163.064   5
  -5  -3  14 523.484 129.225   5
  -5   3  14 589.095 150.789   5
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  -5   3  13 388.391 180.074  34
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  -5   3  13 614.447 161.630   5
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  -5   3  12 141.456 160.816   5
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  -5   3   9 20225.1 465.444   2
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  -5   3   8 556.183 207.035   2
  -5   3   8 403.822 175.651   7
  -5   3   7 478.066 200.515   2
  -5  -3   7 679.091 179.878   2
  -5   3   7 364.227 148.086   7
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  -5   3   6 1374.43 158.591   7
  -5   3   6 1457.92 189.142   2
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  -5   3   5 36770.3 636.949   7
  -5   3   5 38178.4 664.938  10
  -5   3   4 5507.92 184.229   7
   5   3  -4 5008.65 143.511   9
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  -5   3   3 123228. 1842.13  10
   5   3  -3 118747. 1805.71   9
   5  -3  -2 24726.5 452.069   1
   5   3  -2 25279.3 466.752   1
  -5   3   2 26555.2 477.207  10
   5   3  -2 25462.3 450.678   9
   5  -3  -1 1899.63 139.258   1
   5   3  -1 1970.15 154.839   1
   5   3  -1 1742.64 127.596   9
   5  -3   0 99182.6 1516.09   1
   5   3   0 102813. 1534.75   1
   5   3   0 97707.8 1531.04   9
   5  -3   1 4875.09 170.250   1
   5   3   1 4786.35 185.806   1
   5   3   1 4797.42 185.070   9
   5  -3   2 52170.3 824.318   1
   5   3   2 52799.3 851.880   9
   5  -3   3 7000.52 224.202   1
   5   3   3 6340.14 233.495   1
   5  -3   4 137324. 2039.73   1
   5   3   4 127223. 2047.78   1
   5   3   4 133384. 2063.35   9
   5  -3   4 139097. 1958.79   3
   5   3   4 129758. 1961.01   3
   5   3   5 79291.8 1269.18   8
   5   3   5 78616.1 1269.57   9
   5  -3   5 79273.1 1151.77   3
   5   3   5 75433.5 1156.29   3
   5   3   6 21437.5 473.344   9
   5   3   6 21540.9 367.640   3
   5   3   6 20688.1 351.268  12
  -5   3  -7 43238.8 783.996   6
   5   3   7 43663.0 667.772  12
   5   3   7 43847.2 787.395   8
   5   3   7 43850.2 800.739   9
   5   3   8 88716.5 1355.29  25
  -5   3  -8 89772.6 1332.13  23
   5  -3   8 92226.4 1343.92  19
   5   3   8 87723.6 1326.25  12
   5  -3   8 90191.0 1359.40  30
   5   3   8 88886.0 1363.74  37
   5   3   8 89642.9 1357.43  35
   5  -3   9 2311.11 224.996  32
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   5  -3   9 2434.32 181.451  19
   5   3   9 2066.95 205.979  25
   5   3   9 2337.21 227.159  29
   5   3   9 1981.47 141.022  12
   5   3   9 2127.27 229.265  37
   5   3   9 2174.94 207.256  35
   5  -3  10 20904.8 414.878  32
  -5   3 -10 19829.9 360.840  23
   5  -3  10 21563.1 383.258  19
   5   3  10 21982.6 367.169  12
   5   3  10 19223.3 411.569  35
   5   3  10 19811.9 429.096  37
   5   3  10 19887.6 419.483  36
   5   3  10 21597.2 421.582  25
   5   3  10 20875.2 428.506  29
   5  -3  11 9429.96 249.489  12
   5   3  11 8533.03 274.464  36
   5   3  11 8720.88 264.989  35
   5   3  11 8674.26 295.284  37
   5   3  11 9340.36 288.059  25
   5   3  11 9450.13 294.792  29
   5  -3  12 26114.1 436.818  12
   5   3  12 26323.4 483.072  37
   5   3  12 28012.7 477.617  25
   5   3  12 28061.4 481.852  29
   5   3  13 14085.6 308.799  37
   5   3  13 15124.3 308.981  25
   5   3  13 14471.7 305.944  29
   5   3  14 1553.87 139.795  25
   5  -3  14 1441.05 147.169  29
   5   3  15 167.655 54.5206  25
  -5   4  16 2088.68 110.749  37
   5   4 -16 1955.60 84.1353  31
  -5   4  15 529.449 182.984  37
   5   4 -15 661.914 135.820  31
  -5  -4  14 5175.24 149.052   5
  -5   4  14 4771.48 154.711  11
  -5  -4  13 14628.3 292.529  24
  -5  -4  13 13660.1 276.442  15
  -5   4  13 13584.6 275.875  11
  -5   4  13 14574.6 313.325  34
  -5  -4  13 12922.3 258.119   5
  -5   4  13 14069.7 277.848   5
  -5   4  12 95.4554 152.937   5
  -5  -4  12-15.4681 130.420   5
  -5   4  12 192.205 195.885  34
  -5  -4  12 77.1130 154.964  15
  -5  -4  11 5796.25 190.254  15
  -5  -4  11 5464.43 165.726   5
  -5   4  11 5449.30 182.379   5
  -5  -4  10 17112.5 317.258  15
  -5   4  10 16165.5 419.858   2
  -5  -4  10 16623.9 386.493   2
  -5  -4  10 16750.9 296.496   5
  -5   4  10 16836.9 309.691   5
  -5  -4   9 131.375 181.228   2
  -5   4   9 229.325 207.077   2
  -5   4   9 300.154 123.202   5
  -5  -4   9 265.727 107.195   5
  -5  -4   8 881.931 183.204   2
  -5   4   8 737.467 204.839   2
  -5   4   8 607.180 185.707   7
  -5   4   7 4661.87 226.192   7
  -5   4   7 4607.50 246.943  10
  -5  -4   7 4646.15 212.434   2
  -5   4   7 4371.57 235.564   2
  -5   4   6 8557.80 270.626   7
  -5   4   6 9277.23 277.235   2
  -5   4   5 2348.08 177.582   7
  -5   4   5 2094.89 174.685   2
  -5  -4   5 2225.98 156.050   2
  -5   4   4 212161. 3165.52   7
   5   4  -3 145553. 2181.74   9
   5   4  -3 146717. 2199.79   1
   5  -4  -3 146056. 2185.08   1
   5   4  -2 410.548 107.557   9
   5  -4  -2 321.109 117.847   1
   5   4  -2 419.274 133.471   1
   5   4  -1 51702.7 838.437   9
   5  -4  -1 50693.1 820.193   1
   5   4  -1 51600.2 838.197   1
   5   4   0 36132.0 630.575   9
   5  -4   0 36300.3 606.539   1
   5   4   0 36543.8 626.517   1
   5  -4   1 26208.9 461.903   1
   5   4   1 25184.4 475.728   1
   5   4   2 125806. 1949.99   9
   5   4   2 122197. 1922.30   1
   5  -4   3 91172.1 1350.69   1
   5   4   3 82747.4 1356.88   1
   5   4   4 18705.3 415.833   8
   5   4   4 17496.6 390.155   9
   5  -4   4 16628.6 351.771   1
   5   4   4 15300.0 359.052   1
   5  -4   4 16799.1 271.115   3
   5   4   4 15525.0 274.735   3
   5   4   5 46350.4 731.729   3
   5   4   5 47511.9 864.303   8
   5   4   5 46625.9 841.032   9
   5   4   6 1139.47 119.368   3
   5  -4   6 1304.28 111.810   3
   5   4   6 1285.82 203.926   9
   5   4   6 1080.92 216.599   8
   5   4   7-56.8736 192.115   9
   5   4   7 164.322 192.207   8
  -5   4  -7 134.968 194.381   6
   5   4   8 25510.4 461.363  37
   5   4   8 24268.0 442.863  35
   5   4   8 24467.3 435.803  36
   5   4   8 22930.2 435.065  25
  -5   4  -8 23329.9 404.062  23
   5  -4   8 24179.9 426.075  19
   5   4   8 25391.7 443.994  29
   5  -4   8 24475.3 451.414  30
   5   4   8 21829.9 382.107  12
   5   4   8 20116.6 512.195   9
  -5   4  -9 4170.48 169.198  23
   5  -4   9 4370.43 208.820  19
   5   4   9 4508.14 227.741  25
   5   4   9 4342.05 227.705  29
   5  -4   9 4645.81 267.771  30
   5   4   9 4342.91 226.009  36
   5   4   9 3992.26 215.953  35
   5   4   9 4209.71 259.387  37
  -5   4 -10 4122.72 173.510  23
   5  -4  10 4326.18 207.560  19
   5   4  10 4593.73 248.037  25
   5   4  10 5137.91 253.630  29
   5  -4  10 5558.50 250.486  32
   5   4  10 5275.85 225.428  35
   5   4  10 5298.71 280.305  37
   5   4  10 5131.71 235.194  36
  -5   4 -11 997.843 129.361  23
   5  -4  11 1348.32 170.357  19
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   5  -5  10 40759.6 660.366  32
   5   5  10 38445.2 648.142  35
   5   5  10 40605.9 684.083  37
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   5   6   6 905.414 168.454  36
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   5   6   7 578.778 134.474  22
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   5   6   8 930.059 186.427  36
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   5   6   9 7660.01 259.218  25
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   5   6   9 8350.36 307.774  37
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   5   6  10 2279.63 217.617  25
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   5   7   7 6574.25 232.514  29
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   5   7   8 51435.3 790.992  25
   5   7   8 48546.8 782.156  26
   5   7   8 51081.2 789.949  29
   5  -7   8 48651.2 800.062  30
   5   7   8 51962.3 820.652  37
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   5   7   9 28388.1 501.537  29
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   5   7   9 29775.1 544.229  37
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   5   7  10 33525.8 569.910  29
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   5   7  10 36179.1 611.663  37
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   5   7  11 5200.08 189.421  25
   5  -7  12 688.969 75.0476  12
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   5   8 -10 8871.32 244.796  31
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   5   8  -4 19074.4 333.462  16
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   5   8  -2 329.197 159.984   8
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   5   8  -1 869.930 181.313   8
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   5   8   2 103314. 1568.70  26
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   5   8   2 105756. 1577.42  21
   5   8   2 105889. 1583.53  33
   5   8   2 102488. 1559.94  16
   5   8   2 105155. 1709.70   8
   5   8   3 3888.25 161.926  27
   5   8   3 4416.32 179.088  22
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   5   8   3 5084.87 278.345   8
   5   8   3 4498.73 162.408  16
   5   8   4 89.9823 171.470  29
   5   8   4 244.506 129.475  27
   5   8   4 130.645 148.786  26
   5   8   4 125.166 161.034  22
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   5   8   4 28.4048 159.125  21
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   5   8   4 236.337 171.745  33
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   5   8   4 19.4915 133.844  16
   5   8   4-44.7945 220.688   8
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   5  -8   5 63.2676 189.993  19
   5   8   5 167.946 166.329  26
   5   8   5 89.4581 128.154  27
   5   8   5 224.911 180.225  29
   5   8   5 150.687 156.612  33
   5   8   5 155.873 135.892  16
   5  -8   6 1952.92 208.979  19
   5   8   6 1824.04 174.455  25
   5   8   6 2124.27 186.254  26
   5   8   6 1903.45 192.173  29
   5   8   6 1939.59 139.694  27
   5   8   6 1864.36 175.754  22
   5   8   6 1894.85 158.813  21
   5  -8   6 2035.97 195.583  30
   5  -8   7 714.424 203.797  30
   5   8   7 783.812 191.780  29
   5   8   7 706.093 170.153  25
   5   8   7 603.920 176.276  26
   5   8   7 651.602 166.296  22
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   5  -8   7 361.672 205.933  19
   5   8   7 644.165 137.074  21
   5  -8   8 27293.2 487.038  19
   5   8   8 26506.3 470.092  26
   5   8   8 26997.9 466.695  25
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   5  -8   8 26746.4 492.044  30
   5   8   8 27393.8 476.521  29
   5  -8   9 834.951 216.175  30
   5   8   9 719.942 170.912  29
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   5   8   9 682.218 164.334  25
   5  -8  10 271.541 97.6999  12
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   5  -8  10 430.726 174.426  19
   5  -8  11 537.603 74.8509  12
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   6   1   2 5835.69 230.527   1
   6  -1   3 106822. 1588.72   4
   6   1   3 107054. 1591.33   4
   6  -1   3 115094. 1683.53   1
   6   1   3 113671. 1691.95   1
   6  -1   4 4704.65 134.797   3
   6   1   4 4574.20 135.749   3
   6  -1   4 4778.44 234.107   1
   6   1   4 4620.23 237.448   1
   6  -1   5 13527.6 245.553   3
   6   1   5 12803.1 246.042   3
   6  -1   5 12867.7 348.874   1
   6   1   5 12646.9 351.902   1
   6   1   6 17576.9 319.696   3
   6  -1   6 18228.6 317.735   3
   6   1   6 18425.0 450.887   9
   6  -1   7 2682.42 154.399   3
   6   1   7 2316.39 159.125   3
   6   1   7 2626.83 236.740   9
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   6   1   8 2652.54 235.674   9
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   6  -1   8 2437.17 207.160  32
   6   1   8 2054.43 191.708  37
   6   1   8 2345.37 182.190  25
   6   1   9 19660.2 399.098  37
   6   1   9 20336.9 395.887  25
   6  -1   9 19825.6 377.933  25
   6   1   9 20437.8 371.784  12
   6   1   9 20573.4 402.359  32
   6  -1   9 21077.3 409.273  32
   6   1  10 438.729 187.579  32
   6  -1  10 239.262 207.857  32
   6   1  10 288.486 203.679  37
   6   1  10 236.674 198.097  25
   6  -1  10 297.638 171.124  25
   6  -1  10-2.85550 181.056  12
   6   1  10 141.655 159.913  12
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   6   1  11 3957.50 210.317  37
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   6   1  11 4541.43 180.111  12
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   6   1  12 39577.2 658.762  36
   6   1  12 39564.9 633.007  25
   6  -1  12 40483.8 658.983  29
   6   1  12 38888.5 612.103  12
   6  -1  12 41195.6 618.462  12
   6   1  13 1858.96 145.417  25
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   6   2  -3 63000.5 1017.43   9
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   6   2   0 73539.9 1157.54   1
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   6   2   1 49500.2 827.198   1
   6  -2   2 47855.7 790.149   1
   6   2   2 48749.7 809.822   1
   6  -2   2 46604.5 709.095   4
   6   2   2 47464.6 714.470   4
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   6   2   3 32174.1 584.835   1
   6  -2   3 30000.7 469.836   4
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   6   2   4 2357.42 204.813   9
   6  -2   4 2464.29 198.655   1
   6   2   4 2200.49 212.259   1
   6  -2   4 2281.64 109.436   3
   6   2   4 2274.16 116.409   3
   6   2   5 12024.0 346.349   9
   6   2   5 11085.3 306.062   8
   6  -2   5 9505.32 299.264   1
   6   2   5 9646.05 313.516   1
   6  -2   5 10533.5 207.281   3
   6   2   5 9891.10 210.722   3
   6   2   6 6733.24 190.428   3
   6   2   6 6181.79 251.559   8
   6   2   6 6422.02 287.759   9
   6   2   7 20585.8 406.393  37
   6   2   7 21077.6 393.656  25
   6   2   7 20903.0 501.737   9
   6   2   7 20606.8 407.893  29
   6  -2   7 20390.3 417.365  32
   6   2   7 21008.7 363.156  12
   6   2   7 21452.5 379.367   3
   6   2   8 4644.45 202.565  32
   6  -2   8 5182.74 240.606  32
   6   2   8 3207.61 253.180   9
   6  -2   8 4000.00 189.815  19
   6   2   8 4662.37 226.837  37
   6   2   8 4337.35 205.263  25
   6   2   8 4712.15 233.241  29
   6   2   8 3617.06 159.537  12
   6   2   9 3670.32 251.151  29
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   6   2   9 3624.15 236.982  37
   6   2   9 3477.81 222.290  35
   6   2   9 3506.94 214.033  32
   6  -2   9 3499.66 238.815  32
   6   2   9 3843.69 222.143  25
   6   2   9 4119.95 167.084  12
   6   2  10 3122.98 239.667  37
   6   2  10 3413.79 248.644  35
   6  -2  10 3228.33 231.513  32
   6   2  10 3569.36 227.535  25
   6   2  10 3336.14 161.842  12
   6   2  11 20434.2 389.892  25
   6  -2  11 17308.4 346.050  25
   6   2  11 19142.1 393.569  37
   6   2  11 20376.7 403.165  35
   6   2  11 21159.7 414.784  36
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   6  -2  11 19516.8 356.982  12
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   6  -2  12 401.985 127.227  25
   6  -2  12 510.348 141.145  12
   6   2  13 5258.17 175.900  25
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   6   3   0 35479.2 647.034   9
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   6   3   1 9008.88 260.590   1
   6  -3   2 64423.1 1015.11   1
   6   3   2 63903.7 1036.47   1
   6  -3   2 62422.7 937.284   4
   6   3   2 62598.3 943.353   4
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   6   3   4 2659.74 216.317   1
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   6   3   5 22945.0 500.151   8
   6   3   5 23353.3 509.177   9
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   6   3   5 22087.8 379.973   3
   6   3   6 42791.5 827.886   9
   6   3   6 46128.4 830.499   8
   6  -3   6 46687.7 688.799   3
   6   3   6 42166.7 692.212   3
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   6   3   7 5171.75 220.452  29
   6   3   7 5461.49 211.905  32
   6   3   7 4589.89 144.394  12
   6   3   7 4360.51 236.354   8
   6   3   7 4774.43 268.341   9
   6   3   8 13647.3 333.973  37
   6   3   8 13334.1 328.496  35
   6   3   8 13934.0 313.326  25
   6   3   8 12721.6 279.609  26
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   6   3   8 13172.9 255.752  12
   6  -3   9 6299.42 224.675  19
   6   3   9 6834.02 274.895  37
   6   3   9 6940.53 267.822  35
   6   3   9 6910.78 272.623  36
   6   3   9 6323.05 249.697  25
   6   3   9 5779.88 172.762  12
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   6   3  10 7609.02 271.513  35
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   6   3  11-64.8540 204.476  25
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   6   3  11 31.9874 215.813  36
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   6   3  12 16487.7 334.935  25
   6   3  12 16441.9 347.845  29
   6   3  13 35.6819 138.029  25
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   6   4   0 4276.68 202.790   1
   6   4   0 4264.68 204.655   9
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   6   4   1 12421.5 308.200   1
   6   4   1 12481.2 323.517   9
   6   4   2 2304.43 101.578   4
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   6   4   2 2372.43 189.685   1
   6   4   2 2016.56 191.502   9
   6   4   3 15531.3 276.979   3
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   6   4   3 15436.3 368.956   1
   6   4   3 16842.0 392.616   9
   6   4   4 22089.9 378.061   3
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   6   4   4 21284.0 470.424   1
   6   4   4 24861.2 519.789   9
   6   4   5 22810.4 400.913   3
   6   4   5 24475.1 547.557   8
   6   4   5 23560.2 534.109   9
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   6   4   6 9315.62 240.222  25
   6   4   6 8673.49 321.932   9
   6   4   6 9194.46 359.852   8
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   6  -4   6 9931.81 263.647  30
   6   4   6 10400.7 262.648  36
   6   4   6 10397.2 256.086  35
   6   4   6 10102.7 273.542  37
   6   4   6 7963.75 209.356   3
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   6  -4   7 60043.0 957.497  30
   6   4   7 61623.9 955.267  29
   6   4   7 60465.6 948.860  25
   6   4   7 59928.3 946.401  26
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   6   4   7 61128.3 963.237  35
   6   4   7 61578.9 958.699  36
   6   4   7 62253.8 970.198  37
   6   4   7 57506.9 1058.12   8
   6   4   7 58336.1 1064.50   9
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   6  -4   8 18254.5 357.632  19
   6   4   8 17006.8 321.156  18
   6   4   8 17217.6 377.632  35
   6   4   8 16601.8 375.793  36
   6   4   8 17417.8 395.315  37
   6   4   8 17467.9 366.965  25
   6   4   8 16889.0 343.202  26
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   6   4   9 16600.8 357.732  25
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   6   4   9 17008.7 371.363  35
   6   4   9 16144.4 371.511  36
   6   4   9 17207.2 394.464  37
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   6   4  10 12608.8 326.591  29
   6   4  10 12402.4 312.651  35
   6   4  10 11946.1 315.108  36
   6   4  10 12759.8 345.878  37
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   6   4  10 11636.8 310.009  25
   6   4  11 3900.96 225.300  25
   6   4  11 3836.96 232.470  29
   6  -4  11 3392.76 162.736  12
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   6   4  11 3918.18 252.670  37
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   6   4  12 1470.69 185.902  25
   6   4  13 13880.9 263.860  29
   6  -4  13 13808.8 239.136  12
   6  -4  14 1287.84 73.3965  29
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  -6   5   6 19292.0 433.283   7
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   7   0   3 38109.9 597.457   4
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   7  -1  -4 49449.5 856.841   1
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   7   1  -3 3444.22 218.816   1
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   7   1  -2 29905.6 558.353   1
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   7  -1  -1 21108.9 427.148   1
   7   1  -1 20858.6 435.633   1
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   7   1  -1 19929.4 331.555   4
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   7  -1   0 73796.2 1142.76   1
   7   1   0 74495.3 1153.57   1
   7  -1   0 69755.0 1050.95   4
   7   1   0 70670.4 1053.36   4
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  -7   1   0 70649.7 1129.10  10
   7  -1   1 153898. 2370.80   1
   7   1   1 159185. 2382.78   1
   7  -1   1 156727. 2292.59   4
   7   1   1 158297. 2294.92   4
   7  -1   2 33471.5 616.205   1
   7   1   2 33518.3 627.780   1
   7  -1   2 33701.0 525.756   4
   7   1   2 34130.6 529.894   4
   7  -1   3 17925.4 397.427   1
   7   1   3 18320.8 412.519   1
   7  -1   3 16492.6 289.146   4
   7   1   3 16575.1 294.491   4
   7  -1   4 17301.6 408.380   1
   7   1   4 17370.7 425.650   1
   7   1   4 17594.6 313.097   3
   7  -1   4 17714.7 307.943   3
   7  -1   5 1759.81 217.164   1
   7   1   5 1747.73 230.261   1
   7  -1   5 1808.10 134.729   3
   7   1   5 1755.87 141.150   3
   7   1   5 1997.64 251.324   9
   7  -1   6 474.223 156.887  19
   7  -1   6 210.676 143.018   3
   7   1   6 174.697 150.342   3
   7   1   6 387.483 216.336   9
   7   1   6 396.788 185.152  32
   7  -1   6 692.047 195.498  32
   7   1   6 322.363 168.095  29
   7   1   7 45211.7 742.567  29
   7   1   7 45379.1 726.631  25
   7   1   7 44002.9 714.846   3
   7  -1   7 46058.2 711.870   3
   7  -1   7 44528.3 874.593   9
   7   1   7 43501.9 864.022   9
   7   1   7 47491.1 750.496  32
   7  -1   7 46950.4 750.945  32
   7   1   8 2149.23 189.560  25
   7   1   8 1684.73 153.015  12
   7   1   8 2169.53 232.331  29
   7   1   8 2367.62 227.737  32
   7  -1   8 2303.12 237.197  32
   7   1   9 2628.73 200.096  25
   7   1   9 2756.01 227.884  32
   7  -1   9 2671.93 244.758  32
   7   1   9 2677.53 158.457  12
   7   1   9 2390.01 242.047  29
   7   1  10 19069.7 374.299  25
   7   1  10 20556.8 421.986  35
   7  -1  10 19096.6 397.669  32
   7   1  10 19819.6 412.947  29
   7  -1  10 21128.1 360.545  12
   7   1  10 20139.8 350.926  12
   7   1  11 1215.35 251.149  36
   7   1  11 1036.09 219.227  35
   7   1  11 982.764 168.782  25
   7  -1  11 734.121 131.392  25
   7   1  11 1178.49 226.494  29
   7  -1  11 1112.12 216.334  29
   7   1  11 884.318 126.294  12
   7  -1  11 808.861 141.949  12
   7   1  12 65.7787 192.372  36
   7   1  12 169.916 134.497  25
   7   1  12 219.145 191.748  29
   7  -1  12 132.226 177.587  29
   7  -1  12 310.139 109.136  12
   7  -1  13 2222.34 148.330  36
   7   1  13 2137.36 142.701  29
   7  -1  13 2342.68 137.431  29
   7  -1  14 870.583 61.7701  29
  -7   2  16 1865.29 79.0206  37
  -7  -2  15 429.065 86.4902   5
  -7   2  15 342.479 95.9587   5
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  -7   2  14 7466.79 181.122   5
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  -7   2  13 2037.34 154.972   5
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  -7   2  11 10724.0 242.804   5
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  -7   2  10 34592.0 550.092   5
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  -7   2   9 1829.61 245.047   2
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  -7   2   8 4554.56 162.586   5
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  -7   2   7 1538.22 237.720   2
  -7   2   7 1511.28 227.874  10
  -7   2   6 1755.82 212.665  10
  -7   2   5 683.284 191.806  10
   7   2  -4 147089. 2241.55   1
   7  -2  -4 144128. 2229.08   1
  -7   2   4 148890. 2243.29  10
   7  -2  -3 452.084 173.090   1
   7   2  -3 536.069 187.119   1
  -7   2   3 679.602 174.709  10
   7   2  -3 538.272 134.885   9
   7  -2  -2 31007.8 579.671   1
   7   2  -2 31399.4 595.357   1
  -7   2   2 32905.8 593.745  10
   7   2  -2 31723.1 585.362   9
   7  -2  -1 4726.89 222.518   1
   7   2  -1 4969.95 244.555   1
   7   2  -1 4874.74 137.296   4
   7  -2  -1 4599.46 127.355   4
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   7   2  -1 4601.69 218.125   9
   7  -2   0 43891.6 738.285   1
   7   2   0 46352.7 760.581   1
   7   2   0 43094.4 651.817   4
   7  -2   0 40916.5 645.366   4
  -7   2   0 43661.9 740.783  10
   7  -2   1 6072.45 230.477   1
   7   2   1 6082.73 251.459   1
   7  -2   1 6017.33 146.083   4
   7   2   1 6544.34 154.818   4
   7  -2   2 131791. 2010.05   1
   7   2   2 135881. 2031.54   1
   7   2   2 133029. 1928.94   4
   7  -2   3 20718.5 440.081   1
   7  -2   3 19839.8 334.707   4
   7   2   3 20205.8 343.481   4
   7  -2   4 28568.7 568.921   1
   7   2   4 29242.6 593.518   1
   7   2   4 29944.8 483.807   3
   7  -2   4 29890.3 475.480   3
   7  -2   5 27177.2 554.418   1
   7   2   5 26715.7 574.880   1
   7   2   5 28131.3 466.557   3
   7  -2   5 29008.1 459.368   3
   7   2   5 28511.0 570.111   8
   7   2   6 2173.99 201.957   8
   7   2   6 1771.75 245.915   9
   7  -2   6 2065.83 176.572  19
   7   2   6 2186.75 189.531  29
   7   2   6 2326.76 201.826  32
   7  -2   6 2405.01 209.273  32
   7  -2   6 2067.19 151.610   3
   7   2   6 2086.36 164.210   3
   7   2   6 2214.15 167.788  25
   7   2   7 2255.41 185.873  25
   7   2   7 1727.88 251.589   9
   7  -2   7 2170.80 184.651  19
   7   2   7 2391.96 217.091  32
   7  -2   7 2439.08 241.973  32
   7   2   7 2162.69 215.503  29
   7   2   7 1949.98 132.557  12
   7  -2   7 2057.95 159.195   3
   7   2   7 1915.82 171.407   3
   7  -2   8 36523.4 601.529  19
   7   2   8 37739.9 613.657  25
   7   2   8 36332.8 622.331  32
   7  -2   8 38762.0 644.810  32
   7   2   8 35313.9 578.874  12
   7   2   8 37403.4 633.390  29
   7   2   9 884.299 198.707  25
   7   2   9 649.788 257.549  36
   7   2   9 741.933 228.237  35
   7  -2   9 831.979 232.747  32
   7   2   9 783.973 131.687  12
   7   2   9 734.326 236.604  29
   7   2  10 23800.0 441.169  25
   7   2  10 25230.7 481.403  35
   7   2  10 24774.0 484.857  36
   7  -2  10 23619.0 458.342  32
   7   2  10 24102.6 470.233  29
   7  -2  10 24090.8 421.234  12
   7  -2  11 1503.79 139.558  12
   7   2  11 1509.90 181.737  25
   7   2  11 1199.15 224.120  29
   7  -2  11 1380.74 205.551  29
   7   2  11 1375.91 230.476  36
   7   2  11 1170.44 212.440  35
   7  -2  12 6066.27 158.000  12
   7   2  12 6336.13 185.487  25
   7  -2  13 967.934 143.636  36
   7  -2  13 874.044 118.443  29
   7   2  13 707.098 88.7474  25
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  -7  -3  13 258.633 117.901   5
  -7   3  13 439.374 137.072   5
  -7   3  13 95.6211 141.426  34
  -7  -3  12 14587.2 280.860  15
  -7  -3  12 14484.9 266.537   5
  -7  -3  11 13290.0 269.403   5
  -7   3  11 14244.0 285.896   5
  -7  -3  10 20988.4 369.213   5
  -7   3  10 21982.2 383.756   5
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  -7   3   9 8108.28 316.124   2
  -7  -3   9 8826.31 200.003   5
  -7   3   9 8594.12 217.693   5
  -7   3   8 56732.1 969.071   2
  -7  -3   8 56179.8 939.116   2
  -7  -3   8 54044.5 826.805   5
  -7   3   8 54587.6 835.437   5
  -7   3   7 10255.3 349.655  10
  -7   3   7 10639.3 344.198   2
  -7  -3   7 11284.3 318.072   2
  -7   3   6 13882.4 383.003  10
  -7   3   6 13695.7 371.139   2
  -7  -3   6 14396.4 348.521   2
   7   3  -5 37482.6 683.882   1
   7  -3  -5 35887.5 665.322   1
  -7   3   5 36331.0 645.208   7
   7  -3  -4 34737.8 639.984   1
   7   3  -4 35738.8 657.586   1
  -7   3   4 36676.7 671.816  10
  -7   3   4 36058.6 631.058   7
  -7   3   3 71533.2 1134.92  10
   7   3  -3 71363.6 1119.28   1
  -7   3   2 13.8845 177.440  10
   7   3  -2 22.4621 140.035   9
   7  -3  -2 61.1435 168.923   1
   7   3  -2 85.3949 193.830   1
  -7   3   1 82187.2 1293.09  10
   7   3  -1 78816.3 1281.96   9
   7   3  -1 81518.5 1186.49   4
   7  -3  -1 77841.4 1179.83   4
   7  -3  -1 78192.3 1257.82   1
   7   3  -1 84358.5 1285.49   1
   7   3   0 13572.6 347.665   9
  -7   3   0 13707.5 348.569  10
   7  -3   0 12729.8 230.467   4
   7   3   0 13330.3 241.169   4
   7  -3   0 12869.0 312.552   1
   7   3   0 13768.3 344.684   1
   7   3   1 50826.0 851.526   9
   7   3   1 49168.5 732.268   4
   7  -3   1 46434.4 723.200   4
   7  -3   1 47557.1 806.099   1
   7   3   1 49909.7 832.031   1
   7   3   2 1803.08 208.009   9
   7  -3   2 1735.55 105.041   4
   7   3   2 1700.05 120.079   4
   7  -3   2 1719.94 187.955   1
   7   3   2 1835.84 217.138   1
   7   3   3 31903.4 617.088   9
   7  -3   3 29188.8 469.385   4
   7   3   3 29620.5 478.203   4
   7  -3   3 31599.5 573.411   1
   7   3   3 31641.3 603.891   1
   7   3   4 24749.2 550.015   9
   7  -3   4 23482.5 490.921   1
   7   3   4 22726.7 515.534   1
   7   3   4 24497.0 411.478   3
   7  -3   4 25253.1 401.939   3
   7   3   5 10037.0 336.987   8
   7   3   5 10451.8 353.961   9
   7  -3   5 11921.7 261.340  19
   7  -3   5 8766.50 294.470   1
   7   3   5 8449.81 317.553   1
   7   3   5 13422.6 272.864  35
   7  -3   5 10086.7 215.139   3
   7   3   5 9383.01 225.392   3
   7   3   6 3625.87 204.728  32
   7   3   6 3656.94 190.692  25
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   7  -3   6 3577.55 202.846  19
   7   3   6 3538.22 210.386  29
   7  -3   6 3541.42 156.581   3
   7   3   6 3239.79 170.630   3
   7   3   6 3293.12 258.384   9
   7   3   6 3049.97 240.046   8
   7   3   7 15256.4 339.322  29
  -7   3  -7 13537.5 275.471  23
   7  -3   7 15101.7 322.591  19
   7   3   7 12895.3 425.098   9
   7   3   7 15120.5 322.724  25
   7   3   7 14697.3 343.562  32
   7  -3   7 15479.1 369.769  32
   7   3   7 15477.3 347.846  35
   7   3   7 15406.8 351.819  36
   7   3   8 1906.66 247.396  35
   7   3   8 1897.02 252.604  36
   7  -3   8 1119.31 197.816  19
   7   3   8 1338.88 209.888  25
   7   3   8 1486.06 171.121  26
   7   3   8 1512.67 226.070  29
   7  -3   8 1749.41 252.506  32
   7   3   9 900.139 252.438  36
   7   3   9 1136.51 235.611  35
   7   3   9 782.340 142.131  18
   7   3   9 1044.54 204.334  25
   7  -3   9 960.482 246.346  32
   7   3   9 930.957 235.592  29
   7  -3   9 829.498 184.473  19
   7   3  10 6720.78 266.304  35
   7   3  10 6522.52 276.884  36
   7  -3  10 6217.63 254.992  32
   7   3  10 6300.97 240.588  25
   7   3  10 6549.84 269.852  29
   7   3  11 13866.1 294.535  25
   7   3  11 13388.9 309.897  35
   7   3  11 14003.7 315.691  36
   7  -3  12 210.777 100.100  12
   7   3  12 209.242 137.176  25
   7  -3  12 289.824 149.352  29
   7   3  13 840.970 86.9442  25
   7   3  13 885.047 114.823  29
   7  -3  13 780.991 105.163  29
   7  -3  13 855.431 132.714  36
   7   4 -15 72.0917 91.5608  31
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  -7   4  12 1361.65 140.081   5
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  -7  -4  11 293.245 121.120   5
  -7   4  11 364.963 142.210   5
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  -7   4  10 1638.70 153.011   5
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  -7   4   9 336.555 141.093   5
  -7  -4   9 397.740 122.374   5
  -7   4   8 560.633 129.660   5
  -7  -4   8 414.084 114.933   5
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  -7   4   8 382.998 218.805   2
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  -7   4   7 1175.48 218.537   2
  -7  -4   7 1260.62 107.707   5
  -7   4   7 1354.05 126.841   5
  -7   4   7 1245.93 238.997  10
  -7   4   6 97752.8 1539.18   2
  -7  -4   6 101375. 1517.24   2
   7   4  -6 92303.2 1527.94   1
   7  -4  -6 91857.5 1513.40   1
  -7   4   6 95293.6 1524.90   7
  -7   4   6 103097. 1589.70  10
   7  -4  -5 292.132 167.547   1
   7   4  -5 471.210 183.972   1
  -7   4   5 323.097 158.924   7
  -7   4   5 258.891 211.449  10
  -7   4   4 4018.19 204.932   7
   7  -4  -4 3833.48 203.942   1
   7   4  -4 4199.51 223.694   1
  -7   4   4 3935.72 247.450  10
  -7   4   4 3921.35 127.076  11
   7  -4  -3 17153.9 384.089   1
   7   4  -3 17732.2 406.585   1
   7   4  -3 17804.1 380.235   9
  -7   4   3 18219.8 301.328  11
   7  -4  -2 12886.5 310.144   1
   7   4  -2 13490.4 338.591   1
   7  -4  -2 11835.1 221.455   4
   7   4  -2 12640.3 233.577   4
  -7   4   2 12779.6 357.479  10
   7   4  -2 11309.8 312.085   9
   7  -4  -1 32282.1 564.284   1
   7   4  -1 31371.3 485.958   4
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   7   4  -1 30499.0 585.362   9
   7  -4   0 77326.8 1241.53   1
   7   4   0 80551.9 1268.58   1
   7   4   0 81226.1 1179.33   4
   7  -4   0 76521.5 1170.53   4
  -7   4   0 87666.6 1311.01  10
   7   4   0 83217.6 1296.57   9
   7  -4   1 8185.55 247.494   1
   7   4   1 8372.99 274.581   1
   7  -4   1 7921.32 166.963   4
   7   4   1 8245.89 180.846   4
   7   4   1 7882.30 281.245   9
   7  -4   2 8540.53 257.082   1
   7   4   2 8214.26 279.825   1
   7  -4   2 7865.47 166.067   4
   7   4   2 7821.05 179.990   4
   7   4   2 7920.02 300.335   9
   7  -4   3 1547.48 176.406   1
   7   4   3 1288.16 199.816   1
   7   4   3 1388.64 120.881   3
   7  -4   3 1418.94 106.651   3
   7   4   3 1212.25 211.086   9
   7  -4   4 6229.01 238.360   1
   7  -4   4 6366.05 156.398   3
   7   4   4 6001.59 167.547   3
   7   4   5 5195.85 216.503  29
   7   4   5 5235.10 202.254  25
  -7   4  -5 4651.05 165.817  23
   7  -4   5 5343.65 221.763  19
   7  -4   5 5880.98 162.176   3
   7   4   5 5714.01 175.600   3
   7   4   5 5708.62 285.669   8
   7   4   5 5214.20 296.346   9
   7   4   5 4544.43 226.612  35
   7   4   6 82583.3 1244.01  29
   7   4   6 84345.4 1238.07  25
   7   4   6 76291.8 1366.56   9
   7   4   6 77450.9 1365.60   8
   7  -4   6 82705.8 1236.54  19
   7   4   6 83460.5 1252.96  36
   7  -4   6 80790.9 1217.86  17
  -7   4  -6 80267.1 1216.07  23
   7  -4   6 81698.9 1205.74   3
   7   4   6 77270.0 1212.21   3
   7   4   7 2582.58 225.935  29
  -7   4  -7 2642.12 149.892  23
   7  -4   7 2863.80 216.264  19
   7   4   7 2678.47 212.049  25
   7   4   7 2449.07 183.541  26
   7   4   7 2390.90 169.184  18
   7  -4   7 2474.32 159.311  17
   7  -4   7 2557.17 244.621  32
   7   4   7 2761.75 230.671  35
   7   4   7 2476.00 248.342  36
   7   4   8 15970.1 374.183  29
  -7   4  -8 16161.1 303.412  23
   7  -4   8 16915.0 348.946  19
   7   4   8 17793.2 358.961  25
   7   4   8 15666.3 338.373  26
   7   4   8 16029.4 316.786  18
   7  -4   8 17438.0 397.163  32
   7   4   8 17187.6 388.832  35
   7   4   8 16065.4 380.204  36
   7   4   9 12345.1 317.668  29
   7  -4   9 11776.0 283.742  19
   7   4   9 12427.5 328.675  35
   7   4   9 12026.5 328.445  36
   7   4   9 12319.8 303.238  25
   7  -4   9 11839.5 331.064  32
   7   4  10 2779.94 223.404  35
   7   4  10 3104.25 233.483  36
   7  -4  10 2631.99 222.551  32
   7   4  10 2641.91 212.212  25
   7  -4  10 2446.62 172.375  19
   7   4  11 3711.41 187.758  25
  -7   4 -11 2961.16 109.484  20
   7   4  12 16421.8 286.565  25
   7   4  12 16082.4 303.437  29
   7   4  13 1671.86 88.9365  29
   7  -4  13 1522.22 80.7601  29
  -7   5  14 15863.6 288.288  34
  -7  -5  13 1718.25 91.7582   5
  -7   5  13 1749.25 164.610  34
  -7  -5  13 1866.92 129.844  15
  -7  -5  13 1953.66 153.133  24
  -7   5  13 2011.86 119.378  11
  -7   5  12 4321.62 204.088  34
  -7  -5  12 3315.72 120.844   5
  -7  -5  11 4511.25 138.957   5
  -7   5  11 5257.50 186.053  11
  -7  -5  10 18284.3 315.545   5
  -7   5  10 18198.7 327.209   5
  -7  -5  10 19133.7 348.735  15
  -7  -5   9 492.505 154.543  15
  -7   5   9 360.664 156.973  11
  -7   5   9 417.251 128.603   5
  -7  -5   9 355.567 110.032   5
  -7  -5   8 35843.4 564.756  15
  -7   5   8 36353.7 566.353  11
  -7   5   7 209.227 189.747   2
  -7   5   7 99.2045 142.863  11
  -7   5   7 68.3822 115.202   5
  -7   5   7-115.223 187.810   7
  -7   5   6 2548.54 147.812  11
  -7   5   6 2410.91 207.382   2
   7   5  -6 2113.44 194.704   1
  -7   5   6 2315.92 214.031   7
  -7   5   5 10082.6 213.257  11
  -7   5   5 9645.02 293.780   2
   7   5  -5 9106.78 284.827   1
  -7   5   5 9820.40 310.372   7
   7  -5  -4 10374.7 280.100   1
   7   5  -4 10033.2 295.582   1
  -7   5   4 10010.1 316.851   7
  -7   5   4 10477.6 210.759  11
  -7   5   4 10134.7 344.783  10
   7  -5  -3 3736.42 193.927   1
   7   5  -3 4008.01 217.419   1
   7   5  -3 3868.27 131.361   4
  -7   5   3 3726.47 127.981  11
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   7   5  -2 70039.0 1133.30   1
   7   5  -2 70113.5 1044.97   4
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   7  -5  -1 1383.52 154.439   1
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   7   5   4 111003. 1644.00  18
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   7   8   7 754.555 176.047  26
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   7   9   1 39624.7 669.449  33
   7   9   1 39062.4 647.471  22
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   8   0  -6 77526.0 1277.03   1
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   8   0   3 453.607 125.115   4
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   8   1  -4 472.637 209.100   1
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   8   1   0 66351.3 1078.56   1
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   8  -1   0 64466.4 974.117   4
   8   1   0 66010.8 976.965   4
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   8   1   1 4179.37 240.621   1
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   8   1   2 9767.52 213.312   4
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   8   1   2 10088.3 316.998   1
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   8   1   3 1749.99 233.533   1
   8  -1   4 2552.03 228.438   1
   8   1   4 2493.68 236.883   1
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   8   1   4 2825.40 158.490   3
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   8   1   4 3145.32 266.415   9
   8   1   5 2289.68 182.495  29
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   8   1   5 1977.54 232.172   1
   8  -1   5 2256.44 150.513   3
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   8   1   5 2096.25 275.646   9
   8   1   6 4454.94 218.177  29
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   8  -1   6 3839.79 180.346   3
   8   1   6 3983.42 189.427   3
   8   1   6 3768.27 293.110   9
   8   1   6 4746.34 248.259  32
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   8  -1   7 31286.9 507.218   3
   8   1   7 30878.9 511.684   3
   8   1   7 31416.2 517.255  25
   8   1   7 30789.4 544.505  29
   8   1   7 30952.9 560.831  32
   8  -1   7 31406.2 565.068  32
   8   1   8 2591.34 181.204  25
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   8  -1   8 2891.44 262.928  32
   8   1   8 2581.47 144.343  12
   8   1   8 2490.41 225.825  29
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   8   1   9 18304.0 401.759  35
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   8  -1   9 18566.3 331.162  12
   8   1   9 17614.6 382.420  29
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   8   1  10 3781.30 170.151  25
   8   1  10 4442.78 254.038  35
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   8   2  -7 16060.5 416.907   1
   8  -2  -7 15218.8 402.715   1
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   8   2  -6 1827.18 233.759   1
   8  -2  -6 1879.10 219.150   1
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   8  -2  -5 3307.87 226.685   1
   8   2  -5 3364.84 240.173   1
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   8  -2  -4 4417.83 238.936   1
   8   2  -4 5264.45 257.452   1
   8  -2  -3 45660.5 781.480   1
   8   2  -3 47133.4 799.177   1
   8   2  -2 10546.5 314.816   9
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   8   2  -2 11142.4 332.186   1
   8   2  -2 11092.8 227.544   4
   8  -2  -2 10720.5 217.136   4
  -8   2   1 145437. 2261.55  10
   8   2  -1 152094. 2283.03   9
   8  -2  -1 146378. 2246.16   1
   8   2  -1 154173. 2267.93   1
   8   2  -1 151733. 2161.54   4
   8  -2  -1 142523. 2154.91   4
  -8   2   0 17372.1 406.435  10
   8   2   0 17641.6 435.256   9
   8  -2   0 17916.3 398.280   1
   8   2   0 18133.6 418.007   1
   8  -2   0 17031.5 302.592   4
   8   2   0 18784.8 314.059   4
   8   2   1 6107.09 284.866   9
  -8   2  -1 5748.03 246.409  10
   8  -2   1 5358.62 241.079   1
   8   2   1 5521.31 261.592   1
   8  -2   1 5595.97 155.059   4
   8   2   1 5792.43 166.726   4
   8   2   2 975.921 227.946   9
   8  -2   2 852.376 199.767   1
   8   2   2 798.592 218.731   1
   8  -2   2 688.528 115.545   4
   8   2   2 736.094 128.584   4
   8   2   3 14377.6 422.050   9
   8  -2   3 13596.6 256.748   4
   8   2   3 13716.9 267.098   4
   8  -2   3 14160.1 365.665   1
   8   2   3 14577.1 391.911   1
   8   2   4 3869.31 166.192  25
   8   2   4 4122.10 168.315   3
   8  -2   4 4212.65 156.437   3
  -8   2  -4 3513.32 135.581  20
   8  -2   4 3886.32 227.346  32
   8   2   4 3807.97 208.012  36
   8  -2   4 3816.49 237.435   1
   8   2   4 4070.17 258.909   1
   8   2   4 3460.41 179.254  29
   8   2   5 2381.30 186.918  29
   8   2   5 2461.11 169.855  25
   8   2   5 2518.77 212.002   8
   8   2   5 2480.35 273.496   9
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   8   2   5 2339.36 221.182  36
   8   2   5 2276.18 212.747  32
   8  -2   5 2416.28 228.060  32
   8   2   5 2485.64 157.017   3
   8  -2   5 2466.01 146.458   3
   8  -2   5 2124.22 212.403   1
   8   2   5 2138.65 231.679   1
   8  -2   6 10528.2 235.797   3
   8   2   6 10590.0 246.489   3
   8   2   6 10001.0 317.772  36
   8   2   6 10303.7 276.079  29
   8   2   6 10451.5 255.850  25
   8   2   6 10276.8 299.024  32
   8   2   7 3024.26 195.282  25
   8   2   7 3057.17 176.303   3
   8  -2   7 3048.81 165.861   3
   8   2   7 2724.82 222.319  29
   8   2   7 2929.35 245.216  32
   8  -2   7 2941.00 263.884  32
   8   2   8 5815.38 271.704  35
   8   2   8 5780.76 268.324  32
   8  -2   8 5630.24 273.508  32
   8   2   8 5619.41 218.979  25
   8   2   8 5693.88 250.801  29
   8  -2   8 5072.50 230.559  29
   8   2   9 10315.0 325.202  35
   8   2   9 10785.3 332.628  36
   8  -2   9 10388.4 308.945  32
   8   2   9 10348.9 297.722  29
   8   2   9 9816.49 255.391  25
   8   2  10 3388.22 172.012  25
   8   2  10 3106.98 239.331  35
   8   2  10 3065.91 253.722  36
   8  -2  10 2944.16 210.322  32
   8   2  10 3181.14 221.298  29
   8  -2  10 2849.88 199.150  29
   8   2  11 24436.1 412.946  35
   8   2  11 25034.1 422.072  36
   8  -2  11 21256.4 361.895  12
   8   2  11 20632.2 367.669  25
   8   2  11 24278.1 408.638  29
   8  -2  11 21703.2 391.019  29
   8   2  12 449.957 128.308  29
   8  -2  12 291.234 114.359  29
   8  -2  13 175.938 61.8374  36
   8   2  13 213.074 57.8183  29
   8   3 -15 1182.01 79.9675  31
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  -8   3  11 119.726 144.526   5
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  -8   3   8 4550.66 173.395   5
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   8   3  -7 1530.35 218.287   1
  -8   3   7 1642.49 239.528   2
   8  -3  -7 1513.33 204.084   1
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  -8   3   6 1777.72 137.184   5
  -8   3   6 1887.33 238.748  10
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  -8   3   6 1551.54 229.095   2
   8  -3  -6 1865.43 206.218   1
   8   3  -6 1728.62 220.990   1
  -8   3   5 14986.0 404.306  10
   8   3  -5 14664.0 376.949   1
  -8   3   4 30975.8 621.050  10
   8  -3  -4 30384.9 585.790   1
   8   3  -4 31518.8 607.731   1
  -8   3   3 911.295 204.787  10
   8  -3  -3 1028.68 190.407   1
   8   3  -3 1031.59 210.051   1
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   8   3  -2 7481.62 272.786   9
   8   3  -2 8526.69 194.187   4
   8  -3  -2 7874.35 181.248   4
   8  -3  -2 7805.31 266.856   1
   8   3  -2 8042.20 287.997   1
  -8   3   1 14172.8 381.261  10
   8   3  -1 13559.2 373.383   9
   8  -3  -1 14448.8 260.632   4
   8   3  -1 15041.7 272.510   4
   8  -3  -1 14555.0 355.831   1
   8   3  -1 15427.0 381.036   1
  -8   3   0 23292.1 503.232  10
   8   3   0 24122.3 515.021   9
   8  -3   0 22864.7 379.831   4
   8   3   0 24653.8 391.826   4
   8  -3   0 21918.3 458.270   1
   8   3   0 23439.6 488.583   1
  -8   3  -1 63155.4 1085.49  10
   8   3   1 64708.7 1105.28   9
   8  -3   1 63169.4 964.020   4
   8  -3   1 62076.1 1047.23   1
   8   3   1 64270.2 1073.84   1
   8   3   2 7687.96 317.614   9
   8  -3   2 7775.72 270.627   1
   8   3   2 8661.96 300.681   1
   8  -3   2 7761.90 179.674   4
   8   3   2 8409.05 195.982   4
   8   3   3 580.529 134.892   3
   8   3   3 451.556 214.846   9
  -8   3  -3 609.123 121.069  20
   8   3   3 390.689 199.092  36
   8   3   3 514.510 174.051  35
   8   3   3 548.096 191.809  32
   8  -3   3 568.642 190.918  32
   8  -3   3 553.678 184.331   1
   8   3   3 567.244 212.265   1
   8   3   4 2508.65 183.819  29
   8   3   4 2501.07 163.624  25
   8  -3   4 2499.56 135.447   3
   8   3   4 2485.83 152.031   3
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   8  -3   4 2428.01 200.739  19
   8   3   4 2651.73 219.224  36
   8   3   4 2499.88 206.417  35
   8  -3   4 2416.40 161.573  17
   8  -3   4 2550.11 228.946  32
   8  -3   4 2135.75 207.486   1
   8   3   4 2158.72 231.476   1
   8   3   5 85124.7 1288.02  29
   8   3   5 86251.5 1275.60  25
   8   3   5 79323.8 1390.87   8
   8   3   5 81944.8 1430.72   9
  -8   3  -5 82197.7 1264.08  20
   8  -3   5 85797.9 1284.62  19
   8   3   5 83663.0 1297.13  32
   8  -3   5 83924.5 1306.57  32
   8  -3   5 85871.1 1265.30  17
   8  -3   5 84433.4 1254.70   3
   8   3   5 88184.8 1266.52   3
   8   3   5 81670.0 1302.41  35
   8   3   5 81323.6 1300.63  36
  -8   3  -6 4262.71 161.406  20
   8  -3   6 4823.44 230.940  19
   8   3   6 4957.36 209.549  25
   8   3   6 5225.44 235.826  29
   8   3   6 5101.57 261.810  35
   8  -3   6 4370.75 162.889   3
   8   3   6 4338.30 182.246   3
   8   3   7 1982.89 196.869  25
   8  -3   7 1616.73 246.116  32
   8   3   7 1499.36 219.041  29
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  -8   3  -8 472.050 120.973  20
   8   3   8 427.688 259.062  36
   8   3   8 300.057 256.307  35
   8   3   8 497.738 186.990  25
   8   3   8 455.992 174.144  26
   8   3   8 436.758 222.953  29
   8  -3   8 417.153 246.603  32
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   8   3   9-57.7123 251.615  36
   8   3   9 3.97531 234.241  35
   8  -3   9 190.463 228.691  32
   8   3   9-78.1245 218.947  29
   8  -3   9-54.3052 177.419  29
   8   3   9-44.4307 180.631  25
   8   3  10 22090.3 393.662  25
   8   3  10 23777.4 438.011  35
   8   3  10 24428.2 439.827  36
   8  -3  10 22856.2 422.666  32
   8   3  10 24297.6 427.356  29
   8  -3  10 20892.7 399.549  29
   8  -3  10 21649.6 375.629  12
   8  -3  11 18495.2 286.818  12
   8   3  11 17584.8 326.392  29
   8  -3  11 15213.4 306.594  29
   8   3  11 16010.8 295.495  25
   8   3  11 16102.0 333.818  36
   8   3  12 1794.49 117.526  29
   8  -3  12 1346.21 97.8215  29
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  -8   4  10 116.127 149.956  11
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  -8   4   8 3936.07 162.052   5
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   8  -4  -6 4698.53 232.033   1
   8   4  -6 4943.48 251.584   1
  -8   4   5 50159.5 752.957  11
   8   4  -5 48348.6 859.813   1
  -8   4   5 51067.5 910.938  10
  -8   4   4 502.747 101.711  11
  -8   4   4 494.492 222.539  10
   8  -4  -4 398.715 180.253   1
   8   4  -4 345.527 201.758   1
   8  -4  -3 12170.5 234.839   4
   8   4  -3 12926.0 247.738   4
   8  -4  -3 12577.3 324.085   1
   8   4  -3 12957.5 352.492   1
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   8   4  -2 37075.2 693.540   9
   8  -4  -2 36237.1 577.601   4
   8   4  -2 39417.7 588.338   4
   8  -4  -2 35944.8 660.141   1
   8   4  -2 38471.4 690.277   1
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   8   4  -1 900.695 195.280   9
   8  -4  -1 978.292 105.770   4
   8   4  -1 1069.87 125.855   4
   8  -4  -1 973.303 169.839   1
   8   4  -1 1077.56 196.959   1
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   8   4   0 1780.20 214.706   9
   8  -4   0 1604.93 109.826   4
   8   4   0 1637.39 128.967   4
   8  -4   0 1694.96 181.753   1
   8   4   0 1754.22 206.197   1
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   8   4   1 42676.0 789.910   9
   8  -4   1 40972.4 729.314   1
   8   4   1 43375.0 761.261   1
   8  -4   1 40612.9 641.556   4
   8   4   1 43345.3 653.069   4
   8  -4   2 15426.4 268.327   4
   8   4   2 15735.4 282.916   4
   8   4   2 14949.4 427.355   9
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   8  -4   2 15072.3 319.086  19
   8  -4   2 16141.3 368.707   1
   8   4   2 16398.3 398.838   1
   8  -4   2 16417.8 314.958  17
   8  -4   2 14070.5 325.485  32
   8   4   2 13998.8 314.052  35
   8   4   2 14126.7 331.030  36
   8   4   3 5731.06 210.975  29
   8   4   3 7231.51 183.005   3
   8  -4   3 7421.66 167.800   3
   8   4   3 6514.59 304.121   9
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   8  -4   3 6483.22 233.584  19
   8  -4   3 6923.22 246.740   1
   8   4   3 6904.26 272.679   1
   8  -4   3 6703.85 210.538  17
   8  -4   3 5260.90 247.326  32
   8   4   3 5190.62 221.590  35
   8   4   3 4802.44 244.927  36
   8   4   4 1627.58 181.876  29
   8  -4   4 1003.81 119.564   3
   8   4   4 1100.00 137.854   3
   8   4   4 1066.79 242.107   8
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   8   4   4 1761.19 211.927  35
   8   4   4 1796.70 224.419  36
   8  -4   4 1259.99 170.385  17
   8   4   4 810.905 198.941   1
   8  -4   4 956.335 172.449   1
   8  -4   4 1828.27 217.825  32
   8   4   5 8218.36 235.852  25
   8  -4   5 8244.03 197.906   3
   8   4   5 8427.47 212.927   3
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   8  -4   5 8285.02 263.688  19
   8  -4   5 8126.26 291.962  32
   8  -4   5 8078.16 225.879  17
   8   4   5 8444.24 261.409  29
   8   4   5 8269.80 288.131  35
   8   4   6 10707.2 266.215  25
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   8  -4   6 10260.8 284.796  19
   8  -4   6 9840.27 215.291   3
   8   4   6 9519.09 228.756   3
   8  -4   6 9829.67 240.340  17
   8   4   6 9628.09 225.221  16
   8   4   6 10471.6 292.282  29
   8   4   6 9978.97 303.289  35
   8   4   7 25952.9 507.954  36
   8   4   7 25693.0 459.041  18
  -8   4  -7 25801.5 442.251  20
   8  -4   7 26976.9 476.607  19
   8   4   7 27091.7 470.296  25
   8   4   7 26678.5 477.634  26
   8   4   7 26300.5 487.581  29
   8   4   8 18251.4 413.019  35
   8   4   8 18955.0 413.174  36
   8   4   8 17933.4 340.702  18
   8  -4   8 19009.9 412.137  32
   8   4   8 19310.6 390.745  29
   8   4   8 19215.6 365.352  25
   8   4   8 17853.7 363.813  26
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   8   4   9 6645.81 264.891  35
   8   4   9 6378.87 273.534  36
   8  -4   9 6380.89 260.143  32
   8   4   9 6603.06 254.624  29
   8   4   9 6192.11 214.711  25
   8   4  10 1066.02 152.854  25
   8  -4  10 1211.21 189.447  32
   8   4  10 1068.27 191.491  29
   8  -4  10 837.460 147.751  29
  -8   4 -10 882.476 90.8263  20
   8   4  10 1125.48 196.038  35
   8   4  10 1209.83 204.412  36
   8  -4  10 937.560 116.517  12
   8   4  11 1499.55 156.852  29
   8  -4  11 1259.15 116.422  29
   8  -4  12 7379.75 156.414  36
   8  -4  12 4315.83 106.889  29
   8   5 -14 37.2461 87.8852  31
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  -8   5  12 17.6548 110.840  11
  -8   5  12 247.556 158.248  34
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  -8   5  11 3672.45 151.394  11
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  -8   5   9 10336.5 221.393   5
  -8   5   9 11165.4 244.058  11
  -8  -5   9 11472.6 249.057  15
  -8   5   8 7035.30 197.851  11
  -8  -5   8 6699.31 164.974   5
  -8   5   8 6549.23 179.647   5
  -8   5   7 35036.7 535.416  11
  -8   5   7 31324.3 519.632   5
  -8   5   6 13146.1 406.447  10
  -8   5   6 12863.1 252.438   5
  -8   5   5 19383.1 335.031  11
  -8   5   5 19034.5 327.178   5
  -8   5   5 18494.4 424.280   2
   8  -5  -4 18011.1 309.824   4
   8   5  -4 18465.5 319.826   4
  -8   5   4 18705.1 472.171  10
  -8   5   4 18744.4 317.233  11
   8   5  -3 33264.7 632.031   1
  -8   5   3 35686.0 697.393  10
  -8   5   3 35387.2 667.101   7
   8  -5  -3 34068.9 572.498  17
   8   5  -3 34794.0 556.080  18
   8   5  -3 35906.7 544.179   4
   8  -5  -3 33877.3 534.818   4
  -8   5   2 5173.48 285.486  10
   8   5  -2 4502.74 228.959   9
   8   5  -2 3969.13 216.258   1
  -8   5   2 5449.75 172.263  20
   8  -5  -2 5326.52 206.453  17
   8   5  -2 5584.95 172.113  18
   8  -5  -2 4387.84 132.019   4
   8   5  -2 4384.48 145.807   4
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   8   5  -1 1364.68 201.900   9
   8   5  -1 1444.77 182.408   1
   8  -5  -1 1523.82 179.164  17
   8   5  -1 1471.87 140.019  18
   8  -5  -1 1520.66 103.197   4
   8   5  -1 1577.19 119.166   4
   8   5   0 11638.6 354.988   9
  -8   5   0 11741.6 247.863  20
   8   5   0 11122.6 317.542   1
   8  -5   0 11445.1 216.588   4
   8   5   0 11937.7 230.075   4
   8   5   0 12077.9 254.014  18
   8   5   1 5653.14 206.781  35
   8   5   1 6333.20 191.853  18
   8   5   1 6517.34 251.825   1
  -8   5  -1 7241.30 305.176  10
   8   5   1 6434.07 286.143   9
  -8   5  -1 6814.79 188.337  20
   8  -5   1 6188.50 146.715   4
   8   5   1 6453.61 163.389   4
   8   5   1 5306.23 194.003  29
   8   5   2 35273.7 579.585  35
   8   5   2 36228.4 584.704  36
   8  -5   2 35711.2 566.362  17
   8   5   2 34507.8 561.121  18
   8   5   2 32742.3 681.861   9
  -8   5  -2 35828.8 556.266  20
   8  -5   2 34827.9 572.596  19
   8   5   2 34805.4 564.010  29
   8  -5   2 32494.7 524.072   3
   8   5   2 32255.0 531.568   3
   8   5   3 80757.5 1405.85   9
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   8  -5   3 86595.8 1277.67  19
   8   5   3 82228.4 1285.66  35
   8   5   3 83240.1 1288.69  36
   8  -5   3 87540.1 1269.24  17
   8   5   3 83568.6 1271.76  29
   8  -5   3 82361.6 1236.08   3
   8   5   3 81858.1 1242.14   3
   8  -5   4 510.040 112.815   3
   8   5   4 492.469 129.192   3
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   8   5   4 386.041 208.912  35
   8   5   4 213.664 155.839  18
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   8   5   4 201.291 193.573  29
   8   5   4 259.242 174.448  26
   8   5   5 220.455 194.291  29
   8   5   5 192.816 182.341  26
   8   5   5 175.594 153.711  22
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   8   5   5 435.768 134.814  16
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   8   5   5 236.321 153.748  18
   8  -5   5 371.512 111.589   3
   8   5   5 218.543 125.368   3
   8   5   5 122.702 223.528  35
   8   5   6 399.342 196.390  26
   8   5   6 176.107 145.836  22
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   8   5   6 405.446 128.950  16
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   8   5   7 4029.69 269.089  36
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   8   5   8 4038.82 255.922  35
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   8   6  -2 49342.5 765.024  18
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   8   6  -1 17740.7 334.897  18
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   8   6   0 2510.46 230.828   9
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   8   6   0 3156.39 180.581  26
   8   6   1 428.805 161.751  18
   8   6   1 481.268 213.730   9
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   8  -6   2 2550.65 210.836  19
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   8   6   2 2561.56 192.974  26
   8   6   3 5084.06 192.502  16
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   8   6   3 5282.32 223.700  26
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   8  -6   4 43436.7 723.945  19
   8   6   4 45236.7 722.327  22
   8   6   4 42344.8 718.814  29
   8   6   4 43631.2 704.057  16
   8  -6   4 45389.3 712.946  17
   8   6   4 44077.6 708.884  18
   8   6   5 4854.13 233.170  26
   8   6   5 4700.76 201.588  22
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   8   6   5 4369.74 178.407  16
   8   6   5 4424.32 192.366  18
   8   6   5 4921.00 229.547  29
   8   6   5 4863.23 250.429  35
   8   6   5 5048.02 266.511  36
   8   6   6 10362.7 281.045  26
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   8   6   6 9232.72 240.299  18
   8   6   6 9968.14 280.736  29
   8   6   6 10214.9 308.172  36
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   8   6   7 4915.04 182.319  18
   8   6   7 5615.46 219.686  26
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   8   6   8 7171.36 242.898  29
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   8  -6   8 6724.66 232.957  19
   8  -6   9 4693.41 217.842  32
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   8  -6  10 1609.36 90.9645  12
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   8   7  -5 263.861 122.020  16
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   8   7  -4 22780.7 399.058  16
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   8   7  -3 3974.62 168.965  16
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   8   7  -2 8173.38 213.385  16
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   8   7  -1 3149.76 177.461  18
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   8   7  -1 2855.52 162.927  16
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   8   7   0 6247.55 217.980  26
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   8   7   0 5958.32 203.584  16
   8   7   0 6507.89 207.408  18
   8  -7   0 6231.85 235.473  17
   8   7   1 3675.94 203.731  26
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   8  -7   1 3769.67 222.614  17
   8   7   1 3729.67 190.617  18
   8  -7   2 12896.3 310.008  19
   8   7   2 13563.7 291.834  21
   8   7   2 13518.6 308.483  22
   8   7   2 13614.5 309.857  26
   8   7   2 12606.5 283.908  16
   8  -7   3 1428.07 212.122  19
   8   7   3 1459.40 159.567  21
   8   7   3 1421.63 194.235  22
   8   7   3 1410.68 186.102  33
   8   7   3 1428.03 197.734  26
   8   7   3 1505.11 181.220  18
   8   7   3 1604.20 166.485  16
   8   7   4 26221.3 458.605  22
   8   7   4 23661.4 432.942  16
   8  -7   4 24779.9 448.258  17
   8   7   4 25061.1 440.423  18
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   8  -7   4 24202.3 461.421  19
   8   7   5 734.542 199.425  26
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   8  -7   5 748.554 211.491  19
   8   7   5 758.990 169.798  22
   8   7   5 721.051 213.108  29
   8   7   5 560.297 164.895  18
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   8   7   6 11403.9 285.773  26
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   8   7   6 10672.2 255.807  22
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   8   7   6 11887.9 295.831  29
   8  -7   6 11203.7 262.224  17
   8   7   6 11137.7 253.702  18
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   8  -7   7 16205.7 316.784  17
   8  -7   7 18478.7 389.836  32
   8   7   7 17190.0 340.194  26
   8   7   7 17901.2 355.224  29
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   8  -7   9 790.374 167.544  32
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   8   8  -5 37784.1 613.778  22
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   8   8  -4 1050.09 149.526  22
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   8   8   3 994.010 194.419  33
   8   8   3 900.432 180.213  22
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   8   8   4 1795.11 184.688  22
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   8   8   5 13981.5 299.527  22
   8  -8   5 14212.4 300.191  17
   8   8   5 13251.5 272.451  16
   8  -8   6 459.040 233.157  32
   8   8   6 547.611 174.772  26
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   8  -8   9 629.996 125.705  32
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   8   9  -7 4504.18 185.504  33
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   8   9  -5 790.783 194.994  33
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   8   9  -1 1013.02 162.516  22
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   8  -9  -1 899.570 188.510  17
   8   9   0 25905.3 465.544  22
   8   9   0 26588.8 495.688  33
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   8   9   0 27460.8 478.444  21
   8   9   0 26516.5 466.711  26
   8  -9   0 26112.9 469.706  17
   8   9   0 26518.9 457.442  16
   8   9   1 5478.45 219.773  22
   8   9   1 6011.67 248.124  33
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   8  -9   1 5728.03 228.482  17
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   8   9   2 1054.31 157.429  16
   8   9   3 11321.5 274.951  22
   8   9   3 11419.6 256.054  21
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   8   9   3 11464.2 278.866  26
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   8  -9   3 11489.7 277.336  17
   8   9   3 11340.5 248.842  16
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   8   9   4 1316.32 172.226  22
   8   9   5 122.164 151.059  22
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   8   9   5 193.293 170.772  26
   8  -9   5 121.110 163.275  17
   8  -9   5-131.476 212.553  32
   8   9   6 14239.1 287.501  26
   8  -9   6 13932.3 274.164  17
   8  -9   6 14676.5 322.031  32
   8   9   7-12.4552 118.702  26
   8  -9   7 115.016 169.600  32
   8  -9   7 77.3296 112.931  17
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   8  -9   9 2355.93 98.7883  32
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   8  10  -9 2447.93 77.9218  21
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   8  10  -8 10603.1 200.374  21
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   8  10  -7 7007.66 180.076  33
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   8  10  -6 2407.68 164.453  33
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   8  10  -5 1194.17 182.080  33
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   8  10  -4 1873.88 122.685  22
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   8  10  -3 11156.9 262.585  21
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   8  10  -3 9855.68 289.774  33
   8  10  -3 10259.8 231.517  22
   8 -10  -2 26502.9 457.228  17
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   8  10  -2 27624.3 500.162  33
   8  10  -2 27077.8 460.951  22
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   8 -10  -1 10989.8 253.482  17
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   8  10  -1 11501.6 254.513  22
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   8 -10   0 236.747 171.031  17
   8  10   0 237.093 175.432  21
   8  10   0 337.260 152.009  26
   8  10   0 449.242 203.163  33
   8  10   1 342.359 164.073  22
   8 -10   1 273.762 169.433  17
   8  10   1 142.001 164.143  21
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   8  10   1 248.614 155.576  26
   8  10   1 247.090 192.763  33
   8  10   2 3637.08 187.387  22
   8  10   2 3825.57 175.274  21
   8 -10   2 3665.69 192.499  17
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   8 -10   3 735.661 165.275  17
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   8  10   3 774.640 164.400  26
   8  10   3 770.590 133.251  21
   8  10   3 498.313 159.100  22
   8  10   4 11987.9 253.838  22
   8 -10   4 12063.5 254.990  17
   8  10   4 11550.2 261.060  26
  -8  10  -4 11436.1 223.989  20
   8 -10   4 11997.4 275.962  32
   8 -10   5 10816.7 253.597  32
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   9   3   1 14690.1 385.532   1
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   9   3   3 8796.67 263.815  35
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   9  -3   4 848.048 128.841   3
   9   3   4 987.757 148.352   3
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   9  -3   4 1160.60 244.744  32
   9   3   4 1642.56 227.425  35
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   9  -3   5 15711.9 296.652   3
   9   3   5 16350.4 310.899   3
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   9   3   5 16383.2 342.228  29
   9  -3   5 15734.9 307.696  17
   9  -3   5 17243.3 382.080  32
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   9   3   7 29630.1 513.472  26
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   9   7   1 5976.40 205.891  21
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   9   7   2 11610.4 287.415  26
   9   7   2 11524.3 259.613  21
   9   7   2 11255.3 270.732  18
   9   7   2 11016.0 260.372  16
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   9  -7   2 11655.6 306.506  32
   9   7   3 808.751 184.898  22
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   9  -7   3 883.699 228.291  32
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   9   7   4 875.408 170.464  18
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   9   7   5 5080.56 189.033  22
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   9   7   5 4757.28 166.510  16
   9   7   5 5315.68 193.533  18
   9  -7   5 6308.35 266.027  32
   9   7   5 6279.62 226.087  26
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   9  -7   6 7570.05 202.022  17
   9   7   6 7952.40 227.997  26
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   9   7   7 3910.54 165.217  26
   9  -7   7 3709.33 212.237  32
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   9  -7   9 7896.48 169.002  32
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   9   8  -8 338.291 135.213  33
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   9   8  -4 7033.33 200.868  22
   9   8  -4 7320.34 190.565  16
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   9   8  -3 8494.32 226.266  22
   9   8  -3 8947.01 218.911  16
   9   8  -2 2200.83 176.492  22
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   9   8  -2 2588.72 166.811  16
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  13  -1   1 358.443 97.4973  18
  13  -1   2 4225.07 103.398   3
  13   1   2 4139.69 104.404   3
  13  -1   2 4185.63 131.657  18
  13   1   2 4296.69 136.180  18
  13  -1   3 1377.06 66.9037   3
  13   1   3 1438.59 70.0585   3
  13  -1   3 1231.75 98.9301  18
  13   1   3 1227.11 101.484  18
  13   1   4 1424.48 96.4485  18
  13  -1   4 1455.24 94.3297  18
  13   1   5 6805.25 128.250  18
  13  -1   5 6621.32 126.450  18
  13   1   5 6499.52 137.694  26
 -13   2   9 1688.38 47.8842   5
 -13  -2   9 1651.75 58.9479  15
 -13  -2   8 622.482 56.4339   5
 -13   2   8 608.253 58.8921   5
 -13  -2   8 734.022 69.4775  15
 -13  -2   7 228.633 67.4493   5
 -13   2   7 249.331 68.4063   5
  13  -2  -6 13114.5 216.856   4
  13   2  -6 13496.2 218.137   4
 -13  -2   6 13749.6 222.911   5
 -13   2   6 13693.0 224.129   5
 -13  -2   5 1012.55 85.5324   5
 -13   2   5 1022.03 88.6531   5
  13  -2  -5 931.328 69.7879   4
  13   2  -5 918.191 74.5195   4
  13   2  -5 692.802 80.4050  16
  13  -2  -4 18.6868 70.9001   4
  13   2  -4 9.62841 73.6637   4
 -13  -2   4 1.36156 88.3097   5
 -13   2   4 118.080 93.5362   5
  13  -2  -3 881.952 75.2145   4
  13   2  -3 817.128 77.5564   4
 -13   2   3 970.378 97.5089   5
 -13  -2   3 913.661 93.7077   5
  13  -2  -2 1558.29 80.5185   4
  13   2  -2 1552.02 82.9892   4
  13   2  -2 1618.60 112.420  26
  13   2  -1 1419.06 125.397  26
  13  -2  -1 1372.31 80.2236   3
  13   2  -1 1327.55 83.4773   3
  13   2  -1 1385.80 94.8999  18
  13  -2   0 27474.5 413.252   3
  13   2   0 28263.0 415.616   3
  13   2   1 5290.63 173.151  26
  13  -2   1 5785.71 116.704   3
  13   2   1 6075.34 121.122   3
  13   2   1 5419.08 146.741  18
  13  -2   2 1069.34 69.5538   3
  13   2   2 1078.91 72.8108   3
  13   2   2 1190.98 108.447  18
  13   2   3 6197.21 168.774  26
  13  -2   3 6002.97 113.708   3
  13   2   3 5852.74 130.078  16
  13   2   3 6281.10 143.911  18
  13  -2   4 1190.93 78.8615  18
  13   2   4 1212.46 88.9965  18
  13   2   5 521.686 62.5603  18
  13  -2   5 519.967 57.4516  18
  13   2   5 463.609 73.5605  26
 -13  -3   9 538.111 38.1158  15
 -13  -3   8 3796.59 74.6175   5
 -13  -3   8 4249.92 89.5823  15
 -13  -3   7 1283.34 59.5957   5
 -13  -3   7 1405.77 75.3099  15
 -13  -3   6 4569.75 99.1159   5
 -13  -3   5 5631.67 113.567   5
 -13   3   5 5783.69 115.144   5
  13  -3  -5 5325.16 104.479   4
  13   3  -5 5412.51 105.976   4
 -13  -3   4 5414.03 115.996   5
 -13   3   4 5478.28 117.622   5
  13   3  -4 4512.60 127.351  16
  13  -3  -4 4803.91 102.967   4
  13   3  -4 5006.14 105.852   4
  13  -3  -3 353.062 61.7999   4
  13   3  -3 369.694 65.8994   4
 -13  -3   3 482.496 79.9764   5
 -13   3   3 347.206 81.9552   5
  13   3  -2 995.352 99.1381  26
  13  -3  -2 843.873 67.1003   3
  13   3  -2 863.760 70.5982   3
 -13  -3   2 924.822 82.1007   5
  13  -3  -1 6325.97 126.163   3
  13   3  -1 6662.49 129.093   3
  13   3  -1 6754.84 168.406  26
  13   3   0 6973.93 185.470  26
  13  -3   0 7977.78 138.838   3
  13   3   0 8162.74 141.418   3
  13   3   0 7265.35 164.307  18
  13  -3   1 1540.30 65.8442   3
  13   3   1 1397.33 101.575  18
  13   3   2 56.6198 96.1527  18
  13   3   2 188.063 87.3247  16
  13   3   2 62.5049 121.358  26
  13   3   3 5268.17 128.368  18
  13   3   3 5193.75 152.859  26
  13   3   4 558.720 75.8273  18
  13   3   4 622.423 92.8967  26
  13   3   5 883.018 53.7682  18
  13  -3   5 819.219 48.1308  18
  13   3   5 870.986 61.5001  26
 -13  -4   8 3011.75 65.3382  15
 -13  -4   7 139.777 51.4211  15
 -13  -4   6 1739.40 70.7948  15
 -13  -4   6 1746.51 54.5682   5
 -13  -4   5 575.819 64.8172  15
 -13  -4   5 630.981 52.8754   5
  13   4  -4 4327.41 114.314  16
 -13  -4   4 4498.15 92.4706   5
  13   4  -3 12215.1 215.477  16
 -13  -4   3 11868.0 193.369   5
  13   4  -2 26845.4 398.837  16
 -13  -4   2 24109.5 374.824   5
  13   4  -1 227.986 100.312  16
 -13  -4   1 263.934 58.6441   5
  13   4  -1 286.844 96.7869  26
  13   4   0 543.363 102.453  26
  13   4   0 636.755 100.327  16
  13   4   1 584.280 96.6120  22
  13   4   1 574.786 108.927  26
  13   4   2 4668.64 118.965  18
  13   4   2 4639.26 114.459  16
  13   4   2 4366.45 136.116  26
  13   4   3 458.640 72.4078  18
  13   4   3 535.967 90.9899  26
  13   4   4 7650.76 150.406  26
  13   5  -6 1417.78 58.2264  22
  13   5  -5 206.356 74.3593  22
  13   5  -4 14130.3 226.666  22
  13   5  -4 11824.7 208.472  16
  13   5  -3 1047.40 77.2804  16
  13   5  -2 3515.93 122.970  22
  13   5  -2 3521.91 107.187  16
  13   5  -1 237.930 86.5157  16
  13   5  -1 143.832 69.1082  26
  13   5   0 302.505 91.9063  22
  13   5   0 326.405 86.1968  16
  13   5   0 198.661 84.4910  26
  13   5   1 1002.58 83.2436  22
  13   5   1 920.246 85.9223  26
  13   5   2 5201.52 107.498  16
  13   5   2 4636.45 125.366  26
  13   5   3 3167.09 90.5459  26
  13   6  -6 474.981 63.7757  33
  13   6  -5 7545.95 130.338  22
  13   6  -4 1426.10 76.0136  22
  13   6  -4 1851.13 100.256  33
  13   6  -3 9707.00 192.672  33
  13   6  -3 8949.46 166.695  16
  13   6  -2 2261.90 96.0942  22
  13   6  -2 2032.52 80.1859  16
  13   6  -1 2505.31 86.1047  16
  13   6   0 81.4227 70.3472  22
  13   6   0 97.6804 65.5281  16
  13   6   0 41.0787 50.3355  26
  13   6   1 3077.59 81.6405  22
  13   6   1 2421.21 76.8736  26
  13   6   2 693.648 43.9640  16
  13   6   2 670.583 52.8836  26
  13   7  -4 1403.02 62.4653  33
  13   7  -3 96.3788 41.5915  22
  13   7  -3 120.518 54.6167  33
  13   7  -2 258.931 49.1912  22
  13   7  -1 1380.66 59.1250  22
 -14   0   7-0.18850 28.4545   5
 -14   0   6 669.403 45.4707   5
 -14   0   5-14.4172 51.6229   5
 -14   0   4 7999.04 138.432   5
 -14   0   3 9.51481 60.7798   5
 -14   0   2 278.443 61.7608   5
  14   0  -1-2.62373 65.2022  26
 -14   0   1-16.4409 56.7904   5
  14   0   0 2633.46 92.3858  26
  14   0   1 76.8591 75.7613  26
  14   0   2 1557.33 77.4818  26
  14   0   3 14.6320 46.3520  26
 -14  -1   7 204.275 31.6352  15
 -14  -1   6 199.034 40.2697   5
 -14  -1   5 6562.34 114.568   5
  14   1  -4 929.984 55.3196  16
 -14  -1   4 1355.95 57.6876   5
 -14  -1   3 6036.36 114.490   5
 -14  -1   2 17584.4 271.033   5
  14   1  -1 1240.14 70.5633  26
 -14  -1   1 1589.91 63.8665   5
  14   1   0 539.246 75.9114  26
  14   1   1 1832.47 84.9535  26
  14   1   2 3394.93 90.4996  26
  14  -1   2 3288.69 90.6500  26
  14  -1   3 4560.60 90.9141  26
 -14  -2   6 334.421 36.7982  15
 -14   2   6 387.152 31.8733   5
 -14  -2   6 354.434 30.2886   5
 -14  -2   5 7868.20 129.510   5
 -14   2   5 8189.62 129.933   5
 -14  -2   4 664.202 47.9644   5
 -14   2   4 755.886 48.4798   5
  14   2  -3 6712.88 127.305  16
 -14  -2   3 6888.30 119.520   5
 -14   2   3 7086.28 120.125   5
  14   2  -2 493.864 63.9557  16
 -14  -2   2 591.250 50.8688   5
 -14   2   2 542.022 51.1629   5
  14   2  -1 1100.55 71.8377  16
 -14  -2   1 1032.05 53.0910   5
 -14   2   1 1118.47 53.4281   5
  14   2   0 654.976 68.5772  16
 -14   2   0 698.550 45.1171   5
 -14  -2   0 594.091 45.3167   5
  14   2   1 795.747 56.1499  16
 -14  -2  -1 834.169 39.7468   5
  14   2   2 967.294 59.2085  26
  14   2   2 1043.78 42.5709  16
 -14  -3   3 3538.49 66.7778   5
  14   3  -3 3665.41 81.9914  16
 -14  -3   2 1425.89 43.0835   5
  14   3  -2 1829.09 68.2820  16
  14   3  -1 4913.23 105.942  22
  14   3  -1 5283.13 104.008  16
  14   3   0 3200.76 80.6712  16
  14   3   1 1989.43 59.8193  16
  14   4  -4 3034.80 72.0481  22
  14   4  -3 1848.87 67.8394  22
  14   4  -2 2094.84 58.6143  16
  14   4  -1 12353.7 208.104  22
  14   4  -1 13530.3 205.565  16
  14   4   0 849.606 44.5539  16
   0   0   0    0.00    0.00   0
TITL IJ1019a_auto in P2(1)/n
REM P2(1)/n (#14 in standard setting)
CELL 1.54184  11.466647  12.371028  13.581854  90.0000  97.0894  90.0000
ZERR    2.00   0.000132   0.000148   0.000173   0.0000   0.0011   0.0000
LATT  1
SYMM -x+1/2, y+1/2,-z+1/2
SFAC C H N O S Co
UNIT 60.00 72.00 16.00 12.00 8.00 4.00
TREF
HKLF 4
END
;
_shelx_hkl_checksum              64499
_shelx_res_file
;
TITL ij1019_auto in P21/n #14
    ij1019a.res
    created by SHELXL-2016/6 at 10:13:50 on 16-Jun-2023
REM reset to P21/n #14
CELL 1.54184 11.466647 12.371028 13.581854 90 97.0894 90
ZERR 2 0.000132 0.000148 0.000173 0 0.0011 0
LATT 1
SYMM 0.5-X,0.5+Y,0.5-Z
SFAC C H Co N O S
UNIT 60 72 4 16 12 8
EQIV $1 1.5-X,0.5+Y,1.5-Z
EQIV $2 0.5+X,0.5-Y,-0.5+Z
EQIV $3 0.5-X,-0.5+Y,1.5-Z
EQIV $4 -1+X,+Y,+Z
EQIV $5 1-X,-Y,1-Z
EQIV $6 1.5-X,-0.5+Y,1.5-Z
L.S. 10
PLAN  10
TEMP -173
HTAB C11 N2
HTAB C12 S1_$1
HTAB C15 S2_$2
HTAB C21 S2_$3
HTAB C22 S1_$4
HTAB O31 S1_$6
HTAB O31 O11_$5
HTAB C31 S2_$3
BOND $H
HTAB
fmap 2
acta
REM <olex2.extras>
REM <HklSrc "%.\\IJ1019a.hkl">
REM </olex2.extras>
WGHT    0.056300    1.473500
FVAR       4.78103
CO1   3    0.525959    0.091877    0.592922    11.00000    0.02249    0.02112 =
         0.02309   -0.00346    0.00103   -0.00307
N1    4    0.680494    0.138826    0.674190    11.00000    0.02638    0.02781 =
         0.02692   -0.00496   -0.00237   -0.00396
C1    1    0.777436    0.159358    0.703647    11.00000    0.03332    0.02093 =
         0.02130   -0.00184    0.00460    0.00157
S1    6    0.913766    0.187227    0.746064    11.00000    0.02500    0.03774 =
         0.04120   -0.00309   -0.00169   -0.00335
N2    4    0.414321    0.181481    0.671485    11.00000    0.02837    0.02863 =
         0.03022   -0.00623    0.00590   -0.00002
C2    1    0.346339    0.242005    0.696720    11.00000    0.03681    0.02883 =
         0.02223    0.00252    0.00316   -0.00625
S2    6    0.250692    0.328384    0.729941    11.00000    0.05469    0.04152 =
         0.03162    0.00690    0.01524    0.02001
O11   5    0.532733    0.201218    0.479936    11.00000    0.04124    0.02451 =
         0.02567   -0.00003   -0.00160   -0.00834
N11   4    0.586347    0.297204    0.494063    11.00000    0.03244    0.02339 =
         0.02455    0.00254   -0.00134   -0.00319
C11   1    0.569793    0.359186    0.572797    11.00000    0.05141    0.02779 =
         0.03159   -0.00043    0.01131   -0.00540
AFIX  43
H11   2    0.520567    0.334127    0.619345    11.00000   -1.20000
AFIX   0
C12   1    0.623710    0.458678    0.586355    11.00000    0.05752    0.02787 =
         0.03377   -0.00085    0.01024   -0.00832
AFIX  43
H12   2    0.612097    0.501094    0.642635    11.00000   -1.20000
AFIX   0
C13   1    0.694382    0.497196    0.518925    11.00000    0.03972    0.03070 =
         0.02963    0.00576   -0.00284   -0.00602
C14   1    0.709825    0.431188    0.438955    11.00000    0.03785    0.03804 =
         0.03084    0.00338    0.00221   -0.00947
AFIX  43
H14   2    0.758612    0.454784    0.391503    11.00000   -1.20000
AFIX   0
C15   1    0.655228    0.331585    0.427357    11.00000    0.03392    0.03454 =
         0.02747   -0.00014    0.00082   -0.00224
AFIX  43
H15   2    0.666465    0.287397    0.372102    11.00000   -1.20000
AFIX   0
C16   1    0.750602    0.607033    0.533425    11.00000    0.05390    0.03534 =
         0.03179    0.00508   -0.00093   -0.01494
AFIX 137
H16A  2    0.814718    0.613082    0.492246    11.00000   -1.50000
H16B  2    0.781897    0.616432    0.603361    11.00000   -1.50000
H16C  2    0.691764    0.663039    0.514100    11.00000   -1.50000
AFIX   0
O21   5    0.392940    0.020255    0.493266    11.00000    0.02074    0.03214 =
         0.03219   -0.01311   -0.00053   -0.00127
N21   4    0.282158    0.058256    0.482527    11.00000    0.01968    0.02341 =
         0.02913   -0.00513    0.00117   -0.00314
C21   1    0.218562    0.045778    0.558766    11.00000    0.02615    0.02878 =
         0.02931    0.00128    0.00097   -0.00521
AFIX  43
H21   2    0.248923    0.004642    0.615235    11.00000   -1.20000
AFIX   0
C22   1    0.109192    0.093025    0.554393    11.00000    0.02428    0.03619 =
         0.03294   -0.00264    0.00524   -0.00393
AFIX  43
H22   2    0.064668    0.084973    0.608466    11.00000   -1.20000
AFIX   0
C23   1    0.063240    0.152561    0.471322    11.00000    0.02731    0.03024 =
         0.03577   -0.00719   -0.00256   -0.00207
C24   1    0.129922    0.157507    0.392412    11.00000    0.03689    0.02744 =
         0.03170   -0.00077   -0.00120   -0.00096
AFIX  43
H24   2    0.099213    0.193206    0.332881    11.00000   -1.20000
AFIX   0
C25   1    0.239552    0.111368    0.399683    11.00000    0.03296    0.02747 =
         0.02883   -0.00331    0.00463   -0.00436
AFIX  43
H25   2    0.285208    0.117040    0.346108    11.00000   -1.20000
AFIX   0
C26   1   -0.051822    0.211413    0.468268    11.00000    0.03095    0.04593 =
         0.04672   -0.00672   -0.00246    0.00760
AFIX 127
H26A  2   -0.068918    0.248973    0.404593    10.50000   -1.50000
H26B  2   -0.046939    0.264182    0.522437    10.50000   -1.50000
H26C  2   -0.114632    0.159457    0.475782    10.50000   -1.50000
H26D  2   -0.084742    0.199435    0.530615    10.50000   -1.50000
H26E  2   -0.106720    0.184226    0.412771    10.50000   -1.50000
H26F  2   -0.039027    0.288951    0.459426    10.50000   -1.50000
AFIX   0
O31   5    0.495485   -0.040345    0.686908    11.00000    0.04652    0.02351 =
         0.03284   -0.00276    0.00850   -0.00698
AFIX 147
H31   2    0.495536   -0.104304    0.666149    11.00000    0.06083
AFIX   0
C31   1    0.528419   -0.039172    0.791792    11.00000    0.04445    0.03453 =
         0.03302    0.00285    0.00528   -0.00446
AFIX 137
H31A  2    0.611351   -0.059417    0.806657    11.00000   -1.50000
H31B  2    0.479797   -0.090838    0.823227    11.00000   -1.50000
H31C  2    0.516711    0.033542    0.817470    11.00000   -1.50000
AFIX   0
HKLF 4
REM  ij1019_auto in P21/n #14
REM R1 =  0.0376 for    3945 Fo > 4sig(Fo)  and  0.0385 for all    4111 data
REM    231 parameters refined using      0 restraints
END
WGHT      0.0563      1.4735
REM Instructions for potential hydrogen bonds
HTAB C11 N2
HTAB C12 S1_$1
HTAB C15 S2_$2
HTAB C21 S2_$3
HTAB C22 S1_$4
HTAB O31 S1_$6
HTAB O31 O11_$5
HTAB C31 S2_$3
REM Highest difference peak  0.666,  deepest hole -0.570,  1-sigma level  0.064
Q1    1   0.3176  0.3560  0.7436  11.00000  0.05    0.67
Q2    1   0.5631  0.1612  0.6350  11.00000  0.05    0.35
Q3    1   0.6170  0.1220  0.6473  11.00000  0.05    0.33
Q4    1   0.5866  0.1428  0.6501  11.00000  0.05    0.33
Q5    1   0.2201  0.3664  0.6829  11.00000  0.05    0.33
Q6    1   0.4877  0.0889  0.5210  11.00000  0.05    0.32
Q7    1   0.5472  0.1800  0.6135  11.00000  0.05    0.31
Q8    1   0.4799  0.0331  0.5419  11.00000  0.05    0.29
Q9    1   0.5247  0.0877  0.6652  11.00000  0.05    0.28
Q10   1   0.8893  0.1864  0.7968  11.00000  0.05    0.27
;
_shelx_res_checksum              1696
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Co Co1 0.52596(3) 0.09188(3) 0.59292(2) 0.02238(11) Uani d 1 . .
N N1 0.68049(16) 0.13883(15) 0.67419(14) 0.0275(4) Uani d 1 . .
C C1 0.77744(19) 0.15936(17) 0.70365(15) 0.0251(4) Uani d 1 . .
S S1 0.91377(5) 0.18723(5) 0.74606(5) 0.03513(15) Uani d 1 . .
N N2 0.41432(16) 0.18148(15) 0.67148(14) 0.0289(4) Uani d 1 . .
C C2 0.3463(2) 0.24201(18) 0.69672(16) 0.0293(4) Uani d 1 . .
S S2 0.25069(6) 0.32838(5) 0.72994(5) 0.04178(17) Uani d 1 . .
O O11 0.53273(15) 0.20122(12) 0.47994(11) 0.0309(3) Uani d 1 . .
N N11 0.58635(16) 0.29720(15) 0.49406(13) 0.0272(4) Uani d 1 . .
C C11 0.5698(2) 0.3592(2) 0.57280(18) 0.0364(5) Uani d 1 . .
H H11 0.520567 0.334127 0.619345 0.044 Uiso calc 1 . .
C C12 0.6237(3) 0.4587(2) 0.58635(19) 0.0393(6) Uani d 1 . .
H H12 0.612097 0.501094 0.642635 0.047 Uiso calc 1 . .
C C13 0.6944(2) 0.4972(2) 0.51892(17) 0.0339(5) Uani d 1 . .
C C14 0.7098(2) 0.4312(2) 0.43895(18) 0.0357(5) Uani d 1 . .
H H14 0.758612 0.454784 0.391503 0.043 Uiso calc 1 . .
C C15 0.6552(2) 0.3316(2) 0.42736(17) 0.0322(5) Uani d 1 . .
H H15 0.666465 0.287397 0.372102 0.039 Uiso calc 1 . .
C C16 0.7506(3) 0.6070(2) 0.53342(19) 0.0409(6) Uani d 1 . .
H H16A 0.814718 0.613082 0.492246 0.061 Uiso calc 1 . .
H H16B 0.781897 0.616432 0.603361 0.061 Uiso calc 1 . .
H H16C 0.691764 0.663039 0.514100 0.061 Uiso calc 1 . .
O O21 0.39294(13) 0.02026(13) 0.49327(12) 0.0287(3) Uani d 1 . .
N N21 0.28216(15) 0.05826(15) 0.48253(13) 0.0242(3) Uani d 1 . .
C C21 0.21856(19) 0.04578(18) 0.55877(17) 0.0283(4) Uani d 1 . .
H H21 0.248923 0.004642 0.615235 0.034 Uiso calc 1 . .
C C22 0.1092(2) 0.09302(19) 0.55439(18) 0.0310(5) Uani d 1 . .
H H22 0.064668 0.084973 0.608466 0.037 Uiso calc 1 . .
C C23 0.0632(2) 0.15256(19) 0.47132(18) 0.0316(5) Uani d 1 . .
C C24 0.1299(2) 0.15751(19) 0.39241(18) 0.0325(5) Uani d 1 . .
H H24 0.099213 0.193206 0.332881 0.039 Uiso calc 1 . .
C C25 0.2396(2) 0.11137(18) 0.39968(17) 0.0297(4) Uani d 1 . .
H H25 0.285208 0.117040 0.346108 0.036 Uiso calc 1 . .
C C26 -0.0518(2) 0.2114(2) 0.4683(2) 0.0418(6) Uani d 1 . .
H H26A -0.068918 0.248973 0.404593 0.063 Uiso calc 0.5 . .
H H26B -0.046939 0.264182 0.522437 0.063 Uiso calc 0.5 . .
H H26C -0.114632 0.159457 0.475782 0.063 Uiso calc 0.5 . .
H H26D -0.084742 0.199435 0.530615 0.063 Uiso calc 0.5 . .
H H26E -0.106720 0.184226 0.412771 0.063 Uiso calc 0.5 . .
H H26F -0.039027 0.288951 0.459426 0.063 Uiso calc 0.5 . .
O O31 0.49549(16) -0.04034(13) 0.68691(12) 0.0340(4) Uani d 1 . .
H H31 0.495536 -0.104304 0.666149 0.061(11) Uiso calc 1 . .
C C31 0.5284(2) -0.0392(2) 0.79179(18) 0.0373(5) Uani d 1 . .
H H31A 0.611351 -0.059417 0.806657 0.056 Uiso calc 1 . .
H H31B 0.479797 -0.090838 0.823227 0.056 Uiso calc 1 . .
H H31C 0.516711 0.033542 0.817470 0.056 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Co1 0.02249(18) 0.02112(18) 0.02309(18) -0.00307(12) 0.00103(12) -0.00346(12)
N1 0.0264(9) 0.0278(9) 0.0269(9) -0.0040(7) -0.0024(7) -0.0050(7)
C1 0.0333(11) 0.0209(9) 0.0213(9) 0.0016(8) 0.0046(8) -0.0018(7)
S1 0.0250(3) 0.0377(3) 0.0412(3) -0.0034(2) -0.0017(2) -0.0031(2)
N2 0.0284(9) 0.0286(9) 0.0302(9) 0.0000(7) 0.0059(7) -0.0062(7)
C2 0.0368(11) 0.0288(11) 0.0222(10) -0.0063(9) 0.0032(8) 0.0025(8)
S2 0.0547(4) 0.0415(3) 0.0316(3) 0.0200(3) 0.0152(3) 0.0069(2)
O11 0.0412(9) 0.0245(7) 0.0257(7) -0.0083(6) -0.0016(6) 0.0000(6)
N11 0.0324(9) 0.0234(9) 0.0245(8) -0.0032(7) -0.0013(7) 0.0025(7)
C11 0.0514(14) 0.0278(11) 0.0316(12) -0.0054(10) 0.0113(10) -0.0004(9)
C12 0.0575(16) 0.0279(12) 0.0338(12) -0.0083(11) 0.0102(11) -0.0009(9)
C13 0.0397(12) 0.0307(11) 0.0296(11) -0.0060(10) -0.0028(9) 0.0058(9)
C14 0.0378(12) 0.0380(12) 0.0308(12) -0.0095(10) 0.0022(10) 0.0034(10)
C15 0.0339(11) 0.0345(12) 0.0275(11) -0.0022(9) 0.0008(9) -0.0001(9)
C16 0.0539(16) 0.0353(13) 0.0318(12) -0.0149(11) -0.0009(11) 0.0051(10)
O21 0.0207(7) 0.0321(8) 0.0322(8) -0.0013(6) -0.0005(6) -0.0131(6)
N21 0.0197(8) 0.0234(8) 0.0291(9) -0.0031(7) 0.0012(6) -0.0051(7)
C21 0.0262(10) 0.0288(11) 0.0293(10) -0.0052(8) 0.0010(8) 0.0013(8)
C22 0.0243(10) 0.0362(12) 0.0329(12) -0.0039(8) 0.0052(9) -0.0026(9)
C23 0.0273(10) 0.0302(11) 0.0358(12) -0.0021(9) -0.0026(9) -0.0072(9)
C24 0.0369(12) 0.0274(11) 0.0317(11) -0.0010(9) -0.0012(9) -0.0008(9)
C25 0.0330(11) 0.0275(10) 0.0288(11) -0.0044(9) 0.0046(9) -0.0033(9)
C26 0.0310(12) 0.0459(15) 0.0467(15) 0.0076(11) -0.0025(10) -0.0067(12)
O31 0.0465(9) 0.0235(8) 0.0328(8) -0.0070(7) 0.0085(7) -0.0028(6)
C31 0.0445(13) 0.0345(12) 0.0330(12) -0.0045(10) 0.0053(10) 0.0029(10)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co -2.3653 3.6143 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N1 Co1 N2 . . 96.79(7) y
N1 Co1 O11 . . 96.07(7) y
N1 Co1 O21 . 3_656 94.26(7) y
N1 Co1 O21 . . 166.79(7) y
N1 Co1 O31 . . 95.14(7) y
N2 Co1 O21 . 3_656 167.69(7) y
N2 Co1 O21 . . 96.37(7) y
N2 Co1 O31 . . 86.85(7) y
O11 Co1 N2 . . 96.57(7) y
O11 Co1 O21 . . 83.57(6) y
O11 Co1 O21 . 3_656 87.62(7) y
O11 Co1 O31 . . 167.80(6) y
O21 Co1 O21 3_656 . 72.53(6) y
O21 Co1 O31 3_656 . 86.77(7) y
O21 Co1 O31 . . 84.42(7) y
C1 N1 Co1 . . 166.57(18) ?
N1 C1 S1 . . 179.4(2) ?
C2 N2 Co1 . . 165.94(18) ?
N2 C2 S2 . . 178.8(2) ?
N11 O11 Co1 . . 122.38(12) ?
O11 N11 C11 . . 120.70(19) ?
O11 N11 C15 . . 118.81(19) ?
C15 N11 C11 . . 120.5(2) ?
N11 C11 H11 . . 119.7 ?
N11 C11 C12 . . 120.6(2) ?
C12 C11 H11 . . 119.7 ?
C11 C12 H12 . . 119.7 ?
C11 C12 C13 . . 120.6(2) ?
C13 C12 H12 . . 119.7 ?
C12 C13 C14 . . 117.3(2) ?
C12 C13 C16 . . 120.1(2) ?
C14 C13 C16 . . 122.6(2) ?
C13 C14 H14 . . 119.5 ?
C15 C14 C13 . . 120.9(2) ?
C15 C14 H14 . . 119.5 ?
N11 C15 C14 . . 120.1(2) ?
N11 C15 H15 . . 120.0 ?
C14 C15 H15 . . 120.0 ?
C13 C16 H16A . . 109.5 ?
C13 C16 H16B . . 109.5 ?
C13 C16 H16C . . 109.5 ?
H16A C16 H16B . . 109.5 ?
H16A C16 H16C . . 109.5 ?
H16B C16 H16C . . 109.5 ?
Co1 O21 Co1 3_656 . 107.47(6) ?
N21 O21 Co1 . 3_656 130.26(12) ?
N21 O21 Co1 . . 121.46(12) ?
O21 N21 C21 . . 118.04(18) ?
C25 N21 O21 . . 120.21(18) ?
C25 N21 C21 . . 121.67(19) ?
N21 C21 H21 . . 120.2 ?
N21 C21 C22 . . 119.6(2) ?
C22 C21 H21 . . 120.2 ?
C21 C22 H22 . . 119.7 ?
C21 C22 C23 . . 120.6(2) ?
C23 C22 H22 . . 119.7 ?
C22 C23 C26 . . 121.4(2) ?
C24 C23 C22 . . 117.2(2) ?
C24 C23 C26 . . 121.4(2) ?
C23 C24 H24 . . 119.6 ?
C25 C24 C23 . . 120.7(2) ?
C25 C24 H24 . . 119.6 ?
N21 C25 C24 . . 119.9(2) ?
N21 C25 H25 . . 120.0 ?
C24 C25 H25 . . 120.0 ?
C23 C26 H26A . . 109.5 ?
C23 C26 H26B . . 109.5 ?
C23 C26 H26C . . 109.5 ?
C23 C26 H26D . . 109.5 ?
C23 C26 H26E . . 109.5 ?
C23 C26 H26F . . 109.5 ?
H26A C26 H26B . . 109.5 ?
H26A C26 H26C . . 109.5 ?
H26A C26 H26D . . 141.1 ?
H26A C26 H26E . . 56.3 ?
H26A C26 H26F . . 56.3 ?
H26B C26 H26C . . 109.5 ?
H26B C26 H26D . . 56.3 ?
H26B C26 H26E . . 141.1 ?
H26B C26 H26F . . 56.3 ?
H26C C26 H26D . . 56.3 ?
H26C C26 H26E . . 56.3 ?
H26C C26 H26F . . 141.1 ?
H26D C26 H26E . . 109.5 ?
H26D C26 H26F . . 109.5 ?
H26E C26 H26F . . 109.5 ?
Co1 O31 H31 . . 121.0 ?
C31 O31 Co1 . . 123.18(14) ?
C31 O31 H31 . . 109.5 ?
O31 C31 H31A . . 109.5 ?
O31 C31 H31B . . 109.5 ?
O31 C31 H31C . . 109.5 ?
H31A C31 H31B . . 109.5 ?
H31A C31 H31C . . 109.5 ?
H31B C31 H31C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Co1 N1 . 2.0525(18) y
Co1 N2 . 2.0840(18) y
Co1 O11 . 2.0543(16) y
Co1 O21 . 2.1057(15) y
Co1 O21 3_656 2.1043(15) y
Co1 O31 . 2.1301(16) y
N1 C1 . 1.162(3) ?
C1 S1 . 1.635(2) ?
N2 C2 . 1.163(3) ?
C2 S2 . 1.634(2) ?
O11 N11 . 1.340(2) ?
N11 C11 . 1.348(3) ?
N11 C15 . 1.342(3) ?
C11 H11 . 0.9500 ?
C11 C12 . 1.379(3) ?
C12 H12 . 0.9500 ?
C12 C13 . 1.380(3) ?
C13 C14 . 1.388(4) ?
C13 C16 . 1.506(3) ?
C14 H14 . 0.9500 ?
C14 C15 . 1.382(3) ?
C15 H15 . 0.9500 ?
C16 H16A . 0.9800 ?
C16 H16B . 0.9800 ?
C16 H16C . 0.9800 ?
O21 N21 . 1.345(2) ?
N21 C21 . 1.347(3) ?
N21 C25 . 1.342(3) ?
C21 H21 . 0.9500 ?
C21 C22 . 1.378(3) ?
C22 H22 . 0.9500 ?
C22 C23 . 1.395(3) ?
C23 C24 . 1.393(3) ?
C23 C26 . 1.503(3) ?
C24 H24 . 0.9500 ?
C24 C25 . 1.373(3) ?
C25 H25 . 0.9500 ?
C26 H26A . 0.9800 ?
C26 H26B . 0.9800 ?
C26 H26C . 0.9800 ?
C26 H26D . 0.9800 ?
C26 H26E . 0.9800 ?
C26 H26F . 0.9800 ?
O31 H31 . 0.8400 ?
O31 C31 . 1.428(3) ?
C31 H31A . 0.9800 ?
C31 H31B . 0.9800 ?
C31 H31C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
C11 H11 N2 . 0.95 2.40 3.225(3) 144.9
C12 H12 S1 2_656 0.95 2.79 3.688(3) 157.9
C15 H15 S2 4_665 0.95 2.68 3.609(3) 166.8
C21 H21 S2 2_546 0.95 3.03 3.917(2) 156.2
C22 H22 S1 1_455 0.95 2.98 3.821(2) 148.1
O31 H31 S1 2_646 0.84 2.97 3.6106(18) 134.2
O31 H31 O11 3_656 0.84 2.31 3.003(2) 140.6
C31 H31B S2 2_546 0.98 2.83 3.575(3) 133.0