#------------------------------------------------------------------------------ #$Date: 2024-04-27 04:54:31 +0300 (Sat, 27 Apr 2024) $ #$Revision: 291378 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/30/2023092.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023092 loop_ _publ_author_name 'Eder, Felix' 'Weil, Matthias' _publ_section_title ; Synthesis and crystal structure of (NH4)[Ni3(HAsO4)(AsO4)(OH)2] ; _journal_coeditor_code HB8094 _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989024003487 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac '(N H4) [Ni3 (H As O4) (As O4) (O H)2]' _chemical_formula_moiety 'H4 N1 +, As2 H3 Ni3 O10 -' _chemical_formula_sum 'As2 H7 N Ni3 O10' _chemical_formula_weight 507.04 _chemical_name_systematic ; Ammonium trinickel(II) hydrogen arsenate arsenate dihydroxide ; _space_group_crystal_system monoclinic _space_group_IT_number 12 _space_group_name_Hall '-C 2y' _space_group_name_H-M_alt 'C 1 2/m 1' _atom_sites_solution_hydrogens difmap _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 90 _cell_angle_beta 112.658(14) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 10.178(2) _cell_length_b 5.9156(11) _cell_length_c 7.7158(14) _cell_measurement_reflns_used 7257 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 35.92 _cell_measurement_theta_min 4.07 _cell_volume 428.71(15) _computing_cell_refinement ; X-AREA (Stoe, 2021) ; _computing_data_collection ; X-AREA (Stoe, 2021) ; _computing_data_reduction ; X-AREA (Stoe, 2021) ; _computing_molecular_graphics ; DIAMOND (Brandenburg, 2016) ; _computing_publication_material ; publCIF (Westrip, 2010) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.939 _diffrn_measured_fraction_theta_max 0.937 _diffrn_measurement_device_type 'Stoe Stadivari CCD' _diffrn_measurement_method 'rotation method, \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_unetI/netI 0.0709 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 3235 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 35.338 _diffrn_reflns_theta_min 2.861 _diffrn_source Axo_Mo _exptl_absorpt_coefficient_mu 14.228 _exptl_absorpt_correction_T_max 0.3451 _exptl_absorpt_correction_T_min 0.2808 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (LANA; Koziskova et al., 2016) ; _exptl_crystal_colour 'light green' _exptl_crystal_density_diffrn 3.928 _exptl_crystal_description block _exptl_crystal_F_000 488 _exptl_crystal_size_max 0.050 _exptl_crystal_size_mid 0.040 _exptl_crystal_size_min 0.030 _refine_diff_density_max 2.953 _refine_diff_density_min -2.295 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_hydrogen_treatment refxyz _refine_ls_matrix_type full _refine_ls_number_parameters 54 _refine_ls_number_reflns 3235 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.039 _refine_ls_R_factor_all 0.0950 _refine_ls_R_factor_gt 0.0675 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1507P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1984 _refine_ls_wR_factor_ref 0.2288 _reflns_number_gt 2214 _reflns_number_total 3235 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file hb8094.cif _cod_data_source_block I _cod_original_sg_symbol_H-M 'C 2/m' _cod_database_code 2023092 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.536 _shelx_estimated_absorpt_t_max 0.675 _shelx_hkl_file ; 0 -2 0 1611.04 6.82 1 0 -2 -1 871.06 5.83 1 0 2 -9 14.38 8.80 1 0 4 0 8839.61 22.45 1 0 -4 -1 1816.67 66.62 1 0 -4 -2 11.01 4.97 1 0 4 -3 56.58 7.75 1 0 4 -4 2547.00 55.88 1 0 4 -5 1137.59 35.56 1 0 4 -6 198.38 9.36 1 0 4 -7 179.52 8.15 1 0 4 -8 822.78 33.55 1 0 4 -9 280.12 11.24 1 0 4 -10 6.64 6.72 1 0 -6 0 323.52 9.80 1 0 -6 -1 93.83 6.89 1 0 6 -2 702.28 20.71 1 0 -6 -3 198.20 8.80 1 0 -6 -4 186.55 6.56 1 0 6 -6 389.74 17.28 1 0 6 -7 163.99 11.42 1 0 6 -8 64.29 9.06 1 0 -8 0 1758.70 40.91 1 0 -8 -1 416.66 16.25 1 0 8 -2 -0.27 7.64 1 0 -8 -3 27.24 8.22 1 0 8 -4 704.94 18.33 1 0 8 -5 351.04 16.00 1 0 8 -6 65.83 12.72 1 1 3 -11 150.90 13.14 1 1 3 -9 38.33 11.25 1 1 -3 -6 460.47 10.40 1 1 -3 -5 77.37 4.44 1 1 -3 -4 66.46 3.90 1 1 3 -2 1246.74 301.49 1 1 -3 -1 3.45 1.38 1 -1 3 -2 1701.65 10.45 1 -1 3 -4 580.60 8.47 1 -1 3 -5 167.32 8.77 1 -1 3 -7 165.53 12.05 1 -1 3 -9 -3.39 10.06 1 -1 3 -10 100.73 10.85 1 1 -5 -10 136.15 11.47 1 1 5 -9 21.58 10.19 1 1 5 -8 -1.02 6.61 1 1 5 -7 216.71 7.87 1 1 -5 -6 217.81 8.72 1 1 5 -5 112.28 6.17 1 1 5 -4 44.02 5.39 1 1 5 -3 785.21 24.75 1 1 5 -2 1180.17 26.73 1 -1 -5 1 8.97 4.13 1 1 -5 0 304.00 8.07 1 -1 5 -1 389.18 12.13 1 1 -5 2 1108.00 27.26 1 -1 5 -3 22.15 5.75 1 -1 5 -4 212.07 8.85 1 -1 5 -5 116.03 7.14 1 -1 5 -7 76.78 8.92 1 -1 -5 -8 61.90 7.79 1 -1 5 -9 3.46 9.16 1 1 7 -8 -1.23 8.07 1 1 -7 -7 186.28 13.11 1 1 -7 -6 226.63 12.10 1 1 -7 -5 29.17 8.47 1 1 -7 -4 34.34 7.14 1 1 -7 -3 258.91 8.20 1 -1 -7 1 1.85 5.42 1 1 -7 0 61.61 8.21 1 -1 7 -1 250.00 6.24 1 -1 7 -2 476.26 11.15 1 -1 7 -3 0.36 6.62 1 -1 7 -4 185.86 10.02 1 -1 -7 -5 51.21 8.34 1 -1 7 -6 418.85 17.00 1 -1 7 -7 68.88 10.47 1 1 -9 -4 8.21 9.73 1 1 9 -3 206.60 11.07 1 1 -9 -2 284.95 8.48 1 1 -9 -1 3.86 12.46 1 -1 -9 0 69.59 13.35 1 -1 -9 -1 70.05 12.55 1 -1 -9 -2 267.42 9.65 1 -1 -9 -3 7.13 9.88 1 -2 0 0 251.20 1.89 1 -2 0 -1 2890.14 8.84 1 -2 0 -3 2.97 4.32 1 -2 0 -5 558.97 6.20 1 -2 0 -6 413.31 6.93 1 2 4 -10 43.91 13.85 1 2 4 -9 77.97 11.52 1 2 -4 -8 36.43 7.75 1 2 -4 -7 541.60 10.67 1 2 -4 -6 184.04 5.48 1 2 -4 -5 203.60 9.72 1 2 -4 -4 -1.34 3.05 1 2 -4 -3 1226.47 23.11 1 2 -4 -2 610.20 7.13 1 2 -4 -1 121.17 3.93 1 2 -4 0 89.09 4.28 1 2 -4 1 1292.06 10.17 1 2 -4 2 886.73 19.89 1 -2 4 -3 7.79 3.67 1 -2 4 -4 172.45 9.63 1 -2 4 -5 374.02 11.60 1 -2 4 -6 333.37 12.52 1 -2 4 -7 1.18 5.46 1 -2 4 -8 99.04 11.20 1 2 6 -9 773.27 30.15 1 2 6 -8 367.13 14.47 1 2 6 -7 -0.46 6.82 1 2 6 -6 44.01 8.22 1 2 -6 -5 947.14 25.82 1 2 -6 -4 981.16 29.35 1 2 -6 -3 191.27 8.76 1 2 6 -2 456.79 11.35 1 2 6 -1 1699.93 27.60 1 2 -6 0 952.60 22.92 1 -2 6 -1 0.66 4.53 1 -2 6 -2 94.71 6.75 1 -2 -6 -3 1515.40 23.10 1 -2 6 -4 1768.27 29.73 1 -2 -6 -5 60.97 10.22 1 -2 6 -6 2.13 6.68 1 -2 -6 -7 164.72 10.72 1 -2 -6 -8 548.01 20.41 1 2 8 -6 62.46 7.48 1 2 8 -5 61.69 10.98 1 2 -8 -4 5.12 7.65 1 2 -8 -3 338.58 15.30 1 2 8 -2 171.99 8.60 1 2 -8 -1 40.95 6.81 1 -2 -8 0 17.85 6.94 1 2 -8 1 319.17 9.38 1 -2 8 -2 243.80 11.61 1 -2 8 -3 4.36 7.75 1 -2 8 -4 52.53 9.55 1 -2 8 -5 106.29 10.37 1 3 -1 -4 293.79 3.99 1 3 -1 -2 1101.77 11.18 1 3 -1 -1 1354.27 7.36 1 3 -1 0 212.23 3.40 1 -3 -1 -2 858.52 7.35 1 -3 -1 -4 9.72 4.41 1 -3 -1 -5 779.69 17.65 1 -3 -1 -6 302.17 5.05 1 -3 1 -10 193.72 13.64 1 3 5 -10 7.60 14.95 1 3 5 -9 122.38 11.27 1 3 5 -8 112.76 13.67 1 3 -5 -7 407.50 11.04 1 3 -5 -6 84.10 10.51 1 3 -5 -5 202.89 10.32 1 3 -5 -4 142.86 7.03 1 3 -5 -3 876.45 43.57 1 3 -5 -2 283.82 17.12 1 3 -5 -1 336.41 7.20 1 3 -5 0 9.58 3.61 1 -3 5 -1 703.66 17.46 1 -3 5 -2 330.28 12.47 1 -3 5 -3 92.92 7.49 1 -3 5 -4 6.63 5.83 1 -3 5 -5 429.68 10.04 1 -3 5 -6 166.88 10.14 1 -3 -5 -7 83.71 9.13 1 -3 5 -8 39.31 9.74 1 3 -7 -8 31.79 12.75 1 3 -7 -7 246.23 14.09 1 3 -7 -6 73.68 9.19 1 3 -7 -5 72.02 10.23 1 3 7 -4 54.29 9.06 1 3 7 -3 339.26 14.81 1 3 -7 -2 63.19 7.09 1 3 7 -1 162.93 9.29 1 3 -7 0 34.28 9.22 1 3 -7 1 533.71 15.45 1 -3 -7 -2 198.17 9.73 1 -3 7 -3 77.22 7.03 1 -3 7 -4 2.66 7.99 1 -3 7 -5 246.90 12.32 1 -3 7 -6 144.27 16.89 1 3 -9 -4 35.30 10.98 1 3 -9 -3 281.42 18.70 1 3 -9 -2 74.38 8.81 1 3 -9 -1 56.90 13.71 1 3 -9 0 -0.34 14.66 1 -3 -9 -1 157.77 13.19 1 -3 -9 -2 94.24 14.35 1 4 0 -10 776.50 15.93 1 4 0 -9 799.79 8.40 1 4 0 -8 9.99 6.97 1 4 0 -7 50.28 6.34 1 4 0 -6 3172.36 64.40 1 4 0 -4 896.67 7.86 1 -4 0 3 18.12 2.53 1 -4 0 2 344.04 4.17 1 -4 0 1 5220.27 12.89 1 -4 0 0 3365.85 10.27 1 -4 0 -1 1557.60 54.85 1 -4 0 -4 321.72 10.11 1 -4 0 -5 1.98 3.36 1 -4 0 -6 318.86 14.82 1 -4 0 -7 1375.79 51.48 1 -4 0 -8 510.10 13.28 1 -4 0 -9 4.34 12.28 1 4 2 -6 -1.29 5.72 1 4 2 -5 224.25 14.43 1 4 2 -3 1778.35 10.42 1 4 2 -2 85.97 5.62 1 -4 -2 1 471.38 11.58 1 4 2 0 586.69 6.41 1 -4 -2 -1 1625.15 49.58 1 -4 -2 -2 116.16 6.60 1 -4 -2 -3 371.94 7.15 1 -4 -2 -4 30.61 5.14 1 -4 -2 -5 748.95 14.78 1 -4 -2 -6 176.61 6.25 1 4 -6 -8 165.06 13.64 1 4 -6 -7 290.60 17.87 1 4 -6 -6 8.31 7.25 1 4 -6 -5 74.24 4.76 1 4 -6 -4 200.57 10.74 1 4 -6 -3 593.60 31.18 1 4 -6 -2 10.73 6.66 1 4 -6 -1 159.56 5.04 1 -4 -6 0 153.73 11.87 1 4 -6 1 655.40 11.50 1 -4 6 -2 31.73 5.44 1 -4 6 -3 150.26 7.54 1 -4 6 -4 18.40 6.75 1 -4 6 -5 361.93 17.70 1 -4 6 -6 89.13 8.26 1 -4 6 -7 21.96 8.34 1 4 -8 -6 491.41 24.22 1 4 -8 -5 896.52 31.97 1 4 -8 -4 112.48 10.74 1 4 8 -3 -0.69 7.70 1 4 8 -2 187.98 12.92 1 4 -8 -1 831.36 27.09 1 4 -8 0 308.73 14.17 1 -4 -8 -2 300.31 7.72 1 -4 8 -3 566.94 25.70 1 -4 8 -4 92.11 12.01 1 5 1 -12 133.16 14.42 1 5 1 -11 37.67 12.96 1 5 1 -10 109.15 10.50 1 5 -1 -9 8.15 8.09 1 5 1 -8 1038.03 27.35 1 5 -1 -7 484.94 20.08 1 5 1 -6 206.55 12.60 1 5 1 -5 240.83 7.71 1 5 1 -3 1232.60 20.12 1 5 -1 -2 4.39 3.45 1 5 -1 -1 337.72 19.75 1 5 -1 0 1420.39 26.63 1 -5 -1 -1 303.40 284.33 1 -5 1 -2 31.82 3.60 1 -5 1 -3 314.55 6.88 1 -5 -1 -4 264.71 8.51 1 -5 1 -5 411.06 9.40 1 -5 1 -6 42.95 5.82 1 -5 1 -7 74.74 7.36 1 -5 -1 -8 75.39 8.86 1 -5 -1 -9 179.13 16.04 1 5 3 -5 106.25 6.16 1 5 3 -3 855.88 12.87 1 5 3 -1 301.37 5.93 1 -5 -3 0 1074.21 13.52 1 -5 -3 -1 1059.43 38.71 1 -5 -3 -2 27.55 2.80 1 -5 -3 -3 287.73 9.19 1 -5 -3 -4 152.55 6.59 1 -5 -3 -5 309.34 7.93 1 5 -7 -8 260.00 12.18 1 5 -7 -7 128.58 12.69 1 5 -7 -6 30.82 9.74 1 5 -7 -5 16.40 10.53 1 5 -7 -4 335.45 20.79 1 5 -7 -3 263.45 14.79 1 5 -7 -2 21.02 7.37 1 5 -7 -1 92.46 7.11 1 5 -7 0 330.99 9.08 1 -5 -7 -1 540.80 86.81 1 -5 7 -2 11.76 5.94 1 -5 7 -3 111.84 15.33 1 -5 7 -4 43.17 10.10 1 -5 7 -5 121.45 9.74 1 6 0 -12 131.02 13.61 1 6 0 -11 -2.10 8.79 1 6 0 -10 211.32 10.77 1 6 0 -9 136.99 11.49 1 6 0 -8 817.74 27.40 1 6 0 -7 251.97 9.89 1 6 0 -6 416.20 20.05 1 6 0 -5 47.84 8.24 1 -6 0 1 7.57 4.03 1 -6 0 0 1152.55 26.95 1 -6 0 -1 678.04 6.95 1 -6 0 -2 65.49 3.37 1 -6 0 -3 27.06 3.77 1 -6 0 -4 596.29 10.34 1 -6 0 -5 372.14 12.24 1 -6 0 -6 13.86 5.06 1 -6 0 -7 101.88 7.63 1 -6 0 -8 88.44 10.78 1 6 2 -12 3.07 13.01 1 6 2 -11 100.40 13.52 1 6 2 -10 1026.37 47.12 1 6 2 -8 142.59 7.15 1 6 2 -7 594.19 19.85 1 6 2 -6 2636.60 83.07 1 6 2 -5 440.79 14.00 1 6 2 -4 2.49 3.43 1 6 2 -3 816.45 9.87 1 6 2 -2 7477.69 24.34 1 6 -2 -1 3779.96 100.28 1 6 -2 0 35.48 2.69 1 -6 -2 -1 2.46 2.69 1 6 2 2 1280.97 25.44 1 -6 2 -3 1724.36 30.33 1 -6 -2 -4 231.60 8.08 1 -6 -2 -5 151.70 7.32 1 -6 2 -6 524.99 16.03 1 -6 2 -7 497.07 15.81 1 -6 2 -8 13.14 7.43 1 6 4 -11 2.18 13.77 1 6 4 -5 19.73 6.19 1 6 4 -3 448.96 14.24 1 6 4 -2 211.45 8.20 1 6 4 -1 6.78 4.19 1 6 4 0 696.63 10.60 1 -6 -4 -2 47.86 3.31 1 -6 -4 -3 22.61 4.54 1 -6 -4 -4 381.32 10.82 1 -6 -4 -5 235.58 8.96 1 -6 -4 -6 12.73 7.54 1 -6 -4 -7 70.62 6.90 1 7 1 -12 184.77 19.17 1 7 1 -11 4.46 10.29 1 7 1 -10 39.15 5.62 1 7 1 -9 221.24 11.18 1 7 1 -8 445.75 15.87 1 7 1 -7 -0.31 5.59 1 7 1 -6 262.59 10.73 1 7 1 -5 436.61 11.79 1 7 -1 -4 1519.88 39.01 1 7 1 -3 142.23 6.06 1 7 1 -2 428.89 7.28 1 7 1 -1 123.58 4.24 1 7 -1 0 1319.47 21.82 1 -7 1 -1 160.15 5.89 1 -7 1 -2 249.07 7.71 1 -7 1 -3 -0.74 4.34 1 -7 1 -4 714.17 13.16 1 -7 1 -5 238.47 7.65 1 -7 1 -6 18.78 6.31 1 -7 -1 -7 28.86 6.89 1 -7 -1 -8 115.47 10.08 1 7 3 -11 -3.04 7.55 1 7 3 -10 32.93 10.00 1 7 3 -9 149.71 8.79 1 7 -3 -8 289.13 5.45 1 7 3 -7 2.63 6.37 1 7 3 -6 201.75 10.81 1 7 -3 -5 369.15 13.07 1 7 -3 -4 1323.89 29.26 1 7 3 -3 86.23 6.79 1 7 3 -2 383.82 9.01 1 7 -3 -1 62.34 5.67 1 7 3 0 1080.81 28.52 1 -7 -3 -1 161.02 7.09 1 -7 3 -2 147.35 7.42 1 -7 3 -3 -3.65 4.50 1 -7 -3 -4 527.67 16.69 1 -7 -3 -5 167.43 7.91 1 -7 -3 -6 13.07 6.32 1 -7 -3 -7 13.99 7.66 1 7 5 -10 27.08 13.26 1 7 5 -9 143.43 12.72 1 7 5 -3 58.91 6.52 1 7 5 -2 141.62 9.43 1 7 5 -1 66.27 5.96 1 7 5 0 625.17 12.44 1 -7 -5 -1 58.91 7.00 1 -7 -5 -3 -0.08 3.81 1 -7 -5 -4 406.62 11.44 1 -7 -5 -5 149.22 15.41 1 -7 -5 -6 17.62 7.31 1 8 0 -11 846.82 16.95 1 8 0 -10 950.05 16.91 1 8 0 -8 14.44 6.95 1 8 0 -7 882.89 40.17 1 8 0 -6 2326.05 55.26 1 8 0 -5 448.47 13.89 1 8 0 -4 633.93 13.15 1 8 0 -3 1770.38 22.73 1 8 0 -1 7.79 3.99 1 -8 0 0 35.20 4.12 1 8 0 1 1343.56 24.03 1 -8 0 -2 3197.43 39.07 1 -8 0 -3 365.76 7.35 1 -8 0 -4 -0.70 6.43 1 -8 0 -5 72.68 6.34 1 -8 0 -6 668.81 18.87 1 -8 0 -7 240.31 10.68 1 8 2 -12 79.60 11.83 1 8 2 -11 18.83 10.49 1 8 2 -10 6.36 11.05 1 8 2 -9 409.76 10.98 1 8 2 -8 257.94 12.30 1 8 2 -7 28.67 7.01 1 8 -2 -6 108.17 7.73 1 8 -2 -5 797.01 22.42 1 8 -2 -4 716.54 18.81 1 8 2 -3 6.15 3.81 1 8 -2 -2 334.04 10.19 1 -8 -2 1 532.71 10.71 1 8 2 0 871.71 19.73 1 -8 -2 -1 55.10 4.97 1 -8 2 -2 214.89 7.09 1 -8 -2 -3 70.65 5.64 1 -8 2 -4 310.66 5.83 1 -8 2 -5 32.54 6.85 1 -8 -2 -6 64.11 7.36 1 -8 2 -7 16.43 7.56 1 8 4 -11 572.84 35.23 1 8 4 -10 607.56 33.69 1 8 4 -9 11.88 8.25 1 8 -4 -8 9.50 7.82 1 8 -4 -6 1373.22 40.34 1 8 -4 -5 237.11 11.26 1 8 -4 -4 309.78 12.95 1 8 -4 -3 1112.78 28.50 1 8 -4 -2 1449.54 27.70 1 8 -4 -1 12.40 5.39 1 8 -4 0 17.35 4.96 1 -8 4 -1 802.36 23.15 1 -8 4 -2 1793.77 46.52 1 -8 -4 -3 236.37 11.85 1 -8 4 -4 -0.26 6.56 1 -8 4 -5 50.32 7.81 1 -8 -4 -6 435.51 11.56 1 9 1 -12 32.71 14.55 1 9 1 -10 -1.19 7.01 1 9 -1 -9 430.25 14.94 1 9 -1 -8 255.36 9.73 1 9 1 -7 70.22 7.50 1 9 -1 -6 -1.42 4.97 1 9 1 -5 710.75 16.52 1 9 -1 -4 352.90 9.00 1 9 -1 -3 118.90 5.72 1 9 1 -2 44.32 4.77 1 -9 -1 1 737.90 14.36 1 9 -1 0 491.83 12.95 1 -9 -1 -1 11.89 4.32 1 -9 1 -2 61.81 5.41 1 -9 -1 -3 295.22 12.64 1 -9 1 -4 295.64 8.78 1 -9 -1 -5 1.86 6.07 1 -9 1 -6 81.67 8.93 1 9 3 -11 108.44 13.84 1 9 3 -10 -2.40 8.20 1 9 3 -9 341.41 13.54 1 9 -3 -8 180.11 10.57 1 9 -3 -7 66.71 7.90 1 9 3 -6 -1.56 6.45 1 9 -3 -5 636.04 15.92 1 9 3 -4 341.88 15.43 1 9 3 -3 89.72 8.24 1 9 -3 -2 50.60 6.68 1 9 3 -1 505.30 12.88 1 9 3 0 371.24 15.21 1 9 -3 1 7.05 4.96 1 -9 3 -2 29.59 4.34 1 -9 3 -3 246.77 11.47 1 -9 3 -4 216.00 11.37 1 -9 3 -5 6.27 7.51 1 -9 -3 -6 75.19 8.16 1 9 -5 -10 -2.28 7.81 1 9 -5 -9 248.42 16.83 1 9 7 -7 50.88 9.21 1 9 7 -6 -3.13 8.03 1 9 7 -5 332.95 15.28 1 9 7 -4 163.76 13.17 1 9 7 -3 34.89 8.16 1 9 7 -2 20.67 11.24 1 -9 -7 0 161.86 12.06 1 10 0 -12 -0.79 14.25 1 10 0 -11 94.95 12.66 1 10 0 -10 73.48 10.37 1 10 0 -9 446.32 18.97 1 10 0 -8 48.71 11.30 1 10 0 -7 139.54 6.17 1 10 0 -6 51.43 5.75 1 10 0 -5 776.94 11.13 1 10 0 -4 134.23 6.43 1 10 0 -3 129.16 5.01 1 10 0 -2 16.90 5.52 1 10 0 -1 845.18 12.02 1 10 0 0 129.54 8.10 1 -10 0 -1 111.80 6.50 1 -10 0 -2 25.21 7.65 1 -10 0 -3 405.62 14.15 1 -10 0 -4 179.77 9.92 1 -10 0 -5 17.48 12.35 1 -10 0 -6 29.59 6.38 1 10 -2 -11 551.48 24.94 1 10 2 -10 40.87 6.81 1 10 2 -9 0.90 6.99 1 10 -2 -8 547.81 20.23 1 10 2 -7 2206.42 21.85 1 10 2 -6 627.77 24.57 1 10 -2 -5 2.57 5.50 1 10 2 -4 115.00 8.30 1 10 2 -3 1510.24 30.47 1 10 -2 -2 1137.08 18.61 1 10 -2 -1 140.45 7.84 1 -10 -2 0 396.54 13.46 1 -10 2 -1 880.83 20.21 1 -10 -2 -2 375.91 14.03 1 -10 2 -3 3.92 6.27 1 -10 2 -4 78.37 7.78 1 -10 -2 -5 529.91 17.81 1 10 4 -10 48.31 9.52 1 10 -4 -9 323.61 21.23 1 10 4 -8 29.71 7.77 1 10 -4 -7 104.13 11.78 1 10 6 -8 283.46 12.50 1 10 6 -7 1069.09 32.51 1 10 6 -6 312.63 18.39 1 10 6 -5 11.81 6.28 1 10 6 -4 66.26 11.33 1 10 6 -3 724.64 39.34 1 11 1 -11 13.79 12.77 1 11 1 -10 336.20 12.26 1 11 1 -9 313.09 10.14 1 11 1 -8 1.40 8.73 1 11 1 -7 209.65 12.71 1 11 -1 -6 224.29 12.22 1 11 -1 -5 558.02 15.95 1 11 1 -4 26.32 5.70 1 11 -1 -3 181.65 7.05 1 11 1 -2 153.00 7.73 1 11 1 -1 577.58 12.02 1 -11 -1 0 56.82 6.93 1 11 1 1 102.14 8.45 1 -11 1 -2 8.82 5.59 1 -11 1 -3 227.46 9.90 1 -11 -1 -4 46.88 6.59 1 -11 1 -5 17.75 6.69 1 11 3 -10 279.79 22.12 1 11 3 -8 9.24 11.00 1 11 5 -9 214.65 15.48 1 11 5 -8 0.62 7.76 1 11 5 -7 92.27 11.45 1 11 5 -6 148.07 10.05 1 11 5 -5 338.48 13.84 1 11 5 -4 5.06 6.89 1 11 5 -3 122.10 11.85 1 11 5 -2 113.71 11.25 1 11 7 -4 22.04 9.86 1 11 7 -3 47.23 11.19 1 11 7 -2 39.11 11.14 1 12 0 -11 363.34 22.93 1 12 0 -10 25.22 16.54 1 12 0 -9 173.74 10.22 1 12 0 -8 797.64 19.63 1 12 0 -7 508.30 12.08 1 12 0 -6 6.01 11.00 1 12 0 -5 77.42 6.50 1 12 0 -4 1506.27 16.80 1 12 0 -3 1775.72 16.92 1 12 0 -2 52.11 8.22 1 12 0 0 255.07 5.67 1 -12 0 -1 767.68 17.83 1 -12 0 -3 33.82 8.15 1 -12 0 -4 178.77 9.60 1 12 2 -10 342.00 19.45 1 12 2 -8 59.07 16.07 1 12 2 -7 39.32 14.61 1 -12 2 -2 131.45 9.46 1 -12 2 -3 267.51 12.32 1 12 4 -9 114.75 14.99 1 12 4 -8 607.22 18.73 1 12 4 -7 377.74 20.21 1 12 4 -6 6.01 8.37 1 12 4 -5 66.14 10.25 1 12 4 -4 1136.71 19.41 1 12 -6 -6 211.34 14.36 1 12 -6 -5 198.07 10.54 1 12 6 -4 5.62 9.96 1 12 6 -3 45.69 9.13 1 12 -6 -2 101.96 13.12 1 12 6 -1 170.66 13.17 1 13 1 -10 187.09 21.15 1 13 1 -9 7.41 15.95 1 13 1 -8 81.17 17.13 1 13 1 -7 8.69 13.54 1 13 1 -6 576.98 17.08 1 13 3 -9 5.78 15.06 1 13 3 -8 61.39 14.40 1 13 3 -7 4.41 11.60 1 13 3 -6 503.48 14.06 1 13 3 -5 117.73 12.37 1 13 3 -4 53.24 11.79 1 13 3 -3 7.84 5.31 1 13 5 -7 11.95 10.82 1 13 5 -6 380.53 18.96 1 13 -5 -5 74.14 13.14 1 13 -5 -4 60.42 10.12 1 13 5 -3 13.36 10.55 1 13 -5 -2 253.56 15.08 1 13 -5 -1 112.72 11.66 1 14 2 -8 698.45 17.85 1 14 2 -6 80.68 13.61 1 14 2 -5 366.66 14.88 1 14 4 -7 80.12 11.63 1 14 4 -6 259.23 14.80 1 14 4 -5 11.06 10.02 1 14 4 -4 92.38 12.19 1 14 -4 -3 21.92 11.62 1 14 4 -2 321.89 17.42 1 14 4 -1 56.68 9.99 1 15 3 -7 118.36 12.38 1 15 3 -6 130.36 11.40 1 15 -3 -5 3.01 9.56 1 15 3 -4 32.87 11.47 1 15 -3 -3 105.59 13.68 1 15 3 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5 6 100.35 16.81 2 -1 -5 5 51.55 8.96 2 -1 -5 4 16.08 4.86 2 1 -5 -3 333.35 47.17 2 -1 -5 2 533.78 49.38 2 -1 -5 1 6.81 4.09 2 -1 -5 0 147.04 12.99 2 1 5 1 193.94 15.24 2 1 -5 2 524.25 24.33 2 1 5 3 6.17 5.67 2 1 5 4 104.42 11.07 2 1 5 5 53.29 7.26 2 1 5 6 305.20 8.90 2 1 -5 7 27.17 9.48 2 1 -5 8 27.98 7.59 2 1 -5 9 4.59 7.26 2 -1 -7 8 -2.94 8.55 2 -1 -7 7 69.81 16.68 2 -1 7 6 89.52 15.11 2 -1 -7 5 8.12 7.15 2 -1 -7 4 9.26 6.68 2 -1 -7 3 109.14 12.27 2 1 -7 -2 213.64 23.05 2 1 -7 -1 0.22 5.91 2 -1 -7 0 27.02 6.58 2 1 -7 1 115.87 4.77 2 -1 -7 -2 240.87 9.49 2 1 -7 3 0.57 6.36 2 1 7 4 75.67 13.62 2 1 -7 5 18.67 10.06 2 1 7 6 168.53 25.40 2 1 -7 7 25.81 10.36 2 1 -9 -4 4.82 10.84 2 -1 -9 3 65.64 16.32 2 -1 -9 2 93.12 18.20 2 1 -9 -1 2.78 10.07 2 1 -9 0 18.93 11.00 2 -1 -9 -1 21.85 10.71 2 1 -9 2 96.50 19.97 2 1 -9 3 1.40 9.04 2 -2 0 8 4.56 8.02 2 -2 0 7 356.62 10.62 2 -2 0 6 185.01 12.83 2 -2 0 3 1512.72 8.46 2 2 0 1 2214.93 26.35 2 2 0 2 848.01 6.72 2 2 0 3 -4.69 2.64 2 2 0 5 250.53 6.22 2 2 0 6 183.58 6.68 2 2 0 7 -2.06 6.30 2 2 -2 6 6.98 7.15 2 2 -2 10 23.90 11.94 2 -2 -4 4 -6.41 5.54 2 -2 4 3 293.20 5.58 2 2 -4 -2 311.75 28.65 2 2 -4 -1 72.24 4.77 2 2 -4 0 40.16 11.24 2 -2 -4 -1 637.19 7.85 2 2 4 2 440.49 13.37 2 2 4 3 2.14 3.69 2 2 4 4 72.89 7.53 2 2 -4 5 188.91 11.52 2 2 4 6 155.33 13.10 2 2 -4 7 -2.55 6.85 2 2 -4 8 39.98 14.14 2 2 -4 9 54.09 8.81 2 -2 6 9 313.52 51.92 2 -2 6 8 135.52 27.47 2 -2 6 7 2.47 6.98 2 -2 -6 6 12.05 7.93 2 -2 -6 5 401.90 34.45 2 -2 -6 4 375.16 55.81 2 -2 6 3 78.19 13.12 2 -2 -6 2 219.68 13.19 2 -2 -6 1 875.32 34.37 2 2 -6 0 485.27 22.59 2 -2 -6 -1 -0.50 5.03 2 2 -6 2 36.62 7.34 2 2 6 3 659.17 50.63 2 2 -6 4 927.78 17.26 2 2 -6 5 19.17 9.98 2 2 6 6 -0.86 7.33 2 2 6 7 70.39 12.89 2 2 6 8 217.92 32.51 2 -2 -8 6 18.41 10.61 2 -2 8 5 16.42 8.93 2 -2 -8 4 1.65 9.57 2 -2 -8 3 124.06 16.42 2 2 -8 -2 59.46 11.77 2 -2 -8 1 15.42 7.44 2 2 -8 0 6.65 8.52 2 2 -8 1 121.30 17.01 2 2 -8 2 95.41 17.08 2 2 8 3 5.63 7.49 2 2 8 4 16.20 9.62 2 2 8 5 38.64 9.76 2 -3 -1 10 5.06 8.82 2 -3 1 8 60.46 3.81 2 -3 1 7 334.38 26.98 2 -3 1 6 155.95 4.93 2 3 -1 -3 926.37 10.54 2 -3 1 2 606.87 4.54 2 -3 1 1 767.20 23.29 2 3 1 0 136.77 14.73 2 -3 1 -1 958.54 29.08 2 -3 1 -2 502.80 2.96 2 3 -1 4 0.12 3.77 2 3 -1 5 385.54 12.37 2 3 1 7 30.67 7.26 2 3 -1 8 29.23 8.52 2 3 1 9 120.74 12.43 2 3 -3 4 3.20 5.36 2 3 -3 8 16.07 6.48 2 3 -3 9 56.68 12.61 2 -3 -5 10 -3.80 13.45 2 -3 -5 4 63.38 7.63 2 -3 5 3 181.24 5.75 2 -3 -5 2 126.24 18.41 2 -3 -5 1 150.45 11.27 2 -3 -5 0 5.85 4.20 2 3 -5 1 333.27 10.80 2 3 -5 2 140.21 6.71 2 3 5 3 39.89 6.99 2 3 5 4 1.01 5.82 2 3 5 5 186.88 18.22 2 3 5 6 81.26 23.40 2 3 5 7 33.95 12.67 2 3 5 8 15.32 8.08 2 -3 -7 8 8.75 8.92 2 -3 -7 7 85.55 16.65 2 -3 7 6 18.84 8.82 2 -3 -7 5 24.79 10.76 2 -3 -7 4 22.71 7.95 2 -3 -7 3 135.92 13.40 2 3 -7 -2 24.00 4.78 2 -3 -7 1 70.83 7.89 2 3 -7 0 7.30 5.94 2 3 -7 1 256.08 14.66 2 3 7 2 82.89 14.22 2 3 -7 3 29.67 9.36 2 3 7 4 -0.52 8.28 2 3 7 5 105.87 15.95 2 3 -7 6 32.73 22.71 2 -3 -9 4 3.25 11.18 2 -3 -9 3 92.68 17.98 2 3 -9 -2 23.09 10.75 2 3 -9 -1 23.86 10.48 2 3 -9 0 1.95 9.49 2 3 -9 1 46.32 11.96 2 3 -9 2 16.68 13.65 2 -4 0 12 3.14 13.28 2 -4 0 11 21.12 10.33 2 -4 0 10 257.92 26.94 2 -4 0 9 310.73 16.51 2 -4 0 8 2.43 4.50 2 -4 0 7 9.65 5.85 2 -4 0 6 1428.84 48.30 2 -4 0 4 473.73 5.55 2 -4 0 3 12.64 2.65 2 -4 0 2 308.10 3.84 2 -4 0 1 4244.24 10.27 2 4 0 0 1767.87 129.70 2 4 0 1 963.96 8.31 2 4 0 2 1053.53 89.88 2 4 0 3 1545.97 11.54 2 4 0 4 153.22 6.52 2 4 0 5 1.94 3.69 2 4 0 6 111.20 20.34 2 -4 -2 12 40.65 13.91 2 -4 -2 10 4.27 11.18 2 -4 2 9 30.28 6.67 2 -4 2 8 150.90 4.43 2 -4 2 7 339.41 7.27 2 -4 2 6 -2.19 3.00 2 4 -2 -4 345.49 6.01 2 -4 -2 3 666.87 86.88 2 4 -2 -2 41.42 4.51 2 -4 2 1 223.63 13.85 2 4 -2 0 280.61 5.12 2 4 -2 4 2.05 8.67 2 4 -2 5 385.84 9.98 2 4 -4 5 -2.72 8.82 2 4 -4 8 159.93 14.56 2 -4 -6 9 6.16 14.39 2 -4 -6 8 33.35 11.72 2 -4 -6 6 7.58 7.30 2 4 -6 -5 42.24 7.05 2 4 -6 -4 78.92 26.11 2 4 -6 -2 0.80 5.32 2 -4 -6 1 69.20 10.79 2 -4 -6 0 67.23 7.51 2 4 -6 1 286.44 12.05 2 4 -6 2 11.68 7.99 2 4 -6 3 80.52 10.87 2 4 6 4 6.76 8.02 2 4 -6 5 130.70 39.04 2 4 6 6 22.21 17.18 2 4 -6 7 9.25 11.54 2 -4 8 6 119.78 47.23 2 4 -8 -5 357.24 31.62 2 -4 -8 4 28.69 9.75 2 4 -8 -3 -0.16 9.17 2 -4 -8 2 67.94 11.67 2 4 -8 -1 337.30 21.95 2 4 -8 0 110.49 13.08 2 4 -8 1 19.50 9.71 2 4 -8 2 102.36 19.62 2 4 -8 3 198.07 24.46 2 4 8 4 30.20 15.09 2 -5 -1 12 43.79 10.20 2 -5 -1 11 10.12 6.56 2 -5 1 10 44.26 8.19 2 -5 1 9 -4.81 6.52 2 -5 1 8 398.75 19.68 2 -5 -1 7 213.05 12.03 2 -5 -1 6 92.08 10.37 2 -5 1 5 126.30 4.38 2 -5 1 4 823.47 30.42 2 -5 1 3 731.46 16.92 2 5 -1 -2 5.42 2.35 2 -5 1 1 183.57 11.29 2 5 1 0 727.80 45.29 2 5 1 1 486.49 9.86 2 5 -1 2 16.80 2.59 2 5 1 3 151.77 7.27 2 5 -1 4 105.99 18.10 2 5 1 5 173.68 4.85 2 5 -1 6 16.13 4.40 2 5 1 7 28.60 9.46 2 5 1 8 16.04 11.22 2 5 1 9 69.85 14.89 2 -5 3 11 11.20 7.93 2 -5 3 10 26.58 9.02 2 -5 -3 9 1.86 6.22 2 -5 3 8 343.01 8.40 2 5 -3 -6 52.80 6.08 2 -5 3 5 52.39 4.29 2 5 -3 -4 491.74 18.33 2 5 -3 -3 375.13 7.54 2 5 -3 0 500.45 8.12 2 5 -3 1 541.44 54.48 2 5 -3 2 11.39 4.34 2 5 -3 3 143.97 19.21 2 5 -3 4 64.02 7.53 2 5 -3 5 116.52 9.26 2 5 -5 2 -1.90 7.59 2 5 -5 5 80.41 10.56 2 5 -5 6 -12.42 11.82 2 5 -5 7 5.85 12.02 2 5 -7 -6 11.69 11.52 2 -5 -7 5 -0.24 7.31 2 5 -7 -4 142.17 20.46 2 5 -7 -3 80.23 11.81 2 -5 -7 2 10.44 7.10 2 5 -7 -1 24.62 8.94 2 5 -7 0 126.81 12.11 2 5 -7 1 140.84 13.20 2 5 7 2 1.07 7.98 2 5 7 3 38.31 11.15 2 5 7 4 17.14 9.72 2 5 -7 5 28.02 15.86 2 -6 0 12 47.23 12.19 2 -6 0 11 0.98 7.02 2 -6 0 10 76.34 7.25 2 -6 0 9 51.42 5.68 2 -6 0 8 344.69 12.56 2 -6 0 7 107.28 6.60 2 -6 0 6 212.15 6.90 2 -6 0 5 22.62 3.72 2 -6 0 4 888.66 45.66 2 6 0 -3 551.10 17.99 2 -6 0 2 205.66 2.93 2 6 0 -1 7.57 2.46 2 6 0 0 515.82 6.52 2 6 0 1 368.89 8.20 2 6 0 2 33.11 3.93 2 6 0 3 12.10 3.76 2 6 0 4 270.54 19.70 2 6 0 5 140.36 9.17 2 6 0 7 40.86 10.43 2 6 0 8 27.27 12.05 2 -6 2 12 4.57 7.54 2 -6 2 11 34.65 13.94 2 -6 2 10 373.81 32.62 2 -6 -2 9 132.90 20.44 2 -6 -2 8 53.09 9.89 2 -6 -2 7 261.61 25.74 2 -6 -2 6 1282.15 83.21 2 6 -2 -5 221.39 11.19 2 -6 -2 4 2.45 3.58 2 6 -2 -3 409.71 11.00 2 6 2 -1 1872.06 109.03 2 6 -2 0 18.62 2.51 2 6 2 1 -0.01 2.90 2 6 2 2 628.89 40.46 2 6 -2 3 862.37 55.18 2 6 -2 4 95.47 11.21 2 6 2 5 48.96 6.66 2 6 2 6 98.37 11.20 2 6 2 7 168.67 12.66 2 6 2 8 6.20 13.89 2 -6 4 11 -1.13 7.80 2 -6 -4 10 28.43 20.79 2 -6 4 9 22.64 13.02 2 -6 4 8 232.88 10.38 2 -6 4 7 62.66 7.33 2 6 -4 -6 124.11 8.32 2 -6 4 5 6.77 5.63 2 6 -4 -4 418.07 13.30 2 6 -4 -3 221.03 9.57 2 6 -4 -2 93.78 14.25 2 6 -4 -1 5.61 4.36 2 6 -4 0 346.20 26.85 2 6 -4 1 193.66 19.65 2 6 4 2 12.10 10.63 2 6 -4 3 9.42 4.99 2 6 -4 4 157.23 28.98 2 6 -4 5 137.22 13.47 2 6 -4 6 2.96 8.65 2 6 -6 5 33.01 16.74 2 6 -6 6 127.16 19.88 2 -7 1 12 63.13 8.27 2 -7 -1 11 0.45 7.15 2 -7 -1 10 15.05 6.27 2 -7 -1 9 82.45 5.97 2 -7 -1 8 190.59 9.98 2 -7 -1 7 -0.04 4.23 2 -7 -1 6 126.32 5.94 2 -7 1 5 228.26 10.07 2 7 -1 -4 811.98 28.58 2 -7 -1 3 72.12 5.33 2 7 1 -2 175.46 24.34 2 7 -1 -1 55.60 9.00 2 7 -1 0 663.17 14.44 2 7 -1 1 75.42 6.59 2 7 -1 2 114.89 9.10 2 7 -1 3 0.60 5.79 2 7 1 4 299.90 13.65 2 7 1 5 86.82 7.74 2 7 1 6 10.20 9.38 2 7 1 8 25.90 13.77 2 -7 3 11 3.17 6.98 2 -7 3 10 13.68 7.88 2 -7 3 9 55.98 13.21 2 -7 3 8 122.70 13.15 2 -7 -3 7 -2.53 5.67 2 -7 3 6 91.37 7.87 2 7 -3 -5 166.74 16.48 2 7 -3 -4 624.74 31.95 2 7 -3 -3 37.01 5.11 2 7 -3 -2 190.02 12.62 2 7 -3 -1 23.27 5.68 2 7 3 0 494.00 57.79 2 7 -3 1 72.62 9.15 2 7 -3 2 58.21 11.04 2 7 3 3 -8.62 4.95 2 7 3 4 187.65 10.15 2 7 3 5 73.35 8.58 2 7 3 6 -4.43 8.33 2 -7 -5 10 4.00 7.13 2 -7 5 9 56.91 8.65 2 -7 5 8 73.20 28.23 2 -7 5 7 2.12 5.67 2 -7 5 5 61.52 7.10 2 7 -5 -4 280.79 5.83 2 7 -5 -3 15.60 4.67 2 7 -5 -2 57.68 4.36 2 7 -5 -1 28.21 4.59 2 7 -5 0 272.05 38.54 2 7 -5 1 6.23 7.11 2 7 -5 2 65.98 10.02 2 7 -5 3 -5.98 6.93 2 7 -5 4 191.52 17.28 2 7 5 6 -1.48 9.64 2 -8 0 12 25.63 7.53 2 -8 0 11 295.54 16.78 2 -8 0 10 347.02 9.63 2 -8 0 8 5.20 4.22 2 -8 0 7 396.82 12.49 2 -8 0 6 1140.82 29.32 2 -8 0 5 224.60 9.83 2 -8 0 4 329.42 18.67 2 8 0 -3 939.84 38.77 2 8 0 -2 1089.55 102.34 2 8 0 -1 0.89 3.29 2 8 0 0 15.27 4.08 2 8 0 1 628.13 32.63 2 8 0 2 1464.64 72.98 2 8 0 3 160.98 10.86 2 8 0 4 -6.61 4.12 2 8 0 5 23.93 5.71 2 8 0 6 236.52 14.58 2 8 0 7 80.18 13.43 2 -8 2 12 26.59 10.58 2 -8 -2 11 7.26 9.95 2 -8 -2 10 2.00 5.74 2 -8 -2 9 168.22 17.10 2 -8 2 8 108.37 11.98 2 -8 -2 7 11.50 4.84 2 -8 -2 6 49.75 6.46 2 -8 2 5 398.12 16.49 2 8 2 -4 350.00 13.37 2 8 -2 -3 5.82 3.72 2 8 -2 -2 157.48 10.79 2 8 2 -1 251.89 17.89 2 8 2 0 399.39 33.20 2 8 2 1 20.58 6.44 2 8 2 2 95.16 14.98 2 8 2 3 26.40 7.77 2 8 2 4 128.53 8.62 2 8 2 5 12.51 7.73 2 8 2 6 16.37 13.28 2 8 2 7 5.54 15.01 2 -8 -4 11 166.51 28.82 2 -8 4 10 214.76 17.47 2 -8 4 9 -6.91 7.25 2 -8 4 8 4.98 4.87 2 -8 4 7 205.95 8.83 2 -8 4 6 578.51 17.21 2 8 -4 -5 82.94 11.68 2 -8 -4 4 120.71 10.07 2 8 -4 -3 475.63 26.11 2 8 -4 -2 633.86 34.93 2 8 -4 -1 -0.14 6.87 2 8 4 0 3.75 4.73 2 8 -4 1 266.68 49.74 2 8 4 2 556.74 14.00 2 8 -4 3 73.23 18.31 2 8 4 4 -0.49 6.04 2 8 4 5 9.81 13.69 2 8 4 6 173.36 14.94 2 -9 1 12 11.00 9.00 2 -9 1 11 59.81 7.81 2 -9 -1 10 -1.00 6.55 2 -9 1 9 167.19 12.03 2 -9 -1 8 102.57 7.83 2 -9 1 7 30.83 5.05 2 9 -1 -6 -1.17 4.36 2 9 1 -5 352.80 21.26 2 9 1 -4 170.84 10.47 2 9 -1 -3 55.51 5.78 2 9 1 -2 20.40 4.64 2 9 -1 -1 319.15 30.90 2 9 -1 0 224.68 16.00 2 9 1 1 4.11 4.85 2 9 1 2 22.09 6.95 2 9 1 3 109.75 10.90 2 9 1 4 105.36 14.19 2 9 1 5 -2.06 7.83 2 9 1 6 19.49 10.52 2 -9 3 11 35.95 7.87 2 -9 3 10 1.03 6.75 2 -9 3 9 135.34 6.82 2 -9 3 8 66.34 7.75 2 -9 3 7 25.86 5.28 2 -9 3 6 -2.56 4.07 2 -9 -3 5 293.29 20.13 2 9 -3 -4 142.93 18.45 2 9 -3 -3 33.50 6.37 2 9 -3 -2 20.03 4.68 2 9 -3 -1 202.60 22.14 2 9 3 0 133.67 21.18 2 9 3 1 4.52 5.66 2 9 3 2 6.63 5.81 2 9 3 3 86.44 18.73 2 9 3 4 68.15 13.63 2 9 -3 5 -4.01 15.60 2 9 3 6 23.98 13.84 2 -9 5 10 -5.11 8.99 2 -9 5 9 3.40 9.20 2 9 7 0 20.91 13.92 2 9 7 1 -4.83 13.85 2 -10 0 12 -1.10 10.45 2 -10 0 11 33.61 7.78 2 -10 0 10 26.85 7.03 2 -10 0 9 168.05 8.40 2 -10 0 8 26.09 4.76 2 -10 0 7 57.87 6.30 2 -10 0 6 19.54 5.35 2 -10 0 5 363.90 14.73 2 10 0 -4 58.24 9.84 2 10 0 -3 54.18 9.31 2 10 0 -2 9.71 4.21 2 10 0 -1 362.90 40.04 2 10 0 0 46.71 10.13 2 10 0 1 45.34 8.37 2 10 0 2 4.22 6.08 2 10 0 3 140.23 23.84 2 10 0 4 17.21 13.02 2 10 0 5 -1.76 13.94 2 10 0 6 7.87 15.82 2 -10 2 11 164.97 10.94 2 -10 2 10 10.29 7.71 2 -10 2 9 -0.77 6.02 2 -10 2 8 236.82 11.93 2 -10 2 7 831.24 37.91 2 -10 2 6 259.05 22.84 2 -10 -2 5 4.01 5.60 2 10 -2 -4 54.60 7.50 2 10 -2 -3 692.80 34.71 2 10 2 -2 534.11 35.81 2 10 -2 -1 49.21 8.61 2 10 -2 0 156.27 20.76 2 10 2 1 331.84 45.42 2 10 2 2 123.23 18.34 2 10 2 3 3.42 9.06 2 10 -2 4 23.71 10.79 2 10 -2 5 111.43 24.84 2 -10 -6 8 9.90 13.86 2 -10 -6 7 156.14 15.45 2 -10 -6 6 44.85 11.49 2 -10 -6 5 8.55 11.59 2 -11 1 11 8.53 9.84 2 -11 1 10 125.49 8.87 2 -11 1 9 109.40 12.74 2 -11 1 8 1.32 6.53 2 -11 1 7 65.84 7.89 2 -11 -1 6 98.15 6.39 2 11 1 -5 258.45 14.02 2 11 1 -4 9.89 5.13 2 11 -1 -3 76.96 11.82 2 11 -1 -2 63.84 8.23 2 11 1 -1 202.96 27.07 2 11 -1 0 9.07 9.26 2 11 -1 1 36.64 10.70 2 11 1 2 4.48 7.09 2 11 -1 3 64.35 15.84 2 11 -1 4 -4.68 6.99 2 11 -1 5 8.56 14.85 2 11 -3 1 20.94 12.58 2 11 -3 2 4.79 11.65 2 11 -3 3 37.51 13.19 2 -11 -5 9 49.89 14.59 2 -11 -5 8 1.21 7.66 2 -11 -5 7 7.82 10.94 2 -11 -5 6 45.02 11.87 2 -11 -5 4 -0.40 10.16 2 11 -7 -4 11.34 9.04 2 11 -7 -3 17.84 7.95 2 11 7 -2 -1.24 11.90 2 -12 0 9 52.55 6.66 2 -12 0 8 260.21 7.55 2 12 0 -5 33.83 8.30 2 12 0 -4 609.93 14.31 2 12 0 -3 834.26 15.16 2 12 0 -2 1.17 9.27 2 12 0 -1 1.40 5.22 2 12 0 0 80.82 11.20 2 12 0 1 144.97 40.53 2 12 0 2 30.71 18.51 2 12 0 3 14.77 13.26 2 12 0 4 30.44 14.91 2 12 -2 3 51.58 15.79 2 -12 -4 9 34.29 12.91 2 -12 -4 8 153.74 8.28 2 -12 -4 7 103.40 11.55 2 -12 -4 6 7.06 8.82 2 -12 -6 6 49.22 13.77 2 12 -6 -5 63.23 17.19 2 12 -6 -4 4.21 9.46 2 12 -6 -3 16.28 10.27 2 12 6 -2 38.17 12.14 2 12 6 -1 48.91 7.76 2 13 -1 2 56.79 14.43 2 13 -1 3 15.03 15.29 2 -13 -3 9 3.96 8.09 2 -13 -3 8 20.61 7.13 2 -13 -3 7 -0.32 7.10 2 13 3 0 11.80 12.79 2 13 3 1 11.39 13.44 2 13 3 2 50.77 16.06 2 13 -5 -7 -0.05 9.30 2 13 -5 -6 114.85 16.67 2 13 -5 -5 33.95 15.60 2 13 -5 -4 20.45 9.69 2 13 -5 -3 2.69 8.29 2 13 5 -2 68.92 31.94 2 13 5 -1 42.12 14.48 2 -14 -2 9 33.99 14.91 2 14 2 -3 12.05 11.72 2 14 2 -2 -1.29 8.24 2 14 2 -1 77.32 13.98 2 14 2 0 438.34 20.30 2 14 2 1 36.44 14.31 2 14 -4 -7 13.63 10.07 2 14 -4 -6 78.96 17.44 2 14 -4 -5 6.16 8.83 2 14 4 -4 27.98 11.76 2 14 4 -3 -0.51 10.31 2 14 -4 -2 84.92 20.97 2 14 4 -1 17.61 17.28 2 15 -1 0 -7.97 15.63 2 15 -3 -7 24.65 13.26 2 15 -3 -6 25.59 8.80 2 15 3 -5 2.51 12.00 2 15 3 -4 8.68 14.10 2 15 3 -3 31.46 9.18 2 15 3 -2 36.53 14.28 2 0 2 0 238.43 4.60 3 0 4 -1 311.53 24.47 3 0 -4 2 1.05 2.33 3 0 -4 3 -1.30 3.96 3 0 -4 4 244.42 41.83 3 0 4 5 67.51 37.05 3 0 -4 6 12.68 8.49 3 0 -4 7 -3.70 3.92 3 0 -4 8 31.65 13.77 3 0 -4 9 -18.32 9.83 3 0 -4 10 -5.56 6.85 3 0 6 0 53.61 5.23 3 0 6 1 12.76 4.27 3 0 6 2 112.23 10.19 3 0 6 3 28.50 6.81 3 0 -6 4 27.99 5.30 3 0 -6 5 1.09 4.46 3 0 -6 6 51.24 11.42 3 0 6 7 26.08 8.11 3 0 -6 8 7.10 8.52 3 0 8 0 267.10 24.71 3 0 8 1 63.89 9.74 3 0 8 -2 -1.70 8.59 3 0 8 -3 6.43 10.38 3 0 8 4 87.54 14.98 3 0 8 -5 39.83 8.01 3 0 8 6 3.24 8.94 3 -1 -3 8 -8.29 7.08 3 -1 -3 7 52.28 5.73 3 -1 -3 6 99.79 6.44 3 -1 -3 5 -4.00 9.54 3 -1 3 4 -0.98 4.24 3 1 3 -3 247.57 5.44 3 1 3 -2 403.14 4.67 3 1 3 -1 3.29 3.73 3 1 3 0 80.97 8.39 3 1 3 1 223.38 4.86 3 1 3 4 107.54 6.04 3 1 3 5 9.04 6.28 3 1 3 6 157.31 9.27 3 1 3 7 38.70 8.23 3 1 3 9 0.58 9.91 3 -1 -5 10 12.75 10.67 3 -1 -5 9 3.09 6.82 3 -1 -5 8 -1.41 6.85 3 -1 5 7 28.56 6.66 3 -1 -5 6 26.91 9.29 3 -1 -5 5 19.37 4.50 3 1 5 -4 -3.83 7.08 3 1 5 -3 120.47 7.01 3 1 5 -2 167.69 21.63 3 1 5 -1 -2.66 4.34 3 1 5 0 41.51 9.42 3 1 5 1 60.81 4.85 3 -1 5 -2 130.72 20.40 3 1 -5 3 -6.70 6.29 3 1 -5 4 20.72 7.19 3 1 -5 5 17.56 5.26 3 1 -5 6 40.44 8.19 3 1 -5 7 -5.77 7.64 3 1 -5 8 10.57 7.42 3 1 -5 9 0.08 8.07 3 -1 -7 8 -4.63 7.42 3 -1 -7 7 29.22 9.41 3 -1 -7 6 23.46 12.00 3 -1 -7 5 4.24 7.38 3 1 7 -4 3.73 6.61 3 1 7 -3 35.74 9.04 3 1 7 -2 70.81 8.34 3 -1 7 1 -0.90 7.23 3 -1 7 0 14.44 8.50 3 1 7 1 35.22 8.23 3 -1 7 -2 68.18 16.80 3 1 7 3 -3.29 8.12 3 1 -7 4 21.86 8.57 3 1 -7 5 2.13 6.31 3 1 -7 6 60.91 10.11 3 1 -7 7 11.63 7.30 3 1 9 -4 2.87 10.99 3 -1 9 3 30.14 7.50 3 1 9 -2 29.58 11.13 3 1 9 -1 -4.06 7.59 3 1 9 0 11.85 7.96 3 1 9 1 3.77 11.80 3 -1 9 -2 41.12 10.40 3 -1 9 -3 -0.13 10.14 3 -2 0 9 -9.92 8.14 3 -2 0 8 -4.91 11.23 3 -2 0 7 141.46 90.55 3 -2 0 6 17.12 7.75 3 -2 0 3 73.37 6.01 3 -2 0 2 60.72 23.25 3 2 0 -1 45.49 1.62 3 2 0 0 86.90 1.52 3 -2 -4 10 0.70 12.67 3 -2 -4 9 10.58 6.01 3 -2 -4 8 5.83 4.84 3 -2 -4 7 151.93 7.28 3 2 4 -5 42.47 5.98 3 -2 -4 4 1.70 3.52 3 2 4 -3 317.42 9.61 3 2 4 -2 187.03 6.58 3 2 4 1 322.36 8.09 3 2 4 2 245.26 8.53 3 2 4 3 2.41 4.70 3 2 4 4 45.30 10.72 3 2 4 5 55.48 7.74 3 2 4 6 60.24 9.09 3 -2 -6 9 73.07 27.81 3 -2 -6 8 14.80 20.75 3 -2 -6 7 -1.30 6.25 3 -2 -6 6 7.80 5.55 3 -2 -6 5 159.43 8.11 3 -2 6 4 93.93 43.15 3 2 6 -3 15.09 10.84 3 2 6 -2 61.06 13.59 3 -2 6 1 269.58 31.73 3 2 6 0 137.00 43.98 3 2 6 1 0.27 5.27 3 2 6 2 13.84 5.33 3 2 -6 3 177.27 23.74 3 2 -6 4 56.10 17.09 3 2 -6 5 -11.63 9.62 3 2 6 6 2.67 7.82 3 2 -6 7 16.49 8.53 3 2 -6 8 37.00 8.25 3 2 8 -6 0.79 8.77 3 -2 8 5 11.81 8.16 3 -2 8 4 -0.17 8.54 3 -2 8 3 34.34 10.77 3 -2 8 2 17.30 11.46 3 -2 8 1 7.89 8.71 3 -2 8 0 3.68 6.98 3 -2 8 -1 43.14 8.84 3 -2 8 -2 35.56 10.09 3 2 8 3 -1.67 9.44 3 2 8 4 4.62 12.40 3 2 -8 5 14.83 7.74 3 -3 -1 12 9.22 14.27 3 -3 -1 11 20.42 11.08 3 -3 -1 10 -4.90 8.94 3 -3 1 9 40.17 7.67 3 -3 1 7 60.69 6.70 3 -3 1 6 49.01 4.21 3 -3 1 5 8.72 3.76 3 -3 -1 4 36.00 3.50 3 -3 1 3 196.31 46.17 3 -3 1 2 246.96 19.77 3 -3 1 1 337.63 5.36 3 3 1 2 195.96 5.12 3 3 1 4 -1.13 4.26 3 3 1 5 233.82 9.21 3 3 1 6 70.74 13.27 3 3 1 7 -8.69 8.83 3 3 1 8 13.58 7.80 3 3 -1 9 27.64 15.73 3 3 -1 10 29.93 18.68 3 3 3 4 0.03 5.34 3 3 3 8 9.50 8.90 3 3 3 9 34.84 9.20 3 -3 -5 10 4.60 8.11 3 -3 -5 9 35.35 13.74 3 -3 -5 8 23.22 9.40 3 -3 -5 7 96.49 9.24 3 -3 -5 6 21.83 6.25 3 3 5 -5 48.36 7.02 3 3 5 -4 25.91 4.11 3 3 5 -3 225.54 8.08 3 3 5 -2 79.10 6.76 3 3 5 -1 70.61 6.39 3 3 5 0 1.36 3.71 3 3 5 1 173.27 11.99 3 3 5 2 76.71 5.38 3 3 5 3 15.14 7.63 3 3 5 4 -0.77 6.47 3 3 5 5 104.95 10.01 3 3 5 6 24.28 9.62 3 3 5 7 13.22 15.79 3 -3 7 8 0.74 7.87 3 -3 7 7 21.29 17.70 3 -3 7 6 0.42 9.96 3 3 7 -5 9.91 8.77 3 -3 7 4 4.87 7.56 3 -3 7 3 40.07 15.14 3 -3 7 2 -3.47 12.67 3 3 7 -1 25.03 6.48 3 -3 7 0 -3.76 9.80 3 -3 7 -1 41.03 13.38 3 3 7 2 21.64 21.49 3 -3 7 -3 12.55 6.81 3 3 -7 4 -3.55 7.00 3 3 -7 5 22.38 9.67 3 3 -7 6 1.88 12.59 3 3 9 -4 -1.29 9.07 3 3 9 -3 14.29 14.08 3 3 9 -2 11.54 11.28 3 3 9 -1 6.83 7.78 3 3 9 0 -0.68 8.12 3 -3 9 -1 23.00 9.58 3 -3 9 -2 13.71 9.52 3 -4 0 12 -4.42 11.66 3 -4 0 11 -11.81 9.79 3 -4 0 10 50.21 10.84 3 -4 0 9 115.97 8.36 3 -4 0 8 0.73 4.03 3 -4 0 7 2.03 4.69 3 -4 0 6 477.78 40.52 3 -4 0 4 193.59 4.48 3 -4 0 3 5.34 2.10 3 -4 0 2 107.85 5.08 3 -4 0 1 1589.35 45.50 3 4 0 0 821.45 5.30 3 4 0 1 359.62 6.44 3 4 0 2 218.31 4.47 3 4 0 3 666.46 11.04 3 4 0 4 63.66 6.89 3 4 0 5 3.29 4.52 3 4 0 6 26.89 28.21 3 4 0 8 64.39 16.10 3 4 0 9 -3.75 5.78 3 -4 2 8 -19.60 7.13 3 -4 2 7 63.23 4.33 3 -4 2 6 -10.88 2.88 3 -4 2 5 26.71 3.67 3 -4 2 4 12.26 4.54 3 -4 2 3 111.93 4.95 3 4 2 -2 17.30 2.88 3 4 2 -1 76.02 6.33 3 4 2 0 53.99 6.73 3 4 -2 1 287.24 4.92 3 4 2 3 44.76 5.90 3 4 -2 4 -5.24 6.44 3 4 -2 6 24.26 6.17 3 4 2 7 26.39 17.73 3 4 2 8 0.53 11.08 3 4 2 9 23.72 16.42 3 4 4 5 -2.54 8.81 3 4 4 8 95.37 12.90 3 -4 -6 9 4.90 10.38 3 -4 -6 8 33.78 11.35 3 -4 -6 7 64.43 16.56 3 -4 -6 6 2.26 5.66 3 -4 -6 5 16.85 7.96 3 4 6 -4 47.94 8.14 3 4 6 -3 151.09 13.24 3 4 6 -2 6.03 7.02 3 4 6 -1 33.26 6.87 3 4 6 0 29.14 5.93 3 4 6 1 151.32 9.67 3 4 6 2 9.25 5.71 3 4 6 3 41.60 10.92 3 4 6 4 5.02 7.06 3 4 6 5 79.98 9.91 3 4 6 6 24.42 17.85 3 4 6 7 -0.47 17.27 3 4 8 -6 13.23 11.75 3 4 8 -5 -1.52 29.44 3 -4 8 4 -14.64 11.80 3 4 8 -3 2.77 8.54 3 4 8 -2 26.75 8.46 3 -4 8 1 110.43 37.99 3 -4 8 0 50.87 30.13 3 4 8 1 13.89 9.06 3 4 8 2 57.12 15.60 3 4 8 3 111.94 19.46 3 4 8 4 12.80 19.94 3 -5 1 12 11.32 11.18 3 -5 -1 11 9.91 9.62 3 -5 1 10 11.27 6.02 3 -5 -1 9 -12.69 5.34 3 -5 -1 8 149.50 18.18 3 -5 1 7 85.41 7.11 3 -5 -1 6 25.24 8.60 3 -5 1 5 47.96 5.78 3 -5 1 4 250.33 29.43 3 -5 -1 3 270.02 19.27 3 -5 -1 2 0.58 2.28 3 5 -1 -1 76.79 5.48 3 5 -1 0 269.57 58.43 3 5 -1 2 6.26 2.24 3 5 1 3 65.00 5.19 3 5 -1 4 46.41 7.50 3 5 -1 5 72.07 8.18 3 5 -1 6 10.05 6.16 3 5 -1 7 3.79 8.00 3 5 -1 8 4.37 11.57 3 5 -1 9 15.02 12.72 3 -5 3 9 1.17 8.62 3 -5 3 8 49.55 7.50 3 -5 3 7 48.01 8.75 3 -5 3 6 -0.78 6.07 3 -5 -3 5 17.13 4.32 3 -5 -3 4 143.56 21.44 3 5 3 -3 98.33 3.74 3 -5 3 2 -1.34 2.42 3 -5 3 1 46.92 8.39 3 5 -3 0 174.45 36.62 3 5 -3 1 172.57 12.92 3 5 -3 2 4.49 3.97 3 5 -3 3 44.25 8.28 3 5 -3 4 9.27 14.78 3 5 3 5 27.68 20.25 3 5 3 6 7.87 8.15 3 5 -3 7 9.31 15.74 3 5 -3 8 13.82 21.25 3 5 5 2 3.06 7.69 3 5 5 3 38.75 9.03 3 5 5 5 66.25 10.36 3 5 5 6 7.12 10.76 3 5 5 7 14.66 13.36 3 -5 -7 8 34.62 6.16 3 -5 -7 7 13.95 5.06 3 5 7 -6 3.65 9.02 3 5 7 -5 2.88 9.53 3 5 7 -4 66.95 10.86 3 5 7 -3 39.07 7.14 3 5 7 -2 4.03 6.78 3 5 7 -1 18.19 7.61 3 5 7 0 69.79 8.85 3 5 7 1 107.73 15.52 3 5 7 2 -0.16 9.92 3 5 7 3 26.59 13.57 3 5 7 4 1.24 18.06 3 5 7 5 32.62 20.21 3 5 9 -3 7.82 8.70 3 5 9 -2 3.68 8.75 3 5 9 -1 -1.04 10.61 3 5 9 0 9.90 9.14 3 -6 0 12 23.97 13.20 3 -6 0 11 1.88 7.64 3 -6 0 10 33.07 9.00 3 -6 0 9 22.68 5.11 3 -6 0 8 152.52 6.86 3 -6 0 7 48.67 4.68 3 -6 0 6 81.98 6.26 3 -6 0 5 7.70 3.78 3 -6 0 4 303.15 33.75 3 -6 0 3 186.83 17.49 3 6 0 -2 80.49 6.80 3 6 0 -1 1.19 2.13 3 6 0 2 13.05 3.70 3 6 0 3 4.28 3.83 3 6 0 4 109.88 10.11 3 6 0 5 70.32 10.27 3 6 0 7 23.97 7.13 3 6 0 8 11.55 10.12 3 -6 2 12 5.82 9.54 3 -6 -2 11 -0.33 9.25 3 -6 -2 10 111.76 12.33 3 -6 2 9 34.81 8.57 3 -6 2 8 16.58 8.02 3 -6 2 7 55.27 18.93 3 -6 2 6 420.13 40.57 3 -6 2 5 75.79 7.26 3 6 2 -4 0.72 2.37 3 6 2 -3 144.56 14.52 3 6 2 -2 1538.01 62.15 3 6 -2 -1 781.28 55.29 3 6 2 0 8.46 3.71 3 6 -2 1 1.84 3.47 3 6 -2 2 255.66 22.31 3 6 2 3 340.23 24.21 3 6 2 4 39.79 6.51 3 6 -2 5 22.60 7.22 3 6 -2 6 71.24 19.89 3 6 -2 7 63.08 12.34 3 6 -2 8 2.36 11.78 3 -6 4 9 -0.24 10.00 3 -6 4 8 57.52 29.74 3 -6 4 7 13.13 4.39 3 -6 4 6 20.94 5.60 3 -6 4 5 -7.58 5.91 3 -6 -4 4 113.67 24.30 3 -6 4 3 62.08 10.70 3 6 4 -2 29.27 7.84 3 6 4 -1 0.40 3.96 3 6 -4 0 136.83 15.84 3 6 4 1 77.33 13.42 3 6 4 2 8.48 6.97 3 6 -4 3 1.01 5.58 3 6 -4 4 62.42 38.10 3 6 4 5 30.47 17.81 3 6 4 6 -1.71 9.64 3 6 -4 7 3.86 9.32 3 6 6 5 21.66 16.63 3 6 6 6 87.65 21.28 3 6 8 -2 -1.40 13.82 3 6 8 -1 0.13 13.84 3 6 8 0 19.68 14.19 3 6 8 1 19.62 18.00 3 6 8 2 10.39 17.14 3 -7 -1 12 27.66 11.18 3 -7 -1 11 -2.96 6.00 3 -7 -1 10 8.63 5.93 3 -7 1 9 42.39 6.41 3 -7 -1 8 83.77 8.80 3 -7 1 7 -0.75 3.40 3 -7 -1 6 47.40 4.57 3 -7 1 5 84.79 6.02 3 -7 1 4 310.04 17.38 3 -7 1 3 29.50 2.78 3 7 1 -2 83.62 3.64 3 7 1 -1 26.19 3.06 3 7 -1 0 296.55 11.35 3 7 1 1 30.17 4.33 3 7 1 2 47.18 6.32 3 7 1 3 -0.62 4.62 3 7 -1 4 126.32 12.46 3 7 -1 5 37.57 6.27 3 7 1 6 5.34 7.01 3 7 1 7 6.59 12.04 3 7 -1 8 18.81 10.65 3 -7 -3 11 -3.75 7.40 3 -7 -3 10 -0.14 6.35 3 -7 3 9 10.17 7.00 3 -7 3 8 39.60 10.59 3 -7 3 7 -10.63 5.30 3 -7 -3 6 31.55 5.80 3 -7 3 5 39.54 10.95 3 -7 3 4 207.12 15.19 3 -7 -3 3 12.16 4.19 3 7 3 -2 70.77 7.10 3 -7 3 1 9.29 4.50 3 7 3 0 196.19 20.71 3 7 -3 1 24.84 5.65 3 7 3 2 23.73 7.22 3 7 3 3 -3.61 6.10 3 7 3 4 73.31 9.52 3 7 3 5 25.20 9.18 3 7 3 6 2.78 9.27 3 7 3 7 1.41 9.37 3 -7 5 9 7.50 12.77 3 -7 5 8 12.38 19.17 3 -7 5 7 -1.27 7.38 3 7 5 -6 5.02 6.68 3 -7 5 5 4.36 7.86 3 -7 5 4 69.01 16.16 3 7 5 -3 9.35 5.17 3 7 5 -2 27.20 7.21 3 -7 5 1 14.78 6.97 3 -7 5 0 198.37 19.09 3 7 5 1 16.99 8.82 3 7 -5 2 17.74 13.38 3 7 5 3 2.12 7.56 3 7 5 4 50.29 10.89 3 7 5 5 3.39 12.91 3 7 5 6 5.17 7.74 3 7 7 4 64.31 19.50 3 -8 0 12 21.97 13.44 3 -8 0 11 148.04 15.37 3 -8 0 10 167.64 12.28 3 -8 0 9 2.82 7.68 3 -8 0 8 4.69 4.00 3 -8 0 7 163.49 8.36 3 -8 0 6 447.06 15.04 3 -8 0 5 85.35 3.04 3 -8 0 4 130.66 9.05 3 8 0 -3 374.17 17.64 3 -8 0 2 500.34 19.68 3 8 0 -1 0.01 3.16 3 8 0 0 7.36 4.43 3 8 0 1 296.99 9.91 3 8 0 2 646.69 44.20 3 8 0 3 66.28 8.70 3 8 0 4 -2.43 6.11 3 8 0 5 5.05 11.21 3 8 0 6 118.43 13.27 3 8 0 7 42.74 9.89 3 -8 2 12 6.02 8.74 3 -8 -2 11 -1.56 7.15 3 -8 -2 10 2.43 7.37 3 -8 -2 9 57.53 13.06 3 -8 2 8 43.56 8.79 3 -8 2 7 5.12 5.23 3 -8 -2 6 19.64 5.08 3 8 2 -5 141.77 9.76 3 8 2 -4 125.75 9.52 3 8 2 -3 0.01 3.68 3 8 -2 -2 65.38 5.47 3 8 2 -1 103.36 8.89 3 8 -2 0 169.13 12.79 3 8 2 1 7.73 5.53 3 8 -2 2 40.66 6.54 3 8 2 3 11.97 5.84 3 8 -2 4 34.96 8.28 3 8 -2 5 3.82 6.60 3 8 2 6 8.96 8.41 3 8 -2 7 5.09 10.20 3 -8 -4 11 -8.30 11.08 3 -8 -4 10 26.59 15.43 3 -8 -4 9 -5.51 5.45 3 -8 -4 8 -1.98 6.70 3 -8 4 7 50.48 8.86 3 -8 -4 6 117.01 34.20 3 -8 4 5 18.80 9.05 3 -8 -4 4 45.87 7.84 3 -8 4 3 188.99 20.52 3 8 4 -2 296.62 21.40 3 8 4 -1 4.82 5.73 3 8 -4 0 0.33 6.14 3 8 4 1 128.45 20.17 3 8 4 2 349.90 13.20 3 8 4 3 37.35 10.56 3 8 4 4 2.20 8.50 3 8 4 5 -2.73 9.63 3 8 4 6 3.07 24.79 3 8 6 1 11.67 13.66 3 8 6 2 30.19 16.84 3 8 6 3 14.25 16.06 3 8 6 4 50.63 18.15 3 8 8 -1 1.92 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604.39 71.76 -2 -8 8 2 604.39 71.76 3 8 8 -1 32.53 38.44 -1 -8 -8 1 32.53 38.44 -2 16 0 -6 32.53 38.44 3 8 -8 -1 9.12 61.77 -1 16 0 -6 9.12 61.77 -2 -8 8 1 9.12 61.77 3 -8 -8 0 -2.90 47.88 -1 8 8 0 -2.90 47.88 -2 -16 0 7 -2.90 47.88 3 8 -8 0 30.45 58.27 -1 16 0 -7 30.45 58.27 -2 -8 8 0 30.45 58.27 3 9 5 -8 214.66 37.96 -1 -3 -7 6 214.66 37.96 -2 12 2 2 214.66 37.96 3 9 7 -7 86.60 55.12 -1 -6 -8 6 86.60 55.12 -2 15 1 0 86.60 55.12 3 9 -7 -7 34.20 68.95 -1 15 -1 0 34.20 68.95 -2 -6 8 6 34.20 68.95 3 9 7 -6 6.71 30.16 -1 -6 -8 5 6.71 30.16 -2 15 1 -1 6.71 30.16 3 9 -7 -6 -9.75 34.37 -1 15 -1 -1 -9.75 34.37 -2 -6 8 5 -9.75 34.37 3 9 7 -5 408.68 36.76 -1 -6 -8 4 408.68 36.76 -2 15 1 -2 408.68 36.76 3 9 -7 -5 380.58 48.99 -1 15 -1 -2 380.58 48.99 -2 -6 8 4 380.58 48.99 3 9 7 -4 206.73 48.24 -1 -6 -8 3 206.73 48.24 -2 15 1 -3 206.73 48.24 3 9 -7 -4 198.39 47.88 -1 15 -1 -3 198.39 47.88 -2 -6 8 3 198.39 47.88 3 9 7 -3 76.12 31.28 -1 -6 -8 2 76.12 31.28 -2 15 1 -4 76.12 31.28 3 9 -7 -3 20.04 50.50 -1 15 -1 -4 20.04 50.50 -2 -6 8 2 20.04 50.50 3 9 7 -2 -2.51 42.91 -1 -6 -8 1 -2.51 42.91 -2 15 1 -5 -2.51 42.91 3 9 -7 -2 16.68 44.34 -1 15 -1 -5 16.68 44.34 -2 -6 8 1 16.68 44.34 3 9 -7 -1 313.85 52.81 -1 15 -1 -6 313.85 52.81 -2 -6 8 0 313.85 52.81 3 -9 -7 0 195.29 48.48 -1 6 8 1 195.29 48.48 -2 -15 -1 7 195.29 48.48 3 -9 -7 -1 -11.93 48.15 -1 6 8 2 -11.93 48.15 -2 -15 -1 8 -11.93 48.15 3 10 -6 -4 111.41 39.51 -1 14 -2 -3 111.41 39.51 -2 -4 8 2 111.41 39.51 3 -11 -1 -5 18.50 35.27 -1 -4 6 9 18.50 35.27 -2 -7 -5 10 18.50 35.27 3 11 -7 -4 8.35 38.03 -1 16 -2 -4 8.35 38.03 -2 -5 9 2 8.35 38.03 3 -12 0 -1 1305.81 26.72 -1 -6 6 6 1305.81 26.72 -2 -6 -6 6 1305.81 26.72 3 -12 0 -2 285.74 26.36 -1 -6 6 7 285.74 26.36 -2 -6 -6 7 285.74 26.36 3 -12 0 -4 240.81 31.05 -1 -6 6 9 240.81 31.05 -2 -6 -6 9 240.81 31.05 3 13 1 -8 119.14 40.39 -1 5 -7 3 119.14 40.39 -2 8 6 2 119.14 40.39 3 13 1 -1 314.39 37.92 -1 5 -7 -4 314.39 37.92 -2 8 6 -5 314.39 37.92 3 -13 -1 -1 32.60 19.63 -1 -5 7 6 32.60 19.63 -2 -8 -6 7 32.60 19.63 3 -13 -1 -2 238.21 42.73 -1 -5 7 7 238.21 42.73 -2 -8 -6 8 238.21 42.73 3 -13 -1 -3 227.20 100.10 -1 -5 7 8 227.20 100.10 -2 -8 -6 9 227.20 100.10 3 14 0 -9 -31.97 72.38 -1 7 -7 3 -31.97 72.38 -2 7 7 3 -31.97 72.38 3 14 0 -8 113.47 30.01 -1 7 -7 2 113.47 30.01 -2 7 7 2 113.47 30.01 3 14 0 -7 175.30 37.54 -1 7 -7 1 175.30 37.54 -2 7 7 1 175.30 37.54 3 14 0 -6 705.86 94.76 -1 7 -7 0 705.86 94.76 -2 7 7 0 705.86 94.76 3 14 0 -5 -7.68 23.78 -1 7 -7 -1 -7.68 23.78 -2 7 7 -1 -7.68 23.78 3 14 0 -4 227.78 47.46 -1 7 -7 -2 227.78 47.46 -2 7 7 -2 227.78 47.46 3 14 0 -3 36.28 22.56 -1 7 -7 -3 36.28 22.56 -2 7 7 -3 36.28 22.56 3 14 0 -2 742.30 26.80 -1 7 -7 -4 742.30 26.80 -2 7 7 -4 742.30 26.80 3 14 0 -1 140.91 44.31 -1 7 -7 -5 140.91 44.31 -2 7 7 -5 140.91 44.31 3 14 0 0 104.11 43.12 -1 7 -7 -6 104.11 43.12 -2 7 7 -6 104.11 43.12 3 -14 0 -1 -24.60 36.27 -1 -7 7 7 -24.60 36.27 -2 -7 -7 7 -24.60 36.27 3 -14 0 -2 177.75 26.48 -1 -7 7 8 177.75 26.48 -2 -7 -7 8 177.75 26.48 3 15 1 -9 11.72 59.55 -1 6 -8 3 11.72 59.55 -2 9 7 2 11.72 59.55 3 15 1 -8 39.86 32.84 -1 6 -8 2 39.86 32.84 -2 9 7 1 39.86 32.84 3 15 1 -7 318.08 52.37 -1 6 -8 1 318.08 52.37 -2 9 7 0 318.08 52.37 3 15 -1 -7 216.56 44.72 -1 9 -7 0 216.56 44.72 -2 6 8 1 216.56 44.72 3 15 1 -6 308.86 29.49 -1 6 -8 0 308.86 29.49 -2 9 7 -1 308.86 29.49 3 15 -1 -6 271.45 34.17 -1 9 -7 -1 271.45 34.17 -2 6 8 0 271.45 34.17 3 15 1 -5 5.90 28.59 -1 6 -8 -1 5.90 28.59 -2 9 7 -2 5.90 28.59 3 15 -1 -5 20.34 38.44 -1 9 -7 -2 20.34 38.44 -2 6 8 -1 20.34 38.44 3 15 1 -4 70.41 35.36 -1 6 -8 -2 70.41 35.36 -2 9 7 -3 70.41 35.36 3 15 1 -3 186.63 42.39 -1 6 -8 -3 186.63 42.39 -2 9 7 -4 186.63 42.39 3 15 -1 -3 153.10 25.08 -1 9 -7 -4 153.10 25.08 -2 6 8 -3 153.10 25.08 3 15 1 -2 403.09 67.58 -1 6 -8 -4 403.09 67.58 -2 9 7 -5 403.09 67.58 3 15 -1 -2 364.91 40.81 -1 9 -7 -5 364.91 40.81 -2 6 8 -4 364.91 40.81 3 15 1 -1 -6.73 47.47 -1 6 -8 -5 -6.73 47.47 -2 9 7 -6 -6.73 47.47 3 15 -1 -1 16.25 27.45 -1 9 -7 -6 16.25 27.45 -2 6 8 -5 16.25 27.45 3 15 1 0 19.19 53.88 -1 6 -8 -6 19.19 53.88 -2 9 7 -7 19.19 53.88 3 15 -1 0 31.04 26.18 -1 9 -7 -7 31.04 26.18 -2 6 8 -6 31.04 26.18 3 16 0 -7 -11.09 28.86 -1 8 -8 0 -11.09 28.86 -2 8 8 0 -11.09 28.86 3 16 0 -6 28.33 28.50 -1 8 -8 -1 28.33 28.50 -2 8 8 -1 28.33 28.50 3 16 0 -5 614.59 60.23 -1 8 -8 -2 614.59 60.23 -2 8 8 -2 614.59 60.23 3 16 0 -4 812.38 49.11 -1 8 -8 -3 812.38 49.11 -2 8 8 -3 812.38 49.11 3 16 0 -3 154.69 32.57 -1 8 -8 -4 154.69 32.57 -2 8 8 -4 154.69 32.57 3 16 0 -2 147.28 42.95 -1 8 -8 -5 147.28 42.95 -2 8 8 -5 147.28 42.95 3 ; _shelx_hkl_checksum 27374 _shelx_res_file ; TITL final_cm_a.res in C2/m 3domain.res created by SHELXL-2019/3 at 09:07:29 on 19-Jun-2023 REM Old TITL final_cm in Cm REM SHELXT solution in C2/m: R1 0.062, Rweak 0.013, Alpha 0.046 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: As2 N9 Ni3 O2 CELL 0.71073 10.1780 5.9156 7.7158 90.000 112.658 90.000 ZERR 2.000 0.0020 0.0011 0.0014 0.000 0.014 0.000 LATT 7 SYMM -X, Y, -Z SFAC H AS N NI O UNIT 14 4 2 6 20 TEMP 23 L.S. 10 BOND dfix H1 O2 0.89 dfix H2 O4 0.89 omit 2 2 3 LIST 4 FMAP 2 size 0.05 0.04 0.03 acta merg 0 PLAN 20 WGHT 0.150700 BASF 0.26177 0.09377 FVAR 0.50584 NI1 4 0.000000 0.000000 0.000000 10.25000 0.01323 0.01005 = 0.01434 0.00000 0.00627 0.00000 NI2 4 0.250000 0.250000 0.000000 10.50000 0.01357 0.01020 = 0.01534 0.00139 0.00721 0.00010 AS1 2 0.068632 0.500000 0.239479 10.50000 0.01179 0.00880 = 0.01267 0.00000 0.00618 0.00000 O1 5 0.212952 0.500000 0.181328 10.50000 0.01355 0.01182 = 0.01553 0.00000 0.00723 0.00000 O2 5 0.118113 0.500000 0.473660 10.50000 0.02362 0.02766 = 0.01219 0.00000 0.00712 0.00000 O3 5 -0.030933 0.261926 0.164170 11.00000 0.01235 0.01112 = 0.01619 -0.00186 0.00627 -0.00178 O4 5 0.207715 0.000000 0.135749 10.50000 0.01190 0.01216 = 0.01506 0.00000 0.00599 0.00000 N1 3 0.000000 0.000000 0.500000 10.25000 0.03708 0.01632 = 0.01825 0.00000 0.01066 0.00000 H1 1 0.032951 0.500000 0.481360 10.25000 -1.50000 H2 1 0.222802 0.000000 0.256961 10.50000 -1.50000 HKLF 5 REM final_cm_a.res in C2/m REM wR2 = 0.2288, GooF = S = 1.040, Restrained GooF = 1.039 for all data REM R1 = 0.0675 for 2214 Fo > 4sig(Fo) and 0.0950 for all 3235 data REM 54 parameters refined using 2 restraints END WGHT 0.1506 0.0000 REM Highest difference peak 2.953, deepest hole -2.295, 1-sigma level 0.610 Q1 1 0.2134 0.5000 0.3978 10.50000 0.05 2.48 Q2 1 0.1227 0.1256 -0.0025 11.00000 0.05 2.44 Q3 1 0.1482 0.5000 0.1829 10.50000 0.05 2.26 Q4 1 -0.0386 0.2720 0.3693 11.00000 0.05 1.91 Q5 1 0.0927 0.4448 0.3559 11.00000 0.05 1.89 Q6 1 -0.0588 0.3754 0.2453 11.00000 0.05 1.82 Q7 1 0.1334 0.1303 0.5055 11.00000 0.05 1.79 Q8 1 0.1899 0.4035 0.2230 11.00000 0.05 1.78 Q9 1 0.2557 0.3146 0.2405 11.00000 0.05 1.71 Q10 1 0.0670 0.0000 -0.0126 10.50000 0.05 1.69 Q11 1 0.0253 0.0689 0.5974 11.00000 0.05 1.66 Q12 1 -0.0083 0.5000 0.2467 10.50000 0.05 1.64 Q13 1 0.3710 0.1408 -0.0127 11.00000 0.05 1.63 Q14 1 -0.0200 0.5000 0.3128 10.50000 0.05 1.60 Q15 1 0.2030 0.1063 0.2996 11.00000 0.05 1.59 Q16 1 0.3063 0.5000 0.2682 10.50000 0.05 1.58 Q17 1 0.0821 0.0972 0.5451 11.00000 0.05 1.55 Q18 1 0.1037 0.0000 0.6568 10.50000 0.05 1.54 Q19 1 0.3369 0.3557 0.3565 11.00000 0.05 1.49 Q20 1 0.0590 0.3324 0.2475 11.00000 0.05 1.47 ; _shelx_res_checksum 26012 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ni Ni1 0.000000 0.000000 0.000000 0.0123(4) Uani d 1 . . Ni Ni2 0.250000 0.250000 0.000000 0.0125(4) Uani d 1 . . As As1 0.06863(12) 0.500000 0.23948(15) 0.0106(3) Uani d 1 . . O O1 0.2130(9) 0.500000 0.1813(13) 0.0131(14) Uani d 1 . . O O2 0.1181(11) 0.500000 0.4737(14) 0.0211(19) Uani d 1 . . O O3 -0.0309(6) 0.2619(10) 0.1642(9) 0.0130(10) Uani d 1 . . O O4 0.2077(9) 0.000000 0.1357(12) 0.0128(14) Uani d 1 . . N N1 0.000000 0.000000 0.500000 0.024(3) Uani d 1 . . H H1 0.03(2) 0.500000 0.48(7) 0.036 Uiso d 0.5 . . H H2 0.22(2) 0.000000 0.257(9) 0.036 Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Ni1 0.0132(9) 0.0101(8) 0.0143(10) 0.000 0.0063(7) 0.000 Ni2 0.0136(6) 0.0102(6) 0.0153(7) 0.0001(4) 0.0072(5) 0.0014(4) As1 0.0118(5) 0.0088(5) 0.0127(5) 0.000 0.0062(4) 0.000 O1 0.014(3) 0.012(3) 0.016(4) 0.000 0.007(3) 0.000 O2 0.024(4) 0.028(5) 0.012(4) 0.000 0.007(3) 0.000 O3 0.012(2) 0.011(2) 0.016(3) -0.0018(18) 0.0063(19) -0.0019(18) O4 0.012(3) 0.012(3) 0.015(4) 0.000 0.006(3) 0.000 N1 0.037(9) 0.016(6) 0.018(7) 0.000 0.011(6) 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O4 Ni1 O4 . 5 180.0 ? O4 Ni1 O3 . 5 86.6(2) ? O4 Ni1 O3 5 5 93.4(2) ? O4 Ni1 O3 . 6 93.4(2) ? O4 Ni1 O3 5 6 86.6(2) ? O3 Ni1 O3 5 6 84.9(3) ? O4 Ni1 O3 . 2 86.6(2) ? O4 Ni1 O3 5 2 93.4(2) ? O3 Ni1 O3 5 2 95.1(3) ? O3 Ni1 O3 6 2 180.0(3) ? O4 Ni1 O3 . . 93.4(2) ? O4 Ni1 O3 5 . 86.6(2) ? O3 Ni1 O3 5 . 180.0 ? O3 Ni1 O3 6 . 95.1(3) ? O3 Ni1 O3 2 . 84.9(3) ? O4 Ni2 O4 7 . 180.0 ? O4 Ni2 O3 7 8 87.0(3) ? O4 Ni2 O3 . 8 93.1(3) ? O4 Ni2 O3 7 2 93.0(3) ? O4 Ni2 O3 . 2 86.9(3) ? O3 Ni2 O3 8 2 180.0 ? O4 Ni2 O1 7 . 87.6(3) ? O4 Ni2 O1 . . 92.4(3) ? O3 Ni2 O1 8 . 92.4(3) ? O3 Ni2 O1 2 . 87.6(3) ? O4 Ni2 O1 7 7 92.4(3) ? O4 Ni2 O1 . 7 87.6(3) ? O3 Ni2 O1 8 7 87.6(3) ? O3 Ni2 O1 2 7 92.4(3) ? O1 Ni2 O1 . 7 180.0(4) ? O2 As1 O1 . . 110.7(5) ? O2 As1 O3 . 6_565 105.1(3) ? O1 As1 O3 . 6_565 111.9(3) ? O2 As1 O3 . . 105.1(3) ? O1 As1 O3 . . 111.9(3) ? O3 As1 O3 6_565 . 111.8(4) ? As1 O1 Ni2 . . 123.8(3) ? As1 O1 Ni2 . 4 123.8(3) ? Ni2 O1 Ni2 . 4 86.1(3) ? As1 O3 Ni2 . 2 126.1(3) ? As1 O3 Ni1 . . 127.5(3) ? Ni2 O3 Ni1 2 . 89.0(2) ? Ni2 O4 Ni2 4_545 . 98.4(4) ? Ni2 O4 Ni1 4_545 . 97.4(3) ? Ni2 O4 Ni1 . . 97.4(3) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Ni1 O4 . 1.965(8) ? Ni1 O4 5 1.965(8) ? Ni1 O3 5 2.100(6) ? Ni1 O3 6 2.100(6) ? Ni1 O3 2 2.100(6) ? Ni1 O3 . 2.100(6) ? Ni2 O4 7 1.954(6) ? Ni2 O4 . 1.954(6) ? Ni2 O3 8 2.099(6) ? Ni2 O3 2 2.099(6) ? Ni2 O1 . 2.166(7) ? Ni2 O1 7 2.166(7) ? As1 O2 . 1.679(10) ? As1 O1 . 1.693(9) ? As1 O3 6_565 1.701(6) ? As1 O3 . 1.701(6) ?