#------------------------------------------------------------------------------ #$Date: 2024-05-04 04:52:17 +0300 (Sat, 04 May 2024) $ #$Revision: 291490 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/31/2023115.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023115 loop_ _publ_author_name 'Gorbunov, Alexander' 'Bezzubov, Stanislav' 'Malakhova, Maria' 'Kovalev, Vladimir' 'Vatsouro, Ivan' _publ_section_title ; Synthesis and crystal structures of 5,17-dibromo-26,28-dihydroxy-25,27-dipropynyloxycalix[4]arene, 5,17-dibromo-26,28-dipropoxy-25,27-dipropynyloxycalix[4]arene and 25,27-bis(2-azidoethoxy)-5,17-dibromo-26,28-dihydroxycalix[4]arene ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989024003785 _journal_volume 80 _journal_year 2024 _chemical_formula_iupac 'C40 H38 Br2 O4' _chemical_formula_moiety 'C40 H38 Br2 O4' _chemical_formula_sum 'C40 H38 Br2 O4' _chemical_formula_weight 742.52 _chemical_name_systematic ; 5,17-Dibromo-26,28-dipropoxy-25,27-dipropynyloxycalix[4]arene ; _space_group_crystal_system orthorhombic _space_group_IT_number 60 _space_group_name_Hall '-P 2n 2ab' _space_group_name_H-M_alt 'P b c n' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary dual _audit_creation_method ; Olex2 1.3 (compiled Nov 21 2019 18:26:39 for OlexSys, GUI svn.r6003) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 18.1223(7) _cell_length_b 9.9840(4) _cell_length_c 18.2863(7) _cell_measurement_reflns_used 9929 _cell_measurement_temperature 100.0 _cell_measurement_theta_max 31.46 _cell_measurement_theta_min 2.33 _cell_volume 3308.6(2) _computing_cell_refinement ; APEX3 (Bruker, 2017) ; _computing_data_collection ; APEX3 (Bruker, 2017) ; _computing_data_reduction ; SAINT (Bruker, 2017) ; _computing_molecular_graphics ; Olex2 1.3 (Dolomanov et al., 2009) ; _computing_publication_material ; Olex2 1.3 (Dolomanov et al., 2009) ; _computing_structure_refinement ; SHELXL (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 100.0 _diffrn_detector 'Bruker PHOTON III CMOS' _diffrn_detector_area_resol_mean 10.4 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device '3-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 Venture' _diffrn_measurement_method \w-scan _diffrn_radiation_monochromator 'focusing mirrors' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0595 _diffrn_reflns_av_unetI/netI 0.0326 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_h_min -26 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 55960 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 31.534 _diffrn_reflns_theta_min 2.227 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.492 _exptl_absorpt_correction_T_max 0.7462 _exptl_absorpt_correction_T_min 0.5446 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (SADABS; Krause et al., 2015) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.491 _exptl_crystal_description block _exptl_crystal_F_000 1520 _exptl_crystal_size_max 0.35 _exptl_crystal_size_mid 0.25 _exptl_crystal_size_min 0.22 _refine_diff_density_max 0.418 _refine_diff_density_min -0.509 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.036 _refine_ls_hydrogen_treatment refxyz _refine_ls_matrix_type full _refine_ls_number_parameters 283 _refine_ls_number_reflns 5529 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.036 _refine_ls_R_factor_all 0.0446 _refine_ls_R_factor_gt 0.0298 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0275P)^2^+1.7553P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0642 _refine_ls_wR_factor_ref 0.0690 _reflns_number_gt 4481 _reflns_number_total 5529 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file wm5716.cif _cod_data_source_block 2 _cod_database_code 2023115 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.476 _shelx_estimated_absorpt_t_max 0.610 _shelx_hkl_file ; 0 -1 0 -0.10 0.20 0 1 0 0.40 0.30 0 2 0 1912.81 100.39 0 2 0 1879.51 100.29 0 2 0 1939.61 100.39 0 -2 0 1931.01 100.39 0 -2 0 1922.41 100.39 0 -2 0 1788.12 100.29 0 3 0 -0.60 0.70 0 3 0 -0.10 0.80 0 -3 0 0.10 0.60 0 -3 0 1.30 0.80 0 -3 0 0.90 0.80 0 3 0 1.10 0.90 0 -4 0 3907.01 204.08 0 -4 0 3776.52 203.78 0 4 0 3777.62 203.68 0 4 0 4138.19 203.68 0 4 0 3782.52 203.78 0 -4 0 3698.03 203.58 0 -5 0 0.50 1.40 0 5 0 0.70 1.50 0 5 0 0.50 1.30 0 -5 0 -1.30 1.50 0 5 0 -0.50 1.70 0 -5 0 -0.70 1.20 0 -6 0 477.75 27.50 0 -6 0 483.15 26.90 0 -6 0 456.35 26.60 0 6 0 480.95 27.00 0 6 0 469.95 26.90 0 6 0 509.45 26.70 0 -7 0 1.40 2.20 0 7 0 0.80 2.20 0 7 0 0.80 1.90 0 -7 0 0.40 2.00 0 8 0 578.04 31.90 0 -8 0 556.64 31.70 0 8 0 546.25 31.30 0 9 0 -0.10 2.60 0 9 0 1.90 3.40 0 -9 0 -2.00 2.70 0 10 0 563.64 33.50 0 -10 0 590.24 33.50 0 10 0 585.64 33.00 0 -11 0 5.20 4.10 0 11 0 2.00 4.40 0 -12 0 18.10 5.70 0 -12 0 11.30 4.40 0 12 0 14.10 5.80 0 -13 0 -2.60 4.80 0 13 0 -6.20 5.70 0 -13 0 0.90 5.90 0 14 0 57.09 9.50 0 -14 0 48.60 8.80 1 -1 0 173.48 9.60 -1 -1 0 167.68 9.50 1 1 0 164.18 9.60 -1 1 0 183.08 9.40 -1 1 0 184.78 9.50 -1 -1 0 183.38 9.40 1 1 0 172.18 9.60 -1 -1 0 170.48 9.60 -1 1 0 174.58 9.60 1 -2 0 0.90 0.70 -1 -2 0 0.10 0.60 -1 -2 0 0.40 0.40 -1 -2 0 -0.30 0.60 1 2 0 -0.10 0.60 -1 2 0 0.80 0.50 1 -2 0 0.40 0.50 -1 2 0 -0.50 0.50 -1 2 0 0.00 0.60 1 -2 0 0.40 0.50 1 2 0 1.10 0.50 1 2 0 0.30 0.60 -1 -3 0 456.65 24.80 -1 3 0 472.15 24.70 -1 3 0 477.05 24.80 1 3 0 445.16 24.80 1 3 0 443.76 24.50 1 -3 0 433.86 24.60 -1 3 0 438.46 24.60 -1 -3 0 452.65 24.80 -1 -3 0 479.45 24.50 1 -3 0 457.35 24.70 1 -3 0 442.16 24.70 1 -4 0 2.20 1.10 -1 4 0 3.70 1.40 1 -4 0 0.60 1.20 1 4 0 2.10 1.30 -1 4 0 2.70 1.20 1 4 0 1.40 1.20 1 4 0 -0.60 0.80 -1 -4 0 1.60 0.90 -1 4 0 0.30 1.20 -1 -4 0 0.60 1.20 -1 -4 0 0.40 1.10 1 -4 0 1.70 1.00 -1 5 0 417.76 21.40 -1 5 0 392.06 21.40 1 5 0 386.86 21.30 1 5 0 347.57 21.40 -1 -5 0 371.16 21.40 1 -5 0 366.46 21.40 -1 -5 0 417.96 21.20 1 -5 0 326.57 21.20 -1 -5 0 388.36 21.50 -1 5 0 369.86 21.20 1 5 0 387.96 21.60 1 -5 0 399.46 21.30 1 -6 0 0.60 1.70 1 -6 0 3.10 1.70 1 6 0 -0.30 1.80 1 6 0 0.00 1.30 -1 -6 0 -0.60 1.80 -1 -6 0 0.00 1.50 -1 6 0 2.30 1.90 1 -6 0 1.10 1.80 -1 6 0 -0.30 1.50 1 6 0 3.70 2.30 -1 6 0 0.40 1.80 -1 -7 0 783.32 46.90 1 7 0 879.81 46.60 1 7 0 860.61 47.20 -1 -7 0 833.42 46.50 1 -7 0 886.51 46.90 -1 7 0 930.41 46.90 -1 7 0 816.42 47.00 -1 8 0 0.30 2.10 -1 8 0 -0.90 2.40 1 -8 0 -4.10 2.10 -1 -8 0 -1.20 2.80 1 8 0 -0.10 2.70 1 8 0 0.60 2.20 1 -9 0 980.00 50.59 1 9 0 880.01 49.99 -1 -9 0 924.11 50.79 1 9 0 882.41 50.79 -1 9 0 904.31 50.29 -1 9 0 908.81 50.69 -1 10 0 -0.30 3.10 1 10 0 1.80 3.70 1 -10 0 4.00 3.70 -1 -10 0 -4.30 3.60 1 10 0 0.20 2.80 -1 10 0 -2.00 3.50 -1 -11 0 473.75 29.90 1 -11 0 518.95 29.80 1 11 0 517.05 30.40 -1 11 0 516.45 30.20 -1 -12 0 -1.90 4.00 1 -12 0 -4.20 4.40 1 12 0 -1.80 4.90 1 -12 0 0.20 4.30 -1 -12 0 1.40 4.70 -1 12 0 2.80 5.20 1 -13 0 501.15 30.30 1 -13 0 490.15 30.50 -1 13 0 484.15 30.80 1 13 0 505.85 31.40 -1 -13 0 531.75 30.00 -1 -13 0 523.95 31.20 -1 14 0 7.40 7.50 1 -14 0 4.80 6.40 1 14 0 3.80 7.00 -1 -14 0 -10.70 6.00 1 -14 0 4.80 6.70 2 0 0 1114.29 56.29 2 0 0 1029.80 56.19 -2 0 0 1020.20 56.29 -2 0 0 1005.50 56.19 -2 0 0 1136.09 56.19 -2 1 0 -0.10 0.30 2 1 0 0.10 0.40 -2 -1 0 2.40 0.60 -2 -1 0 0.00 0.30 2 1 0 0.50 0.20 2 -1 0 0.00 0.40 2 -1 0 0.40 0.20 -2 1 0 0.30 0.40 -2 1 0 0.50 0.20 2 1 0 1.40 0.60 2 -1 0 -0.30 0.40 2 2 0 944.51 50.49 2 -2 0 976.50 50.19 -2 -2 0 979.60 50.09 -2 2 0 996.50 50.39 2 2 0 900.51 50.09 2 -2 0 947.81 50.39 -2 -2 0 921.11 50.49 -2 2 0 948.91 50.09 2 2 0 931.41 50.49 2 -2 0 875.61 50.49 -2 -2 0 977.00 50.49 -2 2 0 944.41 50.49 2 3 0 0.30 1.00 2 -3 0 -0.20 0.80 2 -3 0 -0.60 0.60 -2 -3 0 -0.40 0.50 2 3 0 1.60 1.00 -2 3 0 0.70 0.90 -2 -3 0 -0.30 0.80 -2 3 0 0.50 0.80 2 -3 0 1.00 0.70 2 3 0 0.70 0.70 -2 -3 0 2.30 1.00 -2 3 0 -0.90 0.60 -2 4 0 1333.77 69.79 -2 4 0 1293.47 69.69 2 -4 0 1282.07 69.69 2 -4 0 1338.97 69.79 2 4 0 1306.57 69.29 -2 4 0 1225.38 69.39 2 -4 0 1338.07 69.49 -2 -4 0 1376.16 69.39 2 4 0 1268.37 69.89 2 4 0 1363.26 69.89 -2 -4 0 1303.77 69.79 -2 -4 0 1201.18 69.79 -2 5 0 -0.20 1.40 -2 -5 0 1.40 1.60 -2 5 0 -1.30 1.40 2 -5 0 1.40 1.60 2 -5 0 1.30 1.50 -2 -5 0 1.70 1.20 -2 -5 0 1.00 1.70 2 5 0 3.10 1.70 -2 5 0 -0.10 1.30 2 5 0 1.80 1.10 2 5 0 -1.40 1.70 2 -5 0 -0.40 1.30 -2 6 0 204.98 11.90 -2 -6 0 188.68 12.00 -2 6 0 189.78 12.00 2 6 0 209.58 11.50 2 -6 0 191.08 11.90 2 6 0 198.18 12.30 -2 6 0 182.08 11.80 2 -6 0 203.38 11.70 -2 -6 0 183.28 11.40 2 -6 0 181.98 11.90 2 7 0 -0.20 1.70 -2 7 0 -0.20 2.10 2 7 0 2.70 2.50 -2 7 0 0.90 2.00 -2 -7 0 -2.20 2.10 -2 7 0 -0.70 2.00 -2 -7 0 2.50 1.80 2 -7 0 -1.60 1.90 -2 8 0 103.89 8.20 -2 -8 0 106.49 8.50 2 8 0 98.79 7.50 2 -8 0 121.49 8.20 -2 -8 0 114.49 7.80 -2 8 0 117.09 8.20 2 8 0 96.29 8.50 2 9 0 -0.30 2.40 2 9 0 -5.60 3.20 -2 9 0 1.30 2.80 -2 -9 0 4.90 3.60 -2 9 0 -4.90 2.80 2 -9 0 -4.70 2.60 -2 10 0 75.99 7.70 2 10 0 71.39 6.90 -2 -10 0 79.19 8.20 2 10 0 81.19 8.60 -2 10 0 78.79 7.80 -2 11 0 3.80 4.20 2 11 0 -0.40 4.70 -2 -11 0 -2.80 4.10 2 -11 0 2.90 4.20 2 11 0 2.30 3.50 -2 -12 0 7.70 7.00 -2 -12 0 2.50 5.10 2 -12 0 2.10 4.40 -2 12 0 4.00 4.50 2 -12 0 7.40 4.80 2 12 0 5.40 5.70 2 -13 0 -2.60 4.90 2 13 0 -3.10 6.00 -2 -13 0 2.60 6.10 2 -13 0 -2.90 5.40 -2 13 0 -2.50 5.70 -2 -13 0 -0.50 4.90 -2 14 0 51.79 9.00 2 -14 0 36.90 9.60 2 14 0 67.49 9.80 -2 -14 0 45.40 8.70 3 0 0 2.20 0.60 3 0 0 0.70 0.50 -3 0 0 0.70 0.50 3 0 0 0.50 0.50 -3 0 0 1.20 0.50 -3 1 0 77.29 4.80 3 1 0 79.19 4.80 -3 1 0 84.99 4.80 3 -1 0 75.19 4.80 3 1 0 79.69 4.90 -3 -1 0 79.69 4.50 -3 -1 0 87.19 5.00 3 -1 0 77.39 4.70 3 1 0 81.09 4.60 3 2 0 2.40 0.90 3 2 0 0.40 0.80 -3 2 0 0.60 0.70 3 -2 0 0.80 0.90 -3 -2 0 1.70 0.80 3 -2 0 -0.10 0.40 -3 -2 0 1.00 0.70 3 2 0 0.10 0.40 3 -2 0 0.80 0.70 -3 2 0 0.10 0.70 -3 -2 0 -0.30 0.40 -3 -3 0 -0.40 1.10 -3 3 0 0.60 1.20 3 -3 0 1.10 1.00 3 -3 0 1.90 1.00 -3 -3 0 1.80 0.60 3 3 0 1.60 1.20 -3 3 0 0.30 0.90 -3 3 0 -0.30 0.60 -3 -3 0 2.40 1.10 3 3 0 1.70 1.20 3 -3 0 0.70 0.80 3 3 0 0.40 0.60 -3 4 0 1.00 0.90 -3 -4 0 0.60 1.40 3 4 0 1.50 0.90 -3 4 0 1.40 1.20 3 -4 0 1.70 1.30 3 4 0 2.90 1.40 -3 -4 0 0.70 1.40 3 -4 0 1.40 0.90 -3 -4 0 -0.10 0.80 3 4 0 4.30 1.80 -3 -5 0 46.40 3.30 3 5 0 43.80 3.30 3 5 0 45.50 4.10 -3 -5 0 42.60 4.00 -3 5 0 40.90 3.40 -3 -5 0 36.10 3.80 3 5 0 41.20 4.40 3 -5 0 44.60 3.50 3 -5 0 41.10 4.00 -3 5 0 46.00 4.00 3 -5 0 40.80 4.00 -3 5 0 41.50 3.80 -3 -6 0 -0.60 2.10 -3 6 0 -1.20 1.50 3 -6 0 1.70 2.00 -3 6 0 4.30 2.00 -3 6 0 1.30 1.70 3 6 0 3.20 2.40 -3 -6 0 0.10 1.40 3 -6 0 1.10 1.50 -3 7 0 108.89 7.80 -3 7 0 102.59 7.30 -3 7 0 102.99 7.40 -3 -7 0 105.99 7.00 -3 -7 0 93.99 7.70 3 7 0 108.79 7.00 3 7 0 115.79 8.40 3 -7 0 101.59 7.30 -3 -8 0 -1.30 2.20 -3 8 0 1.50 2.70 3 8 0 1.90 2.00 3 -8 0 -1.80 2.20 -3 -8 0 0.10 3.00 -3 8 0 -1.40 2.30 3 -9 0 -1.20 2.80 -3 -9 0 4.60 3.70 3 9 0 3.40 3.10 3 9 0 1.70 2.40 -3 9 0 7.00 3.30 -3 9 0 3.10 3.20 -3 -9 0 2.60 4.70 3 -10 0 -1.30 3.10 -3 -10 0 2.00 4.00 -3 10 0 -3.40 3.30 -3 10 0 -1.60 3.50 3 10 0 -3.70 3.80 3 10 0 -1.40 2.60 3 -11 0 3.70 4.30 3 -11 0 11.30 4.50 -3 11 0 6.50 4.20 3 11 0 10.80 4.70 3 11 0 10.00 3.70 -3 -11 0 12.10 5.30 -3 -12 0 12.20 6.30 -3 -12 0 6.10 4.00 3 -12 0 -0.50 4.20 3 -12 0 2.90 4.80 -3 12 0 -2.60 4.60 -3 13 0 -0.70 5.70 -3 -13 0 10.50 6.40 3 13 0 18.30 7.00 3 -13 0 4.40 5.50 3 -13 0 18.50 6.40 3 -14 0 4.00 7.10 -3 14 0 -4.50 6.90 -3 -14 0 5.80 6.90 3 14 0 5.10 7.60 4 0 0 9047.19 506.45 -4 0 0 9999.00 507.05 4 1 0 1.90 0.90 4 1 0 0.00 0.80 -4 -1 0 0.00 0.80 -4 -1 0 0.90 0.80 -4 1 0 0.50 0.70 -4 1 0 -0.30 0.40 4 -1 0 0.90 0.50 4 -1 0 0.10 0.70 4 -1 0 -0.60 0.60 -4 1 0 0.70 0.70 4 1 0 -0.30 0.50 -4 -1 0 0.60 0.50 -4 2 0 462.35 24.90 4 -2 0 465.65 24.90 4 -2 0 441.36 24.70 4 2 0 445.36 24.90 -4 -2 0 445.96 24.30 4 2 0 440.26 24.90 4 2 0 456.05 24.40 -4 -2 0 470.25 24.90 4 -2 0 479.35 24.30 4 2 0 430.86 24.90 -4 2 0 455.65 24.70 -4 -3 0 1.30 0.60 -4 3 0 -0.10 0.90 4 -3 0 0.00 0.70 4 3 0 1.00 1.20 4 -3 0 2.10 1.20 4 -3 0 -0.20 1.10 -4 -3 0 -2.00 1.00 4 3 0 0.00 0.70 -4 3 0 1.30 0.60 -4 3 0 3.10 1.30 4 3 0 -1.00 1.10 -4 -3 0 1.10 1.30 4 -4 0 81.09 4.80 -4 4 0 71.39 4.60 -4 -4 0 81.19 5.60 4 4 0 64.39 5.60 -4 4 0 73.19 5.10 4 -4 0 68.69 5.30 4 4 0 74.39 5.50 -4 4 0 79.99 5.40 -4 -4 0 76.99 5.40 -4 -4 0 75.49 4.50 4 4 0 71.39 4.60 4 -4 0 80.89 5.40 -4 5 0 1.70 1.70 -4 -5 0 -0.30 1.00 -4 5 0 0.40 1.50 4 -5 0 -1.50 1.10 4 5 0 -0.30 1.70 -4 5 0 1.30 1.20 4 5 0 0.50 1.10 4 -5 0 0.50 1.70 -4 -5 0 -0.40 1.70 4 -5 0 1.10 1.90 -4 -6 0 341.17 19.20 -4 6 0 341.77 19.40 4 6 0 349.57 19.20 -4 -6 0 351.76 20.40 -4 6 0 357.36 19.90 4 -6 0 339.07 19.40 4 -6 0 333.77 20.60 4 6 0 345.77 20.40 -4 6 0 361.56 20.20 -4 7 0 0.90 1.90 4 7 0 -0.50 1.50 -4 -7 0 -1.00 2.20 -4 -7 0 -1.10 1.60 4 7 0 -0.60 2.70 -4 7 0 1.10 2.10 4 -7 0 1.40 1.90 -4 7 0 2.90 1.90 -4 8 0 48.30 5.00 4 8 0 45.20 4.30 -4 8 0 44.70 5.40 -4 8 0 43.10 5.10 4 8 0 59.59 6.80 -4 -8 0 45.90 4.70 -4 -8 0 61.79 6.60 4 -8 0 45.20 4.70 -4 9 0 3.00 3.30 4 -9 0 -0.50 2.60 -4 -9 0 0.50 2.60 4 9 0 3.70 3.40 -4 -9 0 3.80 3.80 4 9 0 1.30 2.20 -4 9 0 -1.70 2.80 4 -10 0 72.59 7.30 4 10 0 87.59 8.50 -4 10 0 79.79 7.80 -4 10 0 76.69 8.20 -4 -10 0 99.79 8.50 4 10 0 81.99 6.70 4 -11 0 0.50 4.20 4 -11 0 -2.60 4.20 -4 11 0 5.90 4.30 -4 -11 0 3.90 4.40 4 11 0 -8.70 4.60 4 -12 0 -4.20 4.20 4 12 0 0.90 6.00 4 -12 0 5.20 4.90 -4 -12 0 -5.20 4.70 -4 -12 0 8.00 3.60 -4 12 0 -6.70 4.40 4 -13 0 0.90 5.00 -4 13 0 -0.80 6.00 -4 -13 0 -3.50 6.00 4 13 0 5.00 6.40 -4 -14 0 12.90 7.70 4 -14 0 4.40 7.20 4 14 0 5.70 8.00 -4 14 0 -0.80 6.90 5 0 0 0.90 0.70 5 0 0 -1.20 0.60 -5 0 0 0.50 0.70 5 0 0 1.10 1.00 5 0 0 0.00 0.80 -5 0 0 0.90 1.00 5 1 0 1680.23 82.39 -5 -1 0 1693.93 82.49 5 -1 0 1542.15 82.29 5 1 0 1572.14 82.19 -5 -1 0 1435.56 81.89 5 1 0 1491.55 81.89 -5 1 0 1562.04 82.19 5 -1 0 1397.76 81.79 5 -1 0 1476.55 82.19 -5 1 0 1540.05 81.79 5 -1 0 1600.94 82.29 5 2 0 1.20 1.30 -5 2 0 1.60 1.10 5 -2 0 -0.60 1.10 -5 -2 0 1.50 0.70 -5 2 0 0.10 0.90 5 2 0 1.30 1.20 5 -2 0 0.30 0.60 5 2 0 0.40 1.10 -5 -2 0 -0.40 1.00 5 2 0 0.40 0.60 5 -2 0 0.60 0.50 5 -3 0 248.68 14.40 5 -3 0 262.67 14.20 5 3 0 253.87 14.50 5 3 0 241.58 13.60 5 -3 0 240.28 13.50 -5 3 0 241.88 13.40 5 3 0 257.17 14.50 -5 3 0 253.67 14.40 -5 -3 0 250.07 13.50 -5 3 0 237.78 14.30 5 3 0 244.68 14.30 -5 -3 0 245.38 14.40 5 4 0 -0.30 1.50 5 4 0 1.30 1.00 -5 -4 0 1.20 0.80 -5 -4 0 1.50 1.60 -5 4 0 1.30 1.20 5 -4 0 1.70 1.60 5 4 0 0.30 1.60 5 -4 0 0.20 1.60 -5 4 0 -2.40 1.30 -5 -4 0 -1.20 1.40 -5 4 0 0.50 0.80 5 -4 0 1.60 1.00 5 -5 0 267.77 16.00 -5 5 0 279.07 16.30 5 5 0 282.37 16.40 -5 -5 0 271.67 15.10 5 -5 0 280.77 15.30 -5 5 0 278.37 15.20 5 5 0 271.67 15.20 -5 -5 0 279.87 16.40 -5 5 0 258.67 15.70 5 6 0 1.30 2.20 5 -6 0 -0.90 1.40 -5 -6 0 2.00 1.20 -5 6 0 0.10 1.40 -5 6 0 2.90 2.20 -5 6 0 -2.20 1.50 5 6 0 0.50 1.30 -5 -6 0 2.10 2.20 5 -7 0 388.96 23.00 5 7 0 429.16 24.50 -5 -7 0 410.96 25.10 -5 -7 0 422.56 22.70 -5 7 0 398.16 22.90 -5 7 0 422.86 24.10 -5 7 0 419.96 23.60 5 -8 0 -0.10 2.20 -5 8 0 -0.40 2.50 5 8 0 2.70 3.70 -5 8 0 1.30 2.90 -5 -8 0 -0.90 1.90 -5 8 0 -0.30 2.30 5 8 0 0.60 1.80 -5 -8 0 0.30 2.90 5 -9 0 655.03 36.80 -5 9 0 668.83 37.40 -5 9 0 686.53 38.00 -5 -9 0 611.34 38.00 -5 -9 0 662.23 36.30 5 9 0 702.73 36.40 5 9 0 650.83 38.40 5 10 0 0.60 3.90 -5 10 0 -1.80 3.40 5 -10 0 3.30 3.20 5 10 0 -1.10 2.40 -5 -10 0 0.40 3.00 -5 -10 0 -0.10 4.20 -5 -11 0 514.65 31.40 5 -11 0 513.15 30.80 -5 11 0 557.44 30.60 5 -11 0 488.55 29.50 5 11 0 511.05 31.50 5 -12 0 -4.10 4.60 5 -12 0 -12.90 4.00 -5 -12 0 0.10 5.20 -5 -12 0 -1.90 3.30 5 12 0 -1.30 5.10 -5 12 0 -2.60 4.80 -5 13 0 191.78 14.90 5 -13 0 195.38 15.90 -5 -13 0 182.98 16.00 5 13 0 193.68 16.60 -5 -14 0 -8.10 7.30 -5 14 0 -5.30 6.60 5 -14 0 3.20 7.30 5 14 0 -1.80 8.30 6 0 0 1032.10 55.69 -6 0 0 1061.29 55.69 6 0 0 1085.89 55.99 6 0 0 1006.40 55.79 6 0 0 912.11 55.69 -6 0 0 1168.18 56.59 -6 -1 0 0.30 0.80 6 -1 0 -0.30 0.90 -6 1 0 -0.60 0.70 6 1 0 -0.40 0.80 6 -1 0 1.50 1.20 6 -1 0 -0.20 0.80 6 -1 0 -1.00 0.90 6 1 0 -0.40 1.10 6 1 0 0.70 1.00 -6 -1 0 0.90 1.20 -6 -2 0 1736.83 101.89 -6 -2 0 1865.11 101.39 6 2 0 1873.01 101.49 6 2 0 1953.80 102.09 6 -2 0 1882.41 101.29 -6 2 0 2037.30 101.89 6 -2 0 1962.10 101.89 6 2 0 2006.70 102.19 6 -2 0 1904.31 101.29 6 3 0 0.50 1.50 -6 3 0 1.10 1.30 6 3 0 1.00 1.50 6 -3 0 1.10 0.80 -6 3 0 1.00 1.20 6 3 0 -0.60 0.80 6 -3 0 -0.20 1.40 6 -3 0 1.50 1.30 -6 -3 0 0.20 0.70 6 -3 0 -1.10 0.60 6 3 0 -0.30 1.30 -6 -3 0 1.90 1.50 -6 4 0 2096.19 111.89 -6 -4 0 2296.07 113.29 -6 4 0 2077.19 113.09 -6 4 0 2073.99 112.59 -6 -4 0 2119.19 111.99 6 4 0 2052.39 113.19 6 -4 0 2115.29 111.99 6 4 0 2175.28 112.09 6 -4 0 2029.30 112.79 -6 5 0 0.20 1.70 6 5 0 -0.50 1.00 6 5 0 4.60 2.30 -6 -5 0 -0.90 1.80 -6 5 0 -1.70 1.90 6 -5 0 1.40 1.20 6 -5 0 1.80 2.00 -6 -5 0 1.50 0.90 -6 5 0 -1.70 0.90 -6 -6 0 683.83 37.00 6 -6 0 650.33 37.20 -6 6 0 710.03 38.00 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1.10 7 0 0 -1.20 1.00 -7 1 0 2.60 1.30 7 -1 0 -1.50 1.30 -7 1 0 2.00 1.10 -7 -1 0 1.10 1.30 -7 -1 0 4.10 1.10 7 1 0 -0.10 1.10 7 1 0 3.20 1.50 7 1 0 3.10 1.20 -7 -1 0 -0.70 1.20 7 -1 0 5.60 1.60 7 -1 0 -0.10 1.10 -7 -2 0 -2.00 0.80 -7 -2 0 0.20 1.30 7 -2 0 -0.70 1.20 7 -2 0 2.10 1.30 7 -2 0 0.40 0.80 7 2 0 0.40 1.50 7 2 0 0.10 1.40 -7 2 0 1.30 1.40 7 -2 0 3.60 1.60 7 2 0 -0.40 0.90 7 -2 0 2.40 0.90 7 3 0 696.03 37.50 7 3 0 665.33 36.50 -7 3 0 689.43 37.00 7 -3 0 679.23 36.20 -7 -3 0 657.13 36.30 7 -3 0 718.83 36.30 7 3 0 675.23 37.30 7 3 0 636.74 37.30 7 -3 0 661.53 37.30 -7 -3 0 696.03 37.30 7 -3 0 677.23 37.10 7 -4 0 -0.40 1.70 7 -4 0 0.50 0.90 7 4 0 1.70 2.00 -7 4 0 -0.60 1.40 7 -4 0 1.10 1.00 -7 4 0 1.10 1.70 7 4 0 1.10 1.10 -7 -4 0 -0.70 1.50 -7 -4 0 -1.50 0.90 7 -5 0 312.97 17.10 -7 5 0 318.37 18.50 7 5 0 310.47 17.10 -7 5 0 320.57 17.90 -7 5 0 309.27 16.90 7 5 0 289.07 18.50 -7 -5 0 299.07 18.50 -7 -5 0 321.67 17.00 7 -5 0 305.67 18.70 -7 -6 0 1.60 2.70 -7 6 0 -1.50 1.20 -7 6 0 0.50 2.00 7 6 0 0.80 1.30 -7 6 0 3.00 2.20 7 6 0 -1.00 2.60 7 -6 0 -0.10 1.30 -7 -6 0 0.70 1.10 7 7 0 352.96 21.30 -7 -7 0 336.27 20.80 -7 7 0 322.57 19.00 7 7 0 350.96 19.00 -7 7 0 317.17 19.90 7 -7 0 369.76 20.70 -7 -7 0 347.47 18.90 -7 7 0 365.46 21.00 -7 8 0 1.10 2.10 7 8 0 -0.90 1.60 -7 -8 0 -2.20 3.50 -7 8 0 1.10 2.60 7 -8 0 1.00 1.90 7 8 0 5.20 3.60 -7 -8 0 0.90 1.60 -7 8 0 1.50 3.30 -7 9 0 287.97 16.60 -7 9 0 320.27 18.10 7 9 0 295.17 19.30 -7 -9 0 282.07 18.90 -7 -9 0 288.37 16.10 7 -9 0 260.67 16.60 7 10 0 -0.70 2.10 -7 -10 0 0.40 2.20 -7 10 0 0.30 3.80 7 -10 0 -0.30 2.70 -7 -10 0 -4.10 4.20 7 10 0 -0.80 4.70 7 -10 0 2.50 4.20 -7 11 0 604.94 34.00 -7 -11 0 544.95 34.90 7 -11 0 602.74 34.70 7 -11 0 571.84 32.50 7 -12 0 0.10 5.60 7 12 0 -1.30 6.50 -7 -12 0 12.60 5.50 -7 12 0 0.00 5.30 7 13 0 119.49 14.20 -7 13 0 144.69 13.00 -7 -13 0 142.09 14.30 7 -13 0 134.79 13.30 -7 14 0 -6.10 6.70 7 -14 0 14.80 7.70 -7 -14 0 2.80 7.90 8 0 0 305.57 17.30 8 0 0 307.97 17.20 8 0 0 301.27 17.60 -8 0 0 296.57 17.60 8 0 0 311.67 17.40 -8 0 0 308.27 17.20 8 -1 0 -0.70 1.40 8 1 0 1.80 1.30 8 1 0 0.60 1.70 -8 -1 0 2.30 1.70 -8 1 0 -0.90 1.40 8 -1 0 0.10 1.10 -8 1 0 0.70 1.10 8 -1 0 1.80 1.50 -8 -1 0 -0.30 1.20 8 -1 0 0.20 1.40 8 1 0 1.20 1.50 8 2 0 421.36 23.20 8 2 0 414.76 23.80 8 2 0 441.86 23.90 -8 -2 0 409.46 23.10 -8 -2 0 397.66 23.60 8 -2 0 421.26 23.80 8 -2 0 420.76 23.80 8 -2 0 407.96 22.90 8 -2 0 435.26 23.80 -8 2 0 442.56 23.70 -8 -2 0 434.46 24.00 -8 -3 0 1.70 1.80 8 -3 0 0.10 1.60 8 3 0 0.30 1.20 -8 -3 0 -0.70 1.00 -8 3 0 1.10 1.60 8 -3 0 0.30 1.00 8 -3 0 1.40 1.70 8 -3 0 0.40 0.90 8 3 0 1.20 1.80 8 -4 0 363.76 19.20 8 4 0 335.47 20.70 -8 -4 0 381.56 20.70 -8 -4 0 339.57 19.20 8 4 0 349.47 19.40 8 -4 0 346.67 19.00 8 -4 0 352.16 20.30 -8 4 0 351.26 20.00 -8 5 0 0.60 2.10 8 -5 0 0.80 1.20 8 -5 0 0.00 1.00 8 5 0 -3.20 2.20 -8 -5 0 -2.40 2.10 -8 -5 0 0.90 1.00 8 5 0 1.30 1.30 -8 5 0 -1.80 1.50 -8 6 0 111.29 8.10 -8 6 0 106.49 9.50 8 -6 0 118.79 7.10 -8 6 0 110.69 6.80 -8 -6 0 119.19 6.90 8 6 0 123.49 7.10 -8 -6 0 117.19 8.90 8 7 0 3.00 3.60 8 7 0 -1.00 1.40 -8 7 0 -2.10 2.40 -8 -7 0 4.70 3.10 -8 7 0 1.70 1.40 8 -7 0 -1.20 1.50 -8 -7 0 2.60 1.30 8 8 0 54.69 7.10 -8 8 0 48.60 4.20 -8 -8 0 53.09 6.50 8 8 0 54.49 4.20 8 -8 0 58.69 5.30 -8 -8 0 58.49 4.00 -8 -9 0 1.00 3.50 8 9 0 1.60 5.00 8 -9 0 0.80 3.90 8 -9 0 3.40 2.30 8 9 0 1.40 1.70 -8 9 0 2.90 3.40 -8 -9 0 2.10 1.60 -8 9 0 4.40 3.80 8 -10 0 -0.50 4.40 -8 -10 0 7.40 1.90 -8 10 0 5.30 4.10 8 10 0 0.50 5.60 -8 10 0 5.90 4.00 8 -10 0 10.50 2.80 -8 -10 0 1.30 4.60 -8 -11 0 1.10 5.00 8 -11 0 0.40 2.90 -8 11 0 -1.20 4.60 8 11 0 -1.50 6.00 8 12 0 0.30 6.40 8 -12 0 14.10 6.30 -8 -12 0 11.20 6.80 -8 12 0 6.40 5.40 -8 -13 0 1.30 7.00 8 -13 0 -5.20 6.00 8 13 0 -7.00 8.20 -8 13 0 -5.30 6.10 -8 14 0 2.60 6.90 8 -14 0 16.70 8.40 -8 -14 0 9.80 8.80 8 14 0 2.50 9.50 9 0 0 1.50 1.50 -9 0 0 -0.10 1.80 9 0 0 1.20 1.80 -9 0 0 2.00 1.40 9 0 0 3.70 1.80 9 0 0 5.70 1.90 9 -1 0 114.59 7.70 9 1 0 106.89 7.20 -9 1 0 114.49 7.40 -9 1 0 108.49 7.60 -9 -1 0 135.59 8.20 9 -1 0 101.09 7.00 9 1 0 111.69 7.40 -9 -1 0 105.09 7.30 9 1 0 110.89 7.20 9 -1 0 124.29 7.80 9 -1 0 111.39 7.50 9 -2 0 1.90 1.20 9 -2 0 5.90 2.30 -9 -2 0 1.00 1.90 -9 -2 0 -0.50 1.20 -9 2 0 0.20 1.50 9 -2 0 1.90 1.70 -9 -2 0 0.10 1.80 9 2 0 -0.50 1.30 9 3 0 13.70 2.10 -9 -3 0 13.10 2.90 -9 -3 0 11.30 1.70 9 3 0 9.30 2.70 9 -3 0 7.40 2.50 9 -3 0 9.20 1.60 9 -3 0 7.90 2.50 -9 3 0 9.80 2.20 9 -3 0 10.60 1.60 9 -4 0 0.50 1.00 -9 -4 0 2.90 1.20 9 4 0 -0.90 2.20 -9 -4 0 3.80 2.20 9 -4 0 -0.20 2.00 9 -4 0 0.70 1.30 -9 4 0 -1.70 1.90 9 4 0 4.60 1.50 -9 5 0 49.40 4.60 -9 -5 0 46.20 3.50 -9 -5 0 49.10 5.80 9 -5 0 51.09 3.40 9 5 0 52.29 5.90 9 5 0 44.90 3.80 9 -5 0 49.40 5.20 9 -5 0 54.59 3.60 -9 6 0 5.00 2.50 9 -6 0 2.40 1.20 9 -6 0 0.10 1.30 9 -6 0 1.10 2.80 9 6 0 1.20 3.00 9 6 0 1.80 1.50 -9 -6 0 1.30 3.20 -9 -6 0 -0.60 1.20 -9 -7 0 35.80 3.00 9 7 0 47.30 6.20 -9 7 0 36.90 4.50 9 7 0 36.70 3.20 9 -7 0 31.50 3.20 -9 -7 0 32.30 5.40 9 -7 0 42.30 5.60 -9 8 0 -0.20 1.50 9 -8 0 -0.20 3.90 9 8 0 -1.20 4.20 -9 8 0 -0.20 3.10 -9 -8 0 0.70 1.40 9 -8 0 1.10 1.60 9 8 0 2.10 1.60 -9 -8 0 0.10 3.40 9 -9 0 21.90 5.30 -9 9 0 38.40 3.70 -9 9 0 39.70 5.30 -9 -9 0 38.50 3.00 9 9 0 38.50 3.20 9 9 0 46.20 7.10 -9 -9 0 34.00 6.60 9 -10 0 1.10 4.40 9 10 0 2.30 5.40 9 -10 0 0.80 2.30 -9 10 0 0.00 3.90 -9 -10 0 -1.40 5.10 9 11 0 18.90 7.60 9 -11 0 11.00 5.90 -9 11 0 15.00 5.20 -9 -11 0 18.50 6.80 9 12 0 2.80 6.60 -9 12 0 6.20 5.50 -9 -12 0 -3.70 6.30 9 -12 0 -7.80 5.40 9 13 0 1.70 8.60 -9 -13 0 -2.40 11.30 9 -13 0 -0.40 7.00 -9 13 0 -6.10 5.80 -10 0 0 56.49 4.90 10 0 0 52.09 4.60 10 0 0 57.59 4.50 10 0 0 45.90 4.30 -10 0 0 50.99 4.30 -10 -1 0 0.80 1.60 10 -1 0 -1.10 1.60 -10 1 0 -1.20 1.40 10 1 0 1.80 1.60 -10 -1 0 1.50 2.00 10 1 0 1.50 1.70 10 -1 0 -0.60 1.50 10 1 0 2.20 1.80 -10 1 0 -1.70 2.00 10 -2 0 889.51 50.99 10 2 0 906.01 50.39 10 -2 0 971.50 50.09 -10 -2 0 937.01 51.29 -10 -2 0 970.60 50.89 -10 2 0 949.40 49.99 -10 2 0 890.61 50.69 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-10 -9 0 0.70 3.90 10 -9 0 0.90 1.70 -10 10 0 38.90 5.90 -10 -10 0 39.40 7.80 10 10 0 41.10 7.80 10 -10 0 33.30 3.20 10 11 0 7.90 6.50 -10 11 0 -3.70 4.30 10 -11 0 2.90 5.00 -10 -11 0 -6.00 5.50 10 -12 0 22.40 6.70 -10 -12 0 22.00 7.80 10 12 0 20.70 8.90 10 -13 0 -3.50 7.40 10 13 0 -1.30 8.60 -10 -13 0 -10.40 7.60 -10 13 0 4.60 6.30 11 0 0 2.40 2.00 -11 0 0 3.90 2.50 11 0 0 4.10 2.20 -11 0 0 3.40 1.80 -11 -1 0 187.18 11.70 -11 1 0 187.68 12.20 -11 1 0 192.58 11.40 11 -1 0 181.78 12.10 11 1 0 197.98 11.70 -11 -1 0 191.48 12.30 11 1 0 191.48 11.80 11 -2 0 -0.10 1.60 -11 2 0 -0.20 1.40 -11 2 0 1.70 2.30 11 2 0 -0.50 1.60 11 -2 0 -3.90 1.90 -11 -2 0 0.40 1.90 11 2 0 0.30 1.70 -11 -2 0 -1.00 2.20 11 -3 0 725.53 40.50 11 3 0 720.93 40.50 -11 3 0 734.53 40.00 -11 -3 0 744.03 40.20 11 -3 0 728.83 39.00 11 -3 0 699.03 39.00 11 3 0 709.73 39.50 11 -4 0 -2.70 2.20 11 -4 0 -0.30 1.30 -11 -4 0 0.70 1.60 11 4 0 0.70 2.70 11 4 0 2.30 1.80 -11 4 0 1.90 2.20 11 -4 0 0.50 1.50 11 -5 0 326.67 19.00 -11 5 0 307.17 18.10 11 -5 0 297.87 16.70 -11 -5 0 334.57 18.90 -11 -5 0 306.47 16.90 11 5 0 305.67 19.10 11 -5 0 269.37 16.50 -11 6 0 -3.90 2.60 11 -6 0 -1.40 1.10 -11 -6 0 0.50 1.50 11 -6 0 2.00 1.10 11 -6 0 1.10 3.00 11 6 0 0.10 1.70 -11 -6 0 -1.80 2.70 11 6 0 1.30 3.50 -11 -7 0 147.99 11.50 -11 7 0 132.99 10.30 11 7 0 144.19 12.10 11 7 0 147.69 8.60 -11 -7 0 141.49 8.40 11 -7 0 149.49 11.50 -11 8 0 2.10 3.40 -11 -8 0 0.70 4.20 11 -8 0 1.60 4.30 11 8 0 1.10 4.90 11 -9 0 298.67 19.20 11 9 0 296.57 19.70 -11 9 0 237.38 17.30 -11 -9 0 294.37 24.30 -11 -10 0 3.10 4.90 11 10 0 -3.80 6.20 11 -10 0 6.70 5.10 -11 10 0 -6.40 3.80 -11 11 0 434.36 26.20 -11 -11 0 426.46 27.50 11 11 0 403.06 28.70 11 -11 0 447.16 27.80 11 12 0 -4.30 7.10 -11 12 0 -3.80 5.60 -11 -12 0 -6.10 6.90 11 -12 0 0.40 6.20 11 13 0 68.59 12.40 -11 -13 0 44.90 9.80 -11 13 0 31.80 8.00 11 -13 0 42.20 15.30 12 0 0 1186.68 64.69 -12 0 0 1232.98 65.09 -12 0 0 1155.18 64.19 12 0 0 1189.58 64.99 -12 1 0 -1.70 1.80 12 1 0 1.20 2.00 -12 -1 0 1.70 2.00 12 -1 0 1.40 2.10 12 -1 0 -0.80 1.90 -12 1 0 -0.80 2.30 -12 -1 0 2.00 2.60 -12 -2 0 1073.49 57.29 -12 2 0 1080.79 55.79 -12 2 0 1090.99 56.79 -12 -2 0 952.60 56.39 12 2 0 1015.00 56.19 12 -2 0 1065.59 56.99 12 -2 0 966.20 55.69 12 2 0 1045.40 56.09 -12 3 0 -4.40 2.30 12 3 0 -0.50 1.80 12 -3 0 -0.90 1.60 12 3 0 0.30 2.00 12 3 0 0.90 2.60 -12 -3 0 0.60 2.20 12 -4 0 640.14 37.80 12 -4 0 738.23 40.10 12 -4 0 722.83 38.10 12 4 0 710.73 38.60 -12 -4 0 720.03 39.60 -12 4 0 703.93 39.20 12 4 0 700.63 40.10 12 -5 0 0.30 1.30 12 -5 0 -0.90 3.30 12 5 0 0.30 1.90 -12 -5 0 4.30 3.20 12 5 0 0.20 3.30 -12 5 0 3.40 2.60 12 -5 0 -0.90 1.40 12 6 0 642.04 36.90 12 -6 0 684.93 36.80 12 6 0 616.14 35.60 -12 -6 0 681.03 36.70 -12 6 0 550.14 35.40 -12 7 0 2.40 3.30 12 7 0 -0.30 1.70 12 -7 0 -4.10 3.90 -12 -7 0 -3.50 3.40 12 7 0 0.80 3.90 -12 8 0 48.80 6.40 12 -8 0 72.39 8.60 12 8 0 65.69 8.50 -12 -8 0 76.59 8.70 12 -9 0 -3.40 5.00 12 9 0 2.20 6.80 -12 9 0 0.10 4.20 -12 -9 0 1.30 4.80 12 -10 0 32.80 7.60 12 10 0 41.00 8.90 -12 -10 0 47.70 8.30 -12 10 0 46.00 6.50 -12 -11 0 0.30 5.90 12 -11 0 -8.10 5.90 12 11 0 7.00 7.70 -12 11 0 4.80 4.80 12 -12 0 48.40 9.50 12 12 0 40.90 11.00 -12 -12 0 35.70 14.50 -12 12 0 46.50 8.00 -12 13 0 -8.20 6.30 12 13 0 2.20 10.30 -12 -13 0 -6.30 8.20 12 -13 0 -1.90 7.80 -13 0 0 1.50 2.70 -13 0 0 -1.80 2.20 13 0 0 0.40 2.50 13 -1 0 155.08 10.20 13 1 0 162.38 10.60 -13 -1 0 163.78 10.60 -13 1 0 164.38 11.10 -13 -1 0 176.38 12.60 13 -1 0 149.29 10.80 -13 1 0 155.88 10.10 -13 2 0 -1.60 1.90 -13 -2 0 -5.50 2.20 -13 2 0 6.40 2.90 -13 -2 0 -5.00 2.20 13 2 0 -0.90 2.10 13 -2 0 0.40 2.00 13 -2 0 -0.20 2.50 13 3 0 300.37 17.90 13 -3 0 306.17 16.10 13 3 0 290.37 16.70 13 -3 0 244.58 15.90 -13 3 0 275.07 17.10 13 -3 0 298.17 17.90 13 3 0 262.77 16.30 -13 -3 0 276.67 17.40 -13 -4 0 6.40 3.40 13 -4 0 3.80 3.20 13 -4 0 0.10 1.70 -13 4 0 -3.50 2.80 13 4 0 -1.80 2.20 13 4 0 3.00 3.70 13 -4 0 -0.10 1.90 13 4 0 0.80 2.10 -13 5 0 172.38 11.60 13 -5 0 165.08 9.50 13 5 0 173.88 12.20 13 -5 0 155.38 9.70 -13 -5 0 174.18 12.00 13 5 0 177.28 10.70 13 5 0 152.18 12.20 13 -5 0 170.28 12.20 13 6 0 1.20 4.30 13 -6 0 -3.10 3.40 -13 6 0 0.20 3.30 13 6 0 0.50 2.10 -13 -6 0 0.00 3.30 13 6 0 -0.50 2.10 13 7 0 260.87 16.70 13 -7 0 296.47 19.70 -13 7 0 322.27 18.70 13 7 0 306.17 16.70 -13 -7 0 316.67 19.50 13 7 0 319.57 20.60 13 8 0 4.50 5.50 13 -8 0 3.80 4.90 -13 8 0 -4.50 3.40 -13 -9 0 36.40 6.50 13 -9 0 19.40 5.80 13 9 0 12.10 6.10 -13 9 0 16.10 5.10 -13 -10 0 4.30 5.40 13 10 0 0.10 6.10 -13 10 0 -2.50 4.40 13 -10 0 -0.40 5.70 13 -11 0 98.99 11.40 13 11 0 102.79 12.80 -13 -11 0 98.39 12.00 -13 12 0 5.40 6.30 -13 -12 0 -1.50 7.20 -14 0 0 1029.00 55.79 -14 0 0 1026.10 56.69 14 0 0 1013.80 56.19 -14 1 0 1.40 2.70 -14 -1 0 -3.70 2.30 -14 -1 0 1.80 3.10 -14 1 0 -1.20 2.20 14 -1 0 -0.30 2.90 14 1 0 0.80 2.60 -14 -2 0 30.00 4.60 14 -2 0 36.20 5.30 -14 2 0 34.80 4.00 14 -2 0 35.40 3.90 -14 -2 0 41.20 5.90 -14 2 0 31.50 5.10 14 2 0 33.40 4.60 -14 -3 0 0.70 2.90 14 -3 0 -2.10 2.70 14 3 0 -1.30 2.40 -14 3 0 -3.20 2.90 14 3 0 3.90 3.40 14 -3 0 -3.20 1.90 -14 4 0 75.99 6.90 14 4 0 67.69 6.30 14 -4 0 81.49 5.50 14 4 0 74.69 6.20 -14 -4 0 70.09 7.50 14 -4 0 70.09 7.90 14 4 0 74.09 7.50 -14 -5 0 4.30 3.40 -14 5 0 1.20 3.30 14 5 0 9.30 2.50 14 5 0 0.60 2.40 14 -5 0 0.60 1.60 14 5 0 -0.80 3.70 14 -5 0 1.90 4.00 14 -5 0 2.70 1.90 14 6 0 15.40 5.20 -14 -6 0 24.60 5.50 -14 6 0 17.10 4.50 14 -6 0 14.70 4.70 14 6 0 25.60 3.30 14 6 0 20.50 3.30 -14 7 0 1.50 3.60 -14 -7 0 -1.00 3.80 14 7 0 -0.80 2.00 14 -7 0 3.00 4.40 14 7 0 0.30 4.20 14 7 0 -3.20 2.10 -14 -8 0 27.90 6.70 14 8 0 31.60 7.40 14 -8 0 27.80 6.60 -14 8 0 34.20 5.70 14 9 0 0.30 5.50 -14 9 0 -5.70 4.00 14 -9 0 0.70 4.90 -14 -9 0 13.00 5.20 -14 10 0 9.60 5.40 -14 -10 0 25.00 7.20 14 -10 0 24.80 7.10 14 10 0 17.70 7.50 -14 -11 0 6.70 7.00 14 -11 0 2.50 7.00 -14 11 0 2.70 5.40 14 11 0 -4.10 8.20 14 -12 0 -9.30 7.40 -14 -12 0 -1.10 7.10 -14 12 0 -6.80 6.70 14 12 0 -8.20 9.40 -15 0 0 8.10 3.60 15 0 0 0.80 3.20 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-0.40 6.80 -15 -10 0 -3.00 6.20 -15 11 0 23.30 6.60 -15 -11 0 30.20 8.60 -15 12 0 -2.70 6.50 15 12 0 -33.00 9.10 15 -12 0 -0.10 6.90 -16 0 0 1136.29 61.79 16 0 0 1093.89 61.09 -16 0 0 1099.69 60.59 -16 1 0 0.40 3.40 -16 -1 0 2.40 3.90 16 -1 0 -2.80 3.20 -16 -1 0 5.40 3.40 -16 1 0 3.40 3.00 -16 -2 0 130.09 10.10 -16 2 0 144.59 9.50 16 2 0 116.09 9.60 16 -2 0 142.59 10.70 -16 2 0 134.39 10.80 -16 3 0 -2.90 3.00 16 3 0 4.20 4.50 16 -3 0 5.10 3.80 -16 -3 0 0.10 3.20 16 3 0 -1.30 2.90 16 -3 0 -4.70 2.40 16 -3 0 0.00 2.60 16 -4 0 94.89 7.10 16 4 0 86.79 7.80 -16 -4 0 92.19 8.50 16 -4 0 108.99 9.90 16 -4 0 94.69 7.00 16 4 0 88.39 9.30 -16 4 0 100.29 8.90 16 5 0 0.80 4.80 -16 5 0 2.20 4.10 16 -5 0 -0.10 2.00 16 -5 0 0.40 2.30 -16 -5 0 -6.00 3.10 16 -5 0 -3.40 3.80 16 5 0 3.10 3.00 16 -6 0 127.99 16.00 -16 -6 0 101.89 10.20 16 6 0 95.79 11.80 16 6 0 101.59 7.80 -16 6 0 98.59 9.40 16 6 0 101.69 8.20 -16 -7 0 -3.30 4.70 -16 7 0 -1.60 4.00 16 7 0 1.70 5.80 16 -7 0 -3.10 4.60 -16 8 0 38.40 6.50 16 8 0 16.90 7.40 -16 -8 0 13.40 5.90 16 -8 0 28.80 7.30 16 9 0 6.40 7.10 -16 9 0 2.90 5.20 -16 -9 0 -6.00 5.70 16 -9 0 0.60 6.50 -16 10 0 38.30 7.30 16 10 0 32.60 9.70 16 -10 0 16.90 8.30 -16 -10 0 27.60 7.60 16 -11 0 -10.00 7.40 -16 11 0 -6.10 6.40 16 11 0 -13.80 8.20 -16 -11 0 0.50 6.70 -17 0 0 4.80 4.00 17 0 0 2.80 3.50 -17 0 0 -1.90 3.30 17 1 0 7.40 3.80 17 -1 0 0.80 4.10 -17 1 0 4.00 4.00 -17 1 0 9.80 3.60 -17 -1 0 6.40 4.30 -17 -1 0 10.30 3.90 -17 -2 0 4.50 3.20 -17 2 0 2.20 3.70 17 -2 0 -1.40 3.80 -17 3 0 0.60 3.50 17 -3 0 0.30 2.80 17 3 0 4.20 3.40 17 -3 0 3.50 4.60 -17 -3 0 5.50 3.60 17 3 0 4.50 4.30 17 4 0 2.30 3.60 -17 -4 0 -4.30 3.70 17 -4 0 -3.00 2.80 17 -4 0 4.50 4.30 17 -4 0 3.30 2.90 17 4 0 -3.90 4.00 -17 4 0 -0.10 4.00 17 -5 0 16.10 6.00 17 -5 0 11.60 2.60 -17 5 0 16.10 4.80 -17 -5 0 20.60 5.60 17 -5 0 16.90 3.00 17 5 0 22.00 6.50 17 5 0 17.20 4.20 17 6 0 -4.60 3.30 -17 -6 0 -6.90 4.40 -17 6 0 0.80 4.30 17 6 0 -4.60 5.20 17 -6 0 6.70 5.00 17 7 0 332.17 19.80 -17 -7 0 351.56 22.70 17 -7 0 396.76 24.10 17 7 0 391.06 24.30 -17 7 0 313.37 22.00 17 8 0 4.10 6.60 -17 -8 0 6.10 5.50 -17 8 0 8.20 5.10 17 -8 0 6.90 6.10 17 -9 0 186.48 16.10 17 9 0 158.88 16.60 -17 9 0 166.28 13.90 -17 -9 0 164.08 15.00 -17 10 0 -2.60 6.20 -17 -10 0 6.90 6.50 17 -10 0 -2.60 6.40 17 11 0 105.39 14.70 17 -11 0 102.79 12.60 -17 11 0 78.69 10.50 -18 0 0 1591.44 87.09 18 0 0 1564.44 86.39 -18 0 0 1588.04 85.79 18 -1 0 -3.00 3.90 -18 -1 0 -7.20 3.90 -18 1 0 -1.00 3.40 -18 1 0 1.00 4.10 -18 -1 0 -4.30 3.70 18 1 0 -1.50 3.60 -18 -2 0 802.72 44.40 18 2 0 755.12 44.30 18 -2 0 814.02 45.00 -18 2 0 769.02 44.90 -18 -3 0 -1.50 4.00 18 3 0 12.40 5.00 18 -3 0 2.70 4.00 18 -3 0 -0.10 3.10 18 3 0 1.20 4.10 -18 3 0 0.40 4.30 18 -4 0 434.36 26.40 18 -4 0 528.65 29.50 -18 4 0 481.05 28.60 -18 -4 0 450.35 28.30 18 4 0 448.06 27.40 18 -4 0 494.55 27.60 18 -5 0 -1.80 4.30 -18 5 0 3.20 4.20 18 -5 0 3.10 4.40 18 5 0 0.20 5.30 18 5 0 -3.30 3.60 18 -6 0 225.28 16.50 18 6 0 203.18 13.90 18 6 0 209.38 17.40 -18 6 0 226.08 15.50 -18 -6 0 215.18 16.00 -18 7 0 -4.70 4.40 18 7 0 4.00 6.10 -18 -7 0 -3.40 5.20 18 -7 0 -7.60 5.50 -18 -8 0 139.99 13.00 18 8 0 144.99 14.60 -18 8 0 144.89 12.60 18 -8 0 134.09 14.20 -18 9 0 -5.70 5.70 -18 -9 0 -12.00 9.00 18 -9 0 7.30 8.30 18 9 0 -0.20 7.90 -18 -10 0 181.98 16.80 18 10 0 175.08 17.60 -18 10 0 155.48 14.30 18 -10 0 173.18 17.20 -19 0 0 -2.80 4.50 19 0 0 6.20 4.30 -19 0 0 -1.70 3.70 -19 1 0 146.09 12.00 -19 -1 0 159.58 12.80 -19 -1 0 150.68 11.30 19 -1 0 142.29 12.10 19 1 0 142.19 11.80 -19 1 0 138.49 11.00 19 2 0 5.30 4.10 -19 2 0 -3.90 4.40 19 2 0 7.10 4.90 -19 -2 0 4.40 4.60 19 -2 0 -4.90 4.60 19 3 0 45.70 6.80 -19 3 0 73.29 8.50 19 3 0 48.00 8.40 -19 -3 0 60.09 7.60 19 -3 0 71.69 8.70 19 -3 0 59.29 6.10 19 4 0 -1.20 5.00 -19 4 0 -1.70 5.00 19 -4 0 -0.40 3.40 19 -4 0 3.40 5.40 -19 -4 0 -4.70 3.70 19 5 0 55.89 8.60 19 5 0 62.29 7.20 -19 -5 0 66.59 8.10 19 -5 0 49.99 8.20 -19 5 0 60.99 7.90 -19 6 0 0.80 5.10 19 6 0 2.10 4.10 -19 -6 0 -5.30 5.00 19 -6 0 -4.20 5.50 19 6 0 0.00 6.60 19 7 0 111.19 12.90 -19 7 0 92.49 10.60 -19 -7 0 102.79 11.50 19 -7 0 117.49 12.60 -19 -8 0 0.30 6.20 -19 8 0 1.90 5.40 19 8 0 -2.90 7.50 19 -8 0 6.20 7.00 19 9 0 367.26 25.90 19 -9 0 391.36 25.70 -19 9 0 362.16 23.30 -19 -9 0 282.37 23.90 19 10 0 -5.00 14.20 -19 10 0 -5.90 7.10 -20 0 0 50.59 6.60 20 0 0 44.30 7.00 -20 0 0 53.69 11.90 -20 1 0 -0.10 4.20 20 -1 0 1.60 4.20 20 1 0 -1.30 4.30 -20 1 0 0.40 4.80 -20 -1 0 -2.60 4.20 -20 -1 0 8.40 5.60 20 2 0 66.39 9.00 20 -2 0 50.39 7.80 -20 -2 0 48.30 7.10 20 2 0 43.20 6.70 -20 2 0 58.49 7.90 20 -3 0 0.50 5.00 20 -3 0 1.60 3.80 -20 -3 0 1.20 4.70 -20 3 0 4.80 4.60 20 3 0 4.00 4.70 20 3 0 -3.20 4.70 20 4 0 218.58 16.00 20 -4 0 225.18 14.70 20 4 0 248.88 17.80 -20 -4 0 239.88 16.80 20 -4 0 236.98 17.20 20 5 0 -2.30 5.20 -20 -5 0 -11.50 4.80 20 5 0 -1.80 4.70 -20 5 0 0.50 5.50 20 -5 0 0.80 5.90 -20 6 0 8.90 5.80 20 -6 0 11.50 6.10 -20 -6 0 17.80 6.40 20 6 0 7.00 6.40 20 -7 0 2.70 6.00 -20 -7 0 0.00 5.60 20 7 0 -7.00 5.80 -20 7 0 -8.50 5.10 20 8 0 0.40 7.30 20 -8 0 0.70 6.90 -20 -8 0 12.20 11.80 -20 8 0 1.30 6.00 -20 9 0 -7.70 6.20 20 -9 0 -1.50 8.10 -20 -9 0 -0.40 7.40 20 9 0 -3.00 9.20 -21 0 0 1.70 4.30 21 0 0 -3.50 4.50 -21 0 0 -1.10 5.20 21 1 0 86.19 10.00 -21 -1 0 118.59 10.30 21 -1 0 92.29 10.50 -21 1 0 109.09 11.00 -21 1 0 118.59 9.90 21 2 0 -1.40 4.80 21 -2 0 1.10 4.30 -21 2 0 -0.90 5.10 21 -2 0 3.70 4.80 -21 -2 0 -8.00 4.20 21 2 0 1.10 5.60 21 3 0 137.69 12.40 21 -3 0 141.59 11.20 -21 -3 0 156.88 14.00 -21 3 0 163.58 13.00 21 -3 0 148.79 13.60 21 3 0 159.48 13.80 -21 -4 0 3.60 5.40 -21 4 0 2.70 5.40 21 -4 0 -3.30 4.50 21 -4 0 -1.00 6.30 21 4 0 -5.80 5.50 21 4 0 4.20 5.20 21 -5 0 14.60 6.50 -21 5 0 13.50 6.20 21 5 0 21.70 7.40 21 5 0 14.40 5.60 -21 -5 0 17.20 5.90 -21 -6 0 5.60 6.40 21 6 0 -1.40 6.30 -21 6 0 -13.30 5.50 21 -6 0 12.30 6.40 -21 -7 0 -8.70 6.60 -21 7 0 2.00 6.20 21 -7 0 0.10 7.20 21 7 0 -4.70 7.80 21 8 0 -1.20 8.20 21 -8 0 -2.60 6.60 -21 8 0 -1.80 7.00 -21 -8 0 -7.00 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195.48 12.30 15 4 -2 176.38 13.20 15 -5 -2 5.20 3.80 15 5 2 0.70 2.40 -15 -5 2 9.50 4.40 15 5 2 -2.20 4.50 15 5 2 3.90 2.40 -15 5 -2 1.90 3.70 15 -5 2 1.00 2.80 15 5 -2 4.40 4.40 15 5 -2 9.00 3.40 15 -5 2 6.90 4.20 15 -5 2 1.90 2.70 -15 -5 -2 3.60 4.00 -15 5 2 0.30 3.70 15 6 2 48.50 4.30 -15 -6 2 55.19 7.40 -15 6 -2 54.99 6.50 15 6 2 60.89 4.40 15 -6 -2 57.59 7.50 15 6 2 52.89 7.80 -15 6 2 55.39 6.90 15 -6 2 58.19 8.00 15 -6 2 61.49 5.00 15 -6 2 53.69 5.40 15 6 -2 54.29 8.10 15 6 -2 56.29 6.10 -15 -6 -2 59.99 8.00 -15 7 -2 0.20 4.10 15 -7 -2 -0.90 4.20 -15 -7 2 -0.90 4.00 15 7 2 1.40 5.10 -15 7 2 -4.00 4.30 15 7 -2 1.80 3.20 -15 -7 -2 0.10 4.60 15 -7 2 -0.20 2.30 15 -7 2 0.30 4.70 -15 8 -2 187.38 14.20 15 8 2 187.48 16.90 -15 -8 2 263.17 16.90 15 -8 -2 212.68 15.90 15 8 -2 196.58 13.00 15 -8 2 235.88 16.90 15 8 -2 197.78 16.40 -15 8 2 224.08 15.40 -15 -8 -2 222.38 15.80 -15 9 -2 35.00 6.50 -15 -9 2 44.40 8.20 15 -9 -2 43.90 8.00 15 9 2 35.70 8.60 15 -9 2 35.10 7.50 -15 -9 -2 38.60 8.00 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392.96 21.70 -11 -2 -4 362.36 22.60 -11 2 4 409.06 23.00 11 -2 4 360.56 22.20 11 2 -4 397.46 22.80 11 -2 4 360.96 22.30 -11 2 4 403.56 21.60 -11 -3 4 108.99 8.60 11 3 4 97.29 8.00 -11 3 -4 87.69 7.20 11 3 4 120.19 6.60 11 3 4 90.09 6.40 11 -3 -4 99.39 5.80 -11 3 -4 88.99 7.80 -11 -3 4 117.99 8.00 11 -3 4 97.59 8.00 11 3 -4 100.29 7.70 11 -3 4 102.79 7.40 -11 3 4 104.79 7.80 -11 -3 -4 98.29 7.90 11 -3 4 88.99 7.00 11 -4 -4 185.08 12.00 11 4 4 174.38 9.90 -11 4 -4 177.28 12.10 -11 4 -4 185.48 11.10 11 4 4 169.98 12.10 11 4 4 167.48 9.90 -11 -4 4 174.98 11.80 -11 -4 -4 175.68 11.90 11 -4 4 175.58 11.30 11 4 -4 163.38 11.50 11 -4 4 173.88 10.70 -11 4 4 170.88 12.70 11 4 -4 170.48 12.00 11 5 4 6.00 3.60 11 -5 -4 2.10 3.50 -11 -5 4 4.60 3.10 -11 5 -4 1.60 2.30 -11 5 -4 6.60 3.60 11 -5 4 6.50 2.50 -11 -5 -4 7.90 3.30 11 5 -4 5.00 3.60 11 -5 4 5.30 2.80 11 5 -4 2.10 2.80 -11 5 4 5.90 3.10 -11 6 -4 212.18 12.50 -11 -6 4 190.58 14.00 -11 6 -4 173.68 13.80 11 6 4 228.38 14.60 11 -6 -4 200.88 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2.70 -12 -3 4 -2.80 2.70 12 3 4 -0.20 2.50 12 3 4 2.80 1.80 -12 3 -4 -0.10 2.60 -12 -3 4 -3.10 2.60 -12 -3 -4 -1.80 2.80 12 -3 4 -0.30 2.50 12 3 -4 3.00 2.60 -12 3 4 -0.60 2.40 12 4 4 114.69 9.60 12 4 4 114.19 7.30 12 -4 -4 122.69 9.40 -12 4 -4 124.19 8.70 -12 -4 4 130.19 9.60 -12 4 -4 126.59 9.30 12 4 4 122.99 7.40 -12 4 4 126.49 9.50 12 -4 4 111.59 8.60 12 4 -4 132.09 9.10 12 4 -4 104.79 9.20 -12 -4 -4 110.89 9.30 12 -4 4 121.09 8.10 -12 5 -4 27.10 5.10 12 -5 -4 34.60 5.20 -12 -5 4 26.30 4.70 -12 5 -4 37.30 4.30 12 5 4 23.70 5.10 -12 5 4 23.40 4.50 -12 -5 -4 32.20 5.30 12 -5 4 25.70 3.60 12 5 -4 29.60 5.20 12 -5 4 31.70 4.50 12 5 -4 31.70 4.60 -12 6 -4 54.49 5.70 -12 6 -4 63.79 7.40 -12 -6 4 41.30 6.20 12 6 4 59.49 7.60 12 -6 -4 61.39 7.10 -12 -6 -4 58.89 7.00 12 -6 4 57.49 5.80 12 -6 4 53.29 5.20 -12 6 4 59.39 6.60 12 6 -4 56.29 6.10 12 6 -4 49.99 6.90 -12 7 -4 9.60 3.40 12 -7 -4 11.20 4.40 -12 7 -4 7.70 4.30 12 7 4 9.60 5.00 -12 -7 4 11.70 4.80 12 -7 4 12.70 3.50 12 -7 4 10.50 5.30 12 7 -4 6.30 4.40 -12 7 4 11.10 4.50 -12 -7 -4 9.30 4.40 12 7 -4 13.00 3.80 12 8 4 25.00 6.10 12 -8 -4 14.50 5.40 -12 -8 4 7.70 4.70 -12 8 -4 16.20 5.20 -12 8 -4 7.60 3.70 12 8 -4 28.60 6.60 12 -8 4 22.20 4.20 -12 -8 -4 28.20 5.90 -12 8 4 9.40 4.60 12 8 -4 16.30 4.00 -12 -9 4 9.60 5.30 -12 9 -4 13.30 4.40 12 9 4 14.70 6.50 -12 9 -4 13.20 6.10 12 -9 -4 10.80 5.20 -12 -9 -4 7.10 4.90 12 -9 4 5.50 3.70 12 9 -4 7.90 5.50 -12 9 4 6.10 4.50 12 9 -4 14.40 3.90 12 -10 -4 -2.00 5.30 12 10 4 3.70 6.30 -12 10 -4 0.00 4.00 -12 10 -4 5.60 5.20 -12 -10 4 2.20 6.10 -12 -10 -4 3.00 4.90 -12 10 4 -0.40 5.20 12 10 -4 2.70 3.90 12 -10 4 4.10 3.90 12 10 -4 9.90 6.80 12 11 4 23.20 8.90 -12 11 -4 34.00 6.00 -12 -11 4 31.40 7.80 12 -11 -4 9.70 6.70 12 11 -4 17.00 8.60 -12 11 4 27.80 7.20 -12 -11 -4 35.20 7.90 12 12 4 8.40 8.60 12 -12 -4 16.30 7.50 -12 -12 4 -2.70 6.60 -12 12 4 -3.30 6.30 12 12 -4 -7.60 8.30 -12 -12 -4 6.40 6.60 13 0 4 563.34 32.30 -13 0 4 578.24 31.90 -13 0 -4 574.94 32.40 -13 0 4 600.84 33.20 13 0 -4 553.24 32.70 13 1 4 -3.70 2.70 -13 -1 4 -0.30 2.40 13 1 4 -0.20 2.30 -13 1 -4 0.50 2.80 -13 -1 4 -0.50 3.00 13 -1 -4 -1.20 2.40 13 -1 -4 -3.50 2.00 -13 -1 -4 0.50 2.80 13 1 -4 1.00 2.50 13 -1 4 0.80 2.30 -13 1 4 -3.30 2.50 -13 1 4 -1.80 1.90 -13 2 -4 123.19 9.00 -13 -2 4 112.09 9.50 13 2 4 119.09 9.30 13 2 4 120.79 8.30 13 -2 -4 114.59 9.20 13 2 4 112.49 8.20 13 -2 -4 114.99 7.80 -13 -2 4 147.49 9.20 -13 -2 -4 122.19 9.10 -13 2 4 129.69 7.80 -13 2 4 132.79 9.50 13 -2 4 114.79 8.50 13 2 -4 122.09 9.20 13 3 4 37.90 4.00 -13 3 -4 40.80 5.30 -13 3 -4 21.60 4.20 -13 -3 4 41.60 5.90 -13 -3 4 44.40 5.50 13 -3 -4 36.90 3.40 13 3 4 41.60 5.60 13 -3 -4 47.50 5.90 13 -3 4 41.70 4.70 -13 3 4 40.20 5.30 13 3 -4 40.30 5.20 -13 -3 -4 48.60 5.50 -13 3 4 37.80 3.20 -13 4 -4 142.69 12.00 -13 -4 4 182.68 12.30 13 4 4 170.08 12.60 13 -4 -4 196.58 12.90 -13 4 -4 167.48 11.50 13 4 4 175.78 10.40 13 4 4 186.58 10.40 13 4 -4 174.98 12.00 13 4 -4 165.38 12.50 13 -4 4 184.08 11.70 -13 -4 -4 166.18 12.20 -13 4 4 181.78 12.20 -13 -5 4 6.40 3.90 -13 5 -4 7.50 3.20 13 -5 -4 8.50 3.90 13 5 4 7.50 4.10 -13 5 -4 4.20 4.10 13 5 -4 6.00 3.50 -13 5 4 4.00 3.30 13 5 -4 7.70 4.60 13 -5 4 10.00 3.30 -13 -5 -4 3.20 3.80 -13 6 -4 5.30 3.90 13 6 4 6.50 4.60 -13 -6 4 0.80 4.20 13 -6 -4 -1.00 3.50 -13 6 -4 3.30 2.90 13 -6 4 10.90 4.90 13 6 -4 11.10 3.60 -13 6 4 4.30 3.60 13 6 -4 1.30 4.50 13 -6 4 7.80 3.30 -13 -6 -4 7.50 3.90 -13 7 -4 36.30 6.40 13 -7 -4 37.10 6.70 13 7 4 27.20 6.40 -13 7 -4 47.30 5.50 -13 -7 4 49.20 7.00 13 -7 4 43.70 5.20 13 7 -4 48.30 7.60 -13 7 4 47.40 6.60 13 7 -4 46.60 5.80 13 -7 4 41.30 7.00 -13 -7 -4 42.70 6.60 -13 8 -4 1.30 4.30 -13 -8 4 0.90 4.20 13 8 4 7.90 6.00 13 -8 4 6.90 3.50 13 8 -4 -10.20 5.00 13 8 -4 -1.00 3.40 -13 -8 -4 7.40 5.00 -13 8 4 8.70 4.00 -13 -9 4 4.30 5.60 -13 9 -4 5.30 5.50 13 9 4 6.70 6.50 -13 9 -4 4.20 4.00 13 -9 -4 2.90 4.50 -13 -9 -4 6.00 4.80 -13 9 4 4.00 4.90 13 -9 4 2.40 3.50 13 9 -4 -8.30 3.70 13 9 -4 3.30 6.10 13 10 4 31.20 8.20 -13 10 -4 24.60 5.30 13 -10 -4 22.60 6.70 -13 -10 4 15.00 7.00 -13 -10 -4 14.00 6.00 -13 10 4 33.20 6.60 13 10 -4 30.10 7.70 13 11 4 -5.00 7.60 -13 11 -4 -5.90 4.70 -13 -11 4 -1.40 5.90 13 -11 -4 8.00 6.60 13 -11 4 5.90 7.00 -13 11 4 5.40 5.90 13 11 -4 -6.20 7.50 -13 -11 -4 2.00 7.10 -13 -12 4 16.20 8.70 13 12 4 27.60 10.70 13 -12 4 18.70 8.30 13 12 -4 9.60 9.30 -13 12 4 17.60 7.10 -13 -12 -4 14.00 7.90 14 0 4 53.29 5.90 14 0 -4 44.80 5.60 -14 0 4 55.49 5.30 -14 0 4 46.70 6.30 -14 0 -4 45.50 5.40 -14 1 -4 93.99 8.10 -14 -1 4 100.49 7.90 14 -1 -4 102.99 8.80 14 1 4 99.39 8.40 14 -1 -4 98.19 7.50 -14 -1 4 128.09 9.30 14 1 4 99.49 7.80 -14 1 4 103.89 8.80 14 -1 4 115.19 8.50 -14 1 4 96.39 7.30 14 1 -4 110.69 9.40 14 -2 -4 3.10 2.20 14 -2 -4 3.70 3.40 14 2 4 4.40 3.40 -14 -2 4 0.00 2.80 -14 2 -4 0.20 2.90 -14 -2 4 3.40 3.50 14 2 4 0.80 2.30 -14 2 4 5.10 3.40 14 -2 4 5.70 2.90 14 -2 4 4.00 2.60 -14 -2 -4 1.90 3.10 14 2 -4 -1.10 2.90 -14 2 4 2.20 1.90 14 -3 -4 62.79 5.00 14 3 4 62.79 7.50 -14 3 -4 71.69 6.70 14 3 4 62.19 5.70 -14 -3 4 59.39 7.50 -14 -3 4 72.49 7.00 14 -3 -4 71.09 7.10 14 3 4 70.39 5.70 -14 -3 -4 75.89 7.40 -14 3 4 73.99 7.50 14 -3 4 74.29 6.60 14 3 -4 71.39 7.00 14 4 4 0.80 2.00 14 4 4 -4.10 3.30 -14 4 -4 1.90 3.20 14 4 4 0.80 2.10 14 -4 -4 -2.60 3.50 -14 -4 4 0.30 3.60 -14 4 -4 2.60 3.00 14 -4 4 7.00 3.10 14 4 -4 7.40 3.50 14 4 -4 1.10 3.70 -14 -4 -4 -0.40 3.20 -14 4 4 -0.60 3.40 14 5 4 200.88 14.70 14 -5 -4 186.48 14.10 -14 5 -4 185.58 14.00 14 5 4 193.88 11.30 -14 5 -4 207.88 13.20 -14 -5 4 221.38 14.50 14 5 4 207.18 11.40 -14 5 4 204.48 14.10 -14 -5 -4 199.68 13.90 14 -5 4 205.68 13.30 14 5 -4 193.18 13.60 14 5 -4 204.78 14.60 14 6 4 -2.00 4.00 14 -6 -4 5.70 3.90 -14 6 -4 3.20 3.80 -14 -6 4 -1.30 3.70 -14 6 -4 -1.70 2.90 -14 6 4 -6.60 3.80 -14 -6 -4 -0.70 3.40 14 -6 4 2.90 3.30 14 6 -4 -7.70 3.10 14 6 -4 6.20 4.50 -14 -7 4 241.18 17.80 14 7 4 255.67 20.00 -14 7 -4 297.57 20.10 14 -7 -4 294.67 18.50 14 7 -4 256.97 18.40 14 -7 4 268.17 16.30 -14 7 4 246.28 17.20 -14 -7 -4 258.27 22.10 14 7 -4 257.77 16.70 14 8 4 3.40 5.40 -14 8 -4 5.20 3.60 14 -8 -4 13.50 5.70 -14 -8 4 2.00 5.40 14 -8 4 9.60 3.80 -14 -8 -4 4.90 5.30 -14 8 4 12.40 5.30 14 8 -4 8.00 3.80 -14 -9 4 151.38 13.10 14 9 4 119.69 14.00 14 -9 -4 143.89 12.70 -14 9 -4 144.09 10.90 14 -9 4 147.09 10.10 14 9 -4 154.88 10.80 -14 9 4 146.99 12.40 -14 -9 -4 137.09 12.60 14 9 -4 126.79 13.80 14 10 4 12.80 7.20 14 -10 -4 10.80 5.80 -14 -10 4 18.00 7.40 -14 10 -4 9.00 4.80 14 -10 4 8.90 6.80 -14 -10 -4 -3.60 5.70 14 10 -4 3.30 6.90 -14 10 4 8.50 5.90 -14 11 -4 116.99 11.30 -14 -11 4 103.79 12.80 14 -11 -4 131.39 13.60 14 11 -4 133.99 14.70 -14 11 4 124.89 12.60 14 -11 4 180.58 22.40 14 -12 -4 -8.40 7.40 14 12 4 -0.40 9.40 14 -12 4 3.40 8.10 14 12 -4 18.20 10.00 -14 12 4 10.50 7.10 -14 -12 -4 -1.80 7.80 -15 0 4 923.41 49.70 15 0 -4 893.91 50.59 15 0 4 896.81 50.19 -15 0 4 909.01 50.99 -15 1 -4 39.50 5.80 15 1 4 33.10 4.60 -15 -1 4 30.70 4.60 -15 -1 4 36.10 6.00 15 -1 -4 29.70 5.40 15 1 4 31.60 5.30 -15 1 4 32.30 4.10 15 -1 4 37.80 5.10 -15 -1 -4 29.90 4.90 15 1 -4 27.80 4.80 -15 1 4 36.30 5.50 -15 -2 4 492.65 28.50 15 2 4 474.85 26.90 -15 -2 4 454.45 27.30 15 2 4 441.76 27.90 -15 2 -4 474.35 28.50 15 -2 -4 456.85 26.40 15 -2 -4 475.85 28.00 -15 2 4 492.85 26.20 15 -2 4 438.46 27.00 -15 2 4 518.85 28.10 15 -2 4 500.75 28.10 -15 -2 -4 468.95 27.60 15 2 -4 439.36 27.70 -15 -3 4 20.20 4.40 15 3 4 10.90 3.10 -15 -3 4 15.60 5.00 15 -3 -4 22.30 4.70 15 -3 -4 7.80 2.50 15 3 4 1.50 3.90 15 3 4 8.10 2.80 15 3 -4 8.70 3.90 -15 3 4 12.40 4.20 -15 -3 -4 6.00 3.80 15 -3 4 11.50 4.40 15 -3 4 9.90 3.50 -15 -4 4 264.47 16.80 15 -4 -4 266.67 17.30 15 4 4 261.37 17.40 15 4 4 254.77 14.90 15 -4 4 258.37 17.30 -15 -4 -4 242.28 16.50 -15 4 4 213.28 16.40 15 -4 4 252.57 15.90 15 4 -4 271.27 17.40 15 4 -4 244.38 16.40 -15 5 -4 76.59 8.00 15 -5 -4 85.59 9.00 -15 -5 4 89.19 8.30 15 5 4 76.69 9.10 15 5 4 72.69 5.40 15 5 4 84.39 5.50 15 5 -4 73.99 8.80 -15 -5 -4 65.79 7.90 15 5 -4 80.69 8.10 15 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4 5.60 4.20 -16 4 4 9.20 4.20 -16 -4 -4 5.70 4.60 16 4 -4 4.80 4.00 16 4 -4 11.10 5.30 16 -5 -4 183.28 13.60 -16 -5 4 167.18 12.70 16 5 4 153.08 13.40 -16 5 -4 161.48 11.90 16 5 4 149.09 10.10 16 -5 4 167.48 13.40 -16 5 4 203.18 13.60 -16 -5 -4 181.58 13.20 16 5 -4 161.88 13.20 16 -5 4 175.28 12.20 -16 -6 4 47.30 7.90 16 -6 -4 50.59 7.40 -16 6 -4 46.00 6.00 16 6 4 48.70 7.80 -16 -6 -4 50.59 7.30 -16 6 4 56.39 7.20 16 -6 4 67.99 8.70 16 -6 4 38.20 5.70 16 6 -4 31.80 6.00 16 6 -4 35.10 8.00 16 -7 -4 162.88 13.20 -16 -7 4 173.18 12.90 16 7 4 146.19 13.50 -16 7 -4 149.69 11.70 16 -7 4 152.48 13.10 -16 -7 -4 175.68 13.00 16 -7 4 160.98 11.10 16 7 -4 143.09 14.10 -16 7 4 132.79 12.40 16 7 -4 140.19 11.80 16 -8 -4 5.60 6.00 16 8 4 8.10 6.50 -16 -8 4 9.70 5.80 -16 8 -4 5.10 4.60 -16 8 4 4.80 4.80 -16 -8 -4 17.60 5.70 16 8 -4 4.70 4.70 16 -8 4 -1.40 5.20 16 8 -4 1.30 6.60 16 9 4 128.29 14.60 -16 -9 4 121.79 12.30 16 -9 -4 110.29 12.30 -16 9 -4 116.09 10.40 16 -9 4 136.89 13.70 16 9 -4 105.39 13.50 -16 -9 -4 112.29 11.80 -16 9 4 107.49 11.60 -16 10 -4 9.50 5.40 16 -10 -4 -5.30 6.50 -16 -10 4 11.90 8.30 -16 10 4 6.00 6.40 16 10 -4 1.30 8.50 16 11 4 117.99 15.30 16 -11 -4 133.39 13.80 -16 -11 4 107.39 13.10 16 -11 4 98.99 13.00 -16 11 4 107.89 12.20 -16 -11 -4 114.49 12.90 16 11 -4 81.19 14.10 17 0 4 3.90 3.80 -17 0 -4 10.70 4.20 -17 0 4 -1.70 3.90 -17 0 4 1.70 3.20 17 0 4 2.00 3.50 17 0 -4 3.00 3.90 -17 -1 4 166.98 11.90 -17 1 -4 113.09 10.10 17 1 4 124.69 10.10 17 1 4 134.19 11.10 17 -1 -4 149.39 10.90 -17 -1 4 119.99 9.80 -17 -1 -4 132.19 10.50 -17 1 4 122.89 9.10 -17 1 4 116.99 10.80 17 1 -4 128.99 10.70 17 -1 4 128.69 10.60 17 -1 4 137.19 10.20 17 2 4 64.19 6.70 17 -2 -4 62.19 6.40 17 2 4 56.29 7.60 -17 -2 4 69.29 8.40 -17 -2 4 64.89 7.20 17 -2 -4 69.59 8.10 -17 2 -4 88.99 8.20 17 2 -4 77.79 8.30 -17 -2 -4 60.19 7.20 -17 2 4 73.99 6.00 17 -2 4 66.99 8.10 -17 2 4 68.09 7.80 17 -2 4 69.59 8.00 -17 -3 4 -4.30 4.20 17 -3 -4 -1.50 3.90 -17 -3 4 5.30 3.50 17 -3 -4 1.40 2.80 17 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17 -8 -4 123.99 12.70 -17 -8 -4 119.39 12.10 17 8 -4 97.69 12.20 -17 8 4 119.49 10.80 17 8 -4 94.09 10.00 17 -8 4 110.59 12.30 -17 9 -4 8.80 5.60 17 9 4 13.00 7.80 17 -9 -4 5.50 6.50 -17 -9 4 19.20 7.20 17 -9 4 -1.20 6.90 17 9 -4 22.20 8.10 -17 9 4 4.10 6.30 -17 -9 -4 23.50 7.60 17 -10 -4 18.80 7.90 -17 10 -4 -1.30 6.20 -17 -10 4 5.40 7.30 17 10 4 9.80 8.20 17 10 -4 25.10 14.40 17 -10 4 7.00 8.00 -17 -10 -4 14.50 6.80 -17 10 4 5.50 6.70 17 -11 -4 12.60 12.50 17 11 -4 23.30 9.50 -17 11 4 1.50 10.70 18 0 4 50.89 6.60 -18 0 4 50.39 6.70 -18 0 4 41.00 7.20 18 0 4 60.89 7.70 -18 0 -4 63.19 7.20 18 0 -4 46.90 6.80 18 1 4 34.40 6.70 18 1 4 35.20 5.80 -18 -1 4 38.00 5.60 -18 -1 4 40.20 6.90 18 -1 -4 55.89 7.20 -18 1 -4 42.80 6.20 -18 1 4 25.90 6.20 -18 -1 -4 53.39 6.50 18 -1 4 33.50 6.30 -18 1 4 38.20 5.00 18 -1 4 36.90 5.80 18 1 -4 43.60 6.70 -18 -2 4 23.70 5.00 -18 2 -4 23.20 5.80 18 2 4 29.50 6.50 -18 -2 4 35.70 6.20 18 -2 -4 27.00 5.70 -18 -2 -4 36.20 6.00 18 2 -4 30.70 5.70 -18 2 4 35.80 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23.70 5.50 19 -3 -4 23.60 3.70 19 -3 -4 35.80 7.20 19 3 4 13.00 5.70 -19 3 -4 30.20 5.90 19 3 4 35.00 5.10 -19 -3 4 32.30 7.30 19 3 -4 18.30 5.60 -19 3 4 20.50 6.70 19 -3 4 26.30 5.70 -19 -3 -4 24.60 6.10 19 -3 4 28.30 6.40 19 4 4 75.79 10.30 19 4 4 74.39 7.30 -19 4 -4 72.89 8.20 -19 -4 4 68.09 8.50 19 -4 -4 81.59 10.00 -19 4 4 75.59 9.40 19 4 -4 76.69 9.50 19 -4 4 85.59 10.30 19 4 -4 63.99 8.70 -19 -4 -4 69.59 8.80 19 5 4 0.60 5.50 -19 -5 4 3.60 5.30 -19 5 -4 -0.60 4.50 19 5 4 0.90 3.30 19 -5 -4 -3.50 5.30 19 -5 4 1.20 5.70 -19 -5 -4 -3.40 5.10 19 5 -4 4.30 5.10 19 5 -4 -1.90 5.40 -19 5 4 -9.00 5.10 19 -5 4 4.70 4.70 -19 -6 4 28.20 6.90 19 -6 -4 22.10 6.70 19 6 4 32.20 8.20 -19 6 -4 27.20 6.00 -19 6 4 42.50 7.50 19 6 -4 27.00 6.50 19 6 -4 35.50 8.50 19 -6 4 35.00 8.10 -19 -6 -4 27.00 7.10 19 -6 4 29.40 5.90 -19 -7 4 -0.30 5.50 19 -7 -4 6.90 5.90 -19 7 -4 7.10 5.50 19 7 4 14.00 7.60 19 7 -4 2.40 6.70 19 7 -4 -0.80 5.60 -19 -7 -4 0.80 5.90 19 -7 4 -1.60 6.40 -19 7 4 6.90 6.10 19 8 4 11.00 7.90 -19 -8 4 5.40 6.50 -19 8 -4 19.10 6.40 19 -8 -4 11.40 6.70 19 8 -4 15.30 8.30 19 -8 4 17.40 7.90 -19 8 4 1.20 6.50 -19 -8 -4 25.80 8.30 19 -9 -4 4.00 8.10 -19 -9 4 1.70 7.10 -19 9 -4 7.50 6.90 19 9 4 7.60 9.30 19 9 -4 -1.70 8.60 -19 9 4 -0.40 6.40 -19 -9 -4 8.50 7.90 19 -9 4 1.90 7.70 19 10 -4 18.80 9.90 -19 10 4 6.20 9.40 -20 0 -4 21.70 5.60 20 0 -4 28.10 6.60 -20 0 4 19.70 5.10 20 0 4 31.90 6.70 -20 0 4 21.90 6.50 20 0 4 26.20 5.80 20 -1 -4 4.90 6.20 -20 -1 4 5.20 4.00 20 1 4 3.90 4.50 -20 -1 4 10.10 5.70 -20 -1 -4 6.90 5.20 -20 1 4 12.30 5.20 -20 1 4 11.90 4.30 20 -1 4 -5.10 4.30 20 -1 4 9.20 4.80 20 1 -4 5.70 5.40 20 -2 -4 28.20 6.80 20 2 4 20.50 6.10 -20 -2 4 17.10 7.00 -20 2 -4 13.90 5.90 -20 -2 4 12.60 4.80 20 2 4 13.30 4.80 20 -2 4 23.80 6.20 -20 2 4 20.10 6.10 -20 -2 -4 22.80 6.30 20 -2 4 13.10 5.00 20 2 -4 14.00 5.70 -20 2 4 11.20 4.20 20 3 4 -1.90 3.90 -20 -3 4 -0.60 4.30 20 -3 -4 -1.80 3.10 20 3 4 3.20 5.70 20 -3 -4 -0.90 4.90 -20 3 -4 -1.70 4.70 20 -3 4 7.70 4.70 20 -3 4 1.60 5.60 20 3 -4 4.60 5.20 -20 3 4 0.00 5.60 -20 -3 -4 -5.00 4.10 20 4 4 53.09 9.20 -20 4 -4 58.19 8.20 20 -4 -4 79.99 9.40 -20 -4 4 67.19 8.80 20 4 4 74.99 7.70 -20 -4 -4 82.29 8.90 20 -4 4 81.49 10.30 -20 4 4 62.49 9.20 20 4 -4 53.39 8.50 20 4 -4 54.89 9.20 20 -4 4 65.89 7.90 20 5 4 83.79 11.10 -20 5 -4 102.09 10.30 -20 -5 4 99.89 10.50 20 -5 -4 97.29 11.10 20 5 -4 85.99 11.50 20 -5 4 127.29 10.50 -20 5 4 74.89 9.90 -20 -5 -4 83.59 10.00 20 5 -4 108.79 10.80 20 -5 4 108.49 11.90 20 6 4 18.80 7.10 20 -6 -4 16.40 7.20 -20 -6 4 32.50 7.70 -20 6 -4 35.20 6.70 20 -6 4 16.40 7.50 -20 -6 -4 24.50 6.60 -20 6 4 25.40 7.40 20 6 -4 17.70 7.00 20 6 -4 16.40 6.60 20 7 4 100.89 12.90 -20 -7 4 129.79 12.20 -20 7 -4 114.59 11.20 20 -7 -4 106.19 12.30 20 7 -4 97.89 13.40 -20 -7 -4 137.39 13.20 20 -7 4 107.69 12.90 -20 7 4 95.59 11.50 -20 -8 4 9.80 7.70 20 -8 -4 12.10 8.00 20 8 4 7.40 8.60 -20 8 4 -6.50 5.90 -20 -8 -4 -3.70 6.20 20 8 -4 -9.00 8.10 20 -8 4 -2.30 7.40 -20 9 -4 94.19 14.80 20 -9 -4 80.49 17.90 -20 -9 4 57.89 11.90 20 9 -4 76.39 12.80 21 0 4 141.49 13.50 -21 0 4 167.18 13.80 -21 0 4 151.08 11.90 21 0 4 148.79 12.60 21 0 -4 162.48 14.70 21 1 4 13.20 6.10 -21 -1 4 3.00 5.30 -21 -1 4 1.00 4.30 21 -1 -4 2.90 5.50 21 1 4 5.60 5.10 21 1 -4 2.20 5.40 -21 -1 -4 1.00 5.30 -21 1 4 -2.90 5.10 -21 1 4 2.00 4.20 21 -1 4 13.90 5.50 21 -1 4 -1.80 5.10 21 -1 4 0.90 5.20 -21 -2 4 546.95 30.90 21 2 4 543.35 32.40 21 -2 -4 546.65 32.40 21 2 4 507.65 30.50 -21 -2 4 453.05 32.10 -21 2 -4 525.95 32.70 -21 2 4 492.55 31.70 21 -2 4 505.35 30.70 21 -2 4 532.15 32.00 21 2 -4 474.15 31.40 -21 -2 -4 467.15 31.90 -21 2 4 578.64 29.60 -21 3 -4 20.90 6.40 21 3 4 18.80 6.80 21 -3 -4 29.30 7.80 21 3 4 25.40 5.60 21 -3 4 26.20 6.80 21 -3 4 33.80 6.40 -21 -3 -4 36.00 6.90 21 3 -4 31.90 7.30 -21 3 4 23.10 7.20 -21 4 -4 147.49 13.60 21 4 4 146.49 12.40 21 -4 -4 205.18 16.00 21 4 4 169.28 16.00 -21 -4 4 166.08 13.80 21 -4 4 172.18 13.40 21 4 -4 219.68 15.90 21 -4 4 175.48 15.00 -21 -4 -4 175.18 14.60 -21 4 4 154.98 14.10 21 4 -4 174.18 14.60 21 -5 -4 14.10 7.40 21 5 4 22.70 7.60 -21 -5 4 12.30 6.50 21 5 -4 15.60 6.70 -21 -5 -4 9.20 6.40 21 -5 4 19.60 7.80 -21 5 4 16.10 6.30 21 5 -4 9.10 6.80 21 6 4 122.59 13.80 21 -6 -4 107.79 12.50 -21 6 -4 143.49 14.20 -21 -6 4 133.89 12.80 -21 -6 -4 99.89 11.70 -21 6 4 114.09 12.50 21 -6 4 110.19 13.10 21 6 -4 100.19 11.30 21 6 -4 109.49 13.30 -21 7 -4 -3.40 5.70 -21 -7 4 0.10 6.60 21 -7 -4 -0.40 7.20 21 7 4 -1.10 7.10 -21 -7 -4 8.50 6.30 21 -7 4 14.20 7.40 21 7 -4 -5.50 7.20 -21 7 4 -6.90 5.80 -21 8 -4 137.99 13.50 21 -8 -4 145.89 14.80 21 8 4 103.99 13.80 -21 -8 4 126.99 14.20 -21 -8 -4 165.08 15.40 21 8 -4 137.59 16.50 21 -8 4 134.49 15.40 -21 8 4 128.59 14.90 -22 0 4 -1.30 4.40 22 0 4 -2.80 6.00 -22 0 4 7.90 6.40 22 0 -4 9.20 6.20 22 0 4 -7.20 4.80 22 1 4 -4.10 5.40 -22 -1 4 -5.70 6.40 22 1 4 -8.30 5.10 -22 -1 4 3.60 4.90 22 -1 -4 5.50 5.00 22 -1 4 -1.30 5.50 22 -1 4 -0.10 5.70 22 1 -4 -0.70 5.50 -22 -1 -4 3.30 6.30 -22 1 4 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11.30 -22 -7 4 51.79 9.70 -22 -7 -4 57.89 10.60 22 7 -4 77.49 12.60 22 -7 4 70.99 11.00 -22 8 -4 15.10 8.30 -22 8 4 20.40 8.70 23 0 4 47.80 8.10 23 0 4 48.60 8.80 -23 0 4 49.00 7.30 -23 0 4 42.30 8.50 23 0 -4 61.29 9.00 23 0 4 55.39 8.30 23 1 4 -1.50 5.50 23 -1 -4 -4.90 6.60 -23 -1 4 4.10 5.40 23 1 4 11.30 7.40 -23 -1 4 8.20 6.90 -23 1 4 -3.50 4.80 -23 1 4 -0.80 7.00 23 1 -4 12.20 6.40 23 -1 4 6.40 6.60 23 -1 4 -5.40 6.00 -23 -1 -4 7.60 6.30 23 -1 4 -7.00 5.80 -23 -2 4 136.79 14.20 23 2 4 133.79 12.50 23 -2 -4 143.09 14.30 -23 -2 4 137.59 12.70 23 2 4 119.39 13.70 -23 2 4 118.19 13.90 23 -2 4 127.89 12.70 23 2 -4 133.29 14.00 23 -2 4 147.39 13.20 23 -2 4 152.48 13.70 -23 -2 -4 141.09 13.20 23 3 4 1.60 7.40 23 3 4 -12.60 5.20 -23 3 -4 5.90 6.00 23 -3 -4 -14.80 6.20 -23 -3 4 -7.70 5.40 23 -3 4 12.90 7.30 23 -3 4 -4.90 6.10 -23 -3 -4 0.30 6.20 23 3 -4 4.10 6.50 -23 3 4 -3.10 6.00 23 3 -4 5.20 6.40 23 -4 -4 44.20 9.50 23 4 4 35.00 9.20 -23 -4 4 50.49 8.30 -23 4 -4 58.39 9.00 -23 -4 -4 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-10 53.79 4.00 8 3 -10 52.69 6.10 -8 3 10 54.39 6.00 8 -3 10 34.70 5.30 -8 -3 -10 47.70 5.60 8 -3 10 48.40 3.60 8 -3 10 42.10 3.40 -8 3 10 43.80 3.90 8 -4 -10 8.80 3.60 8 4 10 12.60 3.80 8 4 10 9.10 2.00 -8 -4 10 12.90 4.00 -8 4 -10 10.30 3.60 -8 -4 10 8.00 3.40 -8 -4 -10 11.50 1.90 -8 -4 -10 10.10 3.80 -8 4 10 8.40 2.00 -8 4 10 10.00 1.90 8 4 -10 14.50 4.30 -8 4 10 13.00 3.70 8 -4 10 7.50 3.80 -8 -5 10 139.09 10.20 8 -5 -10 109.29 9.20 8 5 10 104.29 9.70 -8 5 -10 111.19 10.00 -8 5 10 126.19 7.30 -8 -5 -10 118.39 9.80 8 -5 10 124.69 10.50 -8 5 10 114.89 9.40 -8 5 10 122.69 7.10 8 5 -10 143.89 10.30 8 6 10 8.60 4.20 8 -6 -10 7.40 3.90 -8 -6 10 13.70 4.80 -8 6 -10 7.50 3.90 8 6 -10 14.50 4.70 8 -6 10 8.70 4.50 8 6 -10 8.40 3.50 -8 6 10 8.20 4.00 -8 -6 -10 7.60 3.60 -8 -7 10 321.87 21.30 8 -7 -10 319.37 20.60 -8 7 -10 333.57 21.40 8 7 10 340.57 21.90 8 7 -10 352.06 20.80 -8 -7 -10 347.27 20.90 -8 7 10 299.67 20.70 8 -7 10 332.67 21.70 8 7 -10 336.67 21.40 8 -8 -10 31.40 5.50 -8 -8 10 17.90 7.00 8 8 10 26.20 7.60 -8 8 -10 31.90 6.30 8 8 -10 18.30 5.30 -8 -8 -10 35.00 6.10 8 -8 10 33.60 6.80 -8 8 10 32.10 5.90 8 8 -10 33.30 6.40 -8 -9 10 197.18 15.70 -8 9 -10 196.68 15.10 8 -9 -10 217.28 14.40 8 9 10 175.38 15.30 -8 9 10 181.98 14.50 8 9 -10 209.38 14.30 8 9 -10 173.68 14.60 8 -9 10 175.58 15.00 8 10 10 9.30 6.50 -8 10 -10 9.50 6.00 -8 -10 10 2.90 6.50 8 -10 -10 4.50 4.90 8 10 -10 4.20 5.50 -8 10 10 7.70 5.50 -8 -10 -10 11.20 5.40 8 -10 10 4.50 5.60 8 10 -10 2.50 5.90 -8 11 -10 308.27 22.90 8 -11 -10 346.37 21.70 8 11 10 283.67 22.90 8 11 -10 350.26 22.00 -8 -11 -10 288.47 21.30 -8 11 10 330.17 22.60 8 11 -10 326.67 22.20 8 12 10 -5.20 8.30 -8 -12 10 -23.50 7.20 -8 12 -10 9.30 8.90 8 -12 -10 -8.10 6.00 8 -12 10 5.20 7.60 -8 12 10 3.10 7.80 8 12 -10 14.50 7.50 8 12 -10 16.50 7.40 -8 -12 -10 15.10 6.50 9 0 10 2410.16 135.39 -9 0 -10 2468.15 135.69 9 0 10 2596.34 135.59 -9 0 10 2737.03 135.69 9 0 10 2652.63 136.29 -9 0 10 2440.36 136.09 9 0 -10 2468.75 136.59 -9 -1 10 78.59 6.50 9 -1 -10 72.99 6.10 9 -1 -10 79.09 7.00 9 1 10 81.59 6.50 9 1 10 89.19 7.20 -9 -1 10 79.99 7.20 -9 1 -10 76.19 6.50 9 -1 10 68.29 5.70 9 -1 10 65.69 5.60 -9 1 10 71.09 5.80 9 1 -10 78.49 7.10 -9 -1 -10 57.99 5.70 -9 -2 10 975.20 54.59 9 2 10 1014.70 54.69 9 -2 -10 1004.00 55.09 9 2 10 1001.00 53.89 -9 2 -10 917.81 54.49 9 -2 -10 902.41 53.59 -9 -2 10 1038.20 54.99 9 2 10 1054.49 54.79 9 -2 10 1022.00 53.49 -9 -2 -10 1018.30 53.69 -9 2 10 1027.60 53.59 9 -2 10 939.91 53.49 9 2 -10 995.20 55.39 -9 2 10 996.30 54.89 -9 3 -10 0.80 2.90 -9 -3 10 1.30 3.10 9 -3 -10 3.50 1.90 -9 -3 10 -3.30 2.70 9 -3 -10 -1.00 2.70 9 3 10 -0.80 2.00 -9 3 10 -0.90 2.80 9 -3 10 0.60 1.50 9 -3 10 -1.90 2.70 -9 -3 -10 -0.70 1.60 -9 -3 -10 -0.70 3.00 9 3 -10 2.10 3.00 9 -3 10 0.80 1.80 -9 3 10 -2.90 2.60 -9 -4 10 497.75 30.80 9 -4 -10 553.64 31.00 -9 -4 10 470.95 30.60 9 4 10 555.34 31.20 9 4 10 512.15 28.80 -9 4 -10 523.05 31.00 9 -4 10 520.05 31.30 9 -4 10 537.25 28.50 -9 -4 -10 530.95 28.80 9 -4 10 515.15 28.50 -9 4 10 578.64 31.10 -9 -4 -10 543.25 30.80 -9 4 10 566.54 28.80 -9 4 10 531.45 28.70 9 4 -10 533.35 31.40 9 -5 -10 10.00 3.90 9 5 10 6.80 4.10 -9 5 -10 12.30 4.00 -9 -5 10 10.70 4.00 9 5 -10 8.10 4.50 -9 5 10 12.80 4.00 -9 -5 -10 9.40 4.20 9 -5 10 10.30 4.50 -9 -6 10 424.06 25.90 9 6 10 401.96 26.10 -9 6 -10 448.36 26.10 9 -6 -10 421.26 25.40 -9 6 10 423.46 25.80 -9 -6 -10 430.26 25.40 9 6 -10 403.76 26.00 9 -6 10 419.86 26.20 9 6 -10 427.66 25.40 -9 -7 10 12.80 4.90 9 7 10 12.50 5.20 -9 7 -10 6.00 4.40 9 -7 -10 20.50 5.10 -9 7 10 17.90 5.10 9 7 -10 16.40 5.20 -9 -7 -10 14.20 4.30 9 -7 10 10.70 5.30 9 7 -10 21.50 4.90 -9 8 -10 133.29 12.90 9 8 10 138.49 13.10 9 -8 -10 155.08 12.20 -9 -8 10 166.78 13.00 -9 -8 -10 143.59 11.80 9 8 -10 158.78 12.70 9 -8 10 159.38 13.10 9 8 -10 168.58 12.80 9 -9 -10 0.20 4.60 9 9 10 -2.40 5.30 -9 -9 10 10.20 6.00 -9 9 -10 -2.20 5.20 -9 -9 -10 -2.20 4.50 -9 9 10 6.90 5.00 9 9 -10 3.50 5.00 9 -9 10 -1.90 5.50 9 9 -10 -0.30 5.00 -9 10 -10 52.09 9.30 -9 -10 10 68.79 9.50 9 -10 -10 64.99 8.70 9 10 10 70.39 11.10 9 10 -10 70.89 9.50 9 -10 10 72.09 10.00 -9 -10 -10 52.99 8.40 9 10 -10 85.99 9.70 -9 10 10 75.79 9.60 9 11 10 8.80 7.40 -9 -11 10 10.70 7.60 9 -11 -10 15.20 6.60 -9 11 -10 10.10 6.70 -9 11 10 3.40 6.20 -9 -11 -10 3.40 5.80 9 11 -10 -3.50 6.80 9 11 -10 7.00 6.90 -9 12 -10 1.90 7.40 -9 -12 10 0.90 8.50 9 -12 -10 0.40 6.70 9 12 10 10.70 9.50 9 -12 10 7.30 7.90 9 12 -10 10.40 7.50 -9 -12 -10 3.60 6.70 9 12 -10 -1.30 7.70 -9 12 10 3.10 6.30 -10 0 10 5.30 2.60 10 0 -10 -1.00 3.00 -10 0 10 -0.90 2.90 10 0 10 2.00 2.90 -10 0 -10 1.40 2.10 10 0 10 0.00 2.30 10 -1 -10 32.70 4.60 -10 -1 10 47.10 5.90 10 1 10 50.19 5.90 -10 1 -10 39.20 4.80 10 -1 -10 37.60 5.80 10 1 10 49.00 5.30 -10 -1 10 45.70 5.00 -10 1 10 44.10 4.40 10 1 -10 46.70 5.80 10 -1 10 42.80 4.50 10 -1 10 53.89 4.80 10 -1 10 49.60 6.00 -10 -1 -10 44.50 4.70 -10 1 10 36.20 5.40 10 2 10 3.00 3.00 10 2 10 2.20 2.40 -10 2 -10 5.00 3.20 10 -2 -10 6.50 2.40 10 2 10 3.00 2.80 10 -2 -10 4.50 3.00 -10 -2 10 5.40 3.30 -10 -2 10 4.10 3.10 -10 2 10 2.50 1.90 10 -2 10 0.70 3.20 10 -2 10 4.30 2.10 -10 -2 -10 2.10 2.20 10 2 -10 10.10 3.90 -10 2 10 4.20 3.20 10 3 10 6.90 2.40 -10 -3 10 3.90 3.40 10 -3 -10 1.80 3.20 -10 -3 10 3.20 3.10 10 3 10 7.80 3.40 10 -3 -10 10.30 2.30 -10 3 -10 9.40 3.40 -10 3 10 6.30 3.10 -10 -3 -10 -1.00 3.20 10 -3 10 7.80 2.10 -10 -3 -10 6.00 2.00 10 -3 10 4.10 3.30 10 -3 10 6.60 2.40 10 3 -10 7.80 3.40 -10 -4 10 11.50 4.20 10 4 10 11.90 2.10 10 4 10 14.00 4.40 -10 -4 10 16.70 4.30 -10 4 -10 9.00 3.40 10 -4 -10 10.80 3.80 10 -4 10 9.90 2.00 -10 4 10 13.30 1.90 10 -4 10 6.80 3.90 -10 4 10 14.70 1.80 10 4 -10 6.20 4.00 -10 -4 -10 8.70 4.10 10 -4 10 13.20 2.20 -10 4 10 19.20 4.20 -10 -4 -10 11.90 2.00 10 -5 -10 130.19 10.30 -10 -5 10 109.49 9.90 -10 -5 10 131.39 10.20 10 5 10 123.39 10.60 -10 5 -10 107.59 9.80 -10 5 10 134.59 10.10 10 -5 10 118.39 6.90 10 -5 10 138.39 10.90 -10 -5 -10 117.49 9.70 10 -5 10 116.99 6.90 10 5 -10 115.39 10.50 10 -6 -10 36.50 5.60 10 6 10 28.40 6.40 -10 -6 10 36.00 6.10 -10 6 -10 22.90 5.70 10 6 -10 38.70 6.10 -10 -6 -10 29.90 5.30 10 6 -10 40.20 6.60 10 -6 10 36.60 6.30 -10 6 10 29.80 5.60 10 7 10 234.18 17.10 -10 -7 10 253.17 16.90 -10 7 -10 247.28 16.70 10 -7 -10 249.78 16.40 -10 7 10 213.08 16.00 10 7 -10 231.58 16.70 10 7 -10 224.58 16.10 10 -7 10 244.68 17.20 -10 -7 -10 223.28 15.90 -10 -8 10 73.99 9.10 10 8 10 55.49 8.20 -10 8 -10 51.19 8.10 10 -8 -10 54.89 7.40 10 8 -10 70.49 8.40 10 -8 10 41.50 7.60 -10 -8 -10 48.80 7.10 10 8 -10 47.30 7.50 -10 8 10 46.50 7.70 -10 9 -10 303.17 20.70 10 -9 -10 288.97 21.40 10 9 10 294.57 21.40 -10 -9 10 285.07 21.10 10 9 -10 298.87 20.20 10 -9 10 311.47 20.90 -10 -9 -10 305.97 20.20 10 9 -10 317.07 20.90 -10 9 10 273.97 20.00 -10 10 -10 1.80 6.50 10 -10 -10 -4.80 4.80 10 10 10 -6.40 6.20 -10 -10 10 -4.70 6.50 -10 -10 -10 2.40 5.50 10 10 -10 3.70 6.00 -10 10 10 -9.70 6.00 10 10 -10 1.00 6.70 10 -10 10 3.50 6.60 10 -11 -10 195.18 15.40 -10 11 -10 194.28 17.00 -10 11 10 175.78 15.40 -10 -11 -10 180.38 15.50 10 11 -10 172.78 16.60 10 -12 -10 13.10 7.40 10 12 10 6.90 9.60 -10 12 -10 1.20 7.80 -10 -12 10 4.80 8.60 10 12 -10 -6.20 8.30 10 -12 10 1.20 8.20 -10 -12 -10 15.80 7.50 10 12 -10 20.40 13.50 -10 12 10 17.50 8.20 -11 0 10 323.57 17.60 11 0 -10 298.47 18.70 11 0 10 303.17 18.20 11 0 10 297.57 17.60 -11 0 -10 245.48 17.30 -11 0 10 284.07 18.20 11 1 10 29.50 4.90 11 1 10 27.80 4.30 -11 1 -10 23.80 4.30 -11 -1 10 29.50 4.80 11 -1 -10 25.30 5.00 -11 -1 10 19.70 3.90 -11 1 10 22.60 4.30 11 1 -10 25.10 5.00 -11 1 10 31.70 3.80 -11 -1 -10 21.30 3.60 11 -1 10 19.80 3.60 11 -1 10 30.50 5.10 -11 -2 10 246.18 16.00 11 -2 -10 210.18 14.20 11 2 10 236.18 15.60 11 -2 -10 239.18 16.00 -11 2 -10 267.77 15.80 11 2 10 230.58 14.60 11 2 -10 254.87 16.60 11 -2 10 239.88 15.90 11 -2 10 244.28 14.30 -11 2 10 246.08 14.10 -11 2 10 253.27 16.00 11 -2 10 242.78 14.50 -11 -2 -10 234.08 14.30 11 -3 -10 -1.90 2.00 -11 -3 10 4.30 4.10 -11 3 -10 3.40 3.20 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10.00 11 7 -10 93.99 10.10 -11 -8 10 65.19 8.80 11 8 10 42.10 8.40 -11 8 -10 49.70 7.80 11 8 -10 69.99 8.80 -11 8 10 71.69 8.90 -11 -8 -10 56.49 7.70 11 8 -10 59.79 8.40 11 -8 10 61.79 8.40 -11 9 -10 6.80 5.70 11 9 10 8.00 6.80 11 -9 -10 11.50 5.80 -11 -9 10 19.20 6.90 -11 9 10 11.10 5.70 11 -9 10 8.10 6.20 11 9 -10 13.70 6.60 -11 -9 -10 1.30 5.00 11 9 -10 15.20 6.10 11 -10 -10 10.10 6.20 -11 10 -10 7.50 6.70 -11 -10 10 8.30 6.80 11 10 10 5.40 6.50 11 10 -10 11.80 6.60 11 10 -10 13.00 6.80 -11 10 10 6.50 6.70 11 -10 10 1.90 6.60 -11 -10 -10 -0.40 5.90 11 -11 -10 3.00 6.50 -11 11 -10 9.90 7.80 11 11 10 14.50 8.30 -11 -11 10 16.80 8.20 11 -11 10 -0.90 11.20 -11 11 10 -4.80 7.30 -11 -11 -10 1.40 6.70 11 11 -10 3.40 8.20 11 -12 -10 4.20 7.50 -11 12 -10 8.00 12.60 -11 -12 -10 -12.60 6.60 11 12 -10 16.10 9.30 -11 12 10 5.90 6.80 12 0 -10 4.30 3.50 12 0 10 10.60 3.40 12 0 10 9.80 3.60 -12 0 10 9.10 3.10 -12 0 -10 7.70 3.10 -12 0 10 10.80 4.10 12 1 10 234.38 14.30 12 1 10 186.38 13.10 12 -1 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6.50 -14 -5 10 41.80 7.00 14 5 10 48.00 7.80 -14 -5 10 44.00 6.60 14 -5 -10 35.60 7.70 14 -5 10 36.00 7.10 14 -5 10 39.50 4.40 14 5 -10 33.50 7.30 14 -5 10 31.10 7.00 -14 5 10 46.70 10.40 -14 6 -10 0.70 4.20 14 -6 -10 11.20 5.60 -14 -6 10 -3.50 4.10 14 6 10 11.60 6.30 -14 -6 -10 -5.80 4.10 14 6 -10 9.50 5.90 14 -6 10 0.80 5.10 -14 6 10 8.50 5.00 14 6 -10 5.20 4.90 14 -6 10 5.20 2.60 14 -7 -10 80.39 9.80 14 7 10 69.09 9.90 -14 -7 10 62.89 8.80 -14 7 -10 58.99 8.50 14 7 -10 85.89 10.30 14 -7 10 68.99 6.30 -14 -7 -10 65.29 9.10 14 7 -10 72.59 9.00 -14 7 10 68.09 8.80 14 -7 10 71.09 9.10 14 8 10 9.50 6.70 -14 8 -10 4.50 5.60 14 -8 -10 6.30 5.80 -14 -8 10 3.10 5.70 -14 8 10 1.30 5.70 14 8 -10 3.70 6.60 14 -8 10 20.20 6.50 14 8 -10 15.70 7.00 -14 -8 -10 14.70 6.30 14 9 10 175.88 17.00 14 -9 -10 196.68 16.00 -14 9 -10 184.18 15.70 -14 -9 10 175.88 16.40 -14 -9 -10 223.38 16.20 14 -9 10 167.08 16.30 -14 9 10 159.08 15.70 14 9 -10 199.88 16.10 14 9 -10 201.08 16.80 -14 10 -10 12.00 7.70 14 -10 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206.88 16.50 15 -8 10 204.68 16.60 15 8 -10 159.68 15.90 15 8 -10 212.58 17.10 -15 -8 -10 170.88 15.50 -15 8 10 179.28 15.30 15 -9 -10 20.20 7.50 -15 -9 10 22.20 8.90 15 9 -10 7.20 7.00 15 9 -10 12.10 8.20 -15 -9 -10 8.30 6.80 15 -9 10 13.40 7.80 -15 9 10 9.20 6.50 15 -10 -10 32.20 8.90 15 10 10 35.60 10.70 -15 -10 10 29.80 9.10 -15 10 -10 9.80 8.50 -15 -10 -10 26.70 8.50 -15 10 10 32.60 8.20 15 10 -10 22.00 10.10 15 10 -10 24.90 9.40 16 0 10 72.69 8.00 -16 0 10 70.89 8.90 16 0 -10 75.89 9.50 16 0 10 86.09 8.50 -16 0 10 64.49 6.90 -16 0 -10 72.59 7.40 -16 1 -10 1.00 3.60 -16 -1 10 -3.80 4.40 16 -1 -10 1.20 4.60 16 1 10 1.20 4.10 -16 -1 10 0.40 3.60 16 1 10 3.80 4.10 16 -1 10 1.60 3.80 -16 1 10 4.00 4.70 16 1 -10 -5.50 4.50 -16 1 10 3.90 3.30 16 -1 10 4.80 4.60 16 2 10 40.40 6.70 16 -2 -10 25.10 5.50 16 2 10 48.30 5.50 -16 -2 10 22.30 6.40 -16 2 -10 35.20 6.00 16 2 10 40.50 6.80 16 -2 -10 51.29 7.80 -16 -2 10 35.80 5.70 16 -2 10 41.70 6.90 16 2 -10 28.90 6.60 -16 2 10 46.50 4.70 16 -2 10 36.50 5.50 -16 2 10 38.10 6.60 -16 -3 10 90.59 10.10 16 3 10 82.49 7.30 -16 3 -10 111.19 9.70 16 -3 -10 86.19 11.00 16 3 10 91.39 9.10 -16 -3 10 90.39 9.20 16 -3 10 83.39 7.90 -16 3 10 83.59 7.40 -16 -3 -10 74.89 10.00 16 3 -10 77.29 9.80 16 -3 10 84.89 9.70 -16 3 10 79.99 10.70 16 4 10 3.00 4.30 16 -4 -10 5.40 4.10 16 4 10 3.40 2.70 -16 -4 10 2.90 4.70 -16 -4 10 8.60 5.80 -16 4 -10 -2.20 4.20 16 -4 10 -2.90 5.20 16 4 -10 9.80 6.00 16 -4 10 0.60 3.50 -16 -4 -10 -3.50 4.50 -16 4 10 -8.60 3.90 16 5 10 212.58 16.30 16 -5 -10 200.18 15.50 -16 5 -10 185.48 14.60 -16 -5 10 190.98 14.50 -16 -5 -10 197.58 15.10 16 -5 10 183.98 12.50 16 -5 10 181.58 15.10 16 5 -10 192.58 15.70 -16 5 10 181.38 15.20 -16 6 -10 -2.60 5.00 16 6 10 -3.40 6.30 16 -6 -10 2.10 5.80 -16 -6 10 -4.20 5.20 16 6 -10 4.50 6.40 16 -6 10 5.80 6.10 16 -6 10 -1.40 3.30 -16 -6 -10 9.20 5.50 -16 6 10 3.40 5.10 16 6 -10 3.40 6.10 -16 -7 10 80.89 10.70 -16 7 -10 102.09 11.30 16 7 10 60.59 10.40 16 -7 -10 87.39 10.60 -16 -7 -10 79.09 10.10 16 7 -10 75.99 10.40 -16 7 10 76.19 9.70 16 7 -10 76.69 10.50 16 -7 10 72.49 9.90 -16 8 -10 -10.70 6.00 16 -8 -10 -11.00 6.00 16 8 10 -2.20 6.70 -16 -8 10 1.80 5.60 -16 8 10 5.70 6.80 -16 -8 -10 -8.40 5.40 16 8 -10 5.00 7.00 16 -8 10 9.30 7.20 16 8 -10 -12.60 6.80 16 9 10 123.49 15.20 -16 -9 10 141.09 14.10 -16 9 -10 148.79 14.80 16 -9 10 125.59 13.50 -16 -9 -10 124.89 13.20 16 9 -10 156.08 14.80 16 -10 -10 -2.90 7.50 -16 -10 -10 0.90 12.20 -16 10 10 -20.40 7.00 16 10 -10 -2.60 9.20 17 0 10 13.80 5.00 -17 0 -10 13.00 4.80 17 0 -10 17.70 6.20 -17 0 10 33.20 7.90 -17 0 10 12.50 4.20 17 0 10 19.60 6.00 17 1 10 20.80 5.30 17 1 10 15.10 4.40 -17 -1 10 12.40 4.50 17 1 10 22.20 6.20 -17 -1 10 23.20 6.90 -17 1 -10 18.00 5.00 -17 1 10 18.10 3.70 -17 1 10 13.80 5.50 17 -1 10 16.60 5.80 17 -1 10 13.10 4.50 17 1 -10 12.20 5.10 17 -2 -10 236.68 17.50 -17 -2 10 204.48 17.10 17 2 10 236.48 15.30 17 2 10 220.48 16.80 -17 -2 10 230.88 15.80 -17 2 -10 238.68 16.40 17 -2 10 244.48 15.70 17 2 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3.40 3.90 -6 -5 -14 2.80 2.40 -6 6 -14 180.48 13.80 6 6 14 166.28 11.10 -6 -6 14 182.58 14.00 6 6 14 156.48 13.10 6 -6 -14 184.18 12.60 6 6 14 175.88 12.90 6 -6 14 193.68 14.70 -6 6 14 156.38 11.00 -6 6 14 142.49 12.60 6 6 -14 174.08 14.30 -6 -6 -14 172.48 10.50 6 6 -14 176.48 11.80 6 -7 -14 0.60 3.90 -6 7 -14 8.00 5.30 6 7 14 3.60 4.10 -6 -7 14 16.40 6.30 -6 -7 -14 1.20 1.90 -6 -7 -14 8.90 2.40 6 7 -14 5.00 5.20 -6 7 14 4.80 4.60 6 7 -14 8.10 3.70 6 -7 14 -1.70 5.00 -6 7 14 4.30 3.00 -6 -8 14 72.79 9.70 6 8 14 77.59 8.70 6 -8 -14 79.89 8.50 -6 8 -14 69.59 9.70 6 8 14 71.39 10.00 6 8 -14 76.19 7.60 6 8 -14 53.29 10.50 -6 8 14 61.29 6.40 -6 8 14 73.79 8.90 6 9 14 39.00 9.00 6 -9 -14 41.30 7.10 -6 9 -14 49.30 8.70 6 9 14 48.80 7.90 -6 -9 14 58.19 9.30 6 9 -14 52.19 9.40 6 -9 14 63.69 9.90 6 9 -14 49.80 6.30 -6 9 14 45.00 7.70 -6 -10 14 90.79 12.20 -6 10 -14 89.99 11.80 6 -10 -14 101.49 10.40 6 10 14 88.89 11.80 6 -10 14 78.69 12.00 6 10 -14 88.59 11.50 -6 10 14 114.49 12.20 6 -11 -14 19.70 6.90 -6 11 -14 15.40 8.10 6 11 14 18.70 9.00 -6 -11 14 5.20 8.30 6 -11 14 15.20 9.00 -6 11 14 9.90 7.60 6 11 -14 13.00 8.10 6 12 14 26.20 8.50 -6 12 -14 -2.40 13.30 6 -12 -14 12.90 10.50 6 12 -14 -9.40 8.90 7 0 14 156.28 11.80 7 0 14 171.28 10.80 -7 0 14 136.29 11.30 7 0 -14 165.18 12.30 -7 0 14 184.68 11.80 7 1 14 258.07 16.60 7 -1 -14 238.28 16.60 -7 -1 14 262.87 16.40 -7 -1 14 247.98 16.00 -7 1 -14 262.27 16.30 7 1 14 248.08 15.60 7 -1 14 280.27 17.10 7 -1 14 224.08 14.60 7 1 -14 244.98 16.80 -7 1 14 257.17 16.20 -7 1 14 266.97 15.90 7 -1 14 242.18 14.60 -7 -1 -14 239.08 15.50 -7 2 -14 27.10 4.90 7 2 14 32.90 5.20 -7 -2 14 33.80 5.60 7 2 14 41.90 6.00 7 -2 -14 33.80 5.90 -7 -2 14 44.60 5.60 7 -2 14 29.30 5.90 7 2 -14 42.80 6.70 7 -2 14 30.00 3.20 -7 2 14 26.20 4.90 -7 2 14 37.80 4.80 7 -2 14 29.60 3.10 -7 -2 -14 37.10 4.60 -7 -3 14 23.70 4.70 -7 -3 14 35.00 5.30 7 3 14 23.50 4.90 7 3 14 25.60 4.90 7 -3 -14 20.80 4.60 -7 3 -14 10.80 4.60 7 -3 14 20.00 5.20 7 3 -14 24.30 5.80 -7 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7 -15 8.80 5.00 9 -7 15 1.80 6.70 -9 7 15 9.40 5.30 9 7 -15 2.90 5.00 9 7 -15 8.40 5.80 9 8 15 8.90 6.50 -9 -8 15 6.90 6.80 -9 8 -15 4.50 6.70 9 8 15 17.40 6.80 9 -8 -15 12.80 6.20 9 8 -15 14.80 7.30 -9 8 15 12.70 6.10 9 -8 15 22.70 8.20 9 8 -15 13.40 5.70 9 9 15 -1.70 5.90 -9 9 -15 -1.00 6.80 9 9 15 -13.20 7.40 -9 -9 15 10.40 6.50 9 -9 -15 5.80 5.80 9 9 -15 -3.90 7.40 9 -9 15 3.90 7.60 -9 9 15 7.50 6.50 9 9 -15 7.20 6.00 9 10 15 61.29 11.40 -9 10 -15 65.29 10.30 -9 -10 15 69.19 10.90 9 -10 -15 56.49 8.90 9 10 15 65.89 10.30 -9 10 15 57.39 10.20 9 10 -15 65.19 11.50 9 -10 15 63.49 11.50 9 11 15 10.30 8.50 9 -11 -15 -12.30 7.10 9 11 -15 9.60 9.30 9 -11 15 -8.60 9.70 10 0 15 0.20 4.50 10 0 -15 -1.20 3.90 -10 0 15 4.30 4.00 10 0 15 3.00 3.10 -10 0 15 3.50 4.30 -10 0 -15 -0.70 3.40 -10 -1 15 15.20 4.60 -10 -1 15 5.90 4.20 10 1 15 8.00 4.40 10 1 15 10.60 4.40 10 -1 -15 12.90 5.30 -10 1 -15 9.00 4.10 -10 -1 -15 0.70 3.20 10 -1 15 3.80 4.20 10 -1 15 10.70 3.10 -10 1 15 14.80 4.80 10 1 -15 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-25 164.08 15.70 -2 5 25 159.18 14.70 -2 5 25 133.69 14.50 -2 -5 -25 92.99 12.60 -3 0 25 -6.00 7.50 -3 0 25 -6.30 6.00 3 0 25 11.20 8.90 -3 0 -25 -5.90 7.30 3 0 -25 6.10 12.00 -3 1 -25 14.20 8.00 3 1 25 -7.80 8.70 -3 -1 25 7.40 8.20 3 -1 -25 6.10 8.10 3 -1 25 12.80 8.90 -3 1 25 10.20 7.90 -3 1 25 12.70 6.60 3 1 -25 13.00 10.30 -3 -1 -25 -6.80 7.20 -3 -2 25 -0.30 13.80 3 -2 -25 1.10 7.60 3 2 25 7.30 6.50 3 -2 25 -10.70 8.30 3 2 -25 7.80 8.80 -3 2 25 8.70 7.70 -3 -2 -25 3.50 7.30 -3 2 25 2.50 6.60 3 3 25 12.70 6.60 -3 3 -25 13.40 8.40 3 -3 -25 11.70 8.40 -3 -3 25 10.10 8.60 3 -3 25 11.50 8.50 -3 3 25 2.60 7.10 3 3 -25 -4.90 8.70 -3 -3 -25 3.80 7.40 -3 3 25 2.50 7.60 -3 -4 25 5.60 9.50 -3 4 -25 2.30 9.60 3 4 25 21.30 8.90 3 4 25 8.80 7.70 3 -4 -25 1.00 8.20 3 -4 25 0.90 10.40 -3 4 25 21.30 8.40 -3 -4 -25 10.90 8.00 3 4 -25 7.70 9.30 -3 4 25 10.40 7.50 3 5 25 2.40 8.50 3 5 25 6.60 8.70 3 -5 -25 2.00 8.90 -3 5 25 0.50 8.50 -3 5 25 21.40 8.20 -3 -5 -25 1.50 8.10 4 0 -25 0.50 9.40 -4 0 -25 -2.80 7.30 4 0 25 9.40 8.80 -4 0 25 -5.20 7.40 -4 -1 25 66.59 11.40 4 1 25 79.59 12.70 -4 1 -25 87.09 11.90 -4 1 25 78.69 9.80 4 -1 25 91.99 12.80 -4 -1 -25 63.09 10.50 4 1 -25 65.69 11.40 -4 1 25 80.49 11.20 4 -2 -25 1.80 8.70 4 2 25 7.40 6.50 4 2 25 -4.20 8.20 -4 -2 25 2.00 8.10 -4 -2 -25 5.40 7.20 4 -2 25 13.70 9.40 4 2 -25 -10.60 8.50 -4 2 25 -2.00 7.60 -4 2 25 -8.40 6.70 4 -3 -25 57.59 11.90 4 3 25 26.70 8.20 -4 3 -25 40.50 9.80 -4 -3 25 49.10 10.60 4 3 25 33.90 9.80 -4 3 25 32.10 8.30 -4 3 25 53.09 9.60 4 -3 25 39.50 10.10 -4 -3 -25 38.80 8.70 4 3 -25 39.70 10.30 -4 -4 25 8.70 9.40 4 4 25 17.20 7.80 4 4 25 8.60 8.60 -4 4 -25 -0.40 7.50 -4 4 25 9.50 7.10 -4 -4 -25 7.40 8.00 -4 4 25 -4.00 7.80 5 0 25 1.10 8.30 -5 0 25 1.70 6.70 5 0 -25 -11.40 8.00 -5 0 -25 7.60 7.60 -5 0 25 6.90 7.80 -5 1 -25 0.20 7.20 -5 -1 25 -4.90 7.20 -5 -1 25 -7.80 7.70 5 1 25 4.00 8.50 5 -1 -25 -9.00 8.10 -5 1 25 -3.90 6.10 -5 -1 -25 6.20 7.40 5 1 -25 -5.00 8.80 -5 1 25 15.60 7.40 5 -1 25 -8.00 8.20 5 2 25 2.80 8.70 -5 -2 25 -4.20 9.30 -5 2 -25 -1.70 8.60 5 -2 -25 0.70 8.10 5 2 25 7.20 6.50 5 -2 25 8.20 9.20 -5 2 25 4.60 7.70 -5 -2 -25 8.40 7.40 5 2 -25 3.90 9.40 -5 2 25 -1.90 7.10 -5 -3 25 -1.60 8.60 5 3 25 -4.80 7.00 -5 3 -25 18.60 9.20 5 3 25 1.40 7.30 5 -3 -25 0.30 9.20 5 3 -25 -4.40 8.80 5 -3 25 -7.20 8.70 -5 -3 -25 2.90 7.60 -5 3 25 12.70 8.00 -5 3 25 -5.20 7.00 5 -4 -25 2.50 8.40 5 4 25 -4.10 7.50 -5 -4 25 2.90 9.20 -5 4 -25 13.70 9.40 5 4 25 3.90 7.70 -5 -4 -25 -4.30 7.00 -5 4 25 11.90 8.10 -6 0 25 18.20 7.80 -6 0 25 -10.70 7.10 6 0 25 -8.20 7.10 6 0 -25 -20.80 8.50 -6 0 -25 15.70 7.70 6 -1 -25 2.30 8.60 -6 -1 25 -4.60 8.00 -6 -1 25 2.40 7.10 -6 1 -25 0.60 7.90 6 1 25 6.20 8.90 6 -1 25 -1.40 7.90 -6 1 25 16.20 7.50 -6 -1 -25 4.90 7.20 -6 1 25 5.60 7.40 6 1 -25 3.10 7.90 -6 -2 25 2.10 8.10 6 2 25 -0.70 8.80 6 -2 -25 7.40 8.70 -6 2 -25 11.10 8.20 6 2 -25 2.50 9.10 -6 -2 -25 16.40 7.40 -6 2 25 6.70 7.60 -6 2 25 7.50 7.80 6 -2 25 -8.90 7.20 6 3 25 10.50 7.50 -6 3 -25 31.30 9.80 6 3 25 5.80 8.30 6 -3 -25 4.30 8.60 -6 -3 25 -4.30 8.40 6 3 -25 10.00 15.90 -6 -3 -25 -0.40 7.50 -6 3 25 19.60 7.90 -6 3 25 12.70 8.60 -6 4 -25 -18.90 10.70 6 4 25 8.50 8.70 6 -4 -25 -15.60 8.10 6 4 25 -0.90 7.50 -6 -4 25 -6.80 9.50 -6 4 25 5.00 8.30 -6 4 25 -10.50 7.60 -6 -4 -25 16.20 7.80 -7 0 25 -0.70 7.10 -7 0 25 -5.50 7.50 7 0 -25 0.70 9.50 7 0 25 -1.20 8.60 -7 0 -25 -4.10 7.00 -7 1 -25 -0.90 7.80 -7 -1 25 -6.60 7.90 7 1 25 -12.00 7.40 7 -1 -25 0.80 7.90 -7 -1 25 -5.90 7.10 7 1 -25 -1.20 8.30 -7 1 25 6.10 7.70 7 -1 25 -11.70 8.60 -7 -1 -25 3.50 7.70 -7 1 25 -5.80 6.90 -7 -2 25 7.70 8.60 7 2 25 9.80 7.80 7 -2 -25 7.10 9.00 -7 2 -25 -8.00 7.70 -7 2 25 -2.00 7.20 -7 -2 -25 5.50 7.80 7 2 -25 1.40 10.80 7 -2 25 14.30 15.50 -7 2 25 9.30 8.00 7 -3 -25 7.70 8.50 7 3 25 4.00 7.80 7 3 25 -5.60 8.70 -7 -3 25 -4.80 7.70 -7 3 -25 4.50 8.90 -7 3 25 9.00 7.60 -7 3 25 4.30 8.60 -7 -3 -25 -4.10 7.40 8 0 -25 -11.50 9.30 -8 0 -25 3.30 7.20 -8 0 25 1.20 7.60 8 0 25 16.30 13.80 -8 0 25 -9.50 7.50 -8 -1 25 32.00 8.60 8 -1 -25 21.00 10.80 8 1 25 62.79 13.10 -8 1 25 67.49 10.50 8 1 -25 66.29 18.40 -8 1 25 30.20 8.70 -8 -1 -25 54.79 9.50 8 -2 -25 17.50 9.60 8 2 25 12.90 14.60 -8 2 -25 21.80 8.40 -8 -2 25 18.50 9.30 -8 2 25 11.50 7.80 -8 -2 -25 13.00 7.30 -8 2 25 -0.30 7.70 -8 -3 25 99.59 13.70 -8 3 -25 101.29 13.30 8 -3 -25 116.09 14.10 -8 3 25 106.99 12.50 -8 -3 -25 109.19 12.00 -8 3 25 91.19 12.40 -9 0 25 -1.30 8.00 -9 0 25 -6.20 7.30 -9 0 -25 3.40 7.60 -9 1 -25 -7.80 14.40 -9 -1 25 23.30 8.30 -9 -1 -25 -6.20 7.40 -9 1 25 3.40 7.50 -9 1 25 -0.20 7.80 -9 -2 25 1.80 8.90 -9 2 -25 7.20 8.30 -9 -2 -25 25.90 8.00 -9 2 25 17.50 8.30 0 0 -26 -11.50 7.50 0 0 26 6.90 7.30 0 -1 26 -10.80 6.90 0 1 -26 4.70 8.30 0 1 26 6.90 9.00 0 2 26 96.89 13.00 0 2 -26 111.39 14.00 0 2 26 91.59 10.80 0 -2 -26 75.79 13.10 0 -2 26 99.89 14.20 0 3 26 -3.30 8.10 0 -3 -26 -6.20 8.30 0 3 26 7.30 7.30 -1 0 -26 35.30 10.10 1 0 26 47.20 10.60 -1 0 26 32.10 9.60 1 0 -26 53.89 11.00 1 1 26 2.20 8.40 -1 1 -26 1.20 8.50 1 -1 -26 1.20 8.40 -1 -1 26 4.90 7.90 -1 1 26 16.90 9.20 1 -1 26 -11.00 8.80 -1 1 26 3.20 7.40 1 1 -26 -14.50 8.00 -1 -1 -26 -1.90 12.80 1 2 26 6.80 8.50 -1 2 -26 24.20 8.60 -1 -2 26 14.10 9.30 1 2 26 7.60 7.10 -1 2 26 5.20 14.30 -1 -2 -26 4.00 7.90 1 -2 26 4.90 9.40 -1 2 26 14.30 7.60 1 2 -26 15.70 9.10 -1 3 -26 29.00 15.40 1 3 26 7.00 7.00 -1 -3 26 -3.20 14.20 1 3 26 7.00 8.80 -1 -3 -26 17.80 8.50 -1 3 26 13.60 7.90 2 0 26 9.60 9.20 -2 0 26 12.80 9.40 -2 0 -26 1.30 14.00 2 0 -26 13.90 9.20 -2 1 -26 2.40 8.50 -2 -1 26 -7.30 8.40 2 1 26 -4.70 7.90 2 -1 -26 -9.60 7.90 -2 -1 -26 -8.00 7.30 -2 1 26 2.70 7.00 2 1 -26 9.20 9.10 2 -1 26 -1.60 8.40 -2 -2 26 52.59 11.20 2 2 26 41.10 8.60 2 -2 -26 66.49 11.70 2 2 26 46.80 10.30 -2 2 -26 37.80 10.60 2 2 -26 50.29 11.20 -2 -2 -26 42.90 9.80 -2 2 26 33.50 8.50 2 -2 26 58.69 12.20 2 3 26 20.80 9.50 2 3 26 20.60 7.70 -2 3 -26 47.90 17.20 2 -3 -26 19.70 10.60 -2 -3 26 11.70 14.80 -2 3 26 36.60 14.30 -2 -3 -26 33.90 9.40 -2 3 26 22.30 8.30 3 0 -26 126.59 15.10 -3 0 26 119.49 14.10 3 0 26 101.09 14.20 3 -1 -26 -5.20 8.70 -3 -1 26 5.00 8.90 -3 1 -26 2.10 8.30 3 1 26 5.90 8.20 -3 1 26 6.60 7.00 3 1 -26 4.80 9.20 -3 -1 -26 -7.40 7.00 3 -1 26 -1.80 9.10 -3 2 -26 32.50 9.60 3 -2 -26 34.80 10.40 3 2 26 15.80 9.60 -3 -2 26 29.40 10.10 -3 -2 -26 33.30 9.30 -3 2 26 31.80 11.00 3 2 -26 20.60 11.10 -3 2 26 18.50 7.90 -3 -3 26 9.10 14.80 3 3 26 12.60 7.60 3 -3 -26 11.40 8.80 3 3 26 6.30 9.10 -3 3 26 15.30 9.00 -3 -3 -26 1.70 8.30 -3 3 26 -11.60 7.50 -4 0 26 4.70 8.20 4 0 26 11.00 8.40 4 0 -26 2.50 9.30 4 1 26 5.40 8.00 -4 -1 26 4.80 8.40 4 -1 -26 11.60 9.30 -4 1 -26 8.40 8.40 -4 1 26 1.90 6.50 4 1 -26 2.10 8.40 -4 -1 -26 -12.10 7.20 4 -1 26 4.90 10.60 4 -2 -26 -7.50 8.90 4 2 26 -2.90 8.70 -4 -2 26 -2.90 8.90 -4 2 -26 0.80 8.60 -4 -2 -26 2.70 7.70 -4 2 26 -1.70 7.90 -4 2 26 2.70 7.00 4 3 26 59.09 10.80 4 -3 -26 56.79 11.50 4 3 26 55.09 9.60 -4 3 26 41.20 9.30 -4 -3 -26 37.40 9.50 -4 3 26 33.80 9.70 -5 0 -26 2.30 13.30 -5 0 26 -7.10 7.90 5 0 26 0.70 9.10 5 0 -26 -10.60 8.90 5 1 26 4.50 9.30 -5 1 -26 6.60 8.20 -5 -1 26 18.50 9.00 5 -1 -26 -7.80 8.80 -5 -1 -26 7.30 7.90 5 1 -26 -8.00 14.50 -5 1 26 19.10 8.10 -5 2 -26 42.90 10.30 5 2 26 18.00 10.80 -5 -2 26 15.20 10.10 5 -2 -26 35.10 10.40 -5 -2 -26 33.70 9.30 -5 2 26 19.10 9.30 -5 2 26 23.20 7.90 -6 0 26 1.40 8.20 -6 0 26 6.40 8.40 -6 0 -26 16.90 15.60 -6 -1 26 -4.40 8.10 -6 1 -26 3.80 8.20 6 -1 -26 -4.90 9.30 -6 1 26 1.00 7.20 -6 1 26 17.60 13.50 -6 -1 -26 -1.70 7.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 99649 _shelx_res_file ; TITL ga610b5_a.res in Pbcn ga610b5.res created by SHELXL-2018/3 at 12:34:22 on 25-Mar-2024 REM Old TITL ga610b5 in Pbcn REM SHELXT solution in Pbcn: R1 0.108, Rweak 0.002, Alpha 0.029 REM 0.628 for 432 systematic absences, Orientation as input REM Formula found by SHELXT: C19 O3 Br CELL 0.71073 18.1223 9.984 18.2863 90 90 90 ZERR 4 0.0007 0.0004 0.0007 0 0 0 LATT 1 SYMM 0.5-X,0.5-Y,0.5+Z SYMM -X,+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H Br O UNIT 160 152 8 16 L.S. 8 PLAN 1 SIZE 0.35 0.25 0.22 TEMP -173.15 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.027500 1.755300 FVAR 0.24731 BR1 3 0.583749 0.730399 0.320236 11.00000 0.02093 0.00958 = 0.02800 -0.00016 -0.00372 0.00170 O1 4 0.638610 0.139246 0.357639 11.00000 0.01036 0.01026 = 0.01570 0.00121 -0.00237 0.00057 O2 4 0.401866 0.382592 0.374446 11.00000 0.01254 0.01016 = 0.01416 -0.00155 0.00320 0.00041 C1 1 0.570529 0.335737 0.390886 11.00000 0.00943 0.01457 = 0.01243 -0.00060 -0.00232 -0.00052 C2 1 0.559028 0.473138 0.382649 11.00000 0.01116 0.01399 = 0.01456 -0.00349 -0.00154 0.00033 H2 2 0.526417 0.520519 0.415049 11.00000 0.02151 C3 1 0.596362 0.542019 0.328163 11.00000 0.01330 0.00980 = 0.01853 -0.00121 -0.00519 -0.00078 C4 1 0.641153 0.476856 0.278303 11.00000 0.01285 0.01243 = 0.01358 0.00142 -0.00237 -0.00196 H4 2 0.660480 0.524400 0.237584 11.00000 0.01367 C5 1 0.653552 0.339565 0.285850 11.00000 0.00924 0.01267 = 0.01209 -0.00082 -0.00212 -0.00049 C6 1 0.621490 0.272656 0.344951 11.00000 0.00987 0.01042 = 0.01356 0.00016 -0.00273 -0.00053 C7 1 0.523647 0.253291 0.442876 11.00000 0.01191 0.01482 = 0.01245 0.00110 0.00043 0.00009 H7A 2 0.553880 0.187925 0.468668 11.00000 0.01118 H7B 2 0.499526 0.309699 0.480433 11.00000 0.01660 C8 1 0.465777 0.177193 0.399388 11.00000 0.01074 0.01397 = 0.01065 0.00075 0.00250 -0.00040 C9 1 0.472376 0.039884 0.386627 11.00000 0.01315 0.01457 = 0.01666 0.00297 0.00173 0.00230 H9 2 0.512474 -0.005855 0.408104 11.00000 0.01808 C10 1 0.423169 -0.026707 0.341151 11.00000 0.01661 0.01153 = 0.01885 0.00059 0.00410 0.00021 H10 2 0.430009 -0.115870 0.332452 11.00000 0.01907 C11 1 0.366868 0.043530 0.306594 11.00000 0.01362 0.01348 = 0.01517 -0.00040 0.00072 -0.00150 H11 2 0.335443 0.000630 0.272209 11.00000 0.01989 C12 1 0.358697 0.180985 0.317590 11.00000 0.01134 0.01286 = 0.01254 0.00150 0.00199 -0.00063 C13 1 0.407482 0.244483 0.365480 11.00000 0.01147 0.01115 = 0.01106 0.00071 0.00327 -0.00045 C14 1 0.695661 0.262697 0.227402 11.00000 0.00983 0.01432 = 0.01379 0.00040 -0.00021 0.00072 H14A 2 0.731649 0.204456 0.248096 11.00000 0.01907 C15 1 0.706949 0.128276 0.398578 11.00000 0.01153 0.01441 = 0.01571 0.00182 -0.00275 0.00031 H15A 2 0.702892 0.181106 0.444239 11.00000 0.01157 H15B 2 0.746678 0.165875 0.369895 11.00000 0.01441 C16 1 0.721143 -0.017885 0.415205 11.00000 0.01241 0.01368 = 0.01484 0.00304 0.00174 0.00276 H16A 2 0.715311 -0.067638 0.370557 11.00000 0.01533 H16B 2 0.773350 -0.027293 0.430760 11.00000 0.02178 C17 1 0.671336 -0.074766 0.474473 11.00000 0.01690 0.01976 = 0.01806 0.00654 0.00151 0.00170 H17A 2 0.681732 -0.169037 0.483687 11.00000 0.02728 H17B 2 0.679667 -0.026999 0.523171 11.00000 0.03744 H17C 2 0.618627 -0.063043 0.463374 11.00000 0.02681 C18 1 0.352821 0.423416 0.431697 11.00000 0.01652 0.01380 = 0.01408 -0.00191 0.00435 0.00044 H18A 2 0.372615 0.401560 0.480006 11.00000 0.01566 H18B 2 0.304415 0.378029 0.425741 11.00000 0.01594 C19 1 0.344026 0.568809 0.425387 11.00000 0.01506 0.01937 = 0.01560 -0.00229 0.00294 0.00063 C20 1 0.338379 0.686134 0.418285 11.00000 0.02677 0.01730 = 0.02395 -0.00124 0.00634 0.00140 H14B 2 0.722875 0.324219 0.194477 11.00000 -1.50000 H20 2 0.336505 0.775691 0.411447 11.00000 0.04090 HKLF 4 REM ga610b5_a.res in Pbcn REM wR2 = 0.0690, GooF = S = 1.036, Restrained GooF = 1.036 for all data REM R1 = 0.0298 for 4481 Fo > 4sig(Fo) and 0.0446 for all 5529 data REM 283 parameters refined using 0 restraints END WGHT 0.0275 1.7552 REM Highest difference peak 0.418, deepest hole -0.509, 1-sigma level 0.073 Q1 1 0.4658 0.1058 0.3938 11.00000 0.05 0.42 ; _shelx_res_checksum 4609 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Br Br1 0.58375(2) 0.73040(2) 0.32024(2) 0.01950(5) Uani d 1 . . O O1 0.63861(5) 0.13925(9) 0.35764(5) 0.01210(18) Uani d 1 . . O O2 0.40187(5) 0.38259(9) 0.37445(5) 0.01229(19) Uani d 1 . . C C1 0.57053(7) 0.33574(14) 0.39089(7) 0.0121(2) Uani d 1 . . C C2 0.55903(7) 0.47314(14) 0.38265(8) 0.0132(2) Uani d 1 . . H H2 0.5264(10) 0.5205(18) 0.4150(10) 0.022(5) Uiso d 1 . . C C3 0.59636(7) 0.54202(14) 0.32816(8) 0.0139(3) Uani d 1 . . C C4 0.64115(7) 0.47686(13) 0.27830(7) 0.0130(2) Uani d 1 . . H H4 0.6605(9) 0.5244(16) 0.2376(9) 0.014(4) Uiso d 1 . . C C5 0.65355(7) 0.33956(13) 0.28585(7) 0.0113(2) Uani d 1 . . C C6 0.62149(7) 0.27266(13) 0.34495(7) 0.0113(2) Uani d 1 . . C C7 0.52365(8) 0.25329(14) 0.44288(8) 0.0131(2) Uani d 1 . . H H7A 0.5539(10) 0.1879(17) 0.4687(9) 0.011(4) Uiso d 1 . . H H7B 0.4995(10) 0.3097(18) 0.4804(9) 0.017(4) Uiso d 1 . . C C8 0.46578(7) 0.17719(14) 0.39939(7) 0.0118(2) Uani d 1 . . C C9 0.47238(8) 0.03988(14) 0.38663(8) 0.0148(3) Uani d 1 . . H H9 0.5125(10) -0.0059(17) 0.4081(9) 0.018(4) Uiso d 1 . . C C10 0.42317(8) -0.02671(15) 0.34115(8) 0.0157(3) Uani d 1 . . H H10 0.4300(10) -0.116(2) 0.3325(10) 0.019(5) Uiso d 1 . . C C11 0.36687(8) 0.04353(14) 0.30659(8) 0.0141(3) Uani d 1 . . H H11 0.3354(10) 0.0006(18) 0.2722(10) 0.020(4) Uiso d 1 . . C C12 0.35870(7) 0.18099(14) 0.31759(7) 0.0122(2) Uani d 1 . . C C13 0.40748(7) 0.24448(13) 0.36548(7) 0.0112(2) Uani d 1 . . C C14 0.69566(7) 0.26270(14) 0.22740(8) 0.0126(2) Uani d 1 . . H H14A 0.7316(10) 0.2045(18) 0.2481(10) 0.019(5) Uiso d 1 . . C C15 0.70695(8) 0.12828(14) 0.39858(8) 0.0139(3) Uani d 1 . . H H15A 0.7029(9) 0.1811(17) 0.4442(9) 0.012(4) Uiso d 1 . . H H15B 0.7467(10) 0.1659(17) 0.3699(9) 0.014(4) Uiso d 1 . . C C16 0.72114(8) -0.01789(14) 0.41520(8) 0.0136(3) Uani d 1 . . H H16A 0.7153(9) -0.0676(17) 0.3706(10) 0.015(4) Uiso d 1 . . H H16B 0.7734(11) -0.0273(18) 0.4308(10) 0.022(5) Uiso d 1 . . C C17 0.67134(9) -0.07477(16) 0.47447(8) 0.0182(3) Uani d 1 . . H H17A 0.6817(11) -0.169(2) 0.4837(10) 0.027(5) Uiso d 1 . . H H17B 0.6797(12) -0.027(2) 0.5232(12) 0.037(6) Uiso d 1 . . H H17C 0.6186(11) -0.0630(19) 0.4634(10) 0.027(5) Uiso d 1 . . C C18 0.35282(8) 0.42342(14) 0.43170(8) 0.0148(3) Uani d 1 . . H H18A 0.3726(10) 0.4016(17) 0.4800(10) 0.016(4) Uiso d 1 . . H H18B 0.3044(10) 0.3780(17) 0.4257(9) 0.016(4) Uiso d 1 . . C C19 0.34403(8) 0.56881(15) 0.42539(8) 0.0167(3) Uani d 1 . . C C20 0.33838(9) 0.68613(16) 0.41828(9) 0.0227(3) Uani d 1 . . H H14B 0.7229(11) 0.324(2) 0.1945(11) 0.034 Uiso d 1 . . H H20 0.3365(13) 0.776(2) 0.4114(12) 0.041(6) Uiso d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Br1 0.02093(8) 0.00958(7) 0.02800(9) 0.00170(5) -0.00372(6) -0.00016(5) O1 0.0104(4) 0.0103(4) 0.0157(5) 0.0006(3) -0.0024(4) 0.0012(4) O2 0.0125(4) 0.0102(4) 0.0142(4) 0.0004(3) 0.0032(4) -0.0016(3) C1 0.0094(6) 0.0146(6) 0.0124(6) -0.0005(5) -0.0023(4) -0.0006(5) C2 0.0112(5) 0.0140(6) 0.0146(6) 0.0003(5) -0.0015(5) -0.0035(5) C3 0.0133(6) 0.0098(6) 0.0185(7) -0.0008(4) -0.0052(5) -0.0012(5) C4 0.0128(6) 0.0124(6) 0.0136(6) -0.0020(5) -0.0024(5) 0.0014(5) C5 0.0092(5) 0.0127(6) 0.0121(6) -0.0005(4) -0.0021(4) -0.0008(5) C6 0.0099(5) 0.0104(6) 0.0136(6) -0.0005(5) -0.0027(5) 0.0002(5) C7 0.0119(6) 0.0148(6) 0.0125(6) 0.0001(5) 0.0004(5) 0.0011(5) C8 0.0107(5) 0.0140(6) 0.0107(6) -0.0004(5) 0.0025(5) 0.0007(5) C9 0.0131(6) 0.0146(6) 0.0167(6) 0.0023(5) 0.0017(5) 0.0030(5) C10 0.0166(6) 0.0115(6) 0.0188(7) 0.0002(5) 0.0041(5) 0.0006(5) C11 0.0136(6) 0.0135(6) 0.0152(6) -0.0015(5) 0.0007(5) -0.0004(5) C12 0.0113(6) 0.0129(6) 0.0125(6) -0.0006(5) 0.0020(5) 0.0015(5) C13 0.0115(6) 0.0111(6) 0.0111(6) -0.0005(4) 0.0033(4) 0.0007(4) C14 0.0098(6) 0.0143(6) 0.0138(6) 0.0007(5) -0.0002(5) 0.0004(5) C15 0.0115(6) 0.0144(6) 0.0157(6) 0.0003(5) -0.0028(5) 0.0018(5) C16 0.0124(6) 0.0137(6) 0.0148(6) 0.0028(5) 0.0017(5) 0.0030(5) C17 0.0169(7) 0.0198(7) 0.0181(7) 0.0017(6) 0.0015(5) 0.0065(6) C18 0.0165(6) 0.0138(6) 0.0141(6) 0.0004(5) 0.0044(5) -0.0019(5) C19 0.0151(6) 0.0194(7) 0.0156(6) 0.0006(5) 0.0029(5) -0.0023(5) C20 0.0268(8) 0.0173(7) 0.0240(8) 0.0014(6) 0.0063(6) -0.0012(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag C6 O1 C15 . . 110.46(10) ? C13 O2 C18 . . 114.41(10) ? C2 C1 C6 . . 118.46(12) ? C2 C1 C7 . . 121.14(12) ? C6 C1 C7 . . 120.12(12) ? C1 C2 H2 . . 120.6(11) ? C3 C2 C1 . . 119.48(13) ? C3 C2 H2 . . 119.9(11) ? C2 C3 Br1 . . 119.14(10) ? C4 C3 Br1 . . 119.07(11) ? C4 C3 C2 . . 121.77(13) ? C3 C4 H4 . . 119.9(10) ? C3 C4 C5 . . 119.42(13) ? C5 C4 H4 . . 120.6(10) ? C4 C5 C6 . . 118.62(12) ? C4 C5 C14 . . 120.45(12) ? C6 C5 C14 . . 120.73(12) ? O1 C6 C1 . . 118.67(12) ? O1 C6 C5 . . 119.70(12) ? C5 C6 C1 . . 121.60(12) ? C1 C7 H7A . . 110.6(10) ? C1 C7 H7B . . 111.9(10) ? C1 C7 C8 . . 109.25(11) ? H7A C7 H7B . . 107.1(14) ? C8 C7 H7A . . 107.9(10) ? C8 C7 H7B . . 110.0(10) ? C9 C8 C7 . . 121.29(12) ? C9 C8 C13 . . 117.57(12) ? C13 C8 C7 . . 120.91(12) ? C8 C9 H9 . . 118.1(11) ? C10 C9 C8 . . 121.02(13) ? C10 C9 H9 . . 120.8(11) ? C9 C10 H10 . . 118.9(12) ? C9 C10 C11 . . 120.13(13) ? C11 C10 H10 . . 120.8(12) ? C10 C11 H11 . . 120.9(11) ? C10 C11 C12 . . 120.58(13) ? C12 C11 H11 . . 118.4(11) ? C11 C12 C13 . . 118.02(12) ? C11 C12 C14 . 3_655 121.23(12) ? C13 C12 C14 . 3_655 120.38(12) ? O2 C13 C8 . . 118.64(12) ? O2 C13 C12 . . 118.50(12) ? C12 C13 C8 . . 122.59(12) ? C5 C14 H14A . . 111.9(11) ? C5 C14 H14B . . 111.3(13) ? C12 C14 C5 3_655 . 109.01(11) ? C12 C14 H14A 3_655 . 109.3(11) ? C12 C14 H14B 3_655 . 109.0(12) ? H14A C14 H14B . . 106.2(16) ? O1 C15 H15A . . 109.4(10) ? O1 C15 H15B . . 109.1(10) ? O1 C15 C16 . . 108.76(11) ? H15A C15 H15B . . 107.8(14) ? C16 C15 H15A . . 110.9(10) ? C16 C15 H15B . . 110.9(10) ? C15 C16 H16A . . 108.0(10) ? C15 C16 H16B . . 108.1(10) ? C15 C16 C17 . . 113.74(12) ? H16A C16 H16B . . 107.4(14) ? C17 C16 H16A . . 110.3(10) ? C17 C16 H16B . . 109.0(10) ? C16 C17 H17A . . 111.7(11) ? C16 C17 H17B . . 111.1(12) ? C16 C17 H17C . . 112.6(11) ? H17A C17 H17B . . 105.8(16) ? H17A C17 H17C . . 109.8(16) ? H17B C17 H17C . . 105.5(16) ? O2 C18 H18A . . 111.7(10) ? O2 C18 H18B . . 109.8(10) ? O2 C18 C19 . . 106.97(11) ? H18A C18 H18B . . 108.7(14) ? C19 C18 H18A . . 109.4(10) ? C19 C18 H18B . . 110.3(10) ? C20 C19 C18 . . 177.81(16) ? C19 C20 H20 . . 176.8(15) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Br1 C3 . 1.9002(14) ? O1 C6 . 1.3872(16) ? O1 C15 . 1.4513(16) ? O2 C13 . 1.3923(15) ? O2 C18 . 1.4325(16) ? C1 C2 . 1.3957(19) ? C1 C6 . 1.3982(18) ? C1 C7 . 1.5176(19) ? C2 H2 . 0.961(18) ? C2 C3 . 1.387(2) ? C3 C4 . 1.3833(19) ? C4 H4 . 0.950(17) ? C4 C5 . 1.3959(18) ? C5 C6 . 1.3971(19) ? C5 C14 . 1.5211(19) ? C7 H7A . 0.974(17) ? C7 H7B . 0.990(18) ? C7 C8 . 1.5197(19) ? C8 C9 . 1.3957(19) ? C8 C13 . 1.3971(18) ? C9 H9 . 0.944(18) ? C9 C10 . 1.389(2) ? C10 H10 . 0.91(2) ? C10 C11 . 1.390(2) ? C11 H11 . 0.950(18) ? C11 C12 . 1.3949(19) ? C12 C13 . 1.3966(19) ? C12 C14 3_655 1.5209(19) ? C14 H14A . 0.952(18) ? C14 H14B . 0.99(2) ? C15 H15A . 0.990(17) ? C15 H15B . 0.967(17) ? C15 C16 . 1.5126(19) ? C16 H16A . 0.962(18) ? C16 H16B . 0.992(19) ? C16 C17 . 1.520(2) ? C17 H17A . 0.97(2) ? C17 H17B . 1.02(2) ? C17 H17C . 0.98(2) ? C18 H18A . 0.978(17) ? C18 H18B . 0.993(18) ? C18 C19 . 1.465(2) ? C19 C20 . 1.183(2) ? C20 H20 . 0.90(2) ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag Br1 C3 C4 C5 . . . . 176.93(10) ? O1 C15 C16 C17 . . . . -73.91(15) ? C1 C2 C3 Br1 . . . . -177.17(10) ? C1 C2 C3 C4 . . . . 4.4(2) ? C1 C7 C8 C9 . . . . 105.00(14) ? C1 C7 C8 C13 . . . . -69.41(16) ? C2 C1 C6 O1 . . . . 173.62(12) ? C2 C1 C6 C5 . . . . -8.25(19) ? C2 C1 C7 C8 . . . . 101.52(14) ? C2 C3 C4 C5 . . . . -4.7(2) ? C3 C4 C5 C6 . . . . -1.51(19) ? C3 C4 C5 C14 . . . . 173.39(12) ? C4 C5 C6 O1 . . . . -173.87(11) ? C4 C5 C6 C1 . . . . 8.02(19) ? C4 C5 C14 C12 . . . 3_655 -104.49(14) ? C6 O1 C15 C16 . . . . 176.59(11) ? C6 C1 C2 C3 . . . . 1.98(19) ? C6 C1 C7 C8 . . . . -72.24(15) ? C6 C5 C14 C12 . . . 3_655 70.31(16) ? C7 C1 C2 C3 . . . . -171.87(12) ? C7 C1 C6 O1 . . . . -12.46(18) ? C7 C1 C6 C5 . . . . 165.67(12) ? C7 C8 C9 C10 . . . . -173.85(13) ? C7 C8 C13 O2 . . . . -2.26(18) ? C7 C8 C13 C12 . . . . 171.66(12) ? C8 C9 C10 C11 . . . . 1.0(2) ? C9 C8 C13 O2 . . . . -176.87(12) ? C9 C8 C13 C12 . . . . -2.95(19) ? C9 C10 C11 C12 . . . . -0.6(2) ? C10 C11 C12 C13 . . . . -1.5(2) ? C10 C11 C12 C14 . . . 3_655 171.60(13) ? C11 C12 C13 O2 . . . . 177.27(11) ? C11 C12 C13 C8 . . . . 3.34(19) ? C13 O2 C18 C19 . . . . -170.66(11) ? C13 C8 C9 C10 . . . . 0.7(2) ? C14 C5 C6 O1 . . . . 11.25(19) ? C14 C5 C6 C1 . . . . -166.87(12) ? C14 C12 C13 O2 3_655 . . . 4.09(18) ? C14 C12 C13 C8 3_655 . . . -169.84(12) ? C15 O1 C6 C1 . . . . -98.40(14) ? C15 O1 C6 C5 . . . . 83.44(15) ? C18 O2 C13 C8 . . . . -96.01(14) ? C18 O2 C13 C12 . . . . 89.82(14) ?