Crystallography Open Database

Information card for entry 2023132

2023131 << 2023132 >> 2023133

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Coordinates	2023132.cif
Original IUCr paper	HTML

Structure parameters

Chemical name	Bis(4,4-dimethyl-2-phenyl-2-oxazoline-κ<i>N</i>)(hexamethyldisilylamido-κ<i>N</i>)lithium
Formula	C28 H44 Li N3 O2 Si2
Calculated formula	C28 H44 Li N3 O2 Si2
Title of publication	Crystal structure of a three-coordinate lithium complex with monodentate phenyloxazoline and hexamethyldisilylamide ligands
Authors of publication	Carneiro Neto, José Severiano; Iwaya, Eduardo Mariano; Santana, Francielli Sousa; Soares, Jaísa Fernandes
Journal of publication	Acta Crystallographica Section E Crystallographic Communications
Year of publication	2024
Journal volume	80
Journal issue	6
a	15.612 ± 0.002 Å
b	12.7649 ± 0.0017 Å
c	17.18 ± 0.004 Å
α	90°
β	116.243 ± 0.005°
γ	90°
Cell volume	3070.8 ± 0.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0492
Residual factor for significantly intense reflections	0.0352
Weighted residual factors for significantly intense reflections	0.0865
Weighted residual factors for all reflections included in the refinement	0.0915
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
291952 (current)	2024-05-18	cif/ Adding structures of 2023132 via cif-deposit CGI script.	2023132.cif