#------------------------------------------------------------------------------
#$Date: 2024-08-07 01:08:44 +0300 (Wed, 07 Aug 2024) $
#$Revision: 294011 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/31/2023156.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023156
loop_
_publ_author_name
'Näther, Christian'
'Jess, Inke'
_publ_section_title
;
 Syntheses and crystal structures of the five- and sixfold coordinated
 complexes diiso-seleno-cyanato-tris-(2-methyl-pyridine
 <i>N</i>-oxide)cobalt(II) and
 diiso-seleno-cyanato-tetra-kis-(2-methyl-pyridine
 <i>N</i>-oxide)cobalt(II).
;
_journal_coeditor_code           HB8098
_journal_issue                   'Pt 7'
_journal_name_full
'Acta crystallographica. Section E, Crystallographic communications'
_journal_page_first              704
_journal_page_last               708
_journal_paper_doi               10.1107/S2056989024005073
_journal_volume                  80
_journal_year                    2024
_chemical_formula_iupac          '[Co (N C Se)2 (C6 H7 N1 O1)4]'
_chemical_formula_moiety         'C26 H28 Co N6 O4 Se2'
_chemical_formula_sum            'C26 H28 Co N6 O4 Se2'
_chemical_formula_weight         705.39
_chemical_name_systematic
;
Diisoselenocyanatotetrakis(2-methylpyridine <i>N</i>-oxide)cobalt(II)
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_creation_method
;
Olex2 1.3-ac4
(compiled 2020.03.28 svn.rd84adfe8 for Rigaku Oxford Diffraction, GUI svn.r6032)
;
_cell_angle_alpha                90
_cell_angle_beta                 104.2170(10)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   9.38250(10)
_cell_length_b                   39.9164(3)
_cell_length_c                   15.99200(10)
_cell_measurement_reflns_used    27892
_cell_measurement_temperature    100.15
_cell_measurement_theta_max      79.0820
_cell_measurement_theta_min      3.0480
_cell_volume                     5805.82(9)
_computing_cell_refinement
;
CrysAlisPro 1.171.42.87a (Rigaku OD, 2023)
;
_computing_data_collection
;
CrysAlisPro 1.171.42.87a (Rigaku OD, 2023)
;
_computing_data_reduction
;
CrysAlisPro 1.171.42.87a (Rigaku OD, 2023)
;
_computing_molecular_graphics
;
Olex2 1.3-ac4 (Dolomanov et al., 2009)
;
_computing_publication_material
;
Olex2 1.3-ac4 (Dolomanov et al., 2009)
;
_computing_structure_refinement
;
<i>SHELXL2016/6</i> (Sheldrick, 2015b)
;
_computing_structure_solution
;
<i>SHELXT</i> (Sheldrick, 2015a)
;
_diffrn_ambient_temperature      100.15
_diffrn_detector                 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.939
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB Synergy, Dualflex, HyPix'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0203
_diffrn_reflns_av_unetI/netI     0.0138
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       50
_diffrn_reflns_limit_k_min       -49
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            41815
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         80.412
_diffrn_reflns_theta_min         2.214
_diffrn_source                   'micro-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu    7.856
_exptl_absorpt_correction_T_max  0.59636
_exptl_absorpt_correction_T_min  0.48904
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2023)
;
_exptl_crystal_colour            pink
_exptl_crystal_density_diffrn    1.614
_exptl_crystal_description       block
_exptl_crystal_F_000             2824
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.760
_refine_diff_density_min         -0.671
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.046
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     711
_refine_ls_number_reflns         11937
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.046
_refine_ls_R_factor_all          0.0402
_refine_ls_R_factor_gt           0.0379
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0611P)^2^+6.3002P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1068
_refine_ls_wR_factor_ref         0.1085
_reflns_number_gt                11197
_reflns_number_total             11937
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            hb8098.cif
_cod_data_source_block           2
_cod_depositor_comments
'Adding full bibliography for 2023156--2023157.cif.'
_cod_database_code               2023156
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_hkl_file
;
   0   0  -1 32.4030 16.9955   9
   0   0  -2 345906. 3377.45   9
   0   0  -3 189.377 52.2682   9
   0   0  -3 44.2618 53.8906  12
   0   0  -4 3598.34 108.232   9
   0   0  -4 3631.81 107.862  12
   0   0  -5 93.6632 75.9932  12
   0   0  -6 1942.95 109.840  12
   0   0  -7 66.5673 103.176  12
   0   0   7 35.1645 110.861   8
   0   0   8 34192.8 489.776   8
   0   0  -8 34480.7 485.369  12
   0   0  -9 33.8735 124.314  12
   0   0   9 50.3324 124.796   8
   0   0  10 120851. 1397.71   8
   0   0 -10 124260. 1389.33  12
   0   0 -11-43.8776 144.824  12
   0   0  11 45.5733 154.284   8
   0   0  12 1027.57 176.795   8
   0   0  13-86.1313 177.381   8
   0   0  13-12.1046 130.979  21
   0   0  14 277.030 134.418  21
   0   0  15 79.6079 126.271  21
   0   0  16 43092.3 497.262  21
   0   0  17 96.2956 93.4299  21
   0   0 -18 893.168 59.9885   4
   0   0 -19 3.14693 45.4431  24
   0   0  19-44.4987 36.9259   5
   0   1   1 18887.5 202.528   8
   0   1  -1 18825.9 208.782   9
   0   1  -2 6.20859 36.7314   9
   0  -1  -3 303360. 2949.59  13
   0   1  -3 312521. 3006.69   9
   0   1  -4 153.460 71.1496   9
   0   1  -4 177.326 74.1101  12
   0  -1  -5 7413.21 156.454  12
   0   1  -5 7411.30 157.999  12
   0   1   5 7291.59 157.359   8
   0   1  -5 6880.42 165.709   9
   0  -1  -6 17731.1 283.689  12
   0   1   6 17387.1 287.145   8
   0   1  -7 62255.9 739.497  12
   0  -1  -7 63212.1 735.912  12
   0   1   7 61248.7 741.998   8
   0   1  -8 6806.29 198.305  12
   0  -1  -8 6886.72 192.597  12
   0   1   8 6551.11 195.170   8
   0  -1   8 6714.30 210.265   8
   0   1  -9 274.158 125.492  12
   0  -1   9 277.594 140.078   8
   0   1   9 268.394 132.442   8
   0  -1  -9 329.447 124.172  12
   0   1 -10 66740.1 835.965  12
   0  -1 -10 66160.8 834.231  12
   0   1  10 65447.1 844.460   8
   0  -1  10 65984.5 849.498   8
   0  -1 -11 18983.5 371.175  12
   0  -1  11 19411.4 396.194   8
   0   1  11 19148.9 387.758   8
   0  -1  12 177.607 169.735   8
   0   1  12 114.531 166.882   8
   0   1  13 679.855 179.826   8
   0  -1  13 809.763 187.884   8
   0   1  13 818.439 132.601  21
   0  -1  13 781.963 137.734  21
   0  -1 -13 938.785 121.730  30
   0   1  14 338.282 135.139  21
   0  -1  14 354.568 132.150  21
   0  -1 -14 207.032 114.483  30
   0  -1  15 3796.09 152.036  21
   0   1  15 3747.14 152.447  21
   0  -1 -15 3680.83 135.812  30
   0  -1  16 1637.31 126.983  21
   0   1  16 1520.86 124.755  21
   0   1  17 2277.58 107.677  21
   0  -1  17 2326.11 105.881  21
   0   1 -18 7276.26 122.169  24
   0   1 -18 7129.63 113.352   4
   0  -1 -18 7382.81 114.914   4
   0   1 -19 2239.77 57.2908  24
   0  -1  19 2401.04 52.5206   5
   0   2   0 49.1476 12.1063   7
   0   2   1 86.8080 22.1633   8
   0   2  -1 66.9707 27.6323   9
   0   2   2 6816.46 106.457   8
   0   2  -2 6910.60 116.058   9
   0   2   3 59590.4 628.581   8
   0   2  -3 58032.6 641.780   9
   0  -2  -4 267.706 24.7951  13
   0   2   4 274.622 68.8679   8
   0   2  -4 216.907 77.9275   9
   0   2  -4 279.956 83.4124  12
   0   2  -5 43775.4 522.324  12
   0   2  -5 43066.0 528.514   9
   0   2   5 43213.1 518.192   8
   0  -2  -6 670.921 90.3397  12
   0   2   6 601.290 94.1351   8
   0   2  -6 631.369 96.8132  12
   0   2  -6 566.626 92.3136   9
   0  -2  -7 67268.8 772.390  12
   0   2  -7 66255.1 778.300  12
   0   2  -8 30555.4 445.211  12
   0  -2  -8 29911.8 433.491  12
   0   2  -9 8116.56 224.804  12
   0  -2  -9 8574.37 226.514  12
   0  -2   9 8297.19 232.817   8
   0   2   9 7756.79 233.324   8
   0  -2 -10 1179.53 149.902  12
   0   2 -10 1143.05 151.479  12
   0   2  10 1202.52 157.000   8
   0  -2  10 1118.47 167.214   8
   0  -2 -11 8829.00 257.263  12
   0   2  11 8955.39 270.243   8
   0  -2  11 9080.55 279.027   8
   0  -2 -12 46888.1 673.817  12
   0  -2  12 48676.3 710.436   8
   0   2  12 47297.1 699.579   8
   0   2  13 20067.9 418.874   8
   0  -2  13 20337.7 427.077   8
   0  -2  13 19851.3 305.487  21
   0   2  13 20066.3 304.478  21
   0  -2 -13 21031.7 289.680  30
   0   2  14 767.400 134.521  21
   0  -2  14 731.266 135.144  21
   0  -2 -14 905.700 124.052  30
   0  -2  15 12910.2 231.762  21
   0   2  15 12642.2 228.286  21
   0  -2 -15 12936.8 211.025  30
   0   2  16 5798.79 153.857  21
   0  -2  16 5910.17 156.295  21
   0   2  17 8289.04 154.596  21
   0  -2  17 8353.68 155.275  21
   0   2 -18 471.479 71.1524  24
   0  -2 -18 376.537 55.0769   4
   0  -2 -19 521.307 45.7989  24
   0   2 -19 451.045 47.8707  24
   0  -2  19 483.600 38.6223   5
   0   3   0 88.3272 21.7796   7
   0   3   1 15677.8 181.275   8
   0   3   2 3844.43 79.4218   8
   0   3  -2 3931.62 91.2028   9
   0   3  -3 112197. 1148.88   9
   0   3   3 109486. 1128.39   8
   0   3  -4 16022.1 240.721  12
   0   3  -4 16240.1 250.156   9
   0   3   4 15496.7 233.348   8
   0   3   5 185851. 1865.45   8
   0   3  -5 189170. 1883.89   9
   0   3  -6 17564.2 286.579  12
   0  -3  -6 17547.1 271.769  12
   0   3   6 17159.5 276.804   8
   0   3  -7 938.985 112.729  12
   0  -3  -7 930.784 103.671  12
   0   3  -7 896.457 113.394   9
   0   3   7 931.176 115.621   8
   0  -3  -8 10408.2 236.446  12
   0   3  -8 10862.6 249.442  12
   0   3   8 11130.4 245.483   8
   0  -3  -9 838.213 131.303  12
   0   3  -9 722.839 135.627  12
   0  -3   9 765.985 151.995   8
   0   3   9 823.807 144.149   8
   0  -3 -10 22087.1 392.646  12
   0   3  10 22290.5 404.720   8
   0  -3  10 22284.1 414.136   8
   0  -3  11 128.933 158.239   8
   0   3  11 126.093 151.820   8
   0  -3 -11 78.6423 143.600  12
   0  -3  12 49649.2 716.227   8
   0   3  12 48363.8 701.944   8
   0   3  13 14357.6 357.552   8
   0  -3  13 14640.0 363.234   8
   0  -3  13 14614.7 252.924  21
   0   3  13 14596.2 252.303  21
   0  -3 -13 14953.5 237.877  30
   0   3  14 363.519 130.056  21
   0  -3  14 527.747 138.302  21
   0  -3 -14 407.214 118.708  30
   0   3  15 11260.4 215.358  21
   0  -3 -15 10902.2 197.116  30
   0   3  16 1102.12 117.294  21
   0  -3  16 1263.13 118.503  21
   0  -3 -16 1266.38 101.601  30
   0   3  17 1053.37 96.9795  21
   0  -3  17 1157.28 97.8899  21
   0   3 -18 2598.47 83.3605  24
   0  -3 -18 2644.97 72.8736   4
   0   3  18 2476.79 80.3085  21
   0   3 -19 20.1283 43.0951  24
   0  -3 -19 45.1392 42.2716  24
   0  -3  19-27.0370 36.3141   5
   0   4   0 84237.8 849.729   7
   0   4  -1 358459. 3516.79   7
   0   4   1 359988. 3503.44   8
   0   4   1 360323. 3506.23  14
   0   4   2 42298.8 455.970   8
   0   4  -2 42021.6 478.222   9
   0   4   3 166241. 1669.22   8
   0   4  -3 166533. 1695.32   9
   0   4   4 6776.33 140.357   8
   0   4  -4 6376.84 159.437   9
   0   4  -5 593227. 5862.04  12
   0   4   5 600229. 5849.13   8
   0   4  -5 593951. 5878.00   9
   0   4  -6 1012.97 112.124  12
   0   4  -6 992.348 110.052   9
   0   4   6 1014.99 108.416   8
   0  -4  -7 3235.89 137.251  12
   0   4  -7 3131.89 144.285  12
   0   4  -7 2916.63 147.704   9
   0   4   7 2891.21 147.985   8
   0   4  -8 17446.0 316.732  12
   0  -4  -8 18066.0 315.024  12
   0   4   8 17152.5 319.228   8
   0   4   9 52347.6 698.671   8
   0  -4  -9 54456.8 689.839  12
   0  -4 -10 3586.75 176.657  12
   0   4  10 3573.17 189.011   8
   0  -4  10 3737.36 200.987   8
   0  -4 -11 23502.8 415.334  12
   0   4  11 22711.4 428.927   8
   0  -4  11 23519.3 440.547   8
   0  -4 -12 334.271 143.142  12
   0   4  12 300.233 156.227   8
   0  -4  12 363.700 170.227   8
   0  -4  13 5413.21 174.625  21
   0   4  13 5375.11 171.492  21
   0   4  13 5532.40 246.973   8
   0  -4  13 5727.77 254.413   8
   0  -4 -13 5330.43 150.647  30
   0  -4 -14 56.5719 117.372  30
   0   4  14 56.6581 131.020  21
   0  -4  14 135.363 132.680  21
   0  -4 -15 1918.86 125.988  30
   0   4  15 2128.96 141.049  21
   0  -4  15 2291.95 142.519  21
   0  -4 -16 392.853 100.055  30
   0   4  16 347.408 111.860  21
   0  -4  16 302.848 115.649  21
   0   4  17 457.562 91.2954  21
   0   4  18 353.370 65.5466  21
   0   4 -18 321.230 70.1763  24
   0   4 -18 256.690 52.2997   4
   0  -4 -18 303.342 53.7860   4
   0   4  18 166.388 55.1314   5
   0  -4  18 211.220 55.3280   5
   0   4 -19 142.553 42.1071  24
   0  -4 -19 131.496 43.5952  24
   0   4  19 110.379 35.4158   5
   0  -4  19 109.640 35.1582   5
   0   5   0 30.8946 35.4519   7
   0   5   1 23374.7 269.500  14
   0   5  -1 23592.2 283.427   7
   0   5   1 23551.3 268.353   8
   0   5   2 28165.5 323.532   8
   0   5  -2 27419.9 349.672   9
   0   5   3 12048.1 181.692   8
   0   5  -3 11675.9 214.014   9
   0   5   4 13324.3 212.211   8
   0   5  -4 13742.8 236.374   9
   0   5  -5 38249.6 483.084  12
   0   5   5 38305.7 475.248   8
   0   5  -5 37615.2 502.310   9
   0   5  -6 3405.15 142.851  12
   0  -5  -6 3159.83 64.1446  13
   0   5   6 3265.73 132.741   8
   0   5  -6 3387.91 143.418   9
   0   5  -7 7386.54 197.219  12
   0   5   7 7386.58 190.965   8
   0   5  -7 7073.38 201.436   9
   0  -5  -8 48519.8 616.638  12
   0   5   8 48068.7 626.933   8
   0   5  -8 47437.4 644.884   9
   0   5  -9 1571.64 94.5817  16
   0   5   9 1367.64 149.590   8
   0  -5  -9 1700.77 134.606  12
   0   5  10 3870.51 191.620   8
   0  -5  10 3993.25 202.445   8
   0  -5 -10 4181.71 179.219  12
   0   5  11 48781.7 694.931   8
   0  -5  11 49077.6 710.719   8
   0  -5 -11 49472.5 678.635  12
   0  -5 -12 261.864 139.895  12
   0   5  12 345.671 159.582   8
   0  -5  12 320.013 165.170   8
   0  -5  13 6094.85 174.796  21
   0   5  13 5859.71 176.067  21
   0  -5 -13 5876.86 223.026  12
   0  -5 -13 6198.52 163.444  30
   0  -5  13 6206.91 266.395   8
   0   5  13 6044.49 245.403   8
   0  -5 -14 458.886 116.780  30
   0   5  14 408.659 130.480  21
   0  -5  14 500.391 134.004  21
   0  -5 -15 17553.5 253.697  30
   0  -5  15 17846.0 274.616  21
   0   5  15 17517.4 270.284  21
   0   5  16 31494.3 381.767  21
   0  -5  16 31648.9 383.548  21
   0   5 -17 1037.49 95.4684  24
   0   5  17 1051.59 94.7573  21
   0   5 -18 1647.10 76.6770  24
   0   5  18 1589.99 70.5834  21
   0  -5  18 1407.70 62.7346   5
   0   5  18 1398.89 62.6770   5
   0   5 -18 1441.39 59.7519   4
   0  -5 -18 1441.29 61.2160   4
   0   5 -19 47.0475 40.2865  24
   0  -5 -19 61.2343 42.2572  24
   0   5  19 12.9378 32.4723   5
   0  -5  19 39.0658 32.6056   5
   0   6   0 481.065 48.0538   7
   0   6   1 51.1667 38.2889  14
   0   6  -1 41.0209 54.3851   7
   0   6   2 2443.38 83.4374   8
   0   6   3 1789.22 83.5402   8
   0   6  -3 1822.52 104.795   9
   0   6   4 3533.02 111.163   8
   0   6  -4 3791.97 132.474   9
   0   6   5 9720.80 191.457   8
   0   6  -5 9782.57 215.640   9
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   3   0  -8-8.08614 89.4764  13
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   3   0  -5 8129.03 200.680   1
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   3   1  -5 598463. 5931.44  13
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   3   2  -8 143098. 1537.65  13
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   3  -2  -3 168817. 1789.91  13
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   3  -2  -2 177707. 1811.26   1
   3  -2  -2 184193. 1811.94   2
   3   2  -2 180770. 1823.27  13
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   3  -2   0 32034.0 421.490   1
   3  -2   0 31945.5 421.190   2
   3   2   0 32250.1 426.940  13
   3  -2   1 102107. 1015.17   8
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   3  -2   1 98003.3 1086.80   2
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   3  -5   6 87816.8 1000.18   8
   3   5   6 87047.2 1015.97   8
   3   5   6 87219.9 978.878   7
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   3   5   9 17718.6 372.705   8
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   3   5  10 1088.15 174.034   8
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   3   5  15 770.525 81.2652   5
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   3   5  16 10817.6 147.979   6
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   3   6 -14 8526.67 178.975   4
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   3  -6  -6 34072.9 468.900  13
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   3   6  -5 622.808 116.873   9
  -3   6   4 344864. 3398.23   8
   3   6  -4 345011. 3502.52   1
   3  -6  -4 351768. 3494.45   1
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   3  -6  -4 356836. 3505.83  13
   3   6  -4 345743. 3505.69  13
   3   6  -4 350938. 3522.63   9
   3   6  -3 189654. 1986.90   1
   3  -6  -3 190436. 1982.45   1
  -3   6   3 195529. 2010.80  14
   3   6  -3 195976. 2007.55  13
   3  -6  -3 197808. 2006.38  13
   3   6  -3 193400. 2001.93   9
   3  -6  -2 37402.4 461.366   2
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   3   6  -2 36051.3 461.298   1
   3   6  -2 37075.2 457.848   2
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   3   6  -2 36967.9 484.412  13
   3   6  -2 35967.3 459.730   9
   3  -6  -1 192307. 1980.72   2
   3   6  -1 190199. 1976.58   2
   3   6  -1 195319. 1984.53   1
   3  -6  -1 198544. 1984.98   1
   3   6  -1 194562. 1960.38   9
   3   6   0 49721.3 593.441   7
   3  -6   0 47141.0 586.266   2
   3   6   0 46851.6 581.155   2
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   3  -6   0 51648.6 606.984  13
   3   6   0 50147.8 540.144   9
   3   6   1 101059. 1082.77   7
   3  -6   1 101035. 1099.57   2
   3   6   1 101000. 1094.02   2
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   3  -6   1 103485. 1098.84  13
   3  -6   1 99423.6 1014.80   8
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   3   6   2 12354.8 219.150   8
   3   6   2 12518.7 216.547   7
   3  -6   2 12938.2 248.469   2
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   3   6   5 5154.81 151.253   7
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   3  -6   6 198742. 2070.08   8
   3   6   6 197063. 2086.28   8
   3   6   6 194876. 2052.22   7
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   3   6   7 1237.26 146.506   8
   3   6   7 1304.65 112.682   7
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   3   6   8 21999.8 406.734   8
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   3   6   9 494.393 154.120   8
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   3   6  11 160.379 109.747   5
   3  -6  11 291.623 150.771   8
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   3   6  11 254.473 172.249   2
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   3   6  12 13109.1 217.122   5
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   3   6  13 7297.58 156.333   5
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   3   6  14 603.127 95.9003   5
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   3   6  16 1784.01 71.2817   6
   3  -6  16 1741.28 68.4569   6
   3   6  16 1837.13 68.5609   5
   3  -6  16 1845.21 66.5925   5
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   3  -6  17 15.4798 34.0515   6
   3   6  17 60.6272 33.1126   5
   3  -6  17 68.9467 32.2870   5
   3   6  17 9.75898 34.9536   6
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   3  -7 -18 1790.01 71.0197   4
   3   7 -18 1764.63 67.6139   4
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   3  -7 -18 1693.97 70.8226   3
   3   7 -18 1759.47 67.9642   3
   3  -7 -18 1758.55 100.685  30
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   3  -7 -17 4897.35 145.371  30
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   3  -7 -16 7075.77 185.816  30
   3   7 -16 6963.42 183.887  30
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   3   7 -16 7390.46 150.938   4
   3  -7 -16 7536.30 152.354   4
   3   7 -16 7136.46 151.583  24
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   3   7 -14 2873.75 164.988  30
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   3  -7 -14 2369.75 125.558   4
   3   7 -14 2512.27 122.785   4
   3   7 -13 10261.3 199.675   4
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   3  -7 -13 9903.55 317.312   1
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   3  -7 -13 11717.8 229.433  30
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   3   7 -12 891.534 180.576   1
   3  -7 -12 880.129 180.384   1
   3  -7 -12 983.328 108.651   4
   3   7 -12 1008.57 112.804   4
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   3  -7 -11 15732.0 370.693   1
   3   7 -11 14858.6 374.486   1
   3   7 -11 16005.6 239.160   4
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   3   7 -10 3206.30 202.770   1
   3  -7 -10 2797.32 192.679   1
   3  -7 -10 2926.43 111.506   4
   3   7 -10 2997.69 114.415   4
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   3   7  -9 22733.1 291.375   4
   3  -7  -9 22605.5 289.272   4
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   3   9   5 56664.6 729.925   2
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   3   9   6 2086.38 165.717   2
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   4   4 -17 247.140 74.7765   3
   4   4 -17 294.244 74.3923   4
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   4   4 -16 1078.42 95.8061   3
   4  -4 -16 1019.17 100.616   3
   4   4 -16 1238.40 92.2100  24
   4   4 -15 1943.32 117.815   4
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   4   4 -15 1889.86 121.099   3
   4  -4 -15 1739.43 120.362   3
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   4   4 -15 2011.06 157.031  30
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   4   4 -14 861.432 118.731   4
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   4   4 -13 1431.02 194.925   1
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   4   4   1 174585. 1852.87  13
   4   4   1 178349. 1859.27   2
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   4  -4   3 49641.9 576.089   8
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   4  -4   4 60727.6 773.228   2
   4  -4   4 55280.8 658.336   8
   4   4   4 54987.8 683.853   8
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   4   4   5 6947.04 198.537   8
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   4   4   6 283.851 123.470   8
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   4   4   6 461.406 164.139   2
   4   4   7 40440.7 641.589   2
   4  -4   7 38667.3 629.435   2
   4  -4   7 38048.5 544.910   8
   4   4   7 37369.6 562.234   8
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   4   4   8 28074.3 524.482   2
   4  -4   8 27230.6 516.727   2
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   4  -4   8 25697.3 433.842   8
   4   4   8 25552.6 450.258   8
   4   4   9 47129.0 731.455   2
   4  -4   9 48837.3 729.902   2
   4  -4   9 43668.4 637.521   8
   4   4   9 43092.8 650.850   8
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   4   4   9 46028.4 527.348   5
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   4   4  13 26653.4 326.939   6
   4  -4  13 25972.7 321.560   5
   4   4  13 26240.7 323.886   5
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   4   4  14 3320.66 106.683   6
   4  -4  14 3422.76 96.0136   5
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   4   4  14 3505.01 99.8872   5
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   4   4  15 591.649 65.0091   6
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   4   4  16 1239.17 47.3289   5
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   4   5 -15 3981.67 178.256  30
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   4  -5 -14 10250.2 200.088   4
   4   5 -14 10454.5 199.207   4
   4   5 -14 10096.1 199.815   3
   4  -5 -14 10035.7 200.839   3
   4   5 -13 847.026 182.104   1
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   4   5 -12 7108.14 279.983   1
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   4   5 -11 11742.5 336.379   1
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   4   5  -9 116364. 1385.51   1
   4   5  -9 116634. 1199.52   4
   4  -5  -9 118559. 1197.52   4
   4  -5  -8 208.143 74.1938   3
   4   5  -8 87.3680 142.096   1
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   4  -5   2 98146.7 1096.16   2
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   4   5   7 74271.2 945.525   2
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   4   5   7 64434.5 846.654   8
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   4   5  14 1306.80 85.0498   5
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   4   5  15 226.602 59.0766   5
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   4   5  16-2.36412 37.1390   5
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   4   6 -18 624.203 54.9487   3
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   4  -6 -16 775.546 90.8960   4
   4   6 -16 850.529 97.2538   4
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   4  -6 -16 837.921 91.2846   3
   4   6 -16 856.374 88.1836   3
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   4   6 -15 3562.56 128.850   4
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   4   6 -15 3632.99 125.716   3
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   4   6 -14 20063.2 284.003   4
   4  -6 -14 19669.6 285.312   4
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   4   6 -14 19710.3 286.079   3
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   4  -6 -13 37927.3 649.583   1
   4   6 -13 39608.6 658.828   1
   4   6 -13 38388.3 477.436   4
   4  -6 -13 39931.9 475.086   4
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   4   6 -13 42127.3 501.262  30
   4  -6 -13 42155.4 498.474  30
   4   6 -12 30342.1 384.791   4
   4  -6 -12 30082.2 384.054   4
   4   6 -12 32026.0 407.792  30
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   4   6  -8 9940.06 165.496   4
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   4  -6  -7 41475.5 581.041  13
   4   6  -7 43195.8 610.840   1
   4  -6  -7 41865.7 601.116   1
   4   6  -6 13439.0 280.729  13
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   4   6  -5 8310.25 223.542  13
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   4   6  -3 105603. 1168.11  13
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   4   6   4 18450.8 319.244   8
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   4   6   6 6342.17 205.544   8
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   4   6   7 6822.05 265.258   2
   4  -6   7 6731.30 265.751   2
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   4   6   7 6604.96 229.462   8
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   4  -6   8 5910.45 208.722   8
   4   6   8 5728.19 223.899   8
   4  -6   9 1852.42 114.944   5
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   4   6   9 1628.31 167.242   8
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   4   6  11-25.4880 104.504   5
   4  -6  11 16.6100 99.4584   5
   4  -6  12 212.348 95.3814   5
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   4   6  13 402.208 98.1046   6
   4  -6  13 373.079 95.6362   6
   4  -6  13 509.527 91.1516   5
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   4   6  15 1718.42 70.5491   6
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   4   6  15 1878.37 68.9687   5
   4  -6  15 1744.95 68.7840   6
   4  -6  16 2580.48 61.3229  19
   4  -6  16 2618.15 55.2332   6
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   4  -6  16 2630.45 54.2105   5
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   4   7 -18 2432.73 70.5725   4
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   4   7 -18 2384.45 69.3249   3
   4  -7 -18 2385.02 73.0314   4
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   4   7 -17 55.0640 69.3628   3
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   4   7 -17 76.9321 67.1412   4
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   4   7 -16 3994.04 113.934   3
   4   7 -16 3768.79 109.224  24
   4   7 -15 17219.2 286.538  30
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   4   7 -15 18690.7 258.516   4
   4  -7 -15 18555.2 259.800   4
   4   7 -15 18957.4 259.776   3
   4  -7 -15 18614.4 261.454   3
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   4   7 -14 1105.55 114.933   3
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   4  -7 -13 7170.37 160.443   4
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   4  -7 -13 5917.59 189.109  30
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   4   7 -13 6955.54 162.376   3
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   4   7 -12 97.9706 162.429   1
   4  -7 -12 141.046 163.761   1
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   4   7 -11 14245.6 367.352   1
   4  -7 -11 15310.7 365.004   1
   4   7 -10 21576.7 287.571   4
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   4  -7 -10 21550.3 427.134   1
   4   7 -10 21126.1 433.537   1
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   4  -7  -9 1609.93 165.388   1
   4   7  -9 1352.18 94.8486   3
   4  -7  -9 1441.69 89.3924   3
   4   7  -9 1328.73 91.9538   4
   4  -7  -9 1349.25 90.8968   4
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   4   7  -8 26272.3 447.314   1
   4  -7  -8 25950.2 438.288   1
   4   7  -8 23769.8 304.183   3
   4  -7  -8 24865.6 300.973   3
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   4   7  -8 24749.5 303.933   4
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   4  -7  -7 19406.2 356.471   1
   4   7  -7 18539.1 361.802   1
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   4   7  -5 39434.1 566.720   9
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   4   7  -3 121646. 1363.04  13
   4   7  -3 120438. 1333.88   1
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   4   7  -1 22815.7 354.335   1
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   4   7   1 31131.9 439.270   2
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   4   7   2 32630.7 478.591   2
   4  -7   2 33775.1 484.147   2
   4  -7   3 23809.3 322.377   8
   4   7   3 23815.2 353.730   7
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   4   7   3 26804.7 416.997   2
   4  -7   3 25732.2 422.038   2
   4  -7   4 45648.1 557.368   8
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   4   7   4 47276.5 652.234   2
   4  -7   4 46972.1 656.431   2
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   4   7   5 8054.49 262.389   2
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   4   7   5 7654.77 217.501   8
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   4   7   6 7289.36 223.422   8
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   4   7   7 13169.7 305.782   8
   4   7   7 14380.8 361.859   2
   4  -7   7 15110.3 357.207   2
   4  -7   8 213.329 127.534   8
   4   7   8 157.150 142.284   8
   4   7   8 158.076 167.744   2
   4  -7   8 139.993 163.101   2
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   4  -7   9 10689.5 193.406   5
   4   7   9 10894.8 197.203   5
   4   7   9 10477.7 327.974   2
   4  -7   9 11087.9 326.178   2
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   4   7   9 10316.9 294.214   8
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   4   7  10 4502.51 239.750   2
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   4   7  11 4472.17 137.954   5
   4  -7  12 1240.43 104.424   5
   4   7  12 1184.68 106.785   5
   4  -7  13 12528.6 195.651   6
   4  -7  13 12885.4 191.581   5
   4   7  13 12939.1 197.187   6
   4   7  13 13305.1 196.608   5
   4  -7  14 648.869 79.0185   6
   4   7  14 537.124 80.8802   6
   4   7  14 698.091 78.0081   5
   4  -7  14 665.105 75.0532   5
   4   7  15 1964.56 70.8001   6
   4  -7  15 2157.94 65.8066   5
   4   7  15 2167.92 68.0234   5
   4  -7  15 2073.99 69.3364   6
   4   7  16 155.643 35.5673   5
   4  -7  16 150.114 34.3466   5
   4   7  16 216.383 35.5448   6
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   4  -7  16 199.905 35.6439   6
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   4   8 -18 127.461 48.7892   3
   4  -8 -18 182.929 52.9292   3
   4  -8 -18 129.987 91.2460  30
   4   8 -18 85.5393 51.5601   4
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   4  -8 -17 688.165 70.9577   4
   4   8 -17 738.359 71.1936   3
   4   8 -17 736.901 73.3597   4
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   4   8 -16 58.1931 138.962  30
   4  -8 -16 117.655 129.334  30
   4   8 -16 73.6053 83.2537   3
   4  -8 -16 12.4134 85.8340   3
   4   8 -16 128.709 82.9605  24
   4   8 -16 152.641 84.5562   4
   4  -8 -16 59.0753 86.7881   4
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   4   8 -15 1797.19 110.208   4
   4  -8 -15 1609.14 112.261   4
   4   8 -15 2662.08 170.136  30
   4   8 -15 2212.49 104.633  24
   4   8 -15 1604.57 107.031   3
   4  -8 -15 1629.70 108.916   3
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   4   8 -14 276.664 155.178  30
   4  -8 -14-10.3155 100.772   3
   4   8 -14 130.828 96.7956   3
   4   8 -14 210.206 94.7996  24
   4  -8 -14 174.426 99.2964   4
   4   8 -14 161.650 105.069   4
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   4  -8 -13 3145.88 129.124   4
   4   8 -13 3091.74 126.599   4
   4   8 -13 3197.03 176.292  30
   4  -8 -13 3264.55 166.553  30
   4   8 -13 2936.35 212.214   1
   4  -8 -13 3001.01 212.713   1
   4   8 -13 3062.39 114.176  24
   4  -8 -13 2856.93 130.072   3
   4   8 -13 2971.26 129.334   3
   4   8 -12 2706.42 164.253  30
   4  -8 -12 2830.72 154.703  30
   4  -8 -12 2822.11 119.954   4
   4   8 -12 2748.61 127.113   4
   4  -8 -12 2812.62 209.972   1
   4   8 -12 2625.99 207.517   1
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   4   8 -12 2677.16 121.318   3
   4  -8 -12 2700.92 120.489   3
   4   8 -11 4194.60 225.269   1
   4  -8 -11 3959.05 218.557   1
   4   8 -11 4224.44 130.854   4
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   4   8 -10 8124.82 268.981   1
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   4   8  -9-19.2607 80.8971   4
   4  -8  -9 88.7011 76.7328   4
   4  -8  -9 29.0499 78.5342   3
   4   8  -9 52.5205 80.4926   3
   4  -8  -9 70.2228 141.000   1
   4   8  -9 98.0573 146.059   1
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   4  -8  -8 79.5112 70.3681   4
   4   8  -8 175.646 72.8138   4
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   4  -8  -8 3.81383 129.348   1
   4  -8  -8 50.6042 71.6051   3
   4   8  -8 270.301 144.630   1
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   4  -8  -7 39757.0 569.839  13
   4   8  -7 41300.2 592.119   1
   4  -8  -7 41388.6 581.561   1
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   4  -8  -6 4937.74 185.513  13
   4   8  -6 4367.06 187.761   1
   4  -8  -6 4703.14 178.452   1
   4   8  -6 4633.41 206.414   9
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   4  -8  -5 108433. 1272.42  13
   4  -8  -5 116346. 1258.45   1
   4   8  -5 117677. 1269.22   1
   4   8  -5 110904. 1289.26   9
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   4  -8  -4 14002.9 266.924   1
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   4   8  -2 43825.0 573.227   1
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   4   8  -1 16364.7 293.790   1
   4  -8  -1 17076.0 290.897   2
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   4  -8  -1 16616.8 288.484   1
   4   8  -1 16320.5 250.496   9
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   4   8   0 2661.99 133.433   2
   4  -8   0 2889.10 141.043   2
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   4   8   1 11334.7 231.245   7
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   4  -8   1 11401.3 249.931   2
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   4   8   2 53823.9 661.033   7
   4  -8   2 54796.0 679.788  13
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   4   8   2 52953.4 689.004   2
   4  -8   2 54754.0 696.361   2
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   4  -8   3 307616. 3091.40   8
   4  -8   3 317777. 3160.77  13
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   4  -8   3 319280. 3210.30   2
   4   8   3 314435. 3197.54   2
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   4  -8   4 3636.89 126.701   8
   4   8   4 3856.74 142.484   7
   4  -8   4 3664.48 136.993  13
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   4   8   4 3870.56 188.437   2
   4  -8   4 4012.06 185.466   2
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   4 -10  -8 190261. 1917.54   4
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   4 -10  -8 197810. 2082.01   1
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   4 -10  -8 190934. 1917.77   3
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   4 -10  10 18471.5 256.101   5
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   4 -11 -14 1857.54 107.867   3
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   5   0  -8 56.1575 136.708  13
   5   0  -7 234390. 2352.42   3
   5   0  -7 238413. 2353.58   4
   5   0  -7 244431. 2534.23   1
   5   0  -7 239545. 2510.98  13
   5   0  -6 35.4327 70.3617   4
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   5   0  12 66.4207 92.8112   5
   5   0  12 22.4479 91.3210   6
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   5  -1 -18 1923.80 66.4274   4
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   6  -3   5 23180.9 467.547   2
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   6   3   5 21877.7 307.653   6
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   6   3   7 14050.5 233.260   5
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   6   3   8-22.0175 110.040  19
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   6  -5   1 154458. 1744.00   2
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   6   5   2 4770.22 220.336   2
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   6   5   3 32143.5 547.223   2
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   6   5   5 5038.93 142.947   5
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   6  -5   6 7512.86 279.884   2
   6  -5   6 7435.31 164.393   5
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   6   5   6 7376.95 167.539  19
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   6  -5   7 304.906 106.839   5
   6   5   7 180.036 105.726   5
   6   5   7 245.658 113.226   6
   6  -5   7 313.453 111.009   6
   6   5   7 165.439 105.001  19
   6  -5   8 3630.29 133.042   5
   6   5   8 3448.70 133.024   5
   6   5   8 3682.54 139.446   6
   6  -5   8 3620.09 133.623   6
   6   5   8 3212.50 130.393  19
   6  -5   9 3063.41 120.534   5
   6   5   9 3121.81 122.474   5
   6   5   9 3174.91 133.162   6
   6  -5   9 3214.33 128.166   6
   6   5   9 3430.72 122.553  19
   6   5  10 19811.4 265.671   6
   6  -5  10 19712.9 263.327   6
   6  -5  10 20113.1 259.409   5
   6   5  10 19869.6 261.549   5
   6  -5  10 19274.2 277.076  19
   6   5  11 4258.20 117.469   6
   6  -5  11 4046.24 113.527   6
   6  -5  11 4012.66 107.592   5
   6   5  11 4047.32 109.830   5
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   6   5  13 3819.48 77.1909   6
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   6   7  13 674.850 50.2438   6
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   6  -8 -13 4609.62 170.184  30
   6   8 -13 4105.52 186.520  30
   6   8 -12 16838.2 246.334   3
   6  -8 -12 17128.3 243.984   3
   6   8 -12 16716.5 251.903   4
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   7   1 -10 5905.58 161.695   4
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   7  -1  -9 1504.67 191.241   1
   7  -1  -9 394.668 141.988  29
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   7  -1  -9 405.889 156.818  25
   7   1  -8 207.482 102.829   4
   7  -1  -8 167.023 98.3445   4
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   7  -1  -8 451.511 136.822  29
   7   1  -8 413.537 136.466  29
   7  -1  -7 4281.24 234.493   1
   7   1  -7 3952.35 230.171  13
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   7   1  -7 4409.78 133.982   4
   7  -1  -7 4497.76 132.935   4
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   7   1  -6 5934.27 145.339   4
   7  -1  -6 6122.34 143.760   4
   7  -1  -5 704.646 169.995   1
   7   1  -5 473.770 173.832  13
   7  -1  -5 503.914 174.860  13
   7  -1  -5 700.907 93.8103   3
   7   1  -5 627.642 98.2303   4
   7  -1  -5 623.437 96.5517   4
   7  -1  -4 20772.0 414.219   1
   7  -1  -4 20364.4 272.265   3
   7  -1  -4 20747.9 276.727   4
   7   1  -3 103368. 1284.09  13
   7  -1  -3 105347. 1293.25  13
   7   1  -2 6958.87 273.934  13
   7  -1  -2 7344.47 275.010  13
   7   1  -1 25449.3 480.575  13
   7  -1  -1 25441.4 481.728  13
   7   1  -1 25643.3 469.853   2
   7   1   0 5240.25 237.923  13
   7  -1   0 5470.58 236.985  13
   7  -1   0 5933.51 245.786   2
   7  -1   1 3331.55 199.170  13
   7  -1   1 3311.53 211.372   2
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   7  -1   2 5558.60 146.881   5
   7  -1   3 1402.07 191.405   2
   7  -1   3 1392.52 121.141  19
   7   1   3 1395.69 117.003  19
   7  -1   3 1225.18 117.933   6
   7  -1   3 1296.25 117.083   5
   7  -1   4 10207.0 321.511   2
   7  -1   4 10104.2 196.415   5
   7  -1   4 10080.3 199.914  19
   7   1   4 9793.85 193.402  19
   7  -1   5 670.911 118.593   6
   7  -1   5 545.347 117.634   5
   7   1   5 750.372 117.071  19
   7  -1   5 739.770 127.630  19
   7  -1   6 4350.58 151.544   6
   7  -1   6 4684.02 142.576   5
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   7   1   7 10011.3 188.068  19
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   7  -1   8 7741.98 165.125   6
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   7  -1   9 8082.44 148.709   5
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   7  -1   9 7728.24 153.851  19
   7   1  10 767.849 84.7921   6
   7  -1  10 623.194 83.5786   6
   7  -1  10 686.494 80.1238   5
   7   1  10 736.765 75.7812  19
   7  -1  10 731.608 79.8716  19
   7   1  11 366.504 64.1553   6
   7  -1  11 419.085 63.6730   6
   7  -1  11 416.613 60.4235   5
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   7  -1  12 2991.21 61.3728   5
   7  -1  12 2833.40 63.4761   6
   7  -1  13 1795.10 32.9510   5
   7  -1  13 1740.60 33.6562   6
   7   2 -18 103.096 44.3132  20
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   7   2 -17 228.167 64.1806  20
   7  -2 -17 211.048 68.1996  20
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   7  -2 -16 417.824 68.3675   4
   7   2 -16 588.668 87.1166  20
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   7  -2 -13 4811.47 138.918   4
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   7  -2 -12 2294.27 119.639   3
   7  -2 -12 2493.49 127.532   4
   7  -2 -12 1900.72 164.092  25
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   7  -2 -10 15610.7 234.739   4
   7  -2 -10 15983.7 233.048   3
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   7  -2 -10 13948.9 254.428  29
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   7  -2  -9 32938.7 397.165   4
   7  -2  -9 32583.6 393.996   3
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   7  -2  -9 31487.1 412.982  29
   7   2  -9 31650.9 420.661  29
   7   2  -9 30712.6 425.927  25
   7  -2  -9 30723.8 425.568  25
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   7  -2  -7 12219.3 244.475  25
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   7  -2  -7 12694.2 210.732   4
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   7   2  -6 39336.3 652.085  13
   7  -2  -6 40229.4 657.707  13
   7  -2  -6 41887.5 480.407   3
   7  -2  -6 42139.7 483.726   4
   7  -2  -5 2101.40 191.042   1
   7   2  -5 1769.48 198.268  13
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   7  -2  -5 1861.58 104.683   4
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   7  -2  -4 5356.43 131.627   3
   7  -2  -4 5289.99 132.653   4
   7   2  -3 48076.6 728.951  13
   7  -2  -3 48346.4 728.779  13
   7   2  -2 24780.0 484.349  13
   7  -2  -2 26447.1 489.813  13
   7   2  -1 12635.1 338.830  13
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   7  -2   0 1606.87 181.124  13
   7  -2   0 1217.97 173.454   2
   7  -2   1 33210.6 552.590  13
   7  -2   1 35704.9 582.661   2
   7  -2   2 11455.7 322.835   2
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   7  -2   2 11681.7 202.313   6
   7  -2   2 11198.0 197.519   5
   7  -2   3 18182.3 413.178   2
   7   2   3 18785.5 266.956  19
   7  -2   3 19093.4 277.439  19
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   7  -2   4 6281.51 270.430   2
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   7  -2   4 6500.93 161.890   5
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   7  -2   4 7632.22 182.699  19
   7  -2   5 31092.8 391.172   6
   7   2   5 30020.1 388.210  19
   7  -2   5 30513.1 398.850  19
   7  -2   6 2566.18 135.432   6
   7  -2   6 2543.86 131.090   5
   7   2   6 2821.87 132.165  19
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   7  -2   7 869.190 114.464   5
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   7  -2   8 554.806 103.900   5
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   7   2   8 438.569 100.618  19
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   7  -2  11 465.151 62.7340   6
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   7  -2  12 57.6586 40.5091   5
   7  -2  12 95.2658 43.9042   6
   7  -2  13 898.018 26.1308   6
   7  -2  13 1028.25 26.2467   5
   7   3 -18 72.4685 43.2537  20
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   7  -3 -17 1233.98 56.1826   3
   7   3 -17 1319.97 71.6416  20
   7  -3 -16-29.5302 65.1543   4
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   7  -3 -14 801.324 95.3374   3
   7  -3 -14 697.431 97.7763   4
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   7  -3 -13 2419.63 116.817   4
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   7   3 -11 9231.13 212.750  30
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   7   3  -9 23334.8 488.747   1
   7  -3  -9 23455.9 482.030   1
   7  -3  -9 25096.8 337.008   4
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   7  -3  -7 5721.46 189.595  25
   7  -3  -6 473.881 94.0757   3
   7  -3  -6 576.876 166.247   1
   7   3  -6 535.947 166.224   1
   7  -3  -6 516.016 94.0547   4
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   7  -3  -6 693.756 183.904  13
   7  -3  -5 1023.20 169.014   1
   7   3  -5 965.030 174.914   1
   7  -3  -5 1110.46 98.3720   3
   7   3  -5 1009.68 98.1549   3
   7  -3  -5 873.436 100.727   4
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   7   3  -5 776.878 186.485  13
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   7  -3  -4 7618.03 158.171   4
   7  -3  -4 7809.78 155.281   3
   7  -3  -4 8242.11 267.230   1
   7   3  -4 8458.41 270.371   1
   7   3  -3 1190.43 189.589  13
   7  -3  -3 1256.84 187.882  13
   7   3  -2 52230.4 767.330  13
   7  -3  -2 52563.7 769.711  13
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   7  -3  -1 109.226 165.174  13
   7  -3   0 313.170 159.102   2
   7  -3   0 289.994 157.978  13
   7  -3   1 6877.78 262.809   2
   7  -3   1 7565.01 257.656  13
   7  -3   2 29787.9 369.559   5
   7   3   2 30169.7 368.968   5
   7   3   2 28558.7 373.383   6
   7  -3   2 28595.2 376.329   6
   7   3   2 31102.7 402.746  23
   7  -3   2 29073.3 526.913   2
   7   3   2 30661.7 371.621  19
   7  -3   2 31175.9 385.391  19
   7   3   3 1497.74 187.484   2
   7  -3   3 1451.51 186.311   2
   7   3   3 966.803 112.516  19
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   7  -3   3 1163.65 120.835   6
   7  -3   3 1375.78 112.282   5
   7   3   3 1328.16 111.657   5
   7   3   4 19847.2 433.491   2
   7  -3   4 20326.6 432.498   2
   7   3   4 18843.7 277.734  19
   7  -3   4 19987.8 292.549  19
   7  -3   4 19933.1 278.941   5
   7   3   4 19750.3 276.922   5
   7  -3   4 19916.7 285.291   6
   7   3   5 3699.69 136.490  19
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   7  -3   5 3327.12 139.808   5
   7   3   5 3162.32 138.331   5
   7  -3   5 3431.41 139.704   6
   7   3   6 3816.81 136.412  19
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   7  -3   6 3980.43 139.890   5
   7  -3   6 3926.25 138.229   6
   7   3   7 3802.73 128.284  19
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   7  -3   7 3663.61 131.651   5
   7  -3   7 3706.04 139.676   6
   7   3   8 10203.9 175.959  19
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   7  -3   8 10465.5 181.159   5
   7  -3   8 10787.4 184.861   6
   7  -3   9 6949.56 139.475   5
   7  -3   9 6955.55 137.351   6
   7  -3  10 3070.70 100.190  19
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   7  -3  10 3219.14 96.6989   6
   7  -3  11 230.757 61.9328  19
   7  -3  11 237.425 57.0120   5
   7  -3  11 217.146 61.0236   6
   7  -3  12 1975.37 52.1292   5
   7  -3  12 1947.34 53.8274   6
   7   3  13 213.515 20.0593   5
   7  -3  13 226.692 20.0495   5
   7  -3  13 185.130 20.0466   6
   7   3  13 197.869 20.5407   6
   7  -4 -18 8171.18 110.825  20
   7   4 -18 7629.21 104.240  20
   7   4 -17 607.824 64.4095  20
   7   4 -17 599.154 50.7784   4
   7  -4 -17 638.134 52.2863   4
   7   4 -17 633.738 50.4814   3
   7  -4 -17 568.309 50.2503   3
   7   4 -16 3861.61 108.997  20
   7   4 -16 4008.15 95.1750   4
   7  -4 -16 4149.31 93.0424   4
   7   4 -16 4147.11 91.3950   3
   7  -4 -16 3999.93 91.3753   3
   7   4 -15 5851.90 122.060   4
   7  -4 -15 5593.55 123.349   4
   7   4 -15 5702.94 123.941   3
   7  -4 -15 5490.71 122.363   3
   7  -4 -15 5887.31 146.755  25
   7  -4 -15 6172.25 160.440  30
   7   4 -14 29258.5 348.443   3
   7  -4 -14 29030.9 347.446   3
   7   4 -14 29147.2 349.506   4
   7  -4 -14 29485.9 350.369   4
   7  -4 -14 27850.9 365.832  25
   7  -4 -14 27454.2 369.727  30
   7   4 -13 1648.03 111.325   3
   7  -4 -13 1622.78 110.761   3
   7   4 -13 1804.18 113.625   4
   7  -4 -13 1642.84 113.138   4
   7   4 -13 2002.23 155.072  25
   7  -4 -13 2005.26 157.158  25
   7  -4 -13 2158.51 146.135  30
   7   4 -12 6601.49 159.387   3
   7  -4 -12 6808.15 157.096   3
   7   4 -12 6581.17 165.595   4
   7  -4 -12 6781.08 160.553   4
   7   4 -12 9260.36 211.672  25
   7  -4 -12 9032.28 212.461  25
   7  -4 -12 10066.2 204.227  30
   7   4 -11 1573.86 115.781   4
   7  -4 -11 1517.44 117.920   4
   7   4 -11 1436.46 117.099   3
   7  -4 -11 1504.32 115.811   3
   7  -4 -11 2049.35 144.654  30
   7   4 -11 1966.95 171.353  25
   7  -4 -11 1965.48 166.060  25
   7   4 -10 1141.53 115.286   4
   7  -4 -10 1206.59 109.961   4
   7   4 -10 1184.03 109.916   3
   7  -4 -10 1101.84 108.180   3
   7  -4 -10 1335.26 167.482  13
   7  -4 -10 1803.04 135.276  29
   7   4 -10 1661.75 167.840  25
   7  -4 -10 1833.78 168.087  25
   7   4  -9 756.353 106.875   3
   7   4  -9 891.961 177.658   1
   7  -4  -9 933.514 174.649   1
   7   4  -9 831.227 115.744   4
   7  -4  -9 915.389 109.493   4
   7  -4  -9 873.970 107.732   3
   7  -4  -9 1232.38 183.463  13
   7  -4  -9 1857.15 146.111  29
   7   4  -9 1717.66 166.206  25
   7  -4  -9 1726.61 165.705  25
   7   4  -8 10475.6 319.268   1
   7  -4  -8 10756.4 318.188   1
   7   4  -8 10944.2 202.849   4
   7  -4  -8 10791.0 200.318   4
   7   4  -8 10274.4 197.361   3
   7  -4  -8 10448.7 195.405   3
   7  -4  -8 11946.6 331.929  13
   7  -4  -8 15428.6 244.631  29
   7   4  -8 15521.0 251.655  29
   7   4  -8 14178.8 253.973  25
   7   4  -7 4085.92 151.217  20
   7   4  -7 2944.75 122.636   3
   7  -4  -7 2892.64 120.174   3
   7   4  -7 3336.02 124.403   4
   7  -4  -7 3102.78 127.213   4
   7  -4  -7 3501.76 221.337  13
   7  -4  -7 3300.05 214.235   1
   7   4  -7 3370.26 219.569   1
   7   4  -7 4256.26 162.176  29
   7  -4  -7 4348.22 161.780  29
   7  -4  -7 3878.28 174.070  25
   7   4  -7 3891.38 177.263  25
   7  -4  -6 233.866 93.8654   3
   7   4  -6 214.634 96.0326   3
   7  -4  -6 287.678 159.558   1
   7   4  -6 358.409 164.233   1
   7   4  -6 199.582 95.8030   4
   7  -4  -6 227.661 97.4527   4
   7  -4  -6 186.397 171.174  13
   7   4  -6 223.687 165.108  13
   7  -4  -5 824.410 164.393   1
   7   4  -5 852.661 164.956   1
   7  -4  -5 928.873 96.9762   3
   7   4  -5 822.914 94.4479   3
   7   4  -5 885.569 99.5746   4
   7  -4  -5 828.920 98.3001   4
   7  -4  -5 1045.90 189.545  13
  -7   4   5 1025.83 151.350  14
   7   4  -5 1035.51 185.697  13
   7  -4  -4 1634.62 179.008   1
   7   4  -4 1695.75 182.354   1
   7  -4  -4 1893.48 99.8672   3
   7   4  -4 1874.75 100.076   3
   7   4  -4 1939.26 107.564   4
   7  -4  -4 1927.01 103.136   4
  -7   4   4 1991.08 172.333  14
  -7   4   3 8823.33 268.732  14
   7   4  -3 8582.99 297.466  13
   7  -4  -3 8617.44 296.538  13
  -7   4   2 26221.6 462.557  14
   7  -4  -2 26474.0 498.185  13
   7  -4  -1 2155.95 185.605   2
   7   4  -1 2061.96 179.154   2
   7  -4  -1 2308.02 194.185  13
   7  -4   0 1093.29 170.729   2
   7   4   0 1043.02 167.950   2
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   7  -4   1 1024.88 101.869   5
   7   4   1 1099.43 100.722   5
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   7  -4   1 688.468 156.803  13
   7  -4   1 980.975 106.973   6
   7   4   1 881.954 104.796   6
   7   4   2 14461.5 229.270  19
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   7  -4   2 16175.6 235.281   5
   7   4   2 16184.1 233.781   5
   7   4   2 13409.2 255.930  23
   7   4   2 17510.7 381.956   2
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   7   4   2 16435.4 239.508   6
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   7   5  11 4553.90 90.4070   6
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   7   6   2 75247.7 788.475   5
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   7   6   5 16589.1 240.662  19
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   7   6   5 16641.3 249.300   5
   7   6   6 66.6672 91.5341  19
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   7   6   6 86.6611 112.355   6
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   7   6   8 694.215 83.1181  19
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   7  -6   8 869.281 98.4533   5
   7   6   8 821.458 102.173   5
   7  -6   9 86.0476 97.3947  19
   7   6   9 128.028 84.9181   5
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   7  -6   9 177.197 86.3515   6
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   7  -6  10 8501.08 134.166   5
   7  -6  11 209.560 61.1471  19
   7   6  11 237.941 54.4001   5
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   7  -6  11 234.583 55.1710   6
   7  -6  11 319.799 53.6046   5
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   7   8   2 18159.5 263.536   6
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   7   8  10 887.675 71.5651   6
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   7   8  11 213.033 52.5660   6
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   7   8  12 3826.70 59.6791   6
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   7  -9 -15 1137.45 72.3106   4
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   7  -9 -15 1117.72 70.6805   3
   7   9 -15 1155.25 93.9664  20
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   7   9 -14 1173.34 84.7119   4
   7  -9 -14 1186.01 87.1515   4
   7   9 -14 1095.47 84.6801   3
   7  -9 -14 1131.19 84.7094   3
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   7   9 -13 41156.8 470.961   4
   7  -9 -13 41029.2 469.478   4
   7   9 -13 41331.8 470.159   3
   7  -9 -13 41287.3 468.112   3
   7  -9 -13 42790.6 502.968  25
   7   9 -13 43098.3 492.088  20
   7  -9 -13 43636.7 493.094  30
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   7  -9 -12 175.805 90.3089   4
   7  -9 -12 94.5336 144.839  25
   7   9 -12 166.066 95.3744   3
   7  -9 -12 131.849 92.5125   3
   7   9 -12 167.025 123.337  20
   7  -9 -12 130.184 120.864  30
   7  -9 -11 197.390 152.404  25
   7   9 -11 154.235 92.6012   3
   7  -9 -11 204.007 94.0240   3
   7   9 -11 338.444 126.568  20
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   7   9 -10 4268.95 129.610   3
   7  -9 -10 4387.96 126.509   3
   7   9 -10 3373.31 186.777  25
   7   9 -10 3901.38 157.729  20
   7  -9 -10 3384.22 147.581  29
   7   9  -9 1084.20 106.112   4
   7  -9  -9 887.102 101.819   4
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   8   0   7 60.3378 83.3240  19
   8   0   7 56.1851 89.4750   5
   8   0   7 0.91762 94.1207   6
   8   0   8 15950.0 206.092  19
   8   0   8 15998.5 208.511   5
   8   0   8 16371.6 212.456   6
   8   0   9-7.93569 64.2001   6
   8   0   9 22.1348 60.6586   5
   8   0  10 3718.25 71.5763   5
   8   0  10 3694.25 72.1083   6
   8   0  11 1.83340 26.2686   6
   8   0  11 10.4683 26.2386   5
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   8   1 -16 3343.43 75.5964   4
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   8  -1 -15 165.988 88.9519  20
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   8  -1 -15 147.314 64.2596   4
   8  -1 -14 233.835 75.4451   3
   8   1 -14 117.623 121.522  25
   8  -1 -14 116.685 118.873  25
   8   1 -14 360.059 104.669  20
   8   1 -14 256.005 76.4240   4
   8  -1 -14 297.599 77.4771   4
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   8  -1 -12 28139.9 394.682  25
   8  -1 -12 30083.6 390.206  20
   8  -1 -12 31710.3 366.341   3
   8   1 -12 30477.4 369.206   4
   8  -1 -12 31089.5 369.031   4
   8   1 -11 25381.6 364.622  25
   8  -1 -11 25276.0 364.729  25
   8   1 -11 24903.5 347.015  20
   8  -1 -11 24801.1 322.884   3
   8   1 -11 24527.9 325.302   4
   8  -1 -11 24824.9 325.725   4
   8  -1 -10 961.446 168.109  25
   8   1 -10 880.238 170.488  25
   8  -1 -10 1188.65 110.068   3
   8   1 -10 1094.46 112.721   4
   8  -1 -10 1229.36 112.490   4
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   8   1  -9 1714.55 124.029   4
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   8  -1  -9 2000.41 153.904  29
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   8  -1  -9 1863.34 140.816  20
   8   1  -8 542.637 146.214  29
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   8   1   8 2792.07 99.0212   6
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   8   1   9 1621.65 73.3802   6
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   8  -1  10 940.909 50.6145   6
   8   1  10 916.732 50.8139   6
   8  -1  10 868.029 49.0529   5
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   8  -1  11 161.145 26.9088   5
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   8  -2   8 239.526 79.4495   6
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   8  -3 -11 47432.0 537.420   4
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   8  -3  -7 50183.6 607.989  25
   8  -3  -7 50670.0 567.299   3
   8  -3  -7 51103.5 571.786   4
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   8  -3  -6 3171.05 121.052   3
   8  -3  -6 3111.76 124.621   4
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   8  -3  -3 1920.24 148.487  25
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   8  -3  -3 1737.28 117.655  20
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   8  -3   0 21383.8 300.810  19
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   8   3   0 22472.0 291.737   5
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   8  -3   0 20160.9 309.987  29
   8  -3   0 21534.6 435.049  13
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   8  -3   0 22925.6 298.493   6
   8  -3   1 15341.0 233.030   5
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   8  -3   2 747.116 119.043   6
   8  -3   2 851.318 126.799  19
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   8   3   2 981.301 109.905   5
   8  -3   3 6010.84 162.819   6
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   8  -3   3 6145.19 155.191   5
   8  -3   4 1455.37 123.353   6
   8   3   4 1750.18 113.690  19
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   8  -3   4 1595.23 119.404   5
   8  -3   5 15680.1 235.608   6
   8   3   5 15435.2 224.040  19
   8  -3   5 16052.4 241.888  19
   8  -3   5 15869.1 233.265   5
   8  -3   6 1751.54 104.562   6
   8   3   6 1219.33 94.6047  19
   8  -3   6 1310.89 111.647  19
   8  -3   6 1729.37 108.695   5
   8   3   7 364.475 78.2942  19
   8  -3   7 267.897 92.1880  19
   8  -3   7 348.247 83.1292   5
   8  -3   7 311.159 92.3899   6
   8  -3   8 77.8912 76.2140  19
   8  -3   8 92.3951 74.6688   6
   8  -3   8 131.699 73.5108   5
   8  -3   9 1006.17 67.0803   6
   8  -3   9 909.587 67.0813  19
   8  -3   9 1074.33 64.7715   5
   8  -3  10 6413.41 93.1793  19
   8  -3  10 6738.88 95.8060   5
   8   3  11 1788.89 37.1330   5
   8  -3  11 1726.22 36.7462   5
   8  -4 -18 910.867 29.2713  20
   8   4 -17 2652.62 66.4627  20
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   8   4 -16 289.486 66.6797  20
   8   4 -16 227.822 46.7736   4
   8  -4 -16 272.920 47.5112   4
   8   4 -16 299.175 45.9188   3
   8  -4 -16 228.631 45.3172   3
   8   4 -15 98.7297 62.2448   4
   8  -4 -15 73.3743 60.1794   4
   8  -4 -15 53.7522 56.7269   3
   8   4 -15 97.5451 57.4137   3
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   8   4 -14 2371.92 88.9801   3
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   8   4 -13 361.805 89.6783   4
   8  -4 -13 331.652 81.7958   4
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   8   4 -12 1260.19 101.917   3
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   8  -4 -11 301.679 98.9419   4
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   8   4   0 3279.43 139.883  20
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   8   4   1 228.310 108.634   6
   8  -4   1 208.016 109.363   5
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   8   4   2 796.428 111.997   5
   8  -4   2 871.950 112.932   6
   8   4   2 803.068 113.012   6
   8  -4   3 20979.5 297.520  19
   8   4   3 21305.8 285.110   5
   8  -4   3 20828.1 284.130   5
   8  -4   3 21103.3 288.551   6
   8   4   3 21225.1 288.954   6
   8   4   4 1532.72 107.586  19
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   8  -4   4 1522.76 110.791   5
   8  -4   4 1571.44 121.190   6
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   8  -4   5 6913.62 147.172   5
   8  -4   5 6599.75 155.456   6
   8   4   5 6546.78 156.528   6
   8   4   6 7780.16 144.986  19
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   8  -4   6 8627.13 157.497   5
   8  -4   6 8344.82 161.370   6
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   8   4   7 12302.9 185.095   5
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   8  -4   7 12771.6 185.548   6
   8   4   7 12581.9 186.319   6
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   8   4   8 1378.12 81.7616   5
   8  -4   8 1297.80 79.6010   5
   8   4   8 1310.46 82.2628   6
   8  -4   8 1294.11 79.9959   6
   8   4   9 1572.70 66.7096   5
   8  -4   9 1517.48 65.3601   5
   8  -4   9 1538.84 68.2366   6
   8   4   9 1459.35 69.6937   6
   8  -4  10 409.522 43.2085  19
   8   4  10 504.329 45.8849   5
   8  -4  10 517.516 44.4973   5
   8  -4  10 540.936 45.6125   6
   8   4  10 507.565 46.4691   6
   8   4  11 1249.01 30.8767   5
   8  -4  11 1226.94 30.4137   5
   8  -4  11 1066.25 30.4720   6
   8   4  11 1063.87 31.3787   6
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   8  -5 -16 3095.85 68.5281   4
   8  -5 -16 3007.09 66.6645   3
   8   5 -16 2998.25 66.3429   3
   8   5 -16 3007.01 89.2869  22
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   8   5 -15 164.806 55.0509   3
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   8  -5 -15 139.741 59.3124   4
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   8   5 -14 7973.37 134.750   3
   8   5 -14 7871.52 137.118   4
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   8   5 -13 644.768 84.2982   3
   8   5 -13 534.034 88.1414   4
   8  -5 -13 605.364 83.2626   4
   8   5 -12 22463.9 329.459  25
   8  -5 -12 22761.5 328.516  25
   8   5 -12 23385.7 316.501  20
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   8   5 -12 21881.4 283.717   3
   8   5 -12 21542.6 287.356   4
   8  -5 -12 22008.4 285.544   4
   8  -5 -11 12759.6 263.339  25
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   8   5 -11 13921.6 242.993  20
   8  -5 -11 14111.3 244.798  20
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   8   5 -11 15080.1 222.837   3
   8   5 -11 15024.5 226.134   4
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   8   5 -10 13224.0 259.943  25
   8  -5 -10 13548.6 258.651  25
   8  -5 -10 13236.6 232.224  20
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   8   5 -10 11843.0 201.190   3
   8   5 -10 11821.4 202.859   4
   8  -5 -10 11700.7 203.685   4
   8  -5  -9 10198.3 220.410  29
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   8   5  -8 4536.61 137.553   3
   8   5  -8 4570.03 137.720   4
   8  -5  -8 4293.13 137.624   4
   8  -5  -7 17110.2 287.315  29
   8   5  -7 16732.3 288.583  29
   8  -5  -7 16123.6 236.741   3
   8   5  -7 16132.9 239.934   3
   8   5  -7 15576.7 246.935   4
   8  -5  -7 15779.8 239.647   4
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   8   5  -7 16711.5 267.500  22
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   8  -5  -6 28667.6 402.999  29
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   8   5  -6 28271.0 407.675  25
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   8   5  -6 30587.0 403.751  20
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   8   5  -6 29710.6 365.770   3
   8   5  -6 30350.6 368.997   4
   8  -5  -6 29332.6 365.967   4
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   8   5  -1 29933.1 359.110   5
   8  -5  -1 30366.4 363.638   5
   8   5  -1 28116.5 377.726  29
   8  -5  -1 28189.8 393.068  29
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   8   5  -1 27985.6 386.333  20
   8   5  -1 28651.6 355.744  19
   8  -5  -1 29632.9 367.683   6
   8   5  -1 29812.3 362.625   6
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   8  -5   0 5234.05 143.515   5
   8   5   0 4605.91 150.852  29
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   8   5   0 5010.38 145.233   6
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   8  -5   1 9734.12 188.213   5
   8  -5   1 9980.57 187.368   6
   8   5   1 9626.09 185.222   6
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   8  -5   2 2040.00 124.060   5
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   8  -5   3 629.626 112.911   5
   8  -5   3 661.490 110.992   6
   8   5   4 10520.0 180.772  19
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   8   5   4 11373.9 193.709   5
   8  -5   4 11072.7 192.992   5
   8  -5   4 11217.2 192.821   6
   8   5   4 11277.2 194.489   6
   8   5   5 10112.7 171.869  19
   8  -5   5 10039.0 195.505  19
   8   5   5 11349.0 186.698   5
   8  -5   5 11035.7 184.607   5
   8  -5   5 11187.9 189.057   6
   8   5   5 11432.7 192.425   6
   8   5   6 158.998 78.4375  19
   8  -5   6 65.2032 104.755  19
   8   5   6 61.4737 89.0104   5
   8  -5   6 88.0713 87.2164   5
   8  -5   6 59.6254 96.8711   6
   8   5   6 76.5347 99.5671   6
   8  -5   7 452.959 94.3951  19
   8   5   7 681.910 89.0335   5
   8  -5   7 626.259 86.4730   5
   8  -5   7 584.201 84.2647   6
   8   5   7 577.262 86.5532   6
   8  -5   8 894.608 81.0650  19
   8   5   8 1028.16 77.3369   5
   8  -5   8 1013.68 75.5613   5
   8  -5   8 941.378 76.7586   6
   8   5   8 1078.25 79.7722   6
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   8   5   9 5791.37 99.8949   5
   8  -5   9 5847.18 98.6376   5
   8  -5   9 6004.18 101.126   6
   8   5   9 6065.36 103.358   6
   8  -5  10 1751.65 55.4784  19
   8   5  10 1857.79 53.1094   5
   8  -5  10 1878.65 51.9225   5
   8  -5  10 1875.10 53.1120   6
   8   5  10 2003.71 55.1307   6
   8  -5  11 62.4501 21.2199   6
   8   5  11 68.8933 22.7976   6
   8   5  11 78.0213 21.3315   5
   8  -5  11 68.6822 20.8897   5
   8   6 -17 729.145 48.9760  22
   8   6 -17 582.608 45.8883  20
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   8   6 -16 107.333 41.1342   3
   8   6 -16 166.980 61.2010  20
   8  -6 -16 234.404 66.7656  20
   8   6 -16 235.729 67.8036  22
   8   6 -16 98.7653 43.4230   4
   8  -6 -16 107.609 42.6412   4
   8  -6 -15 3351.21 106.060  20
   8   6 -15 3130.76 103.846  20
   8  -6 -15 3521.36 81.5656   3
   8   6 -15 3511.10 82.1485   3
   8   6 -15 3362.55 84.0811   4
   8  -6 -15 3590.77 83.5876   4
   8  -6 -15 2979.81 110.111  25
   8  -6 -14 251.397 68.7137   3
   8   6 -14 216.321 68.7854   3
   8  -6 -14 191.144 115.901  25
   8  -6 -14 300.368 99.4336  20
   8   6 -14 260.463 100.264  20
   8   6 -14 187.248 73.1694   4
   8  -6 -14 253.174 67.7701   4
   8  -6 -13 4670.10 165.591  25
   8   6 -13 4659.93 147.471  20
   8  -6 -13 5289.57 118.721   3
   8   6 -13 5274.89 118.795   3
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   8   6 -12 6345.51 142.036   4
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   8   6 -11 11879.4 244.515  25
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   8  -6 -11 10971.3 186.040   3
   8   6 -11 10608.7 187.116   3
   8   6 -11 10992.9 191.247   4
   8  -6 -11 10961.6 186.640   4
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   8   6 -10 14258.2 216.578   3
   8   6 -10 13966.6 220.481   4
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   8  -6  -9 560.762 99.2522   4
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   8  -6   0 658.489 104.619   5
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   8   6   0 774.650 112.906   6
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   8   6   2 2733.37 124.787   5
   8  -6   2 2751.83 125.507   5
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   8  -6   4 702.627 124.931  19
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   8   6   4 861.933 110.017   5
   8  -6   4 832.892 108.486   5
   8  -6   4 876.187 106.423   6
   8   6   5 29654.8 348.263  19
   8  -6   5 30621.7 377.246  19
   8   6   5 29609.4 359.388   5
   8  -6   5 29329.9 357.837   5
   8  -6   5 30343.7 363.015   6
   8   6   5 30597.4 365.400   6
   8   6   6 5202.86 124.829   5
   8  -6   6 5197.19 123.467   5
   8  -6   6 5032.27 129.775   6
   8   6   6 4935.28 132.113   6
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   8  -6   7 3380.58 104.766   5
   8  -6   7 3595.27 102.772   6
   8   6   7 3478.67 105.479   6
   8  -6   8 108.327 77.1750  19
   8  -6   8 99.1198 67.3469   6
   8   6   8 42.3319 69.0210   6
   8   6   8 40.8265 68.9997   5
   8  -6   8 50.9342 67.2414   5
   8  -6   9 1732.67 72.8470  19
   8   6   9 1708.33 66.3090   5
   8  -6   9 1736.97 64.7302   5
   8  -6   9 1617.67 65.7720   6
   8   6   9 1689.82 68.2206   6
   8  -6  10 1757.23 49.7382   6
   8   6  10 1786.22 52.4474   6
   8   6  10 1880.54 50.4726   5
   8  -6  10 1942.94 49.7143   5
   8  -6  11 217.089 19.9211   6
   8   6  11 223.583 21.2052   6
   8   6  11 219.184 20.1824   5
   8  -6  11 206.457 19.2840   5
   8   7 -17 94.1592 37.6872  20
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   8   7 -16 8715.86 112.272   3
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   8   7 -15 687.368 57.6119   3
   8   7 -15 671.011 59.2373   4
   8  -7 -15 645.381 57.4633   4
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   8   7 -15 953.543 89.5405  22
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   8   7 -14 3306.86 88.4560   3
   8   7 -14 3194.45 94.2775   4
   8  -7 -14 3298.48 91.8546   4
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   8  -7 -13 1615.67 82.6628   3
   8   7 -13 1623.24 84.8590   3
   8   7 -13 1584.82 92.3763   4
   8  -7 -13 1623.03 88.6209   4
   8   7 -13 1652.11 121.628  20
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   8   7 -12 10081.1 169.195   3
   8   7 -12 9919.21 169.034   4
   8  -7 -12 10033.5 169.096   4
   8   7 -12 9449.22 193.902  20
   8  -7 -11 501.742 92.4360   3
   8   7 -11 457.978 92.0804   3
   8   7 -11 379.074 132.702  20
   8   7 -11 421.942 98.4216   4
   8  -7 -11 488.179 89.4795   4
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   8   7 -10 2916.90 149.233  20
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   8   7 -10 3199.62 119.686   3
   8   7 -10 3150.35 117.266   4
   8  -7 -10 3163.08 120.888   4
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   8   7  -9 3505.02 158.459  22
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   8   7  -9 3966.33 132.967   4
   8  -7  -9 4091.43 125.431   4
   8  -7  -9 4194.19 121.849   3
   8   7  -9 4235.04 125.752   3
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   8   7  -8 730.352 103.807   3
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   8  -7  -7 198.820 90.8636   3
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   8  -7  -7 72.3434 97.7029   4
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   8  -7  -6 1633.46 113.021   4
   8  -7  -5 2753.27 163.214  29
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   8   7  -4 27093.3 372.838  22
   8  -7  -4 27960.8 377.815  25
   8   7  -4 27533.8 381.201  20
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   8  -7  -2 25927.2 329.391   5
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   8   7  -1 1068.45 127.695  26
   8   7  -1 1243.48 138.416  20
   8   7  -1 1366.13 101.438  19
   8   7   0 27327.0 341.883   5
   8  -7   0 27269.4 345.255   5
   8  -7   0 27079.4 346.489   6
   8   7   0 26916.4 345.312   6
   8  -7   0 28401.4 374.632  29
   8   7   0 28011.6 357.098  29
   8   7   0 26929.8 362.757  23
   8   7   0 26445.7 372.010  20
   8   7   0 27391.3 334.581  19
   8   7   1 8820.70 161.275  19
   8   7   1 8025.41 169.700   5
   8  -7   1 7896.11 171.872   5
   8  -7   1 8785.21 195.266  19
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   8   7   1 9498.13 198.918  23
   8  -7   1 8406.22 171.523   6
   8   7   1 8285.86 171.289   6
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   8  -7   2 822.771 110.872   5
   8  -7   2 981.620 109.309   6
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   8   7   3 4534.81 121.028  19
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   8  -7   3 4780.61 138.256   5
   8  -7   3 4806.19 138.234   6
   8   7   3 5026.82 139.069   6
   8   7   4 134.910 83.7672  19
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   8  -7   4 273.636 104.244   6
   8   7   4 219.978 104.528   6
   8   7   4 275.449 99.1985   5
   8  -7   4 261.215 99.9631   5
   8   7   5 11544.3 181.981   5
   8  -7   5 11297.8 179.860   5
   8  -7   5 10935.4 187.158   6
   8   7   5 10992.3 189.530   6
   8  -7   6 15978.5 237.482  19
   8   7   6 16554.4 224.110   5
   8  -7   6 16499.1 221.820   5
   8  -7   6 16049.8 224.283   6
   8   7   6 16149.3 227.430   6
   8  -7   7 1204.25 97.0351  19
   8   7   7 1256.25 85.8111   5
   8  -7   7 1266.38 82.3988   5
   8  -7   7 1249.48 86.7745   6
   8   7   7 1235.98 89.6197   6
   8  -7   8 235.993 78.3059  19
   8  -7   8 213.073 68.6855   6
   8   7   8 254.485 71.3407   6
   8   7   8 238.641 65.0716   5
   8  -7   8 214.665 63.5670   5
   8  -7   9 676.182 65.2564  19
   8   7   9 594.328 55.6581   5
   8  -7   9 569.801 54.3338   5
   8  -7   9 554.441 55.8889   6
   8   7   9 590.609 58.6499   6
   8  -7  10 121.715 43.8161  19
   8  -7  10 149.029 37.4651   6
   8   7  10 138.420 39.6434   6
   8   7  10 128.054 36.4164   5
   8  -7  10 151.005 35.9307   5
   8   8 -17 5611.40 82.0807  20
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   8   8 -16 489.814 42.4174   4
   8  -8 -16 851.893 64.5284  20
   8   8 -16 747.849 61.2064  20
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   8  -8 -15 333.424 79.4811  20
   8  -8 -15 312.430 52.3313   3
   8   8 -15 250.351 54.5797   4
   8  -8 -15 257.379 53.0966   4
   8   8 -15 328.061 51.8351   3
   8  -8 -15 157.766 88.2070  25
   8   8 -14 320.169 94.1907  20
   8  -8 -14 406.161 94.0762  20
   8  -8 -14 275.542 64.8331   3
   8   8 -14 255.717 65.2142   3
   8   8 -14 400.741 65.8236   4
   8  -8 -14 290.451 63.5450   4
   8  -8 -14 229.338 111.769  25
   8   8 -13 660.889 111.226  20
   8  -8 -13 433.976 74.3733   3
   8   8 -13 446.389 76.7504   3
   8  -8 -13 778.181 136.444  25
   8  -8 -13 407.197 75.5325   4
   8   8 -13 500.521 76.7220   4
   8  -8 -12 4758.31 169.905  25
   8  -8 -12 3620.14 108.999   3
   8   8 -12 3520.75 109.693   3
   8   8 -12 3676.89 114.827   4
   8  -8 -12 3684.09 107.725   4
   8   8 -12 4526.01 152.788  20
   8  -8 -11 734.660 118.539  29
   8  -8 -11 677.240 156.790  25
   8   8 -11 308.308 94.7855   4
   8  -8 -11 288.456 91.3445   4
   8   8 -11 553.675 128.303  20
   8  -8 -11 313.009 87.6325   3
   8   8 -11 276.562 88.4678   3
   8  -8 -10 128.535 91.1726   3
   8   8 -10 76.0356 91.7632   3
   8  -8 -10 98.9843 156.441  25
   8   8 -10-43.1935 97.9551   4
   8  -8 -10 69.4763 88.8815   4
   8   8 -10 217.605 128.110  22
   8  -8 -10 220.523 118.965  20
   8   8 -10 68.1044 133.133  20
   8  -8 -10 155.359 130.381  29
   8  -8  -9 310.216 93.9506   3
   8   8  -9 296.139 97.4169   3
   8  -8  -9 778.570 137.152  29
   8   8  -9 509.657 133.341  20
   8   8  -9 660.805 136.909  22
   8  -8  -9 571.341 112.794  20
   8   8  -9 313.723 100.994   4
   8  -8  -9 342.695 99.0928   4
   8   8  -9 574.009 168.996  25
   8  -8  -8 1548.59 123.379  20
   8   8  -8 1529.57 133.533  22
   8  -8  -8 1291.35 154.592  29
   8  -8  -8 1844.35 103.523   3
   8   8  -8 1797.34 104.969   3
   8   8  -8 1697.27 115.053   4
   8  -8  -8 1809.90 105.627   4
   8  -8  -8 1389.97 172.528  25
   8   8  -7 2710.28 151.626  22
   8  -8  -7 2636.37 122.133  20
   8   8  -7 2628.17 186.825  25
   8  -8  -7 2849.70 180.813  25
   8  -8  -7 2219.14 111.798   3
   8   8  -7 2199.00 114.785   3
   8   8  -7 2421.60 115.275   4
   8  -8  -7 2240.52 114.786   4
   8  -8  -7 2888.07 169.458  29
   8  -8  -6 230.733 105.931  20
   8   8  -6 61.8514 129.127  22
   8   8  -6 42.8579 143.803  20
   8   8  -6 290.492 105.366   4
   8  -8  -6 343.710 97.8979   4
   8  -8  -6-121.624 142.300  29
   8   8  -6-110.978 166.191  25
   8  -8  -6 135.948 151.770  25
   8   8  -5 454.895 130.608  22
   8   8  -5 495.447 141.803  20
   8  -8  -5 533.257 116.551  19
   8  -8  -5 572.692 154.880  29
   8  -8  -5 442.148 150.584  25
   8  -8  -4 82.9485 111.533  19
   8   8  -4 16.3299 140.336  29
   8  -8  -4 121.922 175.453  13
   8   8  -4-39.5496 124.495  22
   8   8  -4 141.246 139.057  20
   8  -8  -4 82.8719 138.085  25
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   8 -10   6 7329.27 132.714   5
   8 -10   7 82.8477 69.8022   6
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   8  10   7 114.878 69.8010   5
   8 -10   7 76.6568 67.3625   5
   8 -10   8 1096.41 62.9690   6
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   8 -11 -13 4363.51 99.5134   4
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   8  11 -11 14048.3 233.519  22
   8  11 -11 13321.7 219.679  20
   8 -11 -10 2997.54 99.7504   3
   8  11 -10 2963.69 103.158   3
   8  11 -10 2845.75 112.106   4
   8 -11 -10 2875.75 106.099   4
   8 -11 -10 2772.24 175.789  25
   8 -11 -10 2898.68 141.407  29
   8 -11 -10 2941.97 124.369  20
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   8  11 -10 2855.78 147.566  20
   8 -11  -9 3847.08 159.370  29
   8 -11  -9 3511.55 127.919  20
   8  11  -9 3708.23 152.959  22
   8  11  -9 3500.30 162.894  20
   8 -11  -9 2865.03 107.975   3
   8  11  -9 2806.84 109.691   3
   8  11  -9 3001.00 110.603   4
   8 -11  -9 3015.46 105.891   4
   8 -11  -8 2263.01 99.1959   3
   8  11  -8 2253.83 105.160   3
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   8 -11  -8 2064.21 105.721   4
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   8 -11  -8 2413.64 160.499  29
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   8 -11  -7 8696.02 154.538   4
   8 -11  -7 6469.61 194.612  29
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   8 -11  -6 6217.06 198.610  29
   8  11  -6 6629.80 188.775  22
   8 -11  -6 6471.48 204.258  25
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   8  11   0 6775.31 140.602   5
   8 -11   0 6924.12 146.104   5
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   8  11   1 1291.96 99.9066   5
   8 -11   1 1243.67 102.975   5
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   8  11   2 3419.08 117.881   5
   8 -11   2 3475.85 118.674   5
   8 -11   2 3456.19 141.881  19
   8  11   2 2953.23 150.088  23
   8 -11   2 3308.35 120.026   6
   8  11   2 3391.09 121.213   6
   8  11   3 16448.9 273.384  23
   8  11   3 17231.3 234.413   5
   8 -11   3 17154.7 234.544   5
   8 -11   3 16749.6 260.568  19
   8 -11   3 16856.2 233.739   6
   8  11   3 16630.4 236.592   6
   8  11   4 11915.1 186.013   5
   8 -11   4 12153.5 185.903   5
   8 -11   4 11979.9 210.380  19
   8 -11   4 11956.3 183.427   6
   8  11   4 11716.9 185.823   6
   8  11   5 1156.63 87.4054   5
   8 -11   5 1046.19 85.6788   5
   8 -11   5 1250.60 116.345  19
   8 -11   5 1068.96 91.1267   6
   8  11   5 1170.02 93.8264   6
   8  11   6 5835.61 117.325   5
   8 -11   6 5798.77 115.380   5
   8 -11   6 5576.34 114.158   6
   8  11   6 5439.66 118.278   6
   8 -11   7 70.4276 64.0532   6
   8  11   7 71.9311 67.5805   6
   8  11   7 41.6887 65.4622   5
   8 -11   7 95.6287 63.4475   5
   8  11   8 983.229 59.7516   5
   8 -11   8 1045.93 58.2511   5
   8 -11   8 1012.57 59.0538   6
   8  11   8 1056.78 61.2803   6
   8 -11   9 2055.58 50.8049   5
   8 -11   9 1979.22 52.4126   6
   8  11   9 1970.25 54.5417   6
   8 -11  10 2321.50 37.9526   5
   8 -11  10 2307.54 37.9180   6
   8  12 -17 382.758 34.4604  22
   8 -12 -17 400.481 28.7489  20
   8 -12 -16 215.484 48.9423  25
   8 -12 -16 334.545 47.7193  20
   8  12 -16 386.404 55.9238  22
   8  12 -16 372.143 41.4870  20
   8 -12 -15 1865.91 88.4880  25
   8 -12 -15 1765.32 49.8794   3
   8  12 -15 1804.26 53.1556   4
   8 -12 -15 1692.94 51.2463   4
   8 -12 -15 1991.84 76.7869  20
   8  12 -15 2009.33 87.1598  22
   8  12 -15 1855.75 73.6044  20
   8 -12 -14 2867.74 117.157  25
   8 -12 -14 2306.63 66.2743   3
   8  12 -14 2215.65 66.0984   3
   8  12 -14 2214.76 69.3996   4
   8 -12 -14 2257.63 67.1825   4
   8 -12 -14 2895.78 95.9966  20
   8  12 -14 2750.00 97.0641  20
   8  12 -13 331.539 61.8778   4
   8 -12 -13 345.382 62.6286   4
   8  12 -13 397.207 98.2728  20
   8 -12 -13 275.539 59.8156   3
   8  12 -13 293.970 59.3559   3
   8 -12 -13 529.453 124.279  25
   8 -12 -12 2150.74 84.5938   3
   8  12 -12 2208.16 86.2543   3
   8  12 -12 2390.01 86.9751   4
   8 -12 -12 2415.88 84.6351   4
   8 -12 -11 408.002 74.1975   3
   8  12 -11 369.453 72.5709   3
   8 -12 -11 151.101 101.027  29
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   8 -12 -11 316.083 77.6557   4
   8  12 -11 162.850 119.035  20
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   8 -12 -11 191.545 101.403  20
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   8 -12 -10 204.636 119.549  29
   8  12 -10 13.5144 121.810  20
   8 -12 -10 109.851 97.8087  20
   8  12 -10 248.499 127.599  22
   8 -12 -10 174.472 79.4841   3
   8  12 -10 150.361 81.1559   3
   8  12 -10 134.986 85.1020   4
   8 -12 -10 138.515 81.0702   4
   8 -12  -9 54.2221 122.979  29
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   8 -12  -9 100.423 98.6698  20
   8  12  -9 145.745 126.580  22
   8  12  -9 77.9244 83.5947   4
   8 -12  -9 65.7193 84.8880   4
   8 -12  -9 119.921 81.6766   3
   8  12  -9 105.035 80.4563   3
   8 -12  -8 852.294 166.461  25
   8 -12  -8 815.633 140.741  29
   8 -12  -8 977.345 99.7478  20
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   8  12  -8 880.726 146.732  20
   8 -12  -8 1726.19 95.8017   3
   8  12  -8 1530.40 96.9382   3
   8  12  -8 1614.74 103.188   4
   8 -12  -8 1641.73 96.1247   4
   8 -12  -7 2300.96 161.034  29
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   8 -12  -6 504.726 151.868  29
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   8  12  -6 335.825 138.122  20
   8 -12  -5 1032.73 151.999  29
   8  12  -5 669.666 142.274  22
   8 -12  -5 748.269 149.477  25
   8 -12  -4 17693.3 285.934  25
   8  12  -4 17701.2 296.583  22
   8 -12  -3 89.1309 120.000  19
   8 -12  -3 224.229 129.057  25
   8  12  -3 62.4650 139.591  22
   8  12  -3 107.019 136.369  20
   8  12  -3 165.714 112.918  26
   8  12  -2 2419.44 142.669  26
   8 -12  -2 2527.24 172.293  29
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   8 -12  -2 2284.61 134.341  19
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   8 -12  -1 2048.60 131.511  19
   8 -12  -1 2230.62 162.233  29
   8  12  -1 1887.56 101.089   5
   8 -12  -1 1732.20 106.097   5
   8  12  -1 1984.41 145.594  26
   8  12  -1 1833.33 124.439  23
   8 -12  -1 1937.85 113.283   6
   8  12  -1 1957.79 104.211   6
   8 -12   0 1472.10 130.636  19
   8 -12   0 1366.87 158.615  29
   8  12   0 1288.02 148.281  26
   8  12   0 1981.63 102.239   5
   8 -12   0 1957.88 106.223   5
   8  12   0 1405.11 128.873  23
   8 -12   0 1839.74 109.970   6
   8  12   0 1907.19 107.931   6
   8 -12   1 351.676 92.9108   6
   8  12   1 392.815 97.2554   6
   8  12   1 344.162 94.2925   5
   8 -12   1 309.610 96.3589   5
   8 -12   1 474.157 142.187  29
   8  12   1 351.567 144.308  26
   8  12   1 440.661 127.330  23
   8 -12   1 414.844 128.027  19
   8 -12   2 5499.62 156.776  19
   8 -12   2 5605.00 170.471  29
   8 -12   2 5128.11 127.556   6
   8  12   2 4944.77 130.809   6
   8  12   2 5286.95 167.727  23
   8  12   2 4937.51 127.571   5
   8 -12   2 4807.94 128.182   5
   8 -12   3 60.4364 89.2587   6
   8  12   3 101.836 89.3724   6
   8  12   3 57.7530 89.8636   5
   8 -12   3 23.0404 90.6675   5
   8 -12   3 135.600 118.469  29
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   8 -12   3 80.7230 119.851  19
   8 -12   4 17635.0 234.120   6
   8  12   4 18028.9 235.765   6
   8  12   4 17804.8 231.796   5
   8 -12   4 17817.8 231.825   5
   8 -12   5 99.2498 106.836  19
   8 -12   5 82.7812 79.6979   6
   8  12   5 103.067 82.7334   6
   8  12   5 57.2126 79.5354   5
   8 -12   5 40.6443 77.9509   5
   8 -12   6 9332.07 144.972   6
   8  12   6 9551.97 148.320   6
   8 -12   6 9378.37 166.716  19
   8  12   6 9310.15 143.837   5
   8 -12   6 9416.17 142.258   5
   8 -12   7 374.508 85.0408  19
   8 -12   7 315.019 62.5203   6
   8  12   7 286.424 65.1863   6
   8  12   7 315.081 62.4851   5
   8 -12   7 332.664 61.3632   5
   8 -12   8 96.5948 69.2330  19
   8 -12   8 57.5607 49.4362   6
   8  12   8 49.1639 50.9740   6
   8  12   8 42.7504 49.8372   5
   8 -12   8 21.5293 48.7666   5
   8 -12   9 458.761 38.8224   6
   8 -12   9 493.364 37.1101   5
   8  13 -17 38.1100 28.2657  22
   8 -13 -16 221.193 45.6248  20
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   8  13 -16 231.989 36.4023  20
   8 -13 -15 440.630 60.3145  20
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   8  13 -15 290.638 56.6688  20
   8 -13 -15 356.865 75.1223  25
   8 -13 -14 5252.90 86.4664   3
   8  13 -14 5002.71 86.0241   3
   8  13 -14 5032.30 88.8610   4
   8 -13 -14 5276.02 86.5584   4
   8 -13 -14 4724.36 108.715  20
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   8 -13 -13 1214.30 63.6893   3
   8  13 -13 1118.27 63.3732   3
   8  13 -13 1164.87 67.3678   4
   8 -13 -13 1203.95 64.6722   4
   8  13 -13 1156.74 98.5403  20
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   8 -13 -13 1248.13 124.661  25
   8 -13 -12 24202.0 276.130   3
   8  13 -12 24000.2 277.626   3
   8  13 -12 23762.1 280.681   4
   8 -13 -12 23294.7 275.588   4
   8 -13 -12 22962.8 325.625  25
   8 -13 -12 22791.9 297.298  20
   8  13 -12 23451.8 308.138  20
   8 -13 -11 779.918 75.2939   3
   8  13 -11 857.457 77.3177   3
   8  13 -11 810.511 82.8052   4
   8 -13 -11 829.951 72.7366   4
   8 -13 -11 1268.09 153.731  25
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   8 -13 -11 1103.56 100.816  20
   8  13 -11 998.868 115.454  20
   8 -13 -10 12726.7 225.517  29
   8 -13 -10 13184.7 214.039  20
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   8  13 -10 13766.1 237.985  20
   8 -13 -10 14718.4 198.020   3
   8  13 -10 14731.8 199.393   3
   8  13 -10 14541.1 202.317   4
   8 -13 -10 14601.6 200.090   4
   8 -13  -9 2610.62 96.6662   3
   8  13  -9 2545.25 99.4306   3
   8  13  -9 2426.07 103.002   4
   8 -13  -9 2516.37 97.1163   4
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   8 -13  -8 7675.75 154.773  20
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   8  13  -8 8073.01 200.979  20
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   8 -13  -8 7292.58 145.077   4
   8 -13  -7 777.244 139.588  29
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   8 -13  -5 259.799 156.024  29
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   8  13  -4 23762.6 336.448  26
   8 -13  -4 26032.3 363.719  29
   8 -13  -4 24862.0 347.869  25
   8  13  -4 25176.1 363.212  22
   8 -13  -4 24694.1 329.976  19
   8 -13  -3 23.8800 120.914  19
   8 -13  -3 110.762 127.815  25
   8  13  -3 88.3120 112.284  26
   8  13  -3-109.323 141.546  22
   8 -13  -2 387.042 158.137  29
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   8  13  -2 194.406 144.575  20
   8 -13  -1 235.765 119.762  19
   8 -13  -1 298.388 92.6140   6
   8  13  -1 294.430 94.9305   6
   8 -13  -1 249.118 151.683  29
   8  13  -1 83.0800 133.327  26
   8  13  -1 167.857 112.275  23
   8  13  -1 91.3455 137.937  20
   8 -13   0 1623.12 130.654  19
   8 -13   0 1568.54 160.352  29
   8  13   0 1575.42 99.7167   5
   8 -13   0 1590.55 104.680   5
   8  13   0 1478.21 146.519  26
   8  13   0 1398.50 130.927  23
   8 -13   0 1584.30 105.952   6
   8  13   0 1688.36 103.872   6
   8 -13   1 11325.5 217.418  19
   8 -13   1 11446.7 233.827  29
   8  13   1 12110.9 183.503   5
   8 -13   1 12062.5 186.390   5
   8  13   1 10706.3 236.412  26
   8  13   1 11333.2 222.296  23
   8 -13   1 12049.5 190.384   6
   8  13   1 12140.0 185.658   6
   8 -13   2 5508.76 159.400  19
   8 -13   2 4646.82 169.245  29
   8  13   2 6512.27 130.022   5
   8 -13   2 6580.33 131.883   5
   8  13   2 5020.09 170.050  23
   8 -13   2 6207.83 136.802   6
   8  13   2 6247.81 134.689   6
   8 -13   3 20.5580 85.5993   6
   8  13   3 39.1540 88.3171   6
   8  13   3 62.1037 82.6045   5
   8 -13   3 83.9626 83.1244   5
   8 -13   3 66.0026 116.807  29
   8  13   3 61.2269 131.101  23
   8 -13   3 40.9520 119.113  19
   8 -13   4 1692.63 110.361  29
   8 -13   4 1721.09 117.087  19
   8  13   4 1637.74 138.057  23
   8 -13   4 1522.11 88.0322   6
   8  13   4 1481.65 93.6636   6
   8  13   4 1432.79 91.5669   5
   8 -13   4 1384.90 89.9755   5
   8 -13   5 1370.36 115.272  19
   8 -13   5 1586.86 85.1889   6
   8  13   5 1616.16 87.0888   6
   8  13   5 1616.70 83.1554   5
   8 -13   5 1523.58 82.4628   5
   8 -13   6 343.363 96.8537  19
   8 -13   6 481.204 69.1338   6
   8  13   6 489.476 71.1528   6
   8 -13   6 525.382 69.1330   5
   8  13   6 457.875 70.3976   5
   8 -13   7 213.862 80.7797  19
   8 -13   7 113.649 57.1366   6
   8  13   7 188.827 60.5526   6
   8  13   7 155.291 58.0975   5
   8 -13   7 122.230 56.1402   5
   8 -13   8 919.993 71.1778  19
   8 -13   8 893.112 48.9991   6
   8 -13   8 845.325 48.6368   5
   8 -13   9 329.405 52.8765  19
   8 -13   9 320.429 31.3408   6
   8 -13   9 331.208 32.1335   5
   8 -13  10 158.064 32.0713  19
   8  14 -17 1147.75 31.8314  22
   8  14 -16 727.950 54.1543  22
   8  14 -16 614.013 31.3156  20
   8 -14 -15 2.47856 70.4204  25
   8 -14 -15 57.9370 55.6312  20
   8  14 -15 67.6947 67.3097  22
   8  14 -15 114.115 52.4712  20
   8 -14 -14 497.891 43.7865   3
   8 -14 -14 446.951 43.6860   4
   8 -14 -14 404.248 95.1432  25
   8  14 -14 452.104 86.6033  22
   8 -14 -14 382.684 68.4666  20
   8  14 -14 276.466 71.5196  20
   8 -14 -13 1445.39 60.1976   3
   8  14 -13 1359.26 59.3985   3
   8  14 -13 1380.59 63.7915   4
   8 -14 -13 1373.16 61.3502   4
   8 -14 -13 1514.02 122.672  25
   8 -14 -13 1394.17 87.8409  20
   8  14 -13 1317.31 96.0168  20
   8 -14 -12 2015.52 72.6719   3
   8  14 -12 2041.90 73.0757   3
   8  14 -12 1875.08 77.0491   4
   8 -14 -12 1934.90 71.9447   4
   8 -14 -12 1362.80 142.293  25
   8 -14 -12 1417.26 94.8691  20
   8  14 -12 1205.62 111.541  20
   8  14 -11 17131.8 223.140   4
   8 -14 -11 16992.0 216.551   3
   8  14 -11 17033.6 218.416   3
   8 -14 -11 16695.0 216.488   4
   8 -14 -11 17985.3 239.922  20
   8  14 -11 18150.2 262.283  20
   8 -14 -11 17897.4 284.331  25
   8  14 -10 12239.4 231.951  22
   8 -14 -10 11869.4 190.407  20
   8  14 -10 12356.0 223.500  20
   8 -14 -10 12396.1 175.558   3
   8  14 -10 12174.2 177.218   3
   8  14 -10 12175.0 181.963   4
   8 -14 -10 12444.2 176.537   4
   8 -14  -9 367.482 122.339  29
   8  14  -9 444.903 135.490  22
   8 -14  -9 397.589 88.1172  20
   8  14  -9 184.915 130.206  20
   8  14  -9 346.617 82.8045   4
   8 -14  -9 293.839 78.6445   4
   8 -14  -9 442.706 72.6926   3
   8  14  -9 412.532 76.4594   3
   8  14  -8 15493.4 217.322   4
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   8 -15   7 828.130 50.6688   6
   8 -15   7 750.207 50.0808   5
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   8 -17   6 5155.78 114.962  19
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   8 -18  -3 22391.3 348.129  29
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   8 -18   3 365.929 97.8848  19
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   8 -18   6 1168.19 80.6999  19
   8 -18   7 1706.45 71.5443  19
   8 -18   8 1772.34 59.5904  19
   8 -18   9 88.7592 31.4255  19
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   8 -19 -12 14259.0 219.659  25
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   9  -4   9 493.878 23.5136   6
   9   4   9 549.265 25.0744   6
   9   4   9 538.898 23.6621   5
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   9   5 -14 4912.72 88.7895   3
   9   5 -14 4513.60 89.4996   4
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   9  -5 -13 3264.01 84.2610   3
   9   5 -13 3278.24 84.6461   3
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   9   5 -12 1082.35 76.8228   3
   9   5 -12 1024.93 77.9111   4
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   9   5  -2 803.147 121.316  20
   9  -5  -2 1029.47 117.773  19
   9  -5  -2 837.582 145.225  29
   9  -5  -1 261.389 136.386  29
   9  -5  -1 366.057 109.262   6
   9   5  -1 330.590 102.764   6
   9   5  -1 206.500 121.330  29
   9   5  -1 229.013 115.538  20
   9   5  -1 282.590 94.4780  19
   9  -5  -1 234.309 114.974  19
   9   5   0 4999.81 135.947   5
   9  -5   0 4900.05 137.947   5
   9  -5   0 5418.98 161.945  29
   9   5   0 5092.99 126.079  19
   9  -5   0 5112.03 148.527  19
   9  -5   0 4948.01 140.370   6
   9   5   0 4794.56 142.138   6
   9  -5   1 17996.0 260.006  19
   9   5   1 17290.5 243.815   5
   9  -5   1 17491.4 245.812   5
   9  -5   1 18002.5 260.429  29
   9   5   1 16883.8 231.998  19
   9  -5   1 18004.7 248.377   6
   9   5   1 17787.4 245.329   6
   9   5   2 2917.64 111.293   5
   9  -5   2 2916.54 112.306   5
   9   5   2 3083.39 102.867  19
   9  -5   2 2946.55 120.526   6
   9   5   2 3049.61 120.166   6
   9  -5   2 3271.18 127.631  19
   9   5   3 751.731 93.4227   5
   9  -5   3 805.026 93.2980   5
   9   5   3 760.673 79.0870  19
   9  -5   3 777.225 100.339   6
   9   5   3 782.435 100.454   6
   9  -5   3 705.839 108.259  19
   9  -5   4 12388.3 184.640   6
   9   5   4 12549.7 187.921   6
   9   5   4 12857.8 185.871   5
   9  -5   4 12656.7 184.910   5
   9  -5   4 12189.5 191.835  19
   9  -5   5 889.086 80.9915   6
   9   5   5 911.010 81.9018   6
   9   5   5 860.244 79.8441   5
   9  -5   5 839.588 78.1017   5
   9  -5   5 618.084 88.2317  19
   9  -5   6 7893.31 123.772   6
   9   5   6 7763.03 124.897   6
   9   5   6 8272.25 125.565   5
   9  -5   6 8169.26 123.287   5
   9  -5   7 157.848 52.5166   6
   9   5   7 102.794 54.1298   6
   9   5   7 105.046 51.3779   5
   9  -5   7 99.7835 50.2312   5
   9  -5   7 88.4785 56.5923  19
   9  -5   8 857.034 41.4426   6
   9   5   8 929.402 44.0538   6
   9   5   8 824.397 41.5190   5
   9  -5   8 897.099 41.2121   5
   9  -5   9 38.7316 18.6609   6
   9   5   9 28.3667 19.9112   6
   9  -6 -16 469.342 38.7467  20
   9   6 -16 452.418 36.4128  22
   9   6 -15 2056.03 72.1464  20
   9  -6 -15 1967.29 71.7400  20
   9   6 -15 1983.83 67.9318  22
   9  -6 -14 12597.2 152.494   3
   9   6 -14 12385.4 152.423   3
   9   6 -14 11956.6 153.161   4
   9  -6 -14 12039.0 153.301   4
   9   6 -14 10952.8 169.583  22
   9   6 -14 11578.8 174.171  20
   9  -6 -14 11446.3 169.937  20
   9  -6 -14 11395.2 178.728  25
   9  -6 -13 2258.92 73.0751   3
   9   6 -13 2258.77 73.0337   3
   9   6 -13 2238.45 76.6030   4
   9  -6 -13 2153.53 71.7097   4
   9   6 -13 2006.48 98.5412  22
   9   6 -13 2045.82 105.866  20
   9  -6 -13 2041.41 97.6947  20
   9  -6 -13 2007.23 123.341  25
   9  -6 -12 2073.60 81.4932   3
   9   6 -12 2067.52 81.3163   3
   9   6 -12 2124.49 85.5468   4
   9  -6 -12 2170.78 80.9377   4
   9   6 -12 2007.76 110.182  22
   9   6 -12 2037.64 122.848  20
   9  -6 -12 1938.39 109.834  20
   9  -6 -12 1915.99 139.554  25
   9   6 -11 3666.56 106.004   4
   9  -6 -11 3730.98 101.200   4
   9  -6 -11 3665.18 100.918   3
   9   6 -11 3749.11 100.097   3
   9   6 -11 4000.46 132.977  22
   9  -6 -11 3789.94 129.223  20
   9  -6 -11 4001.59 169.416  25
   9   6 -10 20905.7 279.793   4
   9  -6 -10 21118.8 276.613   4
   9  -6 -10 24269.1 302.276  20
   9   6 -10 23819.7 307.050  22
   9   6  -9 2922.60 135.287  22
   9  -6  -9 3215.48 176.837  25
   9   6  -9 2906.21 154.400  20
   9  -6  -9 2875.69 128.671  20
   9   6  -9 3105.50 109.937   4
   9  -6  -9 3198.88 152.038  29
   9   6  -8 4546.75 149.607  22
   9  -6  -8 4907.78 189.420  25
   9  -6  -8 4739.50 174.453  29
   9   6  -8 4896.40 164.836  20
   9  -6  -8 4648.26 143.609  20
   9  -6  -7 439.125 156.672  25
   9   6  -7 332.567 114.484  22
   9   6  -7 273.014 136.713  20
   9  -6  -7 318.591 107.060  20
   9  -6  -7 515.648 152.283  29
   9  -6  -6 581.757 153.000  25
   9   6  -6 519.316 113.439  22
   9   6  -6 651.943 136.220  20
   9  -6  -6 391.475 102.278  20
   9  -6  -6 594.380 154.387  29
   9  -6  -5 880.982 147.840  25
   9   6  -5 839.053 115.450  22
   9   6  -5 947.659 130.455  20
   9  -6  -5 850.564 98.5786  20
   9  -6  -4 29573.8 383.676  25
   9   6  -4 29108.3 388.374  20
   9  -6  -4 30403.6 400.516  29
   9  -6  -3 359.635 150.067  29
   9   6  -3 385.354 129.165  20
   9  -6  -3 377.079 120.122  19
   9  -6  -2 1423.89 155.090  29
   9   6  -2 1181.62 132.335  20
   9  -6  -2 1288.13 119.498  19
   9  -6  -1 2301.03 153.370  29
   9   6  -1 2570.13 141.909  20
   9  -6  -1 3001.97 132.066  19
   9   6  -1 2902.25 107.603  19
   9  -6  -1 3753.57 129.839   6
   9   6  -1 3684.11 124.064   6
   9   6   0 1480.15 108.404   5
   9  -6   0 1361.48 110.484   5
   9   6   0 1794.98 94.7993  19
   9  -6   0 1673.92 126.738  19
   9  -6   0 1516.38 112.188   6
   9   6   0 1502.37 113.767   6
   9  -6   1 2668.68 132.661  19
   9   6   1 3016.91 116.916   5
   9  -6   1 2999.96 119.708   5
   9  -6   1 2233.66 129.175  29
   9   6   1 2529.49 99.5714  19
   9  -6   1 2961.94 119.734   6
   9   6   1 2994.66 114.807   6
   9   6   2 1278.51 96.4614   5
   9  -6   2 1079.52 96.0747   5
   9   6   2 1024.04 83.3502  19
   9  -6   2 1105.45 104.448   6
   9   6   2 1189.55 103.729   6
   9  -6   2 1010.81 116.282  19
   9  -6   3 1625.00 102.714   6
   9   6   3 1782.83 104.404   6
   9   6   3 1836.13 99.8733   5
   9  -6   3 1780.87 97.7458   5
   9  -6   3 1649.40 114.413  19
   9  -6   4 578.066 84.5241   6
   9   6   4 575.951 90.5140   6
   9   6   4 572.779 85.7935   5
   9  -6   4 657.764 86.1560   5
   9  -6   4 396.590 97.5784  19
   9  -6   5 6585.39 121.695   6
   9   6   5 6667.44 124.537   6
   9   6   5 6509.67 118.537   5
   9  -6   5 6548.09 117.839   5
   9  -6   6 1452.55 71.2170   6
   9   6   6 1407.31 72.9928   6
   9   6   6 1271.46 69.8929   5
   9  -6   6 1380.03 69.1131   5
   9  -6   6 1504.64 79.8748  19
   9  -6   7 3423.58 73.7147   6
   9   6   7 3458.67 76.7599   6
   9   6   7 3819.97 75.1997   5
   9  -6   7 3721.38 73.4082   5
   9  -6   7 3400.85 79.1305  19
   9  -6   8 283.395 35.6006   6
   9   6   8 268.830 38.0203   6
   9  -6   8 294.748 39.6819  19
   9   6   8 265.005 36.6430   5
   9  -6   8 271.808 34.8965   5
   9   7 -16 484.665 35.9363  20
   9  -7 -16 425.226 36.2015  20
   9   7 -16 386.995 36.4453  22
   9  -7 -15 493.314 54.9954  20
   9   7 -15 382.573 58.2495  20
   9   7 -15 464.023 56.7871  22
   9   7 -14 692.299 76.1009  22
   9   7 -14 685.284 79.4487  20
   9  -7 -14 775.887 73.4814  20
   9  -7 -14 555.523 91.8708  25
   9   7 -14 1156.67 55.7765   4
   9  -7 -14 1182.73 53.5190   4
   9   7 -13 4238.59 113.348  22
   9   7 -13 4074.03 118.345  20
   9  -7 -13 4136.68 109.984  20
   9  -7 -13 4288.44 134.802  25
   9  -7 -13 3471.39 81.9514   3
   9   7 -13 3458.27 82.7565   3
   9   7 -13 3494.52 86.7552   4
   9  -7 -13 3487.06 83.8629   4
   9   7 -12 1631.72 105.345  22
   9   7 -12 1539.03 114.315  20
   9  -7 -12 1538.03 100.943  20
   9  -7 -12 1639.52 137.017  25
   9  -7 -12 1188.51 68.3032   3
   9   7 -12 1280.87 72.3585   3
   9   7 -12 1254.97 77.8056   4
   9  -7 -12 1275.41 74.0513   4
   9   7 -11 11029.7 202.542  22
   9   7 -11 11481.0 209.603  20
   9  -7 -11 10873.2 193.242  20
   9  -7 -11 10923.3 226.178  25
   9  -7 -11 13000.5 174.517   3
   9   7 -11 12342.2 182.595   4
   9  -7 -11 12655.1 178.294   4
   9   7 -11 12819.8 177.056   3
   9   7 -10 2368.37 126.408  22
   9   7 -10 3399.98 104.898   4
   9  -7 -10 3402.44 105.676   4
   9  -7 -10 2502.65 120.864  20
   9  -7 -10 2007.07 132.366  29
   9  -7  -9 1289.23 109.772  20
   9  -7  -9 1528.10 137.725  29
   9  -7  -9 1427.17 159.601  25
   9   7  -9 1373.18 120.847  22
   9  -7  -8 599.556 105.411  20
   9   7  -8 689.166 121.034  22
   9   7  -8 444.869 133.619  20
   9  -7  -8 896.844 145.233  29
   9  -7  -8 836.464 161.379  25
   9   7  -7 2668.98 155.839  20
   9  -7  -7 2710.29 120.603  20
   9  -7  -7 2842.57 167.518  29
   9  -7  -7 2812.13 172.365  25
   9   7  -7 2614.90 136.436  22
   9   7  -6 1387.72 132.846  20
   9  -7  -6 1050.72 102.503  20
   9  -7  -6 1145.07 154.694  29
   9  -7  -6 1193.25 155.835  25
   9   7  -6 1043.20 121.669  22
   9   7  -5 8679.31 200.614  20
   9  -7  -5 8232.57 202.575  25
   9   7  -4 4783.81 170.602  20
   9  -7  -4 4293.87 184.496  29
   9   7  -4 4444.18 148.926  22
   9  -7  -4 4657.65 164.344  25
   9  -7  -3 11785.2 241.077  29
   9   7  -3 11674.5 227.348  20
   9  -7  -2 5068.66 182.104  29
   9   7  -2 5769.24 173.699  20
   9  -7  -1 28472.0 356.485   6
   9   7  -1 28867.8 353.174   6
   9  -7  -1 28781.8 366.047  19
   9   7   0 789.777 102.011   5
   9  -7   0 778.507 104.348   5
   9  -7   0 721.518 121.658  19
   9   7   0 724.742 83.2924  19
   9  -7   0 752.198 99.6342   6
   9   7   0 662.566 104.600   6
   9  -7   0 772.072 131.746  29
   9  -7   1 127.588 100.118   6
   9   7   1 146.392 95.5650   6
   9   7   1 142.481 92.9589   5
   9  -7   1 144.812 95.4494   5
   9   7   1 114.630 76.8865  19
   9  -7   1 164.828 115.705  19
   9  -7   1 123.217 116.351  29
   9  -7   2 2372.90 112.124   6
   9   7   2 2468.15 113.080   6
   9   7   2 2728.17 107.595   5
   9  -7   2 2642.78 107.646   5
   9  -7   3 576.181 109.427  19
   9  -7   3 446.597 88.8551   6
   9   7   3 430.321 93.2959   6
   9   7   3 428.078 90.7839   5
   9  -7   3 336.948 89.5084   5
   9  -7   4 2138.03 108.866  19
   9  -7   4 1999.08 93.0179   6
   9   7   4 2106.28 91.9842   6
   9   7   4 2008.37 92.8510   5
   9  -7   4 1960.54 90.3695   5
   9  -7   5 5637.27 112.437   6
   9   7   5 5681.18 114.516   6
   9   7   5 5673.38 112.399   5
   9  -7   5 5527.62 109.693   5
   9  -7   6 1312.71 78.4381  19
   9  -7   6 1330.06 67.6816   6
   9   7   6 1457.85 70.3903   6
   9   7   6 1423.19 68.3508   5
   9  -7   6 1466.80 67.0891   5
   9  -7   7 1472.21 63.6256  19
   9  -7   7 1336.76 54.8986   6
   9   7   7 1439.40 57.3034   6
   9   7   7 1324.59 54.7593   5
   9  -7   7 1281.93 53.0353   5
   9  -7   8 1090.28 37.7057   6
   9   7   8 1012.92 40.0985   6
   9   7   8 968.803 39.2887   5
   9  -7   8 967.917 38.2705   5
   9  -7   8 1017.54 44.1045  19
   9   8 -16 42.2019 32.7410  22
   9   8 -16 134.469 29.9840  20
   9  -8 -16 103.285 30.2194  20
   9  -8 -15 76.8358 52.0667  20
   9   8 -15 103.214 54.4930  22
   9   8 -15 1.63129 55.2585  20
   9  -8 -14 13.4356 86.5939  25
   9   8 -14 103.846 45.6690   4
   9  -8 -14 163.966 44.0732   4
   9  -8 -14 50.3947 63.8886  20
   9   8 -14 92.5517 70.7700  22
   9   8 -14 32.0117 71.3915  20
   9  -8 -13 524.865 110.528  25
   9  -8 -13 817.330 56.6926   3
   9   8 -13 672.476 55.1036   3
   9   8 -13 714.164 61.3237   4
   9  -8 -13 804.368 59.1110   4
   9   8 -13 547.738 88.1909  22
   9  -8 -13 591.385 79.3296  20
   9   8 -13 478.306 89.7108  20
   9  -8 -12 1214.94 134.501  25
   9  -8 -12 1948.48 74.5700   3
   9   8 -12 1784.72 76.1238   3
   9   8 -12 1822.22 75.5810   4
   9  -8 -12 1728.61 74.0332   4
   9   8 -12 1375.51 104.881  22
   9   8 -12 1297.91 110.675  20
   9  -8 -12 1287.36 95.4219  20
   9  -8 -11 167.504 141.623  25
   9   8 -11 133.554 72.2115   4
   9  -8 -11 191.510 68.7670   4
   9  -8 -11 82.7983 92.6727  20
   9   8 -11 179.229 101.935  22
   9   8 -11 103.578 114.105  20
   9   8 -10 474.427 83.3078   4
   9  -8 -10 435.528 118.988  29
   9  -8 -10 354.720 99.1411  20
   9   8 -10 382.291 112.404  22
   9  -8  -9 5948.03 172.279  29
   9  -8  -9 6078.96 145.550  20
   9  -8  -9 6116.20 193.797  25
   9   8  -9 6040.52 159.788  22
   9  -8  -8 18347.8 253.976  20
   9  -8  -8 18056.4 294.217  25
   9   8  -8 17837.2 274.467  22
   9  -8  -7 3358.57 167.672  29
   9   8  -7 3985.64 159.783  20
   9  -8  -7 3626.44 122.458  20
   9   8  -7 3479.54 146.138  22
   9  -8  -7 3636.60 174.910  25
   9  -8  -6 116.555 149.665  29
   9   8  -6 164.245 114.590  22
   9   8  -6 280.505 134.617  20
   9  -8  -6 101.694 90.1483  20
   9  -8  -6 219.863 145.090  25
   9  -8  -5 178.186 141.320  29
   9   8  -5 255.755 130.235  20
   9   8  -5 38.4013 115.408  22
   9  -8  -5 131.324 139.148  25
   9   8  -4 1666.15 135.043  20
   9   8  -4 1457.70 127.078  22
   9  -8  -4 1681.72 140.958  25
   9  -8  -3 16.9364 148.145  29
   9   8  -3 24.3286 124.869  20
   9   8  -2 24645.7 349.271  20
   9  -8  -2 25157.6 350.705  29
   9  -8  -1 9199.36 202.741  29
   9   8   0 6180.13 136.058   5
   9  -8   0 6003.16 138.649   5
   9  -8   0 5442.89 164.519  29
   9   8   0 5368.69 116.885  19
   9  -8   0 6010.86 143.902   6
   9   8   0 6160.31 138.879   6
   9  -8   1 1029.12 102.074   6
   9   8   1 1158.28 104.269   6
   9   8   1 1077.13 98.0084   5
   9  -8   1 1003.81 99.2343   5
   9  -8   1 1290.36 122.007  29
   9   8   2 54297.6 580.559   5
   9  -8   2 54821.7 581.373   5
   9  -8   2 53876.0 595.987  19
   9  -8   2 55269.2 582.693   6
   9   8   2 53730.6 583.411   6
   9  -8   3 16790.5 243.742  19
   9   8   3 16980.4 224.742   5
   9  -8   3 17033.3 224.029   5
   9  -8   3 17097.7 227.723   6
   9   8   3 17534.3 228.647   6
   9  -8   4 286.107 92.1117  19
   9  -8   4 206.550 77.1880   6
   9   8   4 227.745 82.5063   6
   9   8   4 193.358 78.2252   5
   9  -8   4 222.300 77.3727   5
   9  -8   5 691.637 85.4474  19
   9   8   5 691.172 69.3994   5
   9  -8   5 652.385 68.4603   5
   9  -8   5 740.717 72.5283   6
   9   8   5 766.416 74.6843   6
   9  -8   6 189.285 69.4034  19
   9  -8   6 240.407 57.4964   6
   9   8   6 201.742 60.7302   6
   9   8   6 187.353 56.5820   5
   9  -8   6 215.839 55.4069   5
   9  -8   7 10032.6 126.482   6
   9   8   7 10353.6 128.805   6
   9   8   7 10047.8 126.717   5
   9  -8   7 10072.6 125.789   5
   9  -8   8 848.188 33.6652   6
   9   8   8 875.528 35.6440   6
   9   8   8 968.192 34.8615   5
   9  -8   8 968.930 33.8400   5
   9   9 -16 3002.94 54.3766  22
   9   9 -16 3099.61 49.7595  20
   9   9 -15 3094.65 76.2925  22
   9   9 -15 3244.48 73.9102  20
   9  -9 -15 3075.77 70.9669  20
   9  -9 -14-43.9318 83.6693  25
   9  -9 -14 16.0118 59.8446  20
   9   9 -14 29.1542 67.1200  22
   9   9 -14-92.5830 70.1207  20
   9  -9 -13 233.433 105.330  25
   9  -9 -13 282.184 74.9915  20
   9   9 -13 292.909 82.1200  22
   9   9 -13 160.907 86.2919  20
   9   9 -13 321.619 55.2080   4
   9  -9 -13 374.386 54.1023   4
   9  -9 -12 998.405 129.767  25
   9   9 -12 1075.18 100.899  22
   9   9 -12 799.584 106.317  20
   9  -9 -12 961.965 86.9942  20
   9   9 -12 1026.32 70.1292   4
   9  -9 -12 1086.83 67.5539   4
   9   9 -11 722.408 109.599  22
   9   9 -11 721.196 76.6262   4
   9  -9 -11 796.487 73.6794   4
   9  -9 -11 630.516 92.9276  20
   9   9 -11 577.870 117.313  20
   9  -9 -10 245.650 113.566  29
   9  -9 -10 94.7058 91.7919  20
   9   9 -10 113.134 110.654  22
   9   9 -10 29.6232 117.533  20
   9  -9  -9 601.032 155.276  25
   9  -9  -9 460.275 129.458  29
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   9 -10   5 2574.66 74.9236   5
   9 -10   6 3075.14 70.9723   6
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   9 -10   6 3263.54 69.8291   5
   9 -10   7 322.939 39.8774   6
   9  10   7 350.426 40.6503   6
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   9  10   7 314.208 38.2397   5
   9 -10   7 352.480 37.4834   5
   9 -10   8 29.7089 32.8332  19
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   9 -11 -14 386.530 80.3744  25
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   9 -11  -6 15537.9 274.164  29
   9 -11  -6 16485.1 268.663  25
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   9 -11  -5 11963.1 224.953  25
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   9 -11   3 608.361 77.4295   6
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   9 -11   3 642.981 75.8668   5
   9 -11   4 2106.02 78.2845   6
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   9 -11   4 2117.13 77.4810   5
   9 -11   5 2957.71 76.8423   6
   9  11   5 3133.19 79.3794   6
   9  11   5 3060.67 76.4558   5
   9 -11   5 3067.50 75.4607   5
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   9 -11   7 1556.21 42.8750   6
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   9 -12 -15 35.8643 49.4226  25
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   9 -12   4 242.268 62.7008   6
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   9 -12   4 311.930 60.4355   5
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   9 -12   5 1800.76 64.2614   6
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   9  12   5 1951.37 64.9358   5
   9 -12   5 1879.89 63.5170   5
   9 -12   6 371.185 42.4311   6
   9 -12   6 360.955 41.6086   5
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   9 -13  -8 6255.25 182.754  25
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   9 -13  -4 6347.19 163.923  25
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   9 -13  -3 494.749 149.093  29
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   9 -13   2 2185.26 84.2332   6
   9  13   2 2351.66 89.9560   6
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   9 -13   3 19363.7 255.703  19
   9 -13   3 19578.3 232.217   6
   9  13   3 19369.1 234.140   6
   9 -13   4 2015.35 94.0551  19
   9 -13   4 1959.98 69.3946   6
   9  13   4 1968.11 72.5459   6
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   9 -13   4 1911.97 68.8977   5
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   9 -13   6 4311.92 67.4631   6
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   9  14 -14 4718.11 82.5970  20
   9 -14 -14 4718.78 99.8102  25
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   9 -14 -13 263.869 88.9075  25
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   9  14 -11 105.170 95.2065  22
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   9 -14 -10 23739.3 294.503  29
   9 -14 -10 24039.4 322.399  25
   9  14 -10 22743.9 308.844  22
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   9 -14  -8 9924.65 197.149  29
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   9 -14  -8 10274.9 213.418  25
   9  14  -7 4256.57 156.586  20
   9 -14  -7 4074.97 161.809  29
   9 -14  -7 4441.78 168.967  25
   9  14  -7 4000.02 155.385  22
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   9 -14  -5 10476.7 220.206  29
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   9 -14  -4 7789.98 200.167  29
   9 -14  -4 8022.67 174.442  25
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   9 -14  -2 458.578 114.514  19
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   9 -14   2 395.112 96.0404  19
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   9 -14   3 817.967 65.2941   6
   9 -14   3 1030.89 98.4803  19
   9 -14   4 4606.23 85.4077   6
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   9 -14   5 412.807 44.1381   6
   9 -14   5 343.331 70.8367  19
   9 -14   6 4860.94 90.0879  19
   9 -14   7 296.548 42.0323  19
   9 -14   8 176.062 22.3016  19
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   9 -15 -14 2424.17 80.2237  25
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   9 -15 -13 638.282 86.7707  25
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   9  15 -12 1206.59 92.0706  22
   9  15 -11 3089.38 106.890  20
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   9  15 -10 8462.21 171.994  22
   9 -15 -10 8457.18 187.483  25
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   9 -15  -9 743.261 110.659  29
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   9 -15  -8 3596.59 159.991  25
   9  15  -8 3095.08 140.313  22
   9 -15  -8 3580.30 137.931  29
   9  15  -7-33.5334 125.654  22
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   9 -15  -7 170.689 136.403  25
   9 -15  -7 35.1028 126.358  29
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   9 -15  -6 217.166 134.552  29
   9 -15  -6 279.047 129.965  25
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   9 -15  -5 16051.5 246.841  25
   9 -15  -5 15335.9 260.269  29
   9 -15  -4 10854.3 223.920  29
   9  15  -3 14013.7 229.219  26
   9 -15  -3 15043.4 226.708  19
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   9 -30  -3 243.835 59.1027  29
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  10   9 -11 2972.19 91.2392  22
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  10   9  -9 358.581 83.5925  22
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  10 -10 -11-63.7395 95.2270  25
  10 -10 -10 756.873 109.146  25
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  10 -10  -9 1251.54 100.794  29
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  10 -10   0 3289.29 112.826  29
  10 -10   4 284.396 49.8279  19
  10 -10   5 1974.53 49.0892  19
  10  11 -14 715.429 30.8696  20
  10  11 -13 1856.89 58.4164  20
  10 -11 -13 1868.88 70.8251  25
  10  11 -12 2771.96 77.7391  20
  10  11 -12 2349.83 74.5697  22
  10  11 -11 62.0017 65.3289  22
  10  11 -11 116.466 71.8338  20
  10 -11 -11 54.3360 92.4859  25
  10  11 -10 0.85848 77.9852  22
  10  11 -10 78.2949 80.7413  20
  10 -11 -10 80.8376 104.361  25
  10 -11  -9 6413.63 150.050  25
  10 -11  -9 6193.67 136.033  29
  10 -11  -8 303.001 103.343  29
  10  11  -8 168.264 87.1380  22
  10 -11  -8 177.391 111.640  25
  10  11  -7 2351.41 115.983  20
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  10 -11  -7 2021.45 126.375  29
  10  11  -6 754.650 107.583  20
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  10 -11  -2 611.575 112.789  29
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  10 -11   0 813.246 94.5783  29
  10 -11   5 594.915 37.5776  19
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  10  12 -12 14892.7 179.451  20
  10  12 -12 13650.6 177.880  22
  10  12 -11 1034.98 74.1012  20
  10 -12 -11 942.264 93.5459  25
  10  12 -11 919.702 70.1722  22
  10  12 -10 9935.13 159.826  20
  10 -12 -10 10318.2 173.884  25
  10  12 -10 9877.39 155.643  22
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  10 -12  -9 6474.67 147.751  25
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  10 -12  -6 777.717 122.221  29
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  10 -12  -5 1645.33 128.912  29
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  10 -12  -3 427.902 116.385  29
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  10 -12   1 1645.64 84.2790  19
  10  13 -13 3520.15 62.4618  20
  10 -13 -13 3339.16 74.3269  25
  10  13 -12 1963.66 66.3583  20
  10  13 -12 1820.48 67.0579  22
  10  13 -11 126.027 62.0063  22
  10  13 -11 181.900 66.1355  20
  10 -13 -11 199.414 84.4490  25
  10  13 -10 586.769 79.4184  20
  10  13 -10 520.971 75.4871  22
  10 -13 -10 634.777 96.7425  25
  10  13  -9 2483.07 101.128  20
  10  13  -9 2235.61 97.8637  22
  10 -13  -9 2382.18 114.979  25
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   0   0   0    0.00    0.00   0
TITL ij1039 in P2(1)/n
REM P2(1)/n (#14 in standard setting)
CELL 1.54184   9.382519  39.916370  15.991961  90.0000 104.2168  90.0000
ZERR    8.00   0.000074   0.000295   0.000134   0.0000   0.0008   0.0000
LATT  1
SYMM -x+1/2, y+1/2,-z+1/2
SFAC C H N O Co Se
UNIT 208.00 224.00 48.00 32.00 8.00 16.00
TREF
HKLF 4
END
;
_shelx_hkl_checksum              26485
_shelx_res_file
;
TITL ij1039_auto in P21/n #14
    ij1039.res
    created by SHELXL-2016/6 at 15:24:08 on 08-Apr-2024
REM reset to P21/n #14
CELL 1.54184 9.3825 39.9164 15.992 90 104.217 90
ZERR 8 0.0001 0.0003 0.0001 0 0.001 0
LATT 1
SYMM 0.5-X,0.5+Y,0.5-Z
SFAC C H Co N O Se
UNIT 208 224 8 48 32 16
EQIV $1 1+X,+Y,+Z
EQIV $2 1-X,1-Y,1-Z
EQIV $3 -X,1-Y,-Z
EQIV $4 -1+X,+Y,+Z
L.S. 10
PLAN  10
TEMP -173
HTAB C15 O21
HTAB C26 O11
HTAB C35 Se1_$1
HTAB C36 O11
HTAB C42 Se3_$2
HTAB C52 Se2_$3
HTAB C55 O61
HTAB C56 Se2_$3
HTAB C65 O81
HTAB C66 Se2_$4
HTAB C75 Se3_$1
HTAB C75 O81
HTAB C76 O51
HTAB C86 Se1_$2
CONF
BOND $H
HTAB
fmap 2
acta
MORE -1
OMIT -1 4 3
REM <olex2.extras>
REM <HklSrc "%.\\ij1039.hkl">
REM </olex2.extras>
WGHT    0.061100    6.300200
FVAR       1.91906
CO1   3    0.856867    0.300734    0.253487    11.00000    0.02926    0.03522 =
         0.03262   -0.00012    0.00656   -0.00107
N1    4    0.704525    0.305279    0.329975    11.00000    0.03742    0.05238 =
         0.04431   -0.00220    0.01444   -0.00119
C1    1    0.621082    0.300863    0.370777    11.00000    0.03446    0.04674 =
         0.03521   -0.00060    0.00291    0.00137
SE1   6    0.488792    0.293439    0.433749    11.00000    0.03537    0.07718 =
         0.03717    0.00799    0.00861    0.00101
N2    4    0.833676    0.351207    0.216581    11.00000    0.05083    0.03494 =
         0.05646    0.00088    0.01726    0.00152
C2    1    0.763995    0.373773    0.184427    11.00000    0.03500    0.04007 =
         0.03940   -0.00537    0.01303   -0.00719
SE2   6    0.656593    0.409423    0.137447    11.00000    0.03332    0.04557 =
         0.03953    0.00369    0.00586    0.00037
O11   5    0.696368    0.291407    0.138488    11.00000    0.02522    0.05937 =
         0.03840    0.00144    0.00532   -0.00919
N11   4    0.562134    0.279032    0.128251    11.00000    0.02579    0.03964 =
         0.03830   -0.00604    0.00801   -0.00296
C11   1    0.456680    0.288579    0.056702    11.00000    0.03231    0.04919 =
         0.03770   -0.00799    0.00805   -0.00025
C12   1    0.319591    0.273920    0.042578    11.00000    0.02969    0.05099 =
         0.04590   -0.01207    0.00387    0.00200
AFIX  43
H12   2    0.246440    0.279411   -0.008091    11.00000   -1.20000
AFIX   0
C13   1    0.286830    0.251434    0.100712    11.00000    0.02998    0.04159 =
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AFIX  43
H13   2    0.191510    0.241859    0.091308    11.00000   -1.20000
AFIX   0
C14   1    0.396003    0.243172    0.172953    11.00000    0.03523    0.03434 =
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AFIX  43
H14   2    0.375413    0.227885    0.213985    11.00000   -1.20000
AFIX   0
C15   1    0.533505    0.256832    0.185854    11.00000    0.02951    0.03679 =
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AFIX  43
H15   2    0.608527    0.250736    0.235095    11.00000   -1.20000
AFIX   0
C16   1    0.499403    0.314611    0.000411    11.00000    0.03574    0.08380 =
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AFIX 137
H16A  2    0.535110    0.334590    0.034815    11.00000   -1.50000
H16B  2    0.413754    0.320524   -0.046059    11.00000   -1.50000
H16C  2    0.577394    0.305811   -0.024481    11.00000   -1.50000
AFIX   0
O21   5    0.866949    0.250204    0.286343    11.00000    0.03136    0.04443 =
         0.06668    0.01832    0.01530    0.00458
N21   4    0.969968    0.230257    0.270814    11.00000    0.03593    0.03252 =
         0.04302    0.00753    0.00865   -0.00039
C21   1    0.942443    0.209569    0.200301    11.00000    0.06422    0.05595 =
         0.04506    0.00752    0.00465   -0.02665
C22   1    1.055568    0.186640    0.193451    11.00000    0.09443    0.03827 =
         0.07629   -0.01287    0.05331   -0.01753
AFIX  43
H22   2    1.038070    0.171341    0.146527    11.00000   -1.20000
AFIX   0
C23   1    1.185272    0.186063    0.251060    11.00000    0.07900    0.04902 =
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AFIX  43
H23   2    1.259130    0.170516    0.245622    11.00000   -1.20000
AFIX   0
C24   1    1.209250    0.207878    0.316795    11.00000    0.05832    0.07474 =
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AFIX  43
H24   2    1.302134    0.208032    0.357349    11.00000   -1.20000
AFIX   0
C25   1    1.102785    0.229964    0.326819    11.00000    0.03985    0.05535 =
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AFIX  43
H25   2    1.123087    0.245224    0.373844    11.00000   -1.20000
AFIX   0
C26   1    0.803000    0.210894    0.137226    11.00000    0.05008    0.07385 =
         0.07808   -0.01621    0.01432   -0.00257
AFIX 137
H26A  2    0.724731    0.203455    0.163751    11.00000   -1.50000
H26B  2    0.806154    0.196186    0.088647    11.00000   -1.50000
H26C  2    0.783446    0.233942    0.116457    11.00000   -1.50000
AFIX   0
O31   5    1.007797    0.288627    0.180298    11.00000    0.03114    0.03439 =
         0.03706   -0.00007    0.00987   -0.00435
N31   4    1.100693    0.311458    0.164047    11.00000    0.02720    0.03286 =
         0.03165   -0.00176    0.00783   -0.00074
C31   1    1.065128    0.328807    0.089052    11.00000    0.02922    0.03829 =
         0.03152   -0.00019    0.00662    0.00153
C32   1    1.166625    0.351340    0.071742    11.00000    0.03710    0.03784 =
         0.03765    0.00372    0.01197    0.00080
AFIX  43
H32   2    1.142666    0.363892    0.019694    11.00000   -1.20000
AFIX   0
C33   1    1.301708    0.355867    0.128681    11.00000    0.03422    0.03667 =
         0.04338   -0.00240    0.01430   -0.00294
AFIX  43
H33   2    1.370726    0.371318    0.116247    11.00000   -1.20000
AFIX   0
C34   1    1.334897    0.337343    0.204733    11.00000    0.02852    0.04142 =
         0.03720   -0.00617    0.00619   -0.00161
AFIX  43
H34   2    1.427367    0.339968    0.244894    11.00000   -1.20000
AFIX   0
C35   1    1.233088    0.315248    0.221326    11.00000    0.02889    0.03851 =
         0.03211    0.00037    0.00419    0.00281
AFIX  43
H35   2    1.255339    0.302541    0.273140    11.00000   -1.20000
AFIX   0
C36   1    0.921124    0.321072    0.028527    11.00000    0.03333    0.06156 =
         0.03230    0.00331    0.00363   -0.00399
AFIX 137
H36A  2    0.916201    0.297105    0.014824    11.00000   -1.50000
H36B  2    0.911002    0.334061   -0.024614    11.00000   -1.50000
H36C  2    0.841353    0.326956    0.055521    11.00000   -1.50000
AFIX   0
O41   5    1.044305    0.311592    0.350590    11.00000    0.03935    0.07582 =
         0.03819   -0.01827    0.00798   -0.01007
N41   4    1.043880    0.327638    0.423989    11.00000    0.04522    0.05519 =
         0.03218   -0.00438    0.00744   -0.00489
C41   1    1.113793    0.357253    0.441124    11.00000    0.04594    0.05326 =
         0.03382    0.00042    0.00818   -0.00294
C42   1    1.117900    0.372860    0.519082    11.00000    0.06587    0.05131 =
         0.04114   -0.00544    0.01421   -0.00903
AFIX  43
H42   2    1.169421    0.393427    0.532417    11.00000   -1.20000
AFIX   0
C43   1    1.048442    0.359064    0.577797    11.00000    0.09256    0.06168 =
         0.03489   -0.00652    0.01928   -0.01115
AFIX  43
H43   2    1.050575    0.370045    0.630794    11.00000   -1.20000
AFIX   0
C44   1    0.975301    0.328696    0.557395    11.00000    0.08151    0.06237 =
         0.04158    0.00557    0.02241   -0.00949
AFIX  43
H44   2    0.925918    0.318749    0.596364    11.00000   -1.20000
AFIX   0
C45   1    0.974812    0.313141    0.480568    11.00000    0.05560    0.05836 =
         0.03946    0.00102    0.01119   -0.00829
AFIX  43
H45   2    0.926239    0.292243    0.466866    11.00000   -1.20000
AFIX   0
C46   1    1.184357    0.371621    0.375253    11.00000    0.05168    0.06819 =
         0.04181   -0.00130    0.01713   -0.00702
AFIX 137
H46A  2    1.268379    0.357690    0.371152    11.00000   -1.50000
H46B  2    1.218275    0.394423    0.392139    11.00000   -1.50000
H46C  2    1.112834    0.372203    0.319137    11.00000   -1.50000
AFIX   0
CO2   3    0.054902    0.550477    0.267904    11.00000    0.02980    0.03706 =
         0.03475    0.00530    0.00881    0.00232
N3    4   -0.112219    0.551219    0.334028    11.00000    0.03244    0.04595 =
         0.04312    0.00732    0.01256    0.00577
C3    1   -0.188893    0.547220    0.379302    11.00000    0.03317    0.03519 =
         0.03964    0.00496    0.00568    0.00321
SE3   6   -0.303405    0.541535    0.453994    11.00000    0.03533    0.04521 =
         0.04398    0.00795    0.01443    0.00154
N4    4    0.026579    0.601762    0.234830    11.00000    0.04288    0.04131 =
         0.04283    0.00711    0.01429    0.00783
C4    1   -0.023324    0.627622    0.212030    11.00000    0.03388    0.04478 =
         0.03150    0.00066    0.01014   -0.00388
SE4   6   -0.103901    0.668018    0.178643    11.00000    0.04327    0.03789 =
         0.03780    0.00388    0.00378   -0.00041
O51   5   -0.087689    0.538730    0.148997    11.00000    0.02969    0.05992 =
         0.04108    0.01302    0.00439   -0.00577
N51   4   -0.228028    0.530485    0.139950    11.00000    0.02993    0.04248 =
         0.03907    0.00477    0.00796   -0.00358
C51   1   -0.332866    0.547139    0.080615    11.00000    0.03537    0.03997 =
         0.03633    0.00400    0.00786   -0.00054
C52   1   -0.477215    0.537601    0.068326    11.00000    0.03360    0.04196 =
         0.03914   -0.00361    0.00752    0.00174
AFIX  43
H52   2   -0.550788    0.548674    0.025880    11.00000   -1.20000
AFIX   0
C53   1   -0.517357    0.512151    0.116675    11.00000    0.03486    0.04158 =
         0.05123   -0.00864    0.01758   -0.00372
AFIX  43
H53   2   -0.617456    0.505829    0.108496    11.00000   -1.20000
AFIX   0
C54   1   -0.407180    0.496080    0.177562    11.00000    0.04423    0.03714 =
         0.05037    0.00132    0.01964   -0.00334
AFIX  43
H54   2   -0.431603    0.478620    0.211947    11.00000   -1.20000
AFIX   0
C55   1   -0.263282    0.505445    0.187948    11.00000    0.04257    0.04185 =
         0.04399    0.00901    0.01310    0.00233
AFIX  43
H55   2   -0.188053    0.494262    0.229107    11.00000   -1.20000
AFIX   0
C56   1   -0.281424    0.574872    0.032419    11.00000    0.04297    0.05985 =
         0.04906    0.01993   -0.00048   -0.00834
AFIX 137
H56A  2   -0.224618    0.591042    0.073505    11.00000   -1.50000
H56B  2   -0.366620    0.586115   -0.004755    11.00000   -1.50000
H56C  2   -0.219314    0.565636   -0.003085    11.00000   -1.50000
AFIX   0
O61   5    0.074711    0.499128    0.299733    11.00000    0.03104    0.03558 =
         0.04236    0.00519    0.01142    0.00302
N61   4    0.192482    0.480961    0.296772    11.00000    0.03319    0.03378 =
         0.03720    0.00416    0.01377    0.00121
C61   1    0.178015    0.455429    0.239672    11.00000    0.04023    0.05090 =
         0.06175   -0.01624    0.01862   -0.00717
C62   1    0.298456    0.435169    0.241813    11.00000    0.05036    0.04458 =
         0.08542   -0.01849    0.03049   -0.00643
AFIX  43
H62   2    0.289413    0.417190    0.201929    11.00000   -1.20000
AFIX   0
C63   1    0.430121    0.440362    0.299845    11.00000    0.04412    0.03997 =
         0.06913    0.01140    0.03025    0.00635
AFIX  43
H63   2    0.510759    0.425707    0.302108    11.00000   -1.20000
AFIX   0
C64   1    0.443389    0.467478    0.355311    11.00000    0.03758    0.05537 =
         0.04495    0.00979    0.01237    0.00787
AFIX  43
H64   2    0.534361    0.472043    0.395294    11.00000   -1.20000
AFIX   0
C65   1    0.323355    0.487733    0.351867    11.00000    0.03679    0.04405 =
         0.03799    0.00101    0.00665    0.00534
AFIX  43
H65   2    0.332637    0.506706    0.388678    11.00000   -1.20000
AFIX   0
C66   1    0.032139    0.451200    0.178327    11.00000    0.04314    0.12789 =
         0.11592   -0.08019    0.00708   -0.00781
AFIX 137
H66A  2   -0.041594    0.445915    0.210397    11.00000   -1.50000
H66B  2    0.036981    0.432891    0.138290    11.00000   -1.50000
H66C  2    0.004750    0.472002    0.145805    11.00000   -1.50000
AFIX   0
O71   5    0.221128    0.543891    0.202024    11.00000    0.03303    0.03821 =
         0.04077    0.00266    0.01378   -0.00110
N71   4    0.308976    0.569362    0.194516    11.00000    0.03072    0.03774 =
         0.03583    0.00242    0.01229    0.00141
C71   1    0.276851    0.588403    0.121620    11.00000    0.03333    0.04130 =
         0.03571    0.00210    0.01183    0.00420
C72   1    0.375566    0.613455    0.113338    11.00000    0.03928    0.04384 =
         0.03944    0.00621    0.01267    0.00399
AFIX  43
H72   2    0.355116    0.627086    0.063102    11.00000   -1.20000
AFIX   0
C73   1    0.502678    0.618853    0.176823    11.00000    0.03925    0.03923 =
         0.04618    0.00223    0.01425   -0.00079
AFIX  43
H73   2    0.569491    0.636000    0.170536    11.00000   -1.20000
AFIX   0
C74   1    0.531245    0.598876    0.249821    11.00000    0.03217    0.04824 =
         0.03960   -0.00137    0.00750    0.00164
AFIX  43
H74   2    0.618290    0.602127    0.294180    11.00000   -1.20000
AFIX   0
C75   1    0.432828    0.574336    0.257606    11.00000    0.03322    0.04059 =
         0.03514    0.00401    0.00798    0.00444
AFIX  43
H75   2    0.451851    0.560697    0.307813    11.00000   -1.20000
AFIX   0
C76   1    0.142351    0.579844    0.054354    11.00000    0.03593    0.05986 =
         0.03726    0.00442    0.00990   -0.00029
AFIX 137
H76A  2    0.149950    0.556819    0.034623    11.00000   -1.50000
H76B  2    0.131994    0.595263    0.005540    11.00000   -1.50000
H76C  2    0.056233    0.581794    0.078453    11.00000   -1.50000
AFIX   0
O81   5    0.225580    0.561595    0.376297    11.00000    0.03497    0.04587 =
         0.03314   -0.00071    0.01028   -0.00074
N81   4    0.206016    0.567792    0.455058    11.00000    0.03300    0.03725 =
         0.03217    0.00199    0.00659    0.00290
C81   1    0.260696    0.596842    0.494410    11.00000    0.04865    0.04061 =
         0.04140   -0.00069    0.00543   -0.00748
C82   1    0.239790    0.603106    0.575863    11.00000    0.06576    0.04975 =
         0.03857   -0.00911    0.00218   -0.00788
AFIX  43
H82   2    0.275400    0.623445    0.604265    11.00000   -1.20000
AFIX   0
C83   1    0.168584    0.580506    0.616476    11.00000    0.05366    0.06112 =
         0.03048   -0.00159    0.00523    0.00276
AFIX  43
H83   2    0.154145    0.585270    0.672016    11.00000   -1.20000
AFIX   0
C84   1    0.118216    0.550679    0.575151    11.00000    0.03465    0.05228 =
         0.03546    0.00925    0.00491    0.00436
AFIX  43
H84   2    0.070081    0.534572    0.602321    11.00000   -1.20000
AFIX   0
C85   1    0.139019    0.544775    0.494239    11.00000    0.03144    0.03668 =
         0.03816    0.00431    0.00463    0.00174
AFIX  43
H85   2    0.105963    0.524319    0.465635    11.00000   -1.20000
AFIX   0
C86   1    0.338810    0.619408    0.446085    11.00000    0.07298    0.04887 =
         0.06015   -0.00260    0.01774   -0.02160
AFIX 137
H86A  2    0.425429    0.607893    0.436153    11.00000   -1.50000
H86B  2    0.369744    0.639797    0.479800    11.00000   -1.50000
H86C  2    0.272588    0.625365    0.390545    11.00000   -1.50000
AFIX   0
HKLF 4
REM  ij1039_auto in P21/n #14
REM R1 =  0.0379 for   11197 Fo > 4sig(Fo)  and  0.0402 for all   11937 data
REM    711 parameters refined using      0 restraints
END
WGHT      0.0612      6.2920
REM Instructions for potential hydrogen bonds
HTAB C15 O21
HTAB C26 O11
HTAB C35 Se1_$1
HTAB C36 O11
HTAB C42 Se3_$2
HTAB C52 Se2_$3
HTAB C55 O61
HTAB C56 Se2_$3
HTAB C65 O81
HTAB C66 Se2_$4
HTAB C75 Se3_$1
HTAB C75 O81
HTAB C76 O51
HTAB C86 Se1_$2
REM Highest difference peak  1.760,  deepest hole -0.671,  1-sigma level  0.075
Q1    1   0.1065  0.4943  0.0320  11.00000  0.05    1.76
Q2    1   1.1429  0.2463  0.4092  11.00000  0.05    1.58
Q3    1  -0.0192  0.6688  0.1980  11.00000  0.05    0.84
Q4    1   0.9610  0.1895  0.1702  11.00000  0.05    0.77
Q5    1  -0.3548  0.5309  0.4130  11.00000  0.05    0.63
Q6    1   0.4292  0.2905  0.4620  11.00000  0.05    0.52
Q7    1   0.4778  0.3134  0.4342  11.00000  0.05    0.51
Q8    1   1.0225  0.3298  0.3387  11.00000  0.05    0.47
Q9    1   0.3977  0.2901  0.3928  11.00000  0.05    0.45
Q10   1   0.8649  0.2173  0.2030  11.00000  0.05    0.43
;
_shelx_res_checksum              78026
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Co Co1 0.85687(5) 0.30073(2) 0.25349(3) 0.03255(11) Uani d 1 . .
N N1 0.7045(3) 0.30528(7) 0.32998(18) 0.0439(6) Uani d 1 . .
C C1 0.6211(3) 0.30086(8) 0.37078(19) 0.0398(6) Uani d 1 . .
Se Se1 0.48879(4) 0.29344(2) 0.43375(2) 0.04996(10) Uani d 1 . .
N N2 0.8337(3) 0.35121(7) 0.21658(19) 0.0467(6) Uani d 1 . .
C C2 0.7640(3) 0.37377(7) 0.18443(19) 0.0375(6) Uani d 1 . .
Se Se2 0.65659(3) 0.40942(2) 0.13745(2) 0.04001(9) Uani d 1 . .
O O11 0.6964(2) 0.29141(6) 0.13849(13) 0.0414(5) Uani d 1 . .
N N11 0.5621(2) 0.27903(6) 0.12825(15) 0.0346(5) Uani d 1 . .
C C11 0.4567(3) 0.28858(8) 0.05670(19) 0.0398(6) Uani d 1 . .
C C12 0.3196(3) 0.27392(8) 0.0426(2) 0.0431(7) Uani d 1 . .
H H12 0.246440 0.279411 -0.008091 0.052 Uiso calc 1 . .
C C13 0.2868(3) 0.25143(8) 0.1007(2) 0.0465(7) Uani d 1 . .
H H13 0.191510 0.241859 0.091308 0.056 Uiso calc 1 . .
C C14 0.3960(3) 0.24317(8) 0.1730(2) 0.0447(7) Uani d 1 . .
H H14 0.375413 0.227885 0.213985 0.054 Uiso calc 1 . .
C C15 0.5335(3) 0.25683(7) 0.1859(2) 0.0390(6) Uani d 1 . .
H H15 0.608527 0.250736 0.235095 0.047 Uiso calc 1 . .
C C16 0.4994(4) 0.31461(11) 0.0004(2) 0.0534(9) Uani d 1 . .
H H16A 0.535110 0.334590 0.034815 0.080 Uiso calc 1 . .
H H16B 0.413754 0.320524 -0.046059 0.080 Uiso calc 1 . .
H H16C 0.577394 0.305811 -0.024481 0.080 Uiso calc 1 . .
O O21 0.8669(2) 0.25020(6) 0.28634(16) 0.0469(5) Uani d 1 . .
N N21 0.9700(3) 0.23026(6) 0.27081(16) 0.0373(5) Uani d 1 . .
C C21 0.9424(5) 0.20957(10) 0.2003(2) 0.0566(9) Uani d 1 . .
C C22 1.0556(6) 0.18664(9) 0.1935(3) 0.0640(12) Uani d 1 . .
H H22 1.038070 0.171341 0.146527 0.077 Uiso calc 1 . .
C C23 1.1853(5) 0.18606(10) 0.2511(3) 0.0663(11) Uani d 1 . .
H H23 1.259130 0.170516 0.245622 0.080 Uiso calc 1 . .
C C24 1.2092(5) 0.20788(11) 0.3168(3) 0.0611(10) Uani d 1 . .
H H24 1.302134 0.208032 0.357349 0.073 Uiso calc 1 . .
C C25 1.1028(4) 0.22996(9) 0.3268(2) 0.0445(7) Uani d 1 . .
H H25 1.123087 0.245224 0.373844 0.053 Uiso calc 1 . .
C C26 0.8030(5) 0.21089(12) 0.1372(3) 0.0676(11) Uani d 1 . .
H H26A 0.724731 0.203455 0.163751 0.101 Uiso calc 1 . .
H H26B 0.806154 0.196186 0.088647 0.101 Uiso calc 1 . .
H H26C 0.783446 0.233942 0.116457 0.101 Uiso calc 1 . .
O O31 1.0078(2) 0.28863(5) 0.18030(12) 0.0339(4) Uani d 1 . .
N N31 1.1007(2) 0.31146(6) 0.16405(14) 0.0305(4) Uani d 1 . .
C C31 1.0651(3) 0.32881(7) 0.08905(17) 0.0332(5) Uani d 1 . .
C C32 1.1666(3) 0.35134(7) 0.07174(19) 0.0370(6) Uani d 1 . .
H H32 1.142666 0.363892 0.019694 0.044 Uiso calc 1 . .
C C33 1.3017(3) 0.35587(7) 0.12868(19) 0.0373(6) Uani d 1 . .
H H33 1.370726 0.371318 0.116247 0.045 Uiso calc 1 . .
C C34 1.3349(3) 0.33734(7) 0.20473(19) 0.0360(6) Uani d 1 . .
H H34 1.427367 0.339968 0.244894 0.043 Uiso calc 1 . .
C C35 1.2331(3) 0.31525(7) 0.22133(18) 0.0337(5) Uani d 1 . .
H H35 1.255339 0.302541 0.273140 0.040 Uiso calc 1 . .
C C36 0.9211(3) 0.32107(9) 0.02853(19) 0.0432(7) Uani d 1 . .
H H36A 0.916201 0.297105 0.014824 0.065 Uiso calc 1 . .
H H36B 0.911002 0.334061 -0.024614 0.065 Uiso calc 1 . .
H H36C 0.841353 0.326956 0.055521 0.065 Uiso calc 1 . .
O O41 1.0443(3) 0.31159(7) 0.35059(15) 0.0514(6) Uani d 1 . .
N N41 1.0439(3) 0.32764(7) 0.42399(16) 0.0446(6) Uani d 1 . .
C C41 1.1138(4) 0.35725(9) 0.4411(2) 0.0446(7) Uani d 1 . .
C C42 1.1179(4) 0.37286(9) 0.5191(2) 0.0526(8) Uani d 1 . .
H H42 1.169421 0.393427 0.532417 0.063 Uiso calc 1 . .
C C43 1.0484(5) 0.35906(10) 0.5778(2) 0.0624(10) Uani d 1 . .
H H43 1.050575 0.370045 0.630794 0.075 Uiso calc 1 . .
C C44 0.9753(5) 0.32870(10) 0.5574(2) 0.0605(10) Uani d 1 . .
H H44 0.925918 0.318749 0.596364 0.073 Uiso calc 1 . .
C C45 0.9748(4) 0.31314(10) 0.4806(2) 0.0512(8) Uani d 1 . .
H H45 0.926239 0.292243 0.466866 0.061 Uiso calc 1 . .
C C46 1.1844(4) 0.37162(10) 0.3753(2) 0.0529(8) Uani d 1 . .
H H46A 1.268379 0.357690 0.371152 0.079 Uiso calc 1 . .
H H46B 1.218275 0.394423 0.392139 0.079 Uiso calc 1 . .
H H46C 1.112834 0.372203 0.319137 0.079 Uiso calc 1 . .
Co Co2 0.05490(5) 0.55048(2) 0.26790(3) 0.03372(11) Uani d 1 . .
N N3 -0.1122(3) 0.55122(7) 0.33403(17) 0.0399(5) Uani d 1 . .
C C3 -0.1889(3) 0.54722(7) 0.37930(19) 0.0366(6) Uani d 1 . .
Se Se3 -0.30340(4) 0.54154(2) 0.45399(2) 0.04069(9) Uani d 1 . .
N N4 0.0266(3) 0.60176(7) 0.23483(17) 0.0417(6) Uani d 1 . .
C C4 -0.0233(3) 0.62762(8) 0.21203(18) 0.0364(6) Uani d 1 . .
Se Se4 -0.10390(4) 0.66802(2) 0.17864(2) 0.04073(9) Uani d 1 . .
O O51 -0.0877(2) 0.53873(6) 0.14900(14) 0.0443(5) Uani d 1 . .
N N51 -0.2280(3) 0.53048(6) 0.13995(16) 0.0372(5) Uani d 1 . .
C C51 -0.3329(3) 0.54714(7) 0.08062(19) 0.0374(6) Uani d 1 . .
C C52 -0.4772(3) 0.53760(8) 0.06833(19) 0.0385(6) Uani d 1 . .
H H52 -0.550788 0.548674 0.025880 0.046 Uiso calc 1 . .
C C53 -0.5174(3) 0.51215(8) 0.1167(2) 0.0413(6) Uani d 1 . .
H H53 -0.617456 0.505829 0.108496 0.050 Uiso calc 1 . .
C C54 -0.4072(4) 0.49608(8) 0.1776(2) 0.0425(7) Uani d 1 . .
H H54 -0.431603 0.478620 0.211947 0.051 Uiso calc 1 . .
C C55 -0.2633(4) 0.50544(8) 0.1879(2) 0.0424(7) Uani d 1 . .
H H55 -0.188053 0.494262 0.229107 0.051 Uiso calc 1 . .
C C56 -0.2814(4) 0.57487(9) 0.0324(2) 0.0527(8) Uani d 1 . .
H H56A -0.224618 0.591042 0.073505 0.079 Uiso calc 1 . .
H H56B -0.366620 0.586115 -0.004755 0.079 Uiso calc 1 . .
H H56C -0.219314 0.565636 -0.003085 0.079 Uiso calc 1 . .
O O61 0.0747(2) 0.49913(5) 0.29973(13) 0.0359(4) Uani d 1 . .
N N61 0.1925(3) 0.48096(6) 0.29677(15) 0.0338(5) Uani d 1 . .
C C61 0.1780(4) 0.45543(9) 0.2397(2) 0.0499(8) Uani d 1 . .
C C62 0.2985(4) 0.43517(9) 0.2418(3) 0.0577(9) Uani d 1 . .
H H62 0.289413 0.417190 0.201929 0.069 Uiso calc 1 . .
C C63 0.4301(4) 0.44036(8) 0.2998(2) 0.0482(8) Uani d 1 . .
H H63 0.510759 0.425707 0.302108 0.058 Uiso calc 1 . .
C C64 0.4434(4) 0.46748(9) 0.3553(2) 0.0456(7) Uani d 1 . .
H H64 0.534361 0.472043 0.395294 0.055 Uiso calc 1 . .
C C65 0.3234(3) 0.48773(8) 0.35187(19) 0.0401(6) Uani d 1 . .
H H65 0.332637 0.506706 0.388678 0.048 Uiso calc 1 . .
C C66 0.0321(5) 0.45120(16) 0.1783(4) 0.098(2) Uani d 1 . .
H H66A -0.041594 0.445915 0.210397 0.147 Uiso calc 1 . .
H H66B 0.036981 0.432891 0.138290 0.147 Uiso calc 1 . .
H H66C 0.004750 0.472002 0.145805 0.147 Uiso calc 1 . .
O O71 0.2211(2) 0.54389(5) 0.20202(13) 0.0365(4) Uani d 1 . .
N N71 0.3090(3) 0.56936(6) 0.19452(15) 0.0340(5) Uani d 1 . .
C C71 0.2769(3) 0.58840(7) 0.12162(18) 0.0362(6) Uani d 1 . .
C C72 0.3756(3) 0.61346(8) 0.1133(2) 0.0403(6) Uani d 1 . .
H H72 0.355116 0.627086 0.063102 0.048 Uiso calc 1 . .
C C73 0.5027(3) 0.61885(8) 0.1768(2) 0.0409(6) Uani d 1 . .
H H73 0.569491 0.636000 0.170536 0.049 Uiso calc 1 . .
C C74 0.5312(3) 0.59888(8) 0.2498(2) 0.0402(6) Uani d 1 . .
H H74 0.618290 0.602127 0.294180 0.048 Uiso calc 1 . .
C C75 0.4328(3) 0.57434(7) 0.25761(18) 0.0364(6) Uani d 1 . .
H H75 0.451851 0.560697 0.307813 0.044 Uiso calc 1 . .
C C76 0.1424(3) 0.57984(9) 0.0544(2) 0.0442(7) Uani d 1 . .
H H76A 0.149950 0.556819 0.034623 0.066 Uiso calc 1 . .
H H76B 0.131994 0.595263 0.005540 0.066 Uiso calc 1 . .
H H76C 0.056233 0.581794 0.078453 0.066 Uiso calc 1 . .
O O81 0.2256(2) 0.56159(5) 0.37630(13) 0.0377(4) Uani d 1 . .
N N81 0.2060(3) 0.56779(6) 0.45506(15) 0.0344(5) Uani d 1 . .
C C81 0.2607(4) 0.59684(8) 0.4944(2) 0.0445(7) Uani d 1 . .
C C82 0.2398(4) 0.60311(9) 0.5759(2) 0.0532(8) Uani d 1 . .
H H82 0.275400 0.623445 0.604265 0.064 Uiso calc 1 . .
C C83 0.1686(4) 0.58051(9) 0.6165(2) 0.0493(8) Uani d 1 . .
H H83 0.154145 0.585270 0.672016 0.059 Uiso calc 1 . .
C C84 0.1182(3) 0.55068(8) 0.57515(19) 0.0414(7) Uani d 1 . .
H H84 0.070081 0.534572 0.602321 0.050 Uiso calc 1 . .
C C85 0.1390(3) 0.54478(7) 0.49424(19) 0.0361(6) Uani d 1 . .
H H85 0.105963 0.524319 0.465635 0.043 Uiso calc 1 . .
C C86 0.3388(5) 0.61941(10) 0.4461(3) 0.0604(10) Uani d 1 . .
H H86A 0.425429 0.607893 0.436153 0.091 Uiso calc 1 . .
H H86B 0.369744 0.639797 0.479800 0.091 Uiso calc 1 . .
H H86C 0.272588 0.625365 0.390545 0.091 Uiso calc 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Co1 0.0293(2) 0.0352(2) 0.0326(2) -0.00107(18) 0.00656(18) -0.00012(18)
N1 0.0374(14) 0.0524(15) 0.0443(14) -0.0012(11) 0.0144(11) -0.0022(12)
C1 0.0345(15) 0.0467(16) 0.0352(14) 0.0014(12) 0.0029(12) -0.0006(12)
Se1 0.03537(18) 0.0772(3) 0.03717(17) 0.00101(16) 0.00861(13) 0.00799(16)
N2 0.0508(16) 0.0349(13) 0.0565(16) 0.0015(12) 0.0173(13) 0.0009(12)
C2 0.0350(15) 0.0401(15) 0.0394(14) -0.0072(12) 0.0130(12) -0.0054(12)
Se2 0.03332(16) 0.04557(17) 0.03953(16) 0.00037(12) 0.00586(12) 0.00369(13)
O11 0.0252(10) 0.0594(13) 0.0384(10) -0.0092(9) 0.0053(8) 0.0014(9)
N11 0.0258(11) 0.0396(12) 0.0383(12) -0.0030(9) 0.0080(9) -0.0060(10)
C11 0.0323(15) 0.0492(16) 0.0377(14) -0.0002(12) 0.0081(11) -0.0080(13)
C12 0.0297(15) 0.0510(17) 0.0459(16) 0.0020(12) 0.0039(12) -0.0121(14)
C13 0.0300(15) 0.0416(16) 0.067(2) -0.0044(12) 0.0099(14) -0.0127(15)
C14 0.0352(16) 0.0343(14) 0.065(2) -0.0014(12) 0.0143(14) -0.0021(14)
C15 0.0295(14) 0.0368(14) 0.0508(17) 0.0009(11) 0.0098(12) -0.0024(12)
C16 0.0357(16) 0.084(3) 0.0388(16) -0.0021(16) 0.0054(13) 0.0087(16)
O21 0.0314(11) 0.0444(12) 0.0667(15) 0.0046(9) 0.0153(10) 0.0183(11)
N21 0.0359(13) 0.0325(11) 0.0430(13) -0.0004(9) 0.0087(10) 0.0075(10)
C21 0.064(2) 0.056(2) 0.0451(18) -0.0266(18) 0.0046(16) 0.0075(15)
C22 0.094(3) 0.0383(17) 0.076(3) -0.0175(19) 0.053(3) -0.0129(17)
C23 0.079(3) 0.049(2) 0.082(3) 0.013(2) 0.042(2) 0.018(2)
C24 0.058(2) 0.075(3) 0.055(2) 0.0298(19) 0.0229(18) 0.0284(19)
C25 0.0399(17) 0.0553(18) 0.0366(15) 0.0067(14) 0.0061(12) 0.0069(13)
C26 0.050(2) 0.074(3) 0.078(3) -0.0026(19) 0.014(2) -0.016(2)
O31 0.0311(10) 0.0344(9) 0.0371(10) -0.0043(8) 0.0099(8) -0.0001(8)
N31 0.0272(11) 0.0329(11) 0.0316(11) -0.0007(9) 0.0078(9) -0.0018(9)
C31 0.0292(13) 0.0383(14) 0.0315(13) 0.0015(11) 0.0066(10) -0.0002(11)
C32 0.0371(15) 0.0378(14) 0.0376(14) 0.0008(11) 0.0120(11) 0.0037(11)
C33 0.0342(14) 0.0367(14) 0.0434(15) -0.0029(11) 0.0143(12) -0.0024(12)
C34 0.0285(14) 0.0414(14) 0.0372(14) -0.0016(11) 0.0062(11) -0.0062(11)
C35 0.0289(13) 0.0385(14) 0.0321(13) 0.0028(11) 0.0042(10) 0.0004(11)
C36 0.0333(15) 0.0616(19) 0.0323(14) -0.0040(13) 0.0036(11) 0.0033(13)
O41 0.0393(12) 0.0758(16) 0.0382(11) -0.0101(11) 0.0080(9) -0.0183(11)
N41 0.0452(15) 0.0552(16) 0.0322(12) -0.0049(12) 0.0074(11) -0.0044(11)
C41 0.0459(17) 0.0533(18) 0.0338(14) -0.0029(14) 0.0082(12) 0.0004(13)
C42 0.066(2) 0.0513(19) 0.0411(17) -0.0090(17) 0.0142(16) -0.0054(14)
C43 0.093(3) 0.062(2) 0.0349(16) -0.011(2) 0.0193(18) -0.0065(15)
C44 0.082(3) 0.062(2) 0.0416(18) -0.009(2) 0.0224(18) 0.0056(16)
C45 0.056(2) 0.058(2) 0.0395(16) -0.0083(16) 0.0112(14) 0.0010(15)
C46 0.052(2) 0.068(2) 0.0418(17) -0.0070(17) 0.0171(15) -0.0013(16)
Co2 0.0298(2) 0.0371(2) 0.0348(2) 0.00232(18) 0.00881(18) 0.00530(18)
N3 0.0324(13) 0.0460(14) 0.0431(13) 0.0058(10) 0.0126(11) 0.0073(11)
C3 0.0332(14) 0.0352(14) 0.0396(14) 0.0032(11) 0.0057(12) 0.0050(11)
Se3 0.03533(17) 0.04521(18) 0.04398(17) 0.00154(13) 0.01443(13) 0.00795(13)
N4 0.0429(14) 0.0413(13) 0.0428(13) 0.0078(11) 0.0143(11) 0.0071(11)
C4 0.0339(14) 0.0448(15) 0.0315(13) -0.0039(12) 0.0101(11) 0.0007(11)
Se4 0.04327(18) 0.03789(16) 0.03780(16) -0.00041(13) 0.00378(13) 0.00388(12)
O51 0.0297(10) 0.0599(13) 0.0411(11) -0.0058(9) 0.0044(8) 0.0130(10)
N51 0.0299(12) 0.0425(13) 0.0391(12) -0.0036(10) 0.0080(9) 0.0048(10)
C51 0.0354(15) 0.0400(14) 0.0363(14) -0.0005(12) 0.0079(11) 0.0040(12)
C52 0.0336(15) 0.0420(15) 0.0391(15) 0.0017(12) 0.0075(12) -0.0036(12)
C53 0.0349(15) 0.0416(15) 0.0512(17) -0.0037(12) 0.0176(13) -0.0086(13)
C54 0.0442(17) 0.0371(14) 0.0504(17) -0.0033(12) 0.0196(14) 0.0013(13)
C55 0.0426(17) 0.0418(15) 0.0440(16) 0.0023(13) 0.0131(13) 0.0090(13)
C56 0.0430(18) 0.060(2) 0.0491(18) -0.0083(15) -0.0005(14) 0.0199(16)
O61 0.0310(10) 0.0356(10) 0.0424(10) 0.0030(8) 0.0114(8) 0.0052(8)
N61 0.0332(12) 0.0338(11) 0.0372(12) 0.0012(9) 0.0138(9) 0.0042(9)
C61 0.0402(18) 0.0509(18) 0.062(2) -0.0072(14) 0.0186(15) -0.0162(16)
C62 0.050(2) 0.0446(18) 0.085(3) -0.0064(15) 0.0305(19) -0.0185(18)
C63 0.0441(18) 0.0400(16) 0.069(2) 0.0063(13) 0.0302(16) 0.0114(15)
C64 0.0376(16) 0.0554(18) 0.0449(16) 0.0079(14) 0.0124(13) 0.0098(14)
C65 0.0368(15) 0.0440(15) 0.0380(14) 0.0053(12) 0.0067(12) 0.0010(12)
C66 0.043(2) 0.128(5) 0.116(4) -0.008(3) 0.007(2) -0.080(4)
O71 0.0330(10) 0.0382(10) 0.0408(10) -0.0011(8) 0.0138(8) 0.0027(8)
N71 0.0307(12) 0.0377(12) 0.0358(11) 0.0014(9) 0.0123(9) 0.0024(9)
C71 0.0333(14) 0.0413(15) 0.0357(14) 0.0042(11) 0.0118(11) 0.0021(11)
C72 0.0393(16) 0.0438(15) 0.0394(14) 0.0040(12) 0.0127(12) 0.0062(12)
C73 0.0392(16) 0.0392(15) 0.0462(16) -0.0008(12) 0.0142(13) 0.0022(13)
C74 0.0322(15) 0.0482(16) 0.0396(15) 0.0016(12) 0.0075(12) -0.0014(13)
C75 0.0332(14) 0.0406(15) 0.0351(13) 0.0044(11) 0.0080(11) 0.0040(11)
C76 0.0359(16) 0.0599(19) 0.0373(15) -0.0003(14) 0.0099(12) 0.0044(14)
O81 0.0350(10) 0.0459(11) 0.0331(10) -0.0007(8) 0.0103(8) -0.0007(8)
N81 0.0330(12) 0.0372(12) 0.0322(11) 0.0029(9) 0.0066(9) 0.0020(9)
C81 0.0486(18) 0.0406(15) 0.0414(16) -0.0075(13) 0.0054(13) -0.0007(13)
C82 0.066(2) 0.0497(18) 0.0386(16) -0.0079(16) 0.0022(15) -0.0091(14)
C83 0.054(2) 0.061(2) 0.0305(14) 0.0028(16) 0.0052(13) -0.0016(14)
C84 0.0346(15) 0.0523(17) 0.0355(14) 0.0044(13) 0.0049(12) 0.0092(13)
C85 0.0314(14) 0.0367(14) 0.0382(14) 0.0017(11) 0.0046(11) 0.0043(11)
C86 0.073(3) 0.0489(19) 0.060(2) -0.0216(18) 0.0177(19) -0.0026(17)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co -2.3653 3.6143 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.7943 1.1372 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N2 Co1 N1 . . 92.43(11) y
N2 Co1 O11 . . 85.49(11) y
N2 Co1 O31 . . 95.84(10) y
O11 Co1 N1 . . 94.63(10) y
O21 Co1 N1 . . 86.10(10) y
O21 Co1 N2 . . 176.62(11) y
O21 Co1 O11 . . 91.58(10) y
O21 Co1 O31 . . 85.57(8) y
O21 Co1 O41 . . 92.05(10) y
O31 Co1 N1 . . 171.62(10) y
O31 Co1 O11 . . 84.73(8) y
O41 Co1 N1 . . 96.79(10) y
O41 Co1 N2 . . 91.15(12) y
O41 Co1 O11 . . 168.23(9) y
O41 Co1 O31 . . 84.39(8) y
C1 N1 Co1 . . 166.2(3) y
N1 C1 Se1 . . 179.1(3) ?
C2 N2 Co1 . . 151.9(3) y
N2 C2 Se2 . . 178.3(3) ?
N11 O11 Co1 . . 128.93(17) y
O11 N11 C11 . . 118.0(2) ?
O11 N11 C15 . . 120.1(2) ?
C15 N11 C11 . . 121.9(3) ?
N11 C11 C12 . . 118.1(3) ?
N11 C11 C16 . . 116.8(3) ?
C12 C11 C16 . . 125.0(3) ?
C11 C12 H12 . . 119.4 ?
C13 C12 C11 . . 121.2(3) ?
C13 C12 H12 . . 119.4 ?
C12 C13 H13 . . 120.8 ?
C12 C13 C14 . . 118.4(3) ?
C14 C13 H13 . . 120.8 ?
C13 C14 H14 . . 119.7 ?
C15 C14 C13 . . 120.6(3) ?
C15 C14 H14 . . 119.7 ?
N11 C15 C14 . . 119.7(3) ?
N11 C15 H15 . . 120.1 ?
C14 C15 H15 . . 120.1 ?
C11 C16 H16A . . 109.5 ?
C11 C16 H16B . . 109.5 ?
C11 C16 H16C . . 109.5 ?
H16A C16 H16B . . 109.5 ?
H16A C16 H16C . . 109.5 ?
H16B C16 H16C . . 109.5 ?
N21 O21 Co1 . . 121.76(17) y
O21 N21 C21 . . 121.3(3) ?
O21 N21 C25 . . 118.7(3) ?
C25 N21 C21 . . 120.0(3) ?
N21 C21 C22 . . 117.2(3) ?
N21 C21 C26 . . 120.6(4) ?
C22 C21 C26 . . 122.3(4) ?
C21 C22 H22 . . 119.1 ?
C23 C22 C21 . . 121.9(4) ?
C23 C22 H22 . . 119.1 ?
C22 C23 H23 . . 120.7 ?
C22 C23 C24 . . 118.6(4) ?
C24 C23 H23 . . 120.7 ?
C23 C24 H24 . . 119.2 ?
C23 C24 C25 . . 121.5(4) ?
C25 C24 H24 . . 119.2 ?
N21 C25 C24 . . 120.7(3) ?
N21 C25 H25 . . 119.6 ?
C24 C25 H25 . . 119.6 ?
C21 C26 H26A . . 109.5 ?
C21 C26 H26B . . 109.5 ?
C21 C26 H26C . . 109.5 ?
H26A C26 H26B . . 109.5 ?
H26A C26 H26C . . 109.5 ?
H26B C26 H26C . . 109.5 ?
N31 O31 Co1 . . 120.96(15) y
O31 N31 C31 . . 119.5(2) ?
O31 N31 C35 . . 118.6(2) ?
C31 N31 C35 . . 121.7(2) ?
N31 C31 C32 . . 118.5(3) ?
N31 C31 C36 . . 117.2(3) ?
C32 C31 C36 . . 124.3(3) ?
C31 C32 H32 . . 119.4 ?
C33 C32 C31 . . 121.2(3) ?
C33 C32 H32 . . 119.4 ?
C32 C33 H33 . . 120.7 ?
C32 C33 C34 . . 118.7(3) ?
C34 C33 H33 . . 120.7 ?
C33 C34 H34 . . 120.2 ?
C35 C34 C33 . . 119.6(3) ?
C35 C34 H34 . . 120.2 ?
N31 C35 C34 . . 120.4(3) ?
N31 C35 H35 . . 119.8 ?
C34 C35 H35 . . 119.8 ?
C31 C36 H36A . . 109.5 ?
C31 C36 H36B . . 109.5 ?
C31 C36 H36C . . 109.5 ?
H36A C36 H36B . . 109.5 ?
H36A C36 H36C . . 109.5 ?
H36B C36 H36C . . 109.5 ?
N41 O41 Co1 . . 124.68(19) y
O41 N41 C41 . . 119.5(3) ?
O41 N41 C45 . . 118.9(3) ?
C41 N41 C45 . . 121.6(3) ?
N41 C41 C42 . . 118.8(3) ?
N41 C41 C46 . . 118.2(3) ?
C42 C41 C46 . . 123.0(3) ?
C41 C42 H42 . . 119.4 ?
C43 C42 C41 . . 121.2(3) ?
C43 C42 H42 . . 119.4 ?
C42 C43 H43 . . 120.8 ?
C42 C43 C44 . . 118.4(3) ?
C44 C43 H43 . . 120.8 ?
C43 C44 H44 . . 120.1 ?
C45 C44 C43 . . 119.7(3) ?
C45 C44 H44 . . 120.1 ?
N41 C45 C44 . . 120.2(3) ?
N41 C45 H45 . . 119.9 ?
C44 C45 H45 . . 119.9 ?
C41 C46 H46A . . 109.5 ?
C41 C46 H46B . . 109.5 ?
C41 C46 H46C . . 109.5 ?
H46A C46 H46B . . 109.5 ?
H46A C46 H46C . . 109.5 ?
H46B C46 H46C . . 109.5 ?
N3 Co2 N4 . . 92.80(10) y
N3 Co2 O61 . . 85.67(9) y
N3 Co2 O71 . . 173.62(9) y
N3 Co2 O81 . . 95.39(9) y
O51 Co2 N3 . . 94.08(10) y
O51 Co2 N4 . . 88.66(10) y
O51 Co2 O61 . . 90.02(9) y
O51 Co2 O71 . . 84.49(9) y
O51 Co2 O81 . . 170.51(9) y
O61 Co2 N4 . . 177.90(9) y
O71 Co2 N4 . . 93.37(9) y
O71 Co2 O61 . . 88.12(8) y
O81 Co2 N4 . . 91.46(10) y
O81 Co2 O61 . . 90.12(8) y
O81 Co2 O71 . . 86.03(8) y
C3 N3 Co2 . . 167.6(2) y
N3 C3 Se3 . . 177.7(3) ?
C4 N4 Co2 . . 163.8(3) y
N4 C4 Se4 . . 178.5(3) ?
N51 O51 Co2 . . 123.32(18) y
O51 N51 C51 . . 118.8(2) ?
O51 N51 C55 . . 119.7(2) ?
C55 N51 C51 . . 121.5(3) ?
N51 C51 C52 . . 118.9(3) ?
N51 C51 C56 . . 116.8(3) ?
C52 C51 C56 . . 124.3(3) ?
C51 C52 H52 . . 119.4 ?
C51 C52 C53 . . 121.2(3) ?
C53 C52 H52 . . 119.4 ?
C52 C53 H53 . . 120.9 ?
C52 C53 C54 . . 118.2(3) ?
C54 C53 H53 . . 120.9 ?
C53 C54 H54 . . 120.0 ?
C55 C54 C53 . . 120.0(3) ?
C55 C54 H54 . . 120.0 ?
N51 C55 C54 . . 120.3(3) ?
N51 C55 H55 . . 119.9 ?
C54 C55 H55 . . 119.9 ?
C51 C56 H56A . . 109.5 ?
C51 C56 H56B . . 109.5 ?
C51 C56 H56C . . 109.5 ?
H56A C56 H56B . . 109.5 ?
H56A C56 H56C . . 109.5 ?
H56B C56 H56C . . 109.5 ?
N61 O61 Co2 . . 123.03(16) y
O61 N61 C61 . . 119.2(3) ?
O61 N61 C65 . . 119.8(2) ?
C65 N61 C61 . . 121.0(3) ?
N61 C61 C62 . . 118.5(3) ?
N61 C61 C66 . . 117.1(3) ?
C62 C61 C66 . . 124.4(3) ?
C61 C62 H62 . . 119.2 ?
C63 C62 C61 . . 121.7(3) ?
C63 C62 H62 . . 119.2 ?
C62 C63 H63 . . 120.7 ?
C62 C63 C64 . . 118.5(3) ?
C64 C63 H63 . . 120.7 ?
C63 C64 H64 . . 120.4 ?
C65 C64 C63 . . 119.3(3) ?
C65 C64 H64 . . 120.4 ?
N61 C65 C64 . . 120.8(3) ?
N61 C65 H65 . . 119.6 ?
C64 C65 H65 . . 119.6 ?
C61 C66 H66A . . 109.5 ?
C61 C66 H66B . . 109.5 ?
C61 C66 H66C . . 109.5 ?
H66A C66 H66B . . 109.5 ?
H66A C66 H66C . . 109.5 ?
H66B C66 H66C . . 109.5 ?
N71 O71 Co2 . . 120.08(16) y
O71 N71 C71 . . 119.4(2) ?
O71 N71 C75 . . 118.8(2) ?
C75 N71 C71 . . 121.7(3) ?
N71 C71 C72 . . 118.0(3) ?
N71 C71 C76 . . 117.5(3) ?
C72 C71 C76 . . 124.4(3) ?
C71 C72 H72 . . 119.4 ?
C73 C72 C71 . . 121.2(3) ?
C73 C72 H72 . . 119.4 ?
C72 C73 H73 . . 120.5 ?
C72 C73 C74 . . 118.9(3) ?
C74 C73 H73 . . 120.5 ?
C73 C74 H74 . . 120.3 ?
C75 C74 C73 . . 119.5(3) ?
C75 C74 H74 . . 120.3 ?
N71 C75 C74 . . 120.7(3) ?
N71 C75 H75 . . 119.6 ?
C74 C75 H75 . . 119.6 ?
C71 C76 H76A . . 109.5 ?
C71 C76 H76B . . 109.5 ?
C71 C76 H76C . . 109.5 ?
H76A C76 H76B . . 109.5 ?
H76A C76 H76C . . 109.5 ?
H76B C76 H76C . . 109.5 ?
N81 O81 Co2 . . 124.24(16) y
O81 N81 C81 . . 118.0(2) ?
O81 N81 C85 . . 119.8(2) ?
C85 N81 C81 . . 122.1(3) ?
N81 C81 C82 . . 117.7(3) ?
N81 C81 C86 . . 117.0(3) ?
C82 C81 C86 . . 125.4(3) ?
C81 C82 H82 . . 119.3 ?
C83 C82 C81 . . 121.5(3) ?
C83 C82 H82 . . 119.3 ?
C82 C83 H83 . . 120.5 ?
C82 C83 C84 . . 119.1(3) ?
C84 C83 H83 . . 120.5 ?
C83 C84 H84 . . 120.5 ?
C85 C84 C83 . . 119.0(3) ?
C85 C84 H84 . . 120.5 ?
N81 C85 C84 . . 120.6(3) ?
N81 C85 H85 . . 119.7 ?
C84 C85 H85 . . 119.7 ?
C81 C86 H86A . . 109.5 ?
C81 C86 H86B . . 109.5 ?
C81 C86 H86C . . 109.5 ?
H86A C86 H86B . . 109.5 ?
H86A C86 H86C . . 109.5 ?
H86B C86 H86C . . 109.5 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Co1 N1 . 2.105(3) y
Co1 N2 . 2.096(3) y
Co1 O11 . 2.104(2) y
Co1 O21 . 2.081(2) y
Co1 O31 . 2.103(2) y
Co1 O41 . 2.086(2) y
N1 C1 . 1.149(4) ?
C1 Se1 . 1.805(3) ?
N2 C2 . 1.157(4) ?
C2 Se2 . 1.798(3) ?
O11 N11 . 1.325(3) ?
N11 C11 . 1.370(4) ?
N11 C15 . 1.352(4) ?
C11 C12 . 1.380(4) ?
C11 C16 . 1.493(5) ?
C12 H12 . 0.9500 ?
C12 C13 . 1.380(5) ?
C13 H13 . 0.9500 ?
C13 C14 . 1.383(5) ?
C14 H14 . 0.9500 ?
C14 C15 . 1.369(4) ?
C15 H15 . 0.9500 ?
C16 H16A . 0.9800 ?
C16 H16B . 0.9800 ?
C16 H16C . 0.9800 ?
O21 N21 . 1.322(3) ?
N21 C21 . 1.370(5) ?
N21 C25 . 1.344(4) ?
C21 C22 . 1.426(6) ?
C21 C26 . 1.444(6) ?
C22 H22 . 0.9500 ?
C22 C23 . 1.334(7) ?
C23 H23 . 0.9500 ?
C23 C24 . 1.341(6) ?
C24 H24 . 0.9500 ?
C24 C25 . 1.371(5) ?
C25 H25 . 0.9500 ?
C26 H26A . 0.9800 ?
C26 H26B . 0.9800 ?
C26 H26C . 0.9800 ?
O31 N31 . 1.330(3) ?
N31 C31 . 1.354(4) ?
N31 C35 . 1.359(3) ?
C31 C32 . 1.386(4) ?
C31 C36 . 1.488(4) ?
C32 H32 . 0.9500 ?
C32 C33 . 1.379(4) ?
C33 H33 . 0.9500 ?
C33 C34 . 1.392(4) ?
C34 H34 . 0.9500 ?
C34 C35 . 1.373(4) ?
C35 H35 . 0.9500 ?
C36 H36A . 0.9800 ?
C36 H36B . 0.9800 ?
C36 H36C . 0.9800 ?
O41 N41 . 1.338(3) ?
N41 C41 . 1.347(4) ?
N41 C45 . 1.364(4) ?
C41 C42 . 1.386(4) ?
C41 C46 . 1.490(5) ?
C42 H42 . 0.9500 ?
C42 C43 . 1.382(5) ?
C43 H43 . 0.9500 ?
C43 C44 . 1.392(6) ?
C44 H44 . 0.9500 ?
C44 C45 . 1.376(5) ?
C45 H45 . 0.9500 ?
C46 H46A . 0.9800 ?
C46 H46B . 0.9800 ?
C46 H46C . 0.9800 ?
Co2 N3 . 2.096(3) y
Co2 N4 . 2.115(3) y
Co2 O51 . 2.092(2) y
Co2 O61 . 2.109(2) y
Co2 O71 . 2.102(2) y
Co2 O81 . 2.098(2) y
N3 C3 . 1.150(4) ?
C3 Se3 . 1.806(3) ?
N4 C4 . 1.155(4) ?
C4 Se4 . 1.805(3) ?
O51 N51 . 1.330(3) ?
N51 C51 . 1.361(4) ?
N51 C55 . 1.350(4) ?
C51 C52 . 1.374(4) ?
C51 C56 . 1.495(4) ?
C52 H52 . 0.9500 ?
C52 C53 . 1.384(4) ?
C53 H53 . 0.9500 ?
C53 C54 . 1.391(5) ?
C54 H54 . 0.9500 ?
C54 C55 . 1.371(5) ?
C55 H55 . 0.9500 ?
C56 H56A . 0.9800 ?
C56 H56B . 0.9800 ?
C56 H56C . 0.9800 ?
O61 N61 . 1.332(3) ?
N61 C61 . 1.353(4) ?
N61 C65 . 1.351(4) ?
C61 C62 . 1.383(5) ?
C61 C66 . 1.485(6) ?
C62 H62 . 0.9500 ?
C62 C63 . 1.366(6) ?
C63 H63 . 0.9500 ?
C63 C64 . 1.385(5) ?
C64 H64 . 0.9500 ?
C64 C65 . 1.376(4) ?
C65 H65 . 0.9500 ?
C66 H66A . 0.9800 ?
C66 H66B . 0.9800 ?
C66 H66C . 0.9800 ?
O71 N71 . 1.333(3) ?
N71 C71 . 1.362(4) ?
N71 C75 . 1.353(4) ?
C71 C72 . 1.391(4) ?
C71 C76 . 1.483(4) ?
C72 H72 . 0.9500 ?
C72 C73 . 1.380(4) ?
C73 H73 . 0.9500 ?
C73 C74 . 1.384(4) ?
C74 H74 . 0.9500 ?
C74 C75 . 1.373(4) ?
C75 H75 . 0.9500 ?
C76 H76A . 0.9800 ?
C76 H76B . 0.9800 ?
C76 H76C . 0.9800 ?
O81 N81 . 1.340(3) ?
N81 C81 . 1.358(4) ?
N81 C85 . 1.351(4) ?
C81 C82 . 1.387(5) ?
C81 C86 . 1.491(5) ?
C82 H82 . 0.9500 ?
C82 C83 . 1.377(5) ?
C83 H83 . 0.9500 ?
C83 C84 . 1.387(5) ?
C84 H84 . 0.9500 ?
C84 C85 . 1.375(4) ?
C85 H85 . 0.9500 ?
C86 H86A . 0.9800 ?
C86 H86B . 0.9800 ?
C86 H86C . 0.9800 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
C15 H15 O21 . 0.95 2.36 3.158(4) 141
C26 H26C O11 . 0.98 2.49 3.367(5) 149
C35 H35 Se1 1_655 0.95 2.96 3.748(3) 141
C36 H36C O11 . 0.98 2.55 3.281(4) 131
C42 H42 Se3 3_666 0.95 2.87 3.811(4) 171
C52 H52 Se2 3_565 0.95 3.05 3.926(3) 153
C55 H55 O61 . 0.95 2.45 3.245(4) 141
C56 H56B Se2 3_565 0.98 3.02 3.933(3) 156
C65 H65 O81 . 0.95 2.40 3.140(4) 135
C66 H66A Se2 1_455 0.98 3.14 3.807(5) 126
C75 H75 Se3 1_655 0.95 2.95 3.726(3) 140
C75 H75 O81 . 0.95 2.62 3.075(3) 110
C76 H76C O51 . 0.98 2.61 3.354(4) 133
C86 H86B Se1 3_666 0.98 3.14 4.109(4) 169
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
Co1 O11 N11 C11 . . . . 151.0(2) ?
Co1 O11 N11 C15 . . . . -31.1(4) ?
Co1 O21 N21 C21 . . . . -99.2(3) ?
Co1 O21 N21 C25 . . . . 82.3(3) ?
Co1 O31 N31 C31 . . . . -95.3(2) ?
Co1 O31 N31 C35 . . . . 88.6(3) ?
Co1 O41 N41 C41 . . . . -117.7(3) ?
Co1 O41 N41 C45 . . . . 63.6(4) ?
O11 N11 C11 C12 . . . . 175.4(3) ?
O11 N11 C11 C16 . . . . -5.4(4) ?
O11 N11 C15 C14 . . . . -177.4(3) ?
N11 C11 C12 C13 . . . . 3.0(5) ?
C11 N11 C15 C14 . . . . 0.3(4) ?
C11 C12 C13 C14 . . . . -1.6(5) ?
C12 C13 C14 C15 . . . . -0.5(5) ?
C13 C14 C15 N11 . . . . 1.1(5) ?
C15 N11 C11 C12 . . . . -2.4(4) ?
C15 N11 C11 C16 . . . . 176.8(3) ?
C16 C11 C12 C13 . . . . -176.1(3) ?
O21 N21 C21 C22 . . . . -174.0(3) ?
O21 N21 C21 C26 . . . . 4.8(5) ?
O21 N21 C25 C24 . . . . 175.0(3) ?
N21 C21 C22 C23 . . . . -2.6(5) ?
C21 N21 C25 C24 . . . . -3.5(5) ?
C21 C22 C23 C24 . . . . -0.4(6) ?
C22 C23 C24 C25 . . . . 1.5(6) ?
C23 C24 C25 N21 . . . . 0.4(6) ?
C25 N21 C21 C22 . . . . 4.5(4) ?
C25 N21 C21 C26 . . . . -176.7(3) ?
C26 C21 C22 C23 . . . . 178.6(4) ?
O31 N31 C31 C32 . . . . -177.0(2) ?
O31 N31 C31 C36 . . . . 0.1(4) ?
O31 N31 C35 C34 . . . . 176.7(2) ?
N31 C31 C32 C33 . . . . 0.8(4) ?
C31 N31 C35 C34 . . . . 0.7(4) ?
C31 C32 C33 C34 . . . . -0.2(4) ?
C32 C33 C34 C35 . . . . -0.2(4) ?
C33 C34 C35 N31 . . . . -0.1(4) ?
C35 N31 C31 C32 . . . . -1.1(4) ?
C35 N31 C31 C36 . . . . 176.1(3) ?
C36 C31 C32 C33 . . . . -176.2(3) ?
O41 N41 C41 C42 . . . . -177.2(3) ?
O41 N41 C41 C46 . . . . 2.4(5) ?
O41 N41 C45 C44 . . . . 178.6(3) ?
N41 C41 C42 C43 . . . . -1.8(6) ?
C41 N41 C45 C44 . . . . 0.0(6) ?
C41 C42 C43 C44 . . . . 0.8(7) ?
C42 C43 C44 C45 . . . . 0.5(7) ?
C43 C44 C45 N41 . . . . -1.0(6) ?
C45 N41 C41 C42 . . . . 1.4(5) ?
C45 N41 C41 C46 . . . . -179.0(3) ?
C46 C41 C42 C43 . . . . 178.6(4) ?
Co2 O51 N51 C51 . . . . 128.0(2) ?
Co2 O51 N51 C55 . . . . -53.5(4) ?
Co2 O61 N61 C61 . . . . -115.5(3) ?
Co2 O61 N61 C65 . . . . 66.0(3) ?
Co2 O71 N71 C71 . . . . -95.9(3) ?
Co2 O71 N71 C75 . . . . 88.0(3) ?
Co2 O81 N81 C81 . . . . -125.5(2) ?
Co2 O81 N81 C85 . . . . 57.2(3) ?
O51 N51 C51 C52 . . . . 177.0(3) ?
O51 N51 C51 C56 . . . . -2.7(4) ?
O51 N51 C55 C54 . . . . -178.2(3) ?
N51 C51 C52 C53 . . . . 1.8(5) ?
C51 N51 C55 C54 . . . . 0.2(5) ?
C51 C52 C53 C54 . . . . -0.8(5) ?
C52 C53 C54 C55 . . . . -0.4(5) ?
C53 C54 C55 N51 . . . . 0.7(5) ?
C55 N51 C51 C52 . . . . -1.5(5) ?
C55 N51 C51 C56 . . . . 178.8(3) ?
C56 C51 C52 C53 . . . . -178.5(3) ?
O61 N61 C61 C62 . . . . -175.1(3) ?
O61 N61 C61 C66 . . . . 5.1(5) ?
O61 N61 C65 C64 . . . . 174.1(3) ?
N61 C61 C62 C63 . . . . 0.1(6) ?
C61 N61 C65 C64 . . . . -4.3(5) ?
C61 C62 C63 C64 . . . . -2.5(6) ?
C62 C63 C64 C65 . . . . 1.7(5) ?
C63 C64 C65 N61 . . . . 1.7(5) ?
C65 N61 C61 C62 . . . . 3.4(5) ?
C65 N61 C61 C66 . . . . -176.5(4) ?
C66 C61 C62 C63 . . . . 179.9(5) ?
O71 N71 C71 C72 . . . . -176.0(2) ?
O71 N71 C71 C76 . . . . 1.0(4) ?
O71 N71 C75 C74 . . . . 175.7(3) ?
N71 C71 C72 C73 . . . . 0.2(4) ?
C71 N71 C75 C74 . . . . -0.3(4) ?
C71 C72 C73 C74 . . . . -0.1(5) ?
C72 C73 C74 C75 . . . . -0.2(5) ?
C73 C74 C75 N71 . . . . 0.4(5) ?
C75 N71 C71 C72 . . . . 0.0(4) ?
C75 N71 C71 C76 . . . . 176.9(3) ?
C76 C71 C72 C73 . . . . -176.5(3) ?
O81 N81 C81 C82 . . . . 179.9(3) ?
O81 N81 C81 C86 . . . . -0.2(4) ?
O81 N81 C85 C84 . . . . 179.9(3) ?
N81 C81 C82 C83 . . . . 1.2(5) ?
C81 N81 C85 C84 . . . . 2.7(4) ?
C81 C82 C83 C84 . . . . 0.7(6) ?
C82 C83 C84 C85 . . . . -0.9(5) ?
C83 C84 C85 N81 . . . . -0.7(4) ?
C85 N81 C81 C82 . . . . -2.9(5) ?
C85 N81 C81 C86 . . . . 177.0(3) ?
C86 C81 C82 C83 . . . . -178.7(4) ?