#------------------------------------------------------------------------------
#$Date: 2024-07-10 04:51:59 +0300 (Wed, 10 Jul 2024) $
#$Revision: 293350 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/31/2023191.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023191
loop_
_publ_author_name
'Abu-Zaied, Mamdouh A.'
'Nawwar, Galal A.'
'Elgemeie, Galal H.'
'Jones, Peter G.'
_publ_section_title
;
 Crystal structures of four thioglycosides involving carbamimidothioate
 groups
;
_journal_coeditor_code           YZ2056
_journal_issue                   8
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi               10.1107/S2056989024006455
_journal_volume                  80
_journal_year                    2024
_chemical_absolute_configuration ad
_chemical_formula_iupac          'C22 H25 N3 O9 S'
_chemical_formula_moiety         'C22 H25 N3 O9 S'
_chemical_formula_sum            'C22 H25 N3 O9 S'
_chemical_formula_weight         507.51
_chemical_name_systematic
;
2',3',4',6'-Tetra-<i>O</i>-acetyl-\b-<i>D</i>-glucopyranosyl
<i>N</i>'-cyano-<i>N</i>-phenylcarbamimidothioate
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           19
_space_group_name_Hall           'P 2ac 2ab'
_space_group_name_H-M_alt        'P 21 21 21'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     dual
_audit_creation_method           SHELXL-2019/3
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   7.11266(11)
_cell_length_b                   13.76500(18)
_cell_length_c                   24.3850(3)
_cell_measurement_reflns_used    133018
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      45.0590
_cell_measurement_theta_min      2.2110
_cell_volume                     2387.43(6)
_computing_cell_refinement
;
CrysAlisPro 1.171.42.79a (Rigaku OD, 2023)
;
_computing_data_collection
;
CrysAlisPro 1.171.42.79a (Rigaku OD, 2023)
;
_computing_data_reduction
;
CrysAlisPro 1.171.42.79a (Rigaku OD, 2023)
;
_computing_molecular_graphics
;
XP, Version 5.1 (Bruker, 1998)
;
_computing_publication_material
;
<i>SHELXL2019/3</i> (Sheldrick, 2015b)
;
_computing_structure_refinement
;
<i>SHELXL2019/3</i> (Sheldrick, 2015b)
;
_computing_structure_solution
;
<i>SHELXT</i> (Sheldrick, 2015a)
;
_diffrn_ambient_temperature      99.9(8)
_diffrn_detector                 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB Synergy'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0740
_diffrn_reflns_av_unetI/netI     0.0215
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       48
_diffrn_reflns_limit_l_min       -48
_diffrn_reflns_number            316930
_diffrn_reflns_theta_full        44.000
_diffrn_reflns_theta_max         44.912
_diffrn_reflns_theta_min         2.231
_diffrn_source                   'micro-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu    0.193
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.87330
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
(CrysAlisPro; Rigaku OD, 2023)
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.412
_exptl_crystal_description       tablet
_exptl_crystal_F_000             1064
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.12
_refine_diff_density_max         0.482
_refine_diff_density_min         -0.210
_refine_ls_abs_structure_details
;
Flack <i>x</i> determined using 7711 quotients
[(<i>I</i>^+^)-(<i>I</i>^-^)]/[(<i>I</i>^+^)+(<i>I</i>^-^)]
(Parsons <i>et al.</i>,  2013)
;
_refine_ls_abs_structure_Flack   0.000(9)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.056
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     338
_refine_ls_number_reflns         19593
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.056
_refine_ls_R_factor_all          0.0329
_refine_ls_R_factor_gt           0.0286
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0480P)^2^+0.0766P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0763
_refine_ls_wR_factor_ref         0.0787
_reflns_number_gt                17947
_reflns_number_total             19593
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            yz2056.cif
_cod_data_source_block           5a
_cod_original_cell_volume        2387.44(6)
_cod_database_code               2023191
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.959
_shelx_estimated_absorpt_t_max   0.977
_shelx_hkl_file
;
   0   0   3 1.60018 0.37738  14
   0   0   3 2.71054 0.50040  12
   0   0   3 1.79862 0.46588  23
   0   0  -3 0.53400 0.38965  23
   0   0   3 0.62446 0.44312  16
   0   0  -3 0.45958 0.42857  16
   0   0  -3 0.66381 0.46368   8
   0   0   3 0.79685 0.44113   7
   0   0  -3 1.18906 0.44031   9
   0   0  -3 0.43037 0.43620   7
   0   0   3 0.97721 0.33902   6
   0   0   3 0.12611 0.41548   8
   0   0   4 16755.7 1059.30  12
   0   0   4 16282.2 1059.26  14
   0   0   4 16778.7 1059.19  11
   0   0  -4 15925.2 1059.27  23
   0   0   4 17151.4 1059.29  23
   0   0  -4 13404.9 1059.26  16
   0   0   4 15619.5 1059.28  16
   0   0   4 16615.5 1059.30   8
   0   0   4 19038.7 1059.25   6
   0   0   4 16944.8 1059.31   7
   0   0  -4 19234.8 1059.32   9
   0   0  -4 15752.7 1059.28   7
   0   0  -4 15998.3 1059.28   8
   0   0   5 1.93326 0.84242   7
   0   0  -5 1.27617 0.86946   7
   0   0  -5 1.55915 0.80180   9
   0   0   5 1.65458 0.79500   8
   0   0  -5 0.31800 0.78487   8
   0   0   5 0.69350 0.62092   6
   0   0   5 1.11104 0.43807  34
   0   0  -5 2.20764 0.47223  24
   0   0   5 1.34706 0.46718  11
   0   0   5 2.09436 0.78601  23
   0   0  -5 0.92874 0.79469  23
   0   0   5 1.08300 0.85432  16
   0   0  -5 1.71187 0.82521  16
   0   0   5 7.18197 0.88154  12
   0   0   5 0.51074 0.68824  14
   0   0  -6 17.5563 1.75730   9
   0   0   6 18.8293 1.59725   6
   0   0   6 19.3079 1.80378   8
   0   0   6 17.9305 1.79689   7
   0   0   6 23.9941 1.47927  34
   0   0  -6 21.1816 1.48439  34
   0   0  -6 20.9605 1.48256  24
   0   0  -6 18.4797 1.47980  11
   0   0   6 18.1893 1.48282  11
   0   0   6 17.3197 1.75849  23
   0   0  -6 20.1152 1.80041  16
   0   0   6 20.1408 1.69808  14
   0   0  -7 1.95177 1.13940   9
   0   0   7 1.85758 1.07617   8
   0   0   7-0.10278 0.99724   7
   0   0   7 1.31439 0.84001   6
   0   0  -7 0.35097 0.54956  34
   0   0  -7 0.23829 0.54830  24
   0   0  -7 0.43596 0.88209  10
   0   0  -7 0.93399 0.58132  11
   0   0   7 0.36398 0.60689  11
   0   0   7 1.60376 1.08283  23
   0   0  -7 1.84384 1.06618  16
   0   0   7-0.80918 0.89313  14
   0   0  -7 3.73534 0.94874  14
   0   0   8 2078.56 125.448   7
   0   0  -8 2151.92 125.445   9
   0   0   8 2154.89 125.471   8
   0   0  -8 1930.48 125.282   6
   0   0  -8 2095.46 125.182  34
   0   0  -8 1703.94 125.154  24
   0   0   8 1870.35 125.173  11
   0   0  -8 1744.92 125.171  11
   0   0   8 2047.24 125.419  23
   0   0  -8 2593.22 125.550  16
   0   0   8 2106.26 125.372  14
   0   0  -9 1.21572 0.82402   6
   0   0  -9 1.28888 1.08035   9
   0   0   9 1.77318 1.00201   8
   0   0   9 0.40627 1.15509   7
   0   0  -9 0.84551 0.57051  34
   0   0  -9 0.34937 0.56977  24
   0   0   9 0.72647 0.86259  26
   0   0  -9 0.43462 0.60170  11
   0   0   9 0.10256 0.58529  11
   0   0   9 3.25359 1.05209  23
   0   0  -9 0.67511 1.05872  16
   0   0   9 0.53062 0.93880  14
   0   0  10 3212.47 213.219   7
   0   0  10 3011.53 213.194   8
   0   0 -10 2619.09 212.987   6
   0   0 -10 2962.81 213.164   9
   0   0 -10 3577.53 212.917  34
   0   0  10 3211.82 213.099  26
   0   0 -10 3506.93 212.913  24
   0   0 -10 3512.89 212.938  11
   0   0  10 3608.71 212.928  11
   0   0  10 3714.59 213.248  23
   0   0 -10 3286.72 213.231  16
   0   0  10 3178.37 213.106  14
   0   0 -11 3.44585 1.22375   6
   0   0 -11 3.08155 1.58973   9
   0   0  11 1.19817 1.44254   8
   0   0  11 1.35869 1.48904   7
   0   0 -11 0.23886 0.72216  34
   0   0 -11-0.53299 0.71723  24
   0   0  11 0.38324 0.98452  26
   0   0 -11 0.46398 0.82828  11
   0   0  11 0.43183 0.79140  11
   0   0  11 1.41456 1.45102  23
   0   0 -11 1.35386 1.51958  16
   0   0 -11 1.93488 0.93521  15
   0   0  11-0.13222 1.14691  14
   0   0 -12 5752.70 348.232  34
   0   0 -12 5997.06 348.241  24
   0   0  12 5245.38 348.465  26
   0   0 -12 5383.17 348.248  11
   0   0  12 4907.64 348.548  23
   0   0  12 5262.49 348.626   8
   0   0 -12 5451.92 348.414   6
   0   0 -12 5295.97 348.595   9
   0   0 -12 5054.57 348.273  15
   0   0  12 5410.33 348.499  14
   0   0 -13 1.51199 0.82605  34
   0   0  13 0.75982 1.21374  26
   0   0 -13 1.81144 1.48837  29
   0   0 -13 0.87901 0.80103  24
   0   0 -13 1.47418 0.89139  11
   0   0  13 2.49461 1.56583  23
   0   0  13 1.86864 1.54375   8
   0   0 -13 2.83636 1.29082   6
   0   0 -13 0.79034 1.60706   9
   0   0 -13 1.28571 1.01438  15
   0   0  13 0.95273 1.31682  14
   0   0 -14 4274.96 255.957  34
   0   0  14 3908.62 256.257  26
   0   0 -14 4203.55 255.949  24
   0   0 -14 4369.86 256.373  29
   0   0 -14 3820.72 255.967  11
   0   0  14 3580.62 256.340  23
   0   0  14 4079.28 256.498   8
   0   0 -14 4189.49 256.482   9
   0   0 -14 3509.21 256.119   6
   0   0 -14 3937.85 256.028  15
   0   0  14 4036.12 256.305  14
   0   0 -15 1.98305 0.81406  34
   0   0  15 0.17639 1.34223  26
   0   0 -15 2.92414 1.54043  29
   0   0 -15 0.37014 0.83136  24
   0   0 -15 2.03784 0.97800  11
   0   0  15 1.37413 1.74715  23
   0   0 -15 2.82653 1.84759   9
   0   0 -15 0.15052 1.23778   6
   0   0  15 3.44812 1.85820   8
   0   0 -15 2.86438 1.05521  15
   0   0  15 0.55846 1.42633  14
   0   0 -16 63.1160 4.52282  34
   0   0  16 63.5249 4.94336  26
   0   0 -16 78.1885 5.24539  29
   0   0 -16 64.9810 4.51895  24
   0   0 -16 61.5568 4.58260  11
   0   0  16 55.0106 5.10858  23
   0   0 -16 74.5097 4.97667   6
   0   0 -16 69.0762 5.31458   9
   0   0  16 62.5659 5.28021   8
   0   0  16 65.7659 5.06492  14
   0   0 -16 71.9648 4.72285  15
   0   0 -17 5.16657 1.07754  34
   0   0  17 2.61160 1.63451  26
   0   0 -17 3.69521 1.10359  24
   0   0 -17 5.44179 2.10050  29
   0   0 -17 3.15210 1.19252  11
   0   0  17 6.94441 2.31895  23
   0   0 -17 6.21556 2.03207  21
   0   0 -17 4.66975 2.36409   9
   0   0 -17 3.96786 1.74895   6
   0   0  17 2.58077 1.94527   8
   0   0 -17 6.82839 1.47649  15
   0   0  17 2.99814 1.81476  14
   0   0 -18 7490.01 471.860  34
   0   0 -18 7402.48 472.421  29
   0   0  18 7236.50 472.298  26
   0   0 -18 7591.99 471.847  24
   0   0 -18 6542.27 471.890  11
   0   0  18 7146.99 472.541  23
   0   0 -18 6598.11 472.487   9
   0   0 -18 7094.77 472.186   6
   0   0  18 7251.86 472.610   8
   0   0  18 7248.12 472.364  14
   0   0 -18 7966.57 472.040  15
   0   0 -19 11.1285 1.31890  34
   0   0  19 6.52987 2.05480  26
   0   0 -19 8.85684 2.48259  29
   0   0 -19 6.48619 1.24603  24
   0   0 -19 5.81566 1.42825  11
   0   0 -19 8.35015 2.49598  21
   0   0  19 12.3388 2.75521  23
   0   0 -19 7.20504 1.98282   6
   0   0  19 3.29161 2.39075   8
   0   0 -19 9.21817 2.53001   9
   0   0 -19 7.99630 1.69356  15
   0   0  19 6.30966 2.26072  14
   0   0 -20 2189.41 136.590  34
   0   0 -20 2071.09 136.554  24
   0   0  20 2080.69 137.127  26
   0   0 -20 2165.22 137.274  29
   0   0 -20 2162.88 136.679  11
   0   0 -20 2126.75 137.244  21
   0   0  20 1895.09 137.309  23
   0   0 -20 2227.31 137.039   6
   0   0 -20 2061.94 137.408   9
   0   0  20 2026.10 137.476   8
   0   0  20 2129.08 137.197  14
   0   0 -20 2256.60 136.802  15
   0   0  21 2.24099 1.92118  26
   0   0 -21-0.15499 1.03032  24
   0   0 -21 4.42015 2.31953  29
   0   0 -21 4.03353 1.37877  11
   0   0 -21 4.84970 2.46221  21
   0   0  21 6.34163 2.45477  23
   0   0 -21 1.95337 1.94712   6
   0   0 -21 2.18514 2.61255   9
   0   0  21 0.74717 2.28049   8
   0   0  21 2.98764 2.31146  14
   0   0 -21 0.72534 1.50204  15
   0   0 -22 279.150 18.0019  29
   0   0  22 272.931 17.7427  26
   0   0 -22 242.598 16.9869  24
   0   0 -22 270.730 17.1877  11
   0   0  22 258.351 18.0945  23
   0   0 -22 298.405 18.0008  21
   0   0 -22 254.220 18.1822   9
   0   0  22 264.176 18.1848   8
   0   0 -22 287.003 17.6677   6
   0   0 -22 249.670 17.2864  15
   0   0 -23 0.33188 2.39173  29
   0   0  23 0.81743 1.90930  26
   0   0 -23-0.12101 1.32042  11
   0   0  23 2.39183 2.80115  23
   0   0 -23 5.35649 1.04906  24
   0   0 -23 2.54460 2.48697  21
   0   0 -23 2.39491 2.10350   6
   0   0  23 5.04048 2.56395   8
   0   0 -23 0.41028 2.64108   9
   0   0 -23 0.15557 1.65133  15
   0   0 -24 63.7320 5.81675  29
   0   0  24 70.9185 5.45209  26
   0   0 -24 60.7136 4.69037  11
   0   0 -24 82.2600 6.27022   9
   0   0 -24 50.5109 5.52680  21
   0   0  24 66.6372 6.14798  23
   0   0 -24 63.5532 4.88509  15
   0   0 -24 71.8989 5.38176   6
   0   0  24 59.5103 5.89976   8
   0   0  25 1.47320 2.15207  26
   0   0 -25-1.11189 2.77712  29
   0   0 -25 2.72508 1.43518  11
   0   0  25 4.00931 3.09113  23
   0   0 -25 7.01776 2.90817  21
   0   0 -25 3.26473 1.67634  15
   0   0 -25 1.82979 2.22790   6
   0   0 -25 5.54522 3.00524   9
   0   0  25 0.46843 3.00081   8
   0   0 -26 660.707 44.2438   6
   0   0  26 681.898 45.0622   8
   0   0 -26 744.026 44.8269  29
   0   0  26 629.645 44.3092  26
   0   0 -26 578.604 44.8048   9
   0   0 -26 682.548 43.7356  11
   0   0 -26 781.389 44.8248  21
   0   0  26 692.216 45.0215  23
   0   0  26 656.345 45.0392  19
   0   0 -26 679.966 43.8851  15
   0   0 -27 7.00489 1.86356  15
   0   0 -27 6.98022 3.18515  29
   0   0  27 3.78360 2.44433  26
   0   0 -27 3.94026 1.46698  11
   0   0 -27 4.98436 3.02712  21
   0   0  27 6.94762 3.28218  23
   0   0  27 5.83904 3.42427  19
   0   0 -27 6.20760 3.62635   9
   0   0  27 2.07531 2.99306   8
   0   0 -27 0.28214 2.28747   6
   0   0 -28 587.447 38.8055   6
   0   0  28 585.047 39.6708   8
   0   0 -28 570.236 39.2685  29
   0   0  28 582.697 38.8960  26
   0   0 -28 590.568 39.7505   9
   0   0 -28 584.527 38.1753  11
   0   0  28 610.206 39.7004  23
   0   0 -28 665.742 39.3804  21
   0   0  28 588.632 39.7423  19
   0   0 -28 580.302 38.3282  15
   0   0 -29 1.80987 3.46060  29
   0   0  29 5.67896 2.74926  26
   0   0 -29 0.34880 1.46291  11
   0   0 -29 3.74445 3.21627  21
   0   0  29 2.19652 3.11513  23
   0   0  29 4.10067 3.69055  19
   0   0 -29 1.50577 2.42494   6
   0   0 -29 1.14942 3.34355   9
   0   0  29 2.27659 3.20754   8
   0   0 -30 44.7866 5.11642  29
   0   0  30 43.0952 5.25293  23
   0   0 -30 30.6191 4.77154  21
   0   0  30 35.5993 4.10436  26
   0   0  30 41.6368 5.46466  19
   0   0 -30 37.8955 5.15953   9
   0   0 -30 39.0866 4.17606   6
   0   0  30 45.8533 5.36013   8
   0   0 -31 18.3081 4.54765  29
   0   0  31 16.0837 3.37919  26
   0   0 -31 15.1816 4.27316  21
   0   0  31 18.7000 4.44342  23
   0   0  31 8.34886 4.18912  19
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  -1   1   9 429.357 26.7827   6
   1  -1   9 428.831 27.1799   8
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   1   1  -9 448.772 26.9357   6
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   1  -1   9 451.891 26.8037   2
   1   1  -9 443.385 26.7994   1
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   1   1  -9 406.499 26.9629  34
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   1   1  -9 559.458 27.2654  29
   1   1  -9 370.622 26.9785  24
   1   1  -9 407.003 26.8529  11
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   1   1  -9 396.632 26.8269  10
   1   1  -9 351.783 27.0762   9
   1  -1   9 424.071 27.1231  23
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   1   1  -9 421.620 26.8356  14
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   1   1  -9 413.224 26.9333  15
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   1   1  -8 1856.13 114.177   6
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   1  -1   8 1876.94 114.393   8
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   1   1  -8 1808.62 114.076   1
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   1   1  -8 2011.58 114.265  34
   1   1  -8 1727.68 114.325  29
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   1   1  -8 1903.47 114.294  24
   1   1  -8 1526.05 114.190  25
   1   1  -8 1834.08 114.387   9
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   1   1  -8 1826.87 114.079  10
   1   1  -8 1959.07 114.143  11
   1   1  -8 1659.87 114.366  22
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   1  -1   8 1968.41 114.374  23
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   1  -1   8 1832.65 114.228  17
   1   1  -8 1612.16 114.161  15
   1   1  -8 1659.78 114.071  14
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  -1   1   7 300.817 19.7862   6
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   1   4 -10 1002.60 60.2881   6
   1  -4  10 923.018 60.2943   8
   1   4 -10 864.684 60.0052   1
   1  -4  10 796.860 60.0072   2
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   1   4 -10 942.215 60.2943  26
   1   4 -10 1214.55 60.2208  25
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   1   4 -10 1115.24 60.5847   9
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  -1   4  10 893.082 60.3292  14
   1  -4   9 1867.49 118.946   8
   1  -4   9 1877.76 118.686   3
   1  -4   9 1979.23 118.777   2
   1   4  -9 2040.82 118.759   1
   1  -4   9 1915.83 118.910   4
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  -1   4   9 1884.75 118.893  32
   1   4  -9 1754.59 118.971  24
   1   4  -9 2468.27 118.923  25
   1   4  -9 1606.50 118.891  29
   1   4  -9 1886.82 118.960  26
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   1   4  -9 1782.51 118.837  11
   1   4  -9 2058.66 119.163   9
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   1   4  -9 1271.31 118.706  21
   1  -4   9 1739.03 118.583  17
   1  -4   9 1885.51 119.135  19
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   1  -4   8 154.225 10.5738   8
  -1  -4  -8 175.152 10.5154   4
   1  -4   8 153.588 10.3147   3
   1  -4   8 184.872 10.5104   2
   1  -4   8 158.948 10.5676   4
   1   4  -8 148.321 10.3912   1
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   1   4  -8 186.871 10.5501  25
   1   4  -8 142.930 10.6383  24
   1   4  -8 160.362 10.6393  26
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   1   4  -8 163.522 10.7541   9
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   1  -4   8 141.709 10.2173  17
   1  -4   8 156.730 10.7694  19
   1  -4   8 155.166 10.1241  15
  -1   4   8 171.769 10.7229  14
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   1  -4   7 1978.52 131.579   8
   1   4  -7 2038.98 131.333   8
   1  -4   7 2088.01 131.384   3
   1  -4   7 1972.62 131.473   2
   1  -4   7 1995.04 131.566   4
   1   4  -7 1949.30 131.439   1
  -1   4   7 1959.01 131.736  33
  -1   4   7 2232.07 131.693  31
   1   4  -7 2548.52 131.706  29
   1   4  -7 2517.46 131.610  25
   1   4  -7 2116.84 131.634  26
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  -1   4   7 2050.44 131.247  11
   1   4  -7 1970.83 131.711   9
  -1   4   7 1948.90 131.346  20
   1   4  -7 2139.34 131.542  21
   1  -4   7 2076.03 131.290  17
   1  -4   7 2112.45 131.756  19
   1  -4   7 2055.04 131.642  13
  -1   4   7 2074.00 131.669  14
   1  -4   7 1972.12 131.235  15
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  -1  -4  -6 566.353 36.7490   4
   1   4  -6 645.660 36.5791   8
   1  -4   6 576.270 36.8193   8
   1  -4   6 551.878 36.8156   4
   1  -4   6 579.984 36.7610   2
   1   4  -6 631.562 36.7753   1
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  -1   4   6 553.237 36.9725  33
   1  -4   6 534.796 36.6106  30
   1   4  -6 617.950 36.8470  29
   1   4  -6 604.213 36.8910  26
   1   4  -6 568.757 36.7869  25
   1   4  -6 579.278 36.5736  10
   1   4  -6 604.387 37.0008   9
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  -1   4   6 582.036 36.9063  10
  -1   4   6 584.419 36.6155  20
   1   4  -6 548.780 36.7688  21
   1   4  -6 425.921 36.4950  17
   1  -4   6 610.828 37.0199  19
   1  -4   6 586.682 36.5459  17
   1  -4   6 578.508 36.8815  13
  -1   4   6 590.195 36.9189  14
   1  -4   6 578.777 36.5363  15
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   1  -4   5 840.525 51.9148   2
   1   4  -5 728.474 51.9563   3
  -1   4   5 939.863 52.1914  33
   1  -4   5 909.992 51.7808  30
   1   4  -5 960.207 51.9967  25
   1   4  -5 849.531 51.9901  26
   1   4  -5 881.668 51.9401  29
   1   4  -5 664.800 51.9847   9
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  -1   4   5 821.367 52.0090  10
   1   4  -5 720.509 51.6958  10
  -1   4   5 842.331 51.7061  11
   1  -4   5 767.937 51.7219   9
   1   4  -5 835.462 51.9157  21
  -1   4   5 845.192 51.7530  20
  -1   4   5 792.847 51.6983  22
   1  -4   5 840.981 52.1104  19
   1  -4   5 898.981 51.7003  17
   1   4  -5 620.518 51.6525  17
   1  -4   5 850.883 51.7161  15
   1  -4   5 820.706 51.9778  13
  -1   4   5 839.086 52.0369  14
  -1   4   5 793.512 51.7863  16
  -1  -4  -4 1977.07 128.901   4
   1  -4   4 2013.80 128.936   2
   1   4  -4 1983.57 129.017   3
  -1   4   4 2347.43 129.178  33
  -1   4   4 2183.15 128.849  29
   1  -4   4 2003.04 128.783  30
   1   4  -4 2433.58 129.042  25
   1   4  -4 2861.02 129.035  29
   1   4  -4 2017.88 129.092   9
   1   4  -4 2002.09 128.955  11
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   1   4  -4 1823.25 128.747  10
   1  -4   4 1884.63 128.732   9
  -1  -4  -4 2092.37 129.067  12
  -1   4   4 2072.25 129.024  10
  -1   4   4 1901.72 128.709  22
  -1  -4  -4 2379.47 128.799  22
   1   4  -4 2309.27 128.773  17
   1  -4   4 2190.14 128.742  17
   1  -4   4 2018.17 129.097  19
  -1   4   4 1989.06 129.013  14
   1  -4   4 1971.29 128.975  13
   1   4  -4 2127.73 128.683  14
   1  -4   4 1843.80 128.751  15
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   1   4  -3 4041.28 249.315   3
   1  -4   3 3841.37 249.210   2
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   1   4  -3 3828.43 249.126  29
  -1   4   3 3883.20 249.353  33
   1   4  -3 4837.44 249.344  25
   1  -4   3 4618.91 249.456  27
  -1   4   3 3882.61 249.139  28
   1   4  -3 3461.26 249.294   9
  -1   4   3 3964.51 249.288  10
  -1   4   3 3755.92 249.066  11
  -1  -4  -3 4042.22 249.322  12
   1  -4   3 3924.71 249.005   9
   1   4  -3 4353.02 249.094  10
  -1  -4  -3 4063.62 249.041  22
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   1  -4   3 3965.61 249.366  19
   1   4  -3 3969.04 249.051  17
   1   4  -3 4166.02 249.012  14
   1  -4   3 3980.98 249.257  13
  -1   4   3 3942.74 249.278  14
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   1   4  -2 1641.75 102.714   3
   1  -4   2 1523.79 102.618   2
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   1   4  -2 1662.45 102.518  29
   1  -4   2 1602.42 102.765  27
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   1   4  -2 1833.06 102.790  28
   1  -4   2 1653.41 102.419   9
   1   4  -2 1494.23 102.492  10
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   1   4  -2 1347.74 102.679   9
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   1   4  -2 1764.08 102.588  22
   1   4  -2 1588.73 102.483  17
   1  -4   2 1610.68 102.757  19
   1   4  -2 1484.63 102.495  19
   1  -4   2 1690.02 102.669  13
   1   4  -2 1533.49 102.447  14
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  -1  -4  -1 1978.77 114.942   4
   1   4  -1 1989.89 115.036   3
   1   4  -1 1842.20 114.912   1
   1  -4   1 1762.17 114.918   2
  -1  -4  -1 1629.53 114.964  30
   1   4  -1 1960.64 114.778  29
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  -1   4   1 1710.38 114.844  28
   1   4  -1 1634.29 114.966  28
   1   4  -1 1888.73 114.773  27
   1  -4   1 1739.04 115.030  27
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   1  -4   1 1714.64 114.698   9
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   1   4  -1 1868.03 114.841  10
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   1   4  -1 1771.86 114.810  22
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   1  -4   1 1814.76 115.036  19
   1   4  -1 1855.30 114.808  17
   1   4  -1 1834.50 114.786  19
   1   4  -1 1807.42 114.788  14
   1  -4   1 1669.44 114.909  13
  -1   4   0 1211.17 81.5354   6
  -1  -4   0 1431.53 81.6919   4
   1  -4   0 1233.16 81.6466   2
   1   4   0 1230.28 81.6051   1
   1   4   0 1255.75 81.7005   3
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   1   4   0 1139.76 81.4309  29
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   1  -4   0 1311.74 81.7695  27
   1   4   0 1461.23 81.5311  27
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   1   4   0 1388.44 81.7777  28
  -1   4   0 1467.67 81.6490  28
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   1   4   0 1338.81 81.5956  10
   1   4   0 1335.08 81.5246  22
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   1   4   0 1149.98 81.4675  19
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  -1  -4   0 1709.35 81.5370  20
   1   4   0 1257.87 81.5456  17
   1   4   0 1332.49 81.5627  14
   1  -4   0 1285.40 81.6503  13
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   1  -4  -1 1747.84 113.064   4
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   1   4   1 1716.60 112.762   8
   1  -4  -1 1710.01 113.013   2
  -1  -4   1 1783.25 113.036   4
   1   4   1 1692.11 113.063   3
   1   4   1 1701.42 112.980   1
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  -1   4  -1 1729.06 113.105  33
  -1  -4   1 1505.83 113.030  30
   1   4   1 1758.67 112.777  29
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  -1  -4   1 1999.67 112.895  27
   1   4   1 1798.71 113.118  28
   1   4   1 1849.58 112.885  27
   1   4   1 1772.47 112.918  26
   1  -4  -1 1734.75 113.114  27
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  -1   4  -1 2022.13 113.011  11
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   1   4   1 2076.70 112.909  22
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   1   4   1 1677.04 112.840  19
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   1  -4  -1 1667.20 112.997  13
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   1  -4  -2 1662.09 109.091   4
   1   4   2 1705.47 108.827   8
   1  -4  -2 1645.01 108.844   6
  -1  -4   2 1663.58 108.804   7
   1   4   2 1724.30 109.009   1
   1   4   2 1813.77 109.122   3
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  -1  -4   2 1727.39 109.072   4
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   1   4   2 1798.38 108.764  29
  -1   4  -2 1742.53 108.893  30
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   1   4   2 1562.74 108.886  26
   1  -4  -2 1646.08 109.130  27
   1  -4  -2 1520.00 108.882  28
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   1   4   2 1956.12 108.953  27
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  -1  -4   2 1755.02 108.888  10
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  -1   4  -2 1718.60 108.834   9
   1  -4  -2 1782.62 108.930  20
   1   4   2 1729.40 108.868  22
  -1  -4   2 1849.64 108.980  19
   1   4   2 1853.19 108.888  19
  -1   4  -2 1550.37 108.840  17
  -1  -4   2 1542.95 108.812  14
   1  -4  -2 1686.87 109.023  13
   1  -4  -3 3886.58 256.632   6
  -1   4  -3 3793.81 256.799   6
   1   4   3 4008.30 256.682   8
  -1  -4   3 4038.86 256.665   7
   1  -4  -3 3952.77 256.908   4
  -1  -4   3 4000.45 256.894   4
   1   4   3 4425.96 256.847   1
  -1   4  -3 4103.79 256.955  33
  -1   4  -3 4074.35 256.678  30
   1  -4  -3 3786.83 256.696  28
  -1  -4   3 4017.80 256.890  26
  -1  -4   3 3823.44 256.705  27
   1  -4  -3 3946.78 256.947  27
  -1   4  -3 3871.51 256.658   9
   1  -4  -3 3955.20 256.663  11
  -1   4  -3 3965.02 256.825  11
   1  -4  -3 3790.80 256.693  20
   1  -4  -3 4229.16 256.641  22
  -1  -4   3 4036.83 256.802  19
   1   4   3 4212.01 256.587  20
  -1  -4   3 4273.63 256.644  17
  -1   4  -3 4300.97 256.655  17
   1  -4  -3 3950.72 256.676  16
  -1  -4   3 3816.10 256.592  14
   1  -4  -3 3904.85 256.832  13
   1  -4  -4 1967.57 127.960   6
  -1   4  -4 1925.83 128.181   6
   1  -4  -4 1877.13 128.254   4
   1   4   4 1990.18 128.079   8
  -1  -4   4 2062.79 128.067   7
  -1  -4   4 1942.13 127.897   8
   1   4   4 2006.28 128.150   1
  -1   4  -4 1971.62 128.068   3
  -1  -4   4 1894.26 128.251   4
  -1   4  -4 2463.12 128.415  33
   1   4   4 2013.45 128.260  32
  -1  -4   4 2013.82 128.273  26
   1  -4  -4 2014.76 128.060  28
   1  -4  -4 2046.24 128.337  27
   1  -4  -4 1988.73 127.992  11
  -1   4  -4 2106.38 128.051   9
  -1   4  -4 1818.77 128.166  11
   1  -4  -4 2066.85 128.000  22
   1  -4  -4 1775.46 128.014  20
   1   4   4 1992.41 127.908  20
   1  -4  -4 2149.99 128.061  16
  -1  -4   4 2050.32 127.965  17
  -1  -4   4 1932.97 128.168  19
  -1   4  -4 2073.52 127.983  17
   1  -4  -4 2054.65 128.219  13
   1  -4  -5 803.687 51.8722   6
  -1   4  -5 691.271 52.0997   6
  -1  -4   5 786.534 51.8711   8
   1  -4  -5 833.384 52.2486   4
   1   4   5 807.310 52.0604   8
  -1  -4   5 808.413 52.0411   7
  -1  -4   5 803.626 52.2295   4
  -1   4  -5 854.270 52.0042   3
   1   4   5 776.247 52.0672   1
  -1   4  -5 822.485 52.2654  33
   1   4   5 803.398 52.1856  33
   1   4   5 796.265 52.2099  32
  -1  -4   5 792.659 52.2234  26
   1  -4  -5 852.752 51.9055  11
  -1   4  -5 745.949 52.1228  11
  -1   4  -5 885.889 52.0279   9
   1  -4  -5 830.127 52.1713  12
   1  -4  -5 784.772 51.9501  20
   1   4   5 810.468 51.8282  20
   1  -4  -5 777.816 51.9334  22
   1  -4  -5 765.517 51.9872  16
  -1  -4   5 820.729 51.8807  17
  -1  -4   5 865.650 52.1774  19
  -1   4  -5 837.892 51.8925  17
   1  -4  -5 854.908 52.1920  13
   1  -4  -6 586.988 37.0413   2
  -1   4  -6 529.235 36.8861   3
   1   4   6 589.748 37.0085   1
  -1  -4   6 551.310 37.1663   4
   1  -4  -6 613.702 37.0112  29
   1   4   6 485.569 37.0733  33
   1   4   6 754.007 37.3236  32
  -1  -4   6 576.187 37.1953  26
  -1   4  -6 504.631 37.0438  11
   1  -4  -6 540.676 37.0820  12
   1   4   6 555.511 37.1908  10
  -1   4  -6 644.024 36.9973   9
   1  -4  -6 571.815 36.7937  11
   1  -4  -6 602.503 36.8869  20
   1   4   6 577.727 36.7629  20
   1  -4  -6 540.210 36.8747  22
   1  -4  -6 555.088 36.9475  16
  -1  -4   6 570.152 37.1165  19
  -1  -4   6 571.389 36.7958  17
  -1   4  -6 571.674 36.7933  17
   1   4   6 574.365 37.0384   8
  -1  -4   6 591.868 37.0265   7
  -1  -4   6 556.545 36.8421   8
  -1   4  -6 644.010 37.1624   6
  -1   4  -7 2055.55 130.197   6
   1   4   7 1984.45 130.134   8
  -1  -4   7 1901.02 129.933   8
  -1  -4   7 2043.77 130.118   7
   1   4   7 1964.89 130.040   1
   1  -4  -7 1837.41 130.045   2
  -1   4  -7 2187.63 129.975   3
  -1  -4   7 1999.93 130.259   4
   1  -4  -7 1888.50 130.027  29
   1   4   7 2042.95 130.247  32
  -1  -4   7 2021.27 130.276  26
   1  -4  -7 1990.73 129.817  11
   1  -4  -7 2097.22 130.186  12
  -1   4  -7 2270.43 130.082   9
   1   4   7 2039.99 130.280  10
   1   4   7 2068.40 129.834  20
   1   4   7 1851.93 130.250  23
   1  -4  -7 1972.20 129.965  22
  -1  -4   7 1994.58 130.201  19
   1  -4  -7 2268.53 129.958  20
   1  -4  -7 2228.71 130.075  16
  -1   4  -7 2058.88 129.840  17
  -1  -4   7 1918.92 129.841  17
   1   4   7 2068.74 130.286  14
  -1   4  -8 170.768 10.3079   6
  -1  -4   8 162.483 10.2092   7
  -1  -4   8 155.570 9.99824   8
   1   4   8 146.301 10.2010   8
   1  -4  -8 158.501 10.1125   2
   1   4   8 136.768 10.0107   1
   1  -4  -8 176.612 10.1413  29
   1   4   8 154.209 10.3241  32
  -1   4  -8 143.240 10.1483  26
  -1  -4   8 151.438 10.3372  26
   1  -4  -8 151.696 9.76346  11
   1  -4  -8 141.382 10.1945  12
  -1   4  -8 137.667 10.0566   9
   1   4   8 161.579 10.3783  10
   1   4   8 131.267 10.2648  23
   1  -4  -8 138.904 9.97860  22
  -1  -4   8 153.456 10.3042  19
   1  -4  -8 158.909 9.94625  20
   1  -4  -8 160.189 10.1121  16
  -1  -4   8 146.090 9.83259  17
   1   4   8 145.102 10.3255  14
  -1  -4   9 1942.14 121.062   7
  -1  -4   9 1957.73 120.889   8
  -1   4  -9 1957.94 121.102   6
   1   4   9 1886.66 121.082   8
   1  -4  -9 2081.03 120.939   2
  -1  -4   9 1624.42 121.035   3
   1   4   9 1893.22 120.862   1
   1   4   9 1882.33 121.158  32
   1  -4  -9 1827.77 120.920  29
  -1   4  -9 1996.67 121.039  26
  -1  -4   9 1975.44 121.212  26
   1  -4  -9 1914.09 120.580  11
   1   4   9 1871.57 121.174  10
  -1   4  -9 1897.58 120.968   9
   1   4   9 1768.54 121.159  23
   1  -4  -9 1901.44 120.887  22
   1  -4  -9 1832.13 120.940  16
  -1  -4   9 1911.12 121.148  19
  -1  -4   9 1716.97 120.678  17
   1   4   9 1902.11 121.203  14
   1  -4  -9 1980.05 121.102  12
   1  -4 -10 952.597 56.7701   6
   1   4  10 834.487 57.1909   8
  -1  -4  10 847.181 57.0039   8
  -1  -4  10 861.696 57.1868   7
   1   4  10 870.636 56.9392   1
  -1  -4  10 841.170 57.2023   3
   1  -4 -10 879.885 56.9803   2
   1   4  10 873.398 57.2695  32
   1  -4 -10 1006.09 57.0981  29
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  -1   4 -10 797.792 57.0586  26
  -1   4 -10 901.167 57.1021   9
   1   4  10 859.202 57.3150  10
   1  -4 -10 864.443 57.0142  22
   1   4  10 875.310 57.3121  23
  -1   4 -10 867.272 56.7000  21
  -1  -4  10 879.081 56.7960  17
   1  -4 -10 1008.53 57.1654  16
  -1  -4  10 896.858 57.3054  19
   1   4  10 895.759 57.3315  14
   1  -4 -10 869.033 57.1968  12
  -1  -4  11 104.823 6.94482   8
  -1  -4  11 100.845 7.15544   7
   1  -4 -11 106.366 6.59461   6
  -1  -4  11 91.2380 7.04692   3
   1  -4 -11 101.862 6.83369   2
   1   4  11 103.196 6.78919   1
   1   4  11 116.758 7.31304  32
   1  -4 -11 97.9516 6.93912  29
  -1   4 -11 104.767 7.04201  26
  -1   4 -11 126.513 7.15174   9
  -1   4 -11 83.2498 6.95936  11
   1   4  11 103.041 7.29171  10
   1  -4 -11 99.3101 6.92682  22
   1   4  11 111.078 7.34035  23
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   1  -4 -11 93.8999 6.98241  16
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   1  -4 -11 94.3563 7.11564  12
   1   4  11 106.111 7.33669  14
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  -1  -4  12 38.4592 3.28192   7
   1  -4 -12 30.8387 2.53350   6
   1  -4 -12 32.5111 2.79654   2
   1   4  12 35.3922 2.76355   1
  -1  -4  12 43.2235 3.29733   3
   1  -4 -12 38.1653 3.04518  29
   1   4  12 31.7605 3.23675  32
   1   4  12 38.4488 2.46139  24
  -1   4 -12 31.8207 2.98303  26
  -1   4 -12 41.0969 3.21012   9
   1   4  12 38.7698 3.42473  10
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   1   4  12 24.6783 3.18899  23
   1  -4 -12 37.8732 3.07807  22
  -1   4 -12 36.1540 2.57008  21
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   1  -4 -12 29.8223 3.03511  16
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   1   4  12 40.3029 3.50276  14
   1  -4 -12 38.9495 3.26897  12
   1  -4 -13 943.491 59.6111   6
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   1   4  13 927.893 59.7296   1
   1  -4 -13 869.455 59.7442   2
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   1  -4 -13 960.763 59.9798  29
   1   4  13 854.118 60.1565  32
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   1   4  13 940.399 60.2872  10
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   1   4  13 825.536 60.1863  23
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   1   4  13 939.268 60.2906  14
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   1   4  14 1014.29 65.0950   1
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   1   4  14 935.494 65.5575  32
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   1   4  14 1050.77 65.7254  10
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   1   4  14 991.155 65.6865  23
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   1  -4 -14 915.640 65.4560  15
   1  -4 -14 967.448 65.5465  12
   1   4  14 1048.20 65.7406  14
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   1   4  15 215.872 14.0385   1
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   1   4  15 238.399 14.8378  10
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   1   4  15 215.642 14.7786  23
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   1   4  15 231.221 14.8129  14
   1  -4 -15 222.489 14.6722  12
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   2   1  12 31.2623 3.22098   8
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   2   3   3 1728.01 114.444   8
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   2   3   4 351.672 23.4314   8
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   2   3   5 83.6390 6.00852   3
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   2   3   5 79.6122 5.73303   4
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   2   3   6 1452.22 90.1224  24
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   2  -3  -6 1402.29 90.1243  12
   2   3   6 1349.27 90.1557  20
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   2   3   6 1396.98 89.9941  19
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   2   3   6 1300.57 90.3490  17
   2  -3  -6 1455.75 90.4147  13
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  -2  -3   7 19.3884 1.79518   8
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   2  -3  -7 18.9618 1.97375   9
   2   3   7 23.3225 2.20056   8
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   2  -3  -7 23.3854 2.28549  29
   2  -3  -7 19.7338 1.56674  28
   2   3   7 22.7411 1.82009  24
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   2   3   7 21.9408 2.01808   1
  -2  -3   7 20.9527 2.23872   3
   2   3   7 18.8780 1.64724   4
   2  -3  -7 18.5886 2.02667   2
   2   3   7 18.8216 1.92176   3
   2  -3  -7 23.4708 2.51781  21
   2  -3  -7 16.6985 2.02705  22
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   2   3   7 18.4104 1.92235  20
   2  -3  -7 21.2981 2.09925  20
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   2   3   7 21.4689 2.29397  17
   2  -3  -7 21.2421 1.76998  16
   2   3   7 24.3272 1.76986  19
   2  -3  -7 21.0742 1.88126  12
   2  -3  -7 20.3509 2.35929  15
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   2  -3  -7 22.9438 2.31613  13
   2   3   7 18.4340 2.31464  14
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   2   3   8 1980.27 128.071   8
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   2  -3  -8 2036.31 127.965   9
   2  -3  -8 2335.10 128.184  29
   2   3   8 2176.69 128.186  32
   2   3   8 2137.95 127.752  24
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   2   3   8 2005.05 127.701   4
   2   3   8 1798.62 127.875   1
   2  -3  -8 2110.36 127.962   2
   2  -3  -8 1718.79 128.090  21
   2  -3  -8 1951.86 127.960  20
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   2  -3  -8 2005.06 127.814  16
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   2   3   8 2054.23 128.195  14
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   2  -3  -9 1007.45 68.4128   9
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   2   3   9 1050.17 68.1256   4
   2   3   9 1070.56 68.5468   8
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   2   3   9 1038.78 68.5771  32
   2  -3  -9 990.175 68.4838  29
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   2   3   9 1030.25 68.1032  24
   2   3   9 941.958 68.2781   1
   2  -3  -9 1041.27 68.3431   2
   2  -3  -9 1070.02 68.4687  22
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   2   3   9 1114.31 68.2689  19
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   2 -11   9 2171.55 138.393   2
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   2 -11   9 2267.15 138.917  27
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   2 -11   9 2343.03 137.851  15
   2 -11   9 2074.12 138.241  13
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   2 -11   8 473.543 32.4439   4
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   2 -11   8 502.000 31.2555  21
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   2 -11   8 514.639 32.2420  13
   2 -11   8 465.447 31.7306  15
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   2 -11   7 384.795 25.2467   4
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   2  11  -7 389.847 25.0118   1
   2  11  -7 372.435 24.9794   3
   2 -11   7 316.611 24.8783   2
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   2  11  -7 344.847 24.6040  29
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   2 -11   7 426.698 25.6563  27
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   2 -11   7 381.112 24.0830  21
   2 -11   7 389.700 25.5447  19
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   2 -11   6 1827.18 118.729   5
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   2 -11   6 1850.69 119.896   4
   2 -11   6 1777.18 119.701   2
   2  11  -6 1834.50 119.662   3
   2  11  -6 2093.81 119.790   1
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   2  11  -6 2040.12 119.403  29
   2  11  -6 1762.24 119.777  33
   2 -11   6 1791.15 120.066  27
   2  11  -6 1570.65 119.585  25
   2  11  -6 1830.78 120.054  28
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   2  11  -6 1738.58 119.267  10
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   2  11  -6 2203.32 119.539  22
   2  11  -6 1633.15 118.970  17
   2 -11   6 1956.12 120.189  19
   2 -11   6 2060.39 119.360  15
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   2 -11   6 1748.41 119.484  13
   2  11  -6 1833.54 119.040  14
   2 -11   5 575.992 39.6597   4
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   2 -11   5 619.381 38.4691   5
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   2 -11   5 539.144 39.4735   2
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   2  11  -5 586.985 39.0554  29
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   2 -11   5 618.331 39.9363  27
   2  11  -5 535.776 39.4716  25
   2  11  -5 755.415 40.2559  28
   2  11  -5 604.826 39.1832  10
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   2  11  -5 723.759 39.2889  22
   2  11  -5 579.151 38.8708  17
   2 -11   5 600.302 39.9280  19
   2 -11   5 605.911 39.1484  15
   2 -11   5 579.628 39.3052  13
   2  11  -5 617.767 38.9334  14
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   2 -11   4 1155.28 72.8139   2
   2  11  -4 1121.97 72.6923   3
   2  11  -4 998.374 72.1620  29
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   2  11  -4 1063.73 72.7655  33
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   2 -11   4 1112.94 73.0655  27
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   2  11  -4 1236.58 73.1934  28
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   2  11  -4 1104.57 72.3895  10
   2  11  -4 1481.05 72.5183  22
   2  11  -4 1183.10 72.1852  17
   2 -11   4 1063.49 72.4742  13
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   2 -11  -4 1122.04 72.4776  13
   2 -11  -5 606.873 39.5790   4
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   2  11   5 588.615 38.5219   8
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   2  11   5 614.003 39.3227   1
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   2 -11  -5 644.697 39.7462  27
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   2 -11  -5 578.509 38.7803  16
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   2  11   5 614.946 39.2354  17
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   2  11   5 571.854 38.3924  13
   2  11   5 584.808 39.2531  14
   2 -11  -5 610.640 39.1192  13
   2 -11  -6 1931.69 121.674   4
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   2  11   6 1848.43 121.326   1
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   2 -11  -6 1842.47 121.482  12
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   2  11   6 1947.03 121.366  17
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   2 -11  -6 1965.29 120.915  16
   2  11   6 1924.11 121.429  14
   2 -11  -6 2083.11 121.303  13
   2 -11  -7 393.488 26.6725   4
   2  11   7 388.102 25.6955   8
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   2 -11  -7 390.317 26.4414   2
   2  11   7 419.456 26.3967   1
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   2 -11  -7 437.643 25.7064  20
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   2  11   9 1995.66 134.851   1
   2 -11  -9 2161.99 135.052   2
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   2  11  10 659.970 41.3407   8
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   2  11  11 96.1405 7.14420   8
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   3   2   4 544.254 34.2987   2
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   3  -2  -5 1764.45 112.684  15
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   3   2   6 2499.17 176.439   8
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   3  -4   4 174.692 11.8068  13
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   3   4  -3 1764.93 94.2845  25
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   3   4  -3 1590.28 93.9993  17
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   3   4  -3 1343.06 93.6486  13
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   3  -4   3 1682.21 93.9675  15
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   3  -4   2 988.223 61.7825   4
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   3  -4   2 898.392 61.8797   2
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   3   4  -2 962.081 61.8545  29
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   3   4  -2 978.007 61.6149  13
   3  -4   2 925.295 61.8271  15
   3  -4   2 940.860 62.0852  13
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   3  -4   1 1915.91 123.875   4
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   3   4  -1 2041.71 124.032   1
   3  -4   1 1902.87 124.005   2
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   3   4  -1 2373.75 124.043  29
   3   4  -1 1737.33 123.734  32
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   3   4  -1 1835.76 124.111  25
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   3  -4   1 2072.64 123.824  21
   3   4  -1 2189.49 124.135  22
   3   4  -1 1619.65 123.856  20
   3  -4   1 1914.74 123.461  16
   3   4  -1 2197.33 124.084  17
   3  -4   1 1981.17 123.984  17
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   3   4  -1 1997.77 123.741  13
   3  -4   1 1882.19 124.175  13
   3  -4   1 2077.81 124.005  15
  -3   4   0 55.7109 4.23551   6
   3  -4   0 62.0900 4.48294   4
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  -3  -4   0 55.7561 4.24124   4
   3  -4   0 51.3144 4.50522   2
   3   4   0 59.9373 4.55644   1
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   3   4   0 54.2572 4.27519  32
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   3   4   0 60.0561 4.03966  33
   3   4   0 53.8972 4.35517  29
   3   4   0 69.5582 4.85608  25
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   3  -4   0 50.1943 4.28383  21
   3   4   0 47.4902 4.37914  20
   3   4   0 36.6673 4.39249  22
   3   4   0 58.3125 4.60695  17
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   3  -4   0 53.8354 4.48353  17
   3  -4   0 56.5492 4.71344  13
   3   4   0 58.1198 4.17792  13
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   3   4   1 1870.87 122.343   1
   3  -4  -1 1817.76 122.364   2
   3   4   1 1863.91 122.335   3
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   3   4   1 2217.14 122.322  29
   3   4   1 1979.67 121.974  33
   3   4   1 1700.92 122.166  32
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   3   4   1 1877.94 122.366  24
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   3   4   1 2249.38 122.663  25
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   3  -4  -1 1997.26 121.861   9
   3  -4  -1 1877.73 122.250  21
   3   4   1 2006.76 122.307  20
   3   4   1 1179.57 122.142  22
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   3  -4  -1 2022.45 122.390  17
   3   4   1 1577.80 122.069  13
   3  -4  -1 2018.27 122.583  13
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   3   4   2 942.462 62.0874   3
   3  -4  -2 893.647 62.0908   2
   3   4   2 989.727 62.1220   1
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   3   4   2 989.730 62.0147  32
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   3   4   2 1029.69 61.7341  33
   3   4   2 928.073 62.0703  24
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   3   4   2 860.280 62.1909  25
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   3  -4  -2 977.235 61.6601   9
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   3  -4  -2 1023.61 62.2044  20
   3  -4  -2 953.914 62.0340  21
   3   4   2 1126.52 62.2496  22
   3   4   2 768.472 61.9147  20
   3  -4  -2 972.273 62.1346  17
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   3   4   2 1061.42 61.9539  13
   3  -4  -2 969.993 62.2811  13
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   3   4   3 1474.00 93.8779   1
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   3   4   3 1405.72 93.8402   3
   3   4   3 1265.06 93.7388  32
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   3   4   3 1417.55 93.5015  33
   3   4   3 1845.25 93.9878  24
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   3  -4  -3 1494.11 93.5603  12
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   3  -4  -3 1538.29 93.4974   9
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   3   4   3 1349.26 93.7348  20
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   3   4   3 1357.87 93.6733  13
   3  -4  -3 1462.75 94.0451  13
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   3   4   4 200.389 12.2845   8
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   3   4   4 171.979 12.3150   3
   3   4   4 214.316 12.4876   1
   3   4   4 190.150 12.0218  33
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   3   4   4 184.721 12.3587  32
   3   4   4 216.843 12.3971  24
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   3  -4  -4 169.402 11.9831   9
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   3  -4  -4 173.180 11.9995  12
   3  -4  -4 174.775 12.3829  21
   3  -4  -4 178.623 11.9229  23
   3   4   4 200.607 12.2963  20
   3  -4  -4 168.597 12.3171  22
   3  -4  -4 188.561 12.4369  20
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   3  -4  -4 196.664 12.5932  13
   3   4   4 183.625 12.2276  13
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   3   4   5 875.877 54.7560   8
   3   4   5 906.868 54.8535   1
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   3   4   5 865.926 54.7977   3
   3   4   5 790.685 54.4796  33
   3  -4  -5 866.216 54.9307  34
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   3   4   5 877.326 54.8489  32
   3   4   5 801.501 54.6768  24
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   3  -4  -5 838.100 54.5090   9
   3  -4  -5 832.037 54.4801  12
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   3  -4  -5 884.394 54.4008  23
   3  -4  -5 843.612 54.8486  20
   3  -4  -5 851.596 54.8116  22
   3   4   5 652.959 54.5818  20
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   3  -4  -5 836.425 54.9692  13
   3   4   5 856.039 54.7086  13
   3  -4  -5 871.182 54.9268  15
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   3   4   6 468.136 29.9043   8
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  -3  -4   6 487.359 30.1815   3
   3   4   6 461.963 29.9313   1
   3   4   6 448.166 29.8747   3
   3  -4  -6 420.644 29.8994   2
   3  -4  -6 494.874 30.1289  34
   3   4   6 426.278 29.6262  33
   3   4   6 476.134 29.8163  24
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   3  -4  -6 462.876 29.6819   9
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   3  -4  -6 460.580 29.6050  12
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   3  -4  -6 432.634 29.9446  20
   3   4   6 619.192 29.9934  20
   3  -4  -6 411.829 29.8746  22
   3  -4  -6 459.841 30.0507  21
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   3   4   6 435.120 29.8292  13
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   3  -4  -6 483.829 30.1660  13
   3  -4  -6 472.331 30.1093  15
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   3   4   7 2179.67 141.501   8
   3   4   7 1926.37 141.415   1
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   3   4   7 2121.66 141.441   3
   3  -4  -7 2228.22 141.529   2
   3   4   7 2210.97 141.080   4
   3  -4  -7 2183.71 141.640  34
   3   4   7 1988.21 141.235  33
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   3   4   7 2793.96 141.457  24
   3  -4  -7 2184.89 141.311   9
   3  -4  -7 2267.58 141.216  12
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   3  -4  -7 2177.99 141.664  21
   3  -4  -7 1999.53 141.468  22
   3   4   7 2281.97 141.422  20
   3  -4  -7 2330.25 141.561  20
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   3   4   7 2202.08 141.703  17
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   3   4   7 2200.26 140.991  19
   3  -4  -7 2187.04 141.659  15
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   3   4   7 2450.85 141.561  13
   3  -4  -7 2441.60 141.802  13
   3   4   8 1109.12 75.6318   8
  -3   4  -8 1202.41 75.7175   6
  -3   4  -8 1136.66 75.2362   9
   3   4   8 1039.43 75.5377   1
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   3   4   8 1242.13 75.6100   3
   3  -4  -8 1270.51 75.6837   2
   3   4   8 1189.58 75.1781   4
   3   4   8 1107.40 75.4077  33
   3  -4  -8 1127.76 75.7624  29
   3   4   8 1247.94 75.4314  24
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   3  -4  -8 1220.86 75.5010   9
   3  -4  -8 1224.22 75.8677  21
   3  -4  -8 1161.60 75.6560  20
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   3  -4  -8 1057.41 75.6050  22
   3   4   8 1063.34 75.6749  23
   3   4   8 1055.78 75.4634  20
   3   4   8 1166.48 75.1610  19
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   3   4   8 1170.92 75.8596  17
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   3  -4  -8 1204.71 75.8632  15
   3  -4  -8 1183.19 75.3448  12
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   3  -4  -8 1315.44 75.9380  13
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  -3   4  -9 82.9245 5.60232   6
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   3   4   9 76.2004 5.42417   8
   3   4   9 57.6938 5.17668   1
   3   4   9 66.5765 5.13860   3
   3  -4  -9 78.0102 5.35875   2
   3   4   9 69.9638 4.75202   4
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   3  -4  -9 72.7267 5.53157  29
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   3   4   9 80.7151 5.04431  24
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   3  -4  -9 58.9377 5.13075   9
   3  -4  -9 62.6665 5.53001  21
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   3   4   9 58.4960 5.09713  20
   3  -4  -9 64.2061 5.28414  22
   3   4   9 66.5302 5.42639  23
   3  -4  -9 69.7291 5.32773  20
   3   4   9 68.8465 4.79441  19
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   3   4   9 63.0090 5.51089  17
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   3  -4  -9 68.1982 5.50669  15
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   3  -4  -9 70.1149 4.99014  12
   3  -4  -9 76.5749 5.62441  13
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   3   4  10 458.390 28.6991   8
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   3  -4 -10 478.660 28.5720   2
   3   4  10 423.811 28.0274   4
   3   4  10 504.709 28.5874   1
   3   4  10 407.964 28.4131   3
   3  -4 -10 523.798 28.8932  29
   3   4  10 351.753 28.1339  24
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   3  -4 -10 420.046 28.4549   9
   3  -4 -10 486.721 28.9241  21
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   3  -4 -10 462.065 28.5898  20
   3   4  10 399.912 28.3754  20
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   3   4  10 364.021 28.5785  23
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   3   4  10 449.984 28.1568  19
   3   4  10 443.254 28.8361  17
   3  -4 -10 437.382 28.7592  15
   3  -4 -10 452.270 28.3031  12
   3  -4 -10 464.201 28.8487  13
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   3   4  11 76.0867 5.79932   8
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   3   4  11 81.3219 5.55003   3
   3   4  11 77.3213 5.56242   1
   3   4  11 69.1869 5.00216   4
   3  -4 -11 73.6673 5.55619   2
   3  -4 -11 76.1481 5.86563  29
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   3   4  11 82.3126 5.20948  24
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   3  -4 -11 79.5986 5.61044   9
   3   4  11 67.6463 5.43738  20
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   3   4  11 76.2878 5.85424  23
   3  -4 -11 72.3264 5.67626  22
   3  -4 -11 86.0324 6.08463  21
   3   4  11 74.6332 5.21618  19
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   3   4  11 75.6070 5.95819  17
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   3  -4 -11 73.1894 5.61236  20
   3  -4 -11 69.7610 5.32684  12
   3  -4 -11 65.4782 5.75338  15
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   3   4  12 138.890 10.3849   8
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   3   4  12 146.295 10.0970   3
   3   4  12 142.620 9.66185   4
   3  -4 -12 144.326 10.1386   2
   3   4  12 167.049 10.1769   1
   3  -4 -12 121.104 10.2870  34
   3  -4 -12 137.576 10.4099  29
   3  -4 -12 150.700 9.62109  28
   3   4  12 143.966 9.74096  24
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   3  -4 -12 165.273 10.3547   9
   3  -4 -12 110.734 10.4074  21
   3   4  12 168.641 10.2229  20
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   3   4  12 152.129 10.5977  17
   3   4  12 149.327 9.90539  19
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   3  -4 -12 160.815 10.5577  15
   3  -4 -12 150.097 10.0427  12
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   3   4  13 1100.61 68.6444   8
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   3   4  13 1155.81 68.2839   1
   3  -4 -13 1101.29 68.2911   2
   3   4  13 1084.65 68.2651   3
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   3   4  13 1106.03 67.8531  24
   3  -4 -13 978.762 68.3829   9
   3  -4 -13 1061.25 68.7506  21
   3   4  13 956.885 68.1959  20
   3  -4 -13 1062.98 68.4815  22
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   4   0   8 386.534 25.6098  34
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   4   0   8 401.530 25.8854  25
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   4   0  -8 334.645 25.9331   9
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   4   0  -9 1979.95 125.811  21
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   4   1 -18 121.565 8.83121  21
   4   1 -18 120.077 8.88033  22
   4  -1  18 123.089 8.59885  23
   4  -1  18 107.129 8.31985  19
   4  -1  18 99.1142 8.28646  17
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   4  -1  18 110.467 8.80439  13
   4   1 -18 98.6714 8.18887  15
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   4  -1  17 1322.54 90.3302   8
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   4   1 -17 1420.87 89.5696   2
   4   1 -17 1393.31 89.5763   1
   4  -1  17 1489.15 89.5987   2
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   4   1 -17 1385.78 90.0602  34
   4  -1  17 1517.59 89.4690  25
   4   1 -17 1334.39 90.0188  24
   4   1 -17 1305.74 89.4671  28
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   4   1 -17 1692.91 90.6621   9
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   4   1 -17 1324.07 90.3441  22
   4  -1  17 1449.79 90.1482  23
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   4  -1  17 1385.50 90.1073  17
   4  -1  17 1360.98 89.9615  19
   4   1 -17 1280.04 89.9499  15
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   4  -1  17 1297.80 90.3923  13
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   4  -1  16 399.439 26.0204   8
   4   1 -16 392.099 25.1854   2
   4   1 -16 385.313 25.1797   1
   4  -1  16 376.668 25.1546   2
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   4   1 -16 371.501 25.6169  34
   4  -1  16 336.369 24.9583  25
   4   1 -16 397.394 25.6929  24
   4   1 -16 324.911 24.9808  28
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   4   1 -16 336.414 25.7806   9
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   4   1 -16 407.129 26.0592  22
   4  -1  16 381.647 25.6215  23
   4  -1  16 407.152 25.7621  17
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   4  -1  16 396.811 25.5812  19
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   4   1 -16 389.048 25.6497  15
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   4  -1  15 294.017 19.2822   8
   4   1 -15 277.623 18.4902   2
   4   1 -15 249.695 18.4645   1
   4  -1  15 306.267 18.5496   2
   4   1 -15 367.190 19.6405  29
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   4   1 -15 302.432 19.0021  34
   4  -1  15 280.761 18.3536  25
   4   1 -15 263.276 18.8859  24
   4   1 -15 327.913 19.1860  25
   4   1 -15 276.396 18.3154  28
   4   1 -15 262.960 19.1413   9
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   4   1 -15 189.121 18.8496  22
   4  -1  15 274.138 18.8866  23
   4  -1  15 287.510 19.0072  17
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   4  -1  15 293.401 18.8311  19
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   4   1 -15 245.440 18.7901  15
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   4  -1  14 112.344 8.79273   8
   4  -1  14 122.801 8.21198   2
   4   1 -14 97.8319 8.10767   1
   4   1 -14 119.592 8.18908   2
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   4   1 -14 121.291 8.90385  29
   4   1 -14 114.666 8.58616  34
   4  -1  14 111.446 7.99502  25
   4   1 -14 109.353 7.91938  28
   4   1 -14 127.899 8.76798  24
   4   1 -14 159.175 9.00873  25
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   4   1 -14 104.109 8.68893   9
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   4   1 -14 103.270 8.75400  22
   4  -1  14 105.854 8.45073  23
   4  -1  14 110.899 8.56093  17
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   4  -1  14 126.897 8.50966  19
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   4   1 -14 105.024 8.49563  15
   4  -1  13 2515.00 158.159   8
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   4  -1  13 2520.19 157.589   2
   4   1 -13 2526.14 157.615   1
   4   1 -13 2466.97 157.581   2
   4  -1  13 2561.19 157.150  34
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   4   1 -13 2093.11 157.962  29
   4   1 -13 2297.66 157.857  34
   4  -1  13 1959.57 157.324  25
   4   1 -13 2394.88 157.321  28
   4   1 -13 2391.80 157.909  24
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   4   1 -13 2674.48 158.076  25
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   4   1 -13 2703.77 158.213   9
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   4   1 -13 2756.98 158.303  22
   4  -1  13 2647.36 157.843  23
   4  -1  13 2380.91 157.902  17
   4  -1  13 2355.64 157.702  19
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   4   1 -13 2626.10 157.979  15
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   4  -1  12 355.360 22.2341   8
   4   1 -12 334.428 21.6839   1
   4  -1  12 330.883 21.6620   2
   4   1 -12 342.208 21.6642   2
   4   1 -12 303.561 22.1064  29
   4  -1  12 335.036 21.2160  34
   4  -1  12 287.848 21.4293  25
   4   1 -12 344.157 22.0373  24
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   4   1 -12 337.280 22.0584  25
   4   1 -12 316.770 21.3354  28
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   4   1 -12 336.731 22.1013   9
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   4   1 -12 216.463 21.7995  22
   4  -1  12 367.886 21.8764  23
   4  -1  12 336.331 22.0098  17
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   4  -1  12 338.809 21.7636  19
   4   1 -12 370.994 22.0919  15
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   4  -1  11 2151.48 134.452   8
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   4  -1  11 2041.27 133.986   1
   4   1 -11 1876.50 133.944   1
   4   1 -11 2111.89 133.987   2
   4  -1  11 2100.28 134.006   2
   4   1 -11 3000.02 134.901  29
   4  -1  11 2117.90 133.632  34
   4   1 -11 2048.16 133.672  28
   4   1 -11 2031.08 134.261  24
   4   1 -11 1778.89 134.164  25
   4  -1  11 2260.18 133.902  25
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   4   1 -11 2153.33 134.398   9
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   4   1 -11 2498.64 134.643  22
   4  -1  11 2070.60 134.033  23
   4  -1  11 2088.71 134.264  17
   4  -1  11 1900.98 133.969  19
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   4   1 -11 2490.70 134.437  15
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   4   1 -10 12.9771 2.02949   2
   4  -1  10 10.3106 1.96945   2
   4  -1  10 5.47300 1.92264   1
   4   1 -10 10.2045 2.02587   1
   4   1 -10 5.74245 2.32189  29
   4  -1  10 6.93800 1.34388  34
   4   1 -10 7.97076 2.21977  24
   4  -1  10 7.04016 1.74649  25
   4   1 -10 8.52737 2.47059  25
   4   1 -10 7.92794 1.45072  28
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   4   1 -10 12.1992 2.40817   9
   4  -1  10 9.32858 1.94815  23
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   4   1 -10 4.54680 2.41673  22
   4   1 -10 4.78253 2.35687  21
   4  -1  10 10.6938 2.26264  17
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   4   1 -10 14.1893 2.26435  17
   4  -1  10 8.94459 1.85365  19
   4   1 -10 14.3386 2.33244  15
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   4  -1   9 1807.82 103.038   2
   4  -1   9 1864.06 103.079   1
   4   1  -9 1601.52 102.961   1
   4   1  -9 1545.69 102.909   2
   4   1  -9 1812.82 103.435  29
   4  -1   9 1517.76 102.638  34
   4  -1   9 1604.83 102.837  25
   4   1  -9 1738.98 103.275  24
   4   1  -9 1542.96 103.179  25
   4   1  -9 1695.87 102.611  28
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   4   1  -9 1653.44 103.231   9
  -4   1   9 1581.32 102.378  12
  -4   1   9 1589.72 102.413  23
   4   1  -9 1715.20 103.361  21
   4   1  -9 2006.85 103.574  22
   4  -1   9 1393.78 102.793  23
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   4   1  -9 1659.10 103.225  20
   4   1  -9 1669.08 103.133  17
   4  -1   9 1413.98 102.840  19
   4  -1   9 1594.57 103.175  17
   4   1  -9 1746.89 103.149  13
   4   1  -9 1491.87 103.105  15
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   4   1  -8 52.3239 4.46083   2
   4  -1   8 63.6042 4.59329   1
   4   1  -8 64.0046 4.62521   1
   4  -1   8 58.8351 4.57193   2
   4   1  -8 57.8488 4.91498  29
   4  -1   8 56.2633 4.20162  34
   4   1  -8 69.9454 4.90337  34
   4  -1   8 43.3155 4.31025  25
   4   1  -8 66.8229 4.90144  24
   4   1  -8 52.7682 4.84400  25
   4   1  -8 58.6602 4.75109   9
  -4   1   8 56.4537 4.15785  10
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   4  -1   8 64.1716 4.97700  20
   4   1  -8 51.2434 4.82493  21
   4   1  -8 53.8330 4.84317  22
   4  -1   8 60.6405 4.36868  23
   4  -1   8 53.7143 4.69636  17
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   4   1  -8 61.5204 4.86230  20
   4   1  -8 39.1611 4.48898  17
   4  -1   8 65.6113 4.50819  19
   4   1  -8 39.4993 4.43264  13
   4   1  -8 55.6100 4.75179  15
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   4  -1   7 188.130 12.0932   1
   4   1  -7 159.264 11.9865   1
   4   1  -7 168.293 12.0066   2
   4  -1   7 163.646 11.9972   2
   4   1  -7 177.222 12.3505  29
   4  -1   7 183.370 11.7862  34
   4   1  -7 169.153 12.1587  34
   4  -1   7 148.541 11.8484  25
   4   1  -7 179.343 12.2941  25
   4   1  -7 172.875 12.2384  24
   4   1  -7 187.984 12.2778   9
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   4   1  -7 204.765 12.4816  22
   4  -1   7 184.598 12.3471  20
   4   1  -7 179.267 12.2437  20
   4   1  -7 199.157 12.4429  21
   4  -1   7 159.744 11.7738  23
   4  -1   7 173.438 12.2129  17
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   4  -1   7 190.492 11.9566  19
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   4   1  -7 149.060 11.9712  13
   4   1  -7 171.434 12.2181  15
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   4  -1   6 270.343 16.2711   1
   4   1  -6 241.968 16.1869   1
   4  -1   6 258.580 16.2418   2
   4   1  -6 244.402 16.1916   2
   4   1  -6 221.281 16.3551  29
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   4   1  -6 236.508 16.2868  34
   4  -1   6 269.747 16.0213  34
   4   1  -6 242.178 16.4108  25
   4   1  -6 256.699 16.4096  24
   4  -1   6 258.050 16.1347  25
   4   1  -6 260.019 16.3671   9
   4  -1   6 260.500 16.4885  20
   4   1  -6 273.561 16.4613  20
   4   1  -6 264.323 16.5335  21
   4   1  -6 322.226 16.7369  22
   4  -1   6 258.120 15.9358  23
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   4  -1   6 227.552 16.3106  17
   4  -1   6 202.421 15.9485  19
   4   1  -6 187.549 16.0569  13
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   4   1  -6 245.796 16.3778  15
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   4  -1   5 708.333 53.5395   2
   4  -1   5 966.591 53.7672   1
  -4   1   5 895.710 53.3955  33
   4   1  -5 908.004 53.8060  34
   4  -1   5 777.588 53.1575  33
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   4  -1   5 684.360 53.3798  34
   4   1  -5 619.468 53.6202  29
  -4   1   5 881.613 53.0455  28
   4  -1   5 890.147 53.6236  25
   4   1  -5 907.217 53.9125  25
   4   1  -5 799.168 53.7364  24
   4   1  -5 897.303 53.7919   9
   4  -1   5 921.178 53.3529  23
   4  -1   5 909.854 53.9065  20
   4   1  -5 930.652 53.9581  21
   4   1  -5 690.918 53.7156  22
   4   1  -5 1019.12 54.0044  20
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   4  -1   5 790.381 53.7454  17
   4   1  -5 558.165 53.4326  13
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   4   1  -5 897.688 53.8738  15
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   4  -1   4 926.522 49.7404   1
   4  -1   4 730.376 49.5588   2
  -4   1   4 826.744 49.2839  33
   4   1  -4 728.015 49.7192  29
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   4  -1   4 713.438 49.4089  34
   4   1  -4 755.254 49.6265  34
   4  -1   4 724.520 49.0685  33
   4   1  -4 825.223 49.8177  25
   4   1  -4 767.832 49.6864  24
  -4   1   4 808.605 49.0387  28
   4  -1   4 867.821 49.6064  25
   4   1  -4 574.161 49.4534   9
   4  -1   4 743.302 49.1834  23
   4   1  -4 698.250 49.6506  20
   4  -1   4 736.861 49.7386  20
   4   1  -4 688.376 49.6740  21
   4   1  -4 934.445 50.0088  22
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   4  -1   4 799.886 49.7569  17
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   4   1  -4 787.409 49.6183  13
   4   1  -4 756.497 49.7221  15
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   4  -1   3 2167.42 148.560   1
   4  -1   3 2455.25 148.660   2
  -4   1   3 2216.76 148.222  33
   4  -1   3 2433.65 148.534  34
   4   1  -3 2899.26 148.981  29
  -4  -1  -3 2452.36 148.447  30
   4  -1   3 2447.41 148.104  33
   4   1  -3 2441.87 148.694  34
   4  -1   3 2211.81 148.548  25
   4  -1   3 2194.20 148.521  27
   4   1  -3 1584.31 148.438  24
   4   1  -3 2204.51 148.720  25
  -4   1   3 2608.66 148.139  28
   4   1  -3 1703.90 148.442   9
   4  -1   3 2249.88 148.167  23
   4  -1   3 2045.67 148.681  20
   4   1  -3 1907.36 148.604  21
   4   1  -3 2500.78 148.884  22
   4   1  -3 2898.13 148.943  20
   4  -1   3 2333.85 148.555  21
   4  -1   3 2326.50 148.747  17
  -4  -1  -3 2904.25 148.646  16
  -4  -1  -3 2436.32 148.268  12
   4   1  -3 2075.43 148.558  13
   4   1  -3 2291.94 148.720  15
   4  -1   3 2357.67 148.671  15
   4  -1   2 259.350 17.5662   1
   4  -1   2 239.375 17.5372   2
  -4  -1  -2 263.441 17.3945   3
   4  -1   2 292.576 17.5484  34
   4  -1   2 258.989 16.9922  33
  -4   1   2 267.545 17.1175  33
   4   1  -2 266.704 17.5866  34
   4   1  -2 288.768 17.1812  27
   4  -1   2 277.659 17.5870  25
   4  -1   2 277.058 17.5030  27
   4   1  -2 206.809 17.4245   9
   4  -1   2 268.892 17.0438  23
   4   1  -2 273.528 17.7530  21
   4   1  -2 228.085 17.6233  20
   4   1  -2 167.363 17.4857  22
   4  -1   2 258.410 17.5356  21
   4  -1   2 219.947 17.6652  20
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   4  -1   2 276.416 17.7393  17
   4  -1   2 274.505 17.0442  12
   4   1  -2 295.313 17.7740  15
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   4   1  -2 319.063 17.7598  13
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   4  -1   1 6863.01 430.527   1
   4   1  -1 6161.87 430.467   1
   4   1  -1 7813.07 430.622   2
   4  -1   1 7332.87 430.585   2
   4   1  -1 6456.43 430.454  34
  -4   1   1 6592.94 430.039  33
   4  -1   1 5871.28 430.370  34
   4   1  -1 6726.07 430.126  27
   4  -1   1 6806.57 430.393  27
   4  -1   1 7432.63 430.561  25
   4  -1   1 7081.17 429.963  12
   4   1  -1 7701.51 430.733  20
   4  -1   1 6759.44 429.954  23
   4   1  -1 6342.63 430.553  21
   4  -1   1 6710.16 430.642  20
   4  -1   1 6779.62 430.478  21
   4   1  -1 5252.81 430.494  22
   4  -1   1 7014.19 430.646  17
  -4  -1  -1 6431.70 430.337  16
  -4  -1  -1 6551.38 430.025  12
  -4   1   1 6408.14 430.110  16
   4   1  -1 7642.22 430.653  13
  -4   1   0 27.3883 2.67112   6
  -4  -1   0 27.4926 2.66066   3
   4  -1   0 25.0578 2.85638   1
   4   1   0 20.3911 2.95350   1
   4   1   0 31.9525 2.94668   2
   4  -1   0 25.4735 3.00183   2
   4   1   0 27.3769 2.79343  34
   4  -1   0 25.4953 2.85131  34
  -4   1   0 20.0214 1.97519  33
   4  -1   0 21.0723 2.53575  27
   4  -1   0 27.6047 3.00405  25
   4   1   0 16.5740 2.17796  27
   4  -1   0 23.5918 1.76500  12
   4   1   0 22.4975 3.12195  21
   4  -1   0 21.3596 3.18529  20
   4   1   0 23.5399 2.95390  20
   4  -1   0 25.7309 3.02832  21
  -4  -1   0 23.1945 1.96901  23
   4   1   0 28.1756 3.25275  17
   4  -1   0 19.6527 3.01680  17
   4   1   0 20.3220 2.79466  13
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   4   1   1 6802.38 443.735   1
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   4   1   1 6952.41 443.874  17
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   4   1   1 7339.40 443.872  13
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   4   1   2 238.374 16.8924   1
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   4   1   2 254.404 16.8437  34
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   4   1   3 2465.55 149.470   1
   4   1   3 2299.68 149.397   2
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   4  -1  -3 2697.26 149.366   9
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   4   1   3 2382.80 149.552  20
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   4   1   4 656.511 49.6392   2
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   4   1   4 739.504 49.7870  25
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   4   1   4 895.579 49.7941  24
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   4   1   4 655.751 49.3946  23
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   4   1   4 642.830 49.7410  20
   4  -1  -4 899.683 50.0820  22
   4   1   4 810.860 49.9945  17
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   4   1   5 845.959 55.4193  34
   4   1   5 813.661 55.6185  25
   4  -1  -5 823.449 55.7109  25
   4   1   5 868.426 55.5188  24
   4  -1  -5 894.088 55.7504  24
   4  -1  -5 770.367 55.4505   9
   4   1   5 945.309 55.3973  23
   4  -1  -5 835.892 55.7271  21
   4   1   5 888.450 55.7752  20
   4  -1  -5 1001.36 55.9325  22
   4   1   5 868.027 55.8005  17
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   4  -1  -5 825.202 55.7017  17
   4  -1  -5 974.168 55.8867  15
   4   1   5 865.372 55.7711  13
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   4   1   6 243.141 16.7742   1
   4  -1  -6 253.435 16.8073   2
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   4   1   6 236.663 16.7435   2
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   4   1   6 249.032 16.1824  33
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   4   1   6 259.852 16.5796  34
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   4  -1  -6 269.646 17.0080  25
   4  -1  -6 311.144 17.1077  24
   4   1   6 247.618 16.8141  25
   4  -1  -6 293.983 16.8660   9
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   4  -1  -6 212.830 16.8738  21
   4   1   6 328.789 17.2241  20
   4   1   6 266.501 16.6086  23
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   4   1   6 229.239 16.9338  17
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   4  -1  -6 240.707 16.9347  15
   4   1   6 277.667 17.0752  13
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   4   1   7 164.605 12.0235   1
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   4   1   7 204.800 12.1325   2
   4  -1  -7 166.860 12.3213  29
   4   1   7 179.885 11.5068  33
   4  -1  -7 184.311 12.2664  34
   4   1   7 175.013 11.7916  34
   4   1   7 136.263 11.7910  24
   4  -1  -7 172.918 12.2496  25
   4  -1  -7 193.929 12.2947  24
   4   1   7 163.990 12.0572  25
   4  -1  -7 186.166 12.0863   9
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   4   1   7 198.766 11.9797  23
   4   1   7 147.176 12.1128  20
   4  -1  -7 138.525 12.1105  21
   4  -1  -7 191.889 12.3979  22
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   4   1   7 184.243 12.3648  17
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   4   1   7 172.514 11.6846  19
   4  -1  -7 165.717 12.1866  15
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   4   1   7 156.083 12.1764  13
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   4  -1  -8 54.2887 4.55197   1
   4   1   8 52.8233 4.54075   1
   4  -1  -8 49.9128 4.48842   2
   4   1   8 57.9666 4.53927   2
   4   1   8 54.9526 4.20997  34
   4  -1  -8 87.5074 5.30975  29
   4  -1  -8 54.1908 4.76001  34
   4  -1  -8 60.6519 4.91218  25
   4  -1  -8 56.3146 4.82413  24
   4   1   8 59.6465 4.63652  25
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   4  -1  -8 52.8249 4.56426   9
   4   1   8 61.2760 4.49959  23
   4   1   8 63.3188 4.87814  20
   4  -1  -8 45.2642 4.77384  21
   4  -1  -8 62.6807 4.88020  22
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   4   1   8 58.2108 4.88176  17
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   4   1   8 53.3338 4.13524  19
   4  -1  -8 60.6468 4.81658  15
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   4   1   8 47.6395 4.73813  13
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   4   1   9 1567.46 101.629   1
   4  -1  -9 1557.07 101.627   1
   4   1   9 1721.42 101.684   2
   4   1   9 1663.01 101.363  34
   4   1   9 1527.29 101.655  25
   4  -1  -9 1614.37 101.910  25
   4  -1  -9 1701.43 101.901  24
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   4  -1  -9 1560.22 101.723   9
   4   1   9 1670.34 101.653  23
   4  -1  -9 1211.75 101.705  21
   4  -1  -9 1244.32 101.708  22
   4   1   9 1716.31 101.911  20
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   4   1   9 1542.89 101.896  17
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   4   1   9 1502.62 101.356  19
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   4   1   9 1462.75 101.869  13
   4  -1  -9 1651.59 101.922  15
   4   1  10 8.86367 1.23839   3
   4  -1 -10 10.3750 2.05336   1
   4   1  10 5.71576 1.84356   2
   4   1  10 5.96983 1.89930   1
   4  -1 -10 7.69043 1.96671   2
   4   1  10 8.49057 2.39948  13
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   4   1  10 6.66512 1.98891  25
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   4  -1 -10 6.97523 1.90021   9
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   4   1  10 10.6275 2.05848  23
   4  -1 -10 9.56213 2.33886  22
   4   1  10 7.18422 2.23258  20
   4  -1 -10 8.55874 2.47782  21
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   4   1  10 7.26838 2.23084  17
   4   1  10 7.52727 1.56627  19
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   4   1  11 1765.24 133.206   1
   4  -1 -11 2133.17 133.328   2
   4   1  11 2134.72 132.950   3
   4   1  11 2206.32 133.307   2
   4  -1 -11 2056.35 133.594  15
   4   1  11 2225.11 133.768  13
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   4  -1 -11 2144.24 133.579  24
   4   1  11 2109.44 133.363  25
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   4  -1 -11 1757.94 133.411   9
   4   1  11 2371.83 133.522  23
   4  -1 -11 1546.86 133.431  21
   4   1  11 1895.51 133.494  20
   4  -1 -11 2364.26 133.816  22
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   4   1  11 2153.40 133.690  17
   4   1  11 2259.01 133.184  19
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   4   1  12 354.264 21.6850   2
   4   1  12 313.753 21.2600   3
   4   1  12 272.231 21.5690   1
   4  -1 -12 344.123 21.7092   2
   4   1  12 320.980 22.1179  13
   4  -1 -12 316.105 21.9704  15
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   4  -1 -12 338.297 21.0794  28
   4  -1 -12 342.867 21.9924  24
   4   1  12 300.857 21.6573  25
   4  -1 -12 314.608 21.9103   9
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   4   1  12 369.807 21.9338  23
   4  -1 -12 297.630 22.0711  21
   4  -1 -12 374.129 22.2753  22
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   4   1  12 331.134 22.0986  17
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   4   1  12 320.280 21.5332  19
   4  -1 -12 324.655 21.9593  20
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   4   1  13 2359.51 154.912   2
   4   1  13 2421.41 154.607   3
   4   1  13 2985.77 155.139   1
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   4  -1 -13 2448.71 155.272  24
   4  -1 -13 2443.77 154.458  28
   4   1  13 2320.11 154.996  25
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   4   1  13 2462.45 155.223  23
   4  -1 -13 2771.13 155.670  21
   4  -1 -13 1898.01 155.189  22
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   4   1  13 2441.26 155.392  17
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   4  -1 -13 3114.54 155.590  20
   4   1  13 2531.48 154.942  19
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   4   1  14 113.104 7.43087   3
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   4   1  14 113.864 7.83404   2
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   4  -1 -14 112.535 8.30459  34
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   4   1  14 138.937 8.39855  23
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   4   1  14 112.897 7.89589  19
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   4   1  15 268.660 18.4883   2
   4   1  15 336.011 18.6860   1
   4   1  15 283.671 18.1775   3
   4  -1 -15 286.484 18.5622   2
   4  -1 -15 221.472 18.7711  34
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   4  -1 -15 275.137 18.9253  24
   4  -1 -15 274.550 18.1082  28
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   4   1  15 270.091 18.5979  25
   4  -1 -15 259.101 19.0066   9
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   4  -1 -15 289.594 19.2167  22
   4   1  15 265.390 18.9185  23
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   4   1  15 282.376 19.1227  17
   4   1  15 293.333 18.6472  19
   4  -1 -15 262.085 18.9354  15
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   4   1  16 414.430 26.4113   2
   4   1  16 390.140 26.0634   3
   4   1  16 446.528 26.4912   1
   4  -1 -16 396.289 26.4160   2
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   4  -1 -16 398.406 26.8929  34
   4   1  16 388.487 26.5064  25
   4  -1 -16 416.972 26.8601  24
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   4  -1 -16 405.279 26.0641  28
   4  -1 -16 410.942 27.0298   9
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   4   1  16 394.694 26.8990  23
   4  -1 -16 442.996 27.2438  22
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   4   1  16 392.139 26.5812  19
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   4   1  16 371.800 26.9332  17
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   4  -1 -16 375.399 26.8546  15
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   4   1  17 1325.53 85.6829   3
   4   1  17 1417.30 86.0018   2
   4   1  17 1456.49 86.0615   1
   4  -1 -17 1320.14 85.9920   2
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   4  -1 -17 1300.14 86.4898  34
   4   1  17 1310.07 86.0940  25
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   4  -1 -17 1397.67 85.7261  28
   4  -1 -17 1354.17 86.4353  24
   4  -1 -17 1221.57 86.5541   9
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   4   1  17 1386.42 86.6096  23
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   4   1  17 1326.54 86.6261  17
   4   1  17 1367.27 86.2446  19
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   4   1  18 103.468 7.22207   3
   4   1  18 134.139 7.76056   1
   4  -1 -18 98.8352 7.55565   2
   4  -1 -18 115.133 8.73122  29
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   4  -1 -18 115.325 8.34150  34
   4  -1 -18 95.1298 8.00134  24
   4   1  18 93.5210 7.70641  25
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   4  -1 -18 106.212 7.35088  28
   4  -1 -18 125.973 8.72711   9
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   4   1  18 103.968 8.33779  23
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   4  -1 -18 117.911 8.65928  22
   4   1  18 102.613 7.91484  19
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   4   1  18 96.8053 8.36723  17
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   4  -1 -18 92.3845 8.08103  15
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   4   1  19 257.098 16.8582   3
   4  -1 -19 259.026 17.1587   2
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   4  -1 -19 228.154 18.0001  29
   4  -1 -19 256.127 17.7920  34
   4  -1 -19 262.311 17.6940  24
   4   1  19 286.488 17.4017  25
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   4  -1 -19 256.428 16.9970  28
   4  -1 -19 227.151 17.8997   9
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   4  -1 -19 290.350 18.3140  22
   4   1  19 260.158 17.9355  23
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   4   1  19 245.161 17.5300  19
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   4   1  19 250.440 17.9586  17
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   4  -2   4 2287.16 129.594   2
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   4   2  -4 1965.94 129.593  29
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   4  -2   4 2353.32 129.448  34
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   4   2  -4 1894.24 129.482  34
   4   2  -4 1838.97 129.584  25
   4  -2   4 1749.36 129.288  25
   4  -2   4 2034.81 129.554  27
   4   2  -4 1826.01 129.521  24
  -4   2   4 2139.49 128.837  28
   4   2  -4 1982.75 129.587   9
   4  -2   4 1799.55 129.583  20
   4   2  -4 1957.08 129.652  22
   4   2  -4 2064.37 129.620  20
   4   2  -4 2158.40 129.731  21
   4  -2   4 1920.07 129.062  23
   4  -2   4 2098.64 129.360  21
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   4  -2   4 2050.81 129.589  17
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   4   2  -4 2160.39 129.472  13
   4  -2   4 1696.08 129.362  15
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   4  -2   3 323.798 17.8902   2
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   4   2  -3 270.875 17.8545  29
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   4  -2   3 285.830 17.6298  34
   4   2  -3 281.826 17.7892  34
   4   2  -3 268.368 17.9006  25
   4  -2   3 269.671 17.7535  27
   4  -2   3 282.243 17.6716  25
   4   2  -3 254.511 17.7761   9
   4  -2   3 354.486 18.1994  20
   4   2  -3 301.126 17.9434  20
   4   2  -3 244.234 17.8443  21
   4  -2   3 280.792 17.6377  21
   4  -2   3 250.736 17.2077  23
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   4  -2   3 273.604 17.8439  17
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   4   2  -3 172.746 17.4243  13
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   4  -2   3 283.232 17.7617  15
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   4  -2   2 1359.62 94.9129   2
   4   2  -2 1066.29 94.8276  29
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   4  -2   2 1638.35 94.9518  34
   4   2  -2 1549.61 95.0107  34
   4  -2   2 1476.72 94.9661  27
   4  -2   2 1576.80 94.9279  25
   4   2  -2 1537.24 95.1443  25
   4   2  -2 2053.14 95.3489   9
   4   2  -2 1513.59 95.0694  20
   4  -2   2 1364.16 95.0720  20
   4   2  -2 1281.53 94.9911  21
   4  -2   2 1507.82 94.8660  21
   4  -2   2 1514.80 94.4430  23
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   4  -2   2 1498.24 95.0571  17
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   4   2  -2 1343.40 94.8543  13
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   4   2  -1 387.782 23.7364  34
   4  -2   1 362.581 23.6548  34
   4   2  -1 361.015 23.1592  27
   4  -2   1 346.345 23.6374  27
   4  -2   1 388.954 23.7014  25
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   4   2  -1 340.185 23.6950   1
   4  -2   1 383.282 23.7596   2
   4   2  -1 373.648 23.6923   2
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   4  -2   1 368.442 23.6433  21
   4   2  -1 320.213 23.7734  21
   4   2  -1 267.381 23.6049  20
   4  -2   1 362.934 23.0916  23
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   4  -2   1 385.015 23.8613  17
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   4   2  -1 281.574 23.5251  13
   4  -2   1 373.528 23.1227  12
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   4   2   0 7996.90 467.633   1
   4  -2   0 6587.50 467.512   2
   4   2   0 7443.01 467.552   2
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   4  -2   0 6239.48 467.437  34
   4   2   0 7811.98 467.558  34
   4   2   0 7401.86 467.091  27
   4  -2   0 7345.84 467.509  27
   4  -2   0 7631.98 467.570  25
   4  -2   0 7252.88 466.924  23
   4   2   0 7332.43 467.682  21
   4   2   0 7468.11 467.653  20
   4  -2   0 7140.59 467.500  21
   4  -2   0 7129.40 467.686  20
   4  -2   0 7318.56 467.647  17
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   4   2   0 7574.66 467.564  13
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   4  -2   0 7231.14 466.962  12
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   4   2   1 368.940 23.6979   2
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   4   2   1 405.759 23.8112   1
   4  -2  -1 334.508 23.6976   2
   4  -2  -1 348.190 23.6897  34
   4   2   1 336.980 23.5942  34
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   4  -2  -1 371.003 23.6509  27
   4   2   1 347.221 23.2384  27
   4   2   1 407.871 23.8052  24
   4  -2  -1 371.621 23.7542  25
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   4   2   1 306.666 23.6611  20
   4  -2  -1 359.042 23.7088  21
   4  -2  -1 359.219 23.8746  20
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   4  -2  -1 382.519 23.8555  17
   4   2   1 426.480 23.8306  13
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   4   2   2 1399.32 92.8445   1
   4  -2  -2 1372.05 92.8417   2
   4   2   2 1504.51 92.8563   2
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   4  -2  -2 1352.12 92.8331  34
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   4   2   2 1448.61 92.7499  34
   4   2   2 1440.74 92.4616  27
   4   2   2 1631.44 92.9086  24
   4  -2  -2 1312.94 92.7172  27
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   4  -2  -2 1352.56 92.5290   9
   4   2   2 1225.60 92.7831  20
   4  -2  -2 1469.16 92.8776  21
   4  -2  -2 1187.82 92.8603  22
   4   2   2 1617.32 93.0840  17
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   4  -2  -2 1693.26 93.0899  17
   4   2   2 1435.10 92.8713  13
  -4   2  -3 252.248 17.6264   5
  -4   2  -3 283.719 17.8317   6
  -4  -2   3 270.999 17.9417   3
   4   2   3 212.132 17.7738   1
   4   2   3 236.724 17.8217   2
   4  -2  -3 264.255 17.9525  34
  -4  -2   3 287.551 17.3146  33
  -4   2  -3 280.116 17.4819  33
   4   2   3 265.932 17.7766  34
   4  -2  -3 236.675 17.7609  27
   4   2   3 286.871 17.9188  24
   4  -2  -3 247.961 17.6045   9
  -4   2  -3 237.589 17.8246  11
  -4  -2   3 252.759 17.3352  12
   4  -2  -3 265.363 18.0773  22
   4  -2  -3 251.956 17.9160  21
   4   2   3 275.845 18.1080  17
   4  -2  -3 282.819 18.0839  17
  -4   2  -3 304.012 17.5311  16
   4  -2  -3 266.106 18.0457  15
   4   2   3 253.571 17.9177  13
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  -4   2  -4 1813.71 128.901   6
  -4  -2   4 2133.58 129.161   3
  -4   2  -4 2026.17 128.662   3
   4   2   4 2113.49 129.088   1
   4   2   4 2137.97 129.061   2
   4   2   4 2001.14 128.905  34
   4  -2  -4 2087.13 129.143  34
   4   2   4 1885.10 128.933  24
   4   2   4 1946.26 129.123  25
   4  -2  -4 1977.14 128.964  27
   4  -2  -4 2069.58 128.840   9
  -4   2  -4 1781.37 128.965  11
  -4  -2   4 1910.72 128.503  12
   4  -2  -4 2157.55 129.185  24
   4  -2  -4 2081.70 129.162  21
   4  -2  -4 1909.41 129.142  22
   4   2   4 2543.04 129.322  20
   4   2   4 1788.53 129.117  17
   4  -2  -4 2208.46 129.237  17
  -4   2  -4 1919.58 128.672  16
   4  -2  -4 1973.68 129.175  15
   4   2   4 2235.61 129.191  13
  -4   2  -5 2120.59 129.892   6
  -4   2  -5 1915.69 129.654   5
  -4  -2   5 1968.74 129.982   3
   4   2   5 1952.12 129.887   1
  -4   2  -5 1951.09 129.461   3
   4   2   5 2179.18 129.945   2
   4   2   5 1993.60 129.737  34
  -4   2  -5 2101.82 129.374  30
   4  -2  -5 1930.78 129.963  34
   4  -2  -5 2153.16 130.054  24
  -4  -2   5 1790.79 129.372  27
   4  -2  -5 2005.38 129.828  27
   4   2   5 2286.44 129.877  24
   4   2   5 1932.94 129.970  25
   4  -2  -5 2202.44 129.781   9
  -4   2  -5 2142.90 129.977  11
  -4  -2   5 1891.69 129.369  12
   4   2   5 2174.22 129.751  23
   4  -2  -5 2052.34 130.065  22
   4  -2  -5 2048.93 130.042  21
   4   2   5 1801.14 129.892  20
   4   2   5 1907.11 130.074  17
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   4  -2  -5 2297.80 130.131  17
   4   2   5 2212.20 130.063  13
   4  -2  -5 2168.13 130.118  15
  -4   2  -6 183.501 11.2872   6
  -4   2  -6 162.370 10.6464   3
   4   2   6 165.775 10.9339   3
   4   2   6 139.741 11.1043   1
   4  -2  -6 163.542 11.2069   2
   4   2   6 184.872 11.2597   2
   4   2   6 176.029 10.5454  33
   4   2   6 175.208 11.0142  34
   4  -2  -6 163.491 11.3139  34
   4   2   6 162.387 11.0756  24
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   4  -2  -6 149.732 11.2763  24
   4  -2  -6 187.809 11.5057  25
   4   2   6 160.827 11.2939  25
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   4  -2  -6 150.339 11.0084   9
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   4  -2  -6 163.930 11.3804  21
   4   2   6 217.551 11.5515  20
   4  -2  -6 124.853 11.1860  22
   4   2   6 172.099 11.0501  23
   4   2   6 150.000 11.3689  17
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   4  -2  -6 140.760 11.2632  17
   4   2   6 164.325 11.3257  13
   4  -2  -6 163.274 11.3960  15
  -4   2  -7 167.599 11.2458   6
   4   2   7 177.241 11.1975   2
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   4   2   7 154.939 10.8843   3
   4   2   7 154.240 11.1447   1
   4  -2  -7 171.836 11.2431   2
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   4  -2  -7 164.865 11.3297  34
   4   2   7 134.224 10.8967  24
   4  -2  -7 151.245 11.2825  24
   4  -2  -7 196.946 11.5331  25
   4   2   7 159.488 11.2774  25
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   4  -2  -7 156.444 11.0603   9
   4   2   7 169.291 11.0793  23
   4  -2  -7 177.677 11.4853  21
   4   2   7 150.420 11.2341  20
   4  -2  -7 119.299 11.1651  22
   4   2   7 136.814 11.3147  17
   4  -2  -7 187.603 11.4916  17
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   4   2   7 171.663 10.6777  19
   4   2   7 171.328 11.3795  13
   4  -2  -7 149.521 11.2969  15
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   4   2   8 614.851 42.5858   8
   4   2   8 638.848 42.4076   2
   4   2   8 608.710 42.4226   1
  -4   2  -8 619.523 41.8749   4
   4  -2  -8 655.143 42.4744   2
   4   2   8 643.174 42.1836   3
   4  -2  -8 652.905 42.6371  34
   4  -2  -8 565.206 42.5107  24
   4   2   8 772.906 42.3500  24
   4   2   8 607.123 42.5055  25
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   4  -2  -8 656.199 42.4222   9
   4   2   8 686.877 42.4385  23
   4  -2  -8 691.238 42.7569  21
   4   2   8 782.869 42.7480  20
   4  -2  -8 620.852 42.6476  22
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   4   2   8 602.981 42.6590  17
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   4   2   8 637.998 42.0206  19
   4  -2  -8 629.191 42.6364  15
   4   2   8 588.070 42.5705  13
   4   2   9 144.234 9.53376   2
   4   2   9 124.259 9.50204   1
   4   2   9 130.740 9.19769   3
   4  -2  -9 137.617 9.56330   2
   4   2   9 138.236 9.80591  13
   4  -2  -9 121.324 9.65451  15
   4  -2  -9 141.936 9.75722  24
   4   2   9 139.280 9.66927  25
   4   2   9 155.055 9.36812  24
   4  -2  -9 126.801 9.49720   9
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   4   2   9 128.805 9.49495  23
   4  -2  -9 127.903 9.83222  21
   4   2   9 105.846 9.53808  20
   4  -2  -9 134.711 9.75108  20
   4  -2  -9 154.029 9.92802  22
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   4   2   9 139.656 9.88307  17
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   4   2   9 136.803 9.10164  19
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   4   2   9 132.886 9.75377   8
   4   2  10 397.933 24.8689   2
   4   2  10 371.673 24.8715   1
   4  -2 -10 382.014 24.8951   2
   4   2  10 390.055 24.6018   3
   4   2  10 405.880 25.2354  13
   4  -2 -10 414.110 25.2353  15
   4  -2 -10 381.424 25.0973  24
   4   2  10 310.262 24.5338  24
   4   2  10 405.442 25.0370  25
   4  -2 -10 409.250 25.0219   9
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   4  -2 -10 385.076 25.2615  21
   4   2  10 390.565 25.0615  20
   4  -2 -10 308.800 24.9772  22
   4  -2 -10 426.659 25.2036  20
   4   2  10 329.282 24.8410  23
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   4   2  10 383.990 25.2377  17
   4   2  10 402.137 24.5490  19
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   4   2  10 390.795 25.1814   8
   4   2  11 704.376 48.1190   2
   4   2  11 719.815 47.8984   3
   4   2  11 844.388 48.3048   1
   4  -2 -11 769.269 48.2383   2
   4   2  11 770.333 48.5642  13
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   4  -2 -11 761.694 48.5401  15
   4  -2 -11 751.606 48.4235  24
   4   2  11 774.430 48.3346  25
   4  -2 -11 896.239 48.5292   9
   4  -2 -11 805.473 48.6917  21
   4  -2 -11 756.123 48.5440  22
   4   2  11 820.194 48.4092  23
   4   2  11 647.870 48.2582  20
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   4   2  11 722.722 48.5366  17
   4   2  11 726.424 47.8987  19
   4  -2 -11 900.037 48.6266  20
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   4   2  11 731.961 48.5144   8
   4   2  12 674.308 42.2351   2
   4   2  12 658.647 41.9746   3
   4  -2 -12 678.429 42.2934   2
   4   2  12 622.035 42.2281   1
   4   2  12 689.870 42.7246  13
   4  -2 -12 608.701 42.5202  15
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   4  -2 -12 670.058 42.5315  24
   4   2  12 672.498 42.4033  25
   4  -2 -12 658.160 42.4768   9
   4   2  12 716.051 42.5371  23
   4  -2 -12 506.240 42.4843  21
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   4  -2 -12 549.035 42.4754  22
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   4   2  12 679.099 42.7129  17
   4  -2 -12 687.962 42.5547  20
   4   2  12 632.608 42.0144  19
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   4   2  12 662.866 42.6413   8
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   4   2  13 301.946 20.0194   2
   4   2  13 299.468 19.7701   3
   4   2  13 242.839 19.9356   1
   4  -2 -13 313.315 20.1056   2
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   4  -2 -13 310.782 20.3820  24
   4   2  13 318.810 20.2532  25
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   4   2  13 356.736 20.4809  23
   4  -2 -13 352.976 20.8568  21
   4  -2 -13 249.872 20.3120  22
   4   2  13 299.783 20.3382  20
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   4   2  13 290.761 19.8745  19
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   4   2  13 316.113 20.6030  13
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   4   2  14 108.594 7.77594   3
   4   2  14 126.083 8.12902   2
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   4  -2 -14 113.091 8.50930  34
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   4  -2 -14 127.056 8.66294   9
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   4  -2 -14 110.634 8.82790  21
   4   2  14 108.051 8.39496  23
   4  -2 -14 100.462 8.51998  22
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   4   2  14 128.071 8.06049  19
   4   2  14 129.751 8.83599  17
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   4  -2 -14 125.272 8.56005  20
   4   2  14 101.904 8.58387  13
   4  -2 -14 115.575 8.60290  15
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   4   2  15 110.489 8.07856   3
   4  -2 -15 114.505 8.39280   2
   4   2  15 120.695 8.46401   1
   4  -2 -15 131.401 8.99660  34
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   4   4   4 298.556 18.2523   2
   4   4   4 271.556 17.5076  33
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   4   4   4 223.449 17.9911  24
   4  -4  -4 269.485 17.7429   9
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   4   4   4 256.335 18.1188  20
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   4  -4  -4 262.019 18.3673  13
   4   4   4 277.851 18.0862  13
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   5  -1   8 22.5920 3.20489   2
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   5   1  -8 42.3999 4.02104  21
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   5   1  -7 2551.07 151.945   1
   5  -1   7 2442.11 151.867   2
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   5   1  -7 2331.42 151.962  34
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   5  -1   5 1402.32 125.770   1
   5   1  -5 2038.72 126.295  29
   5  -1   5 2000.88 125.298  33
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   5  -1   5 1980.76 125.836  34
   5   1  -5 1965.46 126.102  34
   5  -1   5 2168.52 126.050  25
   5   1  -5 1934.94 126.202  25
   5  -1   5 2019.77 125.993  27
   5   1  -5 1806.22 126.079  24
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   5   1  -5 1945.40 126.063   9
   5  -1   5 1992.46 125.519  23
   5  -1   5 1960.30 126.262  20
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   5   1  -5 2061.49 126.348  22
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   5   1  -5 1745.36 126.079  15
   5   1  -5 2274.31 126.187  13
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   5  -1   4 145.417 9.49291   1
   5  -1   4 142.415 9.44580   2
   5  -1   4 131.894 8.49783  33
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   5  -1   4 112.130 9.07441  34
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   5   1  -4 154.880 9.70424  24
   5  -1   4 142.370 9.41753  25
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   5  -1   4 137.184 9.27945  27
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   5   1  -4 167.628 9.62105   9
   5  -1   4 119.560 8.68091  23
   5   1  -4 149.937 9.67418  20
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   5  -1   3 122.974 8.44805  34
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   5  -1   3 112.461 8.67981  17
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   5   1  -3 130.931 8.69740  13
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   5   1  -2 92.1119 8.15804   1
   5  -1   2 127.988 8.37088   2
   5   1  -2 112.465 8.23965   2
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   5  -1   2 118.430 8.17927  34
   5   1  -2 116.951 8.27969  34
   5   1  -2 128.235 7.72852  27
   5  -1   2 113.761 8.09164  27
   5  -1   2 109.432 8.26187  25
   5  -1   2 108.692 7.44894  12
   5  -1   2 96.6656 8.34650  20
   5   1  -2 116.609 8.50048  20
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   5   1  -2 98.6457 8.36208  21
   5  -1   2 113.250 8.26647  21
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   5  -1   2 122.383 8.55697  17
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   5   1  -2 113.128 8.29992  13
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   5   1  -1 29.7520 3.29639   2
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   5  -1   1 30.5115 3.24687   1
   5   1  -1 29.2176 3.19893   1
   5  -1   1 23.2551 3.00264   2
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   5  -1   1 29.8184 3.15164  34
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   5  -1   1 29.2848 2.94785  27
   5  -1   1 25.5144 3.12492  25
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   5  -1   1 38.9904 3.59485  20
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   5  -1   1 24.2034 3.13481  21
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   5  -1   0 158.830 10.9027  34
   5   1   0 141.261 10.7996  34
   5   1   0 159.331 10.4510  27
   5  -1   0 165.496 10.7075  27
   5  -1   0 165.666 11.0612  25
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   5  -1   0 158.473 10.9430   1
   5   1   0 144.992 10.9095   1
   5  -1   0 156.972 10.9393   2
   5   1   0 146.008 10.8923   2
   5   1   0 199.411 11.3634  20
   5  -1   0 151.581 10.9775  21
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   5   1   0 151.010 11.0635  21
   5  -1   0 141.968 11.0472  20
   5  -1   0 174.285 11.1833  17
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   5   1   0 139.902 11.0578  17
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   5  -9 -11 55.3014 4.25078   9
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   5  -9 -11 48.6846 5.44303  21
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   7  -1  -7 354.802 22.2686   2
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   7   3   4 101.061 7.21695  27
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   7   4   7 214.286 13.5394   2
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   7  -4  -7 189.604 13.5012   2
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   7   4   8 82.7923 7.63912  25
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   7  -4  -8 83.2447 6.74089   9
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   7   4   9 218.149 15.8369   2
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   7  -4  -9 192.532 15.1753   9
   7   4   9 268.712 16.2620  20
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   7   4   9 223.962 16.3869  17
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   7   4  13 26.2429 4.19564   1
   7  -4 -13 28.9281 4.08787   2
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   7   7   6 677.152 36.3899  24
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   7   7   6 486.564 35.6791  13
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   7   7   7 21.4536 4.37971  25
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   7   7   9 2.36557 2.79719  13
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   7   7  10 18.9574 3.50184  13
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   7   7  11 71.1813 6.76832  20
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   7  -7 -11 80.3327 7.56660  13
   7   7  11 70.0064 6.83570  13
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   7   7  12 195.077 16.1604   1
   7  -7 -12 250.343 16.6027   2
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   7  -7 -12 228.628 16.7967  34
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   7   7  12 257.084 15.8947  24
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   7  -9  -6 143.672 10.7117  21
   7  -9  -6 125.218 10.8544  20
   7   9   6 131.302 11.0420  17
   7   9   6 132.571 10.2956  20
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   7   9   6 117.163 9.67189  13
   7  -9  -6 149.294 11.2627  15
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   7  -9  -7 339.725 23.8463   2
   7   9   7 317.010 23.5702   1
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   7   9   7 357.595 23.3856  24
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   7   9   7 328.758 24.1564  25
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   7   9   7 374.299 23.1772  20
   7  -9  -7 333.579 23.4677  21
   7  -9  -7 347.931 23.7014  20
   7   9   7 342.814 24.0328  17
   7  -9  -7 357.401 24.1633  13
   7   9   7 332.128 22.7172  13
   7  -9  -7 348.059 23.9822  15
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   7  -9  -8 338.838 23.4416  34
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   7   9   8 395.984 22.9830  24
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   7   9   8 347.352 23.7286  25
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   7   9   8 331.068 22.4959  20
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   7   9   8 361.436 23.7104  17
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   8   1 -17 69.0173 8.10703   9
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   8   1 -16 245.897 19.1262   9
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   8  -1   9 31.4313 5.15287  13
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   8  -1   8 231.109 16.7934  25
   8   1  -8 261.374 17.4656  24
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   8   1  -8 222.472 17.4077  21
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   8  -1   7 191.253 14.6084  17
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   8   1  -6 33.9571 4.52563   2
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   8   1  -6 27.6182 4.94209  21
   8  -1   6 29.1079 4.86432  20
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   8  -1   4 151.913 10.7621  27
   8  -1   4 145.800 11.2954  25
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   8  -1   4 132.267 11.2685   2
   8  -1   4 155.963 11.8772  20
   8   1  -4 186.519 12.1050  20
   8   1  -4 130.439 11.4545  21
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   8  -1   4 141.316 11.5864  17
   8   1  -4 154.793 11.3617  13
   8  -1   4 141.112 11.7030  13
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   8  -1   3 310.109 19.8638  34
   8   1  -3 284.512 19.9516  34
   8  -1   3 273.021 19.3119  27
   8   1  -3 307.979 20.4737  25
   8  -1   3 312.731 20.1186  25
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   8  -1   3 233.689 19.7008   2
   8  -1   3 266.888 20.2234  20
   8   1  -3 342.544 20.6855  20
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   8  -1   3 305.594 20.4599  17
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   8   1  -3 241.200 19.7143  13
   8  -1   3 225.126 19.9482  13
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   8  -1   2 256.390 18.8683  34
   8   1  -2 262.872 19.0315  34
   8  -1   2 283.376 18.5017  27
   8   1  -2 287.797 19.5407  25
   8  -1   2 285.659 19.2200  25
   8   1  -2 306.534 19.4531  24
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   8   1  -2 268.001 19.1848   1
   8  -1   2 286.599 19.2641   2
   8   1  -2 253.531 19.0513   2
   8   1  -2 267.056 19.4386  20
   8  -1   2 242.088 19.3053  20
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   8  -1   2 282.644 19.5775  17
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   8   1  -2 212.580 18.8255  13
   8  -1   2 258.565 19.3823  13
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   8  -1  -3 304.074 20.0693  25
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   8  -1  -3 283.704 20.0526  17
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   8   1   3 308.134 20.2868  17
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   8  -1  -3 237.166 19.7520  13
   8   1   3 227.533 19.6502  13
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   8   1   4 161.909 11.5986   1
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   8  -1  -4 156.339 11.5241  34
   8   1   4 133.401 10.3033  27
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   8  -1  -4 164.574 11.8236  25
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   8  -1  -4 131.565 11.6420  20
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   8   1   5 143.166 12.5523   1
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   8   1   6 20.1433 4.05264   2
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   8   1   6 27.3227 3.91355  34
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   8  -1  -6 34.0376 4.58868  34
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   8   1   6 25.9113 4.49917  25
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   8   1   8 284.737 17.1259   1
   8  -1  -8 233.147 16.7188   2
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   8   1   9 37.4182 4.74612   2
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   8   1   9 36.7010 4.97677   1
   8  -1  -9 34.4955 5.05741  34
   8   1   9 28.2981 3.90009  27
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   8   1  12 66.5816 6.90270   2
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   8   1  12 66.8057 6.79587  25
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   8  -1 -13 264.930 18.9422   2
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   8   1  17 66.1822 7.37691  23
   8   1  17 90.0428 8.54971  20
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   8   1  18 97.5874 8.98982  20
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   8  -1 -19 107.075 9.31552   9
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   8   1  19 107.727 8.69810  23
   8   1  19 97.9689 9.39077  20
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   8  -1 -19 102.988 9.85834  21
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   8   1  19 93.0848 9.74967  17
   8  -1 -19 96.7839 9.42639  15
   8   1  19 95.7353 9.77164  13
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   8  -1 -20 24.7497 4.13343   2
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   8  -1 -20 34.2143 5.50847  34
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   8   1  20 31.3144 4.13974  25
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   8  -1 -20 33.7285 5.21939   9
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   8   1  20 18.5779 4.28103  23
   8  -1 -20 11.9740 5.31325  21
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   8   3 -11 78.3797 8.32424   9
   8  -3  11 86.9374 7.10648  23
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   8  -3  10 4.58940 3.28907   2
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   8   3   2 21.5240 3.90384   2
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   8   3   2 19.6199 3.98866   1
   8  -3  -2 18.8686 4.10246   2
   8   3   2 21.3736 3.67907  34
   8  -3  -2 13.5234 3.79734  34
   8  -3  -2 7.61743 3.25925  27
   8   3   2 19.8117 4.31752  25
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   8   3   2 22.6405 3.89565  24
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   8   3   2 14.7702 4.21120  20
   8  -3  -2 17.0424 4.42438  17
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   8   3   2 14.8056 3.80140  13
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   8  -3  -2 18.3818 4.01669  15
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   8   3   3 129.304 10.8425   1
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   8  -3  -3 103.010 10.3775  34
   8  -3  -3 136.582 10.2607  27
   8   3   3 135.456 9.23018  27
   8   3   3 146.537 11.0774  25
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   8   3   3 164.306 11.2699  20
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   8   3   3 145.290 10.8493  13
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   8   3   4 216.429 16.3089   2
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   8   3   4 241.937 16.6072   1
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   8  -3  -4 220.695 16.4076  34
   8   3   4 208.089 15.0215  27
   8   3   4 233.899 16.6891  25
   8   3   4 218.900 16.2910  24
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   8  -3  -4 206.539 16.4125  21
   8   3   4 193.952 16.3558  20
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   8  -3  -4 260.307 16.9241  17
   8   3   4 238.619 16.9361  17
   8  -3  -4 174.888 16.2305  13
   8   3   4 226.938 16.4125  13
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   8   3   5 62.4001 5.95978   2
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   8   3   5 57.1029 6.05454   1
   8  -3  -5 54.6527 5.93048  34
   8   3   5 43.6082 4.33727  27
   8   3   5 40.9091 5.84183  25
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   8   3   5 59.3608 5.87520  24
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   8   3   5 36.4221 5.82353  17
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   8   3   5 56.9003 5.90406  13
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   8   3   6 167.512 12.3733   2
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   8   3   6 205.291 12.8552   1
   8  -3  -6 163.089 12.5622  34
   8   3   6 186.798 12.4657  24
   8   3   6 178.119 12.7395  25
   8   3   6 160.232 11.2074  27
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   8   3   6 145.370 12.4627  20
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   8  -3  -6 162.610 12.6744  17
   8   3   6 146.107 12.6911  17
   8  -3  -6 212.143 13.1820  13
   8   3   6 167.611 12.5088  13
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   8   3   7 55.2379 5.53390   2
   8   3   7 48.9579 5.61339   1
   8  -3  -7 52.7007 5.38044   2
   8  -3  -7 46.3850 5.59374  34
   8   3   7 39.4525 4.05470  27
   8   3   7 47.9299 5.73376  25
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   8   3   7 53.0740 5.80723  20
   8  -3  -7 49.6275 5.72426  21
   8   3   7 40.5490 5.80859  17
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   8  -3  -7 55.3390 6.03176  17
   8  -3  -7 43.7823 5.60360  13
   8   3   7 36.3100 5.41433  13
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   8   3   8 17.3803 3.88862   2
   8   3   8 16.8016 4.06201   1
   8  -3  -8 9.89508 3.69296   2
   8  -3  -8 17.6782 3.67922  34
   8   3   8 15.6545 4.06945  25
   8   3   8 11.7671 2.41330  27
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   8   3   8 8.21176 3.79358  20
   8  -3  -8 8.11954 3.99365  21
   8   3   8 10.9087 3.84329  17
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   8  -3  -8 13.6988 4.16955  17
   8  -3  -8 15.4184 3.97131  13
   8   3   8 4.92763 3.53803  13
   8  -3  -8 8.16423 3.46836  15
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   8   3   9 132.678 10.6216   2
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   8   3   9 139.703 10.7932   1
   8  -3  -9 142.468 10.7180   2
   8  -3  -9 150.058 11.1106  34
   8   3   9 130.983 10.6888  25
   8   3   9 115.477 9.54000  27
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   8   3   9 120.576 10.6231  20
   8  -3  -9 108.119 10.5798  21
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   8  -4  -4 36.0307 4.66900  34
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   8  -4  -6 112.777 10.1579  34
   8   4   6 133.260 10.5280  25
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   8   4   6 119.261 10.2504  20
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   8  -4  -6 143.609 10.6784  17
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   8  -8  13 144.815 13.2304  13
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   8   8 -12 133.814 9.65351   1
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   8   8 -12 90.3713 9.56871  29
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   8  -8  12 98.9551 8.42098  34
   8  -8  12 93.7102 9.63620  27
   8   8 -12 111.066 10.1316  25
   8   8 -12 114.555 10.0769  24
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   8   8 -12 100.847 10.0483  22
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   8   8 -11 44.8357 5.62004   1
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   8   8 -11 44.1852 5.88717  29
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   8   8 -11 44.7243 6.36775  24
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   8   8 -11 43.4927 6.47306  25
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   8   8 -11 31.9812 5.88777  22
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   8   8 -10 133.489 11.9764  25
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   8   8  -9 21.3021 5.36598  25
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   8  -8   9 28.8015 5.40927  13
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   8   8  -8 56.8589 6.31074   1
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   8  -8   8 37.0158 6.25560  13
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   8   8  -7 165.387 12.9382   1
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   8  -8   7 155.925 12.3835  15
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   8   8  -6 73.7665 7.15725   1
   8  -8   6 60.6612 6.72965   2
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   8  -8   6 53.3647 6.07380  34
   8  -8   6 50.9556 6.66014  27
   8   8  -6 79.6460 7.43030  24
   8   8  -6 56.0028 7.04157  25
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   8  -8   6 66.1641 6.45551  15
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   8  -8   5 88.2440 7.85979   2
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   8  -8   5 73.2915 7.41555  34
   8   8  -5 74.9947 7.95816  24
   8  -8   5 74.8033 8.00311  27
   8   8  -5 64.5114 8.30009  25
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   8  -8   5 81.2285 8.41894  20
   8   8  -5 66.2999 7.98994  22
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   8   8  -5 82.1925 7.85165  20
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   8  -8   5 68.7174 8.39439  13
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   8  -8   5 85.1703 7.70705  15
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   8  -8   4 263.527 18.8042  34
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   8   8  -4 260.648 19.4758  25
   8   8  -4 210.550 18.8298  24
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   8  -8   4 308.088 19.2576  17
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   8  -8   4 279.776 19.8684  13
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   8   8  -4 246.899 17.7993  13
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   8  -8   3 197.873 15.9781   2
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   8  -8   3 223.553 15.8730  34
   8  -8   3 222.174 16.2800  27
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   8   8  -3 258.782 16.6113  24
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   8   8  -3 263.476 16.2387  20
   8   8  -3 196.792 15.9802  17
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   8  -8   2 107.889 8.82007  34
   8  -8   2 97.7479 8.98058  27
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   8   8  -2 92.9241 8.92737  24
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   8  -8   2 91.7787 8.03813  21
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   8   8  -2 87.7117 8.65150  20
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   8   8  -2 90.4236 8.86948  17
   8   8  -2 109.877 7.67812  13
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   8  -8   2 110.910 9.55864  13
   8  -8   2 83.5967 8.58305  15
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   8   8  -1 98.5877 8.70305   1
   8  -8   1 101.099 8.91473   2
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   8  -8   1 81.9250 8.31136  34
   8   8  -1 96.6682 9.15586  25
   8  -8   1 105.438 8.89238  27
   8   8  -1 102.987 8.90761  24
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   8  -8   1 88.5137 7.90533  21
   8  -8   1 96.9493 9.20673  20
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   8   8  -1 110.491 8.67683  20
   8   8  -1 55.1432 8.21101  17
   8   8  -1 111.436 7.57767  13
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   8  -8   1 96.5810 9.26550  13
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   8  -8   1 97.0819 8.65344  15
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  -8   8   0 422.411 27.4846   6
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   8   8   0 371.100 28.4608   1
   8  -8   0 449.857 28.7764   2
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   8  -8   0 368.148 28.2452  34
   8  -8   0 431.204 28.6479  27
   8   8   0 420.151 28.5356  24
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   8  -8   0 390.063 28.7582  20
   8  -8   0 410.155 27.8344  21
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   8   8   0 524.862 28.6891  20
   8   8   0 451.477 28.8057  17
   8   8   0 405.864 27.3849  13
   8  -8   0 411.370 29.0254  13
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   8  -8   0 401.001 28.5007  15
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   8  -8  -1 98.8065 8.58416   2
   8   8   1 73.3882 8.24988   1
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   8  -8  -1 100.126 8.45997  34
   8  -8  -1 100.343 8.60551  27
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   8   8   1 119.178 8.87236  24
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   8  -8  -1 90.0536 8.77082  20
   8  -8  -1 87.0836 7.81351  21
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   8   8   1 111.693 8.48209  20
   8   8   1 94.6247 8.61170  17
   8   8   1 77.9497 7.13443  13
   8  -8  -1 78.9940 8.67923  13
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   8  -8  -1 98.3689 8.64726  15
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   8   8   2 103.995 9.05655   1
   8  -8  -2 112.434 9.14852   2
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   8  -8  -2 115.808 9.14797  34
   8  -8  -2 108.266 9.18708  27
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   8   8   2 79.5343 8.70385  24
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   8  -8  -2 99.0701 9.10841  20
   8  -8  -2 91.7073 8.41827  21
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   8   8   2 124.561 9.05414  20
   8   8   2 83.4548 9.02152  17
   8   8   2 83.1638 7.60228  13
   8  -8  -2 106.618 9.47346  13
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   8  -8  -2 110.386 9.19152  15
  -8   8  -3 223.120 14.6132   6
  -8  -8   3 194.410 15.7051   5
  -8  -8   3 178.228 14.8911   3
   8   8   3 240.278 15.6615   1
  -8  -8   3 247.521 14.6559   4
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   8  -8  -3 188.373 15.3158  34
   8  -8  -3 230.371 15.6056  27
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   8   8   3 147.100 14.7044  24
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   8  -8  -3 199.754 15.5841  20
   8  -8  -3 220.667 15.0380  21
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   8   8   3 192.787 14.9610  20
   8   8   3 192.721 15.5377  17
   8  -8  -3 217.648 15.7923  13
   8   8   3 205.275 14.3060  13
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   8  -8  -3 200.059 15.4645  15
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   8   8   4 254.350 19.9152   1
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   8  -8  -4 257.105 19.9873  34
   8  -8  -4 297.519 20.1026  27
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   8   8   4 276.570 19.7867  24
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   8  -8  -4 306.814 20.4215  20
   8  -8  -4 310.686 19.8190  21
   8   8   4 228.215 19.3805  20
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   8   8   4 294.101 20.4320  17
   8  -8  -4 297.415 20.5782  13
   8   8   4 265.223 19.0121  13
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   8  -8  -4 284.242 20.2400  15
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   8   8   5 91.6415 8.03778   1
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   8  -8  -5 75.4846 7.94625  34
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   8   8   5 85.3402 8.48688  25
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   8   8   5 84.7689 7.68349  24
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   8   8   5 89.2199 7.64563  20
   8  -8  -5 94.3739 7.87949  21
   8  -8  -5 88.2076 8.32393  20
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   8   8   5 90.1514 8.67811  17
   8  -8  -5 83.7337 8.52347  13
   8   8   5 65.6653 6.72377  13
   8  -8  -5 97.2031 8.32180  15
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   8   8   6 44.8155 6.38154   1
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   8  -8  -6 53.3960 6.69574  34
  -8  -8   6 67.7649 7.26245  30
   8   8   6 53.7571 6.12140  24
   8   8   6 65.5064 7.10413  25
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   8  -8  -6 58.4729 6.75547  20
   8  -8  -6 64.8113 6.53405  21
   8   8   6 53.0753 6.76447  17
   8   8   6 56.9472 6.26481  20
   8  -8  -6 56.9955 7.05517  13
   8   8   6 73.6564 5.82758  13
   8  -8  -6 71.1049 7.08642  15
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   8   8   7 195.372 13.2790   1
   8  -8  -7 157.190 12.9970   2
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   8  -8  -7 161.252 13.1485  34
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   8   8   7 182.415 12.6737  24
   8   8   7 166.116 13.5797  25
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   8  -8  -7 174.883 12.8950  21
   8   8   7 180.945 12.7343  20
   8  -8  -7 154.426 13.0358  20
   8   8   7 160.755 13.3847  17
   8  -8  -7 166.084 13.3406  13
   8   8   7 131.289 11.8666  13
   8  -8  -7 149.691 12.9951  15
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   8   8   8 36.8073 5.81229   1
   8  -8  -8 48.2067 6.15241   2
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   8  -8  -8 50.7407 6.55696  34
   8   8   8 54.4215 6.71208  25
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   8   8   8 58.5186 5.81983  24
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   8  -8  -8 49.6579 6.38890  20
   8  -8  -8 56.8599 6.27057  21
   8   8   8 57.9305 6.92383  17
   8   8   8 45.6593 5.58131  20
   8  -8  -8 66.1961 7.08445  13
   8   8   8 63.2380 5.48442  13
  -8   8  -9 23.3921 4.43394   6
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   8   8   9 27.1824 4.78246   1
   8  -8  -9 24.9295 4.71192   2
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   8  -8  -9 14.7446 4.87410  34
   8   8   9 28.9470 5.66519  25
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   8   8   9 34.7600 4.52276  24
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   8  -8  -9 31.2437 5.28417  20
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   8  -9   6 60.3264 6.46212  34
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   8   9   6 62.7442 5.81403  13
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   8   9   7 239.604 17.7351  25
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   8  -9  -7 226.022 17.2440  20
   8   9   7 252.091 16.6614  20
   8   9   7 227.638 17.5853  17
   8  -9  -7 218.350 17.5090  13
   8   9   7 246.295 16.1299  13
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   8   9   8 22.1092 4.53000   1
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   8   9   8 18.4396 3.38274  13
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   8  -9  -9 193.648 15.2490  13
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   8   9  11 68.5213 6.25895  13
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   8   9  13 57.3759 6.66982   1
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   8   9  13 60.3005 7.62800  25
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   8  -9 -13 53.8246 7.07457  21
   8   9  13 55.6144 5.62365  24
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   8   9  13 49.7714 5.86676  20
   8  -9 -13 77.9810 7.13788  20
   8  -9 -13 60.5861 7.34784  13
   8   9  13 57.0050 5.87813  13
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   8  -9 -15 38.8336 5.58993  20
   8   9  15 30.8153 4.53772  20
   8  -9 -15 29.4194 5.80771  15
   8   9  15 32.1035 4.65715  13
   8   9  16 129.422 11.3871   1
   8  -9 -16 136.521 11.5280   2
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   8   9  16 129.865 11.0185  13
   8  -9 -16 133.210 12.2666  15
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   8   9  16 130.867 12.0879  25
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 -14  -2  -5 5.41666 5.74786  18
  14  -2   5 3.50066 6.14578  17
  14  -2   5 2.37469 5.51224  13
 -14  -2  -5-0.73452 5.33122  11
 -14   2   4 2.92321 5.38388  18
 -14  -2  -4 1.54958 5.46107  18
  14  -2   4-0.87964 6.27760  17
  14  -2   4 3.13248 5.67978  13
 -14   2   4 4.11302 4.58759  11
 -14  -2  -4-3.64194 5.19841  11
  14  -2   3 7.03124 5.48303  13
 -14   2   3 3.70051 5.55817  18
 -14  -2  -3 5.41988 5.59329  18
  14  -2   3 5.30345 6.19769  17
  14  -2   3 12.6019 6.49558  20
  14   2  -3 5.98643 6.24710  20
  14  -2   3 19.9266 6.41044   2
 -14   2   3 4.83744 4.87443  11
 -14  -2  -3 12.2599 5.95182  11
  14  -2   2-0.77239 5.97207  13
 -14   2   2 8.22918 5.58046  18
 -14  -2  -2 9.27387 6.01697  18
  14  -2   2 3.61037 6.46456  20
  14   2  -2 7.65860 6.31666  20
  14  -2   2 8.81121 5.67239   2
 -14   2   2 14.9014 5.33527  11
 -14  -2  -2 17.1101 5.47779  11
  14  -2   1 8.46818 5.50685  13
 -14   2   1 9.06793 5.81282  18
 -14  -2  -1 19.2359 6.24049  18
  14  -2   1 10.7750 6.46957  20
  14   2  -1 16.0885 6.49127  20
  14  -2   1 29.7063 6.50393   2
 -14   2   1 19.7129 5.59891  11
 -14  -2  -1 23.9207 6.27355  11
  14  -2   0 9.89728 5.67371  13
 -14   2   0 15.2364 5.80388  18
 -14  -2   0 3.06262 5.68397  18
  14  -2   0 9.89613 6.76506  20
  14   2   0 11.0092 6.27794  20
  14  -2   0 10.4560 6.16686   2
 -14   2   0 11.0472 5.08719  11
 -14  -2   0 17.3182 5.17079  11
  14  -2  -1 12.1361 5.79643  13
 -14   2  -1 9.19206 5.97678  18
 -14  -2   1 9.11878 5.80686  18
  14  -2  -1 22.4880 7.28333  20
  14   2   1 26.9513 6.44655  20
  14  -2  -1 5.62963 5.89196   2
 -14   2  -1 20.5414 5.75654  11
 -14  -2   1 6.81250 5.32923  11
 -14   2  -2 2.30805 5.56218  18
 -14  -2   2 10.5524 5.76754  18
  14  -2  -2 10.7189 6.47542  20
  14   2   2 6.68959 5.99241  20
  14  -2  -2 17.2861 5.77152  13
 -14   2  -2 12.8203 5.54152  11
 -14  -2   2 2.67520 5.10561  11
 -14   2  -3 8.48869 5.51738  18
 -14  -2   3 10.4410 5.61012  18
  14   2   3 9.84427 6.74492  17
  14   2   3 8.34724 6.52182  20
  14  -2  -3 12.4971 6.65329  20
  14  -2  -3 10.4778 5.60884  13
 -14   2  -3 10.2814 5.32981  11
 -14  -2   3 6.55333 5.13391  11
 -14   2  -4-5.40819 5.82166  18
 -14  -2   4-1.47374 5.63356  18
  14   2   4 2.68580 6.64584  17
  14  -2  -4 14.1712 6.74687  20
  14  -2  -4 2.22732 5.27706  13
 -14   2  -4 6.25843 5.27836  11
 -14  -2   4-0.64049 4.70071  11
 -14   2  -5 0.77148 5.70552  18
 -14  -2   5-0.72654 5.24883  18
  14   2   5-1.78930 6.27935  17
  14  -2  -5 9.58336 5.77517  13
 -14   2  -5 0.70401 5.36325  11
 -14   3   3 4.41900 5.19583  18
 -14  -3  -3 0.77165 5.48877  18
  14   3  -3 6.07699 5.99295  17
  14  -3   3 5.65511 5.84000  13
 -14  -3  -3 2.17765 5.16384  11
 -14   3   2-0.74440 5.39841  18
 -14  -3  -2 1.54071 5.47467  18
  14   3  -2 3.49431 6.62998  17
  14  -3   2-3.99539 5.90878  13
 -14   3   2 2.42163 5.09974  11
 -14  -3  -2 2.87154 5.10182  11
 -14   3   1-2.25477 5.64235  18
 -14  -3  -1 2.30117 5.42919  18
  14   3  -1 1.75576 6.41714  17
  14  -3   1-0.79676 5.75563  13
 -14   3   1 0.62115 5.15538  11
 -14  -3  -1-7.09928 5.71073  11
  14  -3   0 7.88498 5.81141  13
 -14   3   0 6.82008 5.49883  18
 -14  -3   0-3.81705 5.83887  18
  14   3   0 4.41057 6.21981  17
  14  -3   0 3.60001 6.21119  20
  14  -3   0 4.01355 5.61279   2
 -14   3   0-2.54374 5.46942  11
 -14  -3   0 7.70334 5.12238  11
 -14   3  -1-3.24670 5.23961  11
 -14  -3   1-3.44711 5.28883  11
  14  -3  -1 1.57170 5.76633  13
 -14   3  -1 1.52406 5.54802  18
 -14  -3   1 4.54678 5.47360  18
  14  -3  -1-0.90056 6.29321  20
 -14   3  -2-0.66167 5.00347  11
 -14  -3   2-0.67754 4.87429  11
 -14   3  -2-0.76543 5.32600  18
 -14  -3   2-4.50785 5.42676  18
  14  -3  -2 6.23118 5.60348  13
 -14   3  -3 11.5174 5.93606  18
 -14  -3   3-2.97532 5.79080  18
  14  -3  -3 4.65488 5.40275  13
   0   0   0    0.00    0.00   0
TITL elg_m2 in P2(1)2(1)2(1)
REM P2(1)2(1)2(1) (#19 in standard setting)
CELL 0.71073   7.112656  13.765001  24.385042  90.0000  90.0000  90.0000
ZERR    5.00   0.000057   0.000091   0.000156   0.0000   0.0000   0.0000
LATT -1
SYMM -x+1/2,-y, z+1/2
SYMM -x, y+1/2,-z+1/2
SYMM  x+1/2,-y+1/2,-z
SFAC C H N O S
UNIT 100.00 115.00 15.00 25.00 5.00
REM  CrysAlisPro recorded range (K): Min=99.4; max=100.5; aver:99.9
TEMP -173
TREF
HKLF 4
END
;
_shelx_hkl_checksum              33813
_shelx_res_file
;
TITL elg_m2 in P2(1)2(1)2(1)
    shelx.res
    created by SHELXL-2019/3 at 10:17:35 on 23-May-2024
CELL 0.71073   7.112656  13.765001  24.385042  90.0000  90.0000  90.0000
ZERR    4.00   0.00011    0.00018    0.00031    0.0000   0.0000   0.0000
LATT -1
SYMM -x+1/2,-y, z+1/2
SYMM -x, y+1/2,-z+1/2
SYMM  x+1/2,-y+1/2,-z
SFAC C H N O S
UNIT 88 100 12 36 4
TEMP -173
SIZE 0.22 0.2 0.12
OMIT     1   0  13
OMIT     0  14   0
OMIT     0   9   6
OMIT     0   9   3
OMIT     0  10   1
OMIT     0   3   7
OMIT     0  10  12
L.S.  8
FMAP  2
PLAN  10
ACTA  88
CONF
BOND $H
REM Instructions for potential hydrogen bonds
EQIV $1 -x+2, y+1/2, -z+1/2
HTAB N1 N3_$1
EQIV $2 -x+1, y-1/2, -z+1/2
HTAB C1 O10_$2
EQIV $3 x-1, y, z
HTAB C3 S1_$3
EQIV $4 x-1/2, -y+1/2, -z+1
HTAB C10 O7_$4
HTAB C22 N2
EQIV $5 -x+1, y+1/2, -z+1/2
HTAB C26 O8_$5
RTAB CONT N1 N3_$1
WGHT    0.048000    0.076600
FVAR       0.86047   0.91482
C1    1    0.679023    0.491773    0.300408    11.00000    0.01778    0.01183 =
         0.01096   -0.00107   -0.00130    0.00272
AFIX  13
H1    2    0.607670    0.469895    0.267301    11.00000   -1.20000
AFIX   0
C2    1    0.596044    0.444850    0.352093    11.00000    0.02037    0.00989 =
         0.01183   -0.00075   -0.00138    0.00177
AFIX  13
H2    2    0.681305    0.455499    0.384141    11.00000   -1.20000
AFIX   0
C3    1    0.401615    0.486260    0.363974    11.00000    0.01831    0.01066 =
         0.01323   -0.00004   -0.00076   -0.00019
AFIX  13
H3    2    0.309321    0.461262    0.336444    11.00000   -1.20000
AFIX   0
SAME O3 O8' C9' C10'
O3    4    0.341634    0.460618    0.418251    11.00000    0.02277    0.01426 =
         0.01539   -0.00120    0.00414   -0.00305
PART 1 21
O8    4    0.187142    0.328641    0.386550    21.00000    0.04461    0.01855 =
         0.02444    0.00097   -0.00159   -0.01302
C9    1    0.225381    0.383112    0.423546    21.00000    0.02500    0.01260 =
         0.01979    0.00355    0.00188   -0.00171
C10   1    0.156887    0.375805    0.481721    21.00000    0.04085    0.02143 =
         0.02560    0.00570    0.01180   -0.00448
AFIX 137
H10A  2    0.243788    0.335424    0.503006    21.00000   -1.50000
H10B  2    0.031472    0.346335    0.482175    21.00000   -1.50000
H10C  2    0.150750    0.440894    0.497907    21.00000   -1.50000
AFIX   0
PART 2 -21
O8'   4    0.040574    0.449641    0.412576   -21.00000    0.02400
C9'   1    0.176528    0.434527    0.440722   -21.00000    0.01732
C10'  1    0.182027    0.395105    0.498224   -21.00000    0.02329
AFIX 137
H10D  2    0.289209    0.423227    0.517864   -21.00000   -1.50000
H10E  2    0.195208    0.324269    0.497011   -21.00000   -1.50000
H10F  2    0.065248    0.412132    0.517263   -21.00000   -1.50000
AFIX   0
PART 0
C4    1    0.405674    0.597022    0.362399    11.00000    0.01485    0.01058 =
         0.01398   -0.00005   -0.00102    0.00118
AFIX  13
H4    2    0.484944    0.622506    0.393062    11.00000   -1.20000
AFIX   0
C5    1    0.485233    0.630449    0.307354    11.00000    0.01581    0.01188 =
         0.01390    0.00081   -0.00130    0.00211
AFIX  13
H5    2    0.409177    0.601467    0.276990    11.00000   -1.20000
AFIX   0
C6    1    0.492133    0.739639    0.300340    11.00000    0.01876    0.01234 =
         0.01594    0.00251   -0.00159    0.00268
AFIX  23
H6A   2    0.573273    0.756840    0.268815    11.00000   -1.20000
H6B   2    0.364335    0.765314    0.293363    11.00000   -1.20000
AFIX   0
C7    1    0.637858    0.279854    0.379098    11.00000    0.03640    0.01221 =
         0.01788    0.00379    0.00718    0.00474
C8    1    0.620110    0.177793    0.358752    11.00000    0.05279    0.01120 =
         0.03317    0.00197    0.01165    0.00383
AFIX 137
H8A   2    0.493557    0.167691    0.343918    11.00000   -1.50000
H8B   2    0.641808    0.132528    0.389119    11.00000   -1.50000
H8C   2    0.713332    0.166268    0.329882    11.00000   -1.50000
AFIX   0
C11   1    0.164475    0.665699    0.418298    11.00000    0.02041    0.01341 =
         0.01764    0.00011    0.00212    0.00282
C12   1   -0.044264    0.680339    0.420594    11.00000    0.01971    0.02612 =
         0.02783    0.00089    0.00665    0.00268
AFIX 137
H11A  2   -0.087665    0.708723    0.385980    11.00000   -1.50000
H11B  2   -0.075191    0.724242    0.450918    11.00000   -1.50000
H11C  2   -0.106371    0.617621    0.426385    11.00000   -1.50000
AFIX   0
C13   1    0.588367    0.877744    0.350529    11.00000    0.01803    0.01118 =
         0.02191    0.00177   -0.00122    0.00189
C14   1    0.651747    0.913683    0.405611    11.00000    0.02449    0.01618 =
         0.02591   -0.00191   -0.00449    0.00016
AFIX 137
H14A  2    0.664811    0.858562    0.430759    11.00000   -1.50000
H14B  2    0.558608    0.959336    0.420204    11.00000   -1.50000
H14C  2    0.773211    0.946622    0.401839    11.00000   -1.50000
AFIX   0
C15   1    0.938111    0.428698    0.224304    11.00000    0.01312    0.00960 =
         0.01346   -0.00093   -0.00051    0.00101
C16   1    1.008188    0.269830    0.239976    11.00000    0.02123    0.01096 =
         0.01715    0.00014    0.00095    0.00392
C21   1    0.875943    0.503620    0.133640    11.00000    0.01434    0.01211 =
         0.01390    0.00071    0.00055    0.00085
C22   1    0.846543    0.419585    0.102746    11.00000    0.02157    0.01487 =
         0.01433   -0.00077   -0.00154   -0.00132
AFIX  43
H22   2    0.840788    0.357998    0.120248    11.00000   -1.20000
AFIX   0
C23   1    0.825702    0.426663    0.046078    11.00000    0.02574    0.02243 =
         0.01437   -0.00121   -0.00114   -0.00030
AFIX  43
H23   2    0.807747    0.369485    0.024898    11.00000   -1.20000
AFIX   0
C24   1    0.830941    0.516509    0.020297    11.00000    0.03550    0.02770 =
         0.01419    0.00383    0.00069    0.00061
AFIX  43
H24   2    0.817216    0.520920   -0.018375    11.00000   -1.20000
AFIX   0
C25   1    0.856396    0.599895    0.051458    11.00000    0.04634    0.02119 =
         0.01897    0.00718    0.00023    0.00032
AFIX  43
H25   2    0.858150    0.661515    0.033920    11.00000   -1.20000
AFIX   0
C26   1    0.879377    0.594390    0.108058    11.00000    0.03175    0.01373 =
         0.01843    0.00354    0.00070    0.00104
AFIX  43
H26   2    0.897212    0.651772    0.129069    11.00000   -1.20000
AFIX   0
S1    5    0.921634    0.451769    0.295796    11.00000    0.01891    0.01705 =
         0.01272   -0.00329   -0.00441    0.00635
O1    4    0.674255    0.594536    0.304217    11.00000    0.01621    0.01094 =
         0.01608    0.00052    0.00068    0.00274
O2    4    0.581214    0.343285    0.340127    11.00000    0.02984    0.00939 =
         0.01796   -0.00127   -0.00270    0.00238
O4    4    0.216025    0.631000    0.368167    11.00000    0.01475    0.01583 =
         0.01572   -0.00029   -0.00017    0.00233
O6    4    0.567035    0.780730    0.350058    11.00000    0.02063    0.01058 =
         0.01749    0.00184   -0.00200    0.00061
O7    4    0.694565    0.304405    0.423343    11.00000    0.08265    0.02128 =
         0.01744    0.00543   -0.00578    0.00955
O9    4    0.273450    0.681392    0.454928    11.00000    0.02881    0.02924 =
         0.02007   -0.00892   -0.00325    0.00755
O10   4    0.556710    0.928430    0.311083    11.00000    0.03597    0.01366 =
         0.02690    0.00636   -0.00678    0.00210
N1    3    0.898579    0.503668    0.191442    11.00000    0.01859    0.00905 =
         0.01394   -0.00041   -0.00146    0.00104
H01   2    0.898391    0.558299    0.207202    11.00000    0.02772
N2    3    0.989731    0.343565    0.205397    11.00000    0.01933    0.00998 =
         0.01473   -0.00016    0.00178    0.00311
N3    3    1.026030    0.199106    0.265560    11.00000    0.03637    0.01388 =
         0.02268    0.00323    0.00121    0.00717
HKLF 4
REM  elg_m2 in P2(1)2(1)2(1)
REM wR2 = 0.0787, GooF = S = 1.056, Restrained GooF = 1.056 for all data
REM R1 = 0.0286 for 17947 Fo > 4sig(Fo) and 0.0329 for all 19593 data
REM 338 parameters refined using 6 restraints
END
WGHT      0.0480      0.0766
REM Highest difference peak  0.482,  deepest hole -0.210,  1-sigma level  0.051
Q1    1   1.0131  0.2412  0.2550  11.00000  0.05    0.48
Q2    1   0.8534  0.5598  0.0317  11.00000  0.05    0.44
Q3    1   0.8854  0.5471  0.1211  11.00000  0.05    0.41
Q4    1   0.9588  0.3833  0.2140  11.00000  0.05    0.39
Q5    1   0.8789  0.4189  0.3011  11.00000  0.05    0.38
Q6    1   0.8520  0.4597  0.1177  11.00000  0.05    0.38
Q7    1   0.5790  0.9008  0.3278  11.00000  0.05    0.36
Q8    1   0.1481  0.3577  0.3967  11.00000  0.05    0.36
Q9    1   0.4149  0.5446  0.3660  11.00000  0.05    0.35
Q10   1   0.2204  0.6768  0.4349  11.00000  0.05    0.35
;
_shelx_res_checksum              40771
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, -y, z+1/2'
'-x, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C C1 0.67902(9) 0.49177(4) 0.30041(2) 0.01352(8) Uani d 1 . .
H H1 0.607670 0.469895 0.267301 0.016 Uiso calc 1 . .
C C2 0.59604(9) 0.44485(4) 0.35209(2) 0.01403(8) Uani d 1 . .
H H2 0.681305 0.455499 0.384141 0.017 Uiso calc 1 . .
C C3 0.40161(9) 0.48626(4) 0.36397(2) 0.01407(8) Uani d 1 . .
H H3 0.309321 0.461262 0.336444 0.017 Uiso calc 1 . .
O O3 0.34163(8) 0.46062(4) 0.41825(2) 0.01747(8) Uani d 1 . .
O O8 0.18714(14) 0.32864(5) 0.38655(3) 0.02920(16) Uani d 0.915(2) A 1
C C9 0.22538(12) 0.38311(5) 0.42355(3) 0.01913(13) Uani d 0.915(2) A 1
C C10 0.15689(18) 0.37581(8) 0.48172(5) 0.0293(2) Uani d 0.915(2) A 1
H H10A 0.243788 0.335424 0.503006 0.044 Uiso calc 0.915(2) A 1
H H10B 0.031472 0.346335 0.482175 0.044 Uiso calc 0.915(2) A 1
H H10C 0.150750 0.440894 0.497907 0.044 Uiso calc 0.915(2) A 1
O O8' 0.0406(10) 0.4496(6) 0.4126(3) 0.0240(13) Uiso d 0.085(2) A 2
C C9' 0.1765(11) 0.4345(6) 0.4407(3) 0.0173(12) Uiso d 0.085(2) A 2
C C10' 0.1820(15) 0.3951(8) 0.4982(4) 0.0233(17) Uiso d 0.085(2) A 2
H H10D 0.289209 0.423227 0.517864 0.035 Uiso calc 0.085(2) A 2
H H10E 0.195208 0.324269 0.497011 0.035 Uiso calc 0.085(2) A 2
H H10F 0.065248 0.412132 0.517263 0.035 Uiso calc 0.085(2) A 2
C C4 0.40567(8) 0.59702(4) 0.36240(2) 0.01314(7) Uani d 1 . .
H H4 0.484944 0.622506 0.393062 0.016 Uiso calc 1 . .
C C5 0.48523(9) 0.63045(4) 0.30735(2) 0.01386(8) Uani d 1 . .
H H5 0.409177 0.601467 0.276990 0.017 Uiso calc 1 . .
C C6 0.49213(9) 0.73964(4) 0.30034(3) 0.01568(9) Uani d 1 . .
H H6A 0.573273 0.756840 0.268815 0.019 Uiso calc 1 . .
H H6B 0.364335 0.765314 0.293363 0.019 Uiso calc 1 . .
C C7 0.63786(13) 0.27985(5) 0.37910(3) 0.02216(13) Uani d 1 . .
C C8 0.62011(18) 0.17779(6) 0.35875(4) 0.0324(2) Uani d 1 . .
H H8A 0.493557 0.167691 0.343918 0.049 Uiso calc 1 . .
H H8B 0.641808 0.132528 0.389119 0.049 Uiso calc 1 . .
H H8C 0.713332 0.166268 0.329882 0.049 Uiso calc 1 . .
C C11 0.16447(10) 0.66570(5) 0.41830(3) 0.01716(9) Uani d 1 . .
C C12 -0.04426(12) 0.68034(7) 0.42059(4) 0.02455(13) Uani d 1 . .
H H11A -0.087665 0.708723 0.385980 0.037 Uiso calc 1 . .
H H11B -0.075191 0.724242 0.450918 0.037 Uiso calc 1 . .
H H11C -0.106371 0.617621 0.426385 0.037 Uiso calc 1 . .
C C13 0.58837(10) 0.87774(4) 0.35053(3) 0.01704(9) Uani d 1 . .
C C14 0.65175(12) 0.91368(5) 0.40561(3) 0.02219(12) Uani d 1 . .
H H14A 0.664811 0.858562 0.430759 0.033 Uiso calc 1 . .
H H14B 0.558608 0.959336 0.420204 0.033 Uiso calc 1 . .
H H14C 0.773211 0.946622 0.401839 0.033 Uiso calc 1 . .
C C15 0.93811(8) 0.42870(4) 0.22430(2) 0.01206(7) Uani d 1 . .
C C16 1.00819(10) 0.26983(4) 0.23998(3) 0.01645(9) Uani d 1 . .
C C21 0.87594(8) 0.50362(4) 0.13364(2) 0.01345(8) Uani d 1 . .
C C22 0.84654(10) 0.41959(5) 0.10275(3) 0.01692(9) Uani d 1 . .
H H22 0.840788 0.357998 0.120248 0.020 Uiso calc 1 . .
C C23 0.82570(12) 0.42666(6) 0.04608(3) 0.02085(11) Uani d 1 . .
H H23 0.807747 0.369485 0.024898 0.025 Uiso calc 1 . .
C C24 0.83094(14) 0.51651(7) 0.02030(3) 0.02580(14) Uani d 1 . .
H H24 0.817216 0.520920 -0.018375 0.031 Uiso calc 1 . .
C C25 0.85640(16) 0.59990(6) 0.05146(3) 0.02884(16) Uani d 1 . .
H H25 0.858150 0.661515 0.033920 0.035 Uiso calc 1 . .
C C26 0.87938(13) 0.59439(5) 0.10806(3) 0.02130(11) Uani d 1 . .
H H26 0.897212 0.651772 0.129069 0.026 Uiso calc 1 . .
S S1 0.92163(2) 0.45177(2) 0.29580(2) 0.01623(3) Uani d 1 . .
O O1 0.67426(7) 0.59454(3) 0.30422(2) 0.01441(7) Uani d 1 . .
O O2 0.58121(9) 0.34328(3) 0.34013(2) 0.01906(8) Uani d 1 . .
O O4 0.21602(7) 0.63100(4) 0.36817(2) 0.01543(7) Uani d 1 . .
O O6 0.56703(8) 0.78073(3) 0.35006(2) 0.01623(7) Uani d 1 . .
O O7 0.69457(18) 0.30441(5) 0.42334(3) 0.0405(2) Uani d 1 . .
O O9 0.27345(10) 0.68139(5) 0.45493(3) 0.02604(11) Uani d 1 . .
O O10 0.55671(11) 0.92843(4) 0.31108(3) 0.02551(11) Uani d 1 . .
N N1 0.89858(8) 0.50367(3) 0.19144(2) 0.01386(7) Uani d 1 . .
H H01 0.898(2) 0.5583(11) 0.2072(6) 0.028(4) Uiso d 1 . .
N N2 0.98973(8) 0.34357(4) 0.20540(2) 0.01468(7) Uani d 1 . .
N N3 1.02603(12) 0.19911(5) 0.26556(3) 0.02431(12) Uani d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
C1 0.0178(2) 0.01183(17) 0.01096(17) 0.00272(15) -0.00130(15) -0.00107(14)
C2 0.0204(2) 0.00989(16) 0.01183(17) 0.00177(16) -0.00138(16) -0.00075(13)
C3 0.0183(2) 0.01066(17) 0.01323(18) -0.00019(15) -0.00076(16) -0.00004(14)
O3 0.0228(2) 0.01426(16) 0.01539(16) -0.00305(15) 0.00414(15) -0.00120(13)
O8 0.0446(4) 0.0185(2) 0.0244(3) -0.0130(3) -0.0016(3) 0.0010(2)
C9 0.0250(3) 0.0126(2) 0.0198(3) -0.0017(2) 0.0019(2) 0.00355(19)
C10 0.0409(5) 0.0214(3) 0.0256(4) -0.0045(3) 0.0118(4) 0.0057(3)
C4 0.01485(19) 0.01058(16) 0.01398(18) 0.00118(14) -0.00102(15) -0.00005(14)
C5 0.0158(2) 0.01188(17) 0.01390(18) 0.00211(15) -0.00130(16) 0.00081(14)
C6 0.0188(2) 0.01234(18) 0.0159(2) 0.00268(16) -0.00159(18) 0.00251(15)
C7 0.0364(4) 0.0122(2) 0.0179(2) 0.0047(2) 0.0072(2) 0.00379(17)
C8 0.0528(6) 0.0112(2) 0.0332(4) 0.0038(3) 0.0116(4) 0.0020(2)
C11 0.0204(2) 0.0134(2) 0.0176(2) 0.00282(18) 0.00212(19) 0.00011(16)
C12 0.0197(3) 0.0261(3) 0.0278(3) 0.0027(2) 0.0066(2) 0.0009(3)
C13 0.0180(2) 0.01118(18) 0.0219(2) 0.00189(16) -0.00122(19) 0.00177(16)
C14 0.0245(3) 0.0162(2) 0.0259(3) 0.0002(2) -0.0045(2) -0.0019(2)
C15 0.01312(18) 0.00960(15) 0.01346(17) 0.00101(13) -0.00051(14) -0.00093(13)
C16 0.0212(2) 0.01096(18) 0.0171(2) 0.00392(17) 0.00095(19) 0.00014(15)
C21 0.01434(19) 0.01211(17) 0.01390(18) 0.00085(14) 0.00055(15) 0.00071(14)
C22 0.0216(2) 0.0149(2) 0.0143(2) -0.00132(18) -0.00154(18) -0.00077(16)
C23 0.0257(3) 0.0224(3) 0.0144(2) -0.0003(2) -0.0011(2) -0.00121(19)
C24 0.0355(4) 0.0277(3) 0.0142(2) 0.0006(3) 0.0007(2) 0.0038(2)
C25 0.0463(5) 0.0212(3) 0.0190(3) 0.0003(3) 0.0002(3) 0.0072(2)
C26 0.0317(3) 0.0137(2) 0.0184(2) 0.0010(2) 0.0007(2) 0.00354(18)
S1 0.01891(6) 0.01705(6) 0.01272(5) 0.00635(5) -0.00441(4) -0.00329(4)
O1 0.01621(16) 0.01094(14) 0.01608(16) 0.00274(12) 0.00068(13) 0.00052(12)
O2 0.0298(2) 0.00939(14) 0.01796(17) 0.00238(15) -0.00270(18) -0.00127(13)
O4 0.01475(16) 0.01583(16) 0.01572(17) 0.00233(13) -0.00017(13) -0.00029(13)
O6 0.02063(19) 0.01058(14) 0.01749(17) 0.00061(13) -0.00200(15) 0.00184(12)
O7 0.0826(7) 0.0213(2) 0.0174(2) 0.0096(3) -0.0058(3) 0.00543(19)
O9 0.0288(3) 0.0292(3) 0.0201(2) 0.0075(2) -0.0032(2) -0.0089(2)
O10 0.0360(3) 0.01366(17) 0.0269(2) 0.00210(19) -0.0068(2) 0.00636(17)
N1 0.01859(19) 0.00905(14) 0.01394(16) 0.00104(13) -0.00146(14) -0.00041(12)
N2 0.01933(19) 0.00998(14) 0.01473(17) 0.00311(14) 0.00178(16) -0.00016(13)
N3 0.0364(3) 0.0139(2) 0.0227(2) 0.0072(2) 0.0012(2) 0.00323(18)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O1 C1 C2 . . 110.91(5) ?
O1 C1 S1 . . 109.24(4) ?
C2 C1 S1 . . 106.79(4) ?
O1 C1 H1 . . 109.9 ?
C2 C1 H1 . . 109.9 ?
S1 C1 H1 . . 109.9 ?
O2 C2 C3 . . 109.70(5) ?
O2 C2 C1 . . 105.78(5) ?
C3 C2 C1 . . 110.36(5) ?
O2 C2 H2 . . 110.3 ?
C3 C2 H2 . . 110.3 ?
C1 C2 H2 . . 110.3 ?
O3 C3 C2 . . 110.69(5) ?
O3 C3 C4 . . 105.95(5) ?
C2 C3 C4 . . 110.61(5) ?
O3 C3 H3 . . 109.8 ?
C2 C3 H3 . . 109.8 ?
C4 C3 H3 . . 109.8 ?
C9' O3 C3 . . 134.5(3) ?
C9 O3 C3 . . 117.56(5) ?
O8 C9 O3 . . 123.80(7) ?
O8 C9 C10 . . 126.31(8) ?
O3 C9 C10 . . 109.88(7) ?
C9 C10 H10A . . 109.5 ?
C9 C10 H10B . . 109.5 ?
H10A C10 H10B . . 109.5 ?
C9 C10 H10C . . 109.5 ?
H10A C10 H10C . . 109.5 ?
H10B C10 H10C . . 109.5 ?
O8' C9' O3 . . 115.0(7) ?
O8' C9' C10' . . 127.9(8) ?
O3 C9' C10' . . 117.0(7) ?
C9' C10' H10D . . 109.5 ?
C9' C10' H10E . . 109.5 ?
H10D C10' H10E . . 109.5 ?
C9' C10' H10F . . 109.5 ?
H10D C10' H10F . . 109.5 ?
H10E C10' H10F . . 109.5 ?
O4 C4 C3 . . 107.79(5) ?
O4 C4 C5 . . 109.65(5) ?
C3 C4 C5 . . 109.28(5) ?
O4 C4 H4 . . 110.0 ?
C3 C4 H4 . . 110.0 ?
C5 C4 H4 . . 110.0 ?
O1 C5 C6 . . 107.81(5) ?
O1 C5 C4 . . 106.87(5) ?
C6 C5 C4 . . 114.23(5) ?
O1 C5 H5 . . 109.3 ?
C6 C5 H5 . . 109.3 ?
C4 C5 H5 . . 109.3 ?
O6 C6 C5 . . 107.87(5) ?
O6 C6 H6A . . 110.1 ?
C5 C6 H6A . . 110.1 ?
O6 C6 H6B . . 110.1 ?
C5 C6 H6B . . 110.1 ?
H6A C6 H6B . . 108.4 ?
O7 C7 O2 . . 123.37(7) ?
O7 C7 C8 . . 126.24(7) ?
O2 C7 C8 . . 110.39(7) ?
C7 C8 H8A . . 109.5 ?
C7 C8 H8B . . 109.5 ?
H8A C8 H8B . . 109.5 ?
C7 C8 H8C . . 109.5 ?
H8A C8 H8C . . 109.5 ?
H8B C8 H8C . . 109.5 ?
O9 C11 O4 . . 123.78(7) ?
O9 C11 C12 . . 125.91(7) ?
O4 C11 C12 . . 110.31(7) ?
C11 C12 H11A . . 109.5 ?
C11 C12 H11B . . 109.5 ?
H11A C12 H11B . . 109.5 ?
C11 C12 H11C . . 109.5 ?
H11A C12 H11C . . 109.5 ?
H11B C12 H11C . . 109.5 ?
O10 C13 O6 . . 123.05(7) ?
O10 C13 C14 . . 125.28(6) ?
O6 C13 C14 . . 111.66(6) ?
C13 C14 H14A . . 109.5 ?
C13 C14 H14B . . 109.5 ?
H14A C14 H14B . . 109.5 ?
C13 C14 H14C . . 109.5 ?
H14A C14 H14C . . 109.5 ?
H14B C14 H14C . . 109.5 ?
N2 C15 N1 . . 122.54(5) ?
N2 C15 S1 . . 121.55(4) ?
N1 C15 S1 . . 115.89(4) ?
N3 C16 N2 . . 172.95(7) ?
C22 C21 C26 . . 120.18(6) ?
C22 C21 N1 . . 123.61(5) ?
C26 C21 N1 . . 116.19(5) ?
C23 C22 C21 . . 119.55(6) ?
C23 C22 H22 . . 120.2 ?
C21 C22 H22 . . 120.2 ?
C24 C23 C22 . . 120.58(7) ?
C24 C23 H23 . . 119.7 ?
C22 C23 H23 . . 119.7 ?
C23 C24 C25 . . 119.49(7) ?
C23 C24 H24 . . 120.3 ?
C25 C24 H24 . . 120.3 ?
C24 C25 C26 . . 120.86(7) ?
C24 C25 H25 . . 119.6 ?
C26 C25 H25 . . 119.6 ?
C25 C26 C21 . . 119.31(7) ?
C25 C26 H26 . . 120.3 ?
C21 C26 H26 . . 120.3 ?
C15 S1 C1 . . 100.24(3) y
C1 O1 C5 . . 111.70(5) ?
C7 O2 C2 . . 117.73(5) ?
C11 O4 C4 . . 117.08(5) ?
C13 O6 C6 . . 116.05(5) ?
C15 N1 C21 . . 128.26(5) ?
C15 N1 H01 . . 114.5(10) ?
C21 N1 H01 . . 116.9(10) ?
C15 N2 C16 . . 119.21(6) ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
C1 O1 . 1.4180(7) ?
C1 C2 . 1.5343(8) ?
C1 S1 . 1.8148(6) y
C1 H1 . 1.0000 ?
C2 O2 . 1.4321(7) ?
C2 C3 . 1.5236(9) ?
C2 H2 . 1.0000 ?
C3 O3 . 1.4347(8) ?
C3 C4 . 1.5254(8) ?
C3 H3 . 1.0000 ?
O3 C9' . 1.345(8) ?
O3 C9 . 1.3560(9) ?
O8 C9 . 1.2042(11) ?
C9 C10 . 1.5033(12) ?
C10 H10A . 0.9800 ?
C10 H10B . 0.9800 ?
C10 H10C . 0.9800 ?
O8' C9' . 1.204(10) ?
C9' C10' . 1.504(12) ?
C10' H10D . 0.9800 ?
C10' H10E . 0.9800 ?
C10' H10F . 0.9800 ?
C4 O4 . 1.4346(8) ?
C4 C5 . 1.5276(8) ?
C4 H4 . 1.0000 ?
C5 O1 . 1.4345(8) ?
C5 C6 . 1.5135(8) ?
C5 H5 . 1.0000 ?
C6 O6 . 1.4400(8) ?
C6 H6A . 0.9900 ?
C6 H6B . 0.9900 ?
C7 O7 . 1.2004(11) ?
C7 O2 . 1.3519(9) ?
C7 C8 . 1.4952(11) ?
C8 H8A . 0.9800 ?
C8 H8B . 0.9800 ?
C8 H8C . 0.9800 ?
C11 O9 . 1.2022(10) ?
C11 O4 . 1.3627(8) ?
C11 C12 . 1.4993(11) ?
C12 H11A . 0.9800 ?
C12 H11B . 0.9800 ?
C12 H11C . 0.9800 ?
C13 O10 . 1.2094(9) ?
C13 O6 . 1.3440(8) ?
C13 C14 . 1.5007(11) ?
C14 H14A . 0.9800 ?
C14 H14B . 0.9800 ?
C14 H14C . 0.9800 ?
C15 N2 . 1.3117(7) y
C15 N1 . 1.3365(7) y
C15 S1 . 1.7759(6) y
C16 N3 . 1.1632(9) ?
C16 N2 . 1.3260(8) y
C21 C22 . 1.3962(9) ?
C21 C26 . 1.3967(9) ?
C21 N1 . 1.4187(8) y
C22 C23 . 1.3932(9) ?
C22 H22 . 0.9500 ?
C23 C24 . 1.3879(11) ?
C23 H23 . 0.9500 ?
C24 C25 . 1.3884(13) ?
C24 H24 . 0.9500 ?
C25 C26 . 1.3919(11) ?
C25 H25 . 0.9500 ?
C26 H26 . 0.9500 ?
N1 H01 . 0.845(15) ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_publ_flag
N1 H01 N3 3_755 0.845(15) 2.118(16) 2.9367(8) 163.2(15) yes
C1 H1 O10 3_645 1.00 2.31 3.3110(8) 176.7 yes
C3 H3 S1 1_455 1.00 2.93 3.8268(6) 149.2 yes
C10 H10A O7 4_456 0.98 2.66 3.4036(12) 133.3 yes
C22 H22 N2 . 0.95 2.34 2.8979(9) 117.1 yes
C26 H26 O8 3_655 0.95 2.54 3.2616(10) 133.3 yes
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion
_geom_torsion_publ_flag
O1 C1 C2 O2 . . . . 171.22(5) ?
S1 C1 C2 O2 . . . . -69.85(5) ?
O1 C1 C2 C3 . . . . 52.63(6) ?
S1 C1 C2 C3 . . . . 171.56(4) ?
O2 C2 C3 O3 . . . . 77.33(6) ?
C1 C2 C3 O3 . . . . -166.51(5) ?
O2 C2 C3 C4 . . . . -165.56(5) ?
C1 C2 C3 C4 . . . . -49.39(6) ?
C2 C3 O3 C9' . . . . -141.6(5) ?
C4 C3 O3 C9' . . . . 98.5(5) ?
C2 C3 O3 C9 . . . . -97.88(7) y
C4 C3 O3 C9 . . . . 142.17(6) ?
C3 O3 C9 O8 . . . . 8.68(12) y
C3 O3 C9 C10 . . . . -172.23(7) ?
C3 O3 C9' O8' . . . . -14.2(10) ?
C3 O3 C9' C10' . . . . 168.7(6) ?
O3 C3 C4 O4 . . . . -65.90(6) ?
C2 C3 C4 O4 . . . . 174.10(4) ?
O3 C3 C4 C5 . . . . 174.99(5) ?
C2 C3 C4 C5 . . . . 54.99(6) ?
O4 C4 C5 O1 . . . . 179.85(4) ?
C3 C4 C5 O1 . . . . -62.21(6) ?
O4 C4 C5 C6 . . . . 60.71(6) ?
C3 C4 C5 C6 . . . . 178.65(5) ?
O1 C5 C6 O6 . . . . -73.30(6) ?
C4 C5 C6 O6 . . . . 45.31(7) y
C26 C21 C22 C23 . . . . 1.71(10) ?
N1 C21 C22 C23 . . . . 179.96(6) ?
C21 C22 C23 C24 . . . . -1.03(12) ?
C22 C23 C24 C25 . . . . -0.28(14) ?
C23 C24 C25 C26 . . . . 0.92(16) ?
C24 C25 C26 C21 . . . . -0.25(15) ?
C22 C21 C26 C25 . . . . -1.08(12) ?
N1 C21 C26 C25 . . . . -179.45(8) ?
N2 C15 S1 C1 . . . . -123.75(5) ?
N1 C15 S1 C1 . . . . 57.56(5) y
O1 C1 S1 C15 . . . . -101.53(4) y
C2 C1 S1 C15 . . . . 138.46(4) ?
C2 C1 O1 C5 . . . . -63.21(6) ?
S1 C1 O1 C5 . . . . 179.34(4) y
C6 C5 O1 C1 . . . . -169.35(5) ?
C4 C5 O1 C1 . . . . 67.42(6) ?
O7 C7 O2 C2 . . . . 2.09(14) y
C8 C7 O2 C2 . . . . -177.59(7) ?
C3 C2 O2 C7 . . . . -105.42(7) ?
C1 C2 O2 C7 . . . . 135.56(7) y
O9 C11 O4 C4 . . . . 10.40(10) y
C12 C11 O4 C4 . . . . -169.32(6) ?
C3 C4 O4 C11 . . . . 102.50(6) y
C5 C4 O4 C11 . . . . -138.63(5) ?
O10 C13 O6 C6 . . . . -3.73(11) y
C14 C13 O6 C6 . . . . 175.24(6) ?
C5 C6 O6 C13 . . . . 178.14(6) y
N2 C15 N1 C21 . . . . 10.42(10) ?
S1 C15 N1 C21 . . . . -170.91(5) y
C22 C21 N1 C15 . . . . 16.38(10) y
C26 C21 N1 C15 . . . . -165.31(7) ?
N1 C15 N2 C16 . . . . -173.19(6) ?
S1 C15 N2 C16 . . . . 8.22(9) y