#------------------------------------------------------------------------------ #$Date: 2024-07-10 04:51:59 +0300 (Wed, 10 Jul 2024) $ #$Revision: 293350 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/31/2023194.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023194 loop_ _publ_author_name 'Abu-Zaied, Mamdouh A.' 'Nawwar, Galal A.' 'Elgemeie, Galal H.' 'Jones, Peter G.' _publ_section_title ; Crystal structures of four thioglycosides involving carbamimidothioate groups ; _journal_coeditor_code YZ2056 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E Crystallographic Communications' _journal_paper_doi 10.1107/S2056989024006455 _journal_volume 80 _journal_year 2024 _chemical_absolute_configuration ad _chemical_formula_iupac 'C23 H27 N3 O9 S' _chemical_formula_moiety 'C23 H27 N3 O9 S' _chemical_formula_sum 'C23 H27 N3 O9 S' _chemical_formula_weight 521.53 _chemical_name_systematic ; 2',3',4',6'-Tetra-O-acetyl-\b-D-galactopyranosyl N'-cyano-N-p-tolylcarbamimidothioate ; _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_method SHELXL-2019/3 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.42044(17) _cell_length_b 14.9634(4) _cell_length_c 22.7580(5) _cell_measurement_reflns_used 63582 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 38.4180 _cell_measurement_theta_min 2.2620 _cell_volume 2526.93(10) _computing_cell_refinement ; CrysAlisPro 1.171.42.100a (Rigaku OD, 2023) ; _computing_data_collection ; CrysAlisPro 1.171.42.100a (Rigaku OD, 2023) ; _computing_data_reduction ; CrysAlisPro 1.171.42.100a (Rigaku OD, 2023) ; _computing_molecular_graphics ; XP, Version 5.1 (Bruker, 1998) ; _computing_publication_material ; SHELXL2019/3 (Sheldrick, 2015b) ; _computing_structure_refinement ; SHELXL2019/3 (Sheldrick, 2015b) ; _computing_structure_solution ; SHELXT (Sheldrick, 2015a) ; _diffrn_ambient_temperature 99.9(9) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0849 _diffrn_reflns_av_unetI/netI 0.0329 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_limit_l_min -37 _diffrn_reflns_number 146926 _diffrn_reflns_theta_full 36.000 _diffrn_reflns_theta_max 36.316 _diffrn_reflns_theta_min 2.249 _diffrn_source 'micro-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 0.184 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.88054 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; (CrysAlisPro; Rigaku OD, 2023) ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.371 _exptl_crystal_description prism _exptl_crystal_F_000 1096 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.04 _refine_diff_density_max 0.452 _refine_diff_density_min -0.214 _refine_ls_abs_structure_details ; Flack x determined using 4554 quotients [(I^+^)-(I^-^)]/[(I^+^)+(I^-^)] (Parsons et al., 2013) ; _refine_ls_abs_structure_Flack 0.005(18) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 334 _refine_ls_number_reflns 12241 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.041 _refine_ls_R_factor_all 0.0426 _refine_ls_R_factor_gt 0.0359 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0589P)^2^+0.1217P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0911 _refine_ls_wR_factor_ref 0.0944 _reflns_number_gt 11008 _reflns_number_total 12241 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file yz2056.cif _cod_data_source_block 5d _cod_original_cell_volume 2526.94(11) _cod_database_code 2023194 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.973 _shelx_estimated_absorpt_t_max 0.993 _shelx_hkl_file ; 0 0 3 0.13993 0.26576 15 0 0 -3 0.47034 0.24378 15 0 0 -3 0.48505 0.32377 19 0 0 3 0.16361 0.27340 19 0 0 -4 60.1069 4.39154 15 0 0 4 55.8420 4.39133 15 0 0 4 57.6760 4.40972 19 0 0 -4 57.0665 4.41383 19 0 0 -5 0.07366 0.47780 15 0 0 5 0.82960 0.44378 15 0 0 5-0.08965 0.49880 19 0 0 -5 0.38684 0.52535 19 0 0 6 142.600 11.1050 15 0 0 -6 154.717 11.1030 15 0 0 6 149.618 11.1288 19 0 0 -6 141.272 11.1290 19 0 0 -7 0.35748 0.51080 15 0 0 7 0.61881 0.49506 15 0 0 -7 0.06898 0.54184 19 0 0 7 0.18583 0.61580 19 0 0 -7 0.41640 0.72144 8 0 0 8 788.881 63.1765 15 0 0 -8 799.140 63.1645 15 0 0 8 970.567 63.2311 19 0 0 -8 872.147 63.1733 18 0 0 -8 827.278 63.2650 8 0 0 -9 0.25968 0.61314 15 0 0 9 0.47188 0.69325 19 0 0 -9 0.19260 0.53157 18 0 0 -9 0.21762 0.76452 8 0 0 10 4258.72 391.495 26 0 0 -10 5486.25 391.548 18 0 0 10 5653.60 391.595 19 0 0 -10 5088.01 391.666 8 0 0 -10 6046.74 391.567 15 0 0 -10 5381.11 391.498 7 0 0 11 0.51872 0.73236 26 0 0 11-0.09522 0.79054 19 0 0 -11 0.55450 0.63938 18 0 0 -11-0.53779 0.78930 8 0 0 -11 1.33484 0.73217 15 0 0 -11 0.36211 0.52730 7 0 0 12 80.0182 6.30789 26 0 0 12 90.5174 6.40877 19 0 0 -12 76.1564 6.30281 18 0 0 -12 83.8304 6.50279 8 0 0 -12 76.9979 6.31542 15 0 0 -12 84.0380 6.26548 7 0 0 13 0.43296 0.77602 26 0 0 13 0.11154 0.77117 19 0 0 -13 0.37834 0.62181 18 0 0 -13-0.16074 0.90015 8 0 0 -13 1.01055 0.78927 15 0 0 -13-0.63114 0.58185 7 0 0 14 372.347 27.4085 26 0 0 -14 372.501 27.4342 18 0 0 14 385.785 27.4957 19 0 0 -14 345.157 27.5976 8 0 0 -14 351.646 27.4097 15 0 0 -14 358.579 27.3516 7 0 0 -15 0.21941 0.64374 18 0 0 -15 1.50081 1.00480 8 0 0 15 0.19693 0.81020 26 0 0 -15-0.31874 0.61759 7 0 0 -16 135.260 10.3915 18 0 0 -16 143.625 10.6604 8 0 0 16 134.444 10.4175 9 0 0 16 135.774 10.3674 26 0 0 -16 131.255 10.2922 7 0 0 -17 0.12476 0.73659 18 0 0 17 0.81801 0.79596 9 0 0 -17 1.07514 1.02185 8 0 0 17 0.43946 0.88114 26 0 0 -17 0.08893 0.68537 7 0 0 -18 4.75045 0.95302 18 0 0 18 4.07202 0.92271 9 0 0 -18 2.51154 1.20749 8 0 0 18 2.18706 0.98481 26 0 0 -18 1.21437 0.74149 7 0 0 19 1.23784 0.87697 9 0 0 -19-0.24170 1.12844 8 0 0 19-0.96056 1.01538 26 0 0 19 0.11346 0.71899 17 0 0 -19-0.27904 0.86711 18 0 0 -20 57.8444 4.83098 8 0 0 20 52.4975 4.51244 9 0 0 20 48.7618 4.41468 26 0 0 20 57.3125 4.38752 17 0 0 -20 53.7762 4.44230 18 0 0 -21-0.26934 1.21263 8 0 0 21-0.34652 0.92173 9 0 0 21 0.49964 0.78019 17 0 0 -21-0.61352 0.87966 18 0 0 -22 4.32374 1.10573 18 0 0 22 4.17818 0.95551 17 0 0 22 3.82756 1.13663 9 0 0 -22 2.54476 1.53216 8 0 0 -23-0.16686 0.98453 18 0 0 -23 0.78837 1.16071 19 0 0 23 1.87627 1.27334 4 0 0 23-1.08430 1.10604 15 0 0 23 0.40728 0.85227 17 0 0 23 0.76524 1.12873 9 0 0 -23-0.29580 1.35673 8 0 0 24 31.9347 2.87742 17 0 0 -24 34.4597 3.03187 18 0 0 -24 30.6865 3.27618 19 0 0 24 26.7442 3.19720 4 0 0 24 34.0133 3.21396 15 0 0 -24 35.3640 3.50621 8 0 0 24 31.6882 3.09557 9 0 0 -25-0.53655 1.07260 18 0 0 -25 0.58029 1.37842 19 0 0 25 2.36187 1.58131 4 0 0 25-0.95983 1.29385 15 0 0 25 0.87326 0.99442 17 0 0 25 1.25789 1.23699 9 0 0 -25-0.64604 1.56033 8 0 0 26 74.4687 5.68310 17 0 0 -26 63.2058 6.04590 19 0 0 -26 63.8256 5.70999 18 0 0 26 65.7927 6.07604 4 0 0 26 66.7691 5.93660 15 0 0 26 76.4871 5.89233 9 0 0 -26 74.1483 6.25696 8 0 0 -27 0.37764 1.13309 18 0 0 -27 0.95196 1.61885 19 0 0 27 1.29295 1.66109 4 0 0 27 0.52490 1.44333 15 0 0 27 0.61522 0.98040 17 0 0 -27 0.34948 1.72961 8 0 0 27 0.68213 1.23476 9 0 0 -28 17.8792 2.41957 19 0 0 -28 11.9439 1.81732 18 0 0 28 14.4817 2.32621 4 0 0 28 14.4710 1.78582 17 0 0 -28 13.3470 2.38648 8 0 0 28 14.8600 2.00797 9 0 0 -29 0.19585 1.26149 18 0 0 -29 3.44569 1.73313 19 0 0 29 1.05241 1.97819 4 0 0 29 1.75894 1.13921 17 0 0 -29 0.74352 1.70703 8 0 0 29 0.24398 1.37715 9 0 0 -30 162.326 13.1387 18 0 0 -30 155.502 13.5237 19 0 0 30 175.806 13.6870 4 0 0 30 181.230 13.0788 17 0 0 30 166.767 13.3103 9 0 0 -30 164.158 13.6625 8 0 0 -31-1.48262 1.84802 19 0 0 -31-0.59906 1.46117 18 0 0 31 0.37766 2.04939 4 0 0 31 1.63323 1.18223 17 0 0 -31-0.39418 1.95012 8 0 0 31 0.25912 1.51173 9 0 0 -32 8.43993 2.23811 19 0 0 -32 7.22417 1.51617 18 0 0 32 6.63926 2.32687 4 0 0 32 7.37094 1.44117 17 0 0 32 9.31127 1.85691 9 0 0 -32 2.82029 2.07760 8 0 0 -33-0.20063 1.33073 18 0 0 -33-1.18629 2.03139 19 0 0 33-0.40293 2.17236 4 0 0 33-0.16327 1.14252 17 0 0 33 0.27227 1.66699 9 0 0 -33-0.82200 2.04926 8 0 0 -34 13.1396 1.85408 18 0 0 -34 10.9530 2.53445 19 0 0 34 10.3488 2.54277 4 0 0 34 7.21426 2.04845 9 0 0 -34 11.3571 2.59292 8 0 0 -35-2.07786 2.13485 19 0 0 35-0.84943 2.10128 4 0 0 35-0.28212 1.65527 9 0 0 -35 2.98356 2.23665 8 0 0 -36 34.3164 4.49537 19 0 0 36 39.9886 4.68847 4 0 0 -36 56.0078 4.89585 8 0 0 36 41.6768 4.24728 9 0 0 -37-0.86119 2.25949 19 0 0 37 1.77153 2.48010 4 0 0 37-1.15041 1.77856 9 0 0 -37 0.43420 2.19785 8 0 0 -38 52.2995 5.74143 19 0 0 38 58.2312 5.34205 9 0 0 -38 64.5352 6.02084 8 0 0 39 0.28787 1.82426 9 0 -1 2 191.652 13.1177 4 0 1 2 169.358 13.1159 8 0 1 -2 179.723 13.1099 26 0 -1 2 174.405 13.1059 26 0 -1 -2 179.550 13.1012 17 0 1 2 180.039 13.1046 17 0 -1 -2 150.271 13.0912 18 0 -1 -2 144.932 13.1035 19 0 -1 -2 184.739 13.1012 15 0 1 2 183.229 13.1014 15 0 -1 2 161.901 13.1039 14 0 1 -2 159.444 13.1057 14 0 1 3 279.804 20.5208 9 0 -1 -3 261.315 20.5365 8 0 1 3 271.282 20.5371 8 0 -1 -3 273.518 20.5152 9 0 1 -3 257.837 20.5162 26 0 1 3 280.667 20.5059 18 0 1 3 265.554 20.5237 19 0 1 3 263.413 20.5084 17 0 -1 -3 289.336 20.5375 19 0 1 -3 290.986 20.5014 15 0 -1 -3 290.585 20.5126 15 0 1 3 269.250 20.5133 15 0 -1 3 268.436 20.5274 4 0 1 -3 274.098 20.5239 4 0 1 4 3.54809 0.53892 9 0 1 4 3.79983 0.67659 8 0 -1 -4 2.85898 0.60228 8 0 1 -4 4.31874 0.56606 26 0 1 4 4.26984 0.50803 18 0 1 -4 3.93009 0.58270 19 0 1 4 4.40203 0.56911 19 0 -1 -4 4.49241 0.59272 19 0 -1 -4 3.56183 0.51509 15 0 1 -4 4.22575 0.48814 15 0 1 4 3.09065 0.50505 15 0 -1 4 3.53614 0.55500 4 0 1 5 7.26771 0.89385 8 0 -1 -5 6.49988 0.86159 8 0 1 -5 5.92526 0.78726 26 0 1 5 5.58779 0.76597 19 0 -1 -5 6.16622 0.81295 19 0 1 5 6.16947 0.71064 18 0 1 -5 5.90514 0.84455 19 0 -1 5 8.59682 0.88681 19 0 1 -5 5.70851 0.75085 15 0 1 5 6.24878 0.73261 15 0 -1 -5 6.31066 0.74794 15 0 -1 5 7.62282 0.86424 4 0 1 -6 973.313 73.5012 15 0 1 6 1012.11 73.5290 15 0 -1 -6 1036.84 73.5189 15 0 1 -6 868.236 73.5320 19 0 -1 -6 1166.82 73.5816 19 0 -1 6 945.801 73.5323 19 0 1 6 1124.22 73.5606 19 0 1 6 879.660 73.4862 18 0 -1 -6 971.608 73.5803 8 0 -1 7 50.5069 4.18211 19 0 -1 -7 51.6857 4.19904 19 0 1 -7 50.0875 4.19132 19 0 1 7 51.6097 4.12615 18 0 1 7 60.1528 4.20942 19 0 -1 -7 56.6871 4.25968 8 0 -1 -7 51.7223 4.14166 15 0 1 7 55.7313 4.18024 15 0 1 -7 57.6047 4.15112 15 0 -1 7 50.8580 4.14958 26 0 -1 8 312.663 24.6542 19 0 1 8 345.937 24.6183 18 0 1 8 303.337 24.6480 19 0 -1 -8 321.526 24.6198 18 0 -1 -8 342.763 24.6962 19 0 -1 -8 365.516 24.7527 8 0 -1 -8 320.363 24.6261 15 0 1 8 338.125 24.6559 15 0 1 -8 299.567 24.6056 15 0 -1 8 357.188 24.6399 26 0 -1 9 70.0827 5.69440 26 0 1 9 83.4774 5.77383 19 0 1 9 64.2942 5.66221 18 0 -1 -9 75.0787 5.69132 18 0 1 -9 71.0937 5.69825 18 0 -1 9 77.6210 5.76582 19 0 -1 -9 70.6857 5.80127 8 0 1 9 82.2066 5.75147 15 0 1 -9 71.6290 5.68678 15 0 -1 -9 82.8200 5.72084 15 0 1 -9 70.9225 5.66571 7 0 -1 10 13.7863 1.60461 26 0 -1 -10 18.0187 1.77130 8 0 1 10 18.5645 1.71359 19 0 1 10 16.9145 1.56634 18 0 1 -10 17.1553 1.60871 18 0 -1 10 18.5591 1.73183 19 0 -1 -10 13.1306 1.53381 18 0 1 -10 17.8569 1.61056 15 0 -1 -10 20.5367 1.65953 15 0 1 10 20.1931 1.66649 15 0 1 -10 19.4134 1.58442 7 0 -1 11 459.978 33.0653 26 0 -1 11 446.150 32.9242 21 0 -1 -11 430.690 33.2009 8 0 -1 11 419.993 33.0991 19 0 1 11 386.555 33.0749 19 0 -1 -11 469.256 33.0750 18 0 1 -11 467.236 33.0850 18 0 1 11 436.074 33.1040 15 0 -1 -11 418.995 33.0583 15 0 1 -11 479.426 33.0711 15 0 -1 -11 425.770 32.9875 7 0 1 -11 444.920 33.0311 7 0 -1 12 50.8944 4.30464 26 0 -1 12 57.6086 4.13532 21 0 1 12 52.7467 4.33829 9 0 -1 -12 48.1805 4.45550 8 0 -1 -12 47.7536 4.27900 18 0 1 12 46.6195 4.33909 19 0 1 -12 56.4909 4.33448 18 0 -1 12 49.6795 4.35918 19 0 1 12 55.4963 4.36313 15 0 1 -12 55.8877 4.31480 15 0 -1 -12 61.5124 4.35516 15 0 -1 -12 53.4683 4.22642 7 0 1 -12 60.9466 4.29200 7 0 -1 13 15.0466 1.47213 26 0 -1 13 13.2062 1.13134 21 0 1 13 12.6354 1.39167 9 0 -1 -13 11.9209 1.58986 8 0 -1 -13 14.1938 1.37872 18 0 1 13 13.8753 1.50163 19 0 1 -13 14.2281 1.40148 18 0 -1 13 15.8844 1.56251 19 0 1 -13 12.0970 1.38468 15 0 1 13 12.2692 1.42467 15 0 -1 -13 14.1106 1.42268 15 0 1 -13 13.5468 1.33231 7 0 -1 -13 15.0924 1.31000 7 0 -1 14 12.9449 1.33766 26 0 -1 14 11.1914 0.98046 21 0 -1 14 16.1544 1.50505 19 0 1 -14 9.68170 1.25625 18 0 -1 -14 10.5344 1.26373 18 0 1 14 10.8995 1.35432 19 0 -1 -14 9.73456 1.48641 8 0 1 14 12.9709 1.35297 9 0 1 -14 10.4948 1.49643 8 0 1 -14 12.5068 1.31573 15 0 -1 -14 11.2878 1.30579 15 0 1 -14 12.7610 1.22937 7 0 -1 -14 12.4626 1.17057 7 0 -1 15 130.171 9.88859 26 0 -1 -15 131.741 9.89652 18 0 1 -15 127.854 9.89481 18 0 1 15 123.404 9.92355 9 0 1 -15 130.248 10.1227 8 0 -1 -15 116.985 10.0716 8 0 1 -15 129.032 9.88258 15 0 1 -15 132.165 9.83685 7 0 -1 -15 130.297 9.79214 7 0 -1 -16 15.4355 1.76220 8 0 1 16 18.8422 1.59748 9 0 1 -16 15.6044 1.75742 8 0 -1 16 12.6482 1.50176 26 0 1 16 14.1253 1.49226 26 0 1 -16 11.5185 1.37702 7 0 -1 -16 14.0761 1.34745 7 0 -1 -16 13.9395 1.48747 18 0 1 16 11.3549 1.36490 17 0 1 -16 12.1577 1.43096 18 0 1 17 46.9212 4.29718 9 0 -1 -17 60.8785 4.61487 8 0 1 -17 46.4421 4.49618 8 0 -1 -17 48.3174 4.23462 18 0 1 17 59.5950 4.25514 17 0 1 -17 52.4993 4.27493 18 0 1 17 46.4747 4.21949 26 0 -1 17 56.2669 4.28134 26 0 1 -17 55.0910 4.20869 7 0 -1 -17 51.2178 4.14611 7 0 1 18 75.8933 6.70139 26 0 -1 18 82.5952 6.71934 26 0 1 18 82.3113 6.79063 9 0 -1 -18 87.2252 7.02966 8 0 1 -18 80.0664 6.99699 8 0 -1 18 99.6115 7.04273 4 0 -1 -18 93.5372 6.77961 18 0 1 -18 85.5929 6.76286 18 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6 42.3669 3.49112 16 0 -7 6 40.4544 3.55996 14 0 -7 6 44.3973 3.60789 12 0 7 -6 47.3418 3.66724 14 0 -7 -6 39.3988 3.51080 13 0 7 -6 38.1531 3.50296 11 0 -7 -7 178.006 13.1595 7 0 7 -7 174.406 13.4155 4 0 7 -7 187.203 13.4023 5 0 7 -7 164.833 13.3413 7 0 -7 7 164.621 13.3831 26 0 7 -7 176.976 13.4782 26 0 -7 7 179.483 13.3484 25 0 7 7 184.222 13.2511 23 0 -7 -7 177.731 13.3687 21 0 -7 7 175.328 13.2837 24 0 7 7 179.693 13.4565 9 0 7 7 175.825 13.4540 8 0 7 7 180.804 13.3875 18 0 -7 -7 153.486 13.3687 18 0 -7 -7 176.277 13.3995 17 0 -7 7 186.598 13.2793 15 0 7 7 183.507 13.4579 17 0 -7 7 168.740 13.3063 16 0 -7 7 157.818 13.3739 14 0 -7 -7 188.794 13.3415 15 0 7 -7 187.600 13.3863 11 0 -7 7 179.510 13.4477 12 0 7 -7 172.637 13.4554 14 0 -7 -7 156.838 13.3550 13 0 7 -8 200.416 17.3351 7 0 7 -8 217.642 17.4129 4 0 7 -8 224.194 17.3987 5 0 -7 -8 225.702 17.4123 3 0 -7 8 219.723 17.3992 3 0 -7 8 239.354 17.4230 26 0 7 -8 227.834 17.4921 26 0 -7 8 215.461 17.3443 25 0 7 -8 248.875 17.2775 24 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1.43627 0.79232 5 0 11 -6 2.56186 1.15674 26 0 11 6 2.05270 0.89419 26 0 11 -6 1.59089 0.84152 25 0 -11 6 1.58947 0.71013 24 0 11 6 1.16941 0.48553 22 0 -11 -6 2.06148 0.93388 21 0 11 6 1.58846 0.68800 23 0 -11 6 1.60911 0.97228 3 0 -11 -6 1.46735 0.96422 3 0 -11 6 2.70781 0.80918 9 0 -11 6 3.17334 0.90843 11 0 -11 -6 0.89346 0.66210 10 0 11 6 2.21997 0.98193 9 0 11 -6 1.57029 0.78460 10 0 -11 6 1.51739 0.54688 15 0 -11 -6 1.54264 0.71458 15 0 11 -6 1.49633 0.86755 16 0 -11 6 1.97861 0.83452 17 0 11 -6 3.10297 1.01134 14 0 -11 -6 1.85063 0.79858 11 0 11 6 1.49487 0.75304 12 0 11 -6 1.40757 0.82416 11 0 -11 6 2.46842 0.84719 12 0 11 -7 29.1166 2.80998 5 0 -11 -7 32.5628 2.78310 5 0 11 -7 31.3932 3.02454 26 0 11 -7 30.1865 2.73749 25 0 11 7 25.9598 2.85515 26 0 -11 7 29.8157 2.73274 24 0 11 7 32.4837 2.53109 22 0 -11 -7 28.9685 2.87447 21 0 11 7 32.5223 2.67250 23 0 -11 -7 39.3427 3.06875 3 0 -11 7 30.1177 2.97853 3 0 11 7 36.6118 2.99450 9 0 -11 7 38.9423 2.91583 11 0 -11 7 31.6838 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0 -11 9 80.9549 6.87530 25 0 -11 9 76.6660 6.81505 24 0 -11 -9 81.6803 6.97916 21 0 11 9 93.4941 6.79479 23 0 -11 9 102.267 7.14866 3 0 -11 -9 76.8232 7.04576 3 0 11 9 93.1977 7.13357 9 0 -11 9 85.7701 6.86934 9 0 -11 9 82.0921 6.84902 17 0 11 9 88.2155 7.10766 17 0 -11 9 82.5941 6.74958 15 0 -11 9 88.3114 7.07002 12 0 11 -9 87.7229 7.14594 14 0 11 9 96.9803 6.90681 12 0 -11 -9 91.2858 7.00427 11 0 -11 -10 6.97721 1.67798 6 0 11 -10 9.52127 1.45239 5 0 -11 10 11.9236 1.72123 6 0 11 10 14.5639 1.68982 26 0 -11 10 14.4817 1.50472 25 0 11 -10 13.1643 1.78943 26 0 -11 -10 12.6180 1.55954 21 0 11 10 13.2433 1.28635 23 0 -11 10 12.6713 1.34062 24 0 -11 10 15.2468 1.72622 3 0 -11 -10 15.4851 1.78835 3 0 -11 10 12.9480 1.44598 9 0 11 10 12.4569 1.66877 9 0 -11 10 14.8139 1.29588 15 0 11 10 12.9073 1.68258 17 0 -11 10 14.7308 1.48381 17 0 -11 -10 9.71307 1.45961 11 0 -11 10 11.0676 1.65791 12 0 11 10 12.3448 1.48228 12 0 11 -10 13.2863 1.80029 14 0 -11 -10 12.6343 1.54454 13 0 11 -11 103.169 7.68120 5 0 -11 -11 78.9632 7.72200 6 0 -11 11 52.7421 7.57217 6 0 11 11 97.4202 7.71693 26 0 11 -11 105.461 7.88867 26 0 -11 11 100.834 7.56561 25 0 11 11 104.351 7.39026 23 0 -11 -11 102.789 7.63620 21 0 -11 -11 111.756 7.79154 3 0 -11 11 89.4802 7.66861 3 0 -11 11 97.7920 7.51165 9 0 11 11 98.3378 7.79486 9 0 11 11 93.3871 7.76372 17 0 -11 11 102.838 7.49812 17 0 -11 11 94.5239 7.41568 15 0 -11 11 92.8252 7.75694 12 0 11 -11 86.7249 7.75406 14 0 11 11 113.808 7.58147 12 0 -11 -11 98.3143 7.63923 13 0 -11 -12 349.092 22.9844 6 0 -11 12 336.757 22.9194 6 0 11 -12 295.882 22.7671 5 0 11 12 298.586 22.7858 26 0 11 -12 301.141 22.9406 26 0 -11 12 289.262 22.6464 25 0 -11 12 236.330 22.7362 21 0 -11 -12 315.969 22.6987 21 0 -11 12 294.794 22.7667 3 0 -11 -12 322.948 22.8394 3 0 -11 12 306.014 22.6007 9 0 11 12 291.749 22.8659 9 0 -11 12 290.165 22.5213 15 0 11 12 295.606 22.8676 17 0 -11 12 296.467 22.5601 17 0 -11 12 309.401 22.8980 12 0 11 -12 265.587 22.8359 14 0 -11 -12 327.613 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249.325 20.0980 26 0 12 -6 268.206 19.9049 25 0 -12 6 242.430 19.9253 24 0 -12 -6 301.357 20.1687 21 0 12 6 282.513 19.8769 23 0 12 6 257.788 19.7525 22 0 -12 -6 239.984 20.1258 3 0 -12 6 231.091 20.0858 3 0 -12 -6 277.793 19.8979 10 0 12 -6 271.820 19.9195 10 0 12 6 252.305 20.0986 9 0 -12 6 259.863 19.9009 9 0 -12 6 264.163 19.9912 11 0 12 -6 262.830 20.1655 14 0 12 -6 252.895 20.0483 16 0 -12 -6 266.411 19.8534 15 0 -12 6 262.531 19.7792 15 0 -12 -6 269.524 20.0124 11 0 -12 6 268.366 20.0438 12 0 12 6 271.232 19.8865 12 0 -12 -7 10.8809 1.48821 5 0 -12 7 21.4112 2.07820 6 0 12 -7 11.8738 1.52682 5 0 12 -7 14.9226 1.53647 25 0 12 -7 14.2139 1.89386 26 0 12 7 12.1378 1.66593 26 0 12 7 13.3621 1.19508 22 0 -12 7 12.9179 1.47949 24 0 -12 -7 12.1677 1.65785 21 0 12 7 14.1621 1.37678 23 0 -12 7 14.8224 1.79340 3 0 -12 -7 11.5653 1.73445 3 0 -12 7 13.7559 1.48630 9 0 -12 7 15.0736 1.60192 11 0 -12 -7 13.9535 1.44150 10 0 12 -7 12.6449 1.52486 10 0 12 7 13.8806 1.73811 9 0 12 -7 10.7615 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-8 254.074 18.4708 11 1 4 -7 79.3546 6.06684 5 1 4 -7 81.7085 6.07295 4 1 4 -7 74.9225 6.00244 7 1 -4 7 102.387 6.07492 6 -1 4 7 95.1893 6.00656 2 1 -4 7 85.4522 5.99578 3 1 4 -7 73.7344 6.11349 26 1 -4 7 70.5195 5.96094 26 1 -4 7 53.8817 5.96214 21 -1 4 7 75.0449 5.93538 21 -1 -4 -7 81.3635 5.93861 22 -1 -4 -7 83.4300 6.07947 8 -1 -4 -7 76.0050 6.01634 9 -1 4 7 74.8309 6.09183 8 -1 4 7 74.6248 6.04839 9 -1 -4 -7 76.7220 6.00085 17 -1 4 7 81.0487 6.05707 17 -1 4 7 81.6478 5.95693 18 -1 4 7 74.3584 6.03013 19 1 -4 7 79.6728 5.91972 15 1 -4 7 75.9678 5.85091 17 -1 4 7 78.2211 5.99623 15 1 -4 7 75.0863 5.98623 14 1 -4 7 71.6000 6.08214 12 1 4 -7 80.3082 6.12154 14 1 4 -7 80.0332 6.04428 11 1 4 -6 126.180 8.48279 5 1 4 -6 136.157 8.43605 7 1 4 -6 108.061 8.44279 4 1 -4 6 113.805 8.39952 3 -1 4 6 107.222 8.38011 3 1 4 -6 115.406 8.51173 26 1 -4 6 103.581 8.36927 26 1 -4 6 86.1382 8.37462 21 -1 -4 -6 122.049 8.34599 22 -1 4 6 122.752 8.36983 21 -1 4 6 114.247 8.44165 9 -1 4 6 115.190 8.48926 8 -1 -4 -6 121.967 8.46904 8 -1 -4 -6 116.698 8.42674 9 -1 4 6 127.295 8.37228 18 -1 4 6 114.099 8.44716 17 1 -4 6 111.155 8.26748 17 -1 4 6 107.607 8.37646 15 1 -4 6 124.093 8.39450 14 -1 -4 -6 115.212 8.40898 17 1 -4 6 115.533 8.30691 15 1 4 -6 119.160 8.44067 11 1 4 -6 117.334 8.51310 14 1 -4 6 103.424 8.46917 12 1 4 -5 1816.85 132.050 5 1 4 -5 2151.65 132.036 7 1 4 -5 2045.78 132.070 4 -1 4 5 1655.74 131.983 3 1 -4 5 1395.53 131.973 3 1 4 -5 1789.58 132.088 26 1 -4 5 1539.56 131.970 26 -1 -4 -5 1754.95 131.950 22 -1 4 5 1719.59 131.979 23 -1 4 5 1771.61 131.974 21 -1 -4 -5 1843.81 132.023 9 -1 4 5 1754.34 132.025 9 -1 4 5 1781.40 132.055 8 -1 4 5 1789.92 131.965 18 -1 -4 -5 1395.75 132.000 18 -1 4 5 1688.08 132.022 17 1 -4 5 1740.87 131.970 14 -1 -4 -5 1833.88 132.011 17 1 -4 5 1816.12 131.899 17 1 -4 5 1731.34 131.899 15 -1 4 5 1903.81 131.984 15 1 4 -5 1596.70 132.008 11 1 4 -5 1991.09 132.107 14 1 4 -4 16.5846 1.23042 7 1 4 -4 13.8100 1.29962 4 1 4 -4 11.7399 1.23097 5 1 -4 4 17.7041 1.27201 3 -1 4 4 15.9584 1.25423 3 1 4 -4 13.9287 1.34039 26 1 -4 4 16.1055 1.20996 24 -1 4 4 12.3140 1.17519 21 1 -4 4 13.4976 1.25952 21 -1 -4 -4 12.8462 1.12397 22 -1 4 4 10.8839 1.17501 23 1 -4 4 12.1943 1.02599 9 -1 4 4 12.7763 1.28513 8 -1 4 4 13.6433 1.23903 9 -1 -4 -4 13.1574 1.25048 9 -1 4 4 10.2256 1.13552 18 1 -4 4 12.6183 1.05372 17 -1 4 4 11.6013 1.22671 17 -1 -4 -4 14.5277 1.24250 18 -1 4 4 12.0956 1.11333 15 1 -4 4 11.9118 1.00939 15 -1 -4 -4 11.1712 1.21841 17 1 -4 4 11.4788 1.13120 14 1 4 -4 10.0876 1.26573 14 1 4 -4 11.4729 1.23384 11 1 4 -3 228.626 19.3733 4 1 4 -3 287.415 19.3578 7 1 4 -3 239.595 19.3738 5 1 -4 3 225.831 19.3589 3 -1 4 3 238.806 19.3534 3 1 4 -3 243.280 19.4110 26 1 -4 3 281.059 19.3745 24 -1 -4 -3 266.076 19.3313 26 -1 -4 -3 278.127 19.3216 22 -1 4 3 248.760 19.3417 21 -1 4 3 273.497 19.3493 23 1 -4 3 343.179 19.4482 21 -1 -4 -3 256.450 19.3660 9 -1 4 3 273.030 19.3650 9 -1 4 3 254.880 19.3787 8 1 -4 3 255.691 19.2567 9 -1 -4 -3 291.196 19.4049 18 1 -4 3 251.518 19.2780 17 -1 4 3 274.586 19.3787 17 1 4 -3 241.646 19.4070 14 1 4 -3 242.257 19.3898 16 1 -4 3 242.363 19.3106 14 -1 4 3 253.458 19.2937 15 -1 -4 -3 244.469 19.3545 17 1 4 -3 246.679 19.3657 11 1 4 -2 12.6451 1.17733 5 1 4 -2 13.9152 1.21240 4 -1 4 2 13.3144 1.18185 3 1 -4 2 11.5700 1.16245 3 1 -4 2 10.9099 1.11698 24 1 4 -2 10.3874 1.18948 26 -1 -4 -2 11.5636 1.08753 26 -1 4 2 8.94331 1.10965 21 1 -4 2 8.96188 1.12251 21 1 -4 2 11.4162 0.98011 9 -1 4 2 13.1227 1.09099 9 -1 -4 -2 12.6792 1.14514 9 -1 4 2 11.7388 1.16615 8 -1 -4 -2 12.8265 1.14840 18 -1 4 2 12.9099 1.12506 17 1 -4 2 11.6511 1.03101 17 1 4 -2 9.78800 1.15271 14 -1 4 2 11.4082 0.98228 15 1 4 -2 11.6873 1.19188 16 1 4 -2 12.5034 1.15420 11 -1 4 2 11.3555 1.15718 12 1 4 -1 1572.85 116.308 5 1 -4 1 1096.13 116.281 6 -1 4 1 1375.20 116.297 6 -1 4 1 1287.54 116.266 3 1 -4 1 1173.74 116.276 3 -1 -4 -1 1575.99 116.274 26 -1 4 1 1713.52 116.314 25 1 -4 1 1572.95 116.300 24 1 4 -1 2017.09 116.300 22 -1 4 1 2172.74 116.345 21 1 -4 1 1623.44 116.196 11 -1 -4 -1 1627.20 116.296 9 -1 4 1 1581.56 116.281 8 -1 4 1 1534.70 116.249 9 1 -4 1 1541.75 116.291 10 1 -4 1 1474.46 116.209 9 -1 -4 -1 1655.92 116.307 18 -1 4 1 1840.95 116.296 17 1 -4 1 1317.85 116.223 17 -1 -4 -1 1634.27 116.301 16 1 4 -1 1533.79 116.318 16 -1 4 1 1491.65 116.185 15 1 4 -1 1645.39 116.340 14 -1 4 1 1471.86 116.286 12 1 4 -1 1651.14 116.303 11 1 -4 0 361.349 30.6420 6 1 4 0 437.909 30.6402 5 -1 4 0 494.700 30.6874 6 1 -4 0 343.266 30.6076 3 -1 4 0 364.723 30.6002 3 -1 -4 0 415.441 30.6076 26 1 -4 0 428.477 30.6358 24 -1 4 0 497.966 30.6546 25 -1 4 0 517.581 30.6531 21 1 -4 0 330.288 30.5987 21 1 4 0 421.878 30.5844 22 -1 4 0 387.155 30.5503 9 -1 -4 0 404.649 30.6126 9 1 -4 0 359.529 30.5993 10 1 -4 0 431.001 30.5566 9 -1 4 0 391.589 30.5767 17 -1 -4 0 325.560 30.5847 18 1 4 0 449.071 30.6563 16 1 4 0 430.320 30.6606 14 -1 -4 0 427.997 30.6249 16 1 4 0 429.227 30.6212 11 -1 4 0 406.913 30.5073 11 -1 4 0 408.846 30.6210 12 1 -4 0 431.706 30.5097 11 1 -4 -1 1449.63 115.127 6 -1 4 -1 1621.71 114.976 5 -1 4 -1 2003.21 115.171 6 1 -4 -1 1566.22 114.978 5 -1 4 -1 1316.77 115.068 3 1 -4 -1 1327.06 115.083 3 -1 -4 1 1529.67 115.090 26 -1 4 -1 1632.80 115.102 25 -1 4 -1 1352.83 115.072 26 1 -4 -1 1771.02 115.126 24 1 4 1 1751.75 115.061 22 -1 4 -1 1626.61 115.094 21 1 -4 -1 1540.24 115.037 9 -1 4 -1 1506.99 115.012 9 1 -4 -1 1494.78 115.091 10 1 4 1 1534.61 115.106 9 1 4 1 1541.40 115.080 18 1 4 1 1655.61 115.124 16 1 -4 -1 1443.78 114.976 15 -1 4 -1 1415.15 115.032 17 1 -4 -1 1518.20 114.979 11 1 4 1 1467.01 115.080 11 -1 4 -1 1598.78 114.993 11 -1 4 -1 1679.59 115.106 12 -1 4 -2 11.3481 0.92566 5 1 -4 -2 7.37003 1.15077 6 -1 4 -2 12.1677 1.05544 4 -1 4 -2 5.34951 1.13855 6 -1 4 -2 11.9411 1.14933 25 -1 4 -2 12.6305 1.09852 26 1 -4 -2 8.65174 1.11704 24 -1 -4 2 12.9589 1.18032 26 1 4 2 12.4853 1.04698 22 1 -4 -2 12.6842 1.07372 23 -1 4 -2 8.84106 1.09562 21 -1 4 -2 11.2385 0.95192 9 1 4 2 9.89318 1.10510 9 1 4 2 12.5219 1.12964 18 1 -4 -2 10.9200 0.95359 15 1 4 2 10.8409 1.14436 16 -1 4 -2 11.9365 1.02345 14 -1 -4 2 11.8900 1.15438 14 -1 4 -2 11.2097 0.98213 17 -1 4 -2 11.7160 0.96025 11 -1 4 -2 12.2980 1.16023 12 -1 -4 3 232.477 18.5729 7 1 -4 -3 150.422 18.5620 6 -1 4 -3 257.903 18.5700 4 -1 4 -3 182.003 18.5678 6 -1 -4 3 252.667 18.6211 26 -1 4 -3 207.468 18.5795 25 1 -4 -3 183.187 18.5753 24 -1 4 -3 285.928 18.6141 26 1 4 3 261.443 18.5478 22 1 -4 -3 260.915 18.5776 23 1 4 3 255.984 18.6220 9 1 4 3 303.944 18.6407 18 -1 -4 3 228.542 18.6047 14 -1 4 -3 260.855 18.5587 14 1 4 3 239.261 18.6124 16 1 -4 -3 293.223 18.5358 15 -1 4 -3 259.472 18.5176 17 1 -4 -3 331.008 18.6928 13 -1 4 -3 251.640 18.6169 12 -1 4 -3 269.273 18.5278 11 -1 -4 3 265.097 18.6293 11 -1 4 -4 12.3910 1.18363 4 -1 -4 4 11.2104 1.17283 7 1 -4 -4 17.3628 1.32740 6 -1 -4 4 14.1929 1.28078 4 -1 4 -4 11.6402 1.16399 26 -1 4 -4 10.2434 1.16575 24 -1 4 -4 12.4105 1.28400 25 1 4 4 12.0643 1.13589 26 -1 -4 4 12.6095 1.02543 25 -1 -4 4 12.5186 1.29107 26 1 4 4 11.7827 1.11617 22 1 -4 -4 13.0862 1.15466 23 -1 4 -4 13.2677 1.12315 11 1 4 4 13.3207 1.23661 9 1 4 4 11.9327 1.23466 18 -1 -4 4 11.7864 1.26022 14 -1 4 -4 13.4982 1.00742 15 -1 4 -4 12.3033 1.05421 16 1 -4 -4 10.6053 1.11363 15 -1 4 -4 13.0240 1.15611 14 -1 -4 4 11.8472 1.24107 11 1 -4 -4 12.8606 1.27689 13 -1 -4 5 1908.63 134.574 4 -1 4 -5 1703.22 134.481 4 -1 -4 5 2044.31 134.529 7 1 -4 -5 1744.57 134.527 6 -1 4 -5 2252.75 134.521 3 -1 -4 5 1820.25 134.406 25 -1 4 -5 1465.23 134.446 24 1 4 5 1802.39 134.459 26 -1 -4 5 1734.90 134.528 26 -1 4 -5 1737.57 134.518 25 -1 4 -5 1749.47 134.498 26 1 -4 -5 1768.62 134.471 23 1 4 5 1769.34 134.531 9 1 4 5 1973.48 134.535 18 -1 -4 5 1737.04 134.527 14 -1 4 -5 1901.31 134.392 15 -1 4 -5 1808.75 134.400 16 1 -4 -5 1796.35 134.456 15 -1 -4 5 1837.29 134.513 16 -1 -4 5 1716.54 134.525 11 1 -4 -5 1526.30 134.523 13 -1 4 -5 1922.53 134.489 14 1 -4 -6 119.544 8.98307 3 -1 4 -6 141.223 8.99391 3 -1 4 -6 111.522 8.97725 26 1 4 6 108.562 8.92569 26 -1 4 -6 127.261 8.96525 24 1 -4 -6 116.723 8.94635 20 1 -4 -6 125.177 8.95891 23 1 -4 -6 106.486 9.04086 8 1 4 6 110.638 9.01683 9 -1 -4 6 106.568 9.00495 11 1 4 6 130.163 9.03233 18 1 -4 -6 126.457 8.96014 15 -1 -4 6 102.325 9.00879 14 -1 4 -6 109.506 8.87214 15 -1 -4 6 119.083 9.00787 16 -1 -4 6 114.778 9.05334 4 1 -4 -6 145.047 9.06115 6 -1 4 -6 105.182 8.96625 4 -1 -4 6 136.479 9.03080 7 1 -4 -7 84.0215 6.14341 3 -1 4 -7 85.0143 6.12609 3 -1 4 -7 75.2055 6.10503 2 -1 4 -7 84.5273 6.11469 1 -1 4 -7 84.1953 6.16394 26 1 -4 -7 79.8522 6.09659 20 -1 4 -7 95.3797 6.14558 24 1 -4 -7 86.8857 6.12916 23 1 -4 -7 79.5083 6.24832 8 1 4 7 75.1677 6.16816 18 1 -4 -7 82.9226 6.10805 18 -1 -4 7 65.7699 6.12566 15 1 -4 -7 81.5594 6.12975 15 -1 4 -7 72.9234 6.04219 15 1 -4 -7 69.8535 6.15154 6 -1 -4 7 72.4543 6.15509 7 -1 -4 7 85.8406 6.25827 4 -1 4 -7 80.9299 6.16751 4 1 -4 -8 247.308 18.0871 3 -1 4 -8 203.330 18.0404 2 -1 4 -8 263.166 18.0700 1 -1 4 -8 255.668 18.1308 26 1 -4 -8 220.981 18.0619 23 -1 4 -8 243.723 18.0725 24 1 -4 -8 245.264 18.0502 20 1 4 8 213.854 18.1347 8 1 -4 -8 239.772 18.2232 8 1 -4 -8 258.015 18.0734 18 1 4 8 199.173 18.1069 18 -1 -4 8 238.261 18.1166 15 1 -4 -8 248.942 18.1006 15 -1 4 -8 229.770 18.0211 15 -1 -4 8 274.431 18.2427 4 -1 -4 8 280.856 18.1695 7 1 -4 -8 265.165 18.1407 6 -1 4 -9 83.6254 6.13291 1 1 -4 -9 82.1009 6.15987 3 -1 4 -9 71.3045 6.12014 2 -1 4 -9 83.1730 6.21543 26 -1 4 -9 61.8539 6.11615 24 1 -4 -9 85.2708 6.11932 20 1 -4 -9 79.9441 6.01034 22 1 -4 -9 83.0912 6.16146 23 1 4 9 73.8282 6.25250 8 1 -4 -9 75.5445 6.32803 8 1 -4 -9 76.5238 6.13654 18 1 4 9 85.0623 6.25367 18 1 4 9 84.1007 6.27729 19 -1 4 -9 87.7564 6.13151 15 -1 -4 9 77.7503 6.20413 15 1 4 9 82.8036 6.23499 17 1 -4 -9 79.7107 6.19477 15 -1 -4 9 88.4292 6.25476 7 1 -4 -9 84.1171 6.20059 6 -1 -4 9 84.6350 6.32485 4 -1 4 -10 93.2432 6.76405 2 -1 4 -10 90.1081 6.74700 1 1 -4 -10 92.4643 6.78145 3 -1 -4 10 90.4029 6.91477 26 -1 4 -10 85.6215 6.85033 26 1 -4 -10 87.1076 6.64985 22 1 -4 -10 80.8357 6.78013 23 -1 4 -10 66.2176 6.74452 24 1 -4 -10 90.2148 6.72782 20 1 -4 -10 93.4727 7.01647 8 1 4 10 86.0500 6.91828 8 -1 4 -10 87.2610 6.94546 19 1 -4 -10 92.4632 6.78481 18 1 4 10 89.6825 6.90769 19 1 4 10 95.1813 6.89239 18 1 4 10 91.9628 6.86300 17 -1 -4 10 101.946 6.88338 15 1 -4 -10 89.8543 6.83912 15 -1 4 -10 92.5271 6.76742 15 -1 -4 10 84.6711 6.94432 4 -1 -4 10 90.3272 6.86955 7 -1 4 -11 32.8286 2.70382 2 1 -4 -11 34.2298 2.72449 3 -1 4 -11 35.9478 2.70137 1 -1 4 -11 32.7010 2.82658 26 -1 -4 11 34.8188 2.92520 26 1 -4 -11 31.5925 2.75001 23 1 4 11 35.0121 2.94670 8 1 -4 -11 33.1730 2.98947 8 1 4 11 31.2369 2.86816 19 -1 4 -11 30.4266 2.91139 19 1 4 11 43.0774 2.92259 18 1 -4 -11 32.7998 2.73059 18 -1 -4 11 39.5381 2.87166 15 -1 4 -11 30.7993 2.72901 15 1 -4 -11 32.1566 2.81524 15 1 4 11 31.7167 2.82333 17 -1 -4 11 35.8183 2.97433 4 1 -4 -12 297.329 22.1750 3 -1 4 -12 311.761 22.1524 1 -1 4 -12 310.073 22.1658 2 -1 -4 12 293.102 22.3212 26 -1 4 -12 292.394 22.2817 26 1 -4 -12 309.637 22.2308 23 1 4 12 254.395 22.3157 8 1 -4 -12 290.730 22.4532 8 1 4 12 299.501 22.3396 19 1 -4 -12 289.450 22.2015 18 1 4 12 308.425 22.3054 18 -1 4 -12 255.045 22.3496 19 -1 -4 12 285.786 22.2771 15 1 4 12 298.943 22.2923 17 -1 4 -12 297.708 22.2039 15 -1 -4 12 290.244 22.3954 4 -1 4 -13 60.9867 5.10324 1 1 -4 -13 66.0672 5.13955 3 -1 4 -13 66.8560 5.12914 2 -1 4 -13 67.9622 5.30001 26 -1 -4 13 71.6657 5.36983 26 1 -4 -13 70.3380 5.22450 23 1 -4 -13 69.5253 5.49546 8 1 4 13 65.8727 5.33828 9 1 4 13 67.5000 5.39968 8 -1 4 -13 59.0411 5.38333 19 1 4 13 65.0951 5.30017 18 1 -4 -13 61.7925 5.17872 18 1 4 13 75.4918 5.32548 17 -1 4 -13 72.4188 5.22640 15 -1 -4 13 71.8919 5.32721 15 1 -4 -13 65.6244 5.06300 7 -1 -4 13 63.7519 5.42302 4 1 -4 -14 114.776 8.54453 3 -1 4 -14 108.764 8.53193 2 -1 4 -14 119.455 8.52284 1 -1 -4 14 115.522 8.76339 26 -1 4 -14 113.960 8.70865 26 1 -4 -14 107.046 8.62324 23 1 -4 -14 108.111 8.61131 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298.864 25.9480 2 -2 2 0 395.580 25.9915 25 2 -2 0 400.581 26.0133 25 -2 -2 0 337.506 25.9289 26 2 2 0 347.995 25.8889 25 -2 2 0 344.619 25.9494 24 -2 2 0 405.312 25.9807 20 2 -2 0 303.763 25.9591 23 -2 2 0 311.294 25.9517 23 2 -2 0 218.465 25.8979 24 2 -2 0 467.017 26.0198 20 2 2 0 372.819 25.9608 22 -2 -2 0 301.454 25.9371 22 2 -2 0 353.365 25.8637 8 2 2 0 298.952 25.8714 10 2 -2 0 354.929 25.9883 10 -2 2 0 359.875 25.8736 8 -2 -2 0 243.981 25.8855 18 -2 -2 0 358.461 25.9719 16 -2 2 0 355.247 25.9741 12 -2 -2 0 357.470 25.8913 13 -2 2 0 357.991 25.8426 11 -2 -2 0 360.419 25.8764 12 2 -2 0 353.428 25.9877 12 -2 -2 0 379.240 25.9786 11 -2 2 -1 195.955 14.5859 5 2 -2 -1 190.370 14.5891 5 2 2 1 195.537 14.7075 5 -2 -2 1 208.389 14.6997 5 2 -2 -1 225.401 14.7296 3 -2 2 -1 165.599 14.6652 3 -2 2 -1 156.089 14.6510 1 -2 2 -1 237.096 14.7468 2 2 -2 -1 187.926 14.6958 1 2 -2 -1 260.705 14.7834 2 -2 2 -1 200.362 14.6893 24 -2 -2 1 195.754 14.6881 26 2 -2 -1 184.997 14.7032 25 2 2 1 192.543 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26.9111 2.24837 2 -2 2 -6 26.3109 2.19236 3 2 -2 -6 31.9407 2.23986 1 2 2 6 24.7916 2.04910 26 -2 -2 6 31.9253 2.39352 26 -2 2 -6 27.1153 2.10903 26 -2 -2 6 23.7202 2.06160 24 2 -2 -6 25.3910 2.31368 23 2 -2 -6 28.2605 2.14844 22 2 2 6 29.7314 2.12596 23 -2 2 -6 32.4007 2.27376 23 -2 -2 6 28.2083 2.26550 11 2 2 6 24.8425 2.21538 9 2 -2 -6 26.3111 2.15531 11 2 2 6 25.4394 2.18381 8 2 2 6 27.5683 2.24619 19 2 2 6 27.9517 2.30635 18 -2 2 -6 27.8847 2.29029 19 2 2 6 22.7908 2.19372 16 -2 -2 6 25.8938 2.27488 15 2 2 6 25.7268 2.18584 12 -2 -2 6 27.5629 2.30539 14 -2 -2 7 352.500 26.2397 4 -2 -2 7 354.667 26.2000 7 -2 2 -7 396.605 26.1734 1 -2 2 -7 291.992 26.1568 2 2 -2 -7 366.902 26.1750 1 -2 2 -7 379.405 26.1710 3 2 -2 -7 354.243 26.1823 2 -2 2 -7 360.962 26.0935 26 2 -2 -7 361.327 26.2040 24 -2 -2 7 355.502 26.2673 26 -2 2 -7 319.791 26.1661 23 -2 2 -7 294.187 26.1370 21 2 -2 -7 351.981 26.1197 22 2 2 7 361.605 26.1754 8 -2 -2 7 368.173 26.2415 11 2 2 7 357.140 26.1923 9 2 2 7 261.767 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56.7725 4.33096 15 2 3 7 59.1627 4.44240 16 2 -3 -7 61.4003 4.43690 15 2 -3 -7 59.3177 4.59170 13 -2 -3 7 58.0482 4.51459 14 -2 -3 8 66.7409 4.81901 7 -2 -3 8 64.1999 4.87107 4 -2 3 -8 83.3919 4.84333 6 2 -3 -8 69.6553 4.78333 2 -2 3 -8 58.2989 4.72728 1 -2 3 -8 48.3559 4.70330 3 2 -3 -8 58.8782 4.75120 3 -2 3 -8 53.5848 4.73884 2 2 3 8 64.5967 4.62924 26 -2 3 -8 58.8477 4.68942 26 2 -3 -8 63.6441 4.81098 24 -2 3 -8 47.2100 4.71430 21 2 -3 -8 58.4364 4.83365 23 2 -3 -8 60.1434 4.66012 22 2 3 8 65.2505 4.79988 8 2 3 8 61.8125 4.80171 9 2 3 8 51.4120 4.77957 19 -2 3 -8 60.6889 4.85438 19 2 3 8 74.5484 4.89218 18 2 3 8 63.2661 4.78983 16 -2 3 -8 64.9167 4.69731 15 2 -3 -8 59.1152 4.77776 15 -2 -3 8 60.5679 4.86224 14 -2 -3 9 167.078 13.0081 7 -2 -3 9 171.832 13.0842 4 -2 3 -9 130.018 12.9283 6 -2 3 -9 131.469 12.9223 2 2 -3 -9 175.846 12.9684 3 -2 3 -9 183.402 12.9442 1 -2 3 -9 165.074 12.9306 3 -2 3 -9 171.779 12.9176 26 2 -3 -9 173.780 13.0294 24 2 3 9 176.098 12.8380 26 -2 3 -9 176.147 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433.800 36.2922 26 2 -4 -3 461.757 36.3755 24 -2 4 -3 418.732 36.3509 25 2 -4 -3 482.606 36.3665 23 2 4 3 516.683 36.3314 22 -2 4 -3 515.963 36.3633 23 2 -4 -3 485.109 36.1792 11 2 -4 -3 493.192 36.3457 8 -2 4 -3 481.495 36.1797 9 -2 4 -3 478.044 36.3593 10 -2 4 -3 467.323 36.2358 17 2 -4 -3 496.168 36.2676 15 -2 -4 3 522.642 36.3810 14 2 -4 -3 469.096 36.4154 13 -2 4 -3 504.389 36.3878 12 -2 4 -3 488.025 36.2186 14 -2 -4 3 478.174 36.3783 11 -2 4 -4 424.221 31.7556 4 -2 4 -4 429.799 31.8694 6 -2 -4 4 444.922 31.8554 7 -2 -4 4 401.842 31.8455 5 -2 4 -4 487.746 31.8727 2 -2 4 -4 460.963 31.8215 26 -2 -4 4 434.097 31.8831 26 -2 4 -4 476.318 31.9093 25 2 4 4 416.907 31.7805 26 2 -4 -4 417.772 31.8584 23 -2 4 -4 309.396 31.7879 23 -2 4 -4 410.891 31.8504 10 2 4 4 432.591 31.8574 18 2 4 4 511.401 31.8610 19 -2 4 -4 427.889 31.7112 17 -2 -4 4 434.781 31.8732 14 2 -4 -4 440.908 31.7745 15 2 -4 -4 440.222 31.9403 13 -2 -4 4 424.437 31.8798 11 2 4 4 413.095 31.6889 12 -2 4 -4 419.110 31.8735 12 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6 -2 -5 8 109.859 9.87404 7 -2 -5 8 120.936 9.97348 4 -2 5 -8 171.041 9.93598 2 2 -5 -8 122.381 9.87451 3 -2 5 -8 140.341 9.85729 1 -2 5 -8 126.261 9.84939 3 2 5 8 129.294 9.78462 26 -2 -5 8 140.348 9.98976 26 -2 5 -8 132.762 9.86046 26 -2 5 -8 124.505 9.86410 24 2 -5 -8 121.580 9.87609 23 2 -5 -8 129.572 9.85605 20 -2 -5 8 128.295 9.95826 11 2 5 8 130.157 9.89878 8 2 5 8 124.722 9.90648 19 2 5 8 148.443 9.96718 18 2 5 8 129.994 9.93226 16 -2 5 -8 124.984 9.72554 15 -2 -5 8 139.952 9.93908 15 2 -5 -8 125.774 9.83243 15 -2 -5 8 128.762 9.95220 14 2 -5 -8 116.787 9.98988 13 -2 -5 9 69.0228 4.86649 7 -2 5 -9 60.1353 4.81883 6 -2 -5 9 59.9418 4.92635 4 2 -5 -9 60.9121 4.80049 3 -2 5 -9 62.3080 4.78229 3 -2 5 -9 54.9710 4.75747 2 -2 5 -9 47.1280 4.70994 1 -2 5 -9 58.8714 4.76486 26 2 5 9 63.5992 4.69648 26 2 -5 -9 61.2246 4.81811 23 -2 5 -9 86.2188 4.88752 24 2 -5 -9 60.0055 4.75903 20 2 5 9 55.9964 4.82121 8 -2 -5 9 62.8924 4.89598 11 2 5 9 58.7555 4.84906 19 2 5 9 58.8994 4.86321 18 -2 -5 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29.9015 4 -2 6 -2 452.228 30.0712 6 -2 6 -2 477.972 30.0399 2 2 -6 -2 376.337 30.0196 3 -2 -6 2 407.858 29.9984 26 -2 6 -2 460.915 30.0571 25 -2 6 -2 363.192 29.9762 26 2 6 2 378.862 29.9815 26 2 -6 -2 446.311 30.0769 24 2 6 2 484.708 29.9790 22 -2 6 -2 391.939 29.9826 21 2 -6 -2 413.173 30.0022 23 -2 6 -2 379.327 29.8421 9 2 -6 -2 383.461 30.0260 10 -2 6 -2 354.359 29.8842 17 2 6 2 415.415 30.0748 16 -2 6 -2 414.722 29.8970 14 2 -6 -2 383.995 29.8275 15 -2 -6 2 375.201 30.0183 11 -2 6 -2 396.132 29.8095 11 -2 6 -2 381.615 30.0036 12 -2 6 -3 492.493 36.7951 5 -2 6 -3 702.425 37.1473 6 -2 6 -3 467.819 36.8936 4 -2 6 -3 340.283 36.9122 2 -2 -6 3 501.655 37.0090 26 2 6 3 512.099 36.9896 26 2 -6 -3 424.197 37.0058 24 -2 6 -3 573.880 37.0317 26 -2 6 -3 408.412 36.9725 25 -2 6 -3 518.667 36.9902 24 2 6 3 484.757 36.9296 22 2 -6 -3 536.393 37.0097 23 -2 6 -3 539.959 37.0101 23 2 -6 -3 493.808 37.0417 10 -2 6 -3 496.297 36.8294 9 2 6 3 445.328 37.0279 16 -2 6 -3 505.675 36.8936 14 -2 -6 3 516.007 37.0315 14 2 -6 -3 485.044 36.8474 15 -2 6 -3 515.596 36.8917 17 -2 -6 3 513.267 37.0461 11 -2 6 -3 493.416 36.8299 11 -2 6 -3 510.819 37.0253 12 2 -6 -3 500.533 36.7868 11 -2 6 -4 254.838 18.2283 5 -2 6 -4 178.996 18.3663 6 -2 6 -4 258.083 18.3281 4 -2 6 -4 205.233 18.3580 2 -2 -6 4 242.789 18.4242 26 -2 6 -4 245.664 18.3908 24 2 -6 -4 231.036 18.4443 24 -2 6 -4 248.280 18.3975 26 -2 6 -4 288.331 18.4852 25 2 6 4 253.837 18.3873 26 2 -6 -4 263.099 18.4099 23 -2 6 -4 245.417 18.3981 23 2 6 4 224.389 18.3203 22 2 6 4 240.574 18.4562 9 2 6 4 209.194 18.3728 18 2 -6 -4 244.962 18.2728 15 -2 -6 4 286.341 18.4832 14 -2 6 -4 255.597 18.3094 14 -2 6 -4 232.870 18.2686 17 -2 6 -4 261.437 18.4541 12 -2 6 -4 251.806 18.2564 11 -2 -6 4 251.098 18.4555 11 -2 6 -5 740.528 41.3072 6 -2 6 -5 560.708 41.1078 4 -2 6 -5 584.354 41.1717 1 -2 6 -5 730.993 41.2515 2 -2 6 -5 503.086 41.1430 3 -2 -6 5 497.592 41.1825 26 2 6 5 518.457 41.1266 26 -2 6 -5 527.537 41.1593 26 -2 6 -5 584.008 41.1743 24 -2 6 -5 495.438 41.1853 25 2 -6 -5 570.203 41.2526 24 2 -6 -5 587.188 41.1815 23 -2 6 -5 409.243 41.1120 23 2 -6 -5 592.641 41.2120 20 2 6 5 641.318 41.2115 8 -2 6 -5 537.515 41.0450 11 2 6 5 515.119 41.2206 9 2 -6 -5 503.247 41.1940 8 2 6 5 572.981 41.1992 18 -2 -6 5 552.225 41.1987 16 -2 6 -5 515.817 41.0260 17 2 -6 -5 585.814 41.0786 15 -2 -6 5 519.356 41.1949 14 2 -6 -5 550.932 41.2787 13 -2 6 -5 544.322 41.0811 14 -2 -6 5 536.543 41.2268 11 -2 6 -5 554.905 41.2159 12 -2 6 -6 62.8335 5.10117 4 -2 6 -6 63.5148 5.20478 6 -2 -6 6 66.2314 5.18763 7 2 -6 -6 57.3098 5.17073 3 -2 6 -6 85.3123 5.21780 1 -2 6 -6 36.6713 5.06045 2 -2 6 -6 74.4410 5.19201 3 -2 6 -6 65.6584 5.24854 25 -2 6 -6 66.0784 5.15648 26 -2 6 -6 60.5404 5.13989 24 2 6 6 63.8662 5.10874 26 -2 -6 6 68.5223 5.24815 26 2 -6 -6 66.8774 5.16516 23 2 -6 -6 57.6319 5.14109 20 -2 6 -6 78.1616 5.08021 11 2 6 6 74.4666 5.21189 8 2 6 6 69.1331 5.20431 19 2 6 6 61.0513 5.19248 18 -2 6 -6 67.0553 4.99667 16 -2 6 -6 67.8147 4.93446 15 2 -6 -6 63.5602 5.06784 15 -2 -6 6 60.4992 5.20220 14 -2 -6 6 63.5499 5.20333 16 -2 -6 6 73.1495 5.27714 11 2 -6 -6 68.0516 5.30595 13 -2 6 -6 68.2514 5.08876 14 -2 -6 7 92.2300 6.71458 7 -2 6 -7 80.7242 6.59896 4 -2 6 -7 54.2157 6.60275 6 -2 -6 7 94.1966 6.81300 4 2 -6 -7 95.5127 6.72440 3 -2 6 -7 94.2951 6.67917 2 -2 6 -7 79.7769 6.63000 3 -2 6 -7 66.2397 6.58273 1 -2 -6 7 97.6554 6.77238 26 -2 6 -7 103.499 6.80028 25 -2 6 -7 73.3350 6.61038 24 -2 -6 7 84.7056 6.41250 24 -2 -6 7 90.3588 6.42824 25 -2 6 -7 81.7216 6.63735 26 2 6 7 87.1477 6.60456 26 2 -6 -7 91.7671 6.66170 23 2 -6 -7 87.4779 6.65946 20 2 6 7 89.1194 6.69008 8 2 6 7 90.5618 6.71354 18 2 6 7 73.4392 6.64942 19 -2 -6 7 96.6043 6.76354 14 -2 6 -7 83.3286 6.46942 16 -2 6 -7 89.3171 6.45125 15 2 -6 -7 89.8775 6.59015 15 -2 -6 7 88.5807 6.71014 16 2 -6 -7 81.7658 6.78028 13 -2 -6 7 88.3439 6.74025 11 -2 6 -8 117.840 8.34790 4 -2 -6 8 110.744 8.49940 4 -2 -6 8 99.9345 8.37662 7 2 -6 -8 109.213 8.38369 3 -2 6 -8 104.116 8.32728 3 -2 6 -8 84.0295 8.29506 2 -2 6 -8 108.895 8.32998 1 -2 -6 8 131.098 8.51011 26 -2 6 -8 111.497 8.35107 24 -2 -6 8 106.269 8.16551 25 -2 6 -8 102.572 8.33837 26 2 6 8 109.833 8.29153 26 2 -6 -8 107.024 8.33948 20 2 -6 -8 105.747 8.34500 23 2 6 8 98.3540 8.36226 8 -2 -6 8 107.729 8.43387 11 2 6 8 113.097 8.42291 18 2 6 8 131.291 8.45923 19 -2 -6 8 112.938 8.41793 16 -2 6 -8 103.752 8.14989 16 -2 -6 8 99.9339 8.40371 14 -2 -6 8 116.353 8.41143 15 -2 6 -8 113.506 8.17241 15 2 -6 -8 110.461 8.30089 15 2 -6 -8 128.516 8.59070 13 -2 -6 9 171.775 14.2952 4 -2 -6 9 193.785 14.2470 7 -2 6 -9 169.351 14.1266 1 2 -6 -9 200.939 14.2301 3 -2 6 -9 218.169 14.2045 3 -2 6 -9 226.566 14.2159 2 -2 6 -9 178.581 14.1776 26 -2 6 -9 180.577 14.1625 24 -2 -6 9 187.220 14.0251 25 2 6 9 179.643 14.1005 26 2 -6 -9 185.125 14.1625 20 2 -6 -9 175.520 14.1627 23 2 6 9 173.227 14.2009 8 -2 -6 9 169.479 14.2431 11 2 6 9 208.664 14.2715 19 2 6 9 225.646 14.3038 18 2 6 9 182.939 14.2556 16 -2 6 -9 168.218 14.0063 15 -2 -6 9 183.847 14.2248 16 -2 -6 9 183.150 14.2249 15 -2 -6 9 202.711 14.2927 14 2 -6 -9 196.499 14.1497 15 2 -6 -9 186.188 14.3492 13 -2 -6 10 195.498 13.1659 7 -2 -6 10 161.517 13.1999 4 -2 6 -10 166.164 13.0074 1 -2 6 -10 153.254 13.0006 3 -2 6 -10 143.760 13.0012 2 2 -6 -10 172.215 13.0762 3 -2 6 -10 170.454 13.0669 26 2 6 10 181.061 12.9854 26 -2 6 -10 217.414 13.1132 24 2 -6 -10 177.019 13.0653 23 2 -6 -10 174.743 13.0326 20 2 6 10 162.621 13.1021 8 2 6 10 149.176 13.0889 19 -2 -6 10 178.753 13.1260 16 -2 -6 10 180.556 13.1215 15 2 -6 -10 171.677 13.0284 15 2 6 10 169.507 13.1386 16 -2 6 -10 169.616 12.9064 15 2 -6 -10 189.845 13.2974 13 -2 -6 11 85.0067 7.37109 7 -2 -6 11 115.715 7.60825 4 -2 6 -11 102.097 7.29202 1 2 -6 -11 103.884 7.35203 3 -2 6 -11 73.7024 7.25182 2 -2 6 -11 103.611 7.37081 26 -2 6 -11 67.4534 7.24615 24 2 -6 -11 103.769 7.49200 24 2 6 11 101.596 7.24551 26 2 -6 -11 103.013 7.34704 23 2 -6 -11 94.4416 7.28347 20 2 6 11 99.1301 7.42138 8 2 6 11 102.369 7.44733 16 -2 -6 11 102.746 7.42250 16 -2 6 -11 90.3194 7.17585 15 -2 -6 11 96.5650 7.38370 15 2 -6 -11 96.7251 7.32503 15 2 -6 -11 86.6354 7.50052 13 -2 -6 12 23.8161 2.15594 7 -2 -6 12 28.9505 2.40563 4 -2 6 -12 22.7677 2.00792 1 -2 6 -12 25.5309 2.07772 2 2 -6 -12 21.8529 2.03851 3 -2 6 -12 23.0452 2.08929 26 2 6 12 23.5983 1.93762 26 2 -6 -12 17.4514 2.01375 23 2 -6 -12 21.8192 1.99066 20 -2 6 -12 17.7598 2.01541 24 2 6 12 20.3712 2.18867 8 -2 6 -12 26.8870 2.34505 19 -2 -6 12 21.3425 2.10268 15 -2 6 -12 23.2627 1.91743 15 2 6 12 23.5938 2.18307 16 2 -6 -12 23.5856 2.34747 13 -2 6 -13 425.947 28.3018 2 2 -6 -13 380.256 28.2994 3 -2 6 -13 360.120 28.2310 1 2 6 13 379.395 28.2055 26 -2 6 -13 394.320 28.3565 26 2 -6 -13 406.367 28.3320 23 -2 6 -13 322.825 28.2521 24 2 6 13 387.482 28.4492 9 -2 6 -13 342.110 28.4636 19 2 6 13 394.580 28.4299 16 -2 6 -13 401.268 28.2115 15 -2 -6 13 359.004 28.3594 15 -2 -6 13 380.148 28.5183 4 -2 -6 13 326.081 28.3527 7 -2 6 -14 85.0480 7.10923 2 -2 6 -14 101.727 7.10815 1 2 -6 -14 90.2213 7.13966 3 -2 6 -14 96.2425 7.22906 26 2 6 14 93.5157 7.05439 26 -2 6 -14 103.751 7.19127 24 2 -6 -14 90.7904 7.17069 23 2 6 14 96.8352 7.34524 9 -2 6 -14 79.0987 7.34677 19 -2 6 -14 88.7168 7.06446 15 -2 -6 14 91.3897 7.26083 15 -2 -6 14 80.5116 7.23460 7 -2 -6 14 89.7039 7.39209 4 -2 6 -15 43.8450 4.00283 2 2 -6 -15 51.5595 4.04041 3 -2 6 -15 47.7631 3.97283 1 -2 6 -15 50.2885 4.14779 26 2 6 15 49.4919 3.94538 26 2 -6 -15 53.3630 4.10231 23 -2 6 -15 56.7607 4.11050 24 2 6 15 48.1735 4.24455 9 -2 6 -15 54.9972 4.39828 19 -2 -6 15 43.2344 4.13886 15 -2 6 -15 53.3801 4.00749 15 -2 -6 15 46.4225 4.33153 4 -2 6 -16-0.66339 0.74313 1 2 -6 -16-0.20151 0.70769 3 -2 6 -16 0.28467 0.74226 2 -2 6 -16 0.13586 0.89707 26 2 6 16 0.23667 0.58949 26 2 -6 -16 0.61100 0.73656 23 2 -6 -16 0.22510 0.31012 22 -2 6 -16-0.77986 0.92946 24 2 -6 -16 0.24090 1.11484 8 2 6 16-0.18266 0.97822 9 -2 6 -16-0.65502 1.11342 19 -2 -6 16-0.63987 0.90125 15 -2 6 -16 0.36927 0.77230 15 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2.05905 15 -2 -6 19 18.0954 2.32706 4 -2 6 -20 25.3917 2.23623 2 -2 6 -20 24.9408 2.17671 1 -2 -6 20 24.5678 2.18901 3 2 6 20 23.6641 2.20985 26 2 -6 -20 24.3172 2.38234 23 2 -6 -20 26.6427 2.07539 22 2 6 20 28.7883 2.71524 9 2 -6 -20 26.2312 2.90152 8 -2 6 -20 25.8756 2.81676 19 2 -6 -20 25.4555 2.30603 18 -2 6 -20 30.3814 2.86230 18 -2 -6 20 25.8664 2.61922 15 -2 -6 20 30.3544 2.86687 4 -2 -6 21 2.21512 0.63009 3 -2 6 -21 1.68525 0.63572 1 2 6 21 0.93777 0.66567 26 2 -6 -21 2.01102 0.52371 22 2 -6 -21 2.85567 1.00820 23 2 -6 -21 0.61710 1.46981 8 2 6 21 3.32063 1.28901 9 -2 6 -21-0.48926 1.25240 18 2 -6 -21 0.93888 0.74944 18 -2 6 -21 0.55237 1.29422 19 -2 -6 21 0.80805 1.18375 15 -2 -6 21 0.45719 0.70924 6 -2 -6 21 3.12338 1.47328 4 2 6 22 31.6807 2.51883 1 -2 -6 22 29.6712 2.45663 3 2 6 22 31.7884 2.59403 26 2 -6 -22 27.5830 2.72667 23 2 -6 -22 30.3068 2.43957 22 2 -6 -22 28.7033 3.28065 8 2 6 22 30.5593 3.09129 9 -2 6 -22 43.1219 3.33119 18 2 -6 -22 30.0633 2.64259 18 -2 6 -22 34.0360 3.26838 19 -2 -6 22 29.8032 3.00165 15 -2 -6 22 34.3821 3.29535 4 -2 -6 22 27.3310 2.48367 6 2 6 23 8.59470 0.89365 2 2 6 23 9.40567 0.90317 1 2 6 23 6.80828 1.00028 26 2 -6 -23 7.39527 1.28558 23 2 -6 -23 5.27510 0.84068 22 2 6 23 8.09461 1.60677 9 2 -6 -23 10.7707 1.98073 8 -2 6 -23 10.6346 1.82020 8 -2 6 -23 5.11297 1.71944 19 2 -6 -23 7.81972 1.11495 18 -2 6 -23 7.52237 1.60989 18 -2 -6 23 7.48616 1.56235 15 -2 -6 23 7.89435 0.84968 6 -2 -6 23 10.8354 2.02548 4 2 6 24 5.49907 0.89908 26 2 -6 -24 4.77825 1.09049 23 2 -6 -24 5.95878 1.69963 8 -2 6 -24 3.13281 1.62147 8 2 6 24 3.94170 1.38816 9 -2 6 -24 2.82120 1.55204 19 2 -6 -24 4.63094 0.95480 18 -2 6 -24 3.99876 1.67547 18 -2 -6 24 3.44082 1.40997 15 -2 -6 24 6.13232 1.83936 4 2 6 25 8.07615 1.04998 26 2 -6 -25 7.16030 1.29311 23 -2 6 -25 11.5411 2.00648 8 2 -6 -25 6.92496 1.90442 8 2 6 25 9.95263 1.77903 9 -2 6 -25 9.13770 1.92752 19 2 -6 -25 7.13702 1.17634 18 -2 6 -25 10.3902 1.80644 18 -2 -6 25 7.87740 1.60514 15 -2 -6 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3.90440 9 -2 8 6 58.7312 4.20303 9 -2 8 6 49.4844 4.20101 8 -2 8 6 49.0103 4.18224 17 -2 -8 -6 61.5283 4.28400 18 2 8 -6 60.8511 4.13177 18 -2 8 6 60.4192 4.11315 18 -2 8 6 49.9685 4.00816 15 2 8 -6 49.3786 4.27695 14 -2 8 6 44.4207 4.15716 12 -2 -8 -6 50.8951 3.89040 13 -2 -8 -5 34.7814 3.06811 5 2 8 -5 35.8255 3.10906 5 2 -8 5 24.8052 3.00013 3 -2 8 5 46.8290 3.13524 2 -2 8 5 35.3959 3.06158 1 2 -8 5 43.7523 3.17792 25 2 8 -5 35.9523 3.22162 26 2 8 -5 38.6821 3.04397 22 -2 8 5 32.7719 3.01077 23 2 -8 5 31.4554 3.02621 24 2 -8 5 47.3507 3.24600 21 -2 -8 -5 36.9599 2.94633 22 2 -8 5 36.3115 2.80682 9 -2 8 5 29.5117 2.98217 9 -2 8 5 36.4349 3.09471 8 -2 -8 -5 27.6088 3.02713 18 2 8 -5 36.0637 2.99142 18 -2 8 5 36.8301 2.97914 18 -2 8 5 38.8084 3.10775 17 2 8 -5 37.5446 3.20790 14 -2 -8 -5 34.3499 3.04039 17 2 8 -5 37.0897 3.08087 11 -2 8 5 43.3238 3.13417 12 -2 -8 -4 51.3584 4.31552 5 2 8 -4 54.4913 4.40168 5 -2 8 4 57.8818 4.35009 2 -2 8 4 61.6859 4.35593 1 2 -8 4 70.4829 4.49349 3 -2 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3.89444 23 2 8 -1 52.4033 3.88925 22 -2 8 1 52.2900 3.91524 8 -2 8 1 48.7278 3.82136 9 2 -8 1 48.0961 3.76461 9 -2 -8 -1 55.9432 3.98644 18 2 8 -1 49.0438 3.89809 18 2 8 -1 45.1200 4.00419 16 2 8 -1 46.2649 4.01621 14 -2 8 1 46.8071 3.87598 17 2 -8 1 41.2354 3.95860 12 -2 8 1 62.4199 4.03227 13 2 8 -1 45.5963 3.90724 11 -2 8 1 45.0258 3.92919 12 2 8 0 173.738 13.2905 5 -2 -8 0 172.444 13.1742 7 -2 -8 0 176.533 13.2315 5 2 -8 0 148.629 13.2410 24 -2 8 0 211.318 13.3202 25 -2 -8 0 178.838 13.2137 26 -2 8 0 191.197 13.3076 26 2 8 0 146.334 13.1322 22 2 -8 0 234.669 13.4275 21 -2 8 0 204.800 13.2516 23 2 -8 0 178.098 13.3217 3 -2 8 0 119.041 13.1371 2 2 -8 0 178.813 13.2648 10 -2 8 0 177.232 13.1291 9 2 -8 0 172.515 13.0967 9 -2 8 0 187.566 13.2112 8 2 8 0 173.400 13.3339 16 -2 8 0 165.229 13.1679 17 2 8 0 186.186 13.3644 14 -2 8 0 173.480 13.2459 12 2 8 0 187.174 13.2531 11 -2 -8 0 182.650 12.9687 12 2 -8 0 154.695 13.2525 12 -2 8 0 257.465 13.3989 13 -2 -8 1 47.1314 3.80095 7 -2 8 -1 47.4390 3.76385 4 2 -8 -1 24.0763 3.80997 6 2 -8 -1 46.9693 3.56157 5 -2 -8 1 46.7173 3.85350 5 2 8 1 56.3283 3.95821 26 -2 8 -1 46.5623 3.89249 25 2 -8 -1 52.3226 3.94262 24 -2 8 -1 53.0942 3.92610 26 -2 8 -1 33.9379 3.77873 24 -2 -8 1 44.2146 3.82970 26 2 8 1 50.4995 3.80753 22 -2 8 -1 56.2638 3.87958 23 -2 8 -1 28.2932 3.74107 2 2 -8 -1 44.7261 3.92248 3 2 -8 -1 53.8055 3.91955 10 -2 8 -1 46.1631 3.71238 9 -2 8 -1 49.2460 3.78604 17 2 8 1 50.9759 3.96873 16 2 -8 -1 48.7875 3.57977 15 -2 8 -1 47.6944 3.78776 14 2 8 1 50.2141 3.98782 14 -2 8 -1 49.1655 3.88702 12 -2 8 -1 48.3440 3.61541 11 -2 -8 1 53.0598 3.61428 12 2 -8 -1 48.6605 3.91585 12 2 -8 -1 46.2077 3.58720 11 2 -8 -2 140.970 8.23045 6 -2 -8 2 112.858 7.90334 7 -2 8 -2 92.7927 7.81172 4 2 -8 -2 97.6687 7.65550 5 -2 -8 2 89.0263 7.87205 5 2 -8 -2 120.572 8.04470 24 -2 8 -2 107.158 7.94241 25 -2 -8 2 100.760 7.90766 26 -2 8 -2 122.063 7.95079 24 2 8 2 110.884 7.97747 26 -2 8 -2 98.1811 7.93653 26 2 8 2 81.6719 7.79008 22 2 -8 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-7 28.5964 2.37150 6 2 8 7 21.3255 2.06333 26 2 -8 -7 25.2548 2.24544 24 -2 8 -7 23.4275 2.09244 24 -2 -8 7 22.1955 1.83464 24 -2 8 -7 22.0192 2.19376 25 -2 8 -7 21.9584 2.12216 26 2 -8 -7 19.6353 2.12939 20 2 -8 -7 24.8623 2.08332 23 -2 8 -7 19.5521 2.08981 2 -2 8 -7 18.0993 2.06714 1 2 -8 -7 25.8563 2.21246 3 2 8 7 21.8693 2.19860 9 -2 8 -7 27.2524 2.19932 10 2 8 7 25.1378 2.21018 8 -2 8 -7 22.3314 1.90824 16 2 -8 -7 19.6181 1.94625 15 -2 -8 7 23.0919 2.15680 16 2 8 7 22.4398 1.80580 12 2 -8 -7 22.1459 2.23961 13 -2 8 -7 27.0421 1.98903 11 -2 8 -7 24.2584 2.04199 14 -2 8 -8 32.1919 2.77418 4 2 -8 -8 47.7866 3.11744 6 -2 8 -8 36.2147 2.80445 24 -2 8 -8 30.3553 2.81467 26 -2 -8 8 31.6826 2.49932 24 -2 8 -8 30.1206 2.88114 25 2 -8 -8 31.5171 2.91291 24 2 8 8 29.9454 2.74521 26 2 -8 -8 38.7591 2.80514 23 2 -8 -8 35.4138 2.84417 20 -2 8 -8 26.5628 2.76567 2 2 -8 -8 33.5970 2.86468 3 -2 8 -8 31.3196 2.76097 1 2 8 8 32.9165 2.94179 9 -2 -8 8 33.9623 2.84982 16 -2 8 -8 31.7728 2.60595 16 -2 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10 31.9049 2.76013 15 -2 8 -10 35.6232 2.69246 11 2 -8 -10 31.2696 2.97068 13 -2 -8 11 113.776 8.87051 4 -2 -8 11 93.6523 8.66476 7 -2 -8 11 104.792 8.43351 25 -2 8 -11 111.358 8.71316 26 -2 8 -11 140.359 8.67517 24 2 8 11 114.583 8.60218 26 2 -8 -11 113.319 8.62956 20 2 -8 -11 113.196 8.59663 23 -2 8 -11 83.5297 8.55266 2 -2 8 -11 118.484 8.66475 4 -2 8 -11 121.765 8.62744 1 2 -8 -11 121.224 8.71850 3 -2 8 -11 112.943 8.43515 15 2 8 11 113.152 8.79647 16 -2 -8 11 111.625 8.67896 15 2 -8 -11 122.019 8.60927 15 -2 8 -11 102.819 8.56153 11 2 -8 -11 108.567 8.82634 13 -2 -8 12 133.816 11.3055 4 -2 -8 12 161.649 11.2637 7 -2 8 -12 137.723 11.1709 26 -2 8 -12 149.845 11.0826 24 2 8 12 142.419 11.0508 26 -2 -8 12 147.922 10.9456 25 2 -8 -12 137.907 11.0664 20 2 -8 -12 136.258 11.0352 23 2 -8 -12 131.969 11.1251 3 -2 8 -12 161.331 11.1211 2 -2 8 -12 154.189 11.0790 1 -2 8 -12 158.717 11.0926 11 2 8 12 137.186 11.2417 16 -2 8 -12 139.664 10.9138 15 -2 -8 12 138.946 11.1365 15 2 -8 -12 138.709 11.3158 13 -2 -8 13 153.833 11.3502 4 -2 -8 13 134.359 11.1507 7 2 8 13 142.598 10.9998 26 -2 -8 13 144.031 10.9270 25 -2 8 -13 125.336 10.9999 24 -2 8 -13 143.011 11.1512 26 2 -8 -13 143.514 11.0144 20 2 -8 -13 131.957 10.9853 23 -2 8 -13 164.919 11.0765 2 2 -8 -13 152.503 11.1256 3 -2 8 -13 142.573 11.0099 1 2 8 13 149.811 11.2405 16 -2 8 -13 146.711 10.8939 15 -2 -8 13 145.742 11.1171 15 2 -8 -13 145.064 11.3193 13 -2 -8 14 141.563 11.4267 4 -2 -8 14 164.059 11.3509 7 -2 -8 14 140.876 11.0393 25 2 8 14 140.779 11.0770 26 -2 8 -14 149.138 11.2632 26 -2 8 -14 155.824 11.1384 24 2 -8 -14 143.433 11.0851 20 2 -8 -14 138.649 11.0817 23 -2 8 -14 163.921 11.1602 2 -2 8 -14 141.911 11.0847 1 2 -8 -14 142.837 11.1776 3 -2 8 -14 148.450 11.4301 19 2 8 14 149.375 11.3365 16 -2 8 -14 130.701 10.9811 15 -2 -8 14 142.822 11.2041 15 2 -8 -14 151.196 11.4598 13 -2 -8 15 48.7129 4.20533 4 2 -8 -15 47.4223 3.87597 3 -2 8 -15 46.2847 3.79700 1 -2 8 -15 49.6082 3.84579 2 -2 8 -15 33.6381 3.76776 24 -2 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1.14519 9 2 -9 -3 12.2211 1.38043 10 -2 9 -3 12.1860 1.37243 10 -2 9 -3 10.7165 1.22739 14 2 9 3 8.72884 1.43566 16 -2 9 -3 11.0140 1.20230 17 2 -9 -3 10.3840 1.02315 15 2 -9 -3 12.3117 1.02305 11 -2 -9 3 11.1412 1.10278 12 -2 9 -3 12.2679 1.43911 12 -2 9 -3 10.8050 1.07210 11 -2 -9 4 32.9098 2.96065 5 2 -9 -4 21.3653 3.00285 6 2 -9 -4 35.1673 2.72727 5 -2 9 -4 36.1287 2.72451 5 -2 -9 4 34.9857 2.94867 7 -2 9 -4 32.1419 2.89025 4 2 9 4 35.9015 2.87500 22 2 -9 -4 41.0633 3.10730 21 -2 9 -4 38.7167 2.99256 24 2 9 4 35.1007 3.02144 26 2 -9 -4 41.5294 3.15305 24 -2 9 -4 34.2566 3.03357 25 -2 9 -4 30.8547 3.00180 26 -2 9 -4 37.3610 3.01843 10 2 -9 -4 35.6660 3.02474 10 2 9 4 33.1991 3.08985 16 2 -9 -4 37.2533 2.75737 15 -2 9 -4 33.4713 2.90769 14 2 -9 -4 33.4569 2.72393 11 -2 9 -4 33.5938 3.03451 12 -2 -9 4 32.3560 2.79835 12 -2 9 -4 33.8110 2.77214 11 -2 9 -5 45.5292 3.15130 5 2 -9 -5 34.5615 3.50815 6 -2 9 -5 42.4214 3.31915 4 2 9 5 36.0830 3.35847 26 -2 9 -5 35.7579 3.29955 24 2 -9 -5 46.9173 3.52875 24 -2 9 -5 44.9282 3.47175 26 -2 9 -5 38.4131 3.41186 25 2 9 5 37.7885 3.23774 22 2 -9 -5 43.3211 3.45963 10 -2 9 -5 47.1320 3.42557 10 2 9 5 34.8314 3.42909 9 -2 9 -5 38.6890 3.29820 14 -2 9 -5 39.6749 3.23436 16 2 9 5 33.3869 3.42285 16 2 -9 -5 37.7749 3.14848 15 -2 -9 5 37.1697 3.21562 12 -2 9 -5 40.8027 3.18314 11 2 -9 -5 39.3214 3.12394 11 2 -9 -6 62.2409 4.59571 6 -2 9 -6 56.1349 4.30190 4 -2 9 -6 52.8111 4.14220 5 -2 9 -6 42.9834 4.33415 25 2 9 6 52.9667 4.35031 26 -2 9 -6 50.3522 4.29480 24 2 -9 -6 52.6599 4.45598 24 -2 -9 6 53.5619 4.14480 24 -2 9 -6 54.6730 4.40938 26 2 9 6 62.4094 4.25720 22 2 9 6 53.2093 4.45369 9 2 -9 -6 41.7090 4.30942 10 -2 9 -6 52.6072 4.28604 14 2 -9 -6 56.0687 4.15091 11 -2 9 -6 54.3489 4.18395 11 -2 9 -6 52.9620 4.20218 16 2 -9 -6 55.7494 4.17312 15 2 9 6 45.2975 4.41723 16 2 -9 -6 49.2620 4.39880 3 -2 9 -7 59.8249 4.64877 4 -2 9 -7 58.3781 4.50742 5 2 -9 -7 63.4484 4.89275 6 -2 9 -7 53.5116 4.71837 25 2 9 7 56.8631 4.68312 26 2 -9 -7 50.7064 4.76467 24 -2 9 -7 52.6553 4.62320 24 -2 -9 7 59.7181 4.44812 24 -2 9 -7 56.6163 4.72052 26 2 -9 -7 58.3590 4.76059 3 2 9 7 58.5179 4.81356 9 2 -9 -7 55.7586 4.51369 15 -2 9 -7 54.1011 4.51010 16 -2 9 -7 59.9538 4.53880 11 2 -9 -7 61.3248 4.50656 11 -2 9 -7 57.8542 4.63908 14 2 9 7 57.3853 4.37155 12 -2 9 -8 45.1799 3.67976 5 2 -9 -8 42.2328 4.00310 6 -2 9 -8 51.6172 3.85364 4 -2 -9 8 45.2736 3.55861 24 2 -9 -8 40.7554 3.94113 24 -2 9 -8 42.5995 3.77225 24 2 9 8 44.0252 3.83394 26 -2 9 -8 44.5645 3.89511 26 2 -9 -8 50.2639 3.89043 20 2 -9 -8 43.4069 3.89533 3 2 9 8 46.0140 3.97093 9 -2 -9 8 46.6140 3.82668 15 -2 9 -8 42.4915 3.65772 16 2 -9 -8 52.1789 3.71933 15 2 -9 -8 55.6089 4.06926 13 -2 9 -8 42.9479 3.78517 14 2 9 8 47.0134 3.55999 12 -2 9 -8 47.7168 3.71668 11 -2 9 -9 233.819 15.7587 4 -2 9 -9 194.954 15.6239 5 2 -9 -9 165.580 15.8048 6 -2 9 -9 216.209 15.8358 26 2 9 9 201.718 15.7384 26 2 -9 -9 226.137 15.9375 24 -2 9 -9 208.912 15.6967 24 -2 -9 9 203.068 15.4571 24 2 9 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3 -3 -2 12.9099 1.30537 8 3 -3 -2 15.9900 1.54838 10 -3 3 -2 16.3356 1.20357 8 3 3 2 10.1242 1.40314 18 3 3 2 14.5185 1.30877 19 -3 -3 2 15.8639 1.35002 18 3 3 2 12.7738 1.39022 14 -3 -3 2 16.5689 1.46286 14 -3 -3 2 12.8700 1.43479 11 3 -3 -2 15.7580 1.19566 11 -3 -3 3 18.7950 1.78472 5 -3 3 -3 18.7312 1.58340 5 3 -3 -3 21.1660 1.60562 5 -3 3 -3 12.1485 1.74855 2 3 -3 -3 15.9798 1.80611 2 -3 -3 3 17.5115 1.58068 25 -3 -3 3 19.8837 1.86302 26 3 3 3 18.0535 1.68707 26 3 3 3 19.0226 1.73946 25 -3 3 -3 22.2692 1.88230 25 3 -3 -3 20.8454 1.86995 23 -3 3 -3 19.4332 1.80551 23 -3 -3 3 17.1336 1.74794 22 -3 3 -3 27.0860 1.85560 24 3 3 3 21.4963 1.75660 23 -3 3 -3 18.9572 1.50900 8 -3 3 -3 21.3962 1.83466 10 3 -3 -3 16.3474 1.66159 8 -3 -3 3 17.5409 1.63006 18 3 3 3 21.1963 1.66335 19 -3 -3 3 16.8321 1.74918 14 3 3 3 22.3556 1.62554 12 3 -3 -3 19.3384 1.54535 11 -3 -3 3 19.4754 1.79328 11 -3 -3 4 68.4686 5.13308 5 3 -3 -4 62.1311 4.98697 5 -3 3 -4 41.0489 5.06053 2 3 -3 -4 56.4000 5.14679 2 -3 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142.050 9.91785 7 -3 3 -7 121.717 9.83977 1 -3 3 -7 112.350 9.83493 3 -3 3 -7 112.304 9.86269 2 3 -3 -7 155.491 9.96365 2 3 -3 -7 154.934 9.93455 1 -3 -3 7 148.961 10.0106 26 3 -3 -7 133.345 9.91010 24 3 3 7 118.583 9.69844 26 -3 3 -7 133.048 9.75790 26 -3 -3 7 131.126 9.71013 24 -3 3 -7 156.616 9.93508 23 3 -3 -7 134.777 9.99676 23 3 3 7 123.960 9.76751 23 3 3 7 118.001 9.78538 8 -3 3 -7 141.252 9.93511 10 3 -3 -7 130.133 9.95536 8 3 3 7 95.3502 9.79990 19 -3 3 -7 140.116 9.92525 19 -3 3 -7 131.832 9.67559 16 3 3 7 127.599 9.88958 16 -3 -3 7 129.207 9.94739 15 -3 -3 7 128.649 9.91906 14 3 -3 -7 127.224 9.75908 11 3 -3 -7 130.847 10.0547 13 -3 -3 7 130.745 9.92370 11 3 3 7 131.218 9.81101 12 -3 -3 8 268.541 21.3133 7 -3 -3 8 294.860 21.3658 4 3 -3 -8 378.825 21.3867 1 -3 3 -8 231.085 21.2416 3 -3 3 -8 300.951 21.3333 2 -3 3 -8 294.357 21.2756 1 3 -3 -8 285.366 21.3269 2 3 -3 -8 292.586 21.3372 24 -3 -3 8 293.202 21.1247 24 -3 -3 8 299.997 21.4050 26 -3 3 -8 291.158 21.1773 26 -3 3 -8 303.582 21.3032 21 -3 3 -8 220.714 21.2600 24 3 -3 -8 286.329 21.4114 23 -3 3 -8 315.361 21.3324 23 3 3 8 280.220 21.1805 23 3 -3 -8 266.776 21.1994 22 3 3 8 280.548 21.3141 9 -3 -3 8 267.913 21.3418 11 3 -3 -8 303.201 21.4300 8 3 3 8 303.709 21.2567 8 3 3 8 287.035 21.2971 19 3 3 8 245.148 21.3083 18 -3 3 -8 269.422 21.3341 19 3 3 8 271.961 21.3005 16 3 -3 -8 286.388 21.2922 15 -3 -3 8 270.262 21.3634 15 3 -3 -8 282.622 21.4723 13 3 -3 -8 276.510 21.1953 11 3 3 8 271.373 21.2434 12 -3 -3 8 279.186 21.3480 14 -3 -3 9 32.3679 2.79255 7 -3 -3 9 32.9427 2.85250 4 -3 3 -9 31.1140 2.74518 3 -3 3 -9 34.1041 2.80994 2 -3 3 -9 36.0758 2.76581 1 3 -3 -9 36.7901 2.79026 1 3 -3 -9 31.2467 2.78028 2 -3 -3 9 31.1217 2.91832 26 -3 3 -9 34.5275 2.62335 26 3 -3 -9 33.7479 2.80804 24 -3 3 -9 27.0713 2.73817 21 3 3 9 35.8049 2.62903 23 -3 3 -9 43.8266 2.85304 23 3 -3 -9 30.4524 2.65919 22 3 -3 -9 36.2090 2.92528 23 3 3 9 29.4645 2.76476 9 3 -3 -9 31.6699 2.90871 8 3 3 9 30.6127 2.72915 8 -3 -3 9 35.3788 2.87213 11 3 3 9 23.5580 2.78296 18 -3 3 -9 31.3774 2.83821 19 3 3 9 35.5200 2.83752 19 3 3 9 34.1961 2.79290 16 3 -3 -9 30.7868 2.76757 15 -3 -3 9 29.6037 2.85753 15 -3 3 -9 36.5496 2.68891 15 3 -3 -9 34.1713 3.00167 13 3 3 9 35.1345 2.75791 12 3 -3 -9 30.2512 2.66259 11 -3 -3 9 31.6744 2.86482 14 -3 -3 10 32.6725 2.76383 4 -3 -3 10 31.6043 2.70552 7 -3 3 -10 33.8605 2.65971 3 3 -3 -10 39.6275 2.70598 1 -3 3 -10 36.6180 2.71839 2 -3 3 -10 24.2834 2.57945 1 3 -3 -10 31.4850 2.68231 2 -3 3 -10 29.9471 2.48902 26 -3 -3 10 31.3610 2.83861 26 3 -3 -10 32.6842 2.71420 24 -3 3 -10 37.5222 2.71707 23 3 -3 -10 33.9312 2.82886 23 -3 3 -10 32.2932 2.64848 21 3 -3 -10 30.5719 2.55382 22 3 3 10 24.5689 2.60753 8 3 -3 -10 29.6934 2.82873 8 3 -3 -10 31.5246 2.58612 11 3 3 10 29.5795 2.67749 9 3 3 10 35.7888 2.74445 19 -3 3 -10 31.7021 2.78111 19 -3 3 -10 22.9094 2.74187 18 3 3 10 30.7677 2.77814 18 3 3 10 32.7565 2.66681 16 3 -3 -10 31.3500 2.68535 15 -3 3 -10 33.2848 2.58072 15 -3 -3 10 29.6119 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1.76449 0.58108 22 3 3 12 2.19423 0.83073 9 -3 3 -12 2.12059 0.69027 8 3 -3 -12 2.42743 0.72949 11 3 3 12 2.20666 0.85060 8 -3 3 -12 0.95412 0.86072 19 -3 3 -12 2.97162 1.06001 18 -3 3 -12 1.29405 0.65990 15 3 3 12 0.96288 0.68361 16 -3 -3 12 2.48120 0.76828 7 -3 3 -12 1.20368 0.77116 6 -3 -3 12 3.24597 0.87481 4 3 -3 -13 24.4267 2.18213 2 3 3 13 24.2896 2.16345 1 -3 3 -13 26.1355 2.16046 1 -3 3 -13 25.5904 2.15939 3 -3 3 -13 26.4899 2.03843 26 3 -3 -13 22.8804 2.26218 24 -3 3 -13 32.2901 2.30316 23 3 -3 -13 23.6178 2.08399 22 3 -3 -13 22.0208 2.34731 23 -3 3 -13 20.4374 2.13384 21 -3 3 -13 23.8376 2.20950 8 3 3 13 25.6929 2.30788 8 3 -3 -13 22.2980 2.17109 11 3 3 13 22.6629 2.24445 9 -3 3 -13 22.1562 2.37246 19 3 3 13 25.1019 2.23104 16 -3 3 -13 29.1824 2.20239 15 -3 -3 13 22.9513 2.35169 4 -3 3 -13 24.6788 2.21901 6 -3 -3 13 23.9953 2.25162 7 3 3 14 55.2903 4.29579 1 -3 3 -14 50.5491 4.24644 1 -3 3 -14 58.2309 4.27547 3 -3 3 -14 53.5804 4.16260 26 3 -3 -14 50.9315 4.36883 24 -3 3 -14 44.7006 4.29935 23 3 -3 -14 48.4514 4.46353 23 -3 3 -14 64.8603 4.31155 21 3 -3 -14 51.3739 4.21704 22 3 -3 -14 58.2716 4.34102 11 3 3 14 56.9961 4.43515 8 -3 3 -14 50.7642 4.34896 8 3 3 14 54.7646 4.40740 9 -3 3 -14 49.4963 4.50947 19 -3 3 -14 52.6366 4.27117 15 3 3 14 54.0522 4.34157 16 -3 3 -14 50.3207 4.30476 6 -3 -3 14 55.2660 4.52224 4 -3 -3 14 56.6636 4.41405 7 3 3 15 45.1632 3.60937 1 3 3 15 51.1953 3.68039 2 -3 3 -15 39.8926 3.54793 3 -3 3 -15 50.4738 3.59842 1 3 -3 -15 43.8985 3.71860 24 3 -3 -15 43.8105 3.56178 22 -3 3 -15 45.1332 3.58490 21 -3 3 -15 46.7048 3.72652 8 3 3 15 41.9753 3.71354 9 -3 3 -15 33.3191 3.78542 19 3 3 15 44.9469 3.65813 16 -3 3 -15 50.6096 3.66317 15 -3 3 -15 36.7656 3.58713 6 -3 -3 15 44.3909 3.88340 4 -3 -3 15 44.3994 3.75683 7 3 3 16 29.1766 2.55440 2 3 3 16 30.2178 2.51392 1 -3 3 -16 26.2928 2.45376 3 3 -3 -16 29.4608 2.67077 24 3 -3 -16 30.7835 2.50322 22 -3 3 -16 27.8193 2.66259 8 3 3 16 33.5815 2.74069 9 -3 3 -16 23.8492 2.79619 19 3 3 16 29.7937 2.59642 16 -3 3 -16 32.7454 2.55224 6 -3 -3 16 28.8574 2.85841 4 -3 -3 16 27.7599 2.63656 7 3 3 17 20.3041 2.03961 2 3 3 17 23.8843 2.02700 1 -3 3 -17 22.1137 1.97725 3 3 -3 -17 20.0656 2.17519 24 3 -3 -17 22.6964 2.02270 22 -3 3 -17 18.5654 2.19235 8 3 3 17 29.0661 2.33585 9 -3 3 -17 21.5722 2.44831 19 3 3 17 18.9812 2.10557 16 -3 3 -17 27.0410 2.09496 6 -3 -3 17 28.9044 2.55513 4 -3 -3 17 22.7313 2.20950 7 3 3 18 16.4040 1.95881 2 3 3 18 24.4729 2.00691 1 -3 3 -18 21.7988 1.95549 3 3 -3 -18 25.6469 2.24307 24 3 -3 -18 23.2309 2.02563 22 3 3 18 22.2509 2.24116 9 -3 3 -18 21.9263 2.27015 8 -3 3 -18 22.3441 2.42856 19 -3 3 -18 19.6475 2.46339 18 3 3 18 23.9422 2.12145 16 -3 -3 18 20.3506 2.19355 7 -3 3 -18 28.1084 2.06870 6 -3 -3 18 19.1860 2.42758 4 3 3 19 56.4387 4.23938 2 -3 -3 19 54.2129 4.17860 3 -3 3 -19 51.4915 4.17138 3 3 3 19 56.1946 4.21554 1 3 -3 -19 49.6874 4.41326 24 3 -3 -19 53.7392 4.25120 22 -3 3 -19 49.5132 4.48263 8 3 3 19 51.6234 4.47033 9 -3 3 -19 43.7577 4.61506 19 -3 3 -19 58.5972 4.72032 18 3 3 19 54.0520 4.35508 16 -3 -3 19 48.5409 4.62805 4 -3 -3 20 22.5130 1.86757 3 3 3 20 21.2184 1.90135 2 3 3 20 18.2370 1.86647 1 3 -3 -20 23.9472 2.21979 24 3 -3 -20 22.3716 1.99552 22 3 3 20 22.4769 2.25056 9 -3 3 -20 22.6883 2.30892 8 -3 3 -20 17.7623 2.37021 18 -3 3 -20 23.3266 2.57530 19 3 3 20 23.5823 2.14016 16 -3 -3 20 21.1175 2.51286 4 3 3 21 10.7744 1.06851 1 3 3 21 9.76261 1.05412 2 3 -3 -21 8.32376 1.41823 24 3 -3 -21 8.69189 1.20180 22 -3 3 -21 9.16214 1.76259 19 -3 3 -21 10.0822 1.72568 18 -3 -3 21 13.5935 1.87171 4 3 3 21 9.32659 1.35937 16 3 3 21 9.91134 1.51657 9 -3 3 -21 8.35151 1.51932 8 3 3 22 14.5997 1.38026 2 3 3 22 16.1003 1.40191 1 -3 3 -22 14.6956 1.95142 8 3 -3 -22 16.4365 2.37506 8 3 3 22 17.0572 1.91796 9 3 -3 -22 17.4520 1.86859 24 -3 3 -22 17.4739 2.20603 18 -3 3 -22 13.0147 2.17907 19 3 3 22 16.4533 1.75845 16 -3 -3 22 18.1310 2.34075 4 3 3 23 47.6757 3.56261 1 3 -3 -23 44.4176 3.98045 24 -3 3 -23 50.9529 4.37625 18 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21.2933 2.16626 13 -3 6 -12 111.036 8.94671 6 -3 -6 12 118.249 9.14716 4 -3 -6 12 123.636 9.05405 7 3 -6 -12 113.770 8.96470 3 -3 6 -12 109.275 8.88996 3 -3 6 -12 94.7892 8.88643 2 -3 6 -12 111.264 8.88547 1 3 6 12 117.024 8.77788 26 -3 6 -12 114.633 8.89977 26 3 -6 -12 124.099 9.10622 24 3 -6 -12 121.799 9.02942 23 3 -6 -12 118.125 9.15843 8 3 6 12 118.113 8.99613 8 3 6 12 112.222 9.05282 9 -3 6 -12 115.364 9.11831 19 3 6 12 119.992 9.05311 16 -3 6 -12 120.259 8.78310 15 -3 -6 12 113.714 9.04578 15 3 -6 -12 127.116 9.28179 13 -3 6 -13 93.0213 7.63374 6 -3 -6 13 92.9487 7.83343 4 -3 -6 13 110.956 7.78686 7 -3 6 -13 86.0801 7.54817 1 3 -6 -13 92.6462 7.63986 3 -3 6 -13 105.311 7.65258 2 -3 6 -13 119.241 7.65277 3 3 6 13 97.6711 7.45196 26 -3 6 -13 101.236 7.61398 26 3 -6 -13 104.344 7.81718 24 3 -6 -13 97.8665 7.72466 23 3 -6 -13 101.590 7.90159 8 3 6 13 97.3993 7.76860 9 -3 6 -13 95.2512 7.83610 19 -3 6 -13 92.6831 7.47539 15 3 6 13 92.1376 7.71340 16 -3 -6 13 102.828 7.78334 15 3 -6 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15.8218 1.57882 1 -3 -8 -25 18.4050 1.72949 3 3 -8 25 14.4952 2.47389 25 -3 -8 -25 17.2730 1.91257 22 -3 8 25 20.1818 2.54651 9 3 8 -25 18.3835 2.34407 19 3 8 -25 15.1264 1.83944 18 -3 -8 -25 14.2777 2.35379 18 -3 8 25 16.5359 2.36381 15 -3 8 25 18.0049 2.52037 17 3 -8 25 15.2008 2.64237 12 3 8 -24 1.62930 1.62771 5 3 -8 24-0.28764 1.41538 4 3 8 -24 1.26554 0.74411 1 -3 -8 -24 0.97162 0.90125 3 3 -8 24 3.77189 1.89925 25 -3 -8 -24 2.44972 1.08137 22 -3 8 24-0.31015 1.52562 9 3 8 -24 2.64273 1.49223 19 3 8 -24 1.26165 1.06288 18 -3 -8 -24 4.27302 1.56895 18 3 -8 24 0.46059 1.03182 20 -3 8 24 2.11356 1.56173 15 -3 8 24 0.85016 1.51083 17 3 -8 24-0.37688 1.92448 12 3 -8 23 64.7303 5.54642 4 3 8 -23 60.4371 5.55612 5 3 8 -23 59.7191 4.94816 1 3 -8 23 59.4456 5.66812 25 3 -8 23 65.5122 5.15965 20 -3 -8 -23 55.2751 5.04813 22 -3 8 23 68.8720 5.65498 9 -3 8 23 65.8987 5.54554 17 -3 -8 -23 65.6580 5.53436 18 3 8 -23 66.8924 5.45719 19 -3 8 23 59.9205 5.39151 15 3 -8 23 59.6554 5.78716 12 3 8 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33.3990 2.70928 1 4 -4 -7 27.2317 2.73561 2 4 -4 -7 27.2650 2.72437 24 -4 -4 7 29.3236 2.46780 25 -4 -4 7 30.5707 2.47694 24 -4 4 -7 29.6301 2.54101 26 4 -4 -7 32.8049 2.85673 23 4 4 7 32.1839 2.60354 23 4 -4 -7 29.7513 2.72051 8 -4 4 -7 31.1108 2.35819 8 4 4 7 32.7523 2.57378 8 4 4 7 28.0558 2.61673 19 -4 4 -7 33.0604 2.71286 19 -4 -4 7 30.9438 2.71895 14 4 4 7 28.0556 2.74929 16 4 -4 -7 35.1047 2.94862 13 -4 -4 7 34.2852 2.77937 11 4 -4 -7 31.0564 2.48232 11 4 4 7 32.9770 2.55783 12 -4 -4 8 60.5127 4.97827 7 4 -4 -8 55.0772 4.82330 5 -4 -4 8 59.2403 4.99298 4 -4 4 -8 53.0198 4.89951 3 -4 4 -8 70.0800 5.02993 2 -4 4 -8 60.8044 4.91268 1 4 -4 -8 70.4603 5.03618 1 4 -4 -8 59.3958 4.99859 2 -4 -4 8 60.3766 4.72097 24 -4 -4 8 65.6629 4.75093 25 4 -4 -8 61.2749 4.98870 24 -4 4 -8 62.6737 4.79715 26 4 -4 -8 60.4841 5.07301 23 4 4 8 60.1003 4.82321 23 -4 4 -8 84.1356 5.04483 21 4 -4 -8 61.6417 5.02563 8 4 4 8 57.6857 4.81421 8 4 4 8 61.0210 4.88567 19 -4 4 -8 66.4217 4.99366 19 -4 4 -8 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25.5612 2.88567 5 4 -6 19 30.6581 2.83832 4 4 6 -19 26.9396 2.51789 1 4 -6 19 27.5825 3.08475 25 -4 -6 -19 27.3413 2.33435 20 -4 -6 -19 29.4368 2.73391 22 -4 6 19 25.3324 2.90436 9 4 6 -19 28.9715 2.70423 19 -4 -6 -19 26.5219 2.91842 18 4 6 -19 25.3758 2.25987 18 -4 6 19 26.4377 2.77562 15 4 -6 19 32.4624 3.17810 12 4 6 -18 23.0747 2.14839 1 4 -6 18 21.1392 2.10586 14 4 -6 18 22.8798 2.64515 12 -4 -6 -18 21.7036 2.28157 22 -4 6 18 27.2909 2.64202 9 4 6 -18 19.9736 1.87743 18 4 6 -18 20.4003 2.23501 19 -4 6 18 24.5087 2.41373 15 4 -6 18 22.6684 2.35086 4 4 6 -18 21.2241 2.55598 5 4 6 -17 59.4809 4.47658 1 4 -6 17 53.4491 4.85420 12 -4 -6 -17 55.6471 4.56374 22 -4 6 17 51.3300 4.69486 9 4 6 -17 53.8594 4.19428 18 4 6 -17 50.2924 4.47672 19 4 -6 17 54.7464 4.34375 14 -4 6 17 48.6447 4.53179 15 4 6 -17 52.4262 4.76912 5 4 -6 17 51.4194 4.55122 4 4 -6 16 142.277 10.7214 12 4 -6 16 95.5067 10.2377 20 -4 -6 -16 119.705 10.3381 22 -4 6 16 137.550 10.5777 9 4 6 -16 136.435 10.0813 18 -4 6 16 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41.9998 3.62766 19 4 -6 13 46.9143 3.75147 20 -4 -6 -13 41.5371 3.73003 22 -4 6 13 40.3101 3.68573 15 4 -6 13 44.9632 3.45905 14 4 6 -13 50.3798 4.01241 5 4 -6 13 42.5809 3.63604 4 -4 6 13 43.4262 3.42080 7 4 -6 12 36.6321 3.40784 12 -4 6 12 35.1365 3.07021 19 -4 6 12 38.3116 2.86729 18 -4 -6 -12 35.2392 3.37764 18 4 6 -12 33.5952 2.92852 18 4 6 -12 34.6756 3.08639 19 4 -6 12 33.9838 3.18870 20 -4 -6 -12 36.5258 3.21437 22 4 -6 12 35.6458 2.88737 14 -4 6 12 35.5437 3.15901 15 4 -6 12 36.3914 3.09730 4 -4 6 12 36.0283 2.88707 7 4 6 -12 41.6890 3.45353 5 4 -6 11 112.686 8.76583 12 -4 6 11 112.412 8.44233 19 -4 -6 -11 87.0776 8.57366 18 4 6 -11 96.9868 8.31066 18 -4 6 11 111.097 8.27271 18 4 6 -11 108.090 8.43394 19 4 -6 11 109.556 8.58702 20 -4 -6 -11 118.463 8.58632 22 -4 6 11 106.642 8.49576 15 4 -6 11 117.205 8.26493 14 4 6 -11 112.824 8.71648 5 4 -6 11 109.242 8.43871 4 4 -6 10 12.6637 1.73054 12 -4 -6 -10 9.54210 1.42211 22 -4 6 10 10.9706 1.14327 22 -4 6 10 12.1334 1.09853 18 -4 6 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6 65.9613 4.85392 8 4 6 6 50.9902 4.80533 19 -4 6 -6 63.2079 4.69445 17 4 6 6 60.1967 5.02886 16 -4 -6 6 62.7372 5.02972 11 4 -6 -6 59.9828 4.59973 11 -4 -6 7 28.1451 2.54447 7 4 -6 -7 26.3804 2.27150 5 4 -6 -7 26.8235 2.55874 3 4 6 7 25.1031 2.35930 26 -4 6 -7 31.7560 2.44160 26 4 6 7 26.0321 2.34392 23 4 -6 -7 23.6717 2.55258 23 -4 -6 7 29.1173 2.22944 24 4 6 7 26.1277 2.40928 8 4 -6 -7 27.4696 2.51763 8 4 6 7 31.0893 2.48354 19 -4 6 -7 28.4409 2.20321 17 -4 6 -7 26.7420 2.21602 15 4 6 7 31.2092 2.66315 16 4 -6 -7 26.7513 2.17699 11 -4 -6 7 29.2393 2.61726 11 4 6 7 27.1215 2.20018 12 4 -6 -8 68.7077 5.65014 5 -4 -6 8 71.2688 5.87151 7 4 -6 -8 66.5721 5.87268 3 -4 -6 8 76.6983 5.55758 24 4 6 8 68.5528 5.67708 26 4 -6 -8 74.5839 5.94614 24 -4 6 -8 71.5354 5.74285 26 4 6 8 77.0742 5.68605 23 4 -6 -8 67.5792 5.90468 23 4 6 8 73.3477 5.76569 8 4 -6 -8 79.7659 5.94065 8 4 6 8 75.8211 5.80397 19 4 6 8 79.1367 5.98691 16 -4 6 -8 73.4224 5.58661 15 -4 6 -8 72.3396 5.52633 17 4 -6 -8 78.5742 6.12495 13 -4 -6 8 73.0276 5.94508 11 4 -6 -8 71.5225 5.56514 11 4 6 8 71.2575 5.58478 12 -4 -6 9 16.9099 1.80897 7 4 6 9 14.8252 1.52194 26 -4 -6 9 15.3231 1.32602 24 -4 6 -9 18.3475 1.62020 26 -4 -6 9 14.3887 1.29989 25 4 6 9 18.3273 1.50720 23 4 -6 -9 20.6947 1.91718 23 4 -6 -9 14.0949 1.77561 24 4 6 9 18.6973 1.71284 8 4 -6 -9 15.7357 1.78048 8 -4 -6 9 19.9638 1.87175 11 -4 6 -9 18.0744 1.83357 19 4 6 9 15.0524 1.83943 16 -4 6 -9 17.6304 1.44495 15 4 -6 -9 15.3989 1.41682 11 4 -6 -9 17.1235 1.99846 13 4 6 9 18.2243 1.48195 12 -4 -6 10 11.1316 1.43247 7 -4 6 -10 11.1107 1.21706 26 -4 -6 10 10.8198 0.94246 25 4 6 10 9.49163 1.11793 26 4 -6 -10 9.56152 1.43866 24 4 -6 -10 14.9406 1.64727 23 4 6 10 9.14217 1.01971 23 4 -6 -10 12.3353 1.47649 8 4 -6 -10 10.6038 1.07421 11 -4 -6 10 11.5424 1.50430 11 4 6 10 9.30882 1.32835 8 -4 6 -10 8.86801 1.38749 19 -4 6 -10 10.9396 1.06735 15 4 6 10 11.4308 1.48843 16 4 -6 -10 12.5240 1.69425 13 4 6 10 9.45415 1.08347 12 -4 -6 11 102.794 8.86398 4 -4 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8.92006 2.31666 18 -6 6 28 10.2013 2.28913 15 6 -6 28 8.78916 2.80413 12 6 6 -27 5.16190 2.14597 5 6 -6 27 3.73175 1.68150 4 -6 6 27 6.48773 1.87656 4 6 -6 27 2.74655 2.40263 25 -6 -6 -27 3.25790 1.72813 22 -6 6 27 4.57764 1.98065 9 6 6 -27 4.49876 2.39181 8 -6 -6 -27 3.45054 1.93312 18 -6 6 27 2.55618 1.83379 15 6 -6 27 2.15438 2.18381 12 6 -6 26 8.43559 2.45053 12 -6 -6 -26 13.2736 2.15764 22 -6 6 26 8.20008 2.28354 9 6 6 -26 14.1876 2.92748 8 6 6 -26 10.9179 1.77778 19 -6 -6 -26 6.80155 2.29896 18 -6 6 26 13.0010 2.20815 15 -6 6 26 12.4895 2.07535 4 6 6 -26 8.55021 2.33134 5 6 -6 26 15.8890 2.16612 4 6 -6 25 10.7225 2.46901 12 -6 -6 -25 11.0555 2.05184 22 -6 6 25 14.5518 2.40428 9 6 6 -25 9.52637 2.52600 8 6 6 -25 8.33217 1.57433 19 -6 -6 -25 8.92782 2.39866 18 -6 6 25 7.79184 2.05974 15 -6 6 25 12.2432 2.03681 4 6 6 -25 12.1494 2.32777 5 6 -6 25 9.09269 1.89552 4 6 6 -24 9.36034 1.53967 1 6 -6 24 6.03459 2.32179 12 -6 -6 -24 12.5969 2.06348 22 -6 6 24 8.49641 2.21459 9 6 6 -24 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1.97229 23 7 -5 -22 7.03693 1.61807 24 7 -5 -22 9.12684 2.23408 8 -7 5 -22 5.48295 2.14280 18 -7 5 -22 3.45641 1.82953 19 -7 -5 22 8.19592 1.91640 7 7 -5 -22 5.79388 1.56048 5 -7 -5 22 6.95776 1.92761 4 7 5 22 8.17751 1.68425 12 7 5 23 9.88483 2.56632 25 7 -5 -23 7.73021 2.22219 23 7 -5 -23 8.92906 1.65906 24 7 -5 -23 7.20183 2.12933 8 -7 5 -23 8.80658 2.33333 18 -7 5 -23 3.59224 1.95574 19 7 5 23 6.95749 1.60118 2 -7 -5 23 9.09727 1.90884 7 7 -5 -23 11.0149 1.94362 5 -7 -5 23 8.12017 2.03119 4 7 5 24 32.2771 4.05394 25 7 -5 -24 34.9098 3.63567 23 7 -5 -24 29.0451 3.10561 24 7 -5 -24 31.2213 3.80726 8 -7 5 -24 32.7067 3.87184 18 -7 5 -24 25.7474 3.47144 19 7 5 24 35.0976 3.24825 2 -7 -5 24 34.1415 3.44921 7 7 -5 -24 30.2619 3.35644 5 -7 -5 24 29.9373 3.58300 4 7 -5 -25 12.6447 2.35919 23 7 -5 -25 10.1655 1.78937 24 7 -5 -25 8.46953 2.38969 8 -7 5 -25 7.01214 2.21113 19 7 5 25 11.8009 2.56121 25 -7 -5 25 3.01124 1.81357 7 7 -5 -25 11.2789 2.04037 5 -7 -5 25 8.61571 2.29182 4 7 -5 -26 5.26241 2.21068 23 7 -5 -26 6.64652 1.63446 24 7 -5 -26 4.99061 2.29637 8 -7 5 -26 6.51661 2.14269 19 7 5 26 5.38223 2.32629 25 7 -5 -26 6.41053 1.90318 5 -7 -5 26 3.74576 2.06396 4 7 -5 -27 14.6838 2.62585 23 7 -5 -27 8.98452 2.71572 8 -7 5 -27 11.1816 2.51738 19 7 5 27 13.7818 3.08234 25 7 -5 -27 13.8299 2.26970 5 -7 -5 27 12.2315 2.43092 4 7 -5 -28 4.51564 2.08893 23 7 -5 -28 10.4595 2.57721 8 -7 5 -28 9.04731 2.50736 18 -7 5 -28 11.1024 2.49493 19 7 5 28 6.10129 2.49153 25 -7 -5 28 7.15338 2.17934 4 7 -5 -28 12.0630 2.17928 5 7 -5 -29 5.80893 2.09735 23 -7 5 -29 2.61350 2.19741 18 -7 5 -29 3.91954 2.33637 19 7 5 29 7.17434 2.61696 25 7 -5 -29 6.02859 1.94162 5 -7 -5 29 1.46217 2.02438 4 7 -5 -29 5.79680 2.48905 8 7 -5 -30 2.27488 2.54835 8 -7 5 -30 1.31256 2.24809 18 -7 5 -30-1.20268 2.13330 19 7 5 30 0.48616 2.47974 25 -7 -5 30 1.47760 2.11911 15 7 -5 -30 1.62210 1.81748 5 -7 -5 30-0.37254 2.07407 4 -7 5 -31 5.71667 2.29399 19 7 -5 -31 4.63085 2.03378 5 -7 -5 31 6.06065 2.31820 4 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3.43059 2.29644 8 -8 -5 -21 5.90540 2.21200 18 -8 5 21 7.12356 2.05417 15 8 -5 21 7.43047 2.22439 12 8 5 -21 7.96950 2.25347 13 -8 -5 -21 3.02684 2.01059 11 8 5 -20 1.46582 1.64979 5 8 5 -20-0.97939 1.46019 1 8 5 -20 0.29215 1.62598 2 8 -5 20 2.60702 2.34246 25 -8 -5 -20-2.29151 1.86641 22 8 5 -20-0.83321 2.01215 8 -8 -5 -20 1.92764 1.90730 18 -8 5 20-0.28899 1.70482 15 8 -5 20 2.30279 2.06910 12 8 5 -20-1.05006 1.73164 13 -8 -5 -20-1.11010 1.72763 11 8 5 -19 2.51207 1.73596 5 8 5 -19 4.03417 1.57808 1 8 5 -19 3.01695 1.92172 2 8 -5 19 3.82554 2.17649 25 -8 -5 -19 5.84772 1.85952 22 8 5 -19 2.81679 2.04811 8 -8 -5 -19 3.76838 1.94952 18 -8 5 19 8.71189 1.88438 15 8 -5 19 4.88465 2.01225 12 8 5 -19 4.06576 1.95941 13 -8 -5 -19 5.05666 1.83048 11 8 5 -18 1.75609 1.69926 5 -8 5 18 3.64377 1.22736 7 8 5 -18 2.84044 1.50849 1 8 5 -18 0.30991 1.77269 2 8 -5 18 2.90660 2.13089 25 -8 -5 -18 5.47927 1.84233 22 8 5 -18 7.77286 2.26719 8 -8 -5 -18 4.05362 1.97487 18 -8 5 18 3.82496 1.68108 15 8 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11 8 5 -11 6.72943 1.79234 5 8 -5 11 9.14486 1.85539 2 8 5 -11 7.43626 1.77791 1 8 -5 11 6.80703 1.93105 1 8 5 -11 10.2894 2.09952 2 8 -5 11 3.54133 1.85246 25 -8 -5 -11 8.07561 1.85133 22 -8 5 11 6.24483 1.48578 22 -8 -5 -11 9.56582 1.88698 18 -8 5 11 7.41045 1.68537 15 -8 -5 -11 9.17541 1.79691 11 8 -5 11 7.36440 1.95029 12 8 5 -10 16.8513 2.36679 5 8 -5 10 18.0749 2.31018 2 8 5 -10 16.4064 2.24639 1 8 5 -10 15.5135 2.46578 2 8 -5 10 14.7054 2.25157 1 8 -5 10 13.1509 2.45466 25 -8 -5 -10 13.9037 2.16515 22 -8 5 10 16.7131 2.05659 22 8 5 -10 16.1531 2.03811 10 -8 -5 -10 12.9849 2.25763 18 -8 5 10 15.0765 2.08729 15 -8 -5 -10 13.0237 2.21255 11 8 -5 10 17.0208 2.47649 12 8 5 -9 30.6023 3.41100 5 8 -5 9 26.5715 3.32866 2 8 5 -9 39.5149 3.71544 2 8 -5 9 32.0730 3.35617 1 8 5 -9 32.4474 3.41471 1 8 -5 9 26.0633 3.39720 25 8 5 -9 34.8311 3.65303 23 -8 -5 -9 26.6460 3.30227 22 -8 5 9 35.4084 3.15677 22 8 5 -9 34.9075 3.14454 10 -8 -5 -9 31.1654 3.36763 18 -8 5 9 32.5616 3.16717 15 8 -5 9 35.7015 3.47505 12 -8 -5 -9 29.1677 3.29233 11 8 5 -8 22.0141 2.88196 5 8 -5 8 24.5588 2.89270 2 8 5 -8 27.4750 3.13778 2 8 -5 8 17.8821 2.72143 1 8 5 -8 23.2902 2.87392 1 8 -5 8 30.7830 3.17528 25 8 5 -8 28.1688 3.17741 23 -8 -5 -8 28.1124 2.94927 22 -8 5 8 27.1405 2.70422 22 8 5 -8 18.7103 2.50873 10 -8 5 8 28.2854 2.19031 18 -8 -5 -8 25.7106 2.85053 18 -8 5 8 26.9856 2.67598 15 -8 -5 -8 22.2415 2.78892 11 8 -5 8 22.9814 2.95039 12 8 5 -7 38.8717 3.96847 5 8 -5 7 38.1296 3.98709 1 8 5 -7 35.2691 4.03124 2 8 5 -7 45.9506 4.03268 1 8 -5 7 39.1899 3.94859 2 8 -5 7 39.8674 4.04662 25 8 5 -7 38.0715 4.14689 23 -8 5 7 47.4637 3.83915 22 8 5 -7 40.3907 3.64968 10 -8 -5 -7 42.7435 3.88039 18 -8 5 7 38.9973 3.33080 18 -8 5 7 39.8004 3.68067 15 -8 -5 -7 40.7245 3.85738 11 8 5 -6 4.32164 1.61628 5 8 -5 6 6.34554 1.67225 2 8 5 -6 7.00037 1.90619 2 8 -5 6 1.71233 1.55205 1 8 5 -6 2.05580 1.58546 1 8 -5 6 4.13080 1.77815 25 8 5 -6 4.45915 1.75713 23 -8 5 6 2.84605 1.23323 22 8 -5 6 4.86790 1.57712 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18.2960 2.29663 17 -8 11 4 17.5285 1.98283 9 -8 11 4 15.4317 2.07401 22 -8 -11 -4 15.3939 2.41548 22 8 11 -4 16.9075 2.64102 14 -8 -11 -4 19.5753 2.64685 11 -8 11 3 23.1314 2.65080 17 -8 -11 -3 24.3829 2.76897 18 -8 11 3 23.0022 2.34149 9 -8 11 3 23.2251 2.52299 22 -8 -11 -3 26.0276 3.07801 11 8 11 -3 25.9390 3.06595 14 -8 -11 -2 24.7139 2.81984 18 8 11 -2 21.0622 3.05324 23 -8 11 2 23.0891 2.63800 22 -8 11 2 29.9320 2.81885 17 -8 -11 -2 25.4783 3.12347 11 8 11 -2 26.5154 3.08554 14 -8 -11 -1 1.26020 1.39104 18 8 11 -1 1.25143 1.58449 23 -8 11 1 2.09904 1.20609 22 -8 11 1 5.31699 1.44267 17 -8 -11 -1 2.74254 1.70778 11 8 11 -1 4.36631 1.86073 14 -8 -11 0 18.5584 2.51658 18 -8 11 0 26.4066 2.52709 17 -8 -11 0 23.2128 2.96931 11 8 11 0 22.2172 2.89625 14 8 11 0 22.5615 2.86088 23 -8 11 0 23.9555 2.56602 22 -8 -11 1 1.02062 1.64816 11 8 11 1 2.44617 1.54153 14 -8 11 -1 1.52044 1.17644 17 -8 -11 1 3.16704 1.59766 7 8 11 1 2.30006 1.54510 23 -8 11 -1 0.75160 1.33894 22 -8 -11 2 23.6585 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2.36526 1 11 5 -8 12.4525 2.86220 2 -11 -5 -7 2.51769 1.71212 11 -11 -5 -7 4.69832 1.84831 18 11 5 -7 2.62872 2.16271 23 -11 5 7 3.49885 1.77237 22 -11 5 7 1.61365 1.78280 15 11 -5 7 0.41049 2.33788 2 11 -5 7 5.89092 2.41518 1 11 5 -7 2.36519 2.03792 1 11 5 -7 5.57453 2.73499 2 -11 -5 -6 2.17143 1.59383 11 -11 -5 -6 2.81010 1.66006 18 11 5 -6 0.43015 2.12034 23 -11 5 6 2.08253 1.76581 22 -11 5 6 3.44867 1.73157 15 11 -5 6 5.36389 2.50759 2 11 -5 6 5.13389 2.22003 1 11 5 -6 0.79367 2.12001 1 11 5 -6 2.33608 2.31961 2 -11 -5 -5 3.06808 1.87104 11 -11 -5 -5-1.07622 1.62448 18 11 5 -5 3.77625 2.42205 23 -11 5 5 1.82274 1.78477 22 -11 5 5 1.05059 1.71385 15 11 -5 5 2.07341 2.16289 2 11 -5 5 2.38980 2.09216 1 11 5 -5 1.59675 2.31768 1 11 5 -5-0.93891 2.26940 2 -11 -5 -4 5.16040 1.78984 11 -11 -5 -4 5.12065 1.69440 18 11 5 -4 11.8688 2.43945 23 -11 5 4 7.15424 2.08497 22 -11 -5 -4 8.65016 2.36960 22 -11 5 4 10.1326 2.02060 15 11 -5 4 6.26497 2.47343 2 11 -5 4 8.39334 2.61738 1 11 5 -4 12.3999 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1.31404 2.36401 2 11 6 -12 2.64312 2.11457 1 11 6 -12 1.33340 2.33237 2 11 6 -12 1.92644 2.36406 23 -11 -6 -12-0.38814 2.30240 22 11 -6 12 0.43800 2.26631 25 -11 -6 -12-1.74874 2.15213 18 -11 6 12-0.54539 1.82422 15 -11 -6 -12 1.05119 1.88916 11 11 -6 11 1.73010 2.23793 25 11 6 -11 0.94550 2.37515 23 -11 -6 -11-0.77546 2.14469 22 -11 -6 -11-0.69392 1.76941 11 11 6 -11-1.91000 2.33864 1 11 6 -11-0.45174 2.25232 2 -11 -6 -11 0.33980 1.81992 18 11 6 -10 1.39567 2.13410 23 -11 -6 -10 0.77126 2.06576 22 -11 6 10 0.26202 1.69232 22 -11 -6 -10 0.34252 1.88325 11 11 6 -10 3.48026 2.19218 1 11 6 -10-0.45716 2.24443 2 -11 -6 -10-0.65917 1.83492 18 11 6 -9 6.39368 2.62863 23 -11 -6 -9 5.38886 2.12508 22 -11 6 9 8.07056 1.94423 22 -11 -6 -9 8.11752 2.14118 11 11 -6 9 6.91733 2.35126 2 11 6 -9 6.23698 2.25633 1 11 6 -9 7.86517 2.51975 2 -11 -6 -9 1.90834 1.97102 18 11 6 -8 22.4238 3.19525 23 -11 -6 -8 16.4574 2.93809 22 -11 6 8 18.4843 2.53141 22 -11 -6 -8 16.0387 2.59367 11 11 -6 8 23.3335 3.13831 2 11 -6 8 12.1351 2.67279 1 11 6 -8 13.7829 2.85659 1 11 6 -8 14.4624 3.08359 2 -11 -6 -8 15.0632 2.47140 18 11 6 -7 15.8018 3.10485 23 -11 6 7 18.3502 2.64646 22 -11 -6 -7 11.9039 2.44081 11 11 -6 7 22.6522 3.20959 2 11 -6 7 18.1252 3.01497 1 11 6 -7 14.5784 3.07804 2 11 6 -7 22.6370 3.19908 1 -11 -6 -7 16.8175 2.53694 18 11 6 -6 6.88961 2.44270 23 -11 6 6 6.64881 1.92346 22 -11 -6 -6 2.60949 1.75555 11 11 -6 6 9.94174 2.42104 2 11 -6 6 4.76210 2.20226 1 11 6 -6 4.73029 2.52961 2 11 6 -6 5.19867 2.23242 1 -11 -6 -6 3.95729 1.80804 18 11 6 -5 10.0847 2.51544 23 -11 6 5 10.3969 2.26798 22 -11 -6 -5 12.2688 2.32104 11 11 -6 5 12.9025 2.71068 2 11 -6 5 9.96400 2.60728 1 11 6 -5 12.3833 2.87582 2 11 6 -5 12.0696 2.64102 1 -11 -6 -5 11.6625 2.07941 18 11 6 -4 4.09199 2.07415 23 -11 6 4 6.98783 1.94313 22 -11 -6 -4 4.47492 1.81787 11 11 -6 4 4.60444 2.40174 2 11 -6 4 11.2045 2.56316 1 11 6 -4 5.73932 2.57163 2 11 6 -4 1.61761 2.14017 1 -11 -6 -4 4.14833 1.73013 18 11 6 -3 17.9195 2.96027 23 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4 6 5.11845 2.01350 22 12 -4 5 11.4572 2.84544 2 12 4 -5 2.93093 2.24771 1 12 -4 5 10.9580 2.59735 1 12 4 -5 4.83226 2.61402 2 12 4 -5 5.61404 2.37598 23 -12 -4 -5 4.38539 2.34799 22 -12 4 5 6.85299 2.15965 22 12 -4 4 8.41681 2.75422 2 12 4 -4 9.68394 2.73146 1 12 -4 4 11.8577 2.68272 1 12 4 -4 15.0485 3.15649 2 12 4 -4 14.7946 2.82715 23 -12 -4 -4 10.2829 2.63861 22 -12 4 4 9.30654 2.45044 22 12 -4 3 3.40240 2.38757 1 12 4 -3 4.89018 2.52252 2 12 4 -3 5.40625 2.46089 23 -12 4 3 9.14481 2.25951 22 -12 -4 -3 7.47896 2.42177 22 12 -4 3 8.46376 2.25415 23 12 -4 2 5.97602 2.47594 1 12 4 -2 3.43296 2.46408 2 12 4 -2 10.1490 2.61374 23 -12 4 2 7.58931 2.24846 22 -12 -4 -2 8.98217 2.47175 22 12 -4 2 6.50657 2.49437 23 12 -4 1 0.85581 2.29413 1 12 4 -1 0.49074 2.37258 2 -12 4 1 3.86242 2.10792 22 12 4 -1-0.39545 2.17617 23 -12 -4 -1 1.94114 2.26742 22 12 -4 1 1.64209 2.11146 23 12 -4 0 1.80221 2.44064 2 12 4 0 0.85372 2.25250 1 12 -4 0 6.85475 2.55233 1 12 4 0 0.98193 2.40251 2 -12 4 0 2.50096 2.12108 22 12 4 0 7.69032 2.37790 23 12 -4 0 3.31757 2.08124 23 -12 -4 0 2.70078 2.17368 22 12 -4 -1 0.45107 2.28472 2 12 4 1-0.42683 2.28737 1 12 -4 -1-2.57207 2.40195 1 -12 4 -1 1.81650 2.01115 22 12 4 1-2.99276 2.32640 23 12 -4 -1-0.41757 2.19268 23 -12 -4 1-2.68752 2.19048 22 -12 -4 2 8.48965 2.54342 15 12 -4 -2 4.50988 2.63644 2 12 4 2 10.6539 2.76108 1 -12 4 -2 6.65186 2.23924 22 12 4 2 5.82185 2.29657 23 12 -4 -2 5.90662 2.43137 23 -12 -4 2 6.87312 2.28563 22 -12 -4 3 2.71637 2.31280 15 12 -4 -3 4.50294 2.44578 2 12 4 3 9.77084 2.49793 1 -12 4 -3 5.63635 2.13069 22 12 4 3 6.01604 2.13830 23 12 -4 -3 2.98895 2.27736 23 -12 -4 3 7.22297 2.25500 22 -12 -4 4 15.1744 2.75802 15 12 -4 -4 8.54220 2.77716 2 12 4 4 10.1559 2.56617 1 12 -4 -4 11.8945 2.79341 1 12 4 4 15.8877 3.14235 2 -12 4 -4 11.8598 2.69625 22 12 4 4 12.3883 2.43002 23 12 -4 -4 13.3143 2.75774 23 -12 -4 5 0.39062 2.25723 15 12 -4 -5 6.71839 2.61305 2 12 4 5 4.21610 2.24483 1 12 -4 -5 5.49958 2.56492 1 12 4 5-0.47827 2.61009 2 -12 4 -5 5.43455 2.17821 22 12 4 5 5.01222 2.08491 23 -12 -4 6 8.21648 2.48001 15 12 -4 -6 12.0378 2.93947 2 12 4 6 12.1495 2.75751 1 12 -4 -6 5.47443 2.41823 1 12 4 6 8.07541 2.83456 2 -12 4 -6 5.50704 2.18922 22 12 4 6 7.73768 2.20148 23 -12 -4 7 2.74052 2.44396 15 12 -4 -7 6.18700 2.48215 2 12 4 7 7.89688 2.51419 1 12 -4 -7 7.08123 2.43936 1 12 4 7-0.47109 2.52820 2 -12 4 -7 2.39407 2.19079 22 12 4 7 5.63256 1.99207 23 -12 -4 8 2.44433 2.06302 7 12 4 8 2.72963 1.94337 23 -12 -4 8 0.39256 2.17426 15 12 -4 -8 0.82678 2.31768 1 12 4 8 0.46491 2.44215 2 12 4 9 2.64203 2.09031 23 12 -4 -9 3.50821 2.12754 10 12 -4 -10 0.39265 2.06059 10 -12 4 -11 3.02883 2.16455 18 -12 -5 -11 31.1455 3.66642 18 -12 -5 -10 2.56240 1.98003 18 -12 5 8 11.9279 2.42697 22 12 5 -7 2.67513 2.28145 23 -12 5 7 2.43791 1.88454 22 12 -5 6 8.29813 2.72937 2 12 5 -6 6.68755 2.47621 1 12 5 -6 12.7232 2.92287 23 -12 5 6 11.2044 2.20314 22 12 -5 5-1.75808 2.27715 2 12 5 -5 1.68205 2.17895 1 12 -5 5 2.51977 2.36901 1 12 5 -5 1.47030 2.46509 2 12 5 -5 3.43759 2.27348 23 -12 -5 -5 0.39820 2.19195 22 -12 5 5 3.49294 1.91765 22 12 -5 4 14.5799 2.84600 2 12 5 -4 5.92108 2.68244 1 12 -5 4 16.4552 2.94309 1 12 5 -4 8.37759 2.92355 2 12 5 -4 7.99134 2.57853 23 -12 5 4 9.40032 2.34576 22 -12 -5 -4 9.49278 2.58122 22 12 -5 3 8.05027 2.68495 1 12 5 -3 1.97882 2.48043 2 12 5 -3 4.51951 2.20143 23 -12 5 3 3.96880 1.96869 22 -12 -5 -3 0.78715 2.16554 22 12 -5 2 18.3502 3.09191 1 12 5 -2 22.3136 3.48241 2 12 5 -2 14.9157 2.89863 23 -12 5 2 15.2404 2.72696 22 -12 -5 -2 18.8201 3.01623 22 12 -5 1 2.56688 2.27625 1 12 5 -1-1.48975 2.53268 2 -12 5 1-1.72632 2.08151 22 12 5 -1-1.96323 2.21255 23 -12 -5 -1 3.51166 2.21189 22 12 -5 1 5.41240 2.28880 23 12 5 0 6.01417 2.36986 1 12 -5 0 5.56852 2.28774 1 12 5 0 2.48270 2.55402 2 -12 5 0-0.35178 2.13543 22 12 5 0 4.96017 2.22601 23 12 -5 0 6.70323 2.32685 23 -12 -5 0 2.71952 2.16136 22 12 -5 -1 1.79883 2.31231 2 12 5 1 3.00731 2.43707 1 12 -5 -1 2.14320 2.35820 1 -12 5 -1 3.22386 2.09224 22 12 5 1-0.37003 2.03642 23 12 -5 -1 1.26645 2.21748 23 -12 -5 1-0.38659 2.15398 22 -12 5 -2 12.0423 2.53695 22 12 5 2 14.3549 2.58914 23 12 -5 -2 15.3213 2.97436 23 -12 -5 2 16.5650 2.86060 22 12 -5 -2 15.7380 2.94389 2 12 5 2 15.4440 3.00699 1 -12 -5 2 9.85184 2.77146 15 -12 5 -3 2.60421 2.08466 22 12 5 3 2.78299 2.04224 23 12 -5 -3-0.42783 2.11791 23 12 -5 -3 1.79712 2.40729 2 12 5 3-0.42771 2.35209 1 -12 -5 3-0.39591 2.38749 15 -12 5 -4 9.81355 2.45106 22 12 5 4 8.76554 2.28023 23 12 -5 -4 14.3463 2.79413 2 12 5 4 8.94711 2.46140 1 12 -5 -4 8.04588 2.81274 1 12 5 4 8.79933 2.90792 2 -12 -5 4 8.75679 2.47786 15 -12 5 -5 0.76685 2.15156 22 12 5 5 2.27381 1.97300 23 12 -5 -5 2.68193 2.33322 2 12 5 5 5.08838 2.34944 1 12 -5 -5 0.84350 2.47811 1 12 5 5 0.48420 2.41801 2 -12 -5 5 0.79769 2.19658 15 -12 5 -6 11.6885 2.69791 22 12 5 6 8.48747 2.22847 23 12 5 6 8.65124 2.92978 2 -12 -5 6 11.1909 2.55565 15 -12 5 -7 3.55700 2.31842 22 12 5 7 3.03175 1.99008 23 12 5 8 11.6768 2.35522 23 -12 5 -11 22.0253 3.10309 18 -12 -6 -10 13.7511 2.43152 18 -12 -6 -10 9.31766 2.23337 11 -12 -6 -9 7.25307 2.16746 11 -12 -6 -8 3.91843 1.90596 11 -12 -6 -7 5.17226 2.04566 11 -12 -6 -6 5.44358 2.12637 11 12 6 -6 7.39169 2.31247 23 -12 6 6 8.73438 2.10938 22 -12 -6 -5 0.31716 1.90241 11 12 6 -5 2.13584 2.19500 23 -12 6 5 0.30805 1.79800 22 -12 -6 -4 6.60643 2.08602 11 12 6 -4 4.17187 2.45475 23 -12 6 4 11.0789 2.29014 22 -12 -6 -3 8.11527 2.18080 11 12 6 -3 11.0020 2.65291 23 -12 6 3 8.09634 2.28190 22 -12 -6 -2 1.23472 1.89031 11 12 6 -2-1.98648 2.18425 23 -12 6 2 1.98441 1.99405 22 -12 -6 -1 4.29303 1.94223 11 -12 6 1 4.72810 2.02020 22 12 6 -1 2.33324 2.19329 23 -12 -6 -1 2.35340 2.10289 22 -12 -6 0 5.18157 1.93794 11 -12 6 0 3.10270 2.01257 22 12 6 0 5.28711 2.24933 23 12 -6 0 2.12460 2.17314 23 -12 -6 0 2.34455 2.21008 22 12 -6 0 5.41013 2.58909 2 12 6 0 7.35493 2.52892 1 12 6 0 3.51589 2.46531 2 -12 -6 1 0.60742 1.77366 11 12 -6 -1 4.51361 2.42589 2 -12 6 -1 0.35167 1.96789 22 12 6 1 4.02400 2.16767 23 12 -6 -1 3.84337 2.32630 23 -12 -6 1 5.45070 2.20298 22 -12 6 -2-0.35855 2.02320 22 12 6 2 1.76780 2.08876 23 12 -6 -2 3.43172 2.19040 23 -12 6 -3 8.05213 2.37964 22 12 6 3 9.83927 2.26726 23 -12 -6 3 6.85289 2.47047 15 -12 6 -4 5.95723 2.33714 22 12 6 4 3.27905 2.00351 23 -12 6 -5 0.37877 2.18507 22 12 6 5 0.63342 1.97840 23 12 6 6 6.41160 1.99277 23 12 6 7 1.75242 1.85537 23 -12 -7 -8 3.75427 2.07607 11 -12 -7 -7 11.1624 2.41051 11 -12 -7 -6-1.34010 2.02181 11 -12 -7 -5 0.33203 2.00526 11 12 7 -5 1.68795 2.23318 23 -12 7 5 3.58762 2.04598 22 -12 -7 -4 0.65928 1.88198 11 12 7 -4 1.65482 2.06497 23 -12 7 4 1.84128 1.96552 22 -12 -7 -3 4.57917 1.90517 11 12 7 -3 3.62825 2.26836 23 -12 7 3 5.03536 2.03126 22 -12 -7 -2 5.19887 2.09655 11 12 7 -2 6.28217 2.24294 23 -12 7 2 6.44231 2.15419 22 -12 -7 -1 1.28678 1.90968 11 -12 7 1 3.96715 1.99301 22 -12 -7 0-0.95950 1.88677 11 -12 7 0-0.33796 2.15174 22 12 7 0 1.48082 2.21962 23 -12 -7 1 2.86754 1.91810 11 -12 7 -1 3.45314 2.02196 22 12 7 1 0.35779 2.12923 23 -12 -7 2 4.76705 2.08483 11 -12 7 -2 6.00095 2.30685 22 12 7 2 6.20914 2.17385 23 -12 -7 3 6.95721 2.04875 11 -12 7 -3 4.31647 2.15551 22 12 7 3 3.98960 1.97624 23 -12 -7 4 2.19546 1.91597 11 -12 7 -4 0.73149 2.02174 22 -12 -7 5 1.25113 1.82836 11 12 7 5 1.83803 1.79084 23 -12 -8 -4 1.37520 1.95127 11 -12 -8 -3 3.07144 1.99955 11 12 8 -3 6.37375 2.30785 23 -12 8 3 7.31545 2.01896 22 -12 -8 -2 10.5133 2.48831 11 12 8 -2 17.0370 2.94988 23 -12 8 2 16.3239 2.53171 22 -12 -8 -1 3.03270 2.13169 11 -12 8 1 7.07574 2.11522 22 12 8 -1 9.77512 2.45761 23 -12 -8 0 32.3954 3.68521 11 -12 8 0 31.9565 3.70157 22 12 8 0 32.0695 3.79698 23 -12 -8 1 9.98594 2.41004 11 -12 8 -1 9.77584 2.42885 22 12 8 1 10.2054 2.35095 23 -12 -8 2 11.2804 2.47792 11 -12 8 -2 11.7384 2.67943 22 -12 -8 3 4.62534 2.04104 11 12 8 3 4.55240 2.09835 23 -12 -8 4 3.28835 1.99765 11 12 8 4 3.40780 2.04277 23 -12 -8 5 6.20446 2.17718 11 12 9 -1 1.83775 2.07526 23 12 9 0-1.77745 2.20234 23 12 9 1 3.42471 2.12261 23 12 9 2 0.65769 1.99309 23 0 0 0 0.00 0.00 0 TITL M4_Mo in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 0.71073 7.420443 14.963430 22.757981 90.0000 90.0000 90.0000 ZERR 4.00 0.000085 0.000201 0.000267 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O S UNIT 92.00 108.00 12.00 20.00 4.00 REM CrysAlisPro recorded range (K): Min=99.3; max=100.5; aver:99.9 TEMP -173 TREF HKLF 4 END ; _shelx_hkl_checksum 25121 _shelx_res_file ; TITL M4_Mo in P2(1)2(1)2(1) shelx.res created by SHELXL-2019/3 at 11:01:03 on 23-May-2024 CELL 0.71073 7.420443 14.963430 22.757981 90.0000 90.0000 90.0000 ZERR 4.00 0.00017 0.0004 0.00054 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O S UNIT 92 108 12 36 4 TEMP -173 SIZE 0.15 0.05 0.04 SHEL 999 0.6 OMIT 0 7 3 OMIT 4 6 0 OMIT 5 0 8 L.S. 6 FMAP 2 PLAN 10 ACTA 72 CONF BOND $H REM Instructions for potential hydrogen bonds EQIV $1 x-1, y, z HTAB N1 N3_$1 HTAB C14 O1_$1 HTAB C4 O7_$1 HTAB C5 N3_$1 EQIV $2 -x, y-1/2, -z+3/2 HTAB C1 O10_$2 HTAB C25 O9_$2 EQIV $3 x+1/2, -y+1/2, -z+2 HTAB C10 O9_$3 EQIV $4 x-1/2, -y+1/2, -z+2 HTAB C10 O3_$4 HTAB C12 O8_$3 WGHT 0.058900 0.121700 FVAR 0.30735 C1 1 0.377325 0.229501 0.768888 11.00000 0.01087 0.01613 = 0.01283 -0.00130 0.00087 -0.00025 AFIX 13 H1 2 0.305633 0.178158 0.753244 11.00000 -1.20000 AFIX 0 C2 1 0.411954 0.217949 0.835313 11.00000 0.01083 0.01447 = 0.01317 -0.00123 0.00063 0.00069 AFIX 13 H2 2 0.493689 0.266177 0.849975 11.00000 -1.20000 AFIX 0 C3 1 0.231431 0.221609 0.867351 11.00000 0.01233 0.01616 = 0.01101 -0.00130 0.00084 -0.00133 AFIX 13 H3 2 0.156478 0.168366 0.856960 11.00000 -1.20000 AFIX 0 C4 1 0.131133 0.307604 0.852092 11.00000 0.01026 0.01519 = 0.01493 -0.00229 0.00025 -0.00124 AFIX 13 H4 2 0.008781 0.307097 0.870508 11.00000 -1.20000 AFIX 0 C5 1 0.113973 0.315254 0.785773 11.00000 0.01015 0.01716 = 0.01518 -0.00012 -0.00011 0.00031 AFIX 13 H5 2 0.036989 0.265376 0.770766 11.00000 -1.20000 AFIX 0 C6 1 0.038359 0.403604 0.764584 11.00000 0.01297 0.02067 = 0.02302 0.00348 0.00034 0.00282 AFIX 23 H6A 2 0.114753 0.453639 0.778354 11.00000 -1.20000 H6B 2 0.034313 0.404954 0.721112 11.00000 -1.20000 AFIX 0 C7 1 0.671692 0.129107 0.855308 11.00000 0.01480 0.02226 = 0.01687 -0.00255 -0.00251 0.00345 C8 1 0.731936 0.035662 0.867405 11.00000 0.02448 0.02243 = 0.04674 -0.00368 -0.01091 0.00833 AFIX 137 H8A 2 0.712097 0.021643 0.908968 11.00000 -1.50000 H8B 2 0.860457 0.029971 0.858225 11.00000 -1.50000 H8C 2 0.662784 -0.005941 0.842957 11.00000 -1.50000 AFIX 0 C9 1 0.156138 0.175553 0.964767 11.00000 0.01530 0.02195 = 0.01331 0.00266 0.00159 0.00208 C10 1 0.182934 0.200079 1.027755 11.00000 0.01839 0.03750 = 0.01301 0.00037 0.00088 0.00252 AFIX 137 H10A 2 0.309037 0.216918 1.034168 11.00000 -1.50000 H10B 2 0.152722 0.148837 1.052697 11.00000 -1.50000 H10C 2 0.104629 0.250583 1.037745 11.00000 -1.50000 AFIX 0 C11 1 0.182204 0.418011 0.926420 11.00000 0.01950 0.01807 = 0.02113 -0.00570 0.00189 -0.00029 C12 1 0.305872 0.490474 0.946015 11.00000 0.02757 0.01947 = 0.02280 -0.00414 -0.00359 -0.00370 AFIX 137 H12A 2 0.393763 0.466129 0.973886 11.00000 -1.50000 H12B 2 0.235980 0.537817 0.965146 11.00000 -1.50000 H12C 2 0.369274 0.515173 0.911908 11.00000 -1.50000 AFIX 0 C13 1 -0.234409 0.481850 0.767806 11.00000 0.01652 0.01676 = 0.02819 -0.00479 -0.00500 0.00290 C14 1 -0.422025 0.481915 0.792430 11.00000 0.01582 0.02273 = 0.04872 -0.00607 0.00024 0.00236 AFIX 137 H14A 2 -0.488383 0.430260 0.777176 11.00000 -1.50000 H14B 2 -0.483761 0.537043 0.780799 11.00000 -1.50000 H14C 2 -0.416446 0.478483 0.835394 11.00000 -1.50000 AFIX 0 C15 1 0.561880 0.204575 0.659709 11.00000 0.00990 0.01736 = 0.01279 -0.00032 0.00012 -0.00018 C16 1 0.868486 0.197251 0.652289 11.00000 0.01212 0.02894 = 0.01243 -0.00341 0.00116 0.00082 C21 1 0.368875 0.167073 0.576474 11.00000 0.01061 0.01957 = 0.01382 -0.00027 -0.00128 0.00056 C22 1 0.460868 0.205696 0.529581 11.00000 0.01447 0.02406 = 0.01558 0.00312 -0.00285 -0.00406 AFIX 43 H22 2 0.544346 0.252735 0.536297 11.00000 -1.20000 AFIX 0 C23 1 0.429587 0.174864 0.472813 11.00000 0.01733 0.02880 = 0.01368 0.00320 -0.00165 -0.00153 AFIX 43 H23 2 0.494175 0.200657 0.441010 11.00000 -1.20000 AFIX 0 C24 1 0.305849 0.107106 0.461553 11.00000 0.01710 0.02363 = 0.01545 -0.00204 -0.00262 0.00311 C25 1 0.213095 0.069762 0.509049 11.00000 0.01710 0.02078 = 0.01879 -0.00273 -0.00199 -0.00116 AFIX 43 H25 2 0.127528 0.023683 0.502248 11.00000 -1.20000 AFIX 0 C26 1 0.244420 0.099185 0.566191 11.00000 0.01320 0.02104 = 0.01736 -0.00042 -0.00044 -0.00129 AFIX 43 H26 2 0.181007 0.072996 0.598105 11.00000 -1.20000 AFIX 0 C27 1 0.269323 0.075821 0.399710 11.00000 0.03084 0.03261 = 0.01744 -0.00410 -0.00410 -0.00012 AFIX 137 H27A 2 0.262273 0.010429 0.399076 11.00000 -1.50000 H27B 2 0.367052 0.095674 0.373854 11.00000 -1.50000 H27C 2 0.154905 0.101027 0.386004 11.00000 -1.50000 AFIX 0 S1 5 0.595554 0.234702 0.733623 11.00000 0.01011 0.02345 = 0.01230 -0.00367 0.00084 -0.00192 O1 4 0.287524 0.311294 0.757968 11.00000 0.01189 0.01697 = 0.01538 0.00136 0.00111 0.00072 O2 4 0.489235 0.131889 0.846436 11.00000 0.01301 0.01615 = 0.01820 -0.00054 -0.00168 0.00124 O3 4 0.269922 0.222119 0.929183 11.00000 0.01525 0.02422 = 0.01032 -0.00039 0.00038 -0.00303 O4 4 0.233581 0.382789 0.873730 11.00000 0.01415 0.01617 = 0.01666 -0.00339 0.00045 -0.00208 O6 4 -0.140135 0.411447 0.788367 11.00000 0.01334 0.02044 = 0.03053 0.00425 0.00061 0.00353 O7 4 0.766187 0.193859 0.852719 11.00000 0.01527 0.02597 = 0.02298 -0.00147 -0.00282 -0.00095 O8 4 0.046615 0.123603 0.946370 11.00000 0.03432 0.03929 = 0.01908 0.00461 0.00039 -0.01932 O9 4 0.053549 0.391906 0.953813 11.00000 0.02880 0.03493 = 0.03473 -0.01617 0.01563 -0.00878 O10 4 -0.172347 0.535615 0.734211 11.00000 0.02905 0.02460 = 0.03665 0.00682 0.00043 0.00772 N1 3 0.398886 0.196286 0.635905 11.00000 0.00940 0.02259 = 0.01351 -0.00163 -0.00099 -0.00044 H01 2 0.304806 0.197011 0.658428 11.00000 0.02868 N2 3 0.707770 0.190050 0.628010 11.00000 0.00943 0.02657 = 0.01275 -0.00333 -0.00009 0.00086 N3 3 1.017351 0.203146 0.668042 11.00000 0.01183 0.04338 = 0.01843 -0.00445 0.00030 0.00051 HKLF 4 REM M4_Mo in P2(1)2(1)2(1) REM wR2 = 0.0944, GooF = S = 1.041, Restrained GooF = 1.041 for all data REM R1 = 0.0359 for 11008 Fo > 4sig(Fo) and 0.0426 for all 12241 data REM 334 parameters refined using 0 restraints END WGHT 0.0589 0.1217 REM Highest difference peak 0.452, deepest hole -0.214, 1-sigma level 0.058 Q1 1 0.0204 0.4201 0.9304 11.00000 0.05 0.45 Q2 1 0.4378 0.1969 0.5000 11.00000 0.05 0.42 Q3 1 0.4220 0.1880 0.5557 11.00000 0.05 0.41 Q4 1 0.3038 0.1348 0.5718 11.00000 0.05 0.41 Q5 1 0.2201 0.0821 0.5390 11.00000 0.05 0.41 Q6 1 0.0801 0.3584 0.7740 11.00000 0.05 0.40 Q7 1 0.1789 0.1850 0.9951 11.00000 0.05 0.39 Q8 1 0.2806 0.0941 0.4315 11.00000 0.05 0.39 Q9 1 0.4848 0.2023 0.6466 11.00000 0.05 0.38 Q10 1 0.3688 0.1437 0.4681 11.00000 0.05 0.38 ; _shelx_res_checksum 10757 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.37733(14) 0.22950(8) 0.76889(5) 0.01328(17) Uani d 1 . . H H1 0.305633 0.178158 0.753244 0.016 Uiso calc 1 . . C C2 0.41195(15) 0.21795(8) 0.83531(5) 0.01282(17) Uani d 1 . . H H2 0.493689 0.266177 0.849975 0.015 Uiso calc 1 . . C C3 0.23143(15) 0.22161(8) 0.86735(5) 0.01317(18) Uani d 1 . . H H3 0.156478 0.168366 0.856960 0.016 Uiso calc 1 . . C C4 0.13113(15) 0.30760(8) 0.85209(5) 0.01346(18) Uani d 1 . . H H4 0.008781 0.307097 0.870508 0.016 Uiso calc 1 . . C C5 0.11397(15) 0.31525(8) 0.78577(5) 0.01416(18) Uani d 1 . . H H5 0.036989 0.265376 0.770766 0.017 Uiso calc 1 . . C C6 0.03836(17) 0.40360(9) 0.76458(6) 0.0189(2) Uani d 1 . . H H6A 0.114753 0.453639 0.778354 0.023 Uiso calc 1 . . H H6B 0.034313 0.404954 0.721112 0.023 Uiso calc 1 . . C C7 0.67169(18) 0.12911(9) 0.85531(6) 0.0180(2) Uani d 1 . . C C8 0.7319(2) 0.03566(11) 0.86740(9) 0.0312(3) Uani d 1 . . H H8A 0.712097 0.021643 0.908968 0.047 Uiso calc 1 . . H H8B 0.860457 0.029971 0.858225 0.047 Uiso calc 1 . . H H8C 0.662784 -0.005941 0.842957 0.047 Uiso calc 1 . . C C9 0.15614(17) 0.17555(9) 0.96477(5) 0.0169(2) Uani d 1 . . C C10 0.18293(19) 0.20008(11) 1.02776(6) 0.0230(3) Uani d 1 . . H H10A 0.309037 0.216918 1.034168 0.034 Uiso calc 1 . . H H10B 0.152722 0.148837 1.052697 0.034 Uiso calc 1 . . H H10C 0.104629 0.250583 1.037745 0.034 Uiso calc 1 . . C C11 0.18220(19) 0.41801(9) 0.92642(6) 0.0196(2) Uani d 1 . . C C12 0.3059(2) 0.49047(10) 0.94601(7) 0.0233(3) Uani d 1 . . H H12A 0.393763 0.466129 0.973886 0.035 Uiso calc 1 . . H H12B 0.235980 0.537817 0.965146 0.035 Uiso calc 1 . . H H12C 0.369274 0.515173 0.911908 0.035 Uiso calc 1 . . C C13 -0.23441(18) 0.48185(9) 0.76781(7) 0.0205(2) Uani d 1 . . C C14 -0.4220(2) 0.48191(11) 0.79243(9) 0.0291(3) Uani d 1 . . H H14A -0.488383 0.430260 0.777176 0.044 Uiso calc 1 . . H H14B -0.483761 0.537043 0.780799 0.044 Uiso calc 1 . . H H14C -0.416446 0.478483 0.835394 0.044 Uiso calc 1 . . C C15 0.56188(15) 0.20458(8) 0.65971(5) 0.01335(18) Uani d 1 . . C C16 0.86849(16) 0.19725(10) 0.65229(5) 0.0178(2) Uani d 1 . . C C21 0.36887(15) 0.16707(8) 0.57647(5) 0.01467(19) Uani d 1 . . C C22 0.46087(17) 0.20570(9) 0.52958(5) 0.0180(2) Uani d 1 . . H H22 0.544346 0.252735 0.536297 0.022 Uiso calc 1 . . C C23 0.42959(18) 0.17486(10) 0.47281(6) 0.0199(2) Uani d 1 . . H H23 0.494175 0.200657 0.441010 0.024 Uiso calc 1 . . C C24 0.30585(18) 0.10711(9) 0.46155(6) 0.0187(2) Uani d 1 . . C C25 0.21309(19) 0.06976(9) 0.50905(6) 0.0189(2) Uani d 1 . . H H25 0.127528 0.023683 0.502248 0.023 Uiso calc 1 . . C C26 0.24442(17) 0.09919(9) 0.56619(5) 0.0172(2) Uani d 1 . . H H26 0.181007 0.072996 0.598105 0.021 Uiso calc 1 . . C C27 0.2693(2) 0.07582(11) 0.39971(6) 0.0270(3) Uani d 1 . . H H27A 0.262273 0.010429 0.399076 0.040 Uiso calc 1 . . H H27B 0.367052 0.095674 0.373854 0.040 Uiso calc 1 . . H H27C 0.154905 0.101027 0.386004 0.040 Uiso calc 1 . . S S1 0.59555(4) 0.23470(2) 0.73362(2) 0.01528(6) Uani d 1 . . O O1 0.28752(12) 0.31129(6) 0.75797(4) 0.01475(15) Uani d 1 . . O O2 0.48923(13) 0.13189(6) 0.84644(4) 0.01579(16) Uani d 1 . . O O3 0.26992(13) 0.22212(7) 0.92918(4) 0.01660(16) Uani d 1 . . O O4 0.23358(13) 0.38279(6) 0.87373(4) 0.01566(15) Uani d 1 . . O O6 -0.14014(13) 0.41145(7) 0.78837(5) 0.02144(19) Uani d 1 . . O O7 0.76619(13) 0.19386(7) 0.85272(5) 0.02141(18) Uani d 1 . . O O8 0.04661(18) 0.12360(9) 0.94637(5) 0.0309(3) Uani d 1 . . O O9 0.05355(18) 0.39191(9) 0.95381(6) 0.0328(3) Uani d 1 . . O O10 -0.17235(17) 0.53562(8) 0.73421(6) 0.0301(2) Uani d 1 . . N N1 0.39889(14) 0.19629(8) 0.63591(4) 0.01517(17) Uani d 1 . . H H01 0.305(3) 0.1970(15) 0.6584(10) 0.029(6) Uiso d 1 . . N N2 0.70777(13) 0.19005(8) 0.62801(4) 0.01625(18) Uani d 1 . . N N3 1.01735(16) 0.20315(10) 0.66804(5) 0.0245(2) Uani d 1 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0109(4) 0.0161(4) 0.0128(4) -0.0002(4) 0.0009(3) -0.0013(4) C2 0.0108(4) 0.0145(4) 0.0132(4) 0.0007(4) 0.0006(3) -0.0012(3) C3 0.0123(4) 0.0162(4) 0.0110(4) -0.0013(4) 0.0008(3) -0.0013(3) C4 0.0103(4) 0.0152(4) 0.0149(4) -0.0012(4) 0.0003(3) -0.0023(4) C5 0.0102(4) 0.0172(5) 0.0152(4) 0.0003(4) -0.0001(3) -0.0001(4) C6 0.0130(4) 0.0207(5) 0.0230(5) 0.0028(4) 0.0003(4) 0.0035(4) C7 0.0148(5) 0.0223(5) 0.0169(5) 0.0034(4) -0.0025(4) -0.0026(4) C8 0.0245(7) 0.0224(6) 0.0467(9) 0.0083(5) -0.0109(7) -0.0037(6) C9 0.0153(5) 0.0220(5) 0.0133(4) 0.0021(4) 0.0016(4) 0.0027(4) C10 0.0184(5) 0.0375(7) 0.0130(5) 0.0025(5) 0.0009(4) 0.0004(5) C11 0.0195(5) 0.0181(5) 0.0211(5) -0.0003(4) 0.0019(4) -0.0057(4) C12 0.0276(7) 0.0195(5) 0.0228(6) -0.0037(5) -0.0036(5) -0.0041(5) C13 0.0165(5) 0.0168(5) 0.0282(6) 0.0029(4) -0.0050(5) -0.0048(5) C14 0.0158(6) 0.0227(6) 0.0487(9) 0.0024(5) 0.0002(6) -0.0061(6) C15 0.0099(4) 0.0174(5) 0.0128(4) -0.0002(4) 0.0001(3) -0.0003(3) C16 0.0121(4) 0.0289(6) 0.0124(4) 0.0008(4) 0.0012(3) -0.0034(4) C21 0.0106(4) 0.0196(5) 0.0138(4) 0.0006(4) -0.0013(3) -0.0003(4) C22 0.0145(5) 0.0241(6) 0.0156(5) -0.0041(4) -0.0028(4) 0.0031(4) C23 0.0173(5) 0.0288(6) 0.0137(5) -0.0015(5) -0.0017(4) 0.0032(4) C24 0.0171(5) 0.0236(6) 0.0155(5) 0.0031(4) -0.0026(4) -0.0020(4) C25 0.0171(5) 0.0208(5) 0.0188(5) -0.0012(4) -0.0020(4) -0.0027(4) C26 0.0132(5) 0.0210(5) 0.0174(5) -0.0013(4) -0.0004(4) -0.0004(4) C27 0.0308(7) 0.0326(7) 0.0174(5) -0.0001(6) -0.0041(5) -0.0041(5) S1 0.01011(10) 0.02345(13) 0.01230(10) -0.00192(10) 0.00084(8) -0.00367(9) O1 0.0119(3) 0.0170(4) 0.0154(4) 0.0007(3) 0.0011(3) 0.0014(3) O2 0.0130(3) 0.0162(4) 0.0182(4) 0.0012(3) -0.0017(3) -0.0005(3) O3 0.0152(4) 0.0242(4) 0.0103(3) -0.0030(3) 0.0004(3) -0.0004(3) O4 0.0142(4) 0.0162(4) 0.0167(4) -0.0021(3) 0.0004(3) -0.0034(3) O6 0.0133(4) 0.0204(4) 0.0305(5) 0.0035(3) 0.0006(4) 0.0043(4) O7 0.0153(4) 0.0260(5) 0.0230(4) -0.0010(4) -0.0028(3) -0.0015(4) O8 0.0343(6) 0.0393(6) 0.0191(4) -0.0193(5) 0.0004(4) 0.0046(4) O9 0.0288(6) 0.0349(6) 0.0347(6) -0.0088(5) 0.0156(5) -0.0162(5) O10 0.0291(5) 0.0246(5) 0.0366(6) 0.0077(4) 0.0004(5) 0.0068(5) N1 0.0094(4) 0.0226(5) 0.0135(4) -0.0004(4) -0.0010(3) -0.0016(3) N2 0.0094(4) 0.0266(5) 0.0128(4) 0.0009(4) -0.0001(3) -0.0033(4) N3 0.0118(4) 0.0434(7) 0.0184(5) 0.0005(5) 0.0003(3) -0.0045(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 C1 C2 . . 110.32(9) ? O1 C1 S1 . . 107.84(8) ? C2 C1 S1 . . 106.88(7) ? O1 C1 H1 . . 110.6 ? C2 C1 H1 . . 110.6 ? S1 C1 H1 . . 110.6 ? O2 C2 C3 . . 107.41(9) ? O2 C2 C1 . . 109.91(9) ? C3 C2 C1 . . 108.53(9) ? O2 C2 H2 . . 110.3 ? C3 C2 H2 . . 110.3 ? C1 C2 H2 . . 110.3 ? O3 C3 C2 . . 107.09(9) ? O3 C3 C4 . . 108.39(9) ? C2 C3 C4 . . 110.46(9) ? O3 C3 H3 . . 110.3 ? C2 C3 H3 . . 110.3 ? C4 C3 H3 . . 110.3 ? O4 C4 C5 . . 108.92(10) ? O4 C4 C3 . . 108.81(9) ? C5 C4 C3 . . 109.29(9) ? O4 C4 H4 . . 109.9 ? C5 C4 H4 . . 109.9 ? C3 C4 H4 . . 109.9 ? O1 C5 C6 . . 103.17(10) ? O1 C5 C4 . . 111.07(9) ? C6 C5 C4 . . 114.40(10) ? O1 C5 H5 . . 109.3 ? C6 C5 H5 . . 109.3 ? C4 C5 H5 . . 109.3 ? O6 C6 C5 . . 107.04(10) ? O6 C6 H6A . . 110.3 ? C5 C6 H6A . . 110.3 ? O6 C6 H6B . . 110.3 ? C5 C6 H6B . . 110.3 ? H6A C6 H6B . . 108.6 ? O7 C7 O2 . . 123.16(13) ? O7 C7 C8 . . 126.25(13) ? O2 C7 C8 . . 110.58(12) ? C7 C8 H8A . . 109.5 ? C7 C8 H8B . . 109.5 ? H8A C8 H8B . . 109.5 ? C7 C8 H8C . . 109.5 ? H8A C8 H8C . . 109.5 ? H8B C8 H8C . . 109.5 ? O8 C9 O3 . . 122.95(12) ? O8 C9 C10 . . 125.76(13) ? O3 C9 C10 . . 111.26(12) ? C9 C10 H10A . . 109.5 ? C9 C10 H10B . . 109.5 ? H10A C10 H10B . . 109.5 ? C9 C10 H10C . . 109.5 ? H10A C10 H10C . . 109.5 ? H10B C10 H10C . . 109.5 ? O9 C11 O4 . . 123.42(13) ? O9 C11 C12 . . 124.70(13) ? O4 C11 C12 . . 111.86(12) ? C11 C12 H12A . . 109.5 ? C11 C12 H12B . . 109.5 ? H12A C12 H12B . . 109.5 ? C11 C12 H12C . . 109.5 ? H12A C12 H12C . . 109.5 ? H12B C12 H12C . . 109.5 ? O10 C13 O6 . . 123.03(13) ? O10 C13 C14 . . 126.35(13) ? O6 C13 C14 . . 110.62(13) ? C13 C14 H14A . . 109.5 ? C13 C14 H14B . . 109.5 ? H14A C14 H14B . . 109.5 ? C13 C14 H14C . . 109.5 ? H14A C14 H14C . . 109.5 ? H14B C14 H14C . . 109.5 ? N2 C15 N1 . . 120.52(10) ? N2 C15 S1 . . 116.65(9) ? N1 C15 S1 . . 122.82(9) ? N3 C16 N2 . . 173.13(13) ? C22 C21 C26 . . 119.94(11) ? C22 C21 N1 . . 121.23(11) ? C26 C21 N1 . . 118.83(11) ? C23 C22 C21 . . 119.49(12) ? C23 C22 H22 . . 120.3 ? C21 C22 H22 . . 120.3 ? C22 C23 C24 . . 121.51(12) ? C22 C23 H23 . . 119.2 ? C24 C23 H23 . . 119.2 ? C23 C24 C25 . . 118.27(11) ? C23 C24 C27 . . 121.11(13) ? C25 C24 C27 . . 120.61(13) ? C26 C25 C24 . . 120.90(12) ? C26 C25 H25 . . 119.6 ? C24 C25 H25 . . 119.6 ? C25 C26 C21 . . 119.88(12) ? C25 C26 H26 . . 120.1 ? C21 C26 H26 . . 120.1 ? C24 C27 H27A . . 109.5 ? C24 C27 H27B . . 109.5 ? H27A C27 H27B . . 109.5 ? C24 C27 H27C . . 109.5 ? H27A C27 H27C . . 109.5 ? H27B C27 H27C . . 109.5 ? C15 S1 C1 . . 106.62(5) y C1 O1 C5 . . 112.36(9) ? C7 O2 C2 . . 116.69(10) ? C9 O3 C3 . . 117.18(10) ? C11 O4 C4 . . 116.97(10) ? C13 O6 C6 . . 114.31(11) ? C15 N1 C21 . . 123.47(10) ? C15 N1 H01 . . 119.4(15) ? C21 N1 H01 . . 115.8(16) ? C16 N2 C15 . . 119.97(10) ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag C1 O1 . 1.4155(15) ? C1 C2 . 1.5431(16) ? C1 S1 . 1.8090(11) y C1 H1 . 1.0000 ? C2 O2 . 1.4322(15) ? C2 C3 . 1.5261(16) ? C2 H2 . 1.0000 ? C3 O3 . 1.4359(14) ? C3 C4 . 1.5265(17) ? C3 H3 . 1.0000 ? C4 O4 . 1.4443(14) ? C4 C5 . 1.5190(16) ? C4 H4 . 1.0000 ? C5 O1 . 1.4361(14) ? C5 C6 . 1.5150(17) ? C5 H5 . 1.0000 ? C6 O6 . 1.4356(16) ? C6 H6A . 0.9900 ? C6 H6B . 0.9900 ? C7 O7 . 1.1975(18) ? C7 O2 . 1.3695(16) ? C7 C8 . 1.494(2) ? C8 H8A . 0.9800 ? C8 H8B . 0.9800 ? C8 H8C . 0.9800 ? C9 O8 . 1.2000(18) ? C9 O3 . 1.3617(15) ? C9 C10 . 1.4930(18) ? C10 H10A . 0.9800 ? C10 H10B . 0.9800 ? C10 H10C . 0.9800 ? C11 O9 . 1.2052(18) ? C11 O4 . 1.3642(16) ? C11 C12 . 1.489(2) ? C12 H12A . 0.9800 ? C12 H12B . 0.9800 ? C12 H12C . 0.9800 ? C13 O10 . 1.2016(19) ? C13 O6 . 1.3484(16) ? C13 C14 . 1.501(2) ? C14 H14A . 0.9800 ? C14 H14B . 0.9800 ? C14 H14C . 0.9800 ? C15 N2 . 1.3190(15) y C15 N1 . 1.3311(15) y C15 S1 . 1.7593(12) y C16 N3 . 1.1647(16) ? C16 N2 . 1.3188(16) y C21 C22 . 1.3924(17) ? C21 C26 . 1.3927(17) ? C21 N1 . 1.4388(16) y C22 C23 . 1.3913(18) ? C22 H22 . 0.9500 ? C23 C24 . 1.3917(19) ? C23 H23 . 0.9500 ? C24 C25 . 1.3980(19) ? C24 C27 . 1.5078(19) ? C25 C26 . 1.3925(18) ? C25 H25 . 0.9500 ? C26 H26 . 0.9500 ? C27 H27A . 0.9800 ? C27 H27B . 0.9800 ? C27 H27C . 0.9800 ? N1 H01 . 0.87(2) ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_site_symmetry_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_publ_flag N1 H01 N3 1_455 0.87(2) 2.15(2) 2.9259(16) 150(2) yes C14 H14A O1 1_455 0.98 2.47 3.4320(18) 165.3 yes C4 H4 O7 1_455 1.00 2.51 3.1985(15) 126.1 yes C5 H5 N3 1_455 1.00 2.52 3.2414(17) 128.7 yes C1 H1 O10 3_546 1.00 2.37 3.2765(16) 150.6 yes C25 H25 O9 3_546 0.95 2.59 3.4223(19) 146.9 yes C10 H10A O9 4_557 0.98 2.45 3.1038(19) 123.5 yes C10 H10C O3 4_457 0.98 2.63 3.4217(17) 138.3 yes C12 H12A O8 4_557 0.98 2.53 3.4790(19) 164.0 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion _geom_torsion_publ_flag O1 C1 C2 O2 . . . . 175.24(9) ? S1 C1 C2 O2 . . . . -67.78(10) ? O1 C1 C2 C3 . . . . 58.03(12) ? S1 C1 C2 C3 . . . . 175.02(7) ? O2 C2 C3 O3 . . . . 68.38(11) ? C1 C2 C3 O3 . . . . -172.83(9) ? O2 C2 C3 C4 . . . . -173.79(9) ? C1 C2 C3 C4 . . . . -55.00(12) ? O3 C3 C4 O4 . . . . 52.67(12) ? C2 C3 C4 O4 . . . . -64.35(11) ? O3 C3 C4 C5 . . . . 171.50(9) ? C2 C3 C4 C5 . . . . 54.47(12) ? O4 C4 C5 O1 . . . . 62.60(12) ? C3 C4 C5 O1 . . . . -56.15(12) ? O4 C4 C5 C6 . . . . -53.69(12) ? C3 C4 C5 C6 . . . . -172.44(10) ? O1 C5 C6 O6 . . . . 177.48(10) ? C4 C5 C6 O6 . . . . -61.75(13) y C26 C21 C22 C23 . . . . -1.10(19) ? N1 C21 C22 C23 . . . . 179.26(12) ? C21 C22 C23 C24 . . . . 1.1(2) ? C22 C23 C24 C25 . . . . -0.4(2) ? C22 C23 C24 C27 . . . . 178.37(13) ? C23 C24 C25 C26 . . . . -0.4(2) ? C27 C24 C25 C26 . . . . -179.13(13) ? C24 C25 C26 C21 . . . . 0.4(2) ? C22 C21 C26 C25 . . . . 0.37(19) ? N1 C21 C26 C25 . . . . -179.98(12) ? N2 C15 S1 C1 . . . . -169.48(10) ? N1 C15 S1 C1 . . . . 10.44(12) y O1 C1 S1 C15 . . . . -83.66(8) y C2 C1 S1 C15 . . . . 157.73(8) ? C2 C1 O1 C5 . . . . -61.80(12) ? S1 C1 O1 C5 . . . . -178.19(7) y C6 C5 O1 C1 . . . . -175.80(10) ? C4 C5 O1 C1 . . . . 61.19(12) ? O7 C7 O2 C2 . . . . -1.84(18) y C8 C7 O2 C2 . . . . 178.96(12) ? C3 C2 O2 C7 . . . . -141.16(10) ? C1 C2 O2 C7 . . . . 100.94(12) y O8 C9 O3 C3 . . . . 12.60(19) y C10 C9 O3 C3 . . . . -165.63(11) ? C2 C3 O3 C9 . . . . -142.63(10) y C4 C3 O3 C9 . . . . 98.19(12) ? O9 C11 O4 C4 . . . . -3.0(2) y C12 C11 O4 C4 . . . . 175.80(11) ? C5 C4 O4 C11 . . . . 143.06(11) ? C3 C4 O4 C11 . . . . -97.88(12) y O10 C13 O6 C6 . . . . -2.8(2) y C14 C13 O6 C6 . . . . 176.91(12) ? C5 C6 O6 C13 . . . . -172.45(11) y N2 C15 N1 C21 . . . . 3.38(19) ? S1 C15 N1 C21 . . . . -176.54(9) y C22 C21 N1 C15 . . . . -50.03(18) y C26 C21 N1 C15 . . . . 130.33(13) ? N1 C15 N2 C16 . . . . -179.05(13) ? S1 C15 N2 C16 . . . . 0.87(17) y