#------------------------------------------------------------------------------ #$Date: 2024-08-02 04:53:16 +0300 (Fri, 02 Aug 2024) $ #$Revision: 293633 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/32/2023229.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023229 loop_ _publ_author_name 'Loukopoulos, Edward' 'Papatriantafyllopoulou, Constantina' 'Moushi, Eleni' 'Kitos, Alexandros A.' 'Tasiopoulos, Anastasios J.' 'Perlepes, Spyros P.' 'Nastopoulos, Vassilios' _publ_section_title ; Solvatomorphism in a series of copper(II) complexes with the 5-phenylimidazole/perchlorate system as ligands ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials' _journal_page_first 347 _journal_page_last 359 _journal_paper_doi 10.1107/S2052520624005948 _journal_volume 80 _journal_year 2024 _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C3 H6 O)' _chemical_formula_sum 'C42 H44 Cl2 Cu N8 O10' _chemical_formula_weight 955.29 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 69.117(6) _cell_angle_beta 80.660(5) _cell_angle_gamma 68.833(5) _cell_formula_units_Z 1 _cell_length_a 9.4814(4) _cell_length_b 9.7136(5) _cell_length_c 13.3146(9) _cell_measurement_reflns_used 2736 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 29.2670 _cell_measurement_theta_min 5.0260 _cell_volume 1067.61(11) _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 10.4223 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.984 _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0449 _diffrn_reflns_av_unetI/netI 0.0695 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.984 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 8762 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.984 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.999 _diffrn_reflns_theta_min 2.880 _diffrn_source 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.705 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.586 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour purple _exptl_crystal_density_diffrn 1.486 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 495 _exptl_crystal_size_max 0.16 _exptl_crystal_size_mid 0.11 _exptl_crystal_size_min 0.10 _refine_diff_density_max 0.857 _refine_diff_density_min -0.856 _refine_diff_density_rms 0.090 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.062 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 294 _refine_ls_number_reflns 4579 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.062 _refine_ls_R_factor_all 0.0727 _refine_ls_R_factor_gt 0.0517 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0548P)^2^+0.4849P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1189 _refine_ls_wR_factor_ref 0.1348 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3483 _reflns_number_total 4579 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file aw5090sup1.cif _cod_data_source_block 8 _cod_database_code 2023229 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.896 _shelx_estimated_absorpt_t_max 0.933 _shelx_res_file ; 8.res created by SHELXL-2014/7 TITL EL26G in P-1 CELL 0.71073 9.4814 9.7136 13.3146 69.117 80.660 68.833 ZERR 1 0.0004 0.0005 0.0009 0.0056 0.0047 0.0045 LATT 1 SFAC C H N O CL CU UNIT 42 44 8 10 2 1 MERG 2 OMIT -2 54 OMIT -1 -1 2 OMIT 0 0 3 SIZE 0.16 0.11 0.10 TEMP -173 MORE -3 FMAP 2 PLAN 10 ACTA BOND BOND $H HTAB LIST 4 L.S. 7 WGHT 0.054800 0.484900 FVAR 2.88086 CU 6 0.000000 0.000000 0.500000 10.50000 0.01826 0.01778 = 0.01851 -0.00323 -0.00156 -0.00400 DFIX 0.86 0.01 N1A H1A N1A 3 -0.275252 0.457161 0.429048 11.00000 0.02537 0.01621 = 0.02452 -0.00814 -0.00404 -0.00486 H1A 2 -0.288010 0.544849 0.435813 11.00000 -1.50000 C2A 1 -0.152687 0.333726 0.467414 11.00000 0.02103 0.02073 = 0.02013 -0.00262 -0.00415 -0.00584 AFIX 43 H2A 2 -0.070488 0.336437 0.498212 11.00000 -1.20000 AFIX 0 N3A 3 -0.162681 0.208167 0.456248 11.00000 0.01986 0.01948 = 0.01905 -0.00378 -0.00031 -0.00660 C4A 1 -0.298922 0.254184 0.408777 11.00000 0.02197 0.02201 = 0.01805 -0.00464 -0.00156 -0.00798 AFIX 43 H4A 2 -0.336638 0.187909 0.390872 11.00000 -1.20000 AFIX 0 C5A 1 -0.370746 0.410256 0.391697 11.00000 0.02101 0.02233 = 0.01556 -0.00457 0.00058 -0.00766 C6A 1 -0.516406 0.514780 0.343015 11.00000 0.02391 0.02093 = 0.01714 -0.00789 -0.00033 -0.00405 C7A 1 -0.550729 0.677161 0.304376 11.00000 0.02562 0.02197 = 0.02969 -0.00781 -0.00280 -0.00685 AFIX 43 H7A 2 -0.478939 0.722098 0.308715 11.00000 -1.20000 AFIX 0 C8A 1 -0.689401 0.772079 0.259856 11.00000 0.03431 0.01865 = 0.02821 -0.00566 -0.00464 -0.00075 AFIX 43 H8A 2 -0.711954 0.882071 0.233298 11.00000 -1.20000 AFIX 0 C9A 1 -0.795349 0.708301 0.253685 11.00000 0.02363 0.03251 = 0.02569 -0.01258 -0.00583 0.00263 AFIX 43 H9A 2 -0.890888 0.774336 0.224189 11.00000 -1.20000 AFIX 0 C10A 1 -0.761744 0.547815 0.290649 11.00000 0.02672 0.03537 = 0.02973 -0.01174 -0.00441 -0.01058 AFIX 43 H10A 2 -0.833339 0.503370 0.285189 11.00000 -1.20000 AFIX 0 C11A 1 -0.623037 0.452081 0.335723 11.00000 0.02572 0.02216 = 0.02576 -0.00756 -0.00360 -0.00525 AFIX 43 H11A 2 -0.600961 0.342149 0.361904 11.00000 -1.20000 AFIX 0 N1B 3 0.316138 0.148966 0.274022 11.00000 0.01935 0.02654 = 0.02238 -0.00788 0.00140 -0.00939 H1B 2 0.409888 0.144885 0.259282 11.00000 -1.50000 C2B 1 0.271528 0.071461 0.372036 11.00000 0.02502 0.02354 = 0.01954 -0.00717 -0.00231 -0.00708 AFIX 43 H2B 2 0.335368 0.014661 0.431602 11.00000 -1.20000 AFIX 0 N3B 3 0.128075 0.084130 0.375164 11.00000 0.02103 0.01924 = 0.02119 -0.00536 -0.00153 -0.00514 C4B 1 0.079050 0.173704 0.272367 11.00000 0.02255 0.01970 = 0.01979 -0.00401 -0.00251 -0.00499 AFIX 43 H4B 2 -0.020576 0.202435 0.249788 11.00000 -1.20000 AFIX 0 C5B 1 0.194862 0.214857 0.208004 11.00000 0.02075 0.01776 = 0.02222 -0.00551 -0.00167 -0.00370 C6B 1 0.204475 0.304096 0.093306 11.00000 0.02329 0.02000 = 0.02155 -0.00584 0.00138 -0.00119 C7B 1 0.294228 0.399452 0.055026 11.00000 0.02916 0.02919 = 0.03227 -0.00015 0.00137 -0.00717 AFIX 43 H7B 2 0.348868 0.410962 0.103658 11.00000 -1.20000 AFIX 0 C8B 1 0.303841 0.478164 -0.054949 11.00000 0.03614 0.03483 = 0.04152 0.00420 0.00746 -0.00903 AFIX 43 H8B 2 0.366616 0.541790 -0.081193 11.00000 -1.20000 AFIX 0 C9B 1 0.223597 0.464311 -0.125069 11.00000 0.04021 0.03742 = 0.02094 0.00079 0.00825 0.00464 AFIX 43 H9B 2 0.231734 0.517577 -0.199890 11.00000 -1.20000 AFIX 0 C10B 1 0.131144 0.373977 -0.088363 11.00000 0.04416 0.03818 = 0.02330 -0.01054 -0.00415 0.00281 AFIX 43 H10B 2 0.073545 0.366790 -0.137269 11.00000 -1.20000 AFIX 0 C11B 1 0.122534 0.293080 0.021029 11.00000 0.03332 0.02829 = 0.02461 -0.00740 -0.00030 -0.00589 AFIX 43 H11B 2 0.059657 0.229518 0.046419 11.00000 -1.20000 AFIX 0 CL 5 0.223424 0.160609 0.621277 11.00000 0.02340 0.02289 = 0.02672 -0.00863 -0.00421 -0.00750 O1 4 0.121958 0.077360 0.628062 11.00000 0.02566 0.02169 = 0.02933 -0.00782 -0.00181 -0.00860 O2 4 0.375240 0.072208 0.597432 11.00000 0.02217 0.04120 = 0.03367 -0.01298 -0.00232 -0.00785 O3 4 0.217515 0.188822 0.720882 11.00000 0.04036 0.03661 = 0.03060 -0.01697 -0.00627 -0.01158 O4 4 0.177757 0.308629 0.535867 11.00000 0.03874 0.02384 = 0.03677 -0.00267 -0.01090 -0.01399 C12 1 0.667454 0.112823 0.120288 11.00000 0.02660 0.03572 = 0.02730 -0.00822 -0.00301 -0.00856 O5 4 0.602629 0.178780 0.185177 11.00000 0.02561 0.03208 = 0.03064 -0.00895 -0.00045 -0.01104 C13 1 0.591742 0.043583 0.070394 11.00000 0.03614 0.04487 = 0.04261 -0.02302 -0.00793 -0.00652 AFIX 137 H13A 2 0.494963 0.040901 0.108882 11.00000 -1.50000 H13B 2 0.656894 -0.062786 0.074766 11.00000 -1.50000 H13C 2 0.573692 0.107205 -0.005203 11.00000 -1.50000 AFIX 0 C14 1 0.827818 0.102132 0.082661 11.00000 0.03436 0.07736 = 0.04856 -0.02704 0.00932 -0.02598 AFIX 137 H14A 2 0.829061 0.175959 0.009882 11.00000 -1.50000 H14B 2 0.885196 -0.004109 0.082015 11.00000 -1.50000 H14C 2 0.873980 0.127560 0.131501 11.00000 -1.50000 AFIX 0 HKLF 4 REM EL26G in P-1 REM R1 = 0.0517 for 3483 Fo > 4sig(Fo) and 0.0727 for all 4579 data REM 294 parameters refined using 1 restraints END WGHT 0.0543 0.5068 REM Instructions for potential hydrogen bonds EQIV $1 -x, -y+1, -z+1 HTAB N1A Cl_$1 HTAB N1A O4_$1 HTAB C2A O4 EQIV $2 -x, -y, -z+1 HTAB C4A O2_$2 HTAB N1B O5 HTAB C2B O2 EQIV $3 -x+1, -y, -z+1 HTAB C2B O2_$3 REM Highest difference peak 0.857, deepest hole -0.856, 1-sigma level 0.090 Q1 1 0.0848 0.0479 0.4669 11.00000 0.05 0.77 Q2 1 -0.1208 0.0775 0.5025 11.00000 0.05 0.53 Q3 1 0.0032 0.1025 0.4925 11.00000 0.05 0.51 Q4 1 -0.0173 0.1203 0.4575 11.00000 0.05 0.48 Q5 1 0.1427 0.1231 0.6438 11.00000 0.05 0.44 Q6 1 0.1711 0.1406 0.7041 11.00000 0.05 0.43 Q7 1 0.3183 0.1903 0.5926 11.00000 0.05 0.43 Q8 1 0.1413 0.1632 0.2184 11.00000 0.05 0.41 Q9 1 -0.4594 0.6915 0.2607 11.00000 0.05 0.40 Q10 1 -0.5234 0.5993 0.2982 11.00000 0.05 0.37 ; _shelx_res_checksum 66247 _shelx_hkl_file ; 0 0 2 6409.14 228.697 6 0 0 3 16072.2 459.021 6 0 0 4 3161.45 235.193 6 0 0 5 4117.25 295.762 6 0 0 6 8183.36 449.809 6 0 0 7 7376.08 463.081 6 0 0 8 11091.6 613.071 6 0 0 -8 10921.3 647.452 6 0 0 -9 15846.2 836.658 6 0 0 9 15816.3 773.852 6 0 0 10 2486.72 332.143 6 0 0 11 1512.71 270.744 6 0 0 12 759.000 220.487 6 0 0 13 8.36277 116.886 6 0 0 14 83.1235 88.6330 6 0 0 15-32.2574 115.718 6 0 0 16 333.258 192.630 6 0 -1 15 89.4655 104.294 6 0 -1 14-41.6387 114.072 6 0 -1 13-386.185 163.499 6 0 -1 12 622.767 190.412 6 0 -1 11 30.6252 101.738 6 0 -1 10 6386.04 525.737 6 0 -1 9 17996.1 828.701 6 0 -1 8 11577.3 625.113 6 0 1 -8 13630.2 743.767 6 0 -1 7 845.022 178.920 6 0 -1 6 1208.48 184.158 6 0 -1 5 6231.66 375.666 6 0 1 -4 3200.15 124.664 5 0 -1 4 3316.92 248.865 6 0 -1 3 1840.84 172.299 6 0 -1 2 23431.8 507.215 6 0 -1 1 16930.8 352.456 6 0 1 2 15941.8 375.641 6 0 1 3 24467.9 551.839 6 0 1 4 3704.11 259.754 6 0 1 5 136.776 81.5198 6 0 1 6 119.857 70.2233 6 0 1 7 24218.7 824.105 6 0 1 8 28301.4 960.372 6 0 -1 -9 7813.50 566.010 6 0 1 9 6914.37 517.691 6 0 1 10 918.634 204.028 6 0 1 11 200.545 105.713 6 0 1 12 562.896 181.298 6 0 1 13 220.244 136.381 6 0 1 14 2329.55 388.186 6 0 1 15 2170.80 392.481 6 0 1 16 1064.45 280.541 6 0 -2 14 1205.17 297.345 6 0 -2 13 1940.21 351.538 6 0 -2 12 3120.16 422.356 6 0 -2 11 6403.09 578.357 6 0 -2 10 324.892 140.506 6 0 -2 9 1940.62 299.023 6 0 -2 8-68.4806 68.4989 6 0 -2 7 2247.65 287.387 6 0 2 -7 2605.94 322.648 6 0 -2 6 901.945 173.891 6 0 2 -6 1035.56 97.5863 5 0 -2 5 495.455 122.822 6 0 -2 4 6629.20 381.977 6 0 -2 3 5727.35 332.701 6 0 -2 2 102405. 1202.07 6 0 -2 1 790.032 102.333 6 0 2 0 303.983 56.4087 4 0 2 1 13174.0 330.571 4 0 2 2 1120.94 116.205 4 0 2 3 18691.6 472.318 4 0 2 4 37318.3 815.165 6 0 2 5 12321.1 527.017 6 0 2 6 43113.8 1041.91 6 0 2 7 22135.8 805.436 6 0 2 8 5123.26 418.777 6 0 -2 -9 23.2483 68.1559 6 0 2 9 144.329 97.4220 6 0 2 10 323.392 104.263 6 0 2 11 4315.67 470.616 6 0 2 12 80.5131 91.6922 6 0 2 12 92.4737 21.3542 5 0 2 13 812.979 233.329 6 0 2 14 4595.13 545.602 6 0 2 15 1751.51 352.294 6 0 2 16 639.144 234.346 6 0 -3 13-79.4958 112.472 6 0 -3 12 2568.39 411.259 6 0 -3 11 4396.81 488.706 6 0 -3 10 480.499 148.997 6 0 -3 9 339.306 145.736 6 0 3 -8 79.3845 36.4946 5 0 -3 8 99.6032 85.7848 6 0 3 -7 4322.91 235.896 5 0 -3 7 4085.70 383.747 6 0 3 -6 1833.14 267.390 6 0 -3 6 1519.36 231.632 6 0 -3 5 6367.95 427.507 6 0 -3 4 19464.0 688.981 6 0 -3 3 19979.6 647.135 6 0 -3 2 41915.2 845.577 6 0 -3 2 36321.7 402.989 2 0 -3 1 132.139 54.5433 6 0 3 0 11006.3 379.814 4 0 3 1 2992.24 190.117 4 0 3 2 63521.0 908.412 4 0 3 3 10827.3 388.901 4 0 3 4 1117.41 146.984 4 0 3 5 20633.9 640.016 4 0 3 5 20968.5 694.255 6 0 3 6 8782.04 498.224 6 0 3 7 3731.50 344.793 6 0 -3 -8 716.480 162.469 6 0 3 8 498.947 131.467 6 0 -3 -9 434.870 140.825 6 0 3 9 767.347 194.914 6 0 -3 -9 662.929 156.851 4 0 3 10 4459.44 443.831 6 0 3 11 1404.54 268.653 6 0 3 12 5596.64 547.309 6 0 3 13 251.481 118.441 6 0 3 14-55.0910 130.977 6 0 3 15 76.6820 102.413 6 0 3 16 37.9085 123.345 6 0 -4 12 1967.20 364.355 6 0 -4 11 634.665 202.842 6 0 -4 10-16.4498 87.7075 6 0 -4 9 696.636 188.275 6 0 -4 8 16.0264 74.1947 6 0 4 -8 23.8361 32.4689 5 0 -4 7 3010.77 348.746 6 0 4 -7 3364.98 232.420 5 0 -4 6 5713.44 443.941 6 0 -4 5 8341.67 503.886 6 0 -4 5 8610.29 282.022 2 0 4 -5 8510.56 573.262 6 0 -4 4 35221.4 504.693 2 0 -4 4 35805.0 980.649 6 0 -4 3 1150.59 172.790 6 0 -4 2 7264.38 392.274 6 0 4 -2 6978.27 290.439 1 0 -4 1 6271.73 337.486 6 0 4 -1 5978.95 348.562 4 0 4 -1 5865.21 209.169 1 0 4 0 1319.82 159.799 4 0 4 1 414.589 77.7671 4 0 4 2-39.7445 54.4360 4 0 4 3 16102.8 527.161 4 0 4 4 724.537 126.463 4 0 4 5 77.3588 59.0710 4 0 4 6 1610.50 207.779 4 0 4 6 1581.90 213.040 6 0 4 7 2466.07 295.759 6 0 4 8 99.7368 70.3897 6 0 4 9 445.509 130.781 6 0 4 10 2121.95 311.793 6 0 4 11 11504.6 759.140 6 0 4 12 4690.92 512.807 6 0 4 13 2248.99 365.721 6 0 4 14-18.3156 99.0364 6 0 4 15 32.1294 109.240 6 0 4 16 87.4456 110.261 6 0 4 17 93.7362 114.703 6 0 -5 11 65.8892 76.9573 6 0 -5 10 584.752 184.900 6 0 -5 9 3546.92 225.048 2 0 -5 9 3676.17 441.459 6 0 5 -9 4221.05 299.311 5 0 -5 8-19.1780 26.7600 2 0 -5 8 16.6127 86.6912 6 0 5 -8-37.3156 43.9999 5 0 -5 7 1617.65 266.438 6 0 -5 7 1359.08 120.619 2 0 -5 6 5564.87 459.990 6 0 -5 6 4815.50 204.414 2 0 -5 5 1909.95 263.519 6 0 5 -5 2239.49 249.774 1 0 5 -4 4540.17 324.991 1 0 -5 4 4488.78 379.561 6 0 -5 3 20.1777 55.0215 6 0 5 -3 102.438 55.7999 1 0 5 -3 120.219 77.0998 6 0 5 -2 3492.72 207.709 1 0 -5 2 3727.51 300.570 6 0 5 -1 1148.64 171.544 4 0 5 -1 844.812 76.9196 1 0 5 0-28.5469 41.7263 4 0 5 0 6.47009 17.0940 2 0 5 1 1399.70 176.522 4 0 5 2 5131.05 332.084 4 0 5 3 36615.6 886.246 4 0 5 4 14557.4 571.021 4 0 5 5 36.5672 41.0688 4 0 5 6 1649.66 211.295 4 0 5 7 211.943 97.3714 6 0 -5 -7 426.324 115.338 4 0 5 7 226.036 85.7362 4 0 -5 -8 701.249 156.031 4 0 5 8 816.161 188.194 6 0 5 9 3587.18 398.588 6 0 5 10 2121.13 316.783 6 0 5 11 863.778 202.223 6 0 5 12 1553.70 296.766 6 0 5 13 255.836 141.820 6 0 5 14 353.081 169.001 6 0 5 15 301.068 167.255 6 0 5 16-81.0051 104.328 6 0 -6 10-104.461 101.134 6 0 -6 9 68.9249 63.1438 6 0 -6 8 26.3090 61.0299 6 0 6 -8 74.7314 52.5149 5 0 -6 7-5.00941 76.9363 6 0 -6 6 4412.46 426.858 6 0 6 -6 4203.15 384.866 1 0 6 -5 3909.38 349.052 1 0 -6 5 3752.31 375.888 6 0 6 -4 2239.40 240.855 1 0 -6 4 2236.63 288.662 6 0 -6 3 2679.14 295.768 6 0 6 -3 2444.76 212.391 1 0 6 -2 71.6527 33.9819 1 0 6 -2 207.768 84.0720 4 0 6 -1 1358.34 208.376 4 0 6 0 6328.77 445.479 6 0 6 0 6362.29 422.419 4 0 6 0 6241.64 248.460 2 0 6 1 4143.64 328.617 4 0 6 1 4441.46 363.502 6 0 6 2 572.595 133.230 6 0 6 2 302.545 88.0017 4 0 6 3 2779.64 272.864 4 0 -6 -3 2834.30 278.197 4 0 -6 -4 17572.3 693.334 4 0 6 4 16590.9 664.935 4 0 6 5 10372.5 540.788 4 0 -6 -5 9427.87 212.183 3 0 -6 -5 11106.9 563.886 4 0 -6 -6 3680.78 333.063 4 0 6 6 3375.99 322.740 4 0 6 7 4160.29 369.874 4 0 6 8 2380.97 313.572 6 0 6 8 2011.73 269.363 4 0 6 9 4677.88 460.763 6 0 6 10 2676.02 372.854 6 0 6 11-118.448 113.202 6 0 6 12 1549.02 307.399 6 0 6 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211.023 5 2 4 -6 1800.01 244.491 1 -2 -4 5 5025.64 380.962 6 2 4 -5 5191.50 326.441 5 2 4 -5 5338.51 444.313 6 2 4 -5 5135.01 378.646 1 2 4 -4 65.6338 51.9782 6 -2 -4 4 160.256 72.9805 6 2 4 -4 160.023 62.6711 5 2 4 -4 143.550 57.6975 1 -2 -4 3 1115.10 163.257 6 2 4 -3 1262.32 166.786 1 2 4 -3 1322.79 165.923 5 2 4 -2 3133.09 233.717 1 2 4 -2 3547.89 244.181 5 2 4 -2 2931.09 264.641 6 -2 -4 2 3576.33 250.790 6 2 4 -1 17389.8 396.816 3 2 4 -1 17766.9 579.682 6 2 4 -1 16451.7 493.281 1 -2 -4 1 18215.3 521.945 1 2 4 0 2506.64 178.994 4 2 4 0 2793.46 138.042 3 -2 -4 0 2622.64 181.207 1 2 4 1 261.010 42.2612 3 -2 -4 -1 215.942 66.6955 1 2 4 1 261.969 57.2211 4 -2 -4 -2 4610.18 155.516 3 -2 -4 -2 4646.36 234.088 4 2 4 2 4897.41 240.640 4 2 4 3 9596.78 359.642 4 -2 -4 -3 9313.84 354.665 4 2 4 4 1137.55 146.410 4 -2 -4 -4 1086.27 137.925 4 -2 -4 -5 13962.9 509.786 4 2 4 5 13457.8 580.271 6 -2 -4 -6 295.604 94.1050 4 2 4 6 409.406 118.924 6 2 4 7 19337.2 791.103 6 -2 -4 -7 21125.8 749.419 4 2 4 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1542.41 121.954 3 2 5 0 4012.18 166.343 3 -2 -5 0 4083.38 235.338 1 2 5 0 3949.07 260.632 4 -2 -5 -1 65.4992 42.8988 1 2 5 1 28.1303 34.0482 4 2 5 2 235.002 60.8095 4 -2 -5 -2 175.520 59.7186 4 -2 -5 -3 28.6915 41.6413 4 2 5 3 36.8076 45.0260 4 -2 -5 -3 12.6959 12.7311 3 2 5 4 25.0320 36.9005 4 -2 -5 -4 51.4387 39.9251 4 -2 -5 -5 5587.07 347.193 4 2 5 5 5715.03 352.592 4 2 5 6 11343.6 530.626 4 2 5 6 10894.0 578.103 6 -2 -5 -6 12466.2 543.291 4 -2 -5 -7 14063.5 616.142 4 2 5 7 12441.3 653.286 6 -2 -5 -8 3963.08 352.011 4 2 5 8 3109.56 345.004 6 -2 -5 -9 120.924 74.3436 4 2 5 9-52.9532 107.762 6 2 5 10 2243.23 326.336 6 2 5 11 345.089 136.574 6 2 5 12 4934.67 533.366 6 2 5 13 1216.35 277.543 6 2 5 14 1218.44 290.094 6 2 5 15 2062.47 397.614 6 2 5 16 1160.85 297.388 6 -2 -6 11 4297.90 500.088 6 -2 -6 10 436.933 161.639 6 -2 -6 9 312.938 151.434 6 2 6 -8-45.5464 66.6065 5 -2 -6 8 9.48578 91.5182 6 2 6 -7-9.48563 67.3071 5 -2 -6 7 25.7597 66.8523 6 2 6 -6 867.151 161.509 5 2 6 -6 998.118 195.074 1 -2 -6 6 1232.59 222.182 6 -2 -6 5 941.059 202.105 6 2 6 -5 1188.31 180.635 5 2 6 -5 1456.44 225.002 1 2 6 -4 5984.26 415.659 1 2 6 -4 5414.02 373.982 5 -2 -6 4 6337.78 446.999 6 -2 -6 3 10369.9 534.821 6 2 6 -3 9215.15 477.018 1 2 6 -2 21113.2 745.972 4 2 6 -2 20520.4 844.631 6 2 6 -2 18348.6 611.936 1 2 6 -1 4054.48 200.039 3 2 6 -1 4560.22 330.752 4 2 6 -1 4436.24 377.175 6 2 6 0 792.056 75.7221 3 2 6 0 841.113 159.550 6 2 6 0 807.042 143.951 4 -2 -6 -1 1358.40 130.592 1 2 6 1 1274.43 164.658 4 2 6 2 589.371 115.908 4 -2 -6 -2 650.309 95.4300 1 2 6 3 663.517 115.058 4 -2 -6 -3 791.659 128.746 4 -2 -6 -4 43.3886 44.3600 4 -2 -6 -4 14.7697 12.8047 3 2 6 4-3.53137 35.3156 4 -2 -6 -5 1457.76 190.866 4 2 6 5 1627.06 204.812 4 2 6 6 6789.68 430.855 4 -2 -6 -6 8347.21 476.104 4 -2 -6 -7 212.388 85.0338 4 2 6 7 117.090 64.8536 4 2 6 7 74.3997 55.9194 6 2 6 8 145.856 102.852 6 -2 -6 -8 367.631 117.569 4 2 6 9 3473.19 402.865 6 2 6 10 167.434 89.5158 6 2 6 11-69.6149 116.123 6 2 6 12 449.570 188.081 6 2 6 13 3242.52 454.930 6 2 6 14 1248.49 304.521 6 2 6 15 2682.64 436.334 6 2 6 16 320.265 141.365 6 -2 -7 10-70.3339 111.651 6 -2 -7 9 170.190 93.1367 6 2 7 -8 1310.86 213.797 5 -2 -7 8 841.920 204.127 6 2 7 -7 1827.96 245.177 5 -2 -7 7 1741.58 294.996 6 2 7 -6 1024.69 185.934 5 -2 -7 6 769.599 187.819 6 -2 -7 5 305.430 118.640 6 2 7 -5 297.102 115.304 1 2 7 -5 319.015 113.374 5 2 7 -4 2559.86 279.592 1 -2 -7 4 2552.23 302.200 6 2 7 -4 3395.14 327.918 5 2 7 -3 282.303 81.4042 1 2 7 -3 421.556 127.581 4 2 7 -2 1949.47 163.255 3 2 7 -2 1913.32 259.448 4 2 7 -1 62.2358 71.2351 4 2 7 -1 57.6172 33.6176 3 2 7 0-9.69611 52.6847 4 2 7 0 1.96334 12.6101 3 2 7 1 6632.66 411.691 4 2 7 2 1810.10 216.548 4 -2 -7 -2 1846.86 141.472 1 -2 -7 -3 7042.89 286.305 1 2 7 3 7148.27 423.094 4 -2 -7 -3 7662.81 442.973 4 2 7 4 1031.58 169.546 4 -2 -7 -4 1438.26 196.470 4 -2 -7 -5 2035.01 104.303 3 2 7 5 2345.38 257.358 4 -2 -7 -5 2313.17 258.638 4 -2 -7 -6 2759.19 286.377 4 2 7 6 2531.82 278.348 4 2 7 7 21.5181 47.0622 4 2 7 8 282.045 115.088 6 2 7 8 711.611 169.537 4 2 7 9 1926.34 315.961 6 2 7 10 4445.90 483.440 6 2 7 11 7137.66 624.975 6 2 7 12 249.043 139.432 6 2 7 13 510.896 187.641 6 2 7 14-57.0039 120.154 6 2 7 15 9.56535 84.1643 6 2 7 16 57.7296 92.7501 6 -2 -8 8 101.653 75.0255 6 -2 -8 7 492.219 160.384 6 2 8 -7 568.317 154.603 5 2 8 -6 948.580 190.619 5 2 8 -5 3087.93 335.715 5 2 8 -5 3499.12 419.456 4 2 8 -4 146.001 82.9366 4 2 8 -3-93.0897 82.0959 4 2 8 -2 4130.12 231.413 3 2 8 -2 3996.89 395.273 4 2 8 -1 548.900 151.045 4 2 8 -1 611.932 71.5166 3 2 8 0 1337.02 214.888 4 2 8 1 4358.96 372.071 4 2 8 1 3875.12 150.504 2 2 8 2 7212.33 471.672 4 -2 -8 -3 3875.44 189.131 1 2 8 3 4162.38 357.624 4 2 8 4 3919.64 349.095 4 -2 -8 -4 4504.62 225.270 1 2 8 5 49.6168 45.4182 4 2 8 6 204.200 90.7001 4 -2 -8 -6 222.399 30.0563 3 2 8 7 1313.21 221.429 4 2 8 8 8739.05 587.626 4 2 8 8 8999.05 665.226 6 2 8 9 4190.67 466.222 6 2 8 9 3492.53 390.617 4 2 8 10 416.191 157.011 6 2 8 11 878.931 229.589 6 2 8 12 263.206 140.697 6 2 8 13 32.0475 84.2921 6 2 8 14 286.576 153.872 6 2 8 15-32.7853 82.0436 6 2 9 -7 4123.20 514.262 4 2 9 -6 3546.56 470.547 4 2 9 -6 3008.67 357.618 5 2 9 -5 1061.13 267.812 4 2 9 -5 781.766 186.380 5 2 9 -4 407.701 118.428 4 2 9 -4 819.943 185.065 5 2 9 -3 1040.57 226.399 4 2 9 -2 1576.03 262.316 4 2 9 -1 2555.95 330.430 4 2 9 0 3823.19 390.427 4 2 9 1 1529.51 243.165 4 2 9 2 0.90935 49.1544 4 2 9 3 153.875 93.2204 4 2 9 4 148.423 87.2502 4 -2 -9 -5 1109.84 105.684 1 2 9 5 1323.94 223.276 4 2 9 6-49.0183 94.4765 4 2 9 7 465.863 141.209 4 2 9 8 7878.69 580.488 4 2 9 9 6252.34 596.801 6 2 9 9 6267.28 540.615 4 2 9 10 2183.87 338.959 4 2 9 10 2257.39 382.805 6 2 9 11 1081.08 269.576 6 2 9 12 303.405 139.225 6 2 9 13 1465.01 326.748 6 2 9 14 1217.45 309.708 6 2 10 -5 329.249 139.580 4 2 10 -5 531.842 161.743 5 2 10 -4-189.564 135.476 4 2 10 -4 241.741 139.153 5 2 10 -3 62.9347 68.1194 4 2 10 -2 175.281 57.6368 4 2 10 -1 3980.78 446.697 4 2 10 0 3225.96 391.136 4 2 10 1 3632.99 415.942 4 2 10 2 661.133 175.836 4 2 10 3 47.2135 69.6464 4 2 10 4 138.471 89.6141 4 2 10 5 946.105 198.853 4 2 10 6 455.774 148.355 4 2 10 7 190.453 103.173 4 2 10 8 2993.25 382.723 4 2 10 9 4039.94 454.493 4 2 10 10 102.641 88.4089 4 2 10 10 51.3687 79.7809 6 2 10 11 202.000 93.8918 6 2 10 12 396.440 175.791 6 2 10 13 1061.19 293.318 6 2 11 -4 438.290 153.096 5 2 11 -3 1588.82 316.954 4 2 11 -2 678.530 216.238 4 2 11 -1 525.372 155.942 4 2 11 0 387.813 160.788 4 2 11 1 580.121 177.562 4 2 11 2 121.025 111.397 4 2 11 3-50.1282 82.4371 4 2 11 4 1153.69 242.572 4 2 11 5 1257.17 252.532 4 2 11 6 2791.62 373.238 4 2 11 7 3322.69 413.488 4 2 11 8 42.7507 74.7228 4 2 11 9 1746.14 310.649 4 2 11 10 207.776 159.581 6 2 11 10-8.18672 111.672 4 2 11 11-97.8208 99.0569 6 2 11 11-7.14806 77.2039 4 2 12 1 1072.60 255.406 4 2 12 2 236.274 122.030 4 2 12 3 325.214 134.722 4 2 12 4 1129.82 259.961 4 2 12 5 1286.57 269.757 4 2 12 6 1204.32 273.314 4 2 12 7 380.258 156.730 4 2 12 8-19.9092 56.5799 4 2 12 9 952.179 232.701 4 -3 10 10-6.78677 56.6121 6 -3 10 9 371.970 145.677 6 -3 9 13 712.358 221.689 6 -3 9 12 703.500 236.686 6 -3 9 11 1280.40 302.125 6 -3 9 10 860.561 239.506 6 -3 9 10 1016.60 253.839 4 -3 9 9 652.821 230.173 6 -3 9 9 497.462 171.066 4 -3 9 8 200.921 116.846 4 -3 9 7 115.283 93.1579 4 -3 9 6 48.8242 78.7990 4 -3 9 5 424.168 165.993 4 -3 9 4-3.19219 84.9971 4 -3 9 3 688.384 202.196 4 -3 9 2 769.301 222.499 4 -3 9 1 1417.06 296.559 4 -3 9 0 930.544 234.649 4 -3 9 -1 12.1623 63.1242 4 -3 8 14-240.767 144.814 6 -3 8 13 307.824 131.070 6 -3 8 12 48.8058 72.9762 6 -3 8 11 1254.92 284.299 6 -3 8 11 1481.47 308.771 4 -3 8 10 1972.35 348.765 4 -3 8 10 1926.24 340.489 6 -3 8 9 363.799 145.599 4 -3 8 9 253.590 148.416 6 -3 8 8 86.0082 91.4027 4 -3 8 7 206.477 115.916 4 -3 8 6 983.248 218.842 4 -3 8 5 9973.58 698.595 4 -3 8 4 6000.22 545.052 4 -3 8 3 1912.08 306.038 4 -3 8 2 2134.36 336.266 4 -3 8 1 1088.81 243.099 4 -3 8 0 610.497 174.848 4 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66.8697 4 -3 7 -7 17.6249 64.8546 4 3 -7 7 45.9668 91.7684 6 -3 6 16 686.266 236.519 6 -3 6 15 2423.42 412.212 6 -3 6 14 428.127 178.655 6 -3 6 13 2168.79 376.654 6 -3 6 12-24.8085 102.644 6 3 -6 -12 138.240 73.9089 3 -3 6 11-101.890 94.9864 6 3 -6 -11 174.948 77.4114 3 3 -6 -10-60.9858 66.8772 3 -3 6 10 159.928 113.905 6 -3 6 9 235.978 133.429 6 3 -6 -9 291.130 111.737 1 3 -6 -9 314.043 90.5727 3 -3 6 9 478.294 157.112 4 -3 6 8 2818.43 354.382 6 3 -6 -8 2748.70 296.319 1 3 -6 -8 3513.24 270.848 3 -3 6 8 3295.96 378.935 4 -3 6 7 5247.50 463.140 4 3 -6 -7 5713.97 309.922 3 3 -6 -7 4836.19 364.418 1 3 -6 -6 1406.09 172.787 1 3 -6 -6 1661.31 155.340 3 -3 6 6 1473.14 243.465 4 -3 6 5 2596.21 313.749 4 -3 6 4 193.138 83.7790 4 -3 6 3 2852.31 334.383 4 -3 6 2 3369.56 352.570 4 -3 6 2 3401.58 287.043 2 -3 6 1 6046.18 466.546 4 -3 6 1 5681.30 235.171 3 -3 6 1 5444.13 352.149 2 -3 6 0 819.210 94.0130 3 -3 6 0 778.562 130.634 2 -3 6 0 789.744 178.365 4 -3 6 -1 5186.40 463.169 4 -3 6 -1 5256.81 252.827 3 -3 6 -2 10574.5 396.205 3 -3 6 -2 11033.5 675.222 4 -3 6 -3 3093.35 371.000 4 -3 6 -4 1018.78 208.874 4 3 -6 4 893.261 201.423 6 -3 6 -5 1223.26 263.700 4 3 -6 5 1788.88 295.590 6 3 -6 6 824.191 209.232 6 3 -6 7-12.0208 65.8873 6 3 -6 8 510.553 179.073 6 -3 5 16 920.380 272.971 6 -3 5 15 1147.06 294.776 6 -3 5 14 216.314 149.376 6 -3 5 13 372.419 132.832 6 -3 5 12 1493.28 300.359 6 -3 5 11-197.730 152.629 6 -3 5 10-31.9206 109.404 6 3 -5 -9 2153.25 243.822 3 -3 5 9 2097.80 309.208 6 -3 5 9 1930.49 294.499 4 3 -5 -8 7667.32 421.339 3 3 -5 -8 6261.07 457.595 1 -3 5 8 6973.55 531.092 4 -3 5 8 7689.49 560.101 6 -3 5 7 9971.46 602.345 4 -3 5 7 10015.5 614.278 6 3 -5 -7 11243.6 467.268 3 3 -5 -7 8981.98 513.601 1 3 -5 -6 1400.29 186.250 1 3 -5 -6 1661.39 164.085 3 -3 5 6 1509.49 229.283 4 3 -5 -5-15.2622 22.0851 3 -3 5 5 78.2420 54.5377 4 3 -5 -5-54.4844 39.1205 1 -3 5 4 999.047 183.123 4 3 -5 -4 814.758 102.491 3 -3 5 3 6.25384 46.4971 6 -3 5 3 55.3812 43.6369 4 -3 5 2-5.18004 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2507.25 296.267 6 -4 -5 5 564.369 135.892 6 4 5 -5 566.774 162.998 6 -4 -5 5 345.098 48.9217 2 4 5 -4 3739.44 287.147 3 4 5 -4 4019.28 353.987 5 -4 -5 4 3597.15 300.180 6 4 5 -4 4050.52 379.194 6 4 5 -4 3622.56 353.634 1 4 5 -3-3.25845 36.7833 6 4 5 -3-45.6635 77.9179 5 -4 -5 3 29.2699 51.8522 6 4 5 -3 31.4239 51.3968 1 4 5 -3 5.80103 29.4625 3 4 5 -2 934.081 161.368 1 4 5 -2 737.347 146.654 5 4 5 -1 560.357 88.1698 4 4 5 -1 527.314 123.582 5 4 5 0 4752.30 224.949 4 4 5 0 4985.56 196.144 2 4 5 0 5155.89 360.972 5 4 5 0 5041.73 256.161 3 4 5 0 4696.20 300.629 6 4 5 1 27838.3 511.923 2 -4 -5 -1 27094.2 592.333 3 4 5 1 27850.0 817.185 5 4 5 1 27706.7 591.636 3 4 5 1 26826.2 533.868 4 4 5 1 29052.4 705.047 6 -4 -5 -1 27418.0 778.861 1 -4 -5 -2 8487.01 295.857 4 4 5 2 8910.87 459.525 5 -4 -5 -2 9340.27 341.947 3 4 5 2 9354.79 330.726 4 4 5 3 5732.31 375.838 5 -4 -5 -3 4932.22 248.564 3 4 5 3 5611.19 277.123 4 -4 -5 -3 5112.97 246.394 4 4 5 4 12746.8 536.806 5 -4 -5 -4 12998.4 419.584 3 -4 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226.996 3 4 6 -3 2525.86 283.797 5 4 6 -3 2554.95 290.697 1 4 6 -3 2919.54 328.815 6 4 6 -2 3259.94 315.927 5 4 6 -2 3449.17 335.438 6 4 6 -2 3750.43 278.478 4 4 6 -1 55.4727 43.4757 6 4 6 -1-15.2999 38.7640 4 4 6 -1 6.97075 54.9697 5 4 6 0 6687.08 436.469 5 4 6 0 7054.69 305.969 3 4 6 0 7090.64 425.741 6 4 6 0 6898.28 326.804 4 4 6 1 21727.6 420.502 2 4 6 1 20801.4 753.060 5 4 6 1 20388.0 505.312 3 4 6 1 21554.8 570.790 4 4 6 1 20872.4 698.066 6 4 6 2 313.431 68.8394 4 4 6 2 278.494 97.7892 5 -4 -6 -2 417.049 95.2693 1 -4 -6 -2 372.377 67.0215 3 4 6 3 2967.65 279.964 5 -4 -6 -3 3093.61 194.454 3 4 6 3 3189.51 232.576 4 -4 -6 -3 2962.45 212.752 4 -4 -6 -4-2.87748 21.8704 3 4 6 4 0.77067 36.5543 4 -4 -6 -4 1.81837 26.8932 4 4 6 5 1076.46 183.154 5 4 6 5 1291.89 171.234 4 -4 -6 -5 1126.19 125.739 3 -4 -6 -5 997.387 146.725 4 -4 -6 -6-22.8904 37.3009 4 4 6 6-7.80726 57.3209 6 -4 -6 -7 962.749 159.744 4 4 6 7 678.099 152.603 6 4 6 7 923.551 167.865 5 4 6 8 9158.69 485.150 5 -4 -6 -8 9651.47 538.998 4 4 6 8 8563.36 591.581 6 4 6 9 16566.5 850.339 6 4 6 9 18863.6 695.337 5 -4 -6 -9 17737.9 778.526 4 4 6 10 6806.75 573.492 6 4 6 10 7336.15 441.871 5 4 6 11 7360.03 438.617 5 4 6 11 5900.25 552.953 6 4 6 12 99.5635 121.212 6 4 6 12 50.9085 48.9509 5 4 6 13 225.691 128.801 6 4 6 13 172.816 63.1202 5 4 6 14 1151.25 288.683 6 4 6 15 547.664 199.820 6 4 6 16-30.1310 76.2262 6 -4 -7 10 613.016 198.002 6 -4 -7 9 1290.84 255.699 6 -4 -7 8 1982.39 306.094 6 -4 -7 7 2781.42 353.506 6 4 7 -6 571.042 136.993 3 4 7 -6 387.337 134.902 5 -4 -7 6 268.438 119.409 6 4 7 -5 211.946 101.811 5 4 7 -5 202.738 72.3841 3 4 7 -4 707.221 161.865 5 4 7 -4 705.341 130.626 3 4 7 -3 1053.69 179.712 4 4 7 -3 1106.56 154.627 3 4 7 -3 907.023 179.333 5 4 7 -3 859.351 171.928 1 4 7 -2 5494.94 435.961 5 4 7 -2 5677.12 378.759 4 4 7 -1 13163.6 658.976 5 4 7 -1 13084.9 551.375 4 4 7 0 5712.82 433.987 5 4 7 0 5557.82 279.767 3 4 7 0 4593.82 387.499 6 4 7 0 4508.29 306.567 4 4 7 1 1655.69 105.285 2 4 7 1 1753.34 226.962 6 4 7 1 1881.90 248.556 5 4 7 1 1598.16 182.083 4 4 7 2 7026.63 443.588 6 4 7 2 6569.29 359.088 4 4 7 2 6464.70 441.611 5 4 7 3 1022.09 144.283 4 -4 -7 -3 1130.97 116.065 3 4 7 4 9.96749 35.7607 4 -4 -7 -4 13.6919 39.2256 4 -4 -7 -4 11.3187 19.9231 3 -4 -7 -5 69.4570 37.1509 3 -4 -7 -5 31.6045 64.5469 4 4 7 5 29.8503 49.6806 4 4 7 6 302.883 93.8908 4 -4 -7 -6 393.932 79.9854 3 -4 -7 -6 333.374 98.4624 4 4 7 7 3635.62 388.502 6 -4 -7 -7 4219.56 353.556 4 4 7 8 4925.30 473.299 6 -4 -7 -8 5320.50 415.142 4 4 7 9 3066.85 382.040 6 4 7 10-177.312 91.3792 6 4 7 10 502.112 149.131 5 4 7 11-97.3372 121.571 6 4 7 11 402.412 137.192 5 4 7 12-90.7246 154.708 6 4 7 12 11.8376 42.5499 5 4 7 13 906.569 239.233 6 4 7 13 1477.71 216.868 5 4 7 14 335.923 175.146 6 4 7 14 62.0112 48.5201 5 4 7 15 2935.86 460.457 6 4 7 16 1875.28 384.665 6 4 8 -9 953.951 204.265 3 -4 -8 9 567.869 187.848 6 -4 -8 8-24.7682 67.6432 6 4 8 -8-63.8433 53.9895 3 4 8 -7 691.831 163.208 3 4 8 -6 264.292 110.922 5 4 8 -6 231.587 82.5562 3 4 8 -5-25.7001 61.3234 4 4 8 -5-28.3609 79.7571 5 4 8 -5-13.9835 41.5083 3 4 8 -4 975.115 201.935 4 4 8 -4 850.955 185.449 5 4 8 -4 979.454 158.307 3 4 8 -3 2089.85 215.669 3 4 8 -3 1632.65 256.799 5 4 8 -3 2047.21 275.196 4 4 8 -2 13330.4 650.718 4 4 8 -2 12247.1 685.588 5 4 8 -1 10549.3 554.039 4 4 8 -1 10788.1 640.395 5 4 8 0 2696.63 318.925 5 4 8 0 2963.78 204.554 3 4 8 0 2865.20 273.807 4 4 8 1 2656.77 318.993 5 4 8 1 2447.15 254.141 4 4 8 2 1333.76 180.236 4 4 8 3 593.676 125.170 4 -4 -8 -4 3253.10 291.000 4 4 8 4 3518.91 301.842 4 4 8 5-61.2238 57.2007 4 -4 -8 -5 47.7446 36.4969 4 -4 -8 -5 11.7271 19.5582 3 -4 -8 -6 17233.2 476.676 3 4 8 6 16260.8 707.868 4 -4 -8 -6 16926.1 708.736 4 4 8 7 11415.7 626.297 4 -4 -8 -7 12540.9 449.433 3 -4 -8 -7 11991.4 617.074 4 4 8 8 4586.66 473.747 6 4 8 9 73.4876 92.7953 6 4 8 10 273.969 130.125 6 4 8 11-2.84705 98.7013 6 4 8 12 103.839 96.0273 6 4 8 13-1.61591 147.218 6 4 8 13 131.427 89.9079 5 4 8 14 94.5725 122.879 6 4 8 14 115.340 73.5290 5 4 8 15 497.644 206.708 6 4 9 -8 105.452 86.0096 4 4 9 -7 353.166 129.292 4 4 9 -6-52.6332 108.192 4 4 9 -6 111.591 63.4656 5 4 9 -5 256.827 116.430 4 4 9 -5 222.052 95.5960 5 4 9 -4 103.641 93.2035 4 4 9 -4 87.0953 76.9364 5 4 9 -4 156.998 71.7266 3 4 9 -3 1971.66 289.068 4 4 9 -3 1850.57 289.058 5 4 9 -3 2305.43 221.727 3 4 9 -2 987.832 199.084 4 4 9 -2 1339.37 242.772 5 4 9 -1 2182.37 313.522 5 4 9 -1 2293.34 286.136 4 4 9 0 488.540 126.020 4 4 9 0 673.230 186.095 5 4 9 1 408.174 115.883 4 4 9 1 899.582 214.540 5 4 9 2-0.96755 54.9368 4 4 9 3 616.277 131.881 4 -4 -9 -3 695.787 125.581 1 4 9 4 3789.77 338.387 4 4 9 5 1895.77 247.451 4 -4 -9 -6 2617.59 162.023 3 4 9 6 2286.60 276.273 4 4 9 7 42.1918 71.8833 4 -4 -9 -7 229.262 51.5953 3 4 9 8 79.3531 97.4704 6 4 9 8-49.3673 69.8760 4 4 9 9 842.117 236.795 6 4 9 10 884.709 236.789 6 4 9 11 387.432 169.229 6 4 9 12 1193.69 290.674 6 4 9 13 4500.16 551.710 6 4 9 14 943.807 280.195 6 4 9 14 1005.57 211.016 5 4 10 -6 341.814 159.864 4 4 10 -5 1473.39 291.150 4 4 10 -5 863.824 210.628 5 4 10 -4 1671.60 291.347 5 4 10 -4 2176.97 351.473 4 4 10 -3 1265.19 247.467 4 4 10 -3 1460.55 280.398 5 4 10 -2-64.9748 65.7797 4 4 10 -2-27.9305 58.4757 5 4 10 -1-66.4806 75.6923 4 4 10 -1 90.4349 96.4675 5 4 10 0 12.7232 42.5182 4 4 10 0 145.064 119.127 5 4 10 1 315.031 129.988 5 4 10 1 363.046 122.099 4 4 10 2 9.87481 46.3864 4 4 10 3 927.649 185.403 4 -4 -10 -3 813.700 119.057 1 -4 -10 -4 5397.34 330.437 1 4 10 4 5275.03 433.889 4 4 10 5 4522.71 411.638 4 4 10 6 1403.84 235.125 4 4 10 7 5415.88 474.540 4 4 10 8-28.9419 80.0038 4 4 10 9 91.5092 117.250 6 4 10 10 153.107 150.531 6 4 10 11 138.732 114.734 6 4 10 12 1735.98 360.367 6 4 10 13 2777.47 453.720 6 4 11 -4 1667.46 311.794 4 4 11 -4 1083.41 247.769 5 4 11 -3 2486.39 373.807 4 4 11 -3 1724.26 309.731 5 4 11 -2 263.302 115.991 4 4 11 -2 215.664 124.224 5 4 11 -1 221.237 114.525 4 4 11 -1 175.792 118.881 5 4 11 0 370.896 140.229 4 4 11 0 256.738 133.736 5 4 11 1 730.764 184.045 4 4 11 1 1113.33 251.568 5 4 11 2 267.730 122.311 4 4 11 3 1462.04 245.564 4 4 11 4 1726.37 271.532 4 4 11 5 584.745 164.918 4 4 11 6 96.1363 80.5619 4 4 11 7 504.781 152.719 4 4 11 8 163.576 99.4998 4 4 11 9-5.93722 69.2731 4 4 11 9 127.183 124.464 6 4 11 10 2771.42 451.016 6 4 11 11 1956.91 391.435 6 4 11 12 150.525 123.039 6 4 12 -1 92.7611 83.5266 4 4 12 0 316.501 138.159 4 4 12 1 333.896 140.028 4 4 12 2 687.313 185.374 4 4 12 3 5.19844 54.9953 4 4 12 4 72.4656 70.5095 4 4 12 5 239.001 99.8656 4 4 12 6 113.925 64.3886 4 4 12 7-15.8861 51.6791 4 4 12 8 194.343 91.3680 4 4 12 9 746.264 205.418 4 4 12 9 827.557 258.353 6 4 13 3-58.0202 66.2884 4 4 13 4 83.1392 73.2873 4 4 13 5 215.437 116.411 4 4 13 6 26.3836 91.3332 4 4 13 7 158.895 99.9786 4 4 13 8 727.933 213.340 4 4 13 9 1778.70 327.339 4 -5 9 9 70.0605 81.5573 6 -5 9 8-97.3563 102.388 6 -5 8 10 483.774 169.862 6 -5 8 9 242.502 129.364 6 -5 8 8 792.657 226.194 4 -5 8 8 862.771 230.892 6 -5 8 7 1533.95 310.387 4 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5 9 -5 1305.85 208.857 3 5 9 -5 1209.49 243.996 4 5 9 -5 843.590 209.901 5 5 9 -4 4816.00 452.539 4 5 9 -4 4236.51 456.130 5 5 9 -4 5222.63 386.903 3 5 9 -3 199.415 82.1747 4 5 9 -3 452.526 148.464 5 5 9 -3 431.611 111.094 3 5 9 -2 316.452 86.7980 3 5 9 -2 307.130 99.1373 4 5 9 -2 287.420 107.502 5 5 9 -1 34.2066 41.2415 3 5 9 -1 26.8269 44.6079 4 5 9 -1 7.43799 104.851 5 5 9 0 437.223 117.216 4 5 9 0 650.656 177.381 5 5 9 1 261.259 88.1711 4 5 9 1 406.534 142.914 5 -5 -9 -1 280.810 106.542 1 5 9 2 961.129 162.418 4 5 9 2 772.169 80.1668 2 5 9 2 1093.56 227.752 5 -5 -9 -2 705.126 151.266 1 5 9 3 717.362 141.026 4 -5 -9 -3 504.356 115.408 1 5 9 3 845.817 202.723 5 5 9 4 912.759 166.511 4 -5 -9 -4 877.808 154.279 1 -5 -9 -5 8585.89 490.358 4 -5 -9 -5 8869.46 356.374 3 5 9 5 10094.4 644.538 5 5 9 5 7617.64 482.994 4 -5 -9 -5 8905.37 538.573 1 -5 -9 -6 3438.58 231.258 3 5 9 6 3585.75 382.598 5 5 9 6 2584.47 292.766 4 -5 -9 -6 3044.44 304.079 4 5 9 7 2352.56 321.859 5 -5 -9 -7 2342.73 198.086 3 -5 -9 -8 23.1306 29.4499 3 5 9 8 243.635 105.005 6 5 9 9 816.305 238.576 6 5 9 9 1331.27 243.186 5 5 9 10 1487.91 303.175 6 5 9 10 1404.52 247.243 5 5 9 11 1473.95 307.777 6 5 9 11 1842.13 279.510 5 5 9 12 2349.99 394.648 6 5 9 12 2698.50 339.426 5 5 9 13 658.088 216.084 6 5 9 13 1184.64 227.319 5 5 9 14 585.212 173.143 6 5 9 14 942.738 204.011 5 5 10 -6-91.6410 87.6738 5 5 10 -5 135.592 90.6920 5 5 10 -4 880.671 214.765 4 5 10 -4 410.905 150.957 5 5 10 -3 261.073 116.372 4 5 10 -3 626.158 191.065 5 5 10 -2 897.219 185.677 4 5 10 -2 497.629 167.198 5 5 10 -1 91.9400 80.9896 4 5 10 -1 74.3696 73.0419 5 5 10 0 570.138 147.529 4 5 10 0 539.154 168.505 5 5 10 1 5173.02 506.106 5 5 10 1 4581.07 389.081 4 5 10 2 1947.23 311.801 5 5 10 2 1763.17 238.671 4 -5 -10 -2 1543.16 210.982 1 -5 -10 -3 5296.35 385.739 1 5 10 3 6150.76 539.888 5 5 10 3 5543.20 418.875 4 -5 -10 -4 4843.06 374.335 1 5 10 4 6050.15 527.109 5 5 10 4 4915.91 404.560 4 5 10 5 3092.53 379.552 5 5 10 5 2466.02 295.126 4 -5 -10 -5 2583.12 284.794 1 5 10 6 83.6101 76.9564 4 -5 -10 -6 26.5774 69.6605 1 5 10 7 3654.97 404.117 5 5 10 7 2714.84 333.297 4 5 10 8 8.37742 97.6911 6 5 10 8 302.740 151.151 5 5 10 9 1911.09 352.857 6 5 10 9 2158.27 321.004 5 5 10 10 3126.33 460.531 6 5 10 10 4188.18 436.803 5 5 10 11 332.313 171.300 6 5 10 11 788.464 198.226 5 5 10 12 609.341 224.972 6 5 10 12 1151.88 230.536 5 5 10 13 352.103 174.228 6 5 10 13 526.558 174.151 5 5 10 14 332.837 145.195 5 5 11 -4 391.213 156.255 5 5 11 -3-91.0143 91.3120 5 5 11 -2 154.934 142.474 5 5 11 -1-1.82406 33.9354 4 5 11 -1 63.3726 98.8646 5 5 11 0 990.471 211.070 4 5 11 0 656.572 194.077 5 5 11 1 1278.36 220.974 4 5 11 1 1301.14 274.155 5 5 11 2 93.5326 71.1645 4 5 11 2 277.377 135.964 5 5 11 3-49.3974 54.7715 4 5 11 3 216.439 137.113 5 5 11 4 596.509 161.465 4 5 11 4 664.401 190.839 5 5 11 5 228.297 89.7561 4 5 11 5 750.478 210.259 5 5 11 6 38.2800 50.5159 4 5 11 6 477.836 192.667 5 5 11 7-7.16147 51.2334 4 5 11 7 489.434 173.574 5 5 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231.860 111.077 4 -8 4 3 382.585 136.008 1 -8 4 3 223.430 105.067 4 -8 4 2 654.181 164.897 4 -8 4 2 570.678 142.173 1 -8 4 1 5136.63 438.316 1 -8 4 1 4784.41 468.347 4 -8 4 0 2414.35 300.201 1 -8 4 0 2393.48 331.882 4 -8 4 -1-14.5208 70.4175 1 -8 4 -1 109.893 88.2660 4 -8 4 -2 332.278 126.380 4 -8 4 -2 493.243 133.005 1 -8 4 -3 134.438 93.6357 4 -8 4 -4 572.541 185.917 4 -8 4 -5-1.78343 87.9946 4 -8 4 -6 1416.99 287.613 4 8 -4 6 1297.27 248.479 6 8 -4 7 53.5249 52.9206 6 8 -4 8 497.584 173.527 6 8 -3 -10 1174.56 249.743 3 8 -3 -9 2084.46 309.819 3 8 -3 -8 1589.44 272.509 3 8 -3 -7 35.5845 43.7288 3 -8 3 7 161.792 104.747 4 -8 3 6 97.6727 91.2364 4 8 -3 -6 23.6293 61.6392 3 -8 3 5-98.4856 94.1416 4 -8 3 4 1822.62 293.216 1 -8 3 4 1864.18 269.135 4 -8 3 3 3235.14 377.329 1 -8 3 3 2659.64 318.369 4 -8 3 2 2988.24 351.640 1 -8 3 2 2399.70 300.228 4 -8 3 1 452.468 132.506 4 -8 3 1 361.545 119.113 1 -8 3 0 1462.41 251.717 1 -8 3 0 1713.89 258.267 4 -8 3 -1-33.1708 75.1321 1 -8 3 -1-25.8821 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5248.51 330.291 4 -8 0 0 1862.45 283.450 1 -8 0 0 1639.83 185.465 4 -8 0 -1 3328.27 199.840 6 -8 0 -1 3589.58 281.123 4 -8 0 -1 3267.46 373.057 1 -8 0 -2 5023.46 463.339 1 -8 0 -2 4756.55 336.833 4 -8 0 -2 4983.20 317.420 6 8 0 3 78.2150 50.5113 6 -8 0 -3 128.549 60.0709 6 -8 0 -3 37.4077 42.3769 4 8 0 4 2439.09 302.610 2 8 0 4 2005.21 222.032 6 -8 0 -4 2200.85 249.995 4 -8 0 -4 2477.72 292.927 6 8 0 5 5461.49 449.554 2 8 0 5 5416.53 397.869 6 -8 0 -5 5967.04 492.620 6 8 0 6 127.614 65.8466 6 8 0 6 193.472 92.7450 2 8 0 7-99.1430 87.4442 6 8 0 7-26.8497 52.8409 2 8 0 8 524.984 159.784 6 8 0 8 669.396 170.474 2 8 0 9 3922.62 405.448 2 8 0 9 3334.63 422.805 6 8 0 10 1922.30 334.062 6 8 0 10 2203.70 308.385 2 8 0 11 2239.63 368.879 6 8 0 11 2823.33 354.760 2 8 0 12 392.412 148.823 6 8 0 12 707.410 181.104 2 8 1 -10 1039.36 227.651 3 8 1 -9 726.379 185.682 3 8 1 -8 1972.92 295.724 3 8 1 -7 1585.12 257.471 3 8 1 -6 383.220 136.386 3 8 1 -5 21.1275 59.1161 3 -8 -1 5-0.40409 91.3065 1 8 1 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118.119 6 8 1 11 10.8719 53.1702 2 8 1 12 67.9523 111.030 6 8 1 12 174.980 94.0905 2 8 1 13-223.619 139.851 6 8 2 -10 1292.14 270.019 3 8 2 -9 3433.76 396.899 3 8 2 -8 81.5699 60.5692 3 8 2 -7 407.929 137.710 3 8 2 -6-14.2518 65.0160 3 -8 -2 5 203.266 136.876 1 8 2 -5 407.332 133.436 3 8 2 -4-29.1626 47.9818 3 8 2 -4 89.5900 40.2550 4 -8 -2 4-73.1990 94.6202 1 8 2 -3-4.76584 52.8260 3 -8 -2 3 92.6012 87.9865 1 -8 -2 2 2027.44 315.167 1 8 2 -2 2051.63 260.346 3 -8 -2 1 13394.6 770.493 1 8 2 -1 14986.9 675.484 3 -8 -2 0 25780.8 1058.46 1 -8 -2 0 24146.1 477.380 4 -8 -2 -1 4431.72 211.576 4 -8 -2 -1 4544.83 441.714 1 8 2 2 3827.54 342.806 2 -8 -2 -2 3759.53 398.490 1 -8 -2 -2 3872.20 212.788 4 8 2 3 666.247 90.5696 6 -8 -2 -3 708.416 103.993 4 8 2 3 757.745 157.537 2 -8 -2 -4 1058.56 135.465 4 -8 -2 -4 1453.18 177.996 6 8 2 4 1148.01 196.513 2 8 2 4 1297.78 164.012 6 8 2 5 466.165 121.157 6 -8 -2 -5 361.297 103.600 6 8 2 5 586.748 139.501 2 8 2 6 349.325 110.173 6 -8 -2 -6 234.775 95.7863 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130.100 2 8 3 6-45.3378 75.2217 6 -8 -3 -6 143.569 75.6883 6 8 3 6 60.2787 49.2052 2 -8 -3 -7 4578.68 417.469 6 8 3 7 5148.39 413.392 2 8 3 7 4489.17 393.886 6 8 3 8 2100.43 288.254 6 8 3 9 42.4846 79.0799 6 8 3 10 223.388 88.5388 6 8 3 11-55.2007 129.892 6 8 3 12 287.138 155.939 6 8 3 13 318.564 172.876 6 8 3 14 2124.48 389.285 6 8 4 -9 212.832 108.305 3 8 4 -8 97.8170 93.0703 3 8 4 -7 42.4281 42.4595 3 8 4 -6-27.2088 64.6742 3 -8 -4 5 3447.31 439.375 1 8 4 -5 4016.14 376.992 3 -8 -4 4 4314.00 470.378 1 8 4 -4 4345.24 382.370 3 -8 -4 3 6373.08 562.605 1 8 4 -3 7387.72 491.134 3 -8 -4 2 4524.50 457.787 1 8 4 -2 5355.05 411.806 3 8 4 -1 38.8402 67.7896 3 -8 -4 1 95.5325 81.2065 1 -8 -4 0 1488.00 263.319 1 -8 -4 -1 1810.52 295.273 1 8 4 2 518.934 69.6678 6 -8 -4 -2 671.991 164.003 1 8 4 2 654.415 136.092 2 8 4 2 419.489 53.4220 6 8 4 3 837.220 113.470 6 8 4 3 859.442 152.965 2 8 4 4 2880.22 294.051 2 -8 -4 -4 2543.95 155.336 4 8 4 4 2659.90 231.116 6 8 4 5 17707.4 715.727 2 8 4 5 16634.9 654.992 6 8 4 6 10610.2 569.948 2 8 4 6 11508.8 591.925 6 8 4 7 4838.45 411.475 6 8 4 8 47.1126 65.5162 6 8 4 9 11.0199 63.2664 6 8 4 10 304.320 119.380 6 8 4 11 3497.40 438.758 6 8 4 12 2021.98 351.141 6 8 4 13 793.491 239.310 6 8 4 14 823.207 257.582 6 8 5 -8-14.6595 56.6828 3 8 5 -7 328.991 124.852 3 8 5 -6 223.042 93.1002 3 8 5 -5 2413.93 293.616 3 -8 -5 4 5726.62 547.544 1 8 5 -4 6082.13 452.591 3 -8 -5 3 3934.10 444.871 1 8 5 -3 4225.44 369.786 3 -8 -5 2 1556.94 279.178 1 8 5 -2 1599.61 228.924 3 8 5 -2 1371.99 136.678 6 8 5 -1 455.750 122.753 3 8 5 -1 359.335 66.4752 6 8 5 -1 283.601 59.2502 6 -8 -5 1 435.445 159.267 1 8 5 0 79.0496 29.8955 6 8 5 0 23.2226 22.2525 6 8 5 1 131.400 44.2670 6 8 5 1 157.255 49.8617 6 -8 -5 -1 84.0123 104.109 1 8 5 2 5549.68 375.155 2 8 5 2 4860.09 230.955 6 -8 -5 -2 5505.15 496.105 1 8 5 2 6192.03 322.845 6 8 5 3 7778.99 453.018 2 -8 -5 -3 7947.77 594.344 1 8 5 3 8609.43 416.861 6 8 5 4-19.0518 46.5095 6 8 5 4 99.1339 59.8655 2 8 5 5 10385.8 540.208 2 -8 -5 -5 10011.5 324.761 4 8 5 5 11310.6 562.042 6 -8 -5 -6-62.5555 39.5427 4 8 5 6-26.4382 82.7235 6 -8 -5 -7 529.004 113.963 4 8 5 7 464.052 144.332 6 8 5 8 588.489 163.630 6 -8 -5 -8 615.244 130.527 4 8 5 9 55.8017 92.5444 6 8 5 10 2954.61 382.922 6 8 5 11 1842.35 319.818 6 8 5 12 2584.06 402.901 6 8 5 13 731.209 217.277 6 8 5 14 23.4427 103.499 6 8 5 15 183.081 145.026 6 8 6 -8 271.839 114.469 3 8 6 -7 4889.90 450.977 3 8 6 -6 1831.24 263.725 3 8 6 -5 3305.35 346.848 3 -8 -6 4 2599.34 386.829 1 8 6 -4 3132.52 326.712 3 -8 -6 3 3016.27 404.348 1 8 6 -3 2648.68 296.698 3 8 6 -2-31.3230 79.0234 3 -8 -6 2 51.3847 84.9007 1 8 6 -1 104.544 55.8187 3 8 6 -1 207.657 67.9133 6 -8 -6 1 36.7705 84.6115 1 8 6 0 210.705 65.0598 6 -8 -6 0 59.6880 70.2296 1 -8 -6 -1-59.9734 98.0049 1 8 6 1 41.4814 33.3659 6 8 6 1 46.3105 44.4474 6 8 6 2 1616.02 203.622 6 8 6 2 1490.11 188.672 2 8 6 2 1259.63 142.731 6 -8 -6 -2 1516.59 262.500 1 8 6 3 4573.06 353.447 6 8 6 3 4061.84 313.960 2 -8 -6 -3 4138.75 445.415 1 8 6 4 3154.45 304.469 6 8 6 4 2949.90 281.254 2 -8 -6 -5 267.637 42.5603 4 8 6 5 355.120 115.348 6 8 6 5 416.967 106.331 2 8 6 6 995.816 188.952 6 -8 -6 -6 1034.19 119.502 4 8 6 7 1524.93 246.049 6 -8 -6 -7 1257.96 158.148 4 -8 -6 -8 1062.08 163.881 4 8 6 8 1118.20 225.559 6 -8 -6 -9-59.2387 68.3192 4 8 6 9 99.7778 89.1918 6 8 6 10 939.484 236.594 6 8 6 11 1450.18 284.531 6 8 6 12 1370.84 290.113 6 8 6 13 237.456 116.678 6 8 6 14-127.851 128.739 6 8 6 15-202.703 165.960 6 8 7 -7 39.1501 67.4000 3 8 7 -6 876.426 189.392 3 8 7 -5-41.2986 60.4515 3 8 7 -4 176.436 87.1768 3 8 7 -3 29.4577 75.8725 3 -8 -7 3-203.393 155.799 1 8 7 -2 1001.17 184.123 3 -8 -7 2 1194.81 251.298 1 8 7 -1 83.7814 75.2442 3 -8 -7 1 48.3032 87.5148 1 -8 -7 0 3330.74 403.754 1 -8 -7 -1 330.254 141.832 1 8 7 2 1070.31 156.552 2 8 7 2 958.227 190.632 6 -8 -7 -2 1066.23 225.561 1 8 7 3 7093.92 491.832 6 8 7 3 6958.74 403.628 2 8 7 3 5571.01 350.837 6 -8 -7 -3 7130.81 582.273 1 8 7 4 2448.61 289.891 6 8 7 4 1972.46 222.279 2 -8 -7 -4 1664.18 295.231 1 8 7 5 193.775 73.2916 2 8 7 5 205.711 59.9894 6 -8 -7 -6 151.725 46.2107 4 8 7 6 379.977 132.409 6 8 7 7 3428.93 381.349 6 8 7 8 2316.21 323.401 6 8 7 9 900.477 206.842 6 8 7 10 268.348 117.300 6 8 7 11 270.332 159.656 6 8 7 12 337.850 158.965 6 8 7 13 517.633 189.771 6 8 7 14 129.740 134.677 6 8 8 -7 148.030 96.4206 3 8 8 -6 187.636 94.4738 3 8 8 -5 322.937 124.714 3 8 8 -4 253.449 102.124 3 8 8 -3 80.2977 54.6894 3 8 8 -2 1379.61 222.171 3 -8 -8 2 1052.68 241.269 1 8 8 -1 585.669 138.921 3 -8 -8 1 796.649 206.630 1 -8 -8 0 381.501 142.092 1 -8 -8 -1 440.852 168.956 1 -8 -8 -2 333.502 122.843 1 8 8 3 128.281 52.3040 6 8 8 3 218.713 76.8344 2 -8 -8 -3 31.6136 78.8787 1 8 8 4 1939.33 285.484 6 8 8 4 1917.54 212.688 2 -8 -8 -4 1684.75 289.204 1 8 8 5 2957.79 364.382 6 8 8 5 3001.76 273.960 2 -8 -8 -5 3365.51 413.352 1 8 8 6 2520.65 345.632 6 8 8 7 5659.56 521.124 6 8 8 8 3962.88 453.565 6 8 8 9 465.322 168.219 6 8 8 10-95.3104 129.044 6 8 8 11 51.2325 84.1021 6 8 8 12-93.4803 101.738 6 8 8 13 245.711 150.773 6 8 8 14 357.335 170.317 6 8 9 -6-201.752 101.722 3 8 9 -5 298.393 121.854 3 8 9 -4 874.590 187.662 3 8 9 -3 1407.11 230.962 3 -8 -9 2 5236.41 546.932 1 8 9 -2 7224.49 512.845 3 -8 -9 1 2747.80 386.622 1 -8 -9 0 270.234 126.815 1 -8 -9 -1-70.0521 89.5024 1 -8 -9 -2 585.752 181.116 1 8 9 2 596.294 172.094 5 -8 -9 -3 244.354 126.101 1 8 9 3 278.618 90.2699 5 8 9 3 266.799 76.3892 2 8 9 4 190.246 69.8243 2 8 9 4 212.438 116.524 5 -8 -9 -4 41.6964 85.7999 1 8 9 5 725.351 132.203 2 8 9 5 838.774 210.226 6 8 9 5 673.758 180.324 5 -8 -9 -5 746.879 207.004 1 8 9 6 425.747 159.475 6 8 9 6 644.962 185.520 5 -8 -9 -6 516.045 176.838 1 8 9 7 389.020 154.275 6 8 9 7 381.553 158.018 5 8 9 8 907.735 239.655 6 8 9 8 845.941 233.404 5 8 9 9 349.483 146.387 6 8 9 9 155.794 110.032 5 8 9 10 1007.08 240.749 6 8 9 10 915.952 220.026 5 8 9 11 4.88725 89.7249 6 8 9 12 104.065 128.979 6 8 9 13 658.849 226.598 6 8 9 14 3057.57 496.936 6 -8 -10 1 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312.663 1 8 11 5 1797.73 341.703 5 8 11 6 391.482 192.154 6 8 11 6 542.044 173.164 5 -8 -11 -6 177.351 80.0473 1 8 11 7 142.370 85.9603 6 8 11 7-110.827 119.841 5 -8 -11 -7 100.603 117.267 1 8 11 8 367.577 153.463 6 8 11 8 758.408 213.239 5 -8 -11 -8 797.044 231.567 1 8 11 9 180.717 128.402 6 8 11 9 241.891 111.105 5 8 11 10 1411.97 317.917 6 8 11 10 1447.67 297.455 5 8 11 11 264.748 146.544 6 8 11 11 487.267 178.136 5 8 11 12 669.508 222.802 5 8 11 13 276.942 140.469 5 8 12 6 429.473 175.424 6 8 12 7 252.755 157.790 6 8 12 8 696.994 235.520 6 8 12 9 1259.14 321.827 6 -9 5 6 573.272 184.965 4 -9 5 5 229.740 121.810 4 -9 5 4 404.151 159.147 4 -9 5 3-50.4627 70.6815 4 -9 5 2 1131.31 260.721 4 -9 5 1 3351.28 439.494 4 -9 5 0 827.527 224.857 4 -9 5 -1 732.796 227.206 4 -9 5 -2 103.659 56.5824 4 9 -4 -8 77.7647 76.8007 3 -9 4 7 31.9237 52.6099 4 -9 4 6 26.3757 50.4468 4 -9 4 5-71.9955 92.2066 4 -9 4 4 4262.59 459.523 4 -9 4 3 188.966 94.6603 4 -9 4 2 344.493 125.069 4 -9 4 1 467.963 154.706 4 -9 4 0 875.650 215.830 4 -9 4 -1-4.27710 67.6411 4 -9 4 -2 47.3057 67.6886 4 -9 4 -3 120.803 54.7475 4 -9 4 -4 188.312 79.3451 4 -9 4 -5 131.133 84.6220 4 9 -3 -8 108.582 98.7706 3 9 -3 -7 1405.85 264.518 3 -9 3 6 1854.15 296.304 4 -9 3 5 607.040 167.662 4 -9 3 4 744.660 178.638 4 -9 3 4 1051.79 234.752 1 -9 3 3 1084.34 215.933 4 -9 3 3 1175.45 238.899 1 -9 3 2 203.037 113.125 4 -9 3 2 191.575 102.083 1 -9 3 1 11.8242 56.6685 4 -9 3 1 73.5112 87.8707 1 -9 3 0 52.0187 52.8861 4 -9 3 0 70.5048 69.9817 1 -9 3 -1 120.287 56.7027 1 -9 3 -1 207.544 87.3698 4 -9 3 -2 806.375 203.970 4 -9 3 -2 754.941 198.272 1 -9 3 -3 1124.73 235.256 4 -9 3 -3 875.023 220.225 1 -9 3 -4 249.220 120.289 4 -9 3 -4 440.309 152.294 1 -9 3 -5 1117.16 240.947 4 -9 3 -5 681.595 173.773 1 -9 3 -6 677.785 193.303 4 -9 3 -7 934.784 237.889 4 9 -2 -9-16.6100 56.2729 3 9 -2 -8 6.68177 47.9435 3 9 -2 -7 1373.41 256.148 3 9 -2 -6 3488.19 399.646 3 -9 2 5 379.126 125.625 4 -9 2 4 615.529 151.554 4 -9 2 4 686.335 197.358 1 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1635.12 293.691 1 -9 1 0 1614.69 218.479 4 -9 1 -1 6444.75 579.575 1 -9 1 -1 6837.03 459.358 4 -9 1 -2 2076.27 331.738 1 -9 1 -2 2353.51 278.609 4 -9 1 -3 855.257 174.993 4 -9 1 -3 824.841 207.944 1 -9 1 -4 83.3680 75.3543 4 9 -1 4-5.39947 39.3424 6 9 -1 5 45.9332 38.7214 6 -9 1 -5 11.9422 39.9186 4 9 -1 6-1.12592 49.0170 6 -9 1 -6 40.9952 47.8646 4 9 -1 7 202.903 108.240 6 -9 1 -7 117.352 75.9331 4 9 -1 7 116.777 87.7216 2 9 -1 8 2902.40 369.010 2 9 -1 8 2477.40 330.852 6 9 -1 9 631.685 168.009 6 9 -1 9 642.390 176.724 2 9 -1 10 1131.05 249.560 6 9 -1 11 801.008 237.202 6 9 0 -9 1668.14 299.978 3 9 0 -8 5197.47 508.677 3 9 0 -7-14.9702 70.6688 3 9 0 -6 1410.09 256.758 3 -9 0 5 2703.08 397.745 1 9 0 -5 3110.18 370.961 3 -9 0 4 387.963 165.024 1 9 0 -4 324.887 119.144 3 -9 0 3 240.439 137.745 1 -9 0 3 279.670 102.727 4 -9 0 2 11.2286 41.8567 4 -9 0 2-25.4547 92.3204 1 -9 0 1 792.902 201.556 1 -9 0 1 1018.88 155.964 4 -9 0 0 1441.18 270.863 1 -9 0 0 1566.87 192.179 4 -9 0 -1 17.0587 30.2859 4 -9 0 -1-51.9476 111.368 1 -9 0 -2 81.0891 52.8287 4 -9 0 -2-26.6337 77.8668 1 -9 0 -3 44.9706 45.2054 4 -9 0 -3-36.5583 90.2315 1 9 0 4-29.5348 41.7814 6 -9 0 -4 23.6252 55.1308 4 9 0 5 42.7029 35.8411 6 -9 0 -5 36.5923 36.3238 4 9 0 5-8.20525 50.9282 2 9 0 6 124.498 81.7463 6 -9 0 -6 34.4305 51.1469 4 9 0 6 148.112 98.5732 2 9 0 7 2547.22 334.817 2 9 0 7 1998.72 276.198 6 9 0 8 6436.61 533.352 2 9 0 8 5608.89 502.473 6 9 0 9 1445.20 271.885 6 9 0 9 1702.26 276.969 2 9 0 10 532.603 182.713 6 9 0 10 644.125 181.923 2 9 0 11-243.569 133.241 6 9 0 12-27.0417 79.7402 6 9 1 -8 531.799 170.890 3 9 1 -7 1163.73 233.104 3 9 1 -6 508.758 143.266 3 9 1 -5 869.797 192.169 3 -9 -1 5 932.022 227.854 1 -9 -1 4 238.279 110.821 1 9 1 -4 834.651 181.980 3 9 1 -3 389.525 138.360 3 -9 -1 3 295.331 144.576 1 -9 -1 2 6195.57 563.991 1 -9 -1 1 13555.4 825.329 1 -9 -1 1 13070.2 484.615 4 -9 -1 0 2914.46 385.490 1 -9 -1 0 3182.61 238.289 4 -9 -1 -1 7.24442 30.8713 4 -9 -1 -1-144.072 138.942 1 -9 -1 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15895.5 707.408 2 -9 -4 -3 17702.5 946.299 1 9 4 4 4609.28 389.572 2 -9 -4 -4 4401.20 173.585 4 -9 -4 -4 3485.01 137.937 4 9 4 4 4713.49 278.235 6 9 4 5 4111.58 374.205 2 9 4 5 3986.79 302.196 6 9 4 6 2153.32 274.656 2 9 4 6 2109.27 244.931 6 9 4 7 424.247 125.868 6 9 4 7 337.274 113.981 2 9 4 8 1089.69 207.425 6 9 4 8 918.773 193.392 2 9 4 9 141.762 78.0039 2 9 4 9 36.9804 66.0917 6 9 4 10 1213.15 247.425 6 9 4 11 2405.18 368.908 6 9 4 12 1338.14 292.949 6 9 4 13 239.416 158.729 6 9 4 14-171.213 131.034 6 9 5 -7 2311.68 315.903 3 9 5 -6 1151.27 222.117 3 9 5 -5 1630.47 262.161 3 -9 -5 5 1327.90 281.114 1 9 5 -4 23.7432 47.9453 3 -9 -5 4 90.0028 76.6101 1 9 5 -3 790.934 175.976 3 -9 -5 3 1130.44 250.297 1 -9 -5 2 598.929 206.689 1 9 5 -2 617.014 155.397 3 -9 -5 1 1168.19 257.855 1 9 5 -1 1390.85 227.302 3 -9 -5 0 79.9835 79.8907 1 -9 -5 -1 539.932 176.632 1 -9 -5 -2 1415.18 275.395 1 9 5 2 788.040 76.9181 6 9 5 2 1209.24 102.771 6 9 5 3 1284.47 197.701 2 -9 -5 -3 910.233 222.493 1 9 5 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2 3 215.331 148.666 1 -10 2 2 303.966 134.830 1 -10 2 1 1138.22 253.152 1 -10 2 0 291.640 114.289 4 -10 2 0 280.191 125.057 1 -10 2 -1 1795.26 315.836 1 -10 2 -1 1766.57 268.269 4 -10 2 -2 2228.88 349.968 1 -10 2 -2 2635.80 337.781 4 -10 2 -3 125.241 71.8336 4 -10 2 -3 312.689 146.448 1 -10 2 -4 78.1381 88.2061 4 -10 2 -4 38.6091 64.6873 1 -10 2 -5 234.959 116.369 4 -10 2 -5 388.482 177.769 1 -10 2 -6 1180.49 246.312 4 -10 2 -7 230.989 118.751 4 10 -1 -6-60.1732 99.7515 3 -10 1 5-70.8861 91.3353 1 -10 1 4 137.413 104.678 1 -10 1 3 87.2030 93.7602 1 -10 1 2 555.345 175.205 1 -10 1 1 3524.67 450.524 1 -10 1 0 2797.00 391.816 1 -10 1 -1 650.571 187.026 1 -10 1 -1 693.391 153.922 4 -10 1 -2 506.230 137.990 4 -10 1 -2 283.670 127.718 1 -10 1 -3-59.8058 57.1530 4 -10 1 -3 89.2248 127.146 1 -10 1 -4-65.8424 58.2457 4 -10 1 -4 97.1088 112.660 1 -10 1 -5 107.627 53.0786 4 -10 1 -5 144.431 106.666 1 -10 1 -6 979.567 202.316 4 -10 1 -7 812.808 191.740 4 -10 1 -8 2069.84 310.139 4 -10 1 -9 3753.52 431.015 4 10 0 -6 154.232 104.671 3 10 0 -5 1602.26 288.646 3 -10 0 5 1129.19 276.159 1 -10 0 4 145.366 146.221 1 -10 0 3 348.323 157.723 1 -10 0 2 272.606 145.107 1 -10 0 1 537.431 164.322 1 -10 0 0 2943.45 418.217 1 -10 0 -1 90.5505 87.9114 1 -10 0 -2-21.4986 39.1869 4 -10 0 -2-8.56915 87.6805 1 -10 0 -3 176.824 77.6857 4 -10 0 -3 203.984 147.789 1 -10 0 -4 2172.42 364.511 1 -10 0 -4 2231.36 268.776 4 -10 0 -5 2340.42 290.758 4 -10 0 -6 883.659 177.063 4 10 0 7 3051.49 387.551 2 -10 0 -7 2376.12 308.586 4 -10 0 -8-151.620 86.2261 4 10 1 -6 844.043 215.493 3 -10 -1 5 1891.10 348.918 1 10 1 -5 2325.07 341.204 3 -10 -1 4 4576.19 540.275 1 10 1 -4 5491.22 509.422 3 -10 -1 3 3476.51 463.363 1 -10 -1 2 735.957 217.855 1 -10 -1 1 12.7668 120.067 1 -10 -1 0-184.001 122.619 1 -10 -1 -1 506.894 195.268 1 -10 -1 -2 595.800 175.653 1 -10 -1 -3 1338.53 280.869 1 -10 -1 -3 1324.93 176.324 4 -10 -1 -4 1233.78 250.031 1 -10 -1 -4 1708.44 214.193 4 -10 -1 -5 1089.37 179.243 4 -10 -1 -6 362.411 111.114 4 10 1 6 324.352 105.227 2 -10 -1 -7 478.811 129.275 4 10 1 7 708.382 180.780 2 10 1 8 65.1316 61.1840 2 10 2 -6 1789.59 300.685 3 10 2 -5 1401.82 263.796 3 -10 -2 5 869.166 248.256 1 10 2 -4-118.386 119.003 3 -10 -2 4-71.2242 77.0212 1 -10 -2 3 2326.42 388.222 1 10 2 -3 2887.44 363.963 3 -10 -2 2 1707.62 320.307 1 -10 -2 1-439.999 175.492 1 -10 -2 0 7.55421 97.4203 1 -10 -2 -1-131.388 134.714 1 -10 -2 -2 4644.99 535.187 1 -10 -2 -3 915.812 242.306 1 -10 -2 -4 4107.62 490.428 1 10 2 5 2716.14 339.200 2 -10 -2 -5 2497.93 243.176 4 -10 -2 -6 413.275 102.690 4 10 2 6 421.460 146.728 2 10 2 7 25.8489 54.3919 2 10 2 8 696.854 178.982 2 10 2 9 783.698 190.204 2 10 3 -6 715.706 180.298 3 10 3 -5 1542.72 269.867 3 -10 -3 5 1280.92 299.755 1 10 3 -4 1641.72 280.847 3 -10 -3 4 1393.08 293.581 1 10 3 -3 580.418 169.251 3 -10 -3 3 682.935 212.585 1 -10 -3 2 414.060 174.345 1 -10 -3 1-49.6009 125.873 1 -10 -3 0-369.071 162.780 1 -10 -3 -1 855.189 231.402 1 -10 -3 -2 5121.90 553.795 1 -10 -3 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220.633 6 10 4 10 910.968 203.600 2 10 4 11 660.158 183.955 6 10 4 12 126.617 88.9278 6 10 4 13-209.158 132.637 6 10 5 -5 307.448 119.209 3 -10 -5 5 469.830 175.833 1 10 5 -4 31.8768 55.9195 3 -10 -5 4-11.8698 94.6909 1 10 5 -3 60.8597 85.4823 3 -10 -5 3 90.1361 137.167 1 10 5 -2 6.08803 44.1843 3 -10 -5 2 160.592 83.3283 1 -10 -5 1 2083.18 362.603 1 -10 -5 0 3430.22 453.638 1 -10 -5 -1 276.280 135.398 1 -10 -5 -2-151.744 160.285 1 -10 -5 -3 434.338 170.274 1 10 5 3 147.649 87.0526 2 -10 -5 -4 725.404 217.589 1 10 5 4 806.098 167.795 2 10 5 5-11.9054 43.5993 2 10 5 6 619.530 153.969 2 10 5 7 1907.08 281.116 2 10 5 7 1741.60 235.843 6 10 5 8 1424.38 235.592 6 10 5 8 1527.55 253.806 2 10 5 9 4485.92 441.438 2 10 5 9 3277.47 376.428 6 10 5 10 666.435 180.126 6 10 5 10 870.696 198.351 2 10 5 11 17.7872 82.0766 2 10 5 11-23.4546 92.3558 6 10 5 12-72.7327 133.513 6 10 5 13 86.8786 86.8804 6 10 6 -5-242.621 113.552 3 10 6 -4 115.371 76.3399 3 -10 -6 4-307.122 158.763 1 10 6 -3 767.555 190.912 3 -10 -6 3 842.976 232.972 1 -10 -6 2 2944.57 438.236 1 10 6 -2 3741.65 399.489 3 -10 -6 1 949.868 248.277 1 -10 -6 0 1195.99 281.623 1 -10 -6 -1 301.543 128.364 1 -10 -6 -2 1174.05 278.039 1 10 6 3 25.5384 50.4156 2 -10 -6 -3 62.7203 83.2039 1 -10 -6 -4 257.686 143.086 1 10 6 4 343.960 115.124 2 10 6 5 270.206 101.990 2 -10 -6 -5 200.777 150.495 1 10 6 6 278.064 102.315 2 10 6 7 4956.41 436.167 2 10 6 7 4341.32 390.329 6 10 6 8 4244.44 406.497 2 10 6 8 3764.53 390.330 6 10 6 9 1504.80 255.466 2 10 6 9 998.390 209.761 6 10 6 10-167.945 115.950 6 10 6 11 48.3494 89.3763 6 10 6 12 670.365 189.836 6 10 6 13 717.602 205.264 6 10 6 14 2129.07 388.501 6 -10 -7 4 1929.74 374.472 1 10 7 -4 2310.79 328.957 3 10 7 -3 2314.86 325.088 3 -10 -7 3 2027.09 371.740 1 10 7 -2 2470.32 324.325 3 -10 -7 2 2393.78 401.046 1 -10 -7 1 19.6047 87.0323 1 -10 -7 0 349.583 170.434 1 -10 -7 -1 1005.24 262.689 1 -10 -7 -2-19.6991 76.5288 1 10 7 3-70.4186 71.7762 2 -10 -7 -3-179.509 130.490 1 10 7 4 401.036 122.367 2 -10 -7 -4 302.713 129.950 1 10 7 5 2078.32 261.681 2 -10 -7 -5 2011.39 356.520 1 10 7 6 845.251 177.768 2 10 7 7 1155.93 226.631 6 10 7 7 1025.33 197.055 2 10 7 8 35.1113 75.3778 6 10 7 8-96.0924 71.3942 2 10 7 9-32.7496 73.9962 2 10 7 9-8.77669 71.2114 6 10 7 10 345.740 150.805 6 10 7 11 116.174 106.253 6 10 7 12 162.609 97.4772 6 10 7 13 27.5628 71.5855 6 10 7 14 34.0541 158.458 6 10 8 -4 3206.63 397.397 3 10 8 -3 538.311 161.013 3 -10 -8 3 235.610 132.492 1 -10 -8 2 739.971 238.874 1 -10 -8 1 182.211 109.898 1 -10 -8 0-37.9723 116.234 1 -10 -8 -1 1656.20 326.925 1 -10 -8 -2 1976.48 361.559 1 -10 -8 -3 706.813 215.414 1 10 8 4 432.103 113.167 2 -10 -8 -4 348.198 153.047 1 10 8 5 2396.24 272.911 2 -10 -8 -5 2254.58 387.433 1 10 8 6 118.396 63.5898 2 -10 -8 -6 117.401 117.420 1 10 8 7-348.952 131.785 6 10 8 7 38.2194 49.8030 2 10 8 8 460.592 158.040 6 10 8 8 108.333 84.0592 2 10 8 9 172.534 129.072 6 10 8 10 488.348 171.484 6 10 8 11 79.5135 115.055 6 10 8 12 255.793 130.743 6 10 8 13 515.690 204.589 6 10 9 -3 40.1028 52.4808 3 -10 -9 2 815.430 238.128 1 -10 -9 1 137.959 108.275 1 -10 -9 0 133.194 127.968 1 -10 -9 -1 772.138 226.375 1 -10 -9 -2 3129.27 453.730 1 -10 -9 -3 1571.33 320.298 1 10 9 4 494.247 123.491 2 -10 -9 -4 319.265 150.889 1 10 9 5 239.363 89.4143 2 -10 -9 -5-11.8045 108.161 1 10 9 6 172.433 80.7725 2 -10 -9 -6 411.175 183.936 1 10 9 7-21.1969 67.5172 2 -10 -9 -7-113.557 103.538 1 10 9 8 262.336 101.007 6 10 9 8 311.138 107.347 2 10 9 9 519.993 171.553 6 10 9 10 5718.37 593.589 6 10 9 11 1098.23 277.008 6 10 9 12 469.081 206.969 6 10 9 13 113.493 114.311 6 -10 -10 1-221.695 143.031 1 -10 -10 0 1547.08 334.400 1 -10 -10 -1 576.421 215.531 1 -10 -10 -2 1402.81 305.479 1 -10 -10 -3 953.998 249.800 1 -10 -10 -4 73.1367 96.9339 1 -10 -10 -5 38.0736 84.6683 1 -10 -10 -6 119.477 124.596 1 10 10 7 746.419 156.268 2 -10 -10 -7 405.672 179.274 1 10 10 8 1933.53 263.079 2 -10 -10 -8 1925.92 383.193 1 10 10 9 532.697 153.526 6 10 10 10 528.503 154.642 6 10 10 11 83.5391 104.723 6 10 10 12 269.752 135.839 6 -10 -11 -1 675.629 227.226 1 -10 -11 -2-165.567 127.111 1 -10 -11 -3 839.117 257.395 1 -10 -11 -4 40.1485 90.9049 1 -10 -11 -5-17.0548 77.9872 1 -10 -11 -6 65.3078 83.6030 1 -10 -11 -7 1077.59 283.698 1 -10 -11 -8 3187.41 476.739 1 -10 -11 -9 472.538 199.704 1 -11 2 4-206.115 128.591 1 -11 2 3 261.019 135.786 1 -11 2 2 605.323 195.732 1 -11 2 1 2309.25 380.620 1 -11 2 0 482.744 185.943 1 -11 2 -1 811.807 216.787 1 -11 2 -2 259.484 136.924 1 -11 1 4 24.3513 72.9951 1 -11 1 3 1379.96 312.202 1 -11 1 2 4182.22 518.196 1 -11 1 1 504.188 184.663 1 -11 1 0 379.197 150.871 1 -11 1 -1 167.292 120.656 1 -11 1 -2-381.474 169.818 1 -11 1 -3-184.519 124.021 1 -11 1 -4 687.116 229.271 1 -11 1 -5 2418.75 394.337 1 -11 1 -6 2817.94 432.779 1 -11 0 4 1589.15 337.693 1 -11 0 3 646.418 222.858 1 -11 0 2 2201.27 387.580 1 -11 0 1 760.264 234.169 1 -11 0 0-133.014 117.063 1 -11 0 -1 772.727 228.653 1 -11 0 -2-144.430 98.6944 1 -11 0 -3 1043.35 271.722 1 -11 0 -4 912.135 258.150 1 -11 0 -5 1102.14 280.804 1 -11 0 -6 1051.69 260.901 1 -11 -1 4 1305.67 313.931 1 -11 -1 3 476.197 193.368 1 -11 -1 2-74.8980 111.061 1 -11 -1 1-260.884 145.519 1 -11 -1 0 132.578 102.623 1 -11 -1 -1 109.191 110.573 1 -11 -1 -2-98.7509 110.591 1 -11 -1 -3 1599.84 340.099 1 -11 -1 -4 1769.49 342.797 1 -11 -1 -5 335.300 164.082 1 -11 -2 4 1371.43 311.555 1 -11 -2 3 273.290 135.579 1 -11 -2 2-44.1675 89.6172 1 -11 -2 1 109.449 106.711 1 -11 -2 0 210.767 141.286 1 -11 -2 -1 335.740 165.646 1 -11 -2 -2 3687.42 493.942 1 -11 -2 -3 341.538 155.524 1 -11 -2 -4 527.157 200.618 1 -11 -2 -5 415.535 183.015 1 11 2 6 142.613 108.114 2 -11 -3 4 600.561 219.772 1 -11 -3 3 58.5934 83.2173 1 -11 -3 2-87.6676 107.031 1 -11 -3 1 386.744 162.372 1 -11 -3 0 1045.99 264.302 1 -11 -3 -1 2722.19 421.871 1 -11 -3 -2 281.587 172.232 1 -11 -3 -3 814.210 235.161 1 -11 -3 -4 524.918 200.553 1 11 3 5 400.645 142.586 2 -11 -3 -5 575.458 195.460 1 11 3 6 882.351 199.101 2 11 3 7 227.739 106.188 2 -11 -4 3 2794.17 442.635 1 -11 -4 2 1099.34 292.197 1 -11 -4 1 3303.84 482.763 1 -11 -4 0 559.272 201.500 1 -11 -4 -1 225.537 150.051 1 -11 -4 -2-184.044 150.416 1 -11 -4 -3-8.25378 107.628 1 -11 -4 -4 1249.17 304.156 1 11 4 5-86.2197 91.6936 2 -11 -4 -5 25.7954 77.8939 1 11 4 6 159.916 79.2301 2 11 4 7 1065.95 223.001 2 11 4 8 1900.85 295.980 2 11 5 -3 1555.50 288.216 3 -11 -5 2 1161.93 301.443 1 -11 -5 1 357.583 175.172 1 -11 -5 0 145.567 112.016 1 -11 -5 -1 214.892 148.692 1 -11 -5 -2 666.581 219.049 1 -11 -5 -3 82.5841 107.542 1 -11 -5 -4 576.845 227.142 1 11 5 4 810.635 186.286 2 -11 -5 -5 1000.13 261.734 1 11 5 5 1415.04 239.703 2 11 5 6 1858.66 279.078 2 11 5 7 3525.41 389.368 2 11 5 8 1525.18 264.323 2 11 5 9-37.9433 60.7527 2 -11 -6 2-100.763 138.365 1 -11 -6 1-120.105 111.160 1 -11 -6 0 217.882 147.399 1 -11 -6 -1 175.245 108.293 1 -11 -6 -2 892.211 257.606 1 -11 -6 -3 205.927 135.490 1 11 6 4 2504.13 306.611 2 -11 -6 -4 2468.18 409.987 1 11 6 5 4200.31 403.905 2 -11 -6 -5 4482.24 550.177 1 11 6 6 1879.18 274.845 2 -11 -6 -6 2090.11 375.523 1 11 6 7-134.022 82.5507 2 11 6 8 54.2738 48.2628 2 11 6 9 208.268 114.377 2 -11 -7 1-114.009 117.967 1 -11 -7 0 117.464 119.631 1 -11 -7 -1 285.578 157.800 1 -11 -7 -2 1083.32 273.730 1 -11 -7 -3 2134.65 390.876 1 11 7 4 236.659 98.9010 2 -11 -7 -4 78.6949 95.9611 1 11 7 5 399.367 119.183 2 -11 -7 -5 199.837 108.267 1 -11 -7 -6 416.107 193.943 1 11 7 6 251.920 122.045 2 11 7 7 1.00374 42.5610 2 11 7 8 265.766 117.691 2 11 7 9 212.133 111.593 2 -11 -8 0 622.092 196.668 1 -11 -8 -1 542.166 211.138 1 -11 -8 -2 1099.36 272.128 1 -11 -8 -3 1029.50 278.336 1 -11 -8 -4 310.755 166.337 1 11 8 5 372.042 120.350 2 -11 -8 -5 435.972 187.540 1 -11 -8 -6 98.7975 124.171 1 11 8 6-18.0961 41.2568 2 11 8 7-57.6445 70.4567 2 -11 -8 -7-140.551 126.502 1 11 8 8 26.7292 36.6177 2 11 8 9 1532.49 254.938 2 -11 -9 -2 1580.24 340.562 1 -11 -9 -3 624.288 217.441 1 -11 -9 -4 243.606 138.984 1 11 9 5 68.7261 50.9741 2 -11 -9 -5-45.2529 152.584 1 11 9 6-125.049 75.2830 2 -11 -9 -6 91.6790 98.5408 1 11 9 7 1631.16 256.773 2 -11 -9 -7 1847.32 381.440 1 11 9 8 827.286 186.623 2 11 9 9 644.229 177.473 2 11 10 8 1554.31 245.029 2 11 10 9 1362.23 238.637 2 -12 -3 -2 337.228 170.074 1 12 6 6 276.091 119.321 2 12 7 5-23.6400 45.6934 2 12 7 6 631.179 168.624 2 12 8 6 236.203 103.802 2 12 8 7 714.978 177.407 2 12 9 6 237.021 106.159 2 12 9 7 1382.21 241.188 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 92120 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.0000 0.0000 0.5000 0.01941(16) Uani 1 2 d S . P . . N1A N -0.2753(3) 0.4572(3) 0.4290(2) 0.0218(5) Uani 1 1 d D . . . . H1A H -0.288(4) 0.545(2) 0.436(3) 0.033 Uiso 1 1 d D U . . . C2A C -0.1527(3) 0.3337(3) 0.4674(2) 0.0217(6) Uani 1 1 d . . . . . H2A H -0.0705 0.3364 0.4982 0.026 Uiso 1 1 calc R U . . . N3A N -0.1627(2) 0.2082(3) 0.4562(2) 0.0202(5) Uani 1 1 d . . . . . C4A C -0.2989(3) 0.2542(3) 0.4088(2) 0.0209(6) Uani 1 1 d . . . . . H4A H -0.3366 0.1879 0.3909 0.025 Uiso 1 1 calc R U . . . C5A C -0.3707(3) 0.4103(3) 0.3917(2) 0.0201(6) Uani 1 1 d . . . . . C6A C -0.5164(3) 0.5148(3) 0.3430(2) 0.0212(6) Uani 1 1 d . . . . . C7A C -0.5507(3) 0.6772(3) 0.3044(3) 0.0260(7) Uani 1 1 d . . . . . H7A H -0.4789 0.7221 0.3087 0.031 Uiso 1 1 calc R U . . . C8A C -0.6894(4) 0.7721(4) 0.2599(3) 0.0295(7) Uani 1 1 d . . . . . H8A H -0.7120 0.8821 0.2333 0.035 Uiso 1 1 calc R U . . . C9A C -0.7953(3) 0.7083(4) 0.2537(3) 0.0292(7) Uani 1 1 d . . . . . H9A H -0.8909 0.7743 0.2242 0.035 Uiso 1 1 calc R U . . . C10A C -0.7617(3) 0.5478(4) 0.2906(3) 0.0297(7) Uani 1 1 d . . . . . H10A H -0.8333 0.5034 0.2852 0.036 Uiso 1 1 calc R U . . . C11A C -0.6230(3) 0.4521(4) 0.3357(3) 0.0251(7) Uani 1 1 d . . . . . H11A H -0.6010 0.3421 0.3619 0.030 Uiso 1 1 calc R U . . . N1B N 0.3161(3) 0.1490(3) 0.2740(2) 0.0225(6) Uani 1 1 d . . . . . H1B H 0.410(4) 0.145(4) 0.259(3) 0.034 Uiso 1 1 d . U . . . C2B C 0.2715(3) 0.0715(3) 0.3720(3) 0.0227(6) Uani 1 1 d . . . . . H2B H 0.3354 0.0147 0.4316 0.027 Uiso 1 1 calc R U . . . N3B N 0.1281(3) 0.0841(3) 0.3752(2) 0.0212(5) Uani 1 1 d . . . . . C4B C 0.0791(3) 0.1737(3) 0.2724(3) 0.0217(6) Uani 1 1 d . . . . . H4B H -0.0206 0.2024 0.2498 0.026 Uiso 1 1 calc R U . . . C5B C 0.1949(3) 0.2149(3) 0.2080(3) 0.0212(6) Uani 1 1 d . . . . . C6B C 0.2045(3) 0.3041(3) 0.0933(3) 0.0239(7) Uani 1 1 d . . . . . C7B C 0.2942(4) 0.3995(4) 0.0550(3) 0.0341(8) Uani 1 1 d . . . . . H7B H 0.3489 0.4110 0.1037 0.041 Uiso 1 1 calc R U . . . C8B C 0.3038(4) 0.4782(4) -0.0549(3) 0.0442(10) Uani 1 1 d . . . . . H8B H 0.3666 0.5418 -0.0812 0.053 Uiso 1 1 calc R U . . . C9B C 0.2236(4) 0.4643(4) -0.1251(3) 0.0421(10) Uani 1 1 d . . . . . H9B H 0.2317 0.5176 -0.1999 0.050 Uiso 1 1 calc R U . . . C10B C 0.1311(4) 0.3740(4) -0.0884(3) 0.0395(9) Uani 1 1 d . . . . . H10B H 0.0735 0.3668 -0.1373 0.047 Uiso 1 1 calc R U . . . C11B C 0.1225(4) 0.2931(4) 0.0210(3) 0.0304(7) Uani 1 1 d . . . . . H11B H 0.0597 0.2295 0.0464 0.037 Uiso 1 1 calc R U . . . Cl Cl 0.22342(8) 0.16061(8) 0.62128(6) 0.02379(19) Uani 1 1 d . . . . . O1 O 0.1220(2) 0.0774(2) 0.62806(18) 0.0254(5) Uani 1 1 d . . . . . O2 O 0.3752(2) 0.0722(3) 0.5974(2) 0.0327(6) Uani 1 1 d . . . . . O3 O 0.2175(2) 0.1888(3) 0.7209(2) 0.0338(6) Uani 1 1 d . . . . . O4 O 0.1778(2) 0.3086(2) 0.5359(2) 0.0329(6) Uani 1 1 d . . . . . C12 C 0.6675(3) 0.1128(4) 0.1203(3) 0.0307(8) Uani 1 1 d . . . . . O5 O 0.6026(2) 0.1788(3) 0.18518(19) 0.0294(5) Uani 1 1 d . . . . . C13 C 0.5917(4) 0.0436(4) 0.0704(3) 0.0398(9) Uani 1 1 d . . . . . H13A H 0.4950 0.0409 0.1089 0.060 Uiso 1 1 calc R U . . . H13B H 0.6569 -0.0628 0.0748 0.060 Uiso 1 1 calc R U . . . H13C H 0.5737 0.1072 -0.0052 0.060 Uiso 1 1 calc R U . . . C14 C 0.8278(4) 0.1021(5) 0.0827(4) 0.0506(11) Uani 1 1 d . . . . . H14A H 0.8291 0.1760 0.0099 0.076 Uiso 1 1 calc R U . . . H14B H 0.8852 -0.0041 0.0820 0.076 Uiso 1 1 calc R U . . . H14C H 0.8740 0.1276 0.1315 0.076 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0183(3) 0.0178(3) 0.0185(3) -0.0032(2) -0.00156(19) -0.00400(19) N1A 0.0254(12) 0.0162(12) 0.0245(15) -0.0081(11) -0.0040(10) -0.0049(10) C2A 0.0210(14) 0.0207(15) 0.0201(17) -0.0026(12) -0.0041(12) -0.0058(11) N3A 0.0199(12) 0.0195(13) 0.0190(14) -0.0038(10) -0.0003(10) -0.0066(10) C4A 0.0220(14) 0.0220(15) 0.0180(17) -0.0046(12) -0.0016(12) -0.0080(12) C5A 0.0210(14) 0.0223(15) 0.0156(16) -0.0046(12) 0.0006(11) -0.0077(11) C6A 0.0239(14) 0.0209(15) 0.0171(16) -0.0079(12) -0.0003(12) -0.0040(11) C7A 0.0256(15) 0.0220(16) 0.0297(19) -0.0078(14) -0.0028(13) -0.0069(12) C8A 0.0343(17) 0.0186(16) 0.028(2) -0.0057(14) -0.0046(14) -0.0008(13) C9A 0.0236(15) 0.0325(18) 0.0257(19) -0.0126(15) -0.0058(13) 0.0026(13) C10A 0.0267(16) 0.0354(18) 0.030(2) -0.0117(15) -0.0044(14) -0.0106(13) C11A 0.0257(15) 0.0222(16) 0.0258(18) -0.0076(13) -0.0036(13) -0.0053(12) N1B 0.0194(12) 0.0265(14) 0.0224(15) -0.0079(11) 0.0014(10) -0.0094(10) C2B 0.0250(15) 0.0235(16) 0.0195(17) -0.0072(13) -0.0023(12) -0.0071(12) N3B 0.0210(12) 0.0192(13) 0.0212(15) -0.0054(11) -0.0015(10) -0.0051(10) C4B 0.0225(14) 0.0197(15) 0.0198(17) -0.0040(12) -0.0025(12) -0.0050(11) C5B 0.0208(14) 0.0178(14) 0.0222(17) -0.0055(12) -0.0017(12) -0.0037(11) C6B 0.0233(15) 0.0200(15) 0.0215(18) -0.0058(13) 0.0014(12) -0.0012(12) C7B 0.0292(17) 0.0292(18) 0.032(2) -0.0002(15) 0.0014(14) -0.0072(13) C8B 0.0361(19) 0.035(2) 0.042(3) 0.0042(17) 0.0075(17) -0.0090(16) C9B 0.040(2) 0.037(2) 0.021(2) 0.0008(16) 0.0082(16) 0.0046(16) C10B 0.044(2) 0.038(2) 0.023(2) -0.0105(16) -0.0042(16) 0.0028(16) C11B 0.0333(17) 0.0283(17) 0.0246(19) -0.0074(14) -0.0003(14) -0.0059(13) Cl 0.0234(4) 0.0229(4) 0.0267(4) -0.0086(3) -0.0042(3) -0.0075(3) O1 0.0257(11) 0.0217(11) 0.0293(13) -0.0078(9) -0.0018(9) -0.0086(9) O2 0.0222(11) 0.0412(14) 0.0337(15) -0.0130(11) -0.0023(10) -0.0079(10) O3 0.0404(13) 0.0366(13) 0.0306(14) -0.0170(11) -0.0063(10) -0.0116(10) O4 0.0387(13) 0.0238(12) 0.0368(15) -0.0027(10) -0.0109(11) -0.0140(10) C12 0.0266(16) 0.0357(19) 0.027(2) -0.0082(16) -0.0030(14) -0.0086(14) O5 0.0256(11) 0.0321(12) 0.0306(14) -0.0089(11) -0.0005(10) -0.0110(9) C13 0.0361(19) 0.045(2) 0.043(2) -0.0230(19) -0.0079(16) -0.0065(16) C14 0.034(2) 0.077(3) 0.049(3) -0.027(2) 0.0093(18) -0.0260(19) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3B Cu N3B 180.0 2_556 . ? N3B Cu N3A 91.61(9) 2_556 . ? N3B Cu N3A 88.39(9) . . ? N3B Cu N3A 88.39(9) 2_556 2_556 ? N3B Cu N3A 91.61(9) . 2_556 ? N3A Cu N3A 180.0 . 2_556 ? C2A N1A C5A 109.0(2) . . ? C2A N1A H1A 121(2) . . ? C5A N1A H1A 130(2) . . ? N3A C2A N1A 110.2(3) . . ? N3A C2A H2A 124.9 . . ? N1A C2A H2A 124.9 . . ? C2A N3A C4A 106.5(2) . . ? C2A N3A Cu 122.86(19) . . ? C4A N3A Cu 130.7(2) . . ? C5A C4A N3A 109.2(3) . . ? C5A C4A H4A 125.4 . . ? N3A C4A H4A 125.4 . . ? C4A C5A N1A 105.1(2) . . ? C4A C5A C6A 130.6(3) . . ? N1A C5A C6A 124.3(3) . . ? C11A C6A C7A 118.9(3) . . ? C11A C6A C5A 119.6(3) . . ? C7A C6A C5A 121.5(3) . . ? C8A C7A C6A 119.9(3) . . ? C8A C7A H7A 120.0 . . ? C6A C7A H7A 120.0 . . ? C9A C8A C7A 120.6(3) . . ? C9A C8A H8A 119.7 . . ? C7A C8A H8A 119.7 . . ? C8A C9A C10A 119.8(3) . . ? C8A C9A H9A 120.1 . . ? C10A C9A H9A 120.1 . . ? C9A C10A C11A 119.8(3) . . ? C9A C10A H10A 120.1 . . ? C11A C10A H10A 120.1 . . ? C6A C11A C10A 120.9(3) . . ? C6A C11A H11A 119.6 . . ? C10A C11A H11A 119.6 . . ? C2B N1B C5B 108.2(2) . . ? C2B N1B H1B 121(2) . . ? C5B N1B H1B 130(2) . . ? N3B C2B N1B 111.4(3) . . ? N3B C2B H2B 124.3 . . ? N1B C2B H2B 124.3 . . ? C2B N3B C4B 105.5(2) . . ? C2B N3B Cu 128.9(2) . . ? C4B N3B Cu 125.55(18) . . ? C5B C4B N3B 110.1(3) . . ? C5B C4B H4B 125.0 . . ? N3B C4B H4B 125.0 . . ? C4B C5B N1B 104.9(3) . . ? C4B C5B C6B 132.0(3) . . ? N1B C5B C6B 123.1(3) . . ? C11B C6B C7B 118.9(3) . . ? C11B C6B C5B 119.4(3) . . ? C7B C6B C5B 121.8(3) . . ? C6B C7B C8B 119.8(4) . . ? C6B C7B H7B 120.1 . . ? C8B C7B H7B 120.1 . . ? C9B C8B C7B 120.4(3) . . ? C9B C8B H8B 119.8 . . ? C7B C8B H8B 119.8 . . ? C8B C9B C10B 120.6(3) . . ? C8B C9B H9B 119.7 . . ? C10B C9B H9B 119.7 . . ? C9B C10B C11B 119.5(4) . . ? C9B C10B H10B 120.3 . . ? C11B C10B H10B 120.3 . . ? C6B C11B C10B 120.8(3) . . ? C6B C11B H11B 119.6 . . ? C10B C11B H11B 119.6 . . ? O3 Cl O2 109.89(14) . . ? O3 Cl O1 110.05(13) . . ? O2 Cl O1 110.00(13) . . ? O3 Cl O4 109.00(14) . . ? O2 Cl O4 108.90(14) . . ? O1 Cl O4 108.98(13) . . ? O5 C12 C13 122.5(3) . . ? O5 C12 C14 121.2(3) . . ? C13 C12 C14 116.3(3) . . ? C12 C13 H13A 109.5 . . ? C12 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? C12 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C12 C14 H14A 109.5 . . ? C12 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C12 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3B 2.000(2) 2_556 ? Cu N3B 2.000(2) . ? Cu N3A 2.002(2) . ? Cu N3A 2.002(2) 2_556 ? N1A C2A 1.341(4) . ? N1A C5A 1.371(4) . ? N1A H1A 0.851(10) . ? C2A N3A 1.318(4) . ? C2A H2A 0.9500 . ? N3A C4A 1.384(4) . ? C4A C5A 1.368(4) . ? C4A H4A 0.9500 . ? C5A C6A 1.472(4) . ? C6A C11A 1.386(4) . ? C6A C7A 1.401(4) . ? C7A C8A 1.385(4) . ? C7A H7A 0.9500 . ? C8A C9A 1.383(5) . ? C8A H8A 0.9500 . ? C9A C10A 1.385(5) . ? C9A H9A 0.9500 . ? C10A C11A 1.389(4) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.341(4) . ? N1B C5B 1.378(4) . ? N1B H1B 0.87(3) . ? C2B N3B 1.316(4) . ? C2B H2B 0.9500 . ? N3B C4B 1.383(4) . ? C4B C5B 1.366(4) . ? C4B H4B 0.9500 . ? C5B C6B 1.470(4) . ? C6B C11B 1.385(5) . ? C6B C7B 1.391(4) . ? C7B C8B 1.395(5) . ? C7B H7B 0.9500 . ? C8B C9B 1.365(6) . ? C8B H8B 0.9500 . ? C9B C10B 1.374(5) . ? C9B H9B 0.9500 . ? C10B C11B 1.392(5) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? Cl O3 1.436(3) . ? Cl O2 1.436(2) . ? Cl O1 1.438(2) . ? Cl O4 1.447(2) . ? C12 O5 1.213(4) . ? C12 C13 1.494(5) . ? C12 C14 1.500(5) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? _cod_database_fobs_code 2023229