#------------------------------------------------------------------------------ #$Date: 2024-08-02 04:53:16 +0300 (Fri, 02 Aug 2024) $ #$Revision: 293633 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/32/2023230.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023230 loop_ _publ_author_name 'Loukopoulos, Edward' 'Papatriantafyllopoulou, Constantina' 'Moushi, Eleni' 'Kitos, Alexandros A.' 'Tasiopoulos, Anastasios J.' 'Perlepes, Spyros P.' 'Nastopoulos, Vassilios' _publ_section_title ; Solvatomorphism in a series of copper(II) complexes with the 5-phenylimidazole/perchlorate system as ligands ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials' _journal_page_first 347 _journal_page_last 359 _journal_paper_doi 10.1107/S2052520624005948 _journal_volume 80 _journal_year 2024 _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, 2(C4 H8 O)' _chemical_formula_sum 'C44 H48 Cl2 Cu N8 O10' _chemical_formula_weight 983.34 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 107.509(6) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 9.0943(5) _cell_length_b 25.0287(17) _cell_length_c 10.0253(5) _cell_measurement_reflns_used 3274 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.7900 _cell_measurement_theta_min 3.2230 _cell_volume 2176.2(2) _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 10.4223 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0894 _diffrn_reflns_av_unetI/netI 0.1087 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 8871 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 24.999 _diffrn_reflns_theta_max 24.999 _diffrn_reflns_theta_min 2.857 _diffrn_source 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.694 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.503 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour pink _exptl_crystal_density_diffrn 1.501 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1022 _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.13 _exptl_crystal_size_min 0.13 _refine_diff_density_max 0.866 _refine_diff_density_min -0.585 _refine_diff_density_rms 0.111 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.175 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 301 _refine_ls_number_reflns 3808 _refine_ls_number_restraints 3 _refine_ls_restrained_S_all 1.174 _refine_ls_R_factor_all 0.0981 _refine_ls_R_factor_gt 0.0621 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0457P)^2^+4.9457P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1411 _refine_ls_wR_factor_ref 0.1568 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2800 _reflns_number_total 3808 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file aw5090sup1.cif _cod_data_source_block 9 _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 2023230 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.857 _shelx_estimated_absorpt_t_max 0.915 _shelx_res_file ; 9.res created by SHELXL-2014/7 TITL EL101A in P21/n CELL 0.71073 9.0943 25.0287 10.0253 90.000 107.509 90.000 ZERR 2 0.0005 0.0017 0.0005 0.000 0.006 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N O CL CU UNIT 88 96 16 20 4 2 MERG 2 FMAP 2 OMIT -2 50 OMIT 7 8 6 OMIT 7 5 4 OMIT 7 6 6 OMIT 7 7 6 OMIT 6 6 2 OMIT 6 11 5 OMIT 6 13 6 OMIT 7 8 5 OMIT 6 17 5 OMIT 7 5 6 OMIT 6 12 6 OMIT 6 15 5 SIZE 0.23 0.13 0.13 TEMP -173 ACTA LIST 4 MORE -3 PLAN 10 BOND $H HTAB L.S. 7 DFIX 0.85 0.01 N1A H1A N1B H1B EQIV $1 1+X, Y, Z DFIX 2.05 0.01 H1B O5_$1 WGHT 0.045700 4.945700 FVAR 1.17493 CU 6 1.000000 0.500000 1.000000 10.50000 0.01317 0.02305 = 0.01415 0.00143 0.00129 -0.00103 N1A 3 0.745774 0.535749 0.596386 11.00000 0.02275 0.02016 = 0.01297 -0.00035 0.00554 -0.00070 H1A 2 0.739527 0.538616 0.510570 11.00000 -1.50000 C2A 1 0.871966 0.520045 0.697460 11.00000 0.01757 0.01687 = 0.01762 0.00129 0.00285 -0.00026 AFIX 43 H2A 2 0.964853 0.508118 0.682366 11.00000 -1.20000 AFIX 0 N3A 3 0.848663 0.523527 0.820818 11.00000 0.01523 0.02551 = 0.01768 -0.00068 0.00500 -0.00255 C4A 1 0.700867 0.541915 0.797338 11.00000 0.01873 0.02659 = 0.01745 0.00017 0.00627 0.00075 AFIX 43 H4A 2 0.652697 0.548295 0.867793 11.00000 -1.20000 AFIX 0 C5A 1 0.633276 0.549682 0.656813 11.00000 0.01707 0.01589 = 0.01642 -0.00197 0.00201 -0.00249 C6A 1 0.478813 0.567861 0.578115 11.00000 0.02190 0.01234 = 0.01918 -0.00483 0.00300 -0.00564 C7A 1 0.440125 0.582660 0.437499 11.00000 0.02551 0.02143 = 0.01936 0.00328 0.00299 -0.00215 AFIX 43 H7A 2 0.515133 0.580158 0.389196 11.00000 -1.20000 AFIX 0 C8A 1 0.293709 0.600911 0.368004 11.00000 0.03181 0.02177 = 0.02134 0.00614 -0.00237 -0.00082 AFIX 43 H8A 2 0.269127 0.610493 0.272104 11.00000 -1.20000 AFIX 0 C9A 1 0.182616 0.605458 0.435480 11.00000 0.02171 0.01851 = 0.03775 0.00365 -0.00602 0.00302 AFIX 43 H9A 2 0.082870 0.618782 0.387595 11.00000 -1.20000 AFIX 0 C10A 1 0.219877 0.590016 0.576203 11.00000 0.02025 0.02775 = 0.03562 -0.00469 0.00599 -0.00150 AFIX 43 H10A 2 0.144207 0.592303 0.623827 11.00000 -1.20000 AFIX 0 C11A 1 0.365331 0.571571 0.645773 11.00000 0.02377 0.02661 = 0.02098 -0.00129 0.00378 -0.00050 AFIX 43 H11A 2 0.388949 0.561218 0.741067 11.00000 -1.20000 AFIX 0 N1B 3 1.331752 0.613959 1.001519 11.00000 0.02193 0.02452 = 0.03188 0.00118 0.01167 -0.00218 H1B 2 1.412479 0.626300 0.984765 11.00000 -1.50000 C2B 1 1.276696 0.563955 0.993703 11.00000 0.02284 0.02384 = 0.03003 -0.00355 0.01131 -0.00354 AFIX 43 H2B 2 1.334644 0.532699 0.990099 11.00000 -1.20000 AFIX 0 N3B 3 1.131238 0.564168 0.991717 11.00000 0.01847 0.02321 = 0.01501 -0.00298 0.00216 -0.00397 C4B 1 1.090768 0.617125 0.995545 11.00000 0.02329 0.02599 = 0.02659 0.00642 0.00768 0.00641 AFIX 43 H4B 2 0.991702 0.629719 0.993927 11.00000 -1.20000 AFIX 0 C5B 1 1.214886 0.648522 1.002002 11.00000 0.02630 0.02443 = 0.01674 0.00761 0.00473 0.00327 C6B 1 1.239809 0.706632 1.018222 11.00000 0.03656 0.02343 = 0.02713 0.00728 0.01338 0.00372 C7B 1 1.382081 0.727527 1.091779 11.00000 0.04259 0.02559 = 0.03987 -0.00033 0.01670 -0.00392 AFIX 43 H7B 2 1.465262 0.704142 1.134292 11.00000 -1.20000 AFIX 0 C8B 1 1.404029 0.782492 1.103842 11.00000 0.06863 0.03199 = 0.04887 -0.00390 0.02752 -0.00988 AFIX 43 H8B 2 1.502327 0.796452 1.153763 11.00000 -1.20000 AFIX 0 C9B 1 1.283975 0.816808 1.043781 11.00000 0.08840 0.02218 = 0.05969 0.00236 0.03771 0.00186 AFIX 43 H9B 2 1.298946 0.854375 1.051808 11.00000 -1.20000 AFIX 0 C10B 1 1.142438 0.796115 0.972186 11.00000 0.07044 0.03454 = 0.05982 0.01301 0.02933 0.01777 AFIX 43 H10B 2 1.058923 0.819494 0.930606 11.00000 -1.20000 AFIX 0 C11B 1 1.120634 0.741182 0.960188 11.00000 0.04780 0.03125 = 0.04621 0.01243 0.01986 0.01126 AFIX 43 H11B 2 1.021868 0.727360 0.911137 11.00000 -1.20000 AFIX 0 CL 5 0.751665 0.569396 1.201123 11.00000 0.01940 0.02165 = 0.01699 -0.00039 0.00607 0.00117 O1 4 0.865869 0.563824 1.128905 11.00000 0.02822 0.04041 = 0.02132 -0.00019 0.01279 0.00055 O2 4 0.611071 0.544880 1.120588 11.00000 0.01907 0.04903 = 0.04237 -0.01543 0.00337 -0.00150 O3 4 0.724528 0.624347 1.222236 11.00000 0.06450 0.02498 = 0.06832 -0.00857 0.03582 0.00162 O4 4 0.807778 0.543410 1.333858 11.00000 0.03068 0.06847 = 0.02439 0.02160 0.01240 0.01350 O5 4 0.536447 0.667775 0.877095 11.00000 0.02979 0.03346 = 0.04215 0.00578 0.01325 -0.00296 C12 1 0.689528 0.688933 0.906764 11.00000 0.03147 0.04311 = 0.05219 0.00332 0.01232 -0.00603 AFIX 23 H12A 2 0.742809 0.673363 0.843101 11.00000 -1.20000 H12B 2 0.750696 0.681137 1.004529 11.00000 -1.20000 AFIX 0 C13 1 0.668307 0.748681 0.883582 11.00000 0.04026 0.03088 = 0.07117 0.00217 0.01994 -0.00502 AFIX 23 H13A 2 0.680307 0.767390 0.973242 11.00000 -1.20000 H13B 2 0.744810 0.763127 0.840659 11.00000 -1.20000 AFIX 0 C14 1 0.506919 0.755491 0.786457 11.00000 0.04935 0.03179 = 0.04265 0.00500 0.02213 0.00588 AFIX 23 H14A 2 0.508086 0.772606 0.697753 11.00000 -1.20000 H14B 2 0.443727 0.777449 0.830511 11.00000 -1.20000 AFIX 0 C15 1 0.444977 0.698643 0.761118 11.00000 0.04092 0.03772 = 0.03529 0.00812 0.01383 0.00327 AFIX 23 H15A 2 0.334881 0.697551 0.757006 11.00000 -1.20000 H15B 2 0.455194 0.684614 0.672000 11.00000 -1.20000 AFIX 0 HKLF 4 REM EL101A in P21/n REM R1 = 0.0621 for 2800 Fo > 4sig(Fo) and 0.0981 for all 3808 data REM 301 parameters refined using 3 restraints END WGHT 0.0454 4.5153 REM Instructions for potential hydrogen bonds EQIV $2 x, y, z-1 HTAB N1A O4_$2 EQIV $3 -x+2, -y+1, -z+2 HTAB C2A O4_$3 HTAB N1B O5_$1 HTAB C2B O2_$1 HTAB C2B O2_$3 HTAB C4B O1 REM Highest difference peak 0.866, deepest hole -0.585, 1-sigma level 0.111 Q1 1 1.0626 0.5002 0.9111 11.00000 0.05 0.87 Q2 1 0.6974 0.6183 1.1195 11.00000 0.05 0.53 Q3 1 0.9998 0.5327 1.0077 11.00000 0.05 0.50 Q4 1 0.5771 0.5714 0.6472 11.00000 0.05 0.49 Q5 1 1.0817 0.5231 0.8413 11.00000 0.05 0.45 Q6 1 0.8034 0.5463 0.8201 11.00000 0.05 0.42 Q7 1 1.3613 0.5249 1.0628 11.00000 0.05 0.42 Q8 1 0.6385 0.5485 0.7140 11.00000 0.05 0.42 Q9 1 0.9039 0.5283 1.1659 11.00000 0.05 0.41 Q10 1 0.7553 0.5255 0.9201 11.00000 0.05 0.41 ; _shelx_res_checksum 25276 _shelx_hkl_file ; 0 0 2 23508.6 239.144 1 0 0 -2 23217.4 273.225 3 0 0 -3-7.63728 40.4481 3 0 0 -3-7.75149 10.2516 2 0 0 3-15.7482 29.3150 1 0 0 3 4.69125 11.2793 2 0 0 -4 1568.69 106.231 3 0 0 4 1583.66 53.7820 2 0 0 4 1639.87 96.3175 1 0 0 5 80.7309 45.0482 1 0 0 -5 113.953 56.4995 3 0 0 5 65.8165 17.9842 2 0 0 6 8366.03 260.765 1 0 0 6 8203.23 138.231 2 0 0 -6 8816.97 295.177 3 0 0 7 331.707 70.0469 1 0 0 7 197.796 22.6178 2 0 0 -7 361.695 86.1668 3 0 0 -8 2166.54 176.592 3 0 0 8 2009.31 158.152 1 0 0 -9 137.873 74.7622 3 0 0 -10 5934.52 324.072 3 0 0 -11 17.3692 58.0258 3 0 0 -12 319.051 100.566 3 0 1 -2 194.425 20.5125 2 0 -1 -2 187.409 38.8423 3 0 -1 2 168.684 27.0990 1 0 -1 3 7946.40 128.387 2 0 -1 -3 8502.18 203.469 3 0 -1 3 7972.55 169.847 1 0 1 -3 8303.62 119.125 2 0 1 -3 8241.45 210.505 3 0 -1 4 250.238 44.3245 1 0 1 -4 327.910 29.5886 2 0 1 -4 288.424 61.5242 3 0 -1 -4 302.435 61.0032 3 0 -1 4 254.095 28.8038 2 0 1 4 248.345 48.8779 1 0 1 5 27198.0 438.765 1 0 -1 -5 27323.8 461.115 3 0 -1 5 28331.4 419.077 1 0 -1 5 26284.4 274.922 2 0 1 -5 28241.3 483.967 3 0 1 -6 55.3439 50.3569 3 0 -1 6 17.9854 16.4554 2 0 -1 -6 13.3215 46.5432 3 0 -1 6 36.3488 37.0187 1 0 1 6-3.69578 39.1209 1 0 -1 -7 3379.61 201.201 3 0 -1 7 3102.58 175.105 1 0 1 7 3108.54 183.443 1 0 -1 7 3400.56 107.444 2 0 1 -7 3247.53 199.925 3 0 1 8 182.693 65.5176 1 0 -1 8 173.433 26.1625 2 0 1 -8 198.404 69.8239 3 0 -1 -8 174.537 68.4905 3 0 -1 -9 8218.95 353.174 3 0 1 -9 7888.62 354.135 3 0 1 9 7125.59 323.739 1 0 1 -10 100.591 72.3687 3 0 -1 -10 37.7420 60.3028 3 0 -1 -11 1098.35 155.678 3 0 1 -11 1109.02 154.460 3 0 -1 -12 91.9394 77.6614 3 0 1 -12 143.284 81.8030 3 0 -2 -2 974.163 60.6079 3 0 2 -2 952.581 47.1776 1 0 2 -2 1068.76 47.0452 2 0 -2 -3 1855.58 98.0920 3 0 2 -3 2111.45 68.9767 2 0 -2 3 1895.39 81.6995 1 0 -2 3 2059.59 74.8003 2 0 2 -4 89.9322 53.0282 3 0 -2 4 34.0790 29.0029 1 0 -2 -4 71.2033 42.0406 3 0 2 -4 72.4277 21.7983 2 0 -2 4 34.9280 18.9089 2 0 2 -5 21.4212 50.7760 3 0 2 -5 41.0784 22.2238 2 0 2 5 52.8496 43.2117 1 0 -2 -5 24.1982 48.9023 3 0 -2 5 4.27856 31.5384 1 0 -2 5 19.8362 19.2558 2 0 -2 6 8825.64 188.593 2 0 2 6 9405.69 297.365 1 0 2 -6 9782.72 316.081 3 0 -2 -6 9655.62 305.724 3 0 -2 6 8845.07 260.641 1 0 -2 -7 181.474 62.4342 3 0 2 -7 228.045 71.2378 3 0 -2 7 220.215 34.8436 2 0 2 7 190.597 60.9731 1 0 2 -8 1.29643 50.0033 3 0 -2 -8 40.1841 60.0701 3 0 2 8 32.9925 49.2200 1 0 -2 8 23.7599 19.5071 2 0 2 9 54.2851 54.3135 1 0 -2 -9 59.0934 65.6316 3 0 2 -9 73.7398 67.8873 3 0 -2 -10 1928.50 191.503 3 0 2 -10 2033.54 199.033 3 0 2 10 1926.06 190.535 1 0 -2 -11 247.565 90.0737 3 0 2 -11 207.564 86.2427 3 0 2 -12 367.325 111.023 3 0 -3 -1 167.278 23.4606 3 0 3 -1 303.336 29.6900 2 0 3 -2 12500.9 174.088 2 0 -3 -2 12382.6 202.816 3 0 -3 3 2468.05 90.5646 2 0 -3 -3 2681.11 117.722 3 0 3 -3 2367.97 84.6312 1 0 3 -3 2563.21 85.0317 2 0 3 -4 2628.55 92.3873 2 0 -3 -4 2646.83 131.408 3 0 -3 4 2414.22 96.8148 2 0 3 -5 1997.69 141.646 3 0 -3 5 1785.32 88.6724 2 0 3 5 2146.48 137.039 1 0 -3 -5 1876.06 126.218 3 0 3 -5 1932.51 86.3912 2 0 3 -6 161.526 30.8913 2 0 -3 6 116.589 29.0775 2 0 3 -6 103.302 56.0985 3 0 -3 -6 125.730 56.3857 3 0 3 6 141.209 55.6464 1 0 3 7 390.514 83.4399 1 0 -3 -7 448.784 83.8594 3 0 3 -7 370.192 83.7360 3 0 -3 7 383.171 48.5322 2 0 -3 -8 1346.25 140.678 3 0 3 -8 1223.43 142.673 3 0 3 8 1379.27 147.404 1 0 -3 8 1050.31 77.0769 2 0 3 -9 258.326 84.7479 3 0 -3 -9 266.294 83.8850 3 0 3 9 218.042 80.9358 1 0 -3 -10 137.835 71.5499 3 0 3 -10 179.839 77.0036 3 0 3 10 216.321 80.9872 1 0 3 -11 87.0736 74.4475 3 0 -3 -11 113.747 76.2186 3 0 3 11 66.8886 62.5451 1 0 3 -12 80.6959 70.7847 3 0 -4 0 12214.1 157.780 3 0 4 -1 9795.56 159.694 2 0 -4 -1 9413.62 132.343 2 0 -4 -1 11284.5 171.716 3 0 -4 -2 675.916 32.5387 2 0 4 2 582.598 30.0477 2 0 4 -2 749.786 55.7958 2 0 -4 -2 649.317 55.6952 3 0 -4 3 43.1668 23.5622 2 0 -4 -3 59.1399 35.8023 3 0 4 -3 31.8462 20.9753 1 0 4 -3 27.0996 24.4573 2 0 4 -4 88.3386 25.6527 1 0 -4 -4 228.866 54.3536 3 0 -4 4 106.015 29.8025 2 0 4 -4 133.228 30.8548 2 0 -4 5 552.267 54.2361 2 0 -4 -5 604.842 76.9649 3 0 4 -5 604.817 52.8276 2 0 -4 6 1279.06 85.3645 2 0 4 6 1492.87 130.674 1 0 4 -6 1383.12 133.289 3 0 4 -6 1437.46 85.7417 2 0 -4 -6 1509.37 126.922 3 0 -4 -7 332.407 73.0287 3 0 4 7 398.961 83.9965 1 0 4 -7 313.233 80.9586 3 0 -4 7 313.134 47.0729 2 0 4 8 10.3304 50.6771 1 0 -4 8 44.1046 24.1802 2 0 -4 -8 32.3264 50.1733 3 0 4 -8 40.6378 56.7497 3 0 4 9 29.4922 56.5781 1 0 -4 -9 22.7755 52.4357 3 0 4 -9-28.2035 55.9457 3 0 4 10 708.362 131.128 1 0 4 -10 738.587 125.489 3 0 -4 -10 788.740 128.925 3 0 4 -11 240.649 91.8088 3 0 4 11 147.596 76.6849 1 0 -4 -11 177.666 73.2023 3 0 4 -12 165.284 81.7819 3 0 -5 0 374.081 42.1446 3 0 5 0 220.396 38.0792 2 0 5 1 6247.84 119.425 2 0 5 -1 6719.63 145.546 2 0 -5 -1 6208.23 126.328 2 0 5 -2 12386.0 206.086 2 0 -5 -2 12299.1 212.586 3 0 -5 -2 11606.1 152.825 2 0 5 2 12069.9 142.559 2 0 -5 3 390.163 46.5148 2 0 -5 -3 352.142 24.2250 2 0 5 -3 421.561 45.8173 2 0 -5 -3 364.655 53.5280 3 0 5 -4 150.166 33.2762 2 0 -5 -4 121.148 44.1225 3 0 -5 4 72.6898 29.5460 2 0 5 -4 76.1258 24.1189 1 0 5 -5 2911.27 118.211 2 0 -5 5 2698.28 124.541 2 0 -5 -5 2867.87 154.239 3 0 -5 6 3087.81 137.572 2 0 5 -6 3195.43 130.700 2 0 5 6 3188.54 189.860 1 0 5 -6 2962.04 187.851 3 0 -5 -6 3072.58 173.699 3 0 5 -7 693.641 108.269 3 0 -5 7 606.951 66.7118 2 0 5 7 790.547 112.303 1 0 -5 -7 703.138 97.5241 3 0 5 -8 1219.28 142.493 3 0 5 8 1281.09 147.080 1 0 -5 8 864.661 82.4329 2 0 -5 -8 1189.32 131.439 3 0 -5 -9 6.06147 50.4901 3 0 5 -9-21.4146 56.8959 3 0 5 9 44.8781 65.0869 1 0 -5 -10-32.6508 58.4477 3 0 5 10 5.73316 59.6085 1 0 5 -10 16.0313 58.3589 3 0 5 11 26.0231 58.1180 1 0 -5 -11-10.1097 53.0794 3 0 5 -11 75.8316 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172.260 2 0 -17 -5-59.9634 118.752 3 0 17 -5 769.295 101.920 2 0 17 -6 1034.10 120.561 2 0 -17 -6 67.3285 98.0668 3 0 -17 -7 152.820 85.0462 3 0 17 -7 456.873 88.3856 2 0 17 -8 46.7750 50.5306 2 0 -17 -8 52.6669 50.8317 3 0 -17 -9 1962.03 212.595 3 0 17 9 1985.91 253.241 1 0 -17 -10 83.2846 61.5535 3 0 17 -10-58.0614 75.1365 3 0 17 10-32.8339 85.5386 1 0 18 0 1989.37 143.750 2 0 18 -1 862.849 103.768 2 0 18 1 922.898 100.132 2 0 -18 -2 2737.21 193.148 3 0 18 -2 2781.84 173.876 2 0 18 2 2814.84 161.814 2 0 18 -3 2513.30 170.308 2 0 18 3 2568.61 155.061 2 0 18 4 271.600 56.8452 2 0 18 -4 217.116 69.1519 2 0 -18 -4 28.0774 75.9106 3 0 18 -5 24.2870 42.8429 2 0 -18 -5-90.1999 100.755 3 0 18 -6 1611.17 149.379 2 0 -18 -6-54.0219 120.103 3 0 -18 -7-152.065 91.5062 3 0 18 -7 127.144 58.4058 2 0 18 -8 2313.15 185.040 2 0 -18 -8 1065.28 194.917 3 0 18 9 1332.16 220.045 1 0 -18 -9 896.552 172.814 3 0 18 -10 352.284 108.260 3 0 -18 -10 308.811 113.111 3 0 18 10 335.732 129.708 1 0 19 0 473.506 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59.3721 2 0 25 -1 670.337 108.169 2 0 25 1 785.192 113.633 2 0 25 -2 481.481 98.4540 2 0 25 2 442.222 89.7069 2 0 25 3 382.999 79.6542 2 0 -25 -3 499.990 86.7502 3 0 25 -3 443.355 96.0333 2 0 -25 -4 471.994 109.209 3 0 25 -4 266.666 79.2135 2 0 -25 -5 454.087 167.637 3 0 25 -5 423.041 96.4510 2 0 25 -6 88.4463 61.0475 2 0 -25 -6-80.9876 154.820 3 0 25 -7 120.397 62.4941 2 0 -25 -8 122.057 88.9121 3 0 25 -8 192.528 71.3301 2 0 26 0 939.443 127.298 2 0 26 1 167.555 68.0424 2 0 26 -1 173.586 69.3531 2 0 26 2 400.015 89.5830 2 0 26 -2 582.237 106.932 2 0 26 -3 272.261 83.3151 2 0 26 3 194.849 66.6735 2 0 -26 -3 231.193 69.4508 3 0 26 -4 788.589 124.239 2 0 -26 -4 1119.83 142.809 3 0 26 -5 221.024 80.4743 2 0 -26 -5 297.602 114.684 3 0 26 -6 110.155 65.9268 2 0 -26 -6-115.879 138.363 3 0 26 -7 18.4357 42.5940 2 0 27 0 90.5182 61.0697 2 0 27 -1 349.158 88.8996 2 0 27 1 324.329 83.3200 2 0 27 -2 39.2641 53.1599 2 0 27 2 46.2851 53.5387 2 0 27 3 93.8923 60.1566 2 0 27 -3 127.626 65.8218 2 0 27 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4587.29 169.338 1 1 0 6 4.55163 13.5426 2 -1 0 -6 41.1099 54.0493 3 1 0 6 6.21651 32.4269 1 1 0 7 4926.71 113.041 2 -1 0 -7 5396.01 249.868 3 1 0 7 4734.87 213.491 1 -1 0 -8 13.8967 53.5304 3 1 0 8-19.7465 40.7307 1 -1 0 -9 20.4176 56.1809 3 1 0 9 53.0935 45.9007 1 -1 0 -10 23.9116 55.4886 3 -1 0 -11 1097.69 161.800 3 1 -1 -12 75.5303 72.5539 3 1 1 -12 93.5312 72.7850 3 1 -1 -11 220.159 78.8958 3 1 1 -11 290.238 97.1996 3 1 -1 -10 168.872 79.0611 3 1 1 -10 172.413 76.1098 3 1 -1 -9-6.71170 54.0892 3 1 1 -9 0.09212 61.9626 3 1 1 -8 3060.27 211.710 3 1 -1 -8 3330.84 213.218 3 -1 1 8 2766.59 200.436 1 -1 -1 8 2680.66 102.545 2 1 1 -7 2874.05 95.2110 2 -1 -1 7 2704.07 104.269 2 -1 1 7 2607.46 176.369 1 1 -1 -7 2851.53 183.123 3 1 1 -7 3106.87 196.670 3 1 1 -6 3476.35 106.188 2 1 -1 -6 3388.61 78.8035 2 1 -1 -6 3855.55 198.319 3 -1 1 6 3441.17 186.214 1 1 1 -6 3886.49 204.154 3 -1 -1 6 3616.55 117.992 2 -1 -1 5 3993.08 118.262 2 1 1 -5 4063.36 112.084 2 -1 1 5 4100.66 182.244 1 1 -1 -5 4441.31 191.697 3 1 1 -5 4061.62 191.024 3 -1 1 5 4109.40 93.9508 2 1 -1 -5 4113.13 89.9000 2 -1 1 4 8487.24 233.520 1 1 -1 -4 8301.85 124.193 2 1 1 -4 8324.86 150.350 2 -1 -1 4 8121.37 159.315 2 1 -1 -4 8652.58 239.206 3 1 1 -4 8444.95 219.647 1 -1 1 4 8182.51 127.673 2 1 1 -3 38703.7 301.100 2 1 -1 -3 37860.4 259.226 2 -1 -1 3 36856.9 312.373 2 1 -1 -3 38059.8 431.128 3 1 1 -3 37413.8 414.206 1 1 -1 -3 38955.4 428.751 1 1 1 -2 429.714 35.4043 2 1 -1 -2 355.921 29.0076 2 1 -1 -2 411.049 44.8419 1 -1 -1 -1 13626.8 172.457 3 -1 -1 -2 16840.1 244.864 3 -1 1 -2 16383.0 234.646 3 -1 1 -3 8225.01 203.274 3 -1 -1 -3 8435.62 206.279 3 1 -1 3 8249.57 146.942 2 1 -1 4 6388.26 136.148 2 1 1 4 6404.77 110.722 2 -1 -1 -4 6726.64 209.523 3 -1 1 -4 7209.02 217.838 3 1 -1 5 343.052 50.8198 1 1 -1 5 289.041 34.7609 2 1 1 5 339.061 29.3196 2 -1 -1 -5 326.426 63.3513 3 -1 1 -5 240.614 58.7470 3 1 -1 6 7378.93 165.803 2 -1 1 -6 7605.97 276.903 3 1 1 6 6997.88 242.968 1 1 -1 6 6390.39 212.751 1 -1 -1 -6 7715.31 274.028 3 1 1 6 7879.37 121.072 2 -1 -1 -7 504.808 89.4977 3 -1 1 -7 474.282 90.0646 3 1 1 7 431.024 77.1594 1 1 -1 7 498.798 75.0214 1 1 -1 7 435.460 42.2967 2 1 -1 8-17.8355 40.7549 1 -1 1 -8-1.75547 48.0817 3 1 1 8 10.1458 42.8179 1 -1 -1 -8 19.5994 53.7494 3 -1 -1 -9 28.4411 52.8762 3 1 1 9 41.9295 50.3498 1 1 -1 9 72.4213 50.2640 1 -1 1 -9 93.9674 62.3887 3 -1 1 -10 2873.49 230.629 3 -1 -1 -10 3003.54 235.585 3 -1 1 -11 106.806 65.6436 3 -1 -1 -11 93.5758 70.4620 3 1 2 -12 927.486 153.628 3 1 -2 -12 913.647 152.961 3 1 -2 -11 17.4431 61.2600 3 1 2 -11 23.8737 63.4462 3 1 2 -10 543.409 111.188 3 1 -2 -10 479.060 103.012 3 -1 2 9 1124.13 147.184 1 1 2 -9 1129.05 141.265 3 1 -2 -9 1283.75 145.407 3 1 2 -8 2225.67 93.8460 2 1 2 -8 2258.36 184.197 3 -1 -2 8 1927.58 99.9935 2 -1 2 8 2110.87 179.664 1 1 -2 -8 2268.37 178.186 3 1 -2 -7 1922.69 153.994 3 1 2 -7 1762.33 155.960 3 -1 -2 7 1634.80 91.0500 2 -1 2 7 1767.47 151.836 1 1 2 -7 1697.30 80.7367 2 -1 -2 6 515.329 50.7056 2 1 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4 3430.16 73.6188 2 1 -2 4 3374.93 113.199 1 1 2 4 3334.51 70.2006 2 -1 2 -4 3553.42 156.363 3 1 -2 5 73.0573 32.2402 1 1 2 5 73.7225 15.2987 2 -1 2 -5 94.8736 52.9629 3 -1 -2 -5 81.2042 48.1258 3 1 2 5 69.9707 15.5642 2 1 -2 5 68.5268 25.6930 2 1 -2 6 74.1287 26.0015 2 1 -2 6 40.7904 30.5417 1 -1 2 -6 36.7147 44.6458 3 -1 -2 -6 61.6494 49.2877 3 1 2 7 1053.88 112.893 1 1 -2 7 834.206 87.2705 1 -1 -2 -7 886.975 110.906 3 1 -2 7 904.172 66.0746 2 -1 2 -7 945.926 115.985 3 -1 -2 -8 835.032 116.012 3 1 -2 8 732.356 93.1429 1 1 2 8 811.262 108.832 1 -1 2 -8 827.836 117.176 3 1 2 9 1238.03 140.721 1 -1 -2 -9 1298.50 149.625 3 -1 2 -9 1272.71 148.019 3 1 2 10-27.2385 52.3160 1 -1 -2 -10 45.7920 60.2089 3 -1 2 -10 47.5977 58.3194 3 -1 2 -11 1132.53 159.793 3 -1 -2 -11 1316.60 168.920 3 1 3 -12 26.3850 69.5064 3 1 -3 -12 19.3887 73.3270 3 1 -3 -11 769.483 133.342 3 1 3 -11 703.662 132.619 3 1 -3 -10 327.056 89.9645 3 1 3 -10 133.557 68.8515 3 -1 3 10 172.294 82.1219 1 -1 3 9-31.8478 59.0719 1 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747.636 119.764 3 -2 4 -9 701.533 112.914 3 -2 -4 -10 754.678 123.024 3 -2 4 -10 923.098 137.848 3 -2 -4 -11-10.0712 53.0394 3 -2 4 -11 7.83318 48.6848 3 2 5 -12 28.0560 62.6672 3 2 -5 -12 77.5805 75.4642 3 2 5 -11 952.939 155.422 3 2 -5 -11 944.629 141.828 3 2 5 -10 12.0982 65.3354 3 -2 5 10 49.1133 73.3929 1 2 -5 -10 29.5754 55.7215 3 2 5 -9 1823.11 111.628 2 -2 5 9 1894.27 198.330 1 2 5 -9 1850.78 190.504 3 2 -5 -9 1987.17 175.718 3 -2 5 8 372.008 96.9424 1 2 5 -8 376.724 55.2271 2 -2 -5 8 356.711 59.0369 2 2 -5 -8 394.461 87.7616 3 -2 5 7 569.345 103.423 1 2 -5 -7 621.515 36.6977 2 2 5 -7 622.828 69.1318 2 2 -5 -7 566.879 90.9052 3 -2 -5 7 536.927 68.8652 2 2 -5 -6 627.236 44.6694 2 -2 5 6 652.193 98.6417 1 2 5 -6 634.178 80.5396 1 -2 -5 6 684.135 74.7337 2 2 5 -6 739.956 73.6589 2 2 -5 -6 664.209 83.7772 3 2 -5 -5 5966.03 139.418 2 -2 -5 5 5862.33 202.069 2 2 5 -5 6037.61 187.250 2 2 -5 -5 5936.83 211.281 3 -2 -5 4 466.044 59.4248 2 2 5 -4 489.212 56.8463 2 2 -5 -4 489.423 60.6767 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5 -8 813.167 113.450 3 -2 -5 -8 725.894 108.767 3 2 5 9 806.798 128.762 1 -2 -5 -9 789.122 118.711 3 -2 5 -9 683.795 114.296 3 -2 5 -10 43.0996 56.0626 3 -2 -5 -10 42.9993 51.3337 3 -2 -5 -11 129.670 65.7610 3 -2 5 -11 138.126 74.8679 3 2 -6 -12 0.76525 62.7236 3 2 6 -12-2.62125 62.4178 3 2 6 -11-36.0472 69.5976 3 2 -6 -11-2.14607 50.1761 3 2 6 -10 1992.69 209.800 3 2 -6 -10 1925.60 184.402 3 -2 6 10 2114.98 227.153 1 2 -6 -9-16.3967 50.3294 3 -2 6 9-7.64738 63.6098 1 2 6 -9 10.1511 25.5660 2 -2 6 8 1641.37 175.614 1 2 6 -8 1574.46 110.017 2 2 -6 -8 1399.76 137.579 3 2 -6 -7 119.934 17.0156 2 2 -6 -7 116.801 52.2596 3 -2 6 7 158.480 75.9180 1 2 -6 -7 132.711 18.5548 2 -2 -6 7 124.987 38.4320 2 2 6 -7 103.683 36.2341 2 2 -6 -6 2239.16 83.2863 2 -2 -6 6 2313.31 138.926 2 2 6 -6 2241.70 148.555 1 2 6 -6 2540.03 133.565 2 -2 6 6 2599.70 191.136 1 2 -6 -6 2510.49 152.820 3 -2 -6 5 330.744 53.6357 2 2 6 -5 331.879 52.2898 2 2 -6 -5 367.318 59.4215 3 -2 -6 4 1149.29 92.9000 2 2 -6 -4 1114.07 85.3055 3 2 6 -4 1182.04 86.3290 2 2 6 -3 366.345 56.0797 2 2 -6 -3 374.155 46.0021 3 -2 6 3 327.673 46.9433 3 -2 6 2 1173.02 63.7589 3 2 -6 -2 1267.37 60.9254 3 2 6 -2 1228.72 85.2159 2 2 6 -1 141.644 40.1474 2 2 -6 -1 36.0093 19.1551 3 -2 6 1 121.280 18.3300 3 2 6 0 10587.1 221.678 2 -2 -6 0 10503.2 247.361 3 2 6 1 2067.23 98.0140 2 -2 -6 -1 2142.90 101.927 2 2 6 2 387.847 46.1477 2 -2 -6 -2 398.465 44.8085 2 -2 6 -2 339.094 43.4433 3 -2 -6 -2 34.1386 69.9408 3 -2 6 -3 255.499 47.6977 3 2 -6 3 269.889 45.7011 2 -2 -6 -3 484.131 117.330 3 2 6 3 263.403 38.2245 2 -2 -6 -3 277.091 36.8685 2 2 -6 4 722.795 69.7698 2 2 6 4 651.766 51.8948 2 -2 6 -4 751.419 80.8916 3 -2 -6 -4 560.893 75.1171 3 -2 6 -5 26.3102 41.4119 3 2 6 5 5.56737 15.5785 2 -2 -6 -5 32.5994 43.4712 3 2 -6 5 32.2493 25.0085 2 -2 6 -6 2716.42 171.180 3 -2 -6 -6 2681.59 170.641 3 2 -6 6 2573.73 145.076 2 -2 -6 -7 513.898 88.5276 3 -2 6 -7 535.328 92.9999 3 -2 6 -8 388.250 88.0096 3 -2 -6 -8 303.757 77.5792 3 -2 6 -9 41.2219 58.4166 3 2 6 9-13.8436 53.1169 1 -2 -6 -9 37.1847 53.0757 3 -2 6 -10 859.966 132.583 3 -2 -6 -10 714.947 120.125 3 2 6 10 818.764 139.526 1 -2 6 -11-12.6006 56.2513 3 2 7 -12 11.9838 63.2808 3 2 -7 -12 73.2214 70.2136 3 2 7 -11 842.325 151.772 3 -2 7 11 1000.50 173.949 1 2 -7 -11 974.488 145.070 3 2 -7 -10 268.704 86.1987 3 2 7 -10 342.379 111.300 3 -2 7 10 208.296 96.9548 1 2 -7 -9 911.427 124.120 3 -2 7 9 745.172 140.818 1 2 7 -9 901.022 87.6116 2 2 -7 -8 875.142 111.019 3 2 7 -8 817.501 85.0676 2 -2 7 8 882.018 138.562 1 2 -7 -7 473.751 33.4747 2 2 -7 -7 516.867 81.2214 3 2 -7 -7 458.410 30.1422 2 -2 7 7 321.308 95.9989 1 2 7 -7 435.749 63.5400 2 -2 -7 6 1317.38 107.957 2 2 -7 -6 1290.33 62.8325 2 2 7 -6 1201.54 112.666 1 2 7 -6 1283.52 99.7450 2 -2 7 6 1311.66 143.471 1 2 -7 -6 1397.78 68.3985 2 2 -7 -6 1304.42 113.099 3 -2 -7 5 3141.37 160.881 2 2 7 -5 3539.95 156.943 2 2 -7 -5 3225.91 154.399 3 -2 -7 4 483.127 62.5816 2 -2 7 4 422.649 60.8287 3 2 7 -4 527.555 66.8046 2 2 -7 -4 409.777 54.6406 3 -2 7 3 2242.82 109.631 3 2 -7 -3 2447.38 103.570 3 2 7 -3 2458.06 122.117 2 2 -7 -2 1347.20 62.8229 3 2 7 -2 1454.28 95.2525 2 -2 7 2 1415.89 70.3450 3 2 7 -1 19878.1 321.772 2 -2 7 1 19158.8 185.769 3 -2 -7 0 321.521 66.7121 3 -2 7 0 255.940 41.5970 1 2 7 0 237.903 46.3976 2 -2 -7 0 253.349 43.2948 2 -2 -7 -1 3986.88 144.967 2 -2 7 -1 4408.87 112.927 1 2 7 1 3927.39 138.529 2 -2 -7 -2 194.450 35.4735 2 2 7 2 199.114 37.6199 2 -2 -7 -2-52.9855 112.901 3 2 7 3 413.509 45.0949 2 -2 -7 -3 360.241 42.4477 2 2 -7 3 439.182 55.8090 2 -2 -7 -3 450.824 84.3325 3 -2 7 -3 416.666 57.6386 3 -2 7 -4 3329.32 158.150 3 2 -7 4 3298.01 150.788 2 2 7 4 3357.99 112.672 2 -2 -7 -4 3412.59 167.167 3 2 7 5 4402.21 114.806 2 -2 -7 -5 5077.76 215.638 3 -2 7 -5 5337.44 220.896 3 -2 -7 -6 523.606 83.1942 3 -2 7 -6 526.630 84.1118 3 -2 7 -7 75.0277 53.8667 3 -2 -7 -7 75.5661 56.5570 3 -2 7 -8 343.597 82.7266 3 -2 -7 -8 350.939 78.4822 3 -2 7 -9 1539.44 164.584 3 -2 -7 -9 1738.57 169.084 3 2 7 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2 -2 8 3 39.8376 26.2163 3 2 -8 -3 24.5174 23.9871 3 2 -8 -2 2328.52 84.4201 3 2 -8 -2 2203.54 101.948 2 2 8 -2 2246.95 118.075 2 -2 8 2 2094.90 88.2710 3 -2 8 1 89.7987 20.9614 3 2 8 -1 146.390 45.3860 2 2 -8 -1-36.6296 42.1907 3 -2 8 1 124.792 46.7881 1 -2 8 0 10268.7 214.178 1 -2 -8 0 10949.5 253.868 2 2 8 0 10535.2 236.215 2 -2 -8 0 11180.7 266.975 3 2 8 1 3749.60 138.922 2 -2 -8 -1 3706.72 147.582 2 -2 -8 -2 1240.16 83.0496 2 2 8 2 1257.20 79.8868 2 2 8 3 11.3691 23.2293 2 -2 -8 -3 13.7943 88.9933 3 -2 -8 -3 8.58383 18.5067 2 2 -8 3 6.05054 20.2050 2 -2 -8 -4 6287.76 238.357 3 -2 8 -4 4539.14 192.960 3 2 8 4 5819.57 153.040 2 -2 -8 -4 5457.50 149.732 2 -2 8 -5 185.413 61.3172 3 -2 -8 -5 190.127 59.8390 3 2 8 5 220.225 30.5873 2 -2 8 -6 5569.83 248.904 3 2 8 6 4981.28 85.6808 2 -2 -8 -6 4988.12 234.394 3 -2 8 -7 20.2980 46.4605 3 -2 -8 -7 36.9362 48.3086 3 -2 8 -8 6.03704 48.7609 3 -2 -8 -8 9.98068 50.0902 3 -2 8 -9-0.09956 50.8822 3 -2 -8 -9-18.1556 47.5648 3 -2 -8 -10 1306.43 158.215 3 2 8 10 1458.66 189.584 1 -2 8 -10 1380.96 167.549 3 -2 8 -11 248.749 86.5886 3 2 9 -12 140.776 85.0393 3 -2 9 12 269.417 120.671 1 2 -9 -12 279.615 91.1874 3 -2 9 11 910.930 170.861 1 2 9 -11 1220.80 180.915 3 2 -9 -11 1164.21 153.892 3 2 -9 -10 130.209 65.2150 3 -2 9 10 163.000 95.7520 1 -2 9 9 1237.43 170.252 1 2 9 -9 1117.72 104.521 2 2 -9 -9 1244.62 141.869 3 2 -9 -8 300.647 73.1050 3 2 9 -8 265.599 56.9928 2 -2 9 8 230.564 88.5390 1 2 -9 -7 290.176 66.0679 3 2 -9 -7 293.223 31.4226 2 2 -9 -7 318.467 30.2689 2 2 9 -7 344.389 63.4453 2 -2 9 7 280.053 87.9756 1 2 -9 -6 2459.36 93.5386 2 2 9 -6 2762.70 155.518 2 -2 9 6 2961.43 210.005 1 2 -9 -6 2707.54 159.003 3 2 9 -5 2924.93 152.964 2 2 -9 -5 2830.58 108.357 2 2 -9 -5 2791.81 145.325 3 2 9 -4 146.387 48.1319 2 2 -9 -4 108.241 29.3373 2 -2 9 4 90.2555 37.8343 3 2 -9 -4 129.935 39.6548 3 2 -9 -3 2127.63 98.9421 3 2 9 -3 2104.71 124.627 2 2 -9 -3 2236.81 105.687 2 -2 9 3 2244.24 111.628 3 2 -9 -2 412.322 50.5036 2 2 -9 -2 460.260 55.0119 3 -2 9 2 402.885 42.7480 3 2 9 -2 380.493 61.2916 2 2 -9 -1 11705.2 236.396 3 2 9 -1 13286.9 282.609 2 -2 9 1 13772.0 186.660 3 -2 9 1 12422.4 276.213 1 -2 -9 0 1273.43 95.1158 2 -2 9 0 1689.44 111.280 3 -2 -9 0 1367.79 102.422 3 2 9 0 1188.34 88.8824 2 -2 9 0 1221.65 82.0235 1 -2 -9 -1 831.251 76.3528 2 2 9 1 897.815 75.4234 2 -2 9 -1 928.208 60.5148 1 2 9 2 392.914 51.4642 2 -2 -9 -2 309.867 46.4885 2 -2 -9 -3 2907.60 124.068 2 2 9 3 2830.15 117.606 2 -2 -9 -4 1969.23 155.315 3 2 9 4 2013.91 97.9032 2 -2 -9 -4 1986.23 96.4360 2 -2 9 -5 5668.14 237.250 3 -2 -9 -5 5793.60 244.077 3 2 9 5 5691.78 144.972 2 -2 9 -6 496.045 84.7033 3 2 9 6 439.717 30.2931 2 -2 -9 -6 429.233 83.6952 3 -2 9 -7 21.4934 46.3231 3 -2 -9 -7 25.3859 45.9486 3 -2 9 -8 426.571 89.9745 3 -2 -9 -8 498.778 94.8500 3 -2 -9 -9 763.396 118.704 3 -2 9 -9 771.412 123.073 3 -2 9 -10 243.412 82.0375 3 -2 -9 -10 284.875 83.6548 3 2 9 10 294.295 106.635 1 -2 9 -11 513.278 111.414 3 -2 10 12 292.665 116.262 1 2 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176.172 2 2 -10 -1 4959.74 139.634 3 -2 10 1 4828.34 121.474 3 -2 -10 0 4697.27 183.740 3 2 10 0 4098.31 160.832 2 -2 -10 0 4361.61 175.805 2 2 10 1 66.7732 35.5706 2 -2 -10 -1 185.248 286.705 3 -2 10 -1 113.099 30.8705 1 -2 -10 -1 108.772 35.3390 2 -2 -10 -2 477.263 59.0247 2 2 10 2 508.188 59.0183 2 -2 10 -2 696.560 45.0079 1 -2 -10 -3 1222.54 86.5061 2 2 10 3 1195.32 83.6757 2 -2 -10 -4 1412.59 166.952 3 2 10 4 2310.88 109.297 2 -2 -10 -4 2165.07 107.349 2 -2 10 -5 181.703 59.8607 3 2 10 5 202.590 34.0750 2 -2 -10 -5 268.406 68.2805 3 -2 10 -6 2246.58 165.364 3 2 10 6 2225.22 72.3075 2 -2 -10 -6 2192.33 162.074 3 -2 -10 -7 48.0297 50.3764 3 -2 10 -7-38.3602 49.6357 3 -2 10 -8 801.830 119.263 3 -2 -10 -8 707.402 108.732 3 -2 -10 -9 348.697 92.6287 3 -2 10 -9 297.528 85.0031 3 2 10 10 669.261 144.142 1 -2 -10 -10 576.693 114.443 3 -2 10 -10 545.761 113.825 3 -2 10 -11 204.270 79.7726 3 -2 11 12 50.1038 78.9694 1 2 11 -11-0.15187 72.0141 3 -2 11 11 26.8750 80.5170 1 2 -11 -11 19.5644 49.8206 3 2 11 -10 184.907 53.9694 2 -2 11 10 217.569 108.990 1 2 -11 -10 280.858 80.2515 3 2 11 -9 1416.30 124.735 2 -2 11 9 1497.88 197.583 1 2 -11 -9 1416.58 148.748 3 2 11 -8 216.993 55.2589 2 -2 11 8 154.780 87.9531 1 2 -11 -8 189.184 62.1305 3 2 11 -7 2635.94 164.787 2 -2 11 7 2987.74 235.879 1 2 -11 -7 2451.65 96.1922 2 2 -11 -7 2562.90 168.855 3 2 -11 -6 1682.52 89.3454 2 2 -11 -6 1778.81 131.761 3 2 11 -6 2008.08 142.810 2 -2 11 6 1993.82 186.710 1 2 -11 -5 2238.55 106.061 2 2 11 -5 2310.50 148.313 2 2 -11 -5 2238.70 130.969 3 -2 11 4 1125.53 96.6802 3 2 -11 -4 1025.34 82.2673 3 2 -11 -4 1034.00 76.9962 2 2 11 -4 1000.86 97.8149 2 2 -11 -3 1390.44 91.1587 2 2 11 -3 1255.91 106.284 2 2 -11 -3 1614.70 97.3548 3 -2 11 3 1303.10 90.9315 3 2 -11 -2 1126.24 84.8093 2 2 11 -2 1145.03 99.1299 2 -2 11 2 1035.92 71.9163 3 2 -11 -1 5828.03 199.559 2 -2 11 1 7235.91 159.955 3 2 11 -1 5610.02 201.092 2 -2 -11 0 816.999 83.9870 2 2 11 0 864.002 83.0815 2 -2 -11 -1 2075.50 125.394 2 2 11 1 2035.18 117.912 2 -2 -11 -1 2087.56 230.311 3 -2 11 -2 2165.81 82.1398 1 -2 -11 -2 2464.44 131.677 2 2 11 2 2366.14 123.346 2 -2 -11 -3 3592.05 152.499 2 2 11 3 3724.04 150.181 2 2 11 4 4566.32 158.181 2 -2 -11 -4 4131.48 154.908 2 2 11 5 2725.14 113.738 2 -2 -11 -5 2474.98 201.367 3 -2 -11 -5 2362.13 105.915 2 -2 11 -6 40.9707 45.5160 3 2 11 6 61.7463 18.2273 2 -2 -11 -6 38.7276 58.3993 3 -2 11 -7 6.96042 47.1071 3 -2 -11 -7 36.0474 59.0594 3 -2 11 -8 54.9889 54.6923 3 -2 -11 -8 175.357 69.1785 3 -2 -11 -9 916.014 133.184 3 -2 11 -9 862.286 131.532 3 2 11 10 122.302 80.9621 1 -2 -11 -10 183.939 68.4155 3 -2 11 -10 127.496 66.4324 3 -2 11 -11 247.890 86.0157 3 -2 12 12 646.703 160.212 1 -2 12 11 487.894 138.259 1 2 12 -11 319.817 115.812 3 2 -12 -11 423.959 97.8617 3 -2 12 10 211.632 104.554 1 2 12 -10 136.452 49.3668 2 2 -12 -10 170.678 63.9992 3 2 -12 -9 1278.38 139.634 3 2 12 -9 1292.86 121.935 2 -2 12 9 1438.31 197.872 1 -2 12 8 345.310 107.938 1 2 -12 -8 241.239 67.6789 3 2 12 -8 227.638 58.7535 2 2 12 -7 420.836 76.1254 2 2 -12 -7 355.798 41.2549 2 -2 12 7 489.023 114.061 1 2 -12 -7 326.875 69.9291 3 2 -12 -6 2166.55 107.470 2 2 12 -6 2404.97 157.228 2 -2 12 6 2349.93 200.953 1 2 -12 -6 2069.45 139.495 3 2 -12 -5 702.505 64.6264 2 2 12 -5 847.946 96.9530 2 -2 12 5 629.159 105.271 1 2 -12 -5 700.771 76.5866 3 2 -12 -4 4553.44 171.176 3 2 -12 -4 4305.71 160.343 2 2 12 -4 4639.22 205.792 2 -2 12 4 4321.38 187.507 3 2 -12 -3 1850.30 108.070 2 2 12 -3 1741.57 126.480 2 -2 12 3 1879.83 111.031 3 -2 12 2 13.5529 22.0152 3 2 -12 -2 58.5250 28.8678 2 2 -12 -2-32.5542 46.3307 3 2 12 -2 86.4740 48.7904 2 2 12 -1 3804.27 174.033 2 -2 12 1 3833.47 124.327 3 2 -12 -1 4148.60 125.794 3 2 12 0 8950.36 255.965 2 -2 -12 0 10578.7 288.885 3 -2 -12 0 9097.77 272.789 2 -2 -12 -1 75.6136 34.3324 2 2 12 1 105.526 40.3592 2 2 12 2 7091.68 220.215 2 -2 12 -2 5290.64 139.130 1 -2 -12 -2 6689.40 223.754 2 -2 -12 -3 653.774 71.6317 2 2 12 3 698.054 72.8065 2 2 12 4 107.577 33.4115 2 -2 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13 -6 2637.94 169.944 2 2 13 -5 155.849 53.7460 2 2 -13 -5 150.149 35.1849 2 2 -13 -5 174.164 46.6535 3 -2 13 5 170.557 71.2576 1 2 13 -4 70.8413 47.9473 2 2 -13 -4 178.467 45.2728 3 2 -13 -4 61.1104 29.9501 2 2 -13 -3 858.443 80.5021 2 2 13 -3 934.725 98.8710 2 -2 13 3 954.129 83.6879 3 2 13 -2 78.8312 43.8060 2 -2 13 2 103.860 31.4116 3 2 13 -1 353.416 64.8356 2 -2 13 1 690.667 50.4414 3 -2 13 0 13328.3 423.890 3 2 13 0 52.9347 42.4966 2 -2 13 -1-21.4678 36.4185 3 2 13 1 59.9796 38.3165 2 2 13 2 47.0019 37.5901 2 -2 -13 -2 36.3171 29.2534 2 -2 -13 -3 4172.34 180.858 2 2 13 3 4531.15 176.918 2 -2 13 -3 4462.50 104.686 1 -2 -13 -4 3500.87 157.997 2 2 13 4 3830.14 158.155 2 -2 -13 -5 987.497 79.6530 2 2 13 5 1259.59 86.7172 2 -2 13 -6 159.569 60.0209 3 2 13 6 183.805 31.6182 2 -2 -13 -6 49.5338 78.6358 3 -2 13 -7 1200.09 136.206 3 -2 -13 -7 1126.21 159.703 3 -2 13 -8 82.4656 58.6818 3 -2 -13 -8 141.564 72.7633 3 -2 13 -9 234.338 79.0569 3 -2 -13 -9 275.870 89.5060 3 2 13 10 27.4041 71.9444 1 -2 -13 -10 7.66380 52.5730 3 -2 13 -10 17.6626 50.3801 3 -2 13 -11 62.7000 56.1136 3 2 13 11 8.99118 64.0424 1 -2 14 11 84.6463 89.5830 1 2 -14 -11 44.6023 49.6802 3 2 14 -10 20.2244 37.4581 2 -2 14 10 64.8098 82.9963 1 2 -14 -10 76.8999 53.4790 3 -2 14 9 36.7051 73.7411 1 2 14 -9 2.22444 32.8799 2 2 -14 -9-21.6580 46.9758 3 2 14 -8 237.417 62.7059 2 2 -14 -8 262.425 67.5452 3 -2 14 8 231.252 97.5437 1 2 -14 -7-20.6714 37.4533 3 2 14 -7 16.3998 38.6454 2 -2 14 7 18.2541 62.9710 1 -2 14 6 496.730 105.920 1 2 14 -6 547.546 86.3181 2 2 -14 -6 512.495 74.9230 3 2 -14 -6 451.069 56.3225 2 2 -14 -5 414.359 64.9697 3 2 14 -5 312.225 68.0911 2 2 -14 -5 306.744 49.2821 2 -2 14 5 408.726 95.0672 1 2 -14 -4 120.175 35.0001 2 2 -14 -4 63.5903 50.9716 3 2 14 -4 103.759 52.2181 2 -2 14 3 501.583 64.3109 3 2 14 -3 490.627 79.4587 2 2 14 -2 1341.56 116.957 2 -2 14 2 1295.43 90.7119 3 -2 14 1 713.725 62.9491 3 2 14 -1 670.212 85.0335 2 -2 14 0 2531.96 197.852 3 2 14 0 2313.83 144.903 2 2 14 1 725.724 82.4529 2 -2 -14 -1 787.735 114.357 3 2 14 2 8655.71 259.444 2 -2 -14 -2 3249.60 307.220 3 -2 -14 -3 374.607 59.7803 2 2 14 3 409.053 62.4635 2 -2 -14 -3 80.1508 98.3245 3 -2 14 -3 309.760 33.5642 1 -2 -14 -4 472.551 62.0908 2 2 14 4 638.800 71.3989 2 2 14 5 545.921 61.0378 2 -2 -14 -5 379.459 53.6415 2 2 14 6 723.043 60.7592 2 -2 -14 -6 137.211 101.277 3 -2 -14 -7 33.8490 104.723 3 -2 14 -7 125.103 59.2893 3 -2 -14 -8 787.085 151.226 3 -2 14 -8 991.439 134.800 3 -2 14 -9 129.968 67.4779 3 -2 -14 -9 226.619 91.7965 3 -2 14 -10-32.8809 51.5104 3 -2 14 -11 218.195 84.2274 3 2 14 11 374.020 131.543 1 2 -15 -11 11.5024 44.9232 3 -2 15 11 88.4984 91.1343 1 -2 15 10 236.162 110.726 1 2 15 -10 272.646 68.9552 2 2 -15 -10 257.694 71.1481 3 2 15 -9 98.6459 49.0148 2 -2 15 9 152.913 88.5321 1 2 -15 -9 128.234 59.1488 3 2 -15 -8 59.6971 45.9591 3 2 15 -8 85.2873 51.4905 2 -2 15 8 8.37833 66.6624 1 2 -15 -7 1875.10 148.461 3 2 15 -7 1941.62 156.852 2 -2 15 7 2010.67 214.946 1 2 15 -6 8.90857 41.7065 2 2 -15 -6 13.8427 21.2803 2 -2 15 6-5.77987 63.6910 1 2 -15 -6 90.6550 44.0713 3 2 15 -5 1132.54 118.210 2 2 -15 -5 1281.96 122.424 3 2 15 -4 1027.10 112.282 2 2 15 -3 4500.55 218.083 2 -2 15 3 4353.08 185.640 3 2 -15 -2 726.909 103.371 3 2 15 -2 823.788 97.6654 2 -2 15 2 879.152 77.8810 3 2 15 -1 550.482 82.2452 2 -2 15 1 429.118 53.7495 3 -2 15 0 2419.87 223.034 3 2 15 0 4997.19 213.699 2 2 15 1 1961.24 134.093 2 -2 15 -1 1878.90 165.525 3 -2 -15 -1 2164.70 159.596 3 -2 -15 -2 91.6773 164.196 3 2 15 2 55.2724 38.7488 2 2 15 3 3381.98 166.154 2 -2 15 -3 2200.21 91.7767 1 -2 -15 -4 55.1571 113.290 3 -2 -15 -4 336.883 56.7944 2 2 15 4 499.012 66.6471 2 2 15 5 222.709 44.9657 2 -2 -15 -5 134.405 34.5969 2 -2 -15 -5 16.4496 143.320 3 -2 15 -7 1473.84 156.893 3 -2 -15 -7 461.087 145.171 3 -2 15 -8 119.161 63.3022 3 -2 -15 -8 10.0123 91.3064 3 -2 -15 -9-109.673 86.8688 3 -2 15 -9-20.7761 48.6937 3 -2 15 -10 0.12146 47.6323 3 -2 16 11 777.161 176.817 1 2 -16 -11 765.606 123.253 3 2 -16 -10 49.7627 51.6436 3 -2 16 10 24.9204 84.2654 1 2 16 -10 20.3245 38.6877 2 2 16 -9 532.571 93.4419 2 2 -16 -9 522.975 96.6591 3 -2 16 9 503.539 143.035 1 2 16 -8 125.326 54.5504 2 -2 16 8 139.659 90.0938 1 2 -16 -8 210.588 61.5688 3 2 -16 -7 110.468 49.1051 3 2 16 -7 22.6949 43.9003 2 -2 16 7 75.6563 79.5783 1 2 -16 -6 632.546 94.5621 3 2 16 -6 499.163 85.8535 2 -2 16 6 464.917 110.049 1 2 -16 -5 49.4662 58.9185 3 2 16 -5 134.735 56.7920 2 2 16 -4 211.547 66.0139 2 2 -16 -4-94.6630 65.1341 3 2 16 -3 411.307 79.1403 2 2 -16 -3 13.8825 43.6989 3 -2 16 2 768.485 76.3530 3 2 16 -2 809.743 98.8823 2 2 -16 -2 779.755 92.9362 3 2 16 -1 351.422 72.0433 2 -2 16 1 357.848 53.0688 3 2 16 0 383.442 69.8242 2 -2 16 0 1825.52 218.221 3 2 16 1 308.872 64.8360 2 -2 -16 -1 497.558 101.587 3 -2 -16 -2 5420.01 350.854 3 2 16 2 6844.68 249.935 2 -2 -16 -3-190.493 205.929 3 2 16 3 1503.47 117.817 2 2 16 4 473.559 68.6723 2 -2 -16 -4 29.4553 95.9624 3 2 16 5 166.234 41.0115 2 -2 -16 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169.908 3 -2 17 -1 2863.42 262.613 3 2 17 2-2.01538 36.5958 2 -2 17 -2-86.8213 42.9103 3 2 17 3 3602.19 182.967 2 -2 -17 -3 739.168 215.158 3 2 17 4 3020.24 162.499 2 -2 17 -4 2543.28 79.8265 1 2 17 5 299.095 52.5836 2 -2 -17 -5 64.8864 128.715 3 -2 -17 -6 31.9166 116.185 3 -2 17 -7 2049.77 185.430 3 -2 -17 -7 106.997 109.670 3 -2 17 -8 405.922 97.1855 3 -2 17 -9 149.596 65.4771 3 -2 -17 -9 21.0275 133.061 3 -2 17 -10 20.0879 45.3449 3 2 -18 -10 1201.70 148.051 3 2 18 -10 883.337 122.180 2 -2 18 10 1097.10 202.257 1 2 18 -9 1910.28 172.878 2 2 -18 -9 2483.01 206.776 3 -2 18 9 2611.66 285.438 1 2 -18 -8 930.763 130.258 3 -2 18 8 834.809 161.683 1 2 18 -8 784.482 110.719 2 2 18 -7 70.0291 44.7352 2 -2 18 7 124.964 90.6664 1 2 -18 -7 112.300 63.5826 3 2 18 -6 464.708 87.8463 2 -2 18 6 500.817 122.033 1 2 -18 -5-201.509 95.1380 3 2 18 -5 307.589 78.3825 2 2 18 -4 11.5885 48.6306 2 2 -18 -4-1.22050 42.2956 3 2 18 -3 22.6064 49.4983 2 2 -18 -3-28.6951 91.7905 3 2 18 -2 1099.46 118.715 2 2 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603.853 59.6011 2 3 10 -6 633.335 85.3874 2 3 -10 -6 667.248 81.2953 3 3 10 -5 2113.59 142.534 2 3 -10 -5 2024.59 121.348 3 3 -10 -4 526.385 59.0088 3 3 10 -4 605.935 80.9639 2 -3 10 3 10991.4 238.702 3 3 -10 -3 10683.6 203.106 3 3 10 -3 11904.6 306.695 2 -3 10 2 14.1185 17.0544 3 3 10 -2 8.26002 37.5962 2 -3 10 2 4.96067 41.1550 1 3 -10 -2-16.0382 36.2390 3 -3 10 1 4418.24 184.637 1 -3 10 1 3541.10 77.8931 3 3 10 -1 4067.21 175.977 2 -3 10 0 767.065 74.5361 1 -3 -10 0 837.969 89.0098 2 -3 -10 0 825.280 93.9642 3 -3 10 0 553.131 32.9120 3 3 10 0 787.115 81.8753 2 3 10 1 5930.30 207.568 2 -3 -10 -1 6195.13 222.939 2 -3 -10 -1 6419.23 374.352 3 -3 10 -2 2347.17 100.949 3 -3 -10 -2 2426.33 136.273 2 3 10 2 2285.45 126.611 2 -3 10 -3 1115.71 84.0359 3 -3 -10 -3 1162.15 92.2358 2 3 10 3 1279.03 94.4308 2 3 10 4 17.3297 27.4362 2 -3 10 -4 20.2242 31.7422 3 -3 -10 -4 3.52372 20.4059 2 -3 10 -5 1137.35 105.567 3 -3 -10 -5 535.841 130.514 3 3 10 5 1137.95 81.6036 2 -3 10 -6 16.6887 39.7671 3 -3 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51.9276 74.3859 1 4 14 -9 119.100 56.0944 2 4 -14 -9 140.471 53.5801 3 4 14 -8 112.455 54.1088 2 -4 14 8 70.5002 81.0654 1 4 -14 -8 113.177 45.4552 3 -4 14 7 1067.88 163.929 1 4 14 -7 1008.71 122.811 2 4 -14 -7 1059.64 104.630 3 -4 14 6 2007.64 199.399 1 4 14 -6 2003.81 163.198 2 4 -14 -6 1977.41 127.364 3 4 14 -5 11.3592 45.0767 2 -4 14 5 59.1111 67.5469 1 4 -14 -5 71.4838 31.0896 3 4 -14 -4 1576.05 127.919 3 4 14 -4 2137.30 161.798 2 -4 14 3 838.779 114.052 1 4 14 -3 812.853 101.650 2 -4 14 2 437.004 80.1543 1 4 14 -2 494.596 82.8405 2 4 14 -1 92.2270 53.6437 2 -4 14 0 2892.64 165.151 1 4 14 0 2926.82 176.057 2 -4 14 -1 212.984 24.3605 3 4 14 1 241.217 59.8681 2 -4 -14 -1 393.391 93.6047 3 -4 14 -2 440.402 43.6669 3 4 14 2 435.230 72.4297 2 -4 14 -3 348.528 48.0254 3 4 14 3 371.435 67.5868 2 -4 -14 -3 566.833 285.002 3 4 14 4 5179.09 221.383 2 -4 14 -4 5259.88 195.492 3 -4 14 -5 121.044 44.3193 3 -4 -14 -5 281.860 168.723 3 4 14 5 128.534 45.9942 2 -4 -14 -6-31.9950 106.359 3 -4 14 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-4 15 0 310.204 21.5008 3 -4 15 -1 3811.94 166.777 3 -4 -15 -1 4359.81 228.861 3 4 15 1 3735.20 199.240 2 4 15 2 552.229 81.8059 2 -4 15 -2 506.025 49.4590 3 4 15 3 26.3261 37.8361 2 -4 15 -3 11.8561 24.1756 3 -4 15 -4 577.370 69.6083 3 4 15 4 693.994 87.2594 2 -4 -15 -4 803.285 241.233 3 4 15 5 1873.65 134.697 2 -4 15 -5 1771.59 128.813 3 -4 15 -6 49.0451 41.5397 3 -4 -15 -6 85.5320 119.974 3 -4 -15 -7-49.7025 128.321 3 -4 -15 -8-90.6793 151.324 3 4 -16 -11 528.762 100.865 3 -4 16 10 1332.04 216.156 1 4 16 -10 1186.53 143.014 2 4 -16 -10 1185.27 137.303 3 -4 16 9-13.6918 78.0200 1 4 16 -9 6.10360 46.8099 2 4 -16 -9 16.2391 35.3140 3 4 16 -8 261.715 76.3428 2 4 -16 -8 260.266 62.6330 3 -4 16 8 331.112 113.881 1 4 16 -7 360.509 84.5420 2 4 -16 -7 339.936 63.1956 3 -4 16 7 397.668 112.835 1 -4 16 6-14.4576 64.2797 1 4 16 -6 15.8241 51.6393 2 4 -16 -6 119.333 38.8422 3 -4 16 5 51.6895 63.5051 1 4 -16 -5 12.4188 48.4574 3 4 16 -5 39.6526 48.5578 2 -4 16 4 3183.22 233.760 1 -4 16 4 2689.21 146.088 3 4 16 -4 3111.66 202.469 2 4 16 -3 438.058 85.0906 2 -4 16 3 382.241 49.6710 3 -4 16 3 445.980 92.2753 1 4 -16 -3 341.927 71.3557 3 4 16 -2 140.086 58.0205 2 -4 16 2 116.994 26.4300 3 -4 16 2 84.3990 56.7154 1 4 16 -1 1861.49 151.185 2 -4 16 1 1764.88 66.0306 3 4 16 0 1710.54 146.974 2 -4 16 0 1515.74 54.9333 3 -4 -16 -1 618.731 113.054 3 4 16 1 513.651 83.3779 2 4 16 2 1062.90 112.942 2 -4 16 -2 1058.21 70.9066 3 -4 16 -3 444.692 56.6928 3 4 16 3 509.635 81.2740 2 -4 16 -4 1514.50 108.881 3 4 16 4 1593.31 131.827 2 -4 16 -5 76.7767 38.8478 3 4 16 5 45.5047 34.6214 2 -4 -16 -6 113.888 131.783 3 -4 -16 -7-43.3958 107.368 3 -4 -16 -8 65.6032 119.862 3 4 -17 -11 99.8514 52.8046 3 -4 17 10-40.8461 75.9369 1 4 17 -10 9.79793 42.6059 2 4 -17 -10 18.4251 32.2333 3 -4 17 9 87.1238 84.5172 1 4 17 -9 9.62086 42.9293 2 4 -17 -9 40.0824 36.4386 3 4 17 -8-0.09290 50.6793 2 -4 17 8 72.5261 83.4996 1 4 -17 -8 63.2556 40.0188 3 -4 17 7 129.542 95.1057 1 4 17 -7 149.206 63.0359 2 4 -17 -7 179.367 50.3811 3 -4 17 6 137.960 82.1723 1 4 17 -6 167.921 63.9382 2 4 -17 -6 187.289 52.8828 3 -4 17 5 173.860 79.9072 1 4 17 -5 226.321 73.9131 2 -4 17 4 860.065 133.245 1 -4 17 4 632.458 73.5977 3 4 17 -4 737.503 108.848 2 -4 17 3 90.3330 33.2492 3 -4 17 3 112.927 65.1955 1 4 -17 -3 121.284 40.2598 3 4 17 -3 100.959 60.5509 2 -4 17 2 1346.58 77.5647 3 -4 17 2 1455.33 146.132 1 4 17 -2 1431.78 139.717 2 4 17 -1-3.54615 44.8372 2 -4 17 1 11.9684 15.7252 3 -4 17 1 28.0155 43.0226 1 4 17 0 365.320 77.4397 2 -4 17 0 220.321 26.3373 3 -4 -17 -1 83.1222 80.1664 3 4 17 1 225.256 66.2991 2 -4 -17 -2 1777.49 195.345 3 4 17 2 892.669 107.344 2 -4 17 -3 106.609 34.6409 3 4 17 3 112.682 49.5861 2 -4 17 -4 40.5023 33.8829 3 4 17 4 27.7022 38.3250 2 -4 -17 -5 326.081 164.977 3 -4 -17 -6 316.588 192.497 3 -4 -17 -7 108.288 141.513 3 4 -18 -11 270.052 70.7222 3 -4 18 10-1.35981 76.7468 1 4 18 -10 3.94267 39.1335 2 4 -18 -10 87.6467 45.4420 3 -4 18 9 869.700 175.372 1 4 18 -9 692.701 117.905 2 4 -18 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4 25 -5 361.398 95.5805 2 4 25 -4 945.102 139.482 2 -4 25 4 905.805 154.596 1 -4 25 3 81.3800 64.1579 1 4 25 -3 34.5904 54.9505 2 -4 25 2 258.906 83.1526 1 4 25 -2 245.368 81.3175 2 4 25 -1 463.249 100.345 2 -4 25 1 573.935 111.673 1 -4 25 0 44.4863 47.5717 1 4 25 0 3.32515 51.1553 2 4 25 1 88.3544 61.1148 2 4 25 2 122.179 60.5714 2 4 25 3 747.945 119.081 2 -4 -25 -3 718.665 125.246 3 -4 -25 -4 705.150 144.682 3 -4 26 7 222.861 105.567 1 -4 26 6 281.660 115.117 1 4 26 -6 329.752 91.2970 2 -4 26 5 309.137 117.865 1 4 26 -5 377.034 93.6597 2 -4 26 4 248.933 91.9707 1 4 26 -4 229.502 79.9355 2 -4 26 3 40.8995 61.4432 1 4 26 -3 67.4568 61.9991 2 -4 26 2 178.677 76.4954 1 4 26 -2 199.018 75.6042 2 -4 26 1 342.904 91.5646 1 4 26 -1 318.782 92.6926 2 4 26 0 766.681 125.118 2 4 26 1 39.8042 51.7831 2 4 26 2-0.30456 42.3387 2 4 26 3 366.279 85.7552 2 -4 -26 -4 534.119 127.160 3 -4 27 6 309.708 115.170 1 -4 27 5 433.948 125.068 1 4 27 -5 403.533 97.9207 2 -4 27 4 68.8037 66.2994 1 4 27 -4 15.8571 51.4108 2 -4 27 3-1.76137 55.7396 1 4 27 -3 14.7332 54.1404 2 -4 27 2 409.480 101.909 1 4 27 -2 578.651 115.109 2 -4 27 1 241.135 83.2618 1 4 27 -1 322.356 93.4679 2 4 27 0 65.3123 58.7025 2 4 27 1 6.75797 46.6906 2 4 27 2-8.98184 46.3921 2 4 27 3 13.9235 39.2945 2 -4 28 6 561.890 146.451 1 -4 28 5 40.3385 68.0370 1 -4 28 4 331.346 107.572 1 4 28 -4 270.754 89.3111 2 -4 28 3-17.0490 56.5329 1 4 28 -3 23.6432 55.5156 2 -4 28 2 161.903 77.5338 1 4 28 -2 144.987 69.8782 2 4 28 -1 68.6397 64.7206 2 4 28 0 1670.69 182.657 2 4 28 1 145.699 65.5112 2 4 28 2 29.9110 56.9505 2 4 28 3 153.769 65.0641 2 -4 29 5 967.946 176.829 1 -4 29 4 16.7614 74.7766 1 -4 29 3 82.1084 70.8346 1 4 29 -3 125.581 69.8786 2 -4 29 2 32.3098 61.1757 1 4 29 -2-43.4440 60.7043 2 4 29 -1 496.354 112.278 2 4 29 0 24.3475 49.7388 2 4 29 1 231.364 79.4628 2 4 29 2 37.5390 49.4949 2 -4 30 4 45.7982 70.1262 1 -4 30 3-2.70447 57.2058 1 -4 30 2 59.0676 57.5474 1 4 30 -1 37.6811 61.2008 2 4 30 0 1743.02 192.275 2 4 30 1 31.7608 45.7314 2 4 30 2 79.7097 55.5875 2 -4 31 4 48.5430 62.0668 1 -4 31 3 240.828 93.1047 1 4 31 1 16.7940 41.9979 2 4 31 2 47.6219 50.3529 2 -4 32 3 209.196 85.3312 1 5 0 -12 13.5234 52.5063 3 5 0 -11 670.054 129.539 3 5 0 -10-30.6687 52.3462 3 5 0 -9 8145.97 279.126 2 5 0 -8-4.58160 27.6449 2 5 0 -7 54.0983 36.0354 2 5 0 -6 8.74161 29.1051 2 5 0 -5 615.842 78.6025 2 5 0 -4 9.11524 37.9477 2 5 0 -3 14182.4 346.126 2 5 0 -2-5.33678 41.0016 2 5 0 -2-3.10011 20.1873 3 5 0 -1 3447.13 169.097 2 5 0 -1-2.40152 65.4786 3 5 0 0 105.824 48.7938 2 5 0 0 93.0612 34.5109 3 5 0 1 1388.56 113.406 2 5 0 1 1526.47 98.9449 3 5 0 2-2.09982 23.9361 3 -5 0 -2 2938.09 264.341 3 -5 0 -3 218.037 114.045 3 5 0 4 7.97988 34.7461 2 -5 0 -4-5.54531 89.9658 3 5 0 5 152.723 52.6952 2 -5 0 -5 76.3588 50.6467 3 5 0 6-25.3292 34.3914 2 -5 0 -6 9.15903 44.4972 3 -5 0 -7 1438.79 145.218 3 -5 0 -8-23.2289 49.2774 3 -5 0 -9 30.3761 45.8747 3 -5 0 -10-49.1647 55.1449 3 5 -1 -12 131.735 70.9822 3 5 1 -12 318.093 100.122 3 5 -1 -11 240.101 86.7085 3 5 1 -11 155.764 78.9875 3 5 1 -10 46.7503 31.1415 2 5 -1 -10 14.9261 52.8669 3 5 1 -10-35.9186 63.1092 3 5 -1 -9 130.654 71.8976 3 5 1 -9 150.075 48.1620 2 5 -1 -9 135.493 44.6067 2 5 1 -8 1051.95 105.266 2 5 -1 -8 955.079 97.3013 2 5 1 -7 534.427 76.2721 2 5 -1 -7 513.096 72.7166 2 5 -1 -6 124.538 42.3659 2 5 1 -6 124.101 43.1076 2 5 1 -5 1055.25 102.137 2 5 -1 -5 925.586 93.4357 2 5 1 -4 2533.22 151.494 2 5 -1 -4 2459.70 149.417 2 5 1 -3 548.311 79.0497 2 5 -1 -3 580.572 79.3547 2 5 -1 -2 406.454 69.2736 2 5 1 -2 385.711 69.5188 2 5 -1 -2 367.097 46.0528 3 5 1 -2 386.086 52.0204 3 5 1 -1 60.8501 61.3213 3 5 -1 -1 1730.45 122.717 2 5 1 -1 1592.57 118.715 2 5 -1 -1-30.0762 73.3620 3 5 1 0 1010.51 100.686 3 5 -1 0 1046.66 73.4362 3 5 1 0 929.887 93.9190 2 5 -1 1 189.854 37.6717 3 5 1 1 167.442 49.0362 2 -5 -1 -1 16.5923 205.929 3 -5 1 -1 227.689 201.250 3 5 1 1 160.549 39.3979 3 5 1 2 2559.28 152.984 2 -5 1 -2 2356.80 259.062 3 5 -1 2 2402.51 130.349 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669.050 85.6647 2 5 -2 -4 687.974 83.1262 2 5 -2 -3 6192.74 225.818 2 5 2 -3 6310.32 234.761 2 5 2 -2 53.5945 44.2063 2 5 -2 -2 16.6464 21.4580 3 5 2 -2 53.2860 36.6073 3 5 2 -1-18.6649 73.3346 3 5 -2 -1-116.409 84.9809 3 5 2 0 275.895 61.6550 2 5 -2 0 399.716 43.4114 3 5 2 0 310.002 74.3559 3 -5 -2 -1 2111.01 266.772 3 -5 2 -1 1538.58 225.250 3 5 2 1 3797.75 166.522 3 5 2 1 3658.81 182.155 2 5 -2 1 3408.85 135.038 3 -5 2 -2 1360.59 225.244 3 5 2 2 1780.94 128.015 2 5 -2 2 1563.01 103.572 3 5 2 3 35.8373 38.4695 2 -5 2 -3-5.83155 69.3099 3 5 2 4 82.2603 44.7296 2 -5 2 -4 44.1060 61.2349 3 5 2 5 368.157 70.8864 2 -5 -2 -5 253.581 73.5148 3 -5 2 -5 277.037 60.7661 3 5 2 6 257.900 57.5127 2 -5 -2 -6 234.209 77.4170 3 -5 2 -6 209.735 61.0384 3 -5 -2 -7 2100.24 174.494 3 -5 2 -7 2085.09 165.759 3 -5 -2 -8 53.5471 50.4236 3 -5 2 -8 79.9936 49.0134 3 -5 -2 -9-36.1795 62.4580 3 -5 2 -9 34.1612 40.8406 3 -5 2 -10 32.8963 47.6092 3 5 -3 -12 116.856 70.6524 3 5 3 -12 192.280 82.6680 3 5 -3 -11 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695.500 88.8582 3 -5 -10 -7 15.6911 132.780 3 -5 10 -7 286.442 64.4649 3 5 -11 -12 140.793 63.6844 3 5 -11 -11 201.844 68.9022 3 5 -11 -10 282.404 73.0111 3 5 11 -10 284.073 72.8911 2 5 -11 -9 6.85238 37.7029 3 5 11 -9 20.8727 45.8717 2 5 11 -8 57.6520 47.1449 2 5 -11 -8 96.9986 45.4420 3 5 -11 -8 95.9031 38.2293 2 5 11 -7 1892.07 157.384 2 5 -11 -7 1839.62 134.943 3 5 -11 -6 112.772 39.9595 3 5 11 -6 82.7747 49.0440 2 5 -11 -5 1099.51 84.0319 3 5 11 -5 1211.83 126.502 2 5 -11 -4 4742.60 140.150 3 5 11 -4 4457.28 228.774 2 5 -11 -3 791.420 55.9811 3 5 11 -3 801.383 102.444 2 5 11 -2 2231.91 160.374 2 5 11 -1 717.506 94.4346 2 5 11 0 716.034 94.9110 2 5 11 1 332.711 69.5029 2 -5 -11 -1 471.378 108.311 3 5 11 2 1624.78 133.919 2 -5 11 -2 978.327 53.0033 3 5 11 3 281.224 64.3929 2 -5 11 -3 303.708 44.5032 3 -5 -11 -4 2829.64 343.248 3 -5 11 -4 2039.37 115.502 3 5 11 4 2124.74 150.460 2 -5 11 -5 166.032 45.9066 3 5 11 5 179.360 54.2601 2 -5 11 -6 248.389 56.7022 3 -5 -11 -6 100.370 155.965 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357.667 52.0115 3 5 13 5 224.804 58.5924 2 -5 -13 -5 1391.19 278.018 3 -5 -13 -6 742.542 253.512 3 -5 -13 -7 282.059 196.110 3 -5 -13 -8 375.287 206.526 3 5 -14 -12-0.44538 39.2077 3 5 -14 -11 60.7185 45.2887 3 5 14 -10 127.725 58.9215 2 5 -14 -10 65.7866 42.4734 3 -5 14 9 2994.11 299.885 1 5 14 -9 2803.42 210.752 2 5 -14 -9 2902.61 193.671 3 -5 14 8 724.698 155.008 1 5 14 -8 616.700 107.079 2 5 -14 -8 740.605 94.4502 3 -5 14 7 42.7132 70.7082 1 5 -14 -7 8.62607 24.6927 3 5 14 -7 24.8315 49.0612 2 5 14 -6 76.3567 54.1118 2 -5 14 6 45.8223 68.4242 1 5 -14 -6 74.6439 32.4892 3 -5 14 5 887.250 138.789 1 5 -14 -5 925.387 75.5191 3 5 14 -5 902.088 114.445 2 5 14 -4 244.809 71.9474 2 5 -14 -4-19.4981 36.1222 3 -5 14 4 285.168 88.4240 1 -5 14 3 2948.04 215.274 1 5 -14 -3 2714.09 110.314 3 5 14 -3 2989.54 192.338 2 5 14 -2 236.290 67.4896 2 5 14 -1 1398.99 133.086 2 5 14 0 18.7832 47.9903 2 -5 -14 -1 5610.27 263.295 3 5 14 1 5758.54 260.503 2 5 14 2 45.3105 43.4978 2 -5 14 -2 149.128 23.1191 3 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32.6753 51.5686 2 9 17 1 44.7784 61.3290 2 9 17 2 243.044 83.5501 2 9 -18 -8 100.040 52.9093 2 9 18 -5 579.038 118.203 2 9 18 -4 1.09971 53.5293 2 9 18 -3 367.577 97.6012 2 9 18 -2 1051.63 153.352 2 9 18 -1 596.352 121.785 2 9 18 0 77.9657 56.4214 2 9 18 1 653.212 123.875 2 9 18 2 293.468 87.4531 2 9 19 -4 381.811 99.9653 2 9 19 -3 206.530 85.8392 2 9 19 -2 475.925 110.585 2 9 19 -1 794.135 135.499 2 9 19 0 118.753 67.7269 2 9 19 1 269.546 87.4339 2 9 19 2 63.8569 51.2089 2 9 20 -2 120.885 71.4922 2 9 20 -1 1288.64 172.245 2 9 20 0 287.903 89.5736 2 9 20 1 198.075 75.9008 2 10 0 -10 20.4681 38.7231 2 10 0 -9-20.7294 51.5635 2 10 0 -8 507.755 107.532 2 10 0 -7-10.8097 51.4708 2 10 0 -6 65.3266 56.9055 2 10 0 -5-7.30037 53.2982 2 10 0 -4 543.468 108.941 2 10 0 -3-1.21781 54.3167 2 10 0 -2 1207.38 158.108 2 10 0 -1-5.56380 53.8288 2 10 0 0 16.5622 51.4359 2 10 0 1-29.5290 55.3775 2 10 0 2 1612.87 188.775 2 10 0 3-8.26588 47.1188 2 10 0 4 28.2425 41.7350 2 10 1 -10-11.1578 37.8266 2 10 -1 -10 45.0082 50.6210 2 10 1 -9 240.726 79.4570 2 10 -1 -9 182.888 72.5946 2 10 1 -8-3.17029 52.4494 2 10 -1 -8 24.3608 53.0393 2 10 1 -7 1024.93 148.349 2 10 -1 -7 1151.27 155.859 2 10 1 -6 477.974 107.483 2 10 -1 -6 496.987 109.101 2 10 1 -5 55.5569 54.6048 2 10 -1 -5 24.7690 48.1631 2 10 1 -4 20.5243 56.0302 2 10 -1 -4-56.1402 57.5371 2 10 1 -3 1297.81 162.101 2 10 -1 -3 1270.92 160.842 2 10 1 -2 120.061 70.4479 2 10 -1 -2 21.6653 53.2927 2 10 1 -1 432.517 101.395 2 10 -1 -1 445.693 103.425 2 10 1 0 4.67887 50.4820 2 10 -1 0-5.16891 52.7915 2 10 1 1 361.939 96.9137 2 10 -1 1 270.839 90.8334 2 10 1 2-17.9581 61.5696 2 10 -1 2-29.7475 57.4881 2 10 1 3 1153.05 162.633 2 10 -1 3 1130.27 162.080 2 10 1 4 306.356 93.1724 2 10 -1 4 311.282 93.5816 2 10 2 -10 4.23412 36.5534 2 10 -2 -10-22.4485 43.7803 2 10 2 -9 43.3146 51.2244 2 10 -2 -9 43.7536 49.0749 2 10 2 -8 1253.05 164.423 2 10 -2 -8 1201.49 160.305 2 10 -2 -7 340.497 92.3719 2 10 2 -7 333.598 91.4647 2 10 -2 -6 447.218 102.943 2 10 2 -6 413.176 98.5138 2 10 -2 -5 484.318 107.300 2 10 2 -5 637.999 122.313 2 10 2 -4 961.638 142.584 2 10 -2 -4 998.355 144.707 2 10 2 -3-2.22160 49.5521 2 10 -2 -3-8.08044 56.3913 2 10 2 -2 703.337 128.755 2 10 -2 -2 684.987 122.716 2 10 2 -1 255.629 82.8307 2 10 -2 -1 265.708 86.3770 2 10 2 0 65.1332 57.9861 2 10 -2 0 26.1316 53.2531 2 10 2 1 2.40886 57.9912 2 10 -2 1 16.0666 52.6755 2 10 2 2 935.319 149.277 2 10 -2 2 866.851 142.402 2 10 2 3 223.851 86.7448 2 10 -2 3 213.205 87.2419 2 10 -2 4 200.553 80.3236 2 10 3 -10 109.243 59.3870 2 10 -3 -10 5.06369 39.0395 2 10 3 -9 263.654 82.0176 2 10 -3 -9 362.624 94.2083 2 10 -3 -8 100.858 61.4641 2 10 3 -8 94.1643 67.8094 2 10 -3 -7 313.097 90.3021 2 10 3 -7 253.996 84.9905 2 10 -3 -6 49.3330 57.1140 2 10 3 -6 67.4690 54.7825 2 10 -3 -5 44.1854 49.9494 2 10 3 -5 15.8265 53.3516 2 10 3 -4 999.991 146.849 2 10 -3 -4 1026.32 143.901 2 10 -3 -3 421.077 102.526 2 10 3 -3 606.862 119.966 2 10 3 -2 570.345 115.490 2 10 -3 -2 662.238 123.348 2 10 3 -1 940.882 143.579 2 10 -3 -1 709.559 126.646 2 10 3 0-7.27275 44.8098 2 10 -3 0-21.9477 50.1179 2 10 3 1 284.792 89.3190 2 10 -3 1 272.666 90.2913 2 10 3 2 196.332 79.0168 2 10 -3 2 89.6476 62.0892 2 10 3 3 270.534 85.3206 2 10 -3 3 260.675 91.6539 2 10 -3 4 258.155 90.4092 2 10 4 -10 140.991 66.2277 2 10 -4 -10 215.266 72.4326 2 10 4 -9 466.822 105.898 2 10 -4 -9 245.402 78.3599 2 10 -4 -8 262.599 84.0914 2 10 4 -8 270.945 88.6962 2 10 -4 -7 91.6887 67.6205 2 10 4 -7 41.6347 55.2291 2 10 -4 -6-14.9782 49.3804 2 10 4 -6 23.1618 52.6991 2 10 -4 -5 63.0098 59.7673 2 10 4 -5 43.9834 52.7498 2 10 -4 -4 365.622 97.0970 2 10 4 -4 425.313 99.1750 2 10 4 -3 578.979 115.944 2 10 -4 -3 589.950 118.190 2 10 4 -2 123.179 69.6186 2 10 -4 -2 176.299 77.3414 2 10 4 -1 94.3296 64.7489 2 10 -4 -1 157.380 70.3763 2 10 4 0 281.421 91.3687 2 10 -4 0 332.877 88.4462 2 10 4 1 171.785 73.6162 2 10 -4 1 164.595 70.0047 2 10 4 2 234.172 87.8748 2 10 -4 2 174.235 71.8908 2 10 4 3 306.649 94.7000 2 10 -4 3 403.514 104.667 2 10 -4 4 213.416 80.6081 2 10 5 -10-6.61210 48.5496 2 10 -5 -10-17.7218 40.8869 2 10 -5 -9 360.709 93.2576 2 10 5 -9 331.154 97.2525 2 10 -5 -8 416.743 99.4073 2 10 5 -8 319.387 90.5396 2 10 -5 -7 136.162 70.3643 2 10 5 -7 210.473 78.9099 2 10 -5 -6 325.250 91.8728 2 10 5 -6 367.770 99.0916 2 10 -5 -5 473.204 103.829 2 10 5 -5 530.190 109.648 2 10 5 -4 681.131 125.552 2 10 -5 -4 749.179 128.941 2 10 -5 -3 207.249 80.3517 2 10 5 -3 242.263 86.4540 2 10 5 -2 303.738 93.1568 2 10 -5 -2 349.460 90.4653 2 10 5 -1 1040.44 150.733 2 10 -5 -1 972.150 143.683 2 10 5 0 44.5533 56.1348 2 10 -5 0 38.0749 52.0748 2 10 5 1 486.163 108.315 2 10 -5 1 422.760 102.160 2 10 -5 2 158.268 71.2512 2 10 5 2 165.159 75.6431 2 10 -5 3 76.5434 64.9799 2 10 5 3 32.0803 48.5282 2 10 -5 4 339.731 96.4423 2 10 6 -10 618.464 118.966 2 10 -6 -9 114.176 63.1172 2 10 6 -9 81.6573 63.8962 2 10 -6 -8 64.4363 52.7112 2 10 6 -8 42.5427 52.1722 2 10 -6 -7-3.99218 47.6647 2 10 6 -7-21.8581 53.6492 2 10 6 -6 894.295 143.333 2 10 -6 -6 810.216 135.430 2 10 -6 -5 37.8403 59.0355 2 10 6 -5 76.6740 64.0599 2 10 6 -4 957.923 147.416 2 10 -6 -4 1052.95 147.173 2 10 -6 -3 42.4657 55.9754 2 10 6 -3 23.1359 54.8255 2 10 -6 -2 148.179 71.7201 2 10 6 -2 190.794 77.6684 2 10 -6 -1 44.0968 58.8526 2 10 6 -1 49.4906 64.0417 2 10 -6 0 989.391 148.218 2 10 6 0 859.764 142.028 2 10 -6 1 38.2104 55.5719 2 10 6 1 49.8895 60.1439 2 10 -6 2 114.970 63.6707 2 10 6 2 207.810 83.9005 2 10 -6 3 46.8226 54.3606 2 10 6 3 15.4503 43.8950 2 10 7 -10 131.405 68.4000 2 10 7 -9 796.227 136.535 2 10 -7 -9 810.176 131.521 2 10 -7 -8 5.58322 40.1599 2 10 7 -8-31.4680 49.0150 2 10 -7 -7 3.78252 46.2769 2 10 7 -7 87.0162 68.2738 2 10 -7 -6 55.8583 55.6933 2 10 7 -6 54.3916 62.7359 2 10 7 -5 2019.61 208.321 2 10 -7 -5 2108.56 202.540 2 10 -7 -4 355.720 94.2910 2 10 7 -4 240.990 87.3250 2 10 -7 -3 54.5070 55.7092 2 10 7 -3 13.2520 52.5386 2 10 -7 -2 20.0162 51.0192 2 10 7 -2 37.8327 60.1438 2 10 -7 -1 1060.60 153.396 2 10 7 -1 975.946 146.416 2 10 -7 0 18.2630 50.7608 2 10 7 0 92.2124 66.2905 2 10 -7 1 563.662 119.577 2 10 7 1 517.529 114.971 2 10 -7 2 47.1544 46.7942 2 10 7 2-26.6644 59.8078 2 10 -7 3 348.435 96.5411 2 10 7 3 311.956 93.9239 2 10 8 -10 826.957 140.763 2 10 -8 -9 219.537 76.5962 2 10 8 -9 215.452 79.5624 2 10 -8 -8 139.991 64.5277 2 10 8 -8 197.935 77.8178 2 10 -8 -7 136.474 72.7026 2 10 8 -7 184.052 76.1358 2 10 -8 -6 418.779 104.138 2 10 8 -6 522.476 113.042 2 10 -8 -5-43.5130 61.0598 2 10 8 -5-13.5553 57.1614 2 10 -8 -4 1261.50 158.892 2 10 8 -4 1140.01 158.786 2 10 -8 -3 238.188 85.0246 2 10 8 -3 186.258 80.1348 2 10 -8 -2 457.780 106.727 2 10 8 -2 456.994 108.609 2 10 -8 -1 128.286 74.7797 2 10 8 -1 133.483 73.9364 2 10 8 0 2332.86 223.858 2 10 -8 0 2612.08 233.725 2 10 -8 1 415.134 105.444 2 10 8 1 298.919 92.8585 2 10 -8 2-15.6679 54.0958 2 10 8 2-10.6098 49.8287 2 10 8 3 47.3162 48.7679 2 10 -9 -9 519.464 107.587 2 10 9 -9 535.170 117.866 2 10 -9 -8-2.93648 41.6094 2 10 9 -8 2.64207 53.4955 2 10 -9 -7 108.232 63.0739 2 10 9 -7 238.739 83.5438 2 10 -9 -6 67.5606 62.2591 2 10 9 -6 117.626 71.6570 2 10 9 -5 617.435 122.405 2 10 -9 -5 568.092 112.033 2 10 -9 -4 210.420 81.4632 2 10 9 -4 119.992 71.3387 2 10 9 -3-5.41956 53.4815 2 10 -9 -3 46.5366 61.0803 2 10 9 -2 83.4694 60.4107 2 10 9 -1 257.179 89.3294 2 10 9 0 63.7866 62.6417 2 10 9 1 285.290 95.3108 2 10 9 2 90.9423 67.7181 2 10 9 3 612.881 124.121 2 10 -10 -9 905.145 140.481 2 10 -10 -8 178.345 71.9343 2 10 10 -8 193.101 80.4818 2 10 10 -7 245.213 82.2761 2 10 -10 -7 208.775 79.3014 2 10 10 -6 281.004 88.0432 2 10 -10 -6 301.172 89.6562 2 10 10 -5 167.204 82.5570 2 10 -10 -5 71.1921 54.3515 2 10 10 -4 135.359 73.2967 2 10 -10 -4 203.582 78.7109 2 10 10 -3 22.4636 57.2113 2 10 10 -2 704.917 128.915 2 10 10 -1 613.948 124.786 2 10 10 0 433.295 107.636 2 10 10 1 458.813 108.514 2 10 10 2 237.067 86.4448 2 10 -11 -9 10.6459 42.9237 2 10 11 -8 206.655 84.0700 2 10 -11 -8 189.625 71.2640 2 10 11 -7 355.420 98.4348 2 10 -11 -7 376.841 94.4854 2 10 11 -6 457.060 106.901 2 10 -11 -6 504.003 108.300 2 10 11 -5 331.283 98.4798 2 10 -11 -5 376.417 95.7146 2 10 11 -4 785.002 137.791 2 10 -11 -4 779.049 129.969 2 10 11 -3 657.794 125.478 2 10 11 -2 93.3006 72.7189 2 10 11 -1 13.8657 51.8072 2 10 11 0-2.76105 48.6334 2 10 11 1 54.4867 60.3729 2 10 11 2 23.8000 51.5902 2 10 -12 -9 237.314 81.1044 2 10 -12 -8 338.568 97.4774 2 10 12 -7 121.082 72.9438 2 10 -12 -7 21.6118 45.7628 2 10 12 -6 99.5617 58.6570 2 10 -12 -6 66.7743 57.6354 2 10 12 -5 26.6025 55.6033 2 10 -12 -5 53.3932 55.7218 2 10 12 -4 713.715 132.460 2 10 12 -3-28.0820 52.4194 2 10 12 -2 244.424 86.5257 2 10 12 -1 425.798 107.664 2 10 12 0 17.5560 50.6904 2 10 12 1 452.285 110.415 2 10 12 2 1012.38 152.790 2 10 -13 -8 2.34086 46.7312 2 10 -13 -7 1121.79 156.031 2 10 13 -6 403.047 105.691 2 10 -13 -6 295.071 94.1749 2 10 13 -5 66.7705 75.1586 2 10 13 -4 59.4574 56.0553 2 10 13 -3 1211.60 167.964 2 10 13 -2-3.78747 52.1478 2 10 13 -1 98.4726 71.3183 2 10 13 0 86.1061 64.5051 2 10 13 1 179.539 76.4191 2 10 13 2 212.461 79.0648 2 10 -14 -8 1031.66 149.944 2 10 -14 -7 30.7832 43.7178 2 10 -14 -6 213.378 78.3350 2 10 14 -5 39.1262 59.2156 2 10 14 -4-11.3513 50.7530 2 10 14 -3 56.6366 63.6077 2 10 14 -2 343.334 98.0233 2 10 14 -1 19.3896 53.1504 2 10 14 0 53.1729 61.9158 2 10 14 1 56.1784 61.5458 2 10 14 2 1910.54 211.846 2 10 -15 -8 31.1722 49.1038 2 10 -15 -7 1113.69 157.375 2 10 15 -3 1701.99 201.797 2 10 15 -2 0.13178 57.0561 2 10 15 -1 253.154 89.4148 2 10 15 0-14.1935 49.7694 2 10 15 1 49.1669 52.4626 2 10 -16 -8 146.673 63.0686 2 10 -16 -7 40.7260 46.9187 2 11 0 -8-34.5786 57.6286 2 11 0 -7 92.1879 64.2963 2 11 0 -6 10.7564 61.4677 2 11 0 -5 223.450 83.0918 2 11 0 -4-3.39135 59.7735 2 11 0 -3 17.9659 52.0109 2 11 0 -2-10.6758 50.2757 2 11 0 -1 138.635 73.8928 2 11 0 0 0.13465 55.2948 2 11 -1 -9 37.6317 49.0216 2 11 1 -8-5.01225 44.8302 2 11 -1 -8-9.26519 53.4456 2 11 -1 -7 139.860 74.0461 2 11 1 -7 56.5681 59.7893 2 11 1 -6 1493.36 188.554 2 11 -1 -6 1721.58 196.999 2 11 1 -5 27.3423 59.3828 2 11 -1 -5-36.6893 68.3408 2 11 1 -4 78.0352 65.8342 2 11 -1 -4 61.4590 59.1322 2 11 1 -3 64.0619 61.5156 2 11 -1 -3 7.73337 53.4817 2 11 1 -2 1115.08 164.308 2 11 -1 -2 1286.80 173.115 2 11 1 -1 48.8643 61.5238 2 11 -1 -1-15.8506 65.9099 2 11 1 0 360.312 99.5233 2 11 -1 0 331.317 102.445 2 11 1 1-6.21439 48.4184 2 11 -2 -9 245.645 82.1358 2 11 2 -8 176.122 76.9319 2 11 -2 -8 185.175 74.5376 2 11 -2 -7 535.435 118.206 2 11 2 -7 481.619 113.857 2 11 -2 -6 59.6694 61.8809 2 11 2 -6-21.2048 56.1567 2 11 2 -5 544.003 120.841 2 11 -2 -5 525.274 119.266 2 11 2 -4 210.368 84.2294 2 11 -2 -4 172.482 78.2800 2 11 2 -3 149.067 74.9016 2 11 -2 -3 183.653 79.8130 2 11 2 -2-20.8762 54.6443 2 11 -2 -2-18.7284 54.2101 2 11 2 -1 372.715 105.459 2 11 -2 -1 264.857 94.1535 2 11 2 0 150.569 75.1556 2 11 -2 0 115.742 68.5082 2 11 2 1 138.416 78.1219 2 11 -3 -9 38.8141 52.9925 2 11 -3 -8 305.668 91.1983 2 11 -3 -7 205.441 84.8482 2 11 3 -7 100.465 67.3604 2 11 3 -6 1154.88 166.289 2 11 -3 -6 1039.45 155.059 2 11 -3 -5 483.788 115.180 2 11 3 -5 456.486 111.774 2 11 3 -4 357.077 104.397 2 11 -3 -4 315.122 89.5072 2 11 3 -3-19.6189 58.0231 2 11 -3 -3 42.1786 58.4969 2 11 3 -2 697.877 130.276 2 11 -3 -2 659.654 129.781 2 11 3 -1 6.71413 55.9796 2 11 -3 -1 13.7746 46.8256 2 11 3 0 184.618 83.5866 2 11 -3 0 121.046 70.2522 2 11 3 1 149.551 73.9401 2 11 -4 -9 44.3415 46.6485 2 11 -4 -8 469.786 112.988 2 11 -4 -7 188.963 81.7769 2 11 4 -7 202.353 84.3302 2 11 -4 -6 53.5243 61.8037 2 11 4 -6 15.5476 57.3526 2 11 -4 -5 527.080 114.320 2 11 4 -5 606.406 126.013 2 11 -4 -4 232.049 90.0056 2 11 4 -4 157.250 79.1561 2 11 -4 -3 380.723 103.497 2 11 4 -3 371.694 104.082 2 11 4 -2-54.7266 66.4497 2 11 -4 -2 15.9586 50.9656 2 11 4 -1 17.2697 56.7508 2 11 -4 -1 25.1908 48.8148 2 11 4 0 514.645 115.797 2 11 4 1 332.854 99.0024 2 11 -5 -9 5.18267 40.1785 2 11 -5 -8 505.883 113.784 2 11 -5 -7 206.397 79.6986 2 11 -5 -6 31.2832 47.9083 2 11 5 -6 78.3153 61.7542 2 11 -5 -5 253.767 89.5080 2 11 5 -5 290.178 98.3126 2 11 -5 -4 507.571 112.965 2 11 5 -4 532.724 118.605 2 11 -5 -3 69.1208 59.4746 2 11 5 -3 65.4246 67.1998 2 11 -5 -2 56.9904 55.8104 2 11 5 -2 105.324 72.4383 2 11 -5 -1 58.9023 59.3136 2 11 5 -1 35.0642 59.3378 2 11 5 0 161.905 78.5353 2 11 -6 -8 78.4555 61.1858 2 11 -6 -7 115.171 70.1376 2 11 -6 -6 22.8515 53.6293 2 11 6 -6 99.0397 70.6475 2 11 6 -5 732.356 139.833 2 11 -6 -5 694.305 132.587 2 11 -6 -4-7.11406 53.8806 2 11 6 -4 7.34946 57.4280 2 11 6 -3 741.366 139.419 2 11 -6 -3 546.345 117.834 2 11 -6 -2 0.12867 47.7401 2 11 6 -2 15.8040 53.8086 2 11 6 -1 226.765 82.3519 2 11 6 0 33.0197 56.8368 2 11 -7 -8 1356.37 178.476 2 11 -7 -7 55.9458 57.8692 2 11 -7 -6 136.812 76.0606 2 11 -7 -5 573.953 120.641 2 11 7 -5 519.642 121.167 2 11 7 -4 949.599 156.679 2 11 -7 -4 1087.99 162.290 2 11 -7 -3 129.015 75.2807 2 11 7 -3-17.9682 62.9683 2 11 -7 -2-25.2029 57.1560 2 11 7 -2 2.95953 58.2852 2 11 7 -1-20.4565 58.3984 2 11 -8 -7 177.239 76.6418 2 11 -8 -6 54.4108 55.7727 2 11 -8 -5 343.563 105.384 2 11 -8 -4 14.5554 60.9879 2 11 8 -4-5.23146 54.4005 2 11 8 -3 555.095 129.527 2 11 -8 -3 698.669 133.614 2 11 8 -2 108.674 69.9941 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 77168 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 1.0000 0.5000 1.0000 0.0174(2) Uani 1 2 d S . P . . N1A N 0.7458(5) 0.53575(15) 0.5964(4) 0.0186(9) Uani 1 1 d D . . . . H1A H 0.740(6) 0.539(2) 0.5106(17) 0.028 Uiso 1 1 d D U . . . C2A C 0.8720(5) 0.52004(18) 0.6975(4) 0.0179(10) Uani 1 1 d . . . . . H2A H 0.9649 0.5081 0.6824 0.021 Uiso 1 1 calc R U . . . N3A N 0.8487(4) 0.52353(16) 0.8208(4) 0.0195(9) Uani 1 1 d . . . . . C4A C 0.7009(5) 0.5419(2) 0.7973(4) 0.0207(10) Uani 1 1 d . . . . . H4A H 0.6527 0.5483 0.8678 0.025 Uiso 1 1 calc R U . . . C5A C 0.6333(5) 0.54968(18) 0.6568(4) 0.0171(10) Uani 1 1 d . . . . . C6A C 0.4788(5) 0.56786(18) 0.5781(4) 0.0185(10) Uani 1 1 d . . . . . C7A C 0.4401(6) 0.58266(19) 0.4375(5) 0.0229(11) Uani 1 1 d . . . . . H7A H 0.5151 0.5802 0.3892 0.028 Uiso 1 1 calc R U . . . C8A C 0.2937(6) 0.6009(2) 0.3680(5) 0.0273(12) Uani 1 1 d . . . . . H8A H 0.2691 0.6105 0.2721 0.033 Uiso 1 1 calc R U . . . C9A C 0.1826(6) 0.6055(2) 0.4355(5) 0.0293(12) Uani 1 1 d . . . . . H9A H 0.0829 0.6188 0.3876 0.035 Uiso 1 1 calc R U . . . C10A C 0.2199(6) 0.5900(2) 0.5762(5) 0.0284(12) Uani 1 1 d . . . . . H10A H 0.1442 0.5923 0.6238 0.034 Uiso 1 1 calc R U . . . C11A C 0.3653(6) 0.5716(2) 0.6458(5) 0.0244(11) Uani 1 1 d . . . . . H11A H 0.3889 0.5612 0.7411 0.029 Uiso 1 1 calc R U . . . N1B N 1.3318(5) 0.61396(17) 1.0015(4) 0.0253(9) Uani 1 1 d D . . . . H1B H 1.412(3) 0.6263(19) 0.985(4) 0.038 Uiso 1 1 d D U . . . C2B C 1.2767(6) 0.5640(2) 0.9937(5) 0.0248(11) Uani 1 1 d . . . . . H2B H 1.3346 0.5327 0.9901 0.030 Uiso 1 1 calc R U . . . N3B N 1.1312(4) 0.56417(16) 0.9917(4) 0.0195(9) Uani 1 1 d . . . . . C4B C 1.0908(6) 0.6171(2) 0.9955(5) 0.0253(11) Uani 1 1 d . . . . . H4B H 0.9917 0.6297 0.9939 0.030 Uiso 1 1 calc R U . . . C5B C 1.2149(6) 0.6485(2) 1.0020(4) 0.0229(11) Uani 1 1 d . . . . . C6B C 1.2398(6) 0.7066(2) 1.0182(5) 0.0282(12) Uani 1 1 d . . . . . C7B C 1.3821(7) 0.7275(2) 1.0918(5) 0.0351(13) Uani 1 1 d . . . . . H7B H 1.4653 0.7041 1.1343 0.042 Uiso 1 1 calc R U . . . C8B C 1.4040(9) 0.7825(2) 1.1038(6) 0.0477(17) Uani 1 1 d . . . . . H8B H 1.5023 0.7965 1.1538 0.057 Uiso 1 1 calc R U . . . C9B C 1.2840(10) 0.8168(3) 1.0438(7) 0.0534(19) Uani 1 1 d . . . . . H9B H 1.2989 0.8544 1.0518 0.064 Uiso 1 1 calc R U . . . C10B C 1.1424(9) 0.7961(3) 0.9722(7) 0.0528(18) Uani 1 1 d . . . . . H10B H 1.0589 0.8195 0.9306 0.063 Uiso 1 1 calc R U . . . C11B C 1.1206(8) 0.7412(2) 0.9602(6) 0.0405(14) Uani 1 1 d . . . . . H11B H 1.0219 0.7274 0.9111 0.049 Uiso 1 1 calc R U . . . Cl Cl 0.75166(13) 0.56940(5) 1.20112(10) 0.0192(3) Uani 1 1 d . . . . . O1 O 0.8659(4) 0.56382(14) 1.1289(3) 0.0288(8) Uani 1 1 d . . . . . O2 O 0.6111(4) 0.54488(16) 1.1206(4) 0.0381(10) Uani 1 1 d . . . . . O3 O 0.7245(5) 0.62435(15) 1.2222(4) 0.0491(11) Uani 1 1 d . . . . . O4 O 0.8078(4) 0.54341(17) 1.3339(3) 0.0403(10) Uani 1 1 d . . . . . O5 O 0.5364(4) 0.66778(15) 0.8771(4) 0.0346(9) Uani 1 1 d . . . . . C12 C 0.6895(7) 0.6889(2) 0.9068(6) 0.0423(15) Uani 1 1 d . . . . . H12A H 0.7428 0.6734 0.8431 0.051 Uiso 1 1 calc R U . . . H12B H 0.7507 0.6811 1.0045 0.051 Uiso 1 1 calc R U . . . C13 C 0.6683(7) 0.7487(2) 0.8836(7) 0.0467(16) Uani 1 1 d . . . . . H13A H 0.6803 0.7674 0.9732 0.056 Uiso 1 1 calc R U . . . H13B H 0.7448 0.7631 0.8407 0.056 Uiso 1 1 calc R U . . . C14 C 0.5069(7) 0.7555(2) 0.7865(6) 0.0394(14) Uani 1 1 d . . . . . H14A H 0.5081 0.7726 0.6978 0.047 Uiso 1 1 calc R U . . . H14B H 0.4437 0.7774 0.8305 0.047 Uiso 1 1 calc R U . . . C15 C 0.4450(7) 0.6986(2) 0.7611(5) 0.0375(14) Uani 1 1 d . . . . . H15A H 0.3349 0.6976 0.7570 0.045 Uiso 1 1 calc R U . . . H15B H 0.4552 0.6846 0.6720 0.045 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.0132(4) 0.0231(5) 0.0141(4) 0.0014(3) 0.0013(3) -0.0010(4) N1A 0.023(2) 0.020(2) 0.0130(18) -0.0003(16) 0.0055(17) -0.0007(18) C2A 0.018(3) 0.017(2) 0.018(2) 0.0013(19) 0.0029(19) 0.000(2) N3A 0.015(2) 0.026(2) 0.0177(19) -0.0007(17) 0.0050(16) -0.0026(18) C4A 0.019(3) 0.027(3) 0.017(2) 0.000(2) 0.0063(19) 0.001(2) C5A 0.017(2) 0.016(2) 0.016(2) -0.0020(19) 0.0020(19) -0.002(2) C6A 0.022(3) 0.012(2) 0.019(2) -0.0048(19) 0.003(2) -0.006(2) C7A 0.026(3) 0.021(3) 0.019(2) 0.003(2) 0.003(2) -0.002(2) C8A 0.032(3) 0.022(3) 0.021(2) 0.006(2) -0.002(2) -0.001(2) C9A 0.022(3) 0.019(3) 0.038(3) 0.004(2) -0.006(2) 0.003(2) C10A 0.020(3) 0.028(3) 0.036(3) -0.005(2) 0.006(2) -0.001(2) C11A 0.024(3) 0.027(3) 0.021(2) -0.001(2) 0.004(2) -0.001(2) N1B 0.022(2) 0.025(2) 0.032(2) 0.0012(19) 0.0117(19) -0.002(2) C2B 0.023(3) 0.024(3) 0.030(3) -0.004(2) 0.011(2) -0.004(2) N3B 0.018(2) 0.023(2) 0.0150(18) -0.0030(16) 0.0022(16) -0.0040(18) C4B 0.023(3) 0.026(3) 0.027(2) 0.006(2) 0.008(2) 0.006(2) C5B 0.026(3) 0.024(3) 0.017(2) 0.008(2) 0.005(2) 0.003(2) C6B 0.037(3) 0.023(3) 0.027(3) 0.007(2) 0.013(2) 0.004(3) C7B 0.043(4) 0.026(3) 0.040(3) 0.000(2) 0.017(3) -0.004(3) C8B 0.069(5) 0.032(3) 0.049(4) -0.004(3) 0.028(3) -0.010(3) C9B 0.088(6) 0.022(3) 0.060(4) 0.002(3) 0.038(4) 0.002(4) C10B 0.070(5) 0.035(4) 0.060(4) 0.013(3) 0.029(4) 0.018(4) C11B 0.048(4) 0.031(3) 0.046(3) 0.012(3) 0.020(3) 0.011(3) Cl 0.0194(6) 0.0216(6) 0.0170(5) -0.0004(5) 0.0061(4) 0.0012(5) O1 0.028(2) 0.040(2) 0.0213(17) -0.0002(15) 0.0128(15) 0.0006(17) O2 0.019(2) 0.049(3) 0.042(2) -0.0154(19) 0.0034(17) -0.0015(19) O3 0.064(3) 0.025(2) 0.068(3) -0.009(2) 0.036(2) 0.002(2) O4 0.031(2) 0.068(3) 0.0244(18) 0.0216(19) 0.0124(16) 0.014(2) O5 0.030(2) 0.033(2) 0.042(2) 0.0058(17) 0.0133(18) -0.0030(18) C12 0.031(3) 0.043(4) 0.052(3) 0.003(3) 0.012(3) -0.006(3) C13 0.040(4) 0.031(3) 0.071(4) 0.002(3) 0.020(3) -0.005(3) C14 0.049(4) 0.032(3) 0.043(3) 0.005(3) 0.022(3) 0.006(3) C15 0.041(4) 0.038(3) 0.035(3) 0.008(3) 0.014(3) 0.003(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0(2) . 3_767 ? N3A Cu N3B 89.11(15) . . ? N3A Cu N3B 90.89(15) 3_767 . ? N3A Cu N3B 90.90(15) . 3_767 ? N3A Cu N3B 89.10(15) 3_767 3_767 ? N3B Cu N3B 180.0 . 3_767 ? C2A N1A C5A 108.7(4) . . ? C2A N1A H1A 125(4) . . ? C5A N1A H1A 126(4) . . ? N3A C2A N1A 110.3(4) . . ? N3A C2A H2A 124.9 . . ? N1A C2A H2A 124.9 . . ? C2A N3A C4A 106.7(4) . . ? C2A N3A Cu 124.3(3) . . ? C4A N3A Cu 128.9(3) . . ? C5A C4A N3A 109.7(4) . . ? C5A C4A H4A 125.2 . . ? N3A C4A H4A 125.2 . . ? C4A C5A N1A 104.6(4) . . ? C4A C5A C6A 131.3(4) . . ? N1A C5A C6A 124.1(4) . . ? C7A C6A C11A 118.3(5) . . ? C7A C6A C5A 122.5(4) . . ? C11A C6A C5A 119.3(4) . . ? C8A C7A C6A 120.6(5) . . ? C8A C7A H7A 119.7 . . ? C6A C7A H7A 119.7 . . ? C9A C8A C7A 121.1(5) . . ? C9A C8A H8A 119.4 . . ? C7A C8A H8A 119.4 . . ? C8A C9A C10A 118.7(5) . . ? C8A C9A H9A 120.7 . . ? C10A C9A H9A 120.7 . . ? C11A C10A C9A 120.4(5) . . ? C11A C10A H10A 119.8 . . ? C9A C10A H10A 119.8 . . ? C10A C11A C6A 120.9(4) . . ? C10A C11A H11A 119.5 . . ? C6A C11A H11A 119.5 . . ? C2B N1B C5B 108.2(4) . . ? C2B N1B H1B 131(4) . . ? C5B N1B H1B 119(3) . . ? N3B C2B N1B 110.7(4) . . ? N3B C2B H2B 124.7 . . ? N1B C2B H2B 124.7 . . ? C2B N3B C4B 106.2(4) . . ? C2B N3B Cu 126.9(3) . . ? C4B N3B Cu 126.7(3) . . ? C5B C4B N3B 109.4(4) . . ? C5B C4B H4B 125.3 . . ? N3B C4B H4B 125.3 . . ? C4B C5B N1B 105.6(4) . . ? C4B C5B C6B 132.3(5) . . ? N1B C5B C6B 122.0(4) . . ? C11B C6B C7B 118.7(5) . . ? C11B C6B C5B 120.0(5) . . ? C7B C6B C5B 121.3(5) . . ? C6B C7B C8B 120.5(6) . . ? C6B C7B H7B 119.8 . . ? C8B C7B H7B 119.8 . . ? C9B C8B C7B 120.3(7) . . ? C9B C8B H8B 119.8 . . ? C7B C8B H8B 119.8 . . ? C10B C9B C8B 119.3(6) . . ? C10B C9B H9B 120.4 . . ? C8B C9B H9B 120.4 . . ? C9B C10B C11B 120.4(6) . . ? C9B C10B H10B 119.8 . . ? C11B C10B H10B 119.8 . . ? C6B C11B C10B 120.9(6) . . ? C6B C11B H11B 119.6 . . ? C10B C11B H11B 119.6 . . ? O3 Cl O2 109.5(3) . . ? O3 Cl O4 109.3(3) . . ? O2 Cl O4 109.8(2) . . ? O3 Cl O1 110.6(2) . . ? O2 Cl O1 109.4(2) . . ? O4 Cl O1 108.3(2) . . ? C12 O5 C15 105.0(4) . . ? O5 C12 C13 105.2(5) . . ? O5 C12 H12A 110.7 . . ? C13 C12 H12A 110.7 . . ? O5 C12 H12B 110.7 . . ? C13 C12 H12B 110.7 . . ? H12A C12 H12B 108.8 . . ? C14 C13 C12 105.4(5) . . ? C14 C13 H13A 110.7 . . ? C12 C13 H13A 110.7 . . ? C14 C13 H13B 110.7 . . ? C12 C13 H13B 110.7 . . ? H13A C13 H13B 108.8 . . ? C13 C14 C15 104.0(5) . . ? C13 C14 H14A 111.0 . . ? C15 C14 H14A 111.0 . . ? C13 C14 H14B 111.0 . . ? C15 C14 H14B 111.0 . . ? H14A C14 H14B 109.0 . . ? O5 C15 C14 105.8(5) . . ? O5 C15 H15A 110.6 . . ? C14 C15 H15A 110.6 . . ? O5 C15 H15B 110.6 . . ? C14 C15 H15B 110.6 . . ? H15A C15 H15B 108.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 1.995(4) . ? Cu N3A 1.995(4) 3_767 ? Cu N3B 2.018(4) . ? Cu N3B 2.018(4) 3_767 ? N1A C2A 1.341(6) . ? N1A C5A 1.381(6) . ? N1A H1A 0.848(10) . ? C2A N3A 1.319(5) . ? C2A H2A 0.9500 . ? N3A C4A 1.372(6) . ? C4A C5A 1.371(6) . ? C4A H4A 0.9500 . ? C5A C6A 1.461(7) . ? C6A C7A 1.396(6) . ? C6A C11A 1.398(7) . ? C7A C8A 1.382(7) . ? C7A H7A 0.9500 . ? C8A C9A 1.379(7) . ? C8A H8A 0.9500 . ? C9A C10A 1.402(7) . ? C9A H9A 0.9500 . ? C10A C11A 1.376(7) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.341(6) . ? N1B C5B 1.372(6) . ? N1B H1B 0.858(10) . ? C2B N3B 1.317(6) . ? C2B H2B 0.9500 . ? N3B C4B 1.379(6) . ? C4B C5B 1.361(7) . ? C4B H4B 0.9500 . ? C5B C6B 1.473(7) . ? C6B C11B 1.372(8) . ? C6B C7B 1.385(8) . ? C7B C8B 1.390(8) . ? C7B H7B 0.9500 . ? C8B C9B 1.377(9) . ? C8B H8B 0.9500 . ? C9B C10B 1.373(10) . ? C9B H9B 0.9500 . ? C10B C11B 1.389(8) . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? Cl O3 1.424(4) . ? Cl O2 1.429(4) . ? Cl O4 1.430(3) . ? Cl O1 1.440(3) . ? O5 C12 1.435(7) . ? O5 C15 1.435(6) . ? C12 C13 1.517(8) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C13 C14 1.507(8) . ? C13 H13A 0.9900 . ? C13 H13B 0.9900 . ? C14 C15 1.523(8) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? _cod_database_fobs_code 2023230