#------------------------------------------------------------------------------ #$Date: 2024-08-02 04:53:16 +0300 (Fri, 02 Aug 2024) $ #$Revision: 293633 $ #$URL: file:///home/coder/svn-repositories/cod/cif/2/02/32/2023233.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023233 loop_ _publ_author_name 'Loukopoulos, Edward' 'Papatriantafyllopoulou, Constantina' 'Moushi, Eleni' 'Kitos, Alexandros A.' 'Tasiopoulos, Anastasios J.' 'Perlepes, Spyros P.' 'Nastopoulos, Vassilios' _publ_section_title ; Solvatomorphism in a series of copper(II) complexes with the 5-phenylimidazole/perchlorate system as ligands ; _journal_coeditor_code AW5090 _journal_issue 4 _journal_name_full 'Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials' _journal_page_first 347 _journal_page_last 359 _journal_paper_doi 10.1107/S2052520624005948 _journal_volume 80 _journal_year 2024 _chemical_formula_moiety 'C36 H32 Cl2 Cu N8 O8, C4 H10 O' _chemical_formula_sum 'C40 H42 Cl2 Cu N8 O9' _chemical_formula_weight 913.25 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 97.084(4) _cell_angle_beta 93.897(4) _cell_angle_gamma 108.096(4) _cell_formula_units_Z 1 _cell_length_a 8.6577(4) _cell_length_b 9.8396(4) _cell_length_c 12.8200(6) _cell_measurement_reflns_used 4469 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.7910 _cell_measurement_theta_min 4.2850 _cell_volume 1023.61(8) _computing_cell_refinement 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.43 (Rigaku OD, 2015)' _computing_molecular_graphics 'PLATON v.270519 (Spek, 2009); MERCURY v.2020.3.0 (Macrae et al., 2020)' _computing_publication_material 'WINGX v.2018.3 (Farrugia, 2012); OLEX2 v.1.3.0 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015); SIR92 (Altomare et al., 1994)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean 10.4223 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.982 _diffrn_measurement_device_type 'Oxford Diffraction SuperNova with Atlas CCD detector' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0228 _diffrn_reflns_av_unetI/netI 0.0300 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.982 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 7915 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.982 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.999 _diffrn_reflns_theta_min 2.921 _diffrn_source 'SuperNova (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.730 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.812 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour blue _exptl_crystal_density_diffrn 1.482 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 473 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.11 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.373 _refine_diff_density_min -0.460 _refine_diff_density_rms 0.058 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 330 _refine_ls_number_reflns 4386 _refine_ls_number_restraints 10 _refine_ls_restrained_S_all 1.050 _refine_ls_R_factor_all 0.0337 _refine_ls_R_factor_gt 0.0311 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0370P)^2^+0.6760P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0803 _refine_ls_wR_factor_ref 0.0830 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4098 _reflns_number_total 4386 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file aw5090sup1.cif _cod_data_source_block 12 _cod_database_code 2023233 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.880 _shelx_estimated_absorpt_t_max 0.937 _shelx_res_file ; 12.res created by SHELXL-2014/7 TITL EL23G in P-1 CELL 0.71073 8.6577 9.8396 12.8200 97.084 93.897 108.096 ZERR 1 0.0004 0.0004 0.0006 0.004 0.004 0.004 LATT 1 SFAC C H N O CL CU UNIT 40 42 8 9 2 1 MERG 2 FMAP 2 OMIT -2 54 SIZE 0.18 0.11 0.09 TEMP -173 ACTA LIST 4 MORE -3 BOND BOND $H HTAB PLAN 10 L.S. 6 WGHT 0.037000 0.676000 FVAR 4.94084 CU 6 0.500000 0.500000 0.000000 10.50000 0.01181 0.01697 = 0.01191 0.00545 0.00048 -0.00014 DFIX 0.86 0.01 N1A H1A N1A 3 0.236060 0.105126 0.076097 11.00000 0.01633 0.01298 = 0.01960 0.00425 0.00466 0.00506 H1A 2 0.232416 0.018392 0.079655 11.00000 -1.50000 C2A 1 0.359485 0.196660 0.036365 11.00000 0.01470 0.01910 = 0.01631 0.00276 0.00223 0.00398 AFIX 43 H2A 2 0.448963 0.172866 0.009511 11.00000 -1.20000 AFIX 0 N3A 3 0.338732 0.324736 0.039944 11.00000 0.01346 0.01643 = 0.01329 0.00418 0.00023 0.00145 C4A 1 0.195005 0.312908 0.083475 11.00000 0.01576 0.01473 = 0.01414 0.00383 0.00161 0.00417 AFIX 43 H4A 2 0.148952 0.388594 0.095778 11.00000 -1.20000 AFIX 0 C5A 1 0.128305 0.176134 0.106392 11.00000 0.01515 0.01372 = 0.01210 0.00251 0.00011 0.00448 C6A 1 -0.021345 0.109909 0.153133 11.00000 0.01452 0.01332 = 0.01218 0.00206 0.00162 0.00247 C7A 1 -0.047306 -0.018646 0.195431 11.00000 0.02183 0.01561 = 0.02392 0.00632 0.00673 0.00780 AFIX 43 H7A 2 0.033232 -0.065802 0.193797 11.00000 -1.20000 AFIX 0 C8A 1 -0.190541 -0.077632 0.239848 11.00000 0.02849 0.01608 = 0.02785 0.00951 0.01029 0.00485 AFIX 43 H8A 2 -0.207660 -0.165553 0.267773 11.00000 -1.20000 AFIX 0 C9A 1 -0.308449 -0.009904 0.243889 11.00000 0.01809 0.02249 = 0.02155 0.00234 0.00745 0.00045 AFIX 43 H9A 2 -0.405766 -0.050466 0.274863 11.00000 -1.20000 AFIX 0 C10A 1 -0.283290 0.117895 0.202269 11.00000 0.01582 0.02285 = 0.02318 0.00235 0.00193 0.00645 AFIX 43 H10A 2 -0.363774 0.165073 0.204983 11.00000 -1.20000 AFIX 0 C11A 1 -0.141933 0.177214 0.156834 11.00000 0.01803 0.01595 = 0.01804 0.00436 0.00035 0.00529 AFIX 43 H11A 2 -0.126616 0.264248 0.127944 11.00000 -1.20000 AFIX 0 DFIX 0.86 0.01 N1B H1B N1B 3 0.131213 0.424492 -0.243055 11.00000 0.01185 0.01982 = 0.01908 0.00218 -0.00055 0.00509 H1B 2 0.029174 0.391404 -0.264073 11.00000 -1.50000 C2B 1 0.191525 0.433589 -0.142548 11.00000 0.01664 0.01752 = 0.01784 0.00466 0.00355 0.00632 AFIX 43 H2B 2 0.126931 0.403986 -0.087314 11.00000 -1.20000 AFIX 0 N3B 3 0.351646 0.488787 -0.130340 11.00000 0.01432 0.01832 = 0.01335 0.00387 0.00238 0.00357 C4B 1 0.395191 0.515983 -0.229640 11.00000 0.01499 0.04407 = 0.01608 0.01192 0.00334 0.00445 AFIX 43 H4B 2 0.503977 0.556729 -0.245722 11.00000 -1.20000 AFIX 0 C5B 1 0.258914 0.475635 -0.300716 11.00000 0.01802 0.03172 = 0.01633 0.00451 0.00184 0.01025 PART 1 AFIX 66 C6B 1 0.227491 0.451756 -0.416686 10.50000 0.02029 0.01901 = 0.01759 0.00556 0.00278 0.01083 C7B 1 0.084075 0.354859 -0.472028 10.50000 0.02200 0.02524 = 0.01600 -0.00094 -0.00208 0.00529 AFIX 43 H7B 2 0.004213 0.295685 -0.435172 10.50000 -1.20000 AFIX 65 C8B 1 0.057508 0.344543 -0.581295 10.50000 0.02985 0.03323 = 0.02136 -0.00175 -0.00472 0.01083 AFIX 43 H8B 2 -0.040511 0.278317 -0.619117 10.50000 -1.20000 AFIX 65 C9B 1 0.174358 0.431123 -0.635221 10.50000 0.03888 0.02456 = 0.01326 0.00261 0.00003 0.01695 AFIX 43 H9B 2 0.156200 0.424072 -0.709900 10.50000 -1.20000 AFIX 65 C10B 1 0.317775 0.528021 -0.579881 10.50000 0.03090 0.03070 = 0.01864 0.00521 0.00451 0.01243 AFIX 43 H10B 2 0.397636 0.587195 -0.616738 10.50000 -1.20000 AFIX 65 C11B 1 0.344343 0.538339 -0.470614 10.50000 0.02202 0.02372 = 0.02009 0.00342 0.00098 0.00811 AFIX 43 H11B 2 0.442362 0.604565 -0.432791 10.50000 -1.20000 AFIX 66 PART 2 C6C 1 0.241866 0.492247 -0.414732 10.50000 0.01775 0.01976 = 0.01262 -0.00013 -0.00365 0.00963 C7C 1 0.135091 0.372567 -0.480928 10.50000 0.02931 0.02587 = 0.02281 0.00585 0.00107 0.00621 AFIX 43 H7C 2 0.073539 0.290903 -0.451927 10.50000 -1.20000 AFIX 65 C8C 1 0.118374 0.372375 -0.589555 10.50000 0.03992 0.03285 = 0.01743 -0.00500 -0.00905 0.00997 AFIX 43 H8C 2 0.045398 0.290579 -0.634797 10.50000 -1.20000 AFIX 65 C9C 1 0.208433 0.491863 -0.631988 10.50000 0.03766 0.02901 = 0.01753 0.00635 0.00493 0.01907 AFIX 43 H9C 2 0.197008 0.491731 -0.706231 10.50000 -1.20000 AFIX 65 C10C 1 0.315209 0.611543 -0.565794 10.50000 0.02960 0.03411 = 0.01969 0.00916 0.00510 0.01374 AFIX 43 H10C 2 0.376760 0.693207 -0.594796 10.50000 -1.20000 AFIX 65 C11C 1 0.331927 0.611737 -0.457166 10.50000 0.02452 0.02390 = 0.01750 0.00469 0.00189 0.00838 AFIX 43 H11C 2 0.404904 0.693533 -0.411926 10.50000 -1.20000 AFIX 0 PART 0 CL 5 0.269879 0.723369 0.126012 11.00000 0.01331 0.01325 = 0.02176 -0.00059 0.00448 0.00314 O1 4 0.399195 0.661306 0.136039 11.00000 0.01778 0.02012 = 0.02808 0.00375 0.00298 0.00866 O2 4 0.212526 0.747793 0.226939 11.00000 0.02809 0.03818 = 0.02516 -0.00533 0.01136 0.00663 O3 4 0.137311 0.627256 0.052180 11.00000 0.01632 0.01920 = 0.02889 -0.00344 -0.00082 0.00342 O4 4 0.331988 0.859564 0.087221 11.00000 0.02174 0.01544 = 0.04633 0.00843 0.00904 0.00657 O5 4 0.500000 0.000000 0.500000 10.50000 0.04744 0.08839 = 0.03946 -0.00208 0.00058 0.03442 SADI 0.01 O5 C12A O5 C12B SADI 0.01 C12A C13A C12B C13B SIMU 0.01 1.0 C13A C13B PART 1 C12A 1 0.605360 -0.065020 0.526860 10.50000 0.05516 0.03107 = 0.03464 0.00312 0.00848 0.01475 AFIX 23 H12A 2 0.591001 -0.148114 0.470809 10.50000 -1.20000 H12B 2 0.574575 -0.105107 0.592427 10.50000 -1.20000 AFIX 0 C13A 1 0.783808 0.020733 0.545088 10.50000 0.03978 0.04952 = 0.03305 -0.00998 -0.00322 0.01450 AFIX 137 H13A 2 0.846976 -0.042533 0.561711 10.50000 -1.50000 H13B 2 0.803104 0.099347 0.604316 10.50000 -1.50000 H13C 2 0.818035 0.061462 0.481157 10.50000 -1.50000 AFIX 0 PART 2 C12B 1 0.656839 0.052993 0.523703 10.50000 0.03393 0.04343 = 0.03134 -0.00439 0.00155 0.00033 AFIX 23 H12C 2 0.680702 0.133920 0.582899 10.50000 -1.20000 H12D 2 0.705539 0.093678 0.462101 10.50000 -1.20000 AFIX 0 C13B 1 0.739004 -0.050917 0.554257 10.50000 0.03285 0.06468 = 0.09575 -0.00891 -0.01247 0.00612 AFIX 137 H13D 2 0.857571 -0.002672 0.566010 10.50000 -1.50000 H13E 2 0.713446 -0.133536 0.497458 10.50000 -1.50000 H13F 2 0.700069 -0.084924 0.619410 10.50000 -1.50000 AFIX 0 HKLF 4 REM EL23G in P-1 REM R1 = 0.0311 for 4098 Fo > 4sig(Fo) and 0.0337 for all 4386 data REM 330 parameters refined using 10 restraints END WGHT 0.0371 0.6659 REM Instructions for potential hydrogen bonds EQIV $1 x, y-1, z HTAB N1A O4_$1 EQIV $2 -x+1, -y+1, -z HTAB C2A O4_$2 HTAB C4A O3 EQIV $3 -x, -y+1, -z HTAB N1B O2_$3 HTAB C2B O3 HTAB C2B O3_$3 EQIV $4 -x+1, -y+1, -z+1 HTAB C13A O2_$4 HTAB C12B O2_$4 REM Highest difference peak 0.373, deepest hole -0.460, 1-sigma level 0.058 Q1 1 0.2303 0.6728 0.2404 11.00000 0.05 0.37 Q2 1 0.3960 0.4926 -0.0627 11.00000 0.05 0.36 Q3 1 0.0541 0.1421 0.1304 11.00000 0.05 0.32 Q4 1 0.1916 0.4401 -0.2790 11.00000 0.05 0.29 Q5 1 0.3307 0.5297 -0.2674 11.00000 0.05 0.29 Q6 1 0.3276 0.4693 -0.2716 11.00000 0.05 0.29 Q7 1 -0.1281 -0.0575 0.2005 11.00000 0.05 0.28 Q8 1 -0.2815 0.0565 0.2221 11.00000 0.05 0.28 Q9 1 0.3811 0.4847 -0.1750 11.00000 0.05 0.27 Q10 1 0.1930 0.6727 0.0763 11.00000 0.05 0.27 ; _shelx_res_checksum 13638 _shelx_hkl_file ; 0 0 2 51032.5 914.219 2 0 0 -3 132774. 2326.71 3 0 0 3 133495. 2324.44 3 0 0 3 137313. 2348.44 2 0 0 4 2234.44 102.405 2 0 0 -4 1804.52 79.0198 3 0 0 4 1960.95 82.9829 3 0 0 -5 120.591 23.7471 3 0 0 5 98.8484 24.2731 3 0 0 5 227.002 37.2811 2 0 0 5 127.517 28.0017 4 0 0 6 9062.35 257.905 4 0 0 6 9862.64 290.742 2 0 0 -6 9376.17 254.613 3 0 0 6 9126.16 253.736 3 0 0 7 12039.8 322.117 3 0 0 7 12268.5 360.528 2 0 0 -7 11916.9 317.773 3 0 0 7 12432.5 336.206 4 0 0 8 40718.8 838.680 3 0 0 -8 39142.9 823.025 3 0 0 8 39652.3 888.020 2 0 0 8 40989.9 848.859 4 0 0 9 21258.2 571.679 2 0 0 -9 19479.6 495.217 3 0 0 9 21177.1 519.712 4 0 0 9 20445.6 513.598 3 0 0 9 21454.5 475.030 1 0 0 10 373.479 59.4783 3 0 0 10 581.818 74.3265 4 0 0 10 422.323 45.4030 1 0 0 10 822.790 102.760 2 0 0 11 7021.24 207.346 1 0 0 11 6747.77 273.269 4 0 0 11 6525.73 311.818 2 0 0 11 6570.29 264.156 3 0 0 12 163.914 50.3197 2 0 0 12 123.519 38.4957 4 0 0 13 4021.07 260.444 2 0 0 13 4224.45 226.144 4 0 0 14 4785.64 299.359 2 0 0 14 4277.24 236.318 4 0 0 15 1671.89 180.516 2 0 0 16 2208.16 221.297 2 0 -1 16 2441.55 242.693 2 0 -1 15 35.8376 35.5080 2 0 -1 15-15.5632 22.2725 4 0 -1 14 416.288 85.7092 2 0 -1 14 524.729 82.4118 4 0 -1 13 76.6824 30.3945 4 0 -1 13 152.766 53.5134 2 0 -1 12 1678.64 135.604 4 0 -1 12 1771.64 163.685 2 0 -1 11 72.7839 32.4644 4 0 -1 11 38.3285 32.3728 2 0 -1 10 14415.4 426.729 4 0 -1 10 14068.1 463.046 2 0 1 -10 13839.7 386.836 3 0 1 -9 33042.4 726.431 3 0 -1 9 34781.0 773.625 4 0 -1 9 34445.1 820.976 2 0 -1 8 8856.20 288.938 4 0 1 -8 8627.63 260.975 3 0 -1 8 8602.37 319.473 2 0 -1 7 12497.5 348.631 4 0 1 -7 11602.0 317.162 3 0 -1 6 11040.4 323.843 2 0 1 -6 9728.00 261.438 3 0 -1 6 10322.1 291.426 4 0 -1 5 7489.94 236.849 2 0 -1 5 6845.35 214.337 4 0 1 -5 6933.98 193.157 3 0 1 -4 9354.34 226.140 3 0 -1 4 9010.19 243.838 4 0 1 -4 8582.44 240.605 4 0 1 -3 28403.6 522.674 1 0 -1 3 28232.0 563.118 4 0 -1 3 29589.9 578.445 2 0 -1 2 72359.1 1284.23 4 0 -1 2 72174.9 1288.87 2 0 1 1 4723.90 107.209 2 0 1 2 4049.95 119.335 3 0 1 2 4171.08 110.951 2 0 1 3 113552. 2018.20 3 0 1 3 117170. 2014.48 2 0 -1 -3 113413. 2020.95 3 0 1 4 794.947 56.5768 3 0 -1 -4 764.507 55.1849 2 0 1 4 945.886 62.9719 2 0 -1 -4 769.624 54.9362 3 0 -1 -5 20168.3 447.759 3 0 1 5 20477.4 450.716 3 0 -1 -5 19480.2 449.520 2 0 1 5 19839.1 456.409 2 0 -1 -6 36287.8 727.541 3 0 -1 -6 32600.3 727.574 2 0 1 6 35954.6 746.167 2 0 1 6 34982.0 723.414 3 0 1 7 124849. 2279.84 2 0 -1 -7 123945. 2245.64 3 0 1 7 121908. 2245.64 3 0 1 8 32115.0 709.220 3 0 1 8 32654.3 747.304 2 0 -1 -8 31948.5 706.831 3 0 1 9 8.35669 19.7825 2 0 1 9 14.1394 20.7221 3 0 1 9 34.3555 21.6937 4 0 1 10 4392.48 203.309 3 0 1 10 3660.52 208.992 2 0 1 10 4021.19 188.923 4 0 1 11 2609.57 157.984 4 0 1 11 2690.64 187.257 2 0 1 11 2533.54 158.160 3 0 1 12 3115.40 218.217 2 0 1 12 3204.14 188.906 3 0 1 12 3011.67 176.842 4 0 1 13 8824.57 395.780 2 0 1 13 8962.19 347.893 3 0 1 13 9204.54 345.741 4 0 1 14 15951.3 508.598 3 0 1 14 15027.8 561.898 2 0 1 15 5558.82 337.104 2 0 1 16 2222.44 218.174 2 0 -2 15 1993.46 210.916 2 0 -2 15 1620.19 156.026 4 0 -2 14 1437.46 142.940 4 0 -2 14 1656.92 182.424 2 0 -2 13 4101.47 272.840 2 0 -2 13 3712.27 223.881 4 0 -2 12 4838.96 245.939 4 0 -2 12 4469.80 273.149 2 0 -2 11 8498.48 363.786 2 0 -2 11 7787.70 314.219 4 0 -2 10 12905.6 448.433 2 0 2 -10 12325.0 356.821 3 0 -2 10 12640.7 402.819 4 0 -2 9 15361.4 439.668 4 0 -2 9 15595.6 480.893 2 0 2 -9 14190.7 384.520 3 0 2 -8 15388.3 389.040 3 0 -2 8 16253.8 473.168 2 0 -2 8 15832.6 435.702 4 0 -2 7 11518.7 357.423 2 0 -2 7 10513.1 322.181 4 0 2 -7 11003.7 313.983 4 0 2 -7 10109.0 282.554 3 0 -2 6 374.872 51.7498 4 0 -2 6 495.017 63.4235 2 0 2 -6 463.705 45.3877 3 0 2 -6 483.894 54.0619 4 0 2 -6 442.597 38.4211 1 0 -2 5 6309.41 209.510 4 0 2 -5 5810.42 158.454 1 0 2 -5 6280.66 204.809 4 0 -2 5 6029.06 217.348 2 0 -2 4 55691.8 1097.45 4 0 -2 4 58620.7 1112.91 2 0 2 -4 57733.7 1091.83 4 0 -2 3 35218.3 703.909 4 0 -2 2 81017.6 1469.59 4 0 -2 1 1361.49 73.6078 4 0 -2 1 1284.04 64.8295 5 0 2 0 101505. 1765.39 6 0 -2 0 99884.4 1805.16 5 0 -2 0 99240.1 1767.39 6 0 2 1 214368. 3626.64 2 0 2 1 211687. 3672.83 3 0 2 2 56778.3 1064.21 3 0 2 2 57949.7 1022.84 2 0 -2 -2 56054.5 1025.42 2 0 2 3 281.667 37.4163 3 0 2 3 309.254 31.4230 2 0 -2 -3 290.207 30.2112 2 0 -2 -4 108606. 1983.15 2 0 2 4 111179. 1985.07 2 0 2 4 112385. 2015.38 3 0 -2 -4 115095. 2022.54 3 0 -2 -5 56714.8 1096.57 2 0 2 5 55734.2 1099.64 2 0 2 5 58576.5 1119.69 3 0 -2 -5 59987.4 1126.57 3 0 2 6 28275.1 629.217 2 0 -2 -6 28830.5 629.832 2 0 -2 -6 30025.6 649.348 3 0 2 6 27535.8 631.134 3 0 2 7 230.977 42.9036 2 0 -2 -7 273.800 45.2090 3 0 2 7 277.677 44.7449 3 0 -2 -7-3.97908 7.95709 2 0 2 8 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586.282 2 0 5 8 3372.66 175.306 2 0 5 8 3011.78 194.651 3 0 5 9 6068.67 294.143 3 0 5 9 6594.52 271.003 2 0 5 10 525.699 85.7843 3 0 5 10 532.255 73.7478 2 0 5 11-22.6817 25.7663 3 0 5 11 12.3161 19.9526 2 0 5 12 308.404 69.5338 3 0 5 12 429.580 72.8103 2 0 5 13 2678.12 212.607 3 0 5 14 7355.75 373.386 3 0 -6 16 39.0498 34.5492 4 0 -6 15 26.0109 35.8083 4 0 -6 14 138.185 62.1736 4 0 -6 13 102.447 57.9722 4 0 -6 12 3731.00 264.340 4 0 -6 11 7764.95 382.173 4 0 -6 10 37167.5 988.745 4 0 -6 9 2771.20 206.098 4 0 -6 8 7818.47 350.705 4 0 6 -7 28.1133 25.7600 5 0 -6 7 95.4612 43.2313 4 0 6 -6 1658.88 131.874 5 0 -6 6 1557.57 143.190 4 0 6 -5 462.063 68.8588 5 0 -6 5 452.087 78.1958 4 0 6 -4 2582.97 160.885 5 0 -6 4 2508.96 176.269 4 0 6 -4 2816.01 159.635 6 0 6 -3 31763.0 760.806 5 0 -6 3 33394.6 814.528 4 0 6 -3 32767.0 735.933 6 0 6 -2 30819.5 688.814 6 0 -6 2 31526.4 776.076 4 0 6 -1 22132.3 593.450 3 0 -6 1 22581.2 609.198 4 0 6 0 26881.8 679.774 3 0 6 1 10115.4 294.658 2 0 6 1 10567.0 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3519.50 5 -1 3 0 197724. 3496.43 3 -1 3 0 202637. 3439.28 2 1 -3 0 197595. 3489.00 6 -1 3 -1 4509.94 150.629 6 -1 3 -1 4114.07 136.735 3 1 -3 1 4240.59 142.238 6 -1 3 -2 32320.4 653.327 2 1 -3 2 33860.1 666.839 2 1 -3 2 35056.0 700.395 4 -1 3 -3 248.657 33.0368 2 1 -3 3 191.957 30.3983 2 1 -3 3 250.777 39.7453 4 1 -3 4 36714.0 765.435 4 1 -3 4 36252.6 762.497 2 -1 3 -4 37616.4 761.249 2 -1 3 -4 36991.0 759.379 4 1 -3 5 9345.46 282.812 4 1 -3 5 9070.70 287.648 2 -1 3 -5 8839.63 267.238 4 -1 3 -6 3660.82 160.001 4 1 -3 6 3468.63 173.672 2 1 -3 6 3371.80 161.431 4 1 -3 7 1865.28 120.217 4 -1 3 -7 1787.64 114.216 4 1 -3 7 1719.50 128.904 2 -1 3 -7 1691.97 85.3300 3 -1 3 -7 1569.77 62.8933 1 1 -3 8 15832.9 478.548 2 1 -3 8 15384.9 439.294 4 -1 3 -8 16508.8 440.828 4 -1 3 -8 16051.1 373.846 3 1 -3 9 8297.16 335.214 2 1 -3 9 8348.89 302.213 4 -1 3 -9 8132.85 239.010 3 -1 3 -10 155.417 30.0212 3 1 -3 10 107.658 39.7446 2 1 -3 10 136.429 39.9477 4 1 -3 11 391.209 65.2885 4 1 -3 11 336.160 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446.878 2 1 -2 8 15480.4 404.463 4 -1 2 -9 2622.49 118.676 3 1 -2 9 2928.09 157.285 4 1 -2 9 3077.52 188.302 2 -1 2 -10 76.6598 22.6042 3 1 -2 10 97.1179 41.9943 2 1 -2 10 149.922 41.5244 4 -1 2 -11 2821.78 136.286 3 1 -2 11 2920.48 172.589 4 1 -2 11 3014.68 213.545 2 1 -2 12 35677.1 948.950 2 1 -2 12 35861.3 852.678 4 1 -2 13 9845.40 436.825 2 1 -2 13 9926.73 367.929 4 1 -2 14 6692.56 368.559 2 1 -2 14 6337.02 293.732 4 1 -2 15 2534.55 232.642 2 1 -2 16 638.218 119.211 2 -1 1 15 106.716 44.2928 2 -1 1 15 82.3381 34.8220 4 -1 1 14 466.543 83.1617 4 -1 1 14 532.835 95.4731 2 -1 1 13 7087.89 318.017 3 -1 1 13 7192.87 313.278 4 -1 1 13 7492.78 357.138 2 -1 1 12 2616.19 176.898 3 -1 1 12 2833.80 162.624 1 -1 1 12 2583.05 191.322 2 -1 1 12 2480.59 174.041 4 -1 1 11 22118.2 605.759 4 -1 1 11 23006.1 617.386 3 -1 1 11 22862.4 646.632 2 -1 1 10 2332.26 147.313 4 -1 1 10 2447.78 157.033 3 -1 1 10 2408.51 163.455 2 -1 1 9 3309.10 181.879 2 -1 1 9 3346.96 174.984 3 -1 1 8 3068.59 158.522 3 -1 1 8 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275.575 2 2 -5 9 1983.43 162.057 2 2 -5 9 2109.38 155.995 4 -2 5 -9 1796.27 96.0859 3 2 -5 10 92.0190 33.6399 4 2 -5 10 128.912 48.4948 2 2 -5 11 7859.48 337.343 4 2 -5 11 7268.91 362.803 2 2 -5 12 21015.7 702.162 2 2 -5 12 20742.7 630.165 4 2 -5 13 12343.2 465.783 4 2 -5 13 12998.3 548.032 2 2 -5 14 1413.06 147.304 4 2 -5 14 1442.43 183.439 2 2 -5 15 217.179 75.4362 2 -2 4 15 8634.65 428.431 3 -2 4 14 11789.3 485.766 3 -2 4 13 4105.43 248.536 2 -2 4 13 3388.01 237.960 3 -2 4 12 2129.27 164.256 2 -2 4 12 1861.28 166.748 3 -2 4 11 5178.20 246.168 2 -2 4 11 4364.38 255.063 3 -2 4 10 5490.91 239.010 2 -2 4 10 4679.18 258.251 3 -2 4 9 276.165 63.0953 3 -2 4 9 196.201 40.5123 2 2 -4 -8 4046.58 171.505 2 -2 4 8 5134.95 195.847 2 -2 4 8 4370.77 230.690 3 -2 4 7 952.681 99.3669 3 2 -4 -7 987.633 70.2796 2 -2 4 7 996.134 74.5327 2 -2 4 6 13976.1 327.273 2 -2 4 6 13141.3 409.682 3 2 -4 -6 12745.9 311.261 2 -2 4 5 23912.3 473.451 2 -2 4 5 24343.1 595.561 3 2 -4 -5 22440.4 463.322 2 2 -4 -4 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52.9692 2 -2 2 -4 17510.6 378.894 4 2 -2 4 17962.9 429.267 2 2 -2 4 17107.3 386.090 4 -2 2 -5 6166.10 181.687 4 2 -2 5 6528.25 232.746 2 2 -2 5 6637.26 193.452 4 -2 2 -6 11313.2 270.085 4 2 -2 6 10516.7 268.788 4 2 -2 6 10511.2 327.397 2 -2 2 -6 8951.37 195.637 3 2 -2 7 9077.85 261.678 4 -2 2 -7 9120.77 256.841 4 2 -2 7 9493.68 321.862 2 -2 2 -7 8469.63 194.532 3 2 -2 8 402.103 48.5184 4 -2 2 -8 346.573 30.3770 3 2 -2 8 490.753 72.6127 2 2 -2 9 4850.48 246.065 2 2 -2 9 4853.67 194.823 4 -2 2 -9 4690.34 145.227 3 -2 2 -10 3252.85 123.304 3 2 -2 10 3460.88 168.414 4 2 -2 10 3384.92 214.743 2 2 -2 11 251.837 46.8844 4 2 -2 11 228.511 58.9443 2 2 -2 12 70.6394 29.4788 4 2 -2 12 111.478 48.8789 2 2 -2 13 2395.72 210.012 2 2 -2 14 4212.84 300.242 2 2 -2 15 4904.62 330.340 2 -2 1 16 104.850 49.2814 4 -2 1 15 143.724 52.9393 4 -2 1 14 269.260 65.5913 4 -2 1 13 607.560 76.9389 1 -2 1 13 487.026 86.0599 4 -2 1 12 259.006 51.8809 1 -2 1 12 188.868 52.7341 3 -2 1 12 148.966 46.7740 4 -2 1 11 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1572.42 2 -2 1 -6 18172.9 378.771 3 2 -1 6 19682.0 408.911 4 2 -1 6 20346.4 383.739 3 2 -1 6 20236.7 505.684 2 -2 1 -7 1773.90 75.3206 3 2 -1 7 1727.53 85.8056 4 2 -1 7 2027.96 79.3262 3 2 -1 7 1756.36 127.366 2 -2 1 -8 469.239 39.9978 3 2 -1 8 369.967 35.9124 3 2 -1 8 300.751 38.5661 4 2 -1 8 416.999 70.4867 2 -2 1 -9 589.565 49.8128 3 2 -1 9 628.588 85.1099 2 2 -1 9 536.043 55.2428 4 2 -1 10 5966.08 213.703 4 -2 1 -10 6005.79 195.472 3 2 -1 10 5990.78 289.586 2 2 -1 11 964.812 81.7178 4 2 -1 11 1021.18 119.947 2 2 -1 12 11988.3 354.658 4 2 -1 12 11221.8 458.713 2 2 -1 13 13088.3 517.415 2 2 -1 14 665.312 114.725 2 2 -1 15 1030.83 152.735 2 -2 0 16 2.18461 33.1068 4 -2 0 15 486.671 92.0038 4 -2 0 14 2075.94 180.029 4 -2 0 13 481.899 81.7454 4 -2 0 12 17238.1 464.036 1 -2 0 12 15667.4 521.880 4 -2 0 11 15217.6 501.169 4 -2 0 11 16724.1 452.176 1 -2 0 10 6180.98 242.482 1 -2 0 10 6387.13 283.064 4 -2 0 9 9657.46 314.011 1 -2 0 9 9314.47 342.261 4 -2 0 8 1778.06 125.626 4 -2 0 8 1751.78 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6173.29 205.713 3 -2 0 -9 5816.22 201.272 3 2 0 10 9423.64 267.146 4 -2 0 -10 8668.69 271.759 3 2 0 10 9593.16 377.397 2 2 0 10 9401.25 277.062 3 2 0 11 8663.59 375.393 2 2 0 11 9725.04 293.512 3 2 0 11 8964.02 274.989 4 2 0 12 8417.02 278.769 3 2 0 12 7563.15 365.538 2 2 0 13 4451.51 282.735 2 2 0 14 359.102 88.8186 2 2 0 15 1941.19 202.108 2 -2 -1 17 494.563 95.5783 4 -2 -1 16 5293.85 315.284 4 -2 -1 15 10361.7 449.238 4 -2 -1 14 4641.46 280.246 4 -2 -1 13 10995.2 443.193 4 -2 -1 12 14524.5 503.526 4 -2 -1 11 18799.2 577.308 4 -2 -1 10 651.430 95.1540 4 -2 -1 9 17041.2 504.385 4 -2 -1 8 11365.7 373.689 4 -2 -1 8 11489.3 330.105 1 -2 -1 7 26779.2 638.076 4 -2 -1 7 25359.8 583.683 1 2 1 -7 25753.0 609.825 3 -2 -1 6 374.890 57.5015 4 2 1 -6 445.360 55.6527 3 -2 -1 6 416.852 49.7272 1 2 1 -5 4018.90 180.766 1 2 1 -5 4076.81 170.724 3 -2 -1 5 4068.13 177.618 4 -2 -1 4 35098.1 751.706 4 2 1 -4 35762.7 750.496 1 -2 -1 3 3098.59 133.671 4 -2 -1 2 979.695 66.9008 4 -2 -1 1 48.1296 17.1743 4 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306.596 35.6534 5 -2 -3 5 332.833 54.2534 4 2 3 -4 19638.8 427.296 5 -2 -3 4 19583.6 511.660 4 -2 -3 3 2866.99 150.348 4 -2 -3 2 46252.6 924.738 4 -2 -3 2 43766.5 855.252 5 -2 -3 1 58226.1 1099.17 5 2 3 -1 57706.2 1125.13 4 -2 -3 1 58476.1 1138.98 4 -2 -3 0 42084.1 843.226 4 2 3 0 41464.8 836.193 4 2 3 1 1456.03 85.9615 4 -2 -3 -1 1372.74 85.3316 4 2 3 1 1320.25 93.8808 2 2 3 2 3725.51 141.930 4 2 3 2 3921.55 168.363 2 -2 -3 -2 4285.60 155.170 4 2 3 3 2682.59 113.041 4 2 3 3 2589.04 137.255 2 2 3 3 2808.52 145.631 3 2 3 4 45555.3 973.918 3 2 3 4 44606.9 896.702 4 2 3 5 36363.8 731.553 4 2 3 5 38680.5 832.198 2 2 3 5 37560.3 814.598 3 2 3 6 6809.80 203.675 4 2 3 6 6986.49 268.080 2 2 3 6 7381.26 267.364 3 2 3 7 9665.83 260.624 4 2 3 7 9507.91 338.617 2 2 3 7 10033.5 335.269 3 2 3 8 53095.5 1024.67 3 2 3 8 49174.4 1043.76 2 2 3 9 2063.92 155.569 2 2 3 9 1530.68 123.628 3 2 3 10 4588.47 254.095 2 2 3 10 4696.72 228.539 3 2 3 11 7241.89 340.687 2 2 3 11 7226.23 303.015 3 2 3 12 1563.61 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334.114 4 2 6 -9 6100.18 264.897 5 2 6 -8 42.6242 27.4444 5 -2 -6 8 83.3279 44.9377 4 -2 -6 7 857.702 116.664 4 2 6 -7 999.015 96.0858 5 2 6 -6 7859.03 289.656 5 -2 -6 6 8028.60 359.043 4 -2 -6 5 30204.4 813.144 4 -2 -6 4 5392.22 273.146 4 -2 -6 3 1655.30 140.914 4 -2 -6 2 13.4355 25.6826 4 2 6 -2 39.5381 19.3820 6 -2 -6 1 19044.6 556.509 4 2 6 -1 19301.0 419.521 6 -2 -6 0 45503.6 1027.04 4 2 6 1 34285.4 795.742 2 2 6 2 12761.8 401.530 2 2 6 2 13190.9 455.926 3 2 6 3 7424.36 328.787 3 2 6 3 7317.74 284.425 2 2 6 4 1331.46 117.328 2 2 6 4 1271.27 129.886 3 2 6 5 969.527 99.6988 2 2 6 5 1039.63 116.916 3 2 6 6 240.622 55.0308 2 2 6 6 227.186 57.0853 3 2 6 7 4249.89 227.594 2 2 6 7 4078.98 246.117 3 2 6 8 20991.8 611.068 2 2 6 8 21111.0 655.434 3 2 6 9 7867.95 341.286 2 2 6 9 8119.73 367.833 3 2 6 10 2167.33 177.949 2 2 6 10 2551.98 201.734 3 2 6 11 1507.35 167.090 2 2 6 11 760.834 122.013 3 2 6 12 7.65031 23.7195 3 -2 -7 13 201.669 74.5772 4 -2 -7 12 407.493 98.9851 4 2 7 -11 767.272 99.3693 5 -2 -7 11 995.472 145.272 4 2 7 -10 13806.8 464.279 5 -2 -7 10 13832.3 572.438 4 2 7 -9 20219.4 590.728 5 -2 -7 9 21534.0 729.033 4 2 7 -8 17098.6 517.485 5 -2 -7 8 18258.6 648.872 4 -2 -7 7 1211.05 148.258 4 2 7 -7 1231.76 112.112 5 -2 -7 6 301.290 69.4863 4 -2 -7 5 2488.93 198.245 4 2 7 -4 1168.19 100.761 6 -2 -7 4 1052.98 126.455 4 2 7 -3 1049.87 88.2828 6 -2 -7 3 972.302 118.918 4 -2 -7 2 25718.7 741.080 4 2 7 -2 27524.6 598.921 6 -2 -7 1 36261.6 913.509 4 -2 -7 0 17974.8 562.297 4 2 7 0 17655.5 526.433 2 2 7 1 3170.12 216.635 3 2 7 1 3051.29 181.790 2 2 7 2 3011.58 212.945 3 2 7 2 2915.51 177.904 2 2 7 3 2340.05 187.796 3 2 7 3 2142.30 150.246 2 2 7 4 742.581 89.1711 2 2 7 4 911.441 117.191 3 2 7 5 1449.14 149.622 3 2 7 5 1386.95 124.011 2 2 7 6 820.245 114.420 3 2 7 6 980.986 107.853 2 2 7 7 8379.35 389.562 3 2 7 7 8646.51 348.876 2 2 7 8 5692.25 282.930 2 2 7 8 5597.91 320.067 3 2 7 9 3310.65 214.809 2 2 7 9 3054.53 232.372 3 2 7 10 45.7273 46.0796 3 2 7 11 822.740 123.564 3 -2 -8 12 1327.39 179.748 4 -2 -8 11 1303.86 176.390 4 -2 -8 10 7410.90 417.747 4 2 8 -9 18102.9 561.464 5 -2 -8 9 17916.9 681.219 4 -2 -8 8 6262.09 367.519 4 -2 -8 7 2879.47 240.399 4 -2 -8 6 6769.60 369.952 4 2 8 -6 6865.17 305.135 6 -2 -8 5 10174.6 461.444 4 2 8 -5 10813.3 377.778 6 2 8 -4 7814.96 291.420 6 -2 -8 4 8122.59 391.243 4 2 8 -3 8272.52 283.344 6 -2 -8 3 8052.06 385.381 4 -2 -8 2 22257.0 694.308 4 -2 -8 1 8862.21 396.391 4 2 8 0 172.594 52.5656 3 2 8 0 238.887 57.1359 2 2 8 1 3724.85 210.962 2 2 8 1 3827.71 254.374 3 2 8 2 2438.59 202.779 3 2 8 2 2266.41 162.732 2 2 8 3 24.9875 27.8817 3 2 8 3 22.0675 18.3233 2 2 8 4 2221.00 195.759 3 2 8 4 2203.03 161.528 2 2 8 5 2297.74 168.189 2 2 8 5 2490.12 213.181 3 2 8 6 5612.16 278.168 2 2 8 6 5774.39 333.026 3 2 8 7 3569.09 260.208 3 2 8 8 73.9639 42.8456 3 2 8 9 6612.10 375.891 3 -2 -9 10 9128.82 494.359 4 -2 -9 9 1672.23 203.155 4 -2 -9 8 318.725 94.2362 4 2 9 -8 218.112 62.5214 6 2 9 -7 37.9917 22.1040 6 -2 -9 7 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41.9124 25.2418 3 -3 7 6 3225.78 215.252 3 -3 7 5 2055.72 166.474 3 -3 7 4 820.074 100.656 3 -3 7 3 1331.86 122.844 3 -3 7 2 9159.32 347.089 3 -3 7 1 14219.3 451.162 3 -3 7 0 225.724 48.2466 3 -3 7 0 194.507 23.0789 2 -3 7 -1 14759.6 484.205 5 -3 7 -1 14904.0 345.936 2 -3 7 -1 15493.0 448.309 3 -3 7 -2 21688.6 555.375 3 -3 7 -2 21472.6 617.168 5 -3 7 -2 19880.4 469.993 2 -3 7 -3 46110.9 994.421 3 -3 7 -3 45984.9 1082.43 5 -3 7 -3 47085.5 950.145 2 -3 7 -4 17348.8 532.231 6 -3 7 -4 16301.8 532.334 5 -3 7 -4 16128.6 449.077 3 -3 7 -4 16085.9 438.075 2 -3 7 -5 6117.56 297.253 6 -3 7 -5 6036.94 231.802 3 -3 7 -5 5838.63 289.693 5 -3 7 -6 39.3167 31.0338 6 -3 7 -6 0.86665 16.9763 3 -3 7 -7 363.705 75.0514 6 -3 7 -7 349.650 50.0805 3 3 -7 7 349.837 72.5284 4 3 -7 7 291.807 62.6532 2 3 -7 8 3787.48 239.731 2 -3 7 -8 3600.53 245.073 6 -3 7 -8 3696.56 167.730 3 3 -7 8 3850.79 242.813 4 -3 7 -9 3897.23 271.408 6 -3 7 -9 3874.48 166.267 3 3 -7 9 3624.19 244.652 2 3 -7 9 3648.52 242.452 4 3 -7 10 19107.6 631.940 4 3 -7 10 19893.1 671.636 2 -3 7 -10 21932.9 724.698 6 3 -7 11 18627.9 636.436 4 -3 7 -11 20332.9 722.949 6 3 -7 11 20832.7 715.332 2 3 -7 12 7743.11 420.066 2 3 -7 12 7289.05 369.033 4 -3 7 -12 7633.56 426.315 6 -3 7 -13 101.412 50.3516 6 3 -7 13 24.3030 33.8043 2 3 -7 13 207.658 65.0277 4 -3 6 13 13.0995 28.8066 3 -3 6 12 259.167 72.2585 3 -3 6 11 3539.57 252.451 3 -3 6 10 4.61334 27.3248 3 -3 6 9 2716.08 207.541 3 -3 6 8 2969.69 211.556 3 -3 6 7 24262.9 694.601 3 -3 6 6 29438.2 772.368 3 -3 6 5 2164.19 159.750 3 -3 6 4 927.138 104.214 3 -3 6 3 4466.90 222.284 3 -3 6 2 8050.28 299.429 3 -3 6 1 273.430 52.0552 3 -3 6 0 1062.54 94.2765 3 -3 6 0 859.321 45.9753 2 -3 6 -1 23978.5 496.462 2 -3 6 -1 25229.2 591.907 3 -3 6 -2 21731.6 486.385 2 -3 6 -2 22873.4 544.613 3 -3 6 -3 2890.07 144.737 3 3 -6 3 2702.77 140.881 2 -3 6 -3 2090.75 116.905 2 -3 6 -4 7309.55 308.084 6 3 -6 4 7274.24 262.080 2 -3 6 -4 7303.46 243.023 3 -3 6 -4 7155.67 247.498 2 -3 6 -5 727.794 92.1940 6 3 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393.590 3 -3 5 7 528.798 79.0836 3 3 -5 -7 507.755 43.0914 2 -3 5 6 732.019 93.2106 3 3 -5 -6 768.791 43.9722 2 -3 5 5 2489.51 161.849 3 -3 5 4 43184.0 959.331 3 -3 5 3 56508.2 1174.73 3 -3 5 2 10320.6 328.390 3 -3 5 1 20963.6 516.553 3 3 -5 0 24.6482 15.2382 6 -3 5 0 48.9499 23.4710 3 -3 5 0 49.9294 10.4621 2 3 -5 1 24073.6 540.280 3 3 -5 1 25086.8 587.491 6 -3 5 -1 24910.3 541.544 3 -3 5 -1 23205.1 473.879 2 3 -5 2 3303.32 137.414 2 -3 5 -2 2835.59 120.977 2 -3 5 -2 3008.11 163.128 4 -3 5 -2 2835.36 132.506 3 -3 5 -3 443.395 59.7436 4 3 -5 3 451.872 53.1352 2 -3 5 -3 472.540 49.7591 2 -3 5 -3 429.517 46.5058 3 -3 5 -4 163.546 32.0806 2 -3 5 -4 142.221 25.3450 3 -3 5 -4 180.386 38.3726 4 3 -5 4 122.846 29.7703 2 3 -5 5 14694.1 421.184 2 -3 5 -5 14747.5 344.208 3 -3 5 -6 817.432 54.1511 3 3 -5 6 720.542 84.2919 4 3 -5 6 797.167 85.8727 2 -3 5 -6 758.385 94.4087 6 -3 5 -7 1825.49 80.8059 3 3 -5 7 1981.14 142.989 4 3 -5 7 1792.15 139.046 2 -3 5 -7 2055.65 163.196 6 -3 5 -8 1705.07 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188.995 4 7 1 3 7291.10 344.469 2 7 1 4 9068.84 394.004 2 7 1 5 23145.8 712.434 2 7 1 6 6223.07 340.399 2 7 1 7 2133.69 196.322 2 7 1 8 1179.59 146.983 2 7 1 9 2870.71 241.695 2 -7 -2 12 496.676 107.859 4 -7 -2 11 74.6844 31.4212 4 -7 -2 10 33.0915 28.9833 4 -7 -2 9 2875.83 239.312 4 -7 -2 8 7354.00 382.123 4 -7 -2 7 19102.7 645.856 4 -7 -2 6 17356.1 591.615 4 -7 -2 5 6450.58 320.457 4 -7 -2 4 1534.11 142.839 4 -7 -2 3 1394.87 129.016 4 7 2 -3 1180.81 136.619 2 -7 -2 2 13.6803 21.0542 4 7 2 -2 40.7982 30.2474 2 -7 -2 1 11159.6 373.081 4 7 2 -1 9872.61 412.341 2 -7 -2 0 1292.50 108.647 4 7 2 0 1232.28 136.382 2 -7 -2 -1 6861.40 252.830 4 7 2 1 6677.94 334.921 2 -7 -2 -2 10890.3 319.466 4 7 2 2 11417.2 445.756 2 7 2 3 1942.87 177.288 2 7 2 4 460.076 86.0963 2 7 2 5 894.243 123.918 2 7 2 6 1346.77 158.682 2 7 2 7 4394.55 290.067 2 7 2 8 6282.06 362.045 2 7 2 9 6639.12 380.874 2 -7 -3 11 1289.04 170.070 4 -7 -3 10 938.482 140.643 4 -7 -3 9 8006.97 411.595 4 -7 -3 8 12458.6 513.467 4 -7 -3 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476.549 2 8 -3 6 1469.23 156.566 2 8 -3 7 971.714 128.260 2 8 -3 8 73.7030 39.0929 2 8 -3 9 2203.01 213.642 2 8 -3 10 2066.25 212.224 2 -8 2 13 2427.91 229.962 1 -8 2 12 1902.17 202.056 1 -8 2 11 119.246 55.8482 4 -8 2 11 37.3976 45.8900 1 -8 2 10 3279.82 261.134 1 -8 2 10 3481.09 257.185 4 -8 2 9 368.619 84.6908 4 -8 2 9 355.902 86.3577 1 -8 2 8 4079.63 283.576 1 -8 2 7 6392.53 354.425 1 -8 2 6 4081.98 274.715 1 8 -2 -6 4625.60 257.834 2 8 -2 -5 386.998 72.5138 2 -8 2 5 489.232 89.0787 1 -8 2 4 1373.65 152.784 1 8 -2 -4 1422.93 131.710 2 8 -2 -3 1740.42 145.941 2 -8 2 3 1871.39 172.134 1 -8 2 2 95.3422 23.9229 5 8 -2 -2 137.276 49.6741 2 -8 2 2 70.0633 39.2942 1 -8 2 1 3975.48 177.119 5 8 -2 -1 4074.86 230.153 2 -8 2 1 4061.42 244.826 1 8 -2 0 3968.18 230.589 2 8 -2 1 21956.0 639.728 2 8 -2 2 38571.1 959.060 2 8 -2 3 16747.0 559.619 2 -8 2 -3 17295.5 423.828 4 8 -2 4 9751.61 413.342 2 8 -2 5 214.954 61.7360 2 8 -2 6 494.464 93.7648 2 8 -2 7-26.4054 43.4131 2 8 -2 8 21.0598 35.8007 2 8 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334.390 2 -8 0 4 118.572 48.0942 4 8 0 -4 83.3799 28.1468 2 -8 0 3 9583.82 384.141 4 8 0 -3 11879.2 443.583 2 -8 0 2 8298.14 328.693 4 8 0 -2 7552.58 348.868 2 -8 0 1 6780.94 282.656 4 8 0 -1 5761.86 303.591 2 8 0 0 15636.6 546.782 2 -8 0 0 16465.0 471.999 4 8 0 1 14275.9 521.454 2 -8 0 -1 16217.4 440.342 4 8 0 2 3463.01 234.861 2 8 0 3 726.051 107.768 2 8 0 4 1196.40 143.601 2 8 0 5 5571.27 326.314 2 8 0 6 26288.9 812.814 2 8 0 7 12942.2 536.976 2 8 0 8 2716.19 235.806 2 -8 -1 11 6691.21 400.389 4 -8 -1 10 6195.15 375.263 4 -8 -1 9 9058.48 449.090 4 -8 -1 8 1754.20 181.692 4 -8 -1 7 256.510 69.4423 4 -8 -1 6 3879.54 257.839 4 -8 -1 5 3157.53 221.268 4 -8 -1 4 23308.9 691.347 4 8 1 -4 23944.8 730.947 2 -8 -1 3 29235.9 774.132 4 8 1 -3 28195.8 814.593 2 -8 -1 2 1535.99 136.055 4 8 1 -2 1713.37 163.806 2 -8 -1 1 782.889 91.6080 4 8 1 -1 737.817 108.374 2 8 1 0 6.16489 31.5643 2 -8 -1 0 4.45917 18.1135 4 8 1 1 3803.24 249.552 2 8 1 2 6477.57 341.256 2 8 1 3 910.619 125.601 2 8 1 4 25583.7 790.406 2 8 1 5 11338.5 487.573 2 8 1 6 1580.41 178.321 2 8 1 7 70.2173 40.9042 2 -8 -2 10 1672.88 191.162 4 -8 -2 9 491.421 100.664 4 -8 -2 8 171.018 64.4927 4 -8 -2 7 563.111 98.6705 4 -8 -2 6 8935.64 410.331 4 -8 -2 5 23191.8 707.441 4 -8 -2 4 24332.9 712.558 4 8 2 -4 25488.5 782.847 2 -8 -2 3 12517.6 459.271 4 8 2 -3 14558.8 539.596 2 -8 -2 2 2846.50 189.039 4 8 2 -2 2476.89 206.726 2 -8 -2 1 634.083 84.3824 4 8 2 -1 654.767 107.157 2 8 2 0 83.7635 42.6205 2 -8 -2 0 18.8666 17.1566 4 8 2 1 1084.10 137.721 2 8 2 2-13.6694 35.3475 2 8 2 3 1439.14 161.536 2 8 2 4 3838.38 269.754 2 8 2 5 171.998 60.4734 2 8 2 6 75.8811 51.5078 2 -8 -3 9 2194.26 220.321 4 -8 -3 8 4468.08 304.911 4 -8 -3 7 11233.1 490.616 4 -8 -3 6 8100.35 397.179 4 -8 -3 5 3162.58 232.284 4 -8 -3 4 2784.42 210.873 4 8 3 -4 2709.11 230.131 2 -8 -3 3 78.0424 46.8971 4 8 3 -3 106.760 47.0539 2 -8 -3 2 748.387 99.7889 4 8 3 -2 741.099 117.455 2 -8 -3 1-12.6936 20.3177 4 8 3 -1-6.59544 35.5574 2 8 3 0 13671.5 545.773 2 8 3 1 14707.8 571.094 2 8 3 2 17253.7 631.083 2 8 3 3 5337.33 330.112 2 8 3 4 410.852 92.3458 2 8 3 5 1521.74 174.675 2 -8 -4 9 6587.56 401.545 4 -8 -4 8 4858.26 333.300 4 -8 -4 7 4467.27 312.017 4 -8 -4 6 380.601 86.5370 4 -8 -4 5 499.529 98.3103 4 8 4 -5 769.997 133.776 2 -8 -4 4 253.250 68.3720 4 8 4 -4 398.751 94.1568 2 -8 -4 3 128.432 45.2578 4 8 4 -3 298.860 83.7055 2 -8 -4 2 3106.44 215.810 4 8 4 -2 3558.24 263.990 2 8 4 -1 7863.05 409.416 2 8 4 0 9031.54 443.161 2 8 4 1 4042.14 287.226 2 8 4 2 2341.10 216.584 2 8 4 3 1323.58 166.088 2 -8 -5 7 110.772 47.1502 4 -8 -5 6-25.8288 38.7698 4 -8 -5 5 40.3623 37.2960 4 -8 -5 4 2807.30 227.474 4 -8 -5 3 2066.41 188.997 4 8 5 -3 1945.02 202.570 2 8 5 -2 2778.55 241.766 2 8 5 -1 1869.02 199.767 2 -8 -6 6 637.207 121.341 4 -8 -6 5 1042.99 150.124 4 -9 11 2 3935.34 282.758 3 -9 10 4 88.4943 46.0598 3 -9 10 3 752.374 124.781 3 -9 10 2 58.2178 40.3573 3 -9 10 1 388.547 81.8373 3 -9 10 -1 983.680 151.840 5 -9 10 -2 2051.59 220.928 5 -9 10 -3 1707.79 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5 -4 2310.19 180.223 1 9 -5 4 2236.97 181.862 2 9 -5 5 445.046 85.9161 2 9 -5 6-23.6335 30.5208 2 9 -5 7 1468.31 166.582 2 9 -5 8-22.9450 42.9287 2 -9 4 9 2897.73 264.124 1 -9 4 8 6051.58 381.526 1 -9 4 7 798.093 136.481 1 9 -4 -6 67.0042 30.3395 2 -9 4 6 82.0120 48.3915 1 -9 4 5 344.355 87.0798 1 9 -4 -5 526.013 79.9760 2 9 -4 -4 4254.82 228.483 2 -9 4 4 4194.92 294.311 1 9 -4 -3 7411.63 313.368 2 -9 4 3 6584.44 370.449 1 -9 4 2 10402.3 350.990 5 9 -4 -2 10046.4 379.321 2 -9 4 2 9976.22 451.639 1 -9 4 1 25499.8 656.489 5 9 -4 -1 23240.6 658.434 2 -9 4 1 24276.8 757.653 1 -9 4 0 23580.4 633.134 5 -9 4 0 21286.1 693.119 1 9 -4 0 21760.2 639.125 2 -9 4 -1 2821.05 212.525 1 9 -4 1 2863.47 201.172 2 9 -4 2 460.778 80.5547 2 -9 4 -2 444.526 81.4139 1 9 -4 3-20.3897 34.0665 2 9 -4 4 182.106 54.7901 2 9 -4 5 709.311 110.927 2 9 -4 6 1137.39 140.836 2 9 -4 7 1134.69 147.132 2 9 -4 8 2337.42 215.420 2 -9 3 10 9418.40 485.518 1 -9 3 9 10807.4 517.735 1 -9 3 8 1224.23 165.091 1 9 -3 -8 1524.46 147.927 2 -9 3 7 84.3155 48.3611 1 9 -3 -7 40.5384 30.0426 2 -9 3 6 955.617 141.323 1 9 -3 -6 1048.62 117.202 2 -9 3 5 865.066 132.393 1 9 -3 -5 768.101 99.3300 2 -9 3 4 6545.11 365.169 1 9 -3 -4 6678.85 308.570 2 -9 3 3 15628.0 583.177 1 9 -3 -3 15411.8 512.017 2 9 -3 -2 2498.23 182.664 2 -9 3 2 2798.24 221.378 1 9 -3 -1 6049.42 297.343 2 -9 3 1 6379.28 336.192 1 -9 3 0 487.669 72.7524 5 9 -3 0 469.975 81.3569 2 -9 3 0 255.388 68.3638 1 9 -3 1 1960.82 168.631 2 9 -3 2 112.688 47.5311 2 9 -3 3 2373.48 194.753 2 9 -3 4 13824.4 522.974 2 9 -3 5 7424.37 376.226 2 9 -3 6 4069.28 280.076 2 9 -3 7 1451.31 164.740 2 9 -3 8 469.209 99.2803 2 -9 2 10 2196.29 218.140 4 -9 2 10 2262.52 224.906 1 -9 2 9-11.7486 30.3610 4 -9 2 9 38.0484 27.5574 1 -9 2 8 1755.18 181.307 4 -9 2 8 1906.48 201.719 1 -9 2 7 69.3848 44.0084 4 9 -2 -7 12.1048 26.2835 2 -9 2 7 65.4826 48.3969 1 9 -2 -6 2929.93 212.138 2 -9 2 6 3382.73 260.422 1 9 -2 -5 11559.6 443.769 2 -9 2 5 12013.7 507.247 1 9 -2 -4 26415.2 753.517 2 -9 2 4 26986.2 821.843 1 9 -2 -3 6886.08 328.008 2 9 -2 -2 3272.99 220.943 2 9 -2 -1 23.7272 24.3061 2 9 -2 0 214.349 57.7583 2 -9 2 0 323.620 61.2327 4 9 -2 1 13.1517 23.6946 2 -9 2 -1-10.1424 18.0869 4 9 -2 2 147.591 55.2543 2 9 -2 3 2131.27 191.702 2 9 -2 4 14452.1 553.247 2 9 -2 5 11565.7 491.014 2 9 -2 6 4187.12 288.873 2 9 -2 7 980.109 141.400 2 -9 1 10 785.292 135.369 4 -9 1 9 100.298 58.4786 4 -9 1 8 232.452 76.2411 4 -9 1 7 65.8802 47.1038 4 9 -1 -7 8.51406 28.5895 2 -9 1 6 4647.92 289.475 4 9 -1 -6 3604.39 247.978 2 -9 1 5 10916.6 461.596 4 9 -1 -5 13083.3 487.846 2 -9 1 4 2362.40 191.591 4 9 -1 -4 2620.07 201.263 2 9 -1 -3 505.831 89.6255 2 -9 1 3 578.015 94.2505 4 9 -1 -2 2039.06 181.776 2 -9 1 2 2156.14 168.997 4 9 -1 -1 6393.84 331.403 2 -9 1 1 6929.07 301.685 4 9 -1 0 1014.45 127.432 2 -9 1 0 1074.51 105.670 4 9 -1 1 2832.47 217.246 2 9 -1 2 14307.0 532.750 2 9 -1 3 20240.9 676.915 2 9 -1 4 4786.65 304.874 2 9 -1 5 2156.07 203.147 2 9 -1 6 393.822 86.6118 2 9 -1 7 2352.56 220.457 2 -9 0 9 919.092 136.985 4 -9 0 8 8765.68 437.475 4 -9 0 7 8178.32 404.800 4 -9 0 6 4666.27 289.871 4 9 0 -6 5344.74 316.965 2 -9 0 5-32.5075 25.9547 4 9 0 -5-21.0552 34.0635 2 -9 0 4 1149.88 131.033 4 9 0 -4 1212.39 143.010 2 -9 0 3 602.761 93.8043 4 9 0 -3 569.320 98.9048 2 -9 0 2 1522.09 141.438 4 9 0 -2 1471.45 157.214 2 9 0 -1 5838.51 327.787 2 -9 0 1 5643.45 270.462 4 9 0 0 3366.95 240.158 2 9 0 1 2967.65 231.022 2 9 0 2 562.746 100.831 2 9 0 3 296.653 78.8480 2 9 0 4 1801.75 183.740 2 9 0 5 5334.18 336.550 2 9 0 6 10439.4 489.577 2 -9 -1 9 5710.05 364.337 4 -9 -1 8 5477.79 343.620 4 -9 -1 7 190.812 61.8737 4 -9 -1 6 287.014 71.0219 4 9 1 -6 383.212 91.0299 2 -9 -1 5 263.765 63.7174 4 9 1 -5 236.548 64.9281 2 -9 -1 4 129.393 48.9793 4 9 1 -4 265.325 71.8405 2 -9 -1 3 4633.42 268.137 4 9 1 -3 5037.69 306.845 2 -9 -1 2 5483.97 276.755 4 9 1 -2 6058.33 339.734 2 9 1 -1 22712.3 741.425 2 9 1 0 3812.69 268.643 2 9 1 1 862.364 125.627 2 9 1 2-81.3446 56.1357 2 9 1 3 382.152 86.1289 2 9 1 4 1335.10 164.751 2 -9 -2 8 55.0127 40.4277 4 -9 -2 7 506.552 97.2937 4 -9 -2 6 258.358 76.8936 4 9 2 -6 337.589 84.1309 2 -9 -2 5 726.860 114.040 4 9 2 -5 1005.48 143.595 2 -9 -2 4 9888.49 431.887 4 9 2 -4 12120.8 511.828 2 -9 -2 3 23047.7 694.898 4 9 2 -3 23704.4 771.003 2 9 2 -2 10045.9 466.432 2 9 2 -1 9839.04 462.182 2 9 2 0 788.205 130.433 2 9 2 1 1589.68 175.820 2 9 2 2 1340.89 165.735 2 9 2 3 1537.05 175.703 2 -9 -3 8 2154.97 219.159 4 -9 -3 7 1607.77 187.746 4 -9 -3 6 4819.30 314.571 4 -9 -3 5 10142.6 468.069 4 9 3 -5 12070.0 540.710 2 -9 -3 4 12874.5 520.888 4 9 3 -4 14044.4 580.354 2 9 3 -3 2720.63 237.515 2 9 3 -2-26.7849 34.9904 2 9 3 -1 429.380 99.0917 2 9 3 0 34.6176 41.7256 2 -9 -4 7 8145.20 445.843 4 -9 -4 6 6656.76 388.216 4 -9 -4 5 2548.74 223.784 4 -10 10 -1 286.984 86.8823 5 -10 9 4 6041.66 361.558 3 -10 9 3 2846.88 234.058 3 -10 9 2 356.695 81.2794 3 -10 9 0 141.223 73.0457 1 -10 9 -1 9.56148 33.9095 5 -10 9 -1-63.6306 49.7989 1 -10 9 -2 3488.54 304.102 1 -10 9 -3 7949.83 449.410 1 -10 9 -3 9345.42 488.684 5 -10 9 -4 4283.87 329.397 5 -10 8 3 421.061 113.407 1 -10 8 2 2063.71 244.060 1 -10 8 1 1317.56 188.354 1 -10 8 0 4514.53 297.735 5 -10 8 0 4510.46 344.186 1 -10 8 -1 1094.76 149.030 5 -10 8 -1 952.646 152.867 1 -10 8 -2 1894.92 201.703 5 -10 8 -2 1592.65 189.649 1 -10 8 -3 790.871 127.697 1 -10 8 -3 1051.51 150.473 5 -10 8 -4 1554.02 191.242 5 -10 8 -5 69.3069 40.0413 5 -10 7 4 425.264 111.479 1 -10 7 3 50.7150 53.0693 1 -10 7 2 232.924 81.4272 1 -10 7 1 6768.35 342.884 5 -10 7 1 6711.34 410.394 1 -10 7 0 1863.43 178.775 5 -10 7 0 1549.28 188.816 1 -10 7 -1 63.4628 40.4642 5 -10 7 -1 64.4952 46.8675 1 -10 7 -2-41.7250 34.9267 5 -10 7 -2 49.5842 32.7121 1 -10 7 -3 675.980 116.029 5 -10 7 -3 762.836 117.751 1 -10 7 -4 178.192 64.6924 5 10 -7 5 499.779 95.5990 2 10 -7 6 1916.98 194.421 2 10 -7 7 4501.74 307.086 2 -10 6 5 442.778 108.786 1 -10 6 4 3479.46 294.614 1 -10 6 3 9424.26 494.947 1 -10 6 2 3954.62 302.837 1 -10 6 1 2920.99 252.490 1 -10 6 0 827.610 114.450 5 -10 6 0 618.954 111.762 1 -10 6 -1 2640.12 208.871 5 -10 6 -1 2852.86 233.497 1 10 -6 1 2819.75 199.628 2 -10 6 -2 30.0017 26.9277 1 -10 6 -2 112.067 50.6184 5 10 -6 2 108.257 39.7438 2 10 -6 3 455.310 87.5240 2 -10 6 -3 442.407 91.8054 5 -10 6 -3 489.641 91.9791 1 10 -6 4 942.176 124.956 2 -10 6 -4 984.207 122.977 1 10 -6 5 728.314 113.899 2 10 -6 6 4453.22 301.626 2 10 -6 7 1109.15 153.236 2 -10 5 6 7815.84 449.799 1 -10 5 5 15121.0 642.221 1 -10 5 4 8288.24 447.951 1 -10 5 3 355.984 90.8888 1 -10 5 2 84.9651 52.1723 1 10 -5 -2 61.3412 32.3417 2 10 -5 -1 1926.32 165.000 2 -10 5 1 2090.85 206.390 1 -10 5 0 333.877 79.6982 1 10 -5 0 347.600 74.4298 2 -10 5 -1 32.9828 31.0368 5 10 -5 1-2.48072 22.7039 2 -10 5 -1 17.6843 25.0670 1 -10 5 -2 1319.32 144.208 5 -10 5 -2 1177.98 144.780 1 10 -5 2 1460.46 151.229 2 10 -5 3 7964.77 378.703 2 10 -5 4 5996.17 331.406 2 10 -5 5 2919.91 231.035 2 10 -5 6 231.041 71.7322 2 10 -5 7 1009.27 148.364 2 -10 4 6 2948.04 264.356 1 -10 4 5 2969.38 259.379 1 -10 4 4 938.448 142.347 1 10 -4 -4 1227.39 129.297 2 10 -4 -3 318.802 69.3886 2 -10 4 3 409.039 98.2866 1 10 -4 -2 177.798 53.7051 2 -10 4 2 137.135 60.3056 1 10 -4 -1 1980.17 169.950 2 -10 4 1 2038.60 198.595 1 10 -4 0 3184.85 222.209 2 -10 4 0 3305.88 245.377 1 10 -4 1 9078.14 405.325 2 10 -4 2 19265.9 642.838 2 10 -4 3 17917.4 622.548 2 10 -4 4 3216.35 243.348 2 10 -4 5 322.231 80.8267 2 10 -4 6 261.858 64.8608 2 -10 3 8 254.079 78.6152 4 -10 3 7 1518.39 185.765 1 10 -3 -6 4704.91 277.302 2 -10 3 6 4729.27 329.019 1 10 -3 -5 1026.79 129.510 2 -10 3 5 1211.00 162.129 1 10 -3 -4 14.4353 29.5985 2 -10 3 4-12.3668 45.0699 1 10 -3 -3 24.6941 29.2661 2 -10 3 3-3.57033 38.4790 1 10 -3 -2 6287.05 324.047 2 10 -3 -1 8867.71 395.372 2 10 -3 0 2389.43 196.844 2 10 -3 1 427.030 84.2855 2 10 -3 2 926.062 126.537 2 10 -3 3 1475.14 166.881 2 10 -3 4 31.7929 29.8710 2 10 -3 5 2076.81 205.601 2 10 -3 6 3512.74 274.987 2 -10 2 8 1795.41 194.114 4 10 -2 -8 2119.93 193.284 2 -10 2 7 144.642 58.8704 4 10 -2 -7 214.144 66.0449 2 -10 2 6 46.7495 34.8762 4 10 -2 -6 63.2863 39.9811 2 10 -2 -5 584.592 101.150 2 -10 2 5 555.266 96.6871 4 10 -2 -4 8433.67 396.001 2 -10 2 4 8209.23 379.802 4 10 -2 -3 8149.40 386.816 2 -10 2 3 7853.58 360.244 4 10 -2 -2 11652.7 472.016 2 -10 2 2 11650.5 439.280 4 10 -2 -1 5733.01 323.340 2 -10 2 1 5785.88 284.834 4 10 -2 0 1492.01 161.996 2 10 -2 1 302.728 73.0527 2 10 -2 2 125.893 46.2036 2 10 -2 3 610.656 109.361 2 10 -2 4 303.351 79.7003 2 10 -2 5 4238.08 300.693 2 10 -1 -9 87.6224 48.7864 2 -10 1 8-41.3525 43.5774 4 10 -1 -8-45.7270 41.5766 2 -10 1 7 212.531 71.2318 4 10 -1 -7 234.883 68.6042 2 -10 1 6 1479.78 166.681 4 10 -1 -6 1345.09 158.353 2 -10 1 5 2728.72 222.935 4 10 -1 -5 2946.52 232.925 2 -10 1 4 3296.04 240.374 4 10 -1 -4 4361.36 284.737 2 10 -1 -3 2090.85 196.101 2 -10 1 3 2205.09 182.289 4 10 -1 -2 1964.08 190.572 2 -10 1 2 2174.56 174.280 4 10 -1 -1 291.516 74.7425 2 10 -1 0 41.9407 26.8229 2 10 -1 1 2008.44 195.625 2 10 -1 2 2638.30 225.454 2 10 -1 3 3201.58 254.318 2 10 -1 4 1601.29 185.963 2 -10 0 8 1241.96 169.976 4 10 0 -8 1392.57 174.013 2 -10 0 7 1486.98 177.085 4 10 0 -7 1440.94 172.816 2 -10 0 6 4746.83 315.547 4 10 0 -6 5067.21 322.531 2 -10 0 5 12609.6 519.554 4 10 0 -5 12377.3 524.457 2 -10 0 4 8633.13 406.096 4 10 0 -4 8895.80 437.820 2 10 0 -3 244.653 72.1682 2 -10 0 3 332.614 71.0786 4 10 0 -2 288.746 80.3790 2 10 0 -1 36.9199 28.3115 2 10 0 0 113.728 51.0319 2 10 0 1 922.710 136.378 2 10 0 2 306.916 83.1469 2 -10 -1 7 8519.93 448.509 4 -10 -1 6 2483.15 222.187 4 10 1 -6 2667.61 241.235 2 -10 -1 5 257.687 67.1367 4 10 1 -5 272.928 76.8218 2 -10 -1 4 1069.93 132.932 4 10 1 -4 930.526 139.407 2 10 1 -3 178.446 67.9007 2 10 1 -2 992.319 149.145 2 10 1 -1 6857.23 389.910 2 10 1 0 2950.54 250.914 2 -10 -2 7 4490.14 315.809 4 -10 -2 6 217.860 63.8748 4 -10 -2 5 149.436 57.9954 4 -11 8 -1 17.9654 38.1197 1 -11 8 -2 4380.01 315.430 1 -11 7 0 2954.64 262.195 1 -11 7 -1 7579.45 420.402 1 -11 7 -2 3069.69 255.629 1 -11 6 1 3176.23 269.773 1 -11 6 0 4613.83 321.747 1 -11 6 -1 2881.00 248.052 1 -11 6 -2 247.776 70.7070 1 11 -6 4 1656.25 177.432 2 -11 5 2 19575.8 730.862 1 -11 5 1 1977.15 207.618 1 -11 5 0 757.941 121.551 1 11 -5 1 109.960 48.8715 2 11 -5 2 26.7377 23.6438 2 11 -5 3 1374.03 163.112 2 11 -5 4 1270.81 157.447 2 11 -4 -2 65.7720 36.2560 2 11 -4 -1 1024.34 134.307 2 11 -4 0 45.9352 34.0657 2 11 -4 1 641.108 110.873 2 11 -4 2 197.528 63.6717 2 11 -4 3 1905.95 195.350 2 -11 3 6 776.215 123.541 4 -11 3 5 1427.66 162.653 4 11 -3 -4 844.230 120.101 2 -11 3 4 917.865 126.377 4 11 -3 -3 4.97253 28.5000 2 -11 3 3 17.4638 28.6573 4 11 -3 -2 821.120 123.283 2 11 -3 -1-1.92349 24.9375 2 11 -3 0 834.708 129.588 2 11 -3 1 3459.18 263.153 2 11 -3 2 2373.63 222.003 2 11 -2 -6 668.575 115.642 2 -11 2 6 605.800 114.687 4 11 -2 -5 1018.36 141.582 2 -11 2 5 1179.37 153.887 4 11 -2 -4 24.6102 36.3533 2 -11 2 4 75.6989 47.3914 4 11 -2 -3 995.297 137.322 2 11 -2 -2 2146.41 210.296 2 11 -2 -1 2830.51 238.282 2 11 -2 0 6292.43 360.098 2 11 -2 1 2502.72 228.350 2 -11 1 6 2342.28 222.500 4 11 -1 -6 2117.12 213.291 2 11 -1 -5 19.6426 32.2138 2 -11 1 5 54.6664 50.2053 4 11 -1 -4 1717.28 188.893 2 11 -1 -3 3442.61 268.423 2 11 -1 -2 5250.70 334.585 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 77675 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu Cu 0.5000 0.5000 0.0000 0.01443(9) Uani 1 2 d S . P . . N1A N 0.23606(17) 0.10513(15) 0.07610(11) 0.0159(3) Uani 1 1 d D . . . . H1A H 0.232(3) 0.0184(12) 0.0797(17) 0.024 Uiso 1 1 d D U . . . C2A C 0.3595(2) 0.19666(18) 0.03637(13) 0.0170(3) Uani 1 1 d . . . . . H2A H 0.4490 0.1729 0.0095 0.020 Uiso 1 1 calc R U . . . N3A N 0.33873(16) 0.32474(14) 0.03994(10) 0.0151(3) Uani 1 1 d . . . . . C4A C 0.19500(19) 0.31291(17) 0.08347(12) 0.0149(3) Uani 1 1 d . . . . . H4A H 0.1490 0.3886 0.0958 0.018 Uiso 1 1 calc R U . . . C5A C 0.12830(19) 0.17613(17) 0.10639(12) 0.0137(3) Uani 1 1 d . . . . . C6A C -0.02134(19) 0.10991(17) 0.15313(12) 0.0138(3) Uani 1 1 d . . . . . C7A C -0.0473(2) -0.01865(18) 0.19543(14) 0.0195(3) Uani 1 1 d . . . . . H7A H 0.0332 -0.0658 0.1938 0.023 Uiso 1 1 calc R U . . . C8A C -0.1905(2) -0.07763(19) 0.23985(15) 0.0238(4) Uani 1 1 d . . . . . H8A H -0.2077 -0.1656 0.2678 0.029 Uiso 1 1 calc R U . . . C9A C -0.3084(2) -0.00990(19) 0.24389(14) 0.0220(4) Uani 1 1 d . . . . . H9A H -0.4058 -0.0505 0.2749 0.026 Uiso 1 1 calc R U . . . C10A C -0.2833(2) 0.11789(19) 0.20227(14) 0.0207(3) Uani 1 1 d . . . . . H10A H -0.3638 0.1651 0.2050 0.025 Uiso 1 1 calc R U . . . C11A C -0.1419(2) 0.17721(18) 0.15683(13) 0.0173(3) Uani 1 1 d . . . . . H11A H -0.1266 0.2642 0.1279 0.021 Uiso 1 1 calc R U . . . N1B N 0.13121(17) 0.42449(15) -0.24305(11) 0.0171(3) Uani 1 1 d D . . . . H1B H 0.0292(13) 0.391(2) -0.2641(16) 0.026 Uiso 1 1 d D U . . . C2B C 0.1915(2) 0.43359(17) -0.14255(13) 0.0169(3) Uani 1 1 d . . . . . H2B H 0.1269 0.4040 -0.0873 0.020 Uiso 1 1 calc R U . . . N3B N 0.35165(16) 0.48879(15) -0.13034(10) 0.0156(3) Uani 1 1 d . . . . . C4B C 0.3952(2) 0.5160(2) -0.22964(14) 0.0255(4) Uani 1 1 d . . . . . H4B H 0.5040 0.5567 -0.2457 0.031 Uiso 1 1 calc R U . . . C5B C 0.2589(2) 0.4756(2) -0.30072(13) 0.0214(4) Uani 1 1 d . . . . . C6B C 0.2275(5) 0.4518(4) -0.4167(2) 0.0176(12) Uani 0.5 1 d G . P A 1 C7B C 0.0841(5) 0.3549(4) -0.4720(3) 0.0222(12) Uani 0.5 1 d G . P A 1 H7B H 0.0042 0.2957 -0.4352 0.027 Uiso 0.5 1 calc R U P A 1 C8B C 0.0575(4) 0.3445(4) -0.5813(3) 0.0289(13) Uani 0.5 1 d G . P A 1 H8B H -0.0405 0.2783 -0.6191 0.035 Uiso 0.5 1 calc R U P A 1 C9B C 0.1744(4) 0.4311(4) -0.6352(2) 0.0242(11) Uani 0.5 1 d G . P A 1 H9B H 0.1562 0.4241 -0.7099 0.029 Uiso 0.5 1 calc R U P A 1 C10B C 0.3178(3) 0.5280(4) -0.5799(2) 0.0259(8) Uani 0.5 1 d G . P A 1 H10B H 0.3976 0.5872 -0.6167 0.031 Uiso 0.5 1 calc R U P A 1 C11B C 0.3443(3) 0.5383(3) -0.4706(2) 0.0218(8) Uani 0.5 1 d G . P A 1 H11B H 0.4424 0.6046 -0.4328 0.026 Uiso 0.5 1 calc R U P A 1 C6C C 0.2419(5) 0.4922(4) -0.4147(2) 0.0164(11) Uani 0.5 1 d G . P A 2 C7C C 0.1351(6) 0.3726(4) -0.4809(3) 0.0265(12) Uani 0.5 1 d G . P A 2 H7C H 0.0735 0.2909 -0.4519 0.032 Uiso 0.5 1 calc R U P A 2 C8C C 0.1184(5) 0.3724(3) -0.5896(3) 0.0319(14) Uani 0.5 1 d G . P A 2 H8C H 0.0454 0.2906 -0.6348 0.038 Uiso 0.5 1 calc R U P A 2 C9C C 0.2084(5) 0.4919(4) -0.6320(2) 0.0258(12) Uani 0.5 1 d G . P A 2 H9C H 0.1970 0.4917 -0.7062 0.031 Uiso 0.5 1 calc R U P A 2 C10C C 0.3152(4) 0.6115(3) -0.56579(19) 0.0264(8) Uani 0.5 1 d G . P A 2 H10C H 0.3768 0.6932 -0.5948 0.032 Uiso 0.5 1 calc R U P A 2 C11C C 0.3319(4) 0.6117(3) -0.45717(18) 0.0217(7) Uani 0.5 1 d G . P A 2 H11C H 0.4049 0.6935 -0.4119 0.026 Uiso 0.5 1 calc R U P A 2 Cl Cl 0.26988(5) 0.72337(4) 0.12601(3) 0.01654(10) Uani 1 1 d . . . . . O1 O 0.39920(15) 0.66131(13) 0.13604(10) 0.0214(3) Uani 1 1 d . . . . . O2 O 0.21253(17) 0.74779(16) 0.22694(11) 0.0319(3) Uani 1 1 d . . . . . O3 O 0.13731(15) 0.62726(13) 0.05218(10) 0.0228(3) Uani 1 1 d . . . . . O4 O 0.33199(16) 0.85956(13) 0.08722(12) 0.0271(3) Uani 1 1 d . . . . . O5 O 0.5000 0.0000 0.5000 0.0568(7) Uani 1 2 d DS . P . . C12A C 0.6054(6) -0.0650(5) 0.5269(4) 0.0401(10) Uani 0.5 1 d D . P B 1 H12A H 0.5910 -0.1481 0.4708 0.048 Uiso 0.5 1 calc R U P B 1 H12B H 0.5746 -0.1051 0.5924 0.048 Uiso 0.5 1 calc R U P B 1 C13A C 0.7838(6) 0.0207(7) 0.5451(5) 0.0426(13) Uani 0.5 1 d D U P B 1 H13A H 0.8470 -0.0425 0.5617 0.064 Uiso 0.5 1 calc R U P B 1 H13B H 0.8031 0.0993 0.6043 0.064 Uiso 0.5 1 calc R U P B 1 H13C H 0.8180 0.0615 0.4812 0.064 Uiso 0.5 1 calc R U P B 1 C12B C 0.6568(5) 0.0530(5) 0.5237(4) 0.0401(11) Uani 0.5 1 d D . P B 2 H12C H 0.6807 0.1339 0.5829 0.048 Uiso 0.5 1 calc R U P B 2 H12D H 0.7055 0.0937 0.4621 0.048 Uiso 0.5 1 calc R U P B 2 C13B C 0.7390(9) -0.0509(8) 0.5543(7) 0.069(2) Uani 0.5 1 d D U P B 2 H13D H 0.8576 -0.0027 0.5660 0.104 Uiso 0.5 1 calc R U P B 2 H13E H 0.7134 -0.1335 0.4975 0.104 Uiso 0.5 1 calc R U P B 2 H13F H 0.7001 -0.0849 0.6194 0.104 Uiso 0.5 1 calc R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu 0.01181(14) 0.01697(15) 0.01191(14) 0.00545(10) 0.00048(10) -0.00014(11) N1A 0.0163(7) 0.0130(6) 0.0196(7) 0.0043(5) 0.0047(5) 0.0051(5) C2A 0.0147(8) 0.0191(8) 0.0163(7) 0.0028(6) 0.0022(6) 0.0040(6) N3A 0.0135(6) 0.0164(7) 0.0133(6) 0.0042(5) 0.0002(5) 0.0014(5) C4A 0.0158(7) 0.0147(7) 0.0141(7) 0.0038(6) 0.0016(6) 0.0042(6) C5A 0.0151(7) 0.0137(7) 0.0121(7) 0.0025(6) 0.0001(6) 0.0045(6) C6A 0.0145(7) 0.0133(7) 0.0122(7) 0.0021(6) 0.0016(6) 0.0025(6) C7A 0.0218(8) 0.0156(8) 0.0239(8) 0.0063(6) 0.0067(7) 0.0078(7) C8A 0.0285(9) 0.0161(8) 0.0279(9) 0.0095(7) 0.0103(8) 0.0048(7) C9A 0.0181(8) 0.0225(9) 0.0215(8) 0.0023(7) 0.0074(7) 0.0005(7) C10A 0.0158(8) 0.0229(9) 0.0232(8) 0.0024(7) 0.0019(7) 0.0064(7) C11A 0.0180(8) 0.0160(8) 0.0180(8) 0.0044(6) 0.0004(6) 0.0053(6) N1B 0.0118(6) 0.0198(7) 0.0191(7) 0.0022(5) -0.0005(5) 0.0051(5) C2B 0.0166(8) 0.0175(8) 0.0178(8) 0.0047(6) 0.0035(6) 0.0063(6) N3B 0.0143(6) 0.0183(7) 0.0133(6) 0.0039(5) 0.0024(5) 0.0036(5) C4B 0.0150(8) 0.0441(11) 0.0161(8) 0.0119(8) 0.0033(7) 0.0045(8) C5B 0.0180(8) 0.0317(10) 0.0163(8) 0.0045(7) 0.0018(6) 0.0103(7) C6B 0.020(2) 0.019(2) 0.018(2) 0.0056(16) 0.0028(19) 0.0108(19) C7B 0.022(3) 0.025(2) 0.016(2) -0.0009(17) -0.0021(17) 0.0053(17) C8B 0.030(3) 0.033(3) 0.021(2) -0.0018(18) -0.005(2) 0.011(2) C9B 0.039(3) 0.025(3) 0.013(2) 0.0026(18) 0.0000(18) 0.017(2) C10B 0.031(2) 0.031(2) 0.0186(18) 0.0052(16) 0.0045(17) 0.0124(18) C11B 0.0220(19) 0.024(2) 0.0201(18) 0.0034(16) 0.0010(14) 0.0081(16) C6C 0.018(2) 0.020(3) 0.013(2) -0.0001(13) -0.0037(16) 0.0096(16) C7C 0.029(3) 0.026(2) 0.023(2) 0.0058(19) 0.001(2) 0.006(2) C8C 0.040(4) 0.033(3) 0.017(2) -0.005(2) -0.009(2) 0.010(3) C9C 0.038(3) 0.029(3) 0.018(2) 0.0063(19) 0.0049(19) 0.019(2) C10C 0.030(2) 0.034(2) 0.0197(18) 0.0092(17) 0.0051(15) 0.0137(18) C11C 0.0245(19) 0.024(2) 0.0175(17) 0.0047(15) 0.0019(14) 0.0084(16) Cl 0.01331(18) 0.01325(18) 0.0218(2) -0.00059(14) 0.00448(15) 0.00314(14) O1 0.0178(6) 0.0201(6) 0.0281(6) 0.0037(5) 0.0030(5) 0.0087(5) O2 0.0281(7) 0.0382(8) 0.0252(7) -0.0053(6) 0.0114(6) 0.0066(6) O3 0.0163(6) 0.0192(6) 0.0289(7) -0.0034(5) -0.0008(5) 0.0034(5) O4 0.0217(6) 0.0154(6) 0.0463(8) 0.0084(5) 0.0090(6) 0.0066(5) O5 0.0474(15) 0.088(2) 0.0395(13) -0.0021(13) 0.0006(11) 0.0344(15) C12A 0.055(3) 0.031(2) 0.035(2) 0.0031(18) 0.008(2) 0.015(2) C13A 0.040(3) 0.050(4) 0.033(2) -0.010(3) -0.003(2) 0.015(3) C12B 0.034(2) 0.043(3) 0.031(2) -0.0044(19) 0.0016(18) 0.000(2) C13B 0.033(4) 0.065(5) 0.096(6) -0.009(4) -0.012(3) 0.006(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3A Cu N3A 180.0 . 2_665 ? N3A Cu N3B 89.00(5) . 2_665 ? N3A Cu N3B 91.00(5) 2_665 2_665 ? N3A Cu N3B 91.00(5) . . ? N3A Cu N3B 89.00(5) 2_665 . ? N3B Cu N3B 180.0 2_665 . ? C2A N1A C5A 108.81(13) . . ? C2A N1A H1A 121.5(15) . . ? C5A N1A H1A 129.7(15) . . ? N3A C2A N1A 110.30(14) . . ? N3A C2A H2A 124.8 . . ? N1A C2A H2A 124.8 . . ? C2A N3A C4A 106.19(13) . . ? C2A N3A Cu 124.72(11) . . ? C4A N3A Cu 128.89(11) . . ? C5A C4A N3A 109.94(14) . . ? C5A C4A H4A 125.0 . . ? N3A C4A H4A 125.0 . . ? C4A C5A N1A 104.74(14) . . ? C4A C5A C6A 131.12(15) . . ? N1A C5A C6A 124.13(14) . . ? C7A C6A C11A 118.68(15) . . ? C7A C6A C5A 121.88(15) . . ? C11A C6A C5A 119.44(14) . . ? C8A C7A C6A 120.18(16) . . ? C8A C7A H7A 119.9 . . ? C6A C7A H7A 119.9 . . ? C9A C8A C7A 120.77(16) . . ? C9A C8A H8A 119.6 . . ? C7A C8A H8A 119.6 . . ? C8A C9A C10A 119.35(16) . . ? C8A C9A H9A 120.3 . . ? C10A C9A H9A 120.3 . . ? C11A C10A C9A 120.54(16) . . ? C11A C10A H10A 119.7 . . ? C9A C10A H10A 119.7 . . ? C10A C11A C6A 120.48(15) . . ? C10A C11A H11A 119.8 . . ? C6A C11A H11A 119.8 . . ? C2B N1B C5B 108.59(14) . . ? C2B N1B H1B 122.8(15) . . ? C5B N1B H1B 128.6(15) . . ? N3B C2B N1B 111.10(14) . . ? N3B C2B H2B 124.5 . . ? N1B C2B H2B 124.5 . . ? C2B N3B C4B 105.49(14) . . ? C2B N3B Cu 126.11(11) . . ? C4B N3B Cu 127.74(11) . . ? C5B C4B N3B 109.91(15) . . ? C5B C4B H4B 125.0 . . ? N3B C4B H4B 125.0 . . ? C4B C5B N1B 104.91(15) . . ? C4B C5B C6B 135.0(2) . . ? N1B C5B C6B 118.9(2) . . ? C4B C5B C6C 129.9(2) . . ? N1B C5B C6C 125.0(2) . . ? C7B C6B C11B 120.0 . . ? C7B C6B C5B 123.0(2) . . ? C11B C6B C5B 116.9(2) . . ? C8B C7B C6B 120.0 . . ? C8B C7B H7B 120.0 . . ? C6B C7B H7B 120.0 . . ? C7B C8B C9B 120.0 . . ? C7B C8B H8B 120.0 . . ? C9B C8B H8B 120.0 . . ? C8B C9B C10B 120.0 . . ? C8B C9B H9B 120.0 . . ? C10B C9B H9B 120.0 . . ? C11B C10B C9B 120.0 . . ? C11B C10B H10B 120.0 . . ? C9B C10B H10B 120.0 . . ? C10B C11B C6B 120.0 . . ? C10B C11B H11B 120.0 . . ? C6B C11B H11B 120.0 . . ? C7C C6C C11C 120.0 . . ? C7C C6C C5B 115.1(2) . . ? C11C C6C C5B 124.7(2) . . ? C6C C7C C8C 120.0 . . ? C6C C7C H7C 120.0 . . ? C8C C7C H7C 120.0 . . ? C9C C8C C7C 120.0 . . ? C9C C8C H8C 120.0 . . ? C7C C8C H8C 120.0 . . ? C10C C9C C8C 120.0 . . ? C10C C9C H9C 120.0 . . ? C8C C9C H9C 120.0 . . ? C9C C10C C11C 120.0 . . ? C9C C10C H10C 120.0 . . ? C11C C10C H10C 120.0 . . ? C10C C11C C6C 120.0 . . ? C10C C11C H11C 120.0 . . ? C6C C11C H11C 120.0 . . ? O2 Cl O3 109.66(8) . . ? O2 Cl O1 110.24(8) . . ? O3 Cl O1 109.57(7) . . ? O2 Cl O4 109.28(8) . . ? O3 Cl O4 109.24(8) . . ? O1 Cl O4 108.82(7) . . ? C12B O5 C12B 180.0 2_656 . ? C12A O5 C12A 180.0 2_656 . ? O5 C12A C13A 118.8(4) . . ? O5 C12A H12A 107.6 . . ? C13A C12A H12A 107.6 . . ? O5 C12A H12B 107.6 . . ? C13A C12A H12B 107.6 . . ? H12A C12A H12B 107.1 . . ? C12A C13A H13A 109.5 . . ? C12A C13A H13B 109.5 . . ? H13A C13A H13B 109.5 . . ? C12A C13A H13C 109.5 . . ? H13A C13A H13C 109.5 . . ? H13B C13A H13C 109.5 . . ? O5 C12B C13B 115.5(4) . . ? O5 C12B H12C 108.4 . . ? C13B C12B H12C 108.4 . . ? O5 C12B H12D 108.4 . . ? C13B C12B H12D 108.4 . . ? H12C C12B H12D 107.5 . . ? C12B C13B H13D 109.5 . . ? C12B C13B H13E 109.5 . . ? H13D C13B H13E 109.5 . . ? C12B C13B H13F 109.5 . . ? H13D C13B H13F 109.5 . . ? H13E C13B H13F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu N3A 2.0012(13) . ? Cu N3A 2.0012(13) 2_665 ? Cu N3B 2.0072(13) 2_665 ? Cu N3B 2.0072(13) . ? N1A C2A 1.342(2) . ? N1A C5A 1.377(2) . ? N1A H1A 0.851(9) . ? C2A N3A 1.323(2) . ? C2A H2A 0.9500 . ? N3A C4A 1.376(2) . ? C4A C5A 1.367(2) . ? C4A H4A 0.9500 . ? C5A C6A 1.463(2) . ? C6A C7A 1.398(2) . ? C6A C11A 1.400(2) . ? C7A C8A 1.389(2) . ? C7A H7A 0.9500 . ? C8A C9A 1.382(3) . ? C8A H8A 0.9500 . ? C9A C10A 1.387(2) . ? C9A H9A 0.9500 . ? C10A C11A 1.384(2) . ? C10A H10A 0.9500 . ? C11A H11A 0.9500 . ? N1B C2B 1.339(2) . ? N1B C5B 1.371(2) . ? N1B H1B 0.852(9) . ? C2B N3B 1.313(2) . ? C2B H2B 0.9500 . ? N3B C4B 1.386(2) . ? C4B C5B 1.361(2) . ? C4B H4B 0.9500 . ? C5B C6B 1.469(3) . ? C5B C6C 1.493(3) . ? C6B C7B 1.3900 . ? C6B C11B 1.3900 . ? C7B C8B 1.3900 . ? C7B H7B 0.9500 . ? C8B C9B 1.3900 . ? C8B H8B 0.9500 . ? C9B C10B 1.3900 . ? C9B H9B 0.9500 . ? C10B C11B 1.3900 . ? C10B H10B 0.9500 . ? C11B H11B 0.9500 . ? C6C C7C 1.3900 . ? C6C C11C 1.3900 . ? C7C C8C 1.3900 . ? C7C H7C 0.9500 . ? C8C C9C 1.3900 . ? C8C H8C 0.9500 . ? C9C C10C 1.3900 . ? C9C H9C 0.9500 . ? C10C C11C 1.3900 . ? C10C H10C 0.9500 . ? C11C H11C 0.9500 . ? Cl O2 1.4364(13) . ? Cl O3 1.4370(12) . ? Cl O1 1.4379(12) . ? Cl O4 1.4441(13) . ? O5 C12B 1.293(4) 2_656 ? O5 C12B 1.293(4) . ? O5 C12A 1.317(4) 2_656 ? O5 C12A 1.317(4) . ? C12A C13A 1.499(6) . ? C12A H12A 0.9900 . ? C12A H12B 0.9900 . ? C13A H13A 0.9800 . ? C13A H13B 0.9800 . ? C13A H13C 0.9800 . ? C12B C13B 1.489(7) . ? C12B H12C 0.9900 . ? C12B H12D 0.9900 . ? C13B H13D 0.9800 . ? C13B H13E 0.9800 . ? C13B H13F 0.9800 . ? _cod_database_fobs_code 2023233