#------------------------------------------------------------------------------
#$Date: 2024-08-07 04:59:08 +0300 (Wed, 07 Aug 2024) $
#$Revision: 294020 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/02/32/2023235.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2023235
loop_
_publ_author_name
'R\"owekamp-Krugley, Natalia'
'Reuter, Hans'
_publ_section_title
;
[SnF(bipy)(H2O)]2[SnF6], a mixed-valent inorganic tin(II)--tin(IV)
compound
;
_journal_coeditor_code OI2009
_journal_issue 9
_journal_name_full
'Acta Crystallographica Section E Crystallographic Communications'
_journal_paper_doi 10.1107/S2056989024007400
_journal_volume 80
_journal_year 2024
_chemical_formula_iupac '[Sn F (C10 H8 N2) (H2 O1)]2 [Sn F6]'
_chemical_formula_moiety '2(C10 H10 F1 N2 O1 Sn +), F6 Sn 2-'
_chemical_formula_sum 'C20 H20 F8 N4 O2 Sn3'
_chemical_formula_weight 856.47
_chemical_name_systematic
;
Bis[aqua(2,2'-bipyridine)fluoridotin(II)] hexafluoridotin(IV)
;
_space_group_crystal_system triclinic
_space_group_IT_number 2
_space_group_name_Hall '-P 1'
_space_group_name_H-M_alt 'P -1'
_atom_sites_solution_hydrogens mixed
_atom_sites_solution_primary direct
_audit_creation_method SHELXL-2014/7
_cell_angle_alpha 97.073(2)
_cell_angle_beta 98.474(2)
_cell_angle_gamma 100.644(2)
_cell_formula_units_Z 1
_cell_length_a 7.4579(4)
_cell_length_b 8.4601(5)
_cell_length_c 9.8864(6)
_cell_measurement_reflns_used 9888
_cell_measurement_temperature 100(2)
_cell_measurement_theta_max 28.85
_cell_measurement_theta_min 2.48
_cell_volume 599.06(6)
_computing_cell_refinement
;
SAINT (Bruker, 2009)
;
_computing_data_collection
;
APEX2 (Bruker, 2009)
;
_computing_data_reduction
;
SAINT (Bruker, 2009)
;
_computing_molecular_graphics
;
DIAMOND (Brandenburg, 2006), Mercury (Macrae et al.
(2020)
;
_computing_publication_material
;
publCIF (Westrip, 2010)
;
_computing_structure_refinement
;
SHELXL2014/7 (Sheldrick, 2015)
;
_computing_structure_solution
;
SHELXS97 (Sheldrick 2008)
;
_diffrn_ambient_temperature 100(2)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type 'Bruker APEXII CCD'
_diffrn_measurement_method '\f and \w scans'
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_reflns_av_R_equivalents 0.0626
_diffrn_reflns_av_unetI/netI 0.0336
_diffrn_reflns_limit_h_max 9
_diffrn_reflns_limit_h_min -9
_diffrn_reflns_limit_k_max 11
_diffrn_reflns_limit_k_min -10
_diffrn_reflns_limit_l_max 13
_diffrn_reflns_limit_l_min -13
_diffrn_reflns_number 28904
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 27.996
_diffrn_reflns_theta_min 2.996
_exptl_absorpt_coefficient_mu 3.193
_exptl_absorpt_correction_T_max 0.713
_exptl_absorpt_correction_T_min 0.434
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
(SADABS; Krause et al., 2015
;
_exptl_crystal_colour colourless
_exptl_crystal_density_diffrn 2.374
_exptl_crystal_description plate
_exptl_crystal_F_000 406
_exptl_crystal_size_max 0.168
_exptl_crystal_size_mid 0.150
_exptl_crystal_size_min 0.047
_refine_diff_density_max 0.887
_refine_diff_density_min -0.693
_refine_ls_extinction_coef 0.0061(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_extinction_method
;
SHELXL2014/7 (Sheldrick, 2015)
;
_refine_ls_goodness_of_fit_ref 1.051
_refine_ls_hydrogen_treatment refU
_refine_ls_matrix_type full
_refine_ls_number_parameters 172
_refine_ls_number_reflns 2864
_refine_ls_number_restraints 0
_refine_ls_restrained_S_all 1.051
_refine_ls_R_factor_all 0.0262
_refine_ls_R_factor_gt 0.0223
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0240P)^2^+0.4078P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.0517
_refine_ls_wR_factor_ref 0.0533
_reflns_number_gt 2611
_reflns_number_total 2864
_reflns_threshold_expression 'I > 2\s(I)'
_cod_data_source_file oi2009.cif
_cod_data_source_block I
_cod_database_code 2023235
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min 0.616
_shelx_estimated_absorpt_t_max 0.864
_shelx_hkl_file
;
-2 0 0 192.97 15.15
-2 0 0 185.02 14.83
-2 0 0 195.59 14.34
-2 0 0 187.31 14.13
-2 0 0 197.65 15.00
-2 0 0 192.18 14.34
-2 0 0 186.41 14.46
-2 0 0 183.62 14.94
-2 0 0 206.58 14.49
2 0 0 203.97 15.00
2 0 0 210.37 14.54
2 0 0 189.72 14.51
2 0 0 209.62 14.97
2 0 0 187.54 14.99
-3 0 0 328.44 23.81
-3 0 0 308.54 23.56
-3 0 0 298.58 24.06
-3 0 0 330.61 23.01
-3 0 0 330.20 22.77
-3 0 0 317.15 23.37
-3 0 0 298.92 23.36
-3 0 0 307.50 23.74
-3 0 0 305.96 22.98
-3 0 0 312.15 22.32
3 0 0 287.50 23.80
3 0 0 289.97 23.79
-4 0 0 312.20 21.16
-4 0 0 278.58 20.51
-4 0 0 299.42 21.47
-4 0 0 298.36 21.18
-4 0 0 273.42 21.48
-4 0 0 274.00 20.94
-4 0 0 309.59 21.86
-4 0 0 278.34 20.93
-4 0 0 278.56 21.67
-4 0 0 251.78 21.87
4 0 0 272.18 21.90
4 0 0 284.67 21.91
-5 0 0 5.20 0.62
-5 0 0 5.20 0.63
-5 0 0 3.90 0.54
-5 0 0 5.53 0.66
-5 0 0 5.20 0.67
-5 0 0 4.28 0.59
-5 0 0 3.57 0.54
-5 0 0 4.87 0.47
-5 0 0 4.50 0.56
-5 0 0 4.78 0.61
-5 0 0 5.48 0.49
5 0 0 4.65 0.70
5 0 0 5.78 0.75
-6 0 0 3.72 0.54
-6 0 0 2.51 0.56
-6 0 0 2.30 0.55
-6 0 0 3.03 0.51
-6 0 0 3.21 0.55
-6 0 0 2.69 0.58
-6 0 0 3.82 0.49
-6 0 0 3.39 0.44
-6 0 0 4.01 0.64
-6 0 0 3.21 0.61
-6 0 0 2.52 0.55
6 0 0 4.06 0.69
6 0 0 4.23 0.72
-7 0 0 155.13 12.39
-7 0 0 159.74 12.01
-7 0 0 150.23 12.00
-7 0 0 166.31 11.65
-7 0 0 164.80 11.54
-7 0 0 167.21 11.88
-7 0 0 163.01 11.52
-7 0 0 160.57 12.16
-7 0 0 148.34 11.99
-7 0 0 156.26 12.21
7 0 0 141.13 12.36
7 0 0 155.86 12.44
-8 0 0 5.51 1.00
-8 0 0 7.18 0.82
-8 0 0 6.56 0.94
-8 0 0 7.00 1.00
-8 0 0 4.71 0.90
-8 0 0 5.29 0.88
-8 0 0 6.09 0.94
8 0 0 7.16 1.03
8 0 0 6.90 1.07
-9 0 0 5.27 0.95
-9 0 0 3.86 0.89
9 0 0 4.43 0.83
9 -1 0 0.19 0.47
-9 1 0 0.54 0.55
-9 1 0 1.73 0.59
8 -1 0 0.64 0.53
8 -1 0 0.89 0.43
-8 1 0 0.77 0.42
-8 1 0 0.54 0.32
-8 1 0 -0.37 0.41
-8 1 0 0.71 0.44
-8 1 0 0.20 0.46
7 -1 0 118.66 10.13
7 -1 0 137.23 10.22
-7 1 0 121.13 9.51
-7 1 0 142.40 9.75
-7 1 0 133.50 9.39
-7 1 0 124.24 9.84
-7 1 0 128.81 9.85
-7 1 0 118.71 10.15
-7 1 0 139.61 9.96
6 -1 0 10.16 1.07
6 -1 0 11.28 1.11
-6 1 0 11.45 0.99
-6 1 0 10.58 0.96
-6 1 0 10.31 1.01
-6 1 0 8.01 0.98
-6 1 0 10.09 0.92
-6 1 0 9.06 0.99
-6 1 0 9.76 1.04
-6 1 0 11.94 1.04
-6 1 0 9.95 0.95
5 -1 0 8.25 0.87
5 -1 0 10.01 0.91
-5 1 0 6.74 0.78
-5 1 0 8.28 0.82
-5 1 0 8.54 0.78
-5 1 0 8.97 0.84
-5 1 0 8.74 0.75
-5 1 0 8.22 0.85
4 -1 0 25.61 2.11
4 -1 0 27.69 2.11
-4 1 0 25.60 2.07
-4 1 0 25.22 2.04
-4 1 0 26.74 2.03
-4 1 0 25.03 2.03
-4 1 0 26.60 2.01
-4 1 0 21.82 1.98
3 -1 0 362.25 28.51
-3 1 0 392.80 28.50
-3 1 0 363.23 28.53
-3 1 0 382.17 28.56
-3 1 0 358.44 27.59
2 -1 0 192.29 15.01
2 -1 0 197.59 15.02
1 -1 0 59.62 4.18
-1 1 0 50.22 3.96
-1 1 0 46.42 3.95
-1 1 0 52.14 4.05
-1 1 0 52.76 3.97
-1 -1 0 190.85 15.96
-1 -1 0 222.72 15.08
-1 -1 0 220.24 15.86
-1 -1 0 198.45 15.30
-1 -1 0 189.84 15.99
-1 -1 0 216.19 16.18
-1 -1 0 219.01 14.99
-1 -1 0 189.20 15.46
-1 -1 0 211.31 15.75
-1 -1 0 175.18 15.46
-1 -1 0 200.60 16.02
-1 -1 0 235.36 15.73
-1 -1 0 216.31 14.98
1 1 0 232.03 15.98
1 1 0 210.42 15.31
1 1 0 214.78 14.98
1 1 0 187.54 16.17
1 1 0 210.47 15.01
-2 -1 0 10.12 0.98
-2 -1 0 11.44 1.07
-2 -1 0 9.36 0.87
-2 -1 0 8.73 0.98
-2 -1 0 10.45 0.99
-2 -1 0 11.39 0.97
-2 -1 0 11.39 0.93
-2 -1 0 10.75 0.93
-2 -1 0 7.89 0.94
-2 -1 0 13.63 0.93
-2 -1 0 9.39 0.95
-2 -1 0 11.52 0.97
-2 -1 0 11.23 1.04
-2 -1 0 9.63 1.00
-2 -1 0 10.10 0.99
2 1 0 10.75 0.91
2 1 0 11.49 1.06
2 1 0 9.90 0.97
2 1 0 12.29 0.92
2 1 0 11.66 0.82
2 1 0 10.00 0.86
2 1 0 10.21 0.91
2 1 0 11.44 0.82
2 1 0 11.20 1.01
2 1 0 11.55 0.95
-3 -1 0 40.44 3.02
-3 -1 0 41.77 3.29
-3 -1 0 38.65 3.17
-3 -1 0 32.43 3.30
-3 -1 0 37.29 3.32
-3 -1 0 41.00 3.03
-3 -1 0 43.27 3.08
-3 -1 0 37.85 3.23
-3 -1 0 41.23 3.25
-3 -1 0 43.39 3.31
-3 -1 0 41.07 3.22
-3 -1 0 41.09 3.14
-3 -1 0 42.73 3.12
-3 -1 0 37.10 3.17
-3 -1 0 42.76 3.21
3 1 0 35.08 3.10
3 1 0 42.98 3.35
3 1 0 42.58 3.35
3 1 0 39.53 3.03
3 1 0 43.62 3.15
3 1 0 39.41 3.23
3 1 0 40.21 3.04
-4 -1 0 347.27 30.23
-4 -1 0 414.05 28.94
-4 -1 0 366.33 28.38
-4 -1 0 387.83 29.96
-4 -1 0 380.24 28.28
-4 -1 0 359.93 28.94
-4 -1 0 446.12 30.20
-4 -1 0 441.82 29.28
-4 -1 0 345.42 29.19
-4 -1 0 362.54 29.24
-4 -1 0 397.99 28.30
-4 -1 0 370.93 29.73
-4 -1 0 378.78 29.69
4 1 0 397.84 29.11
4 1 0 430.38 30.30
4 1 0 383.01 29.11
4 1 0 444.69 29.87
4 1 0 366.39 29.84
4 1 0 405.05 30.09
4 1 0 429.80 30.30
-5 -1 0 18.30 1.71
-5 -1 0 20.58 1.62
-5 -1 0 18.09 1.66
-5 -1 0 17.26 1.51
-5 -1 0 15.71 1.62
-5 -1 0 19.45 1.67
-5 -1 0 19.55 1.73
-5 -1 0 15.91 1.64
-5 -1 0 18.20 1.60
-5 -1 0 16.59 1.71
-5 -1 0 16.78 1.53
-5 -1 0 18.62 1.66
-5 -1 0 17.03 1.68
5 1 0 18.44 1.44
5 1 0 15.94 1.77
5 1 0 18.87 1.82
5 1 0 19.64 1.44
-6 -1 0 10.11 1.13
-6 -1 0 10.44 1.09
-6 -1 0 8.00 1.10
-6 -1 0 10.46 1.00
-6 -1 0 10.45 1.18
-6 -1 0 9.75 1.13
-6 -1 0 8.87 1.01
-6 -1 0 10.69 1.14
-6 -1 0 10.41 1.20
-6 -1 0 8.50 1.14
-6 -1 0 9.61 1.10
6 1 0 10.41 1.28
6 1 0 8.32 1.20
-7 -1 0 86.20 7.01
-7 -1 0 92.06 6.87
-7 -1 0 87.84 7.12
-7 -1 0 86.94 7.29
-7 -1 0 85.29 7.13
-7 -1 0 98.40 6.83
-7 -1 0 81.44 7.35
-7 -1 0 99.39 7.25
-7 -1 0 100.25 6.97
7 1 0 85.62 7.38
7 1 0 90.04 7.42
-8 -1 0 50.43 4.29
-8 -1 0 51.34 4.31
-8 -1 0 50.73 4.46
-8 -1 0 49.95 4.23
-8 -1 0 50.45 4.16
-8 -1 0 51.86 4.20
8 1 0 51.88 4.49
8 1 0 49.62 4.42
-9 -1 0 4.67 1.03
9 1 0 2.87 0.99
9 -2 0 9.47 1.02
-9 2 0 9.73 1.64
-9 2 0 9.78 1.08
-9 2 0 9.71 1.11
8 -2 0 3.83 0.61
8 -2 0 4.36 0.66
-8 2 0 5.10 0.73
-8 2 0 5.60 1.08
-8 2 0 4.34 0.65
-8 2 0 3.79 0.61
-8 2 0 4.09 0.65
7 -2 0 61.23 5.04
7 -2 0 60.41 5.06
-7 2 0 67.62 4.91
-7 2 0 59.07 4.82
-7 2 0 72.92 4.93
-7 2 0 61.82 4.88
-7 2 0 67.30 4.82
-7 2 0 57.36 5.47
-7 2 0 60.90 5.07
6 -2 0 66.61 5.48
6 -2 0 61.84 5.47
-6 2 0 70.29 5.30
-6 2 0 75.06 5.32
-6 2 0 77.42 5.29
-6 2 0 69.72 5.90
-6 2 0 69.66 5.22
-6 2 0 71.12 5.48
-6 2 0 65.18 5.19
5 -2 0 1.31 0.31
5 -2 0 0.75 0.27
-5 2 0 0.61 0.23
-5 2 0 0.74 0.38
-5 2 0 1.12 0.23
-5 2 0 1.05 0.22
4 -2 0 0.08 0.20
-4 2 0 0.17 0.16
-4 2 0 0.13 0.31
3 -2 0 212.85 17.35
3 -2 0 250.41 17.38
-3 2 0 214.12 17.84
2 -2 0 29.87 2.66
2 -2 0 30.11 2.52
2 -2 0 32.64 2.53
-2 2 0 31.31 2.52
-2 2 0 32.73 2.42
-2 2 0 29.14 2.65
-2 2 0 34.45 2.55
-2 2 0 31.44 2.41
-2 2 0 33.01 2.49
-2 2 0 31.44 2.50
1 -2 0 38.37 2.90
1 -2 0 41.46 2.91
1 -2 0 34.59 2.78
1 -2 0 34.55 3.05
1 -2 0 38.63 2.79
1 -2 0 43.07 3.07
1 -2 0 38.85 3.06
1 -2 0 35.79 2.89
1 -2 0 39.15 2.89
1 -2 0 42.61 2.86
1 -2 0 32.16 3.12
1 -2 0 33.32 3.00
1 -2 0 40.22 2.85
-1 2 0 40.62 2.88
-1 2 0 42.25 2.89
-1 2 0 41.74 2.80
-1 2 0 36.90 2.81
-1 2 0 35.81 2.81
-1 2 0 37.85 2.92
-1 2 0 36.48 2.92
-1 2 0 37.17 3.03
-1 2 0 38.50 3.06
-1 2 0 39.72 2.91
-1 2 0 36.10 3.13
-1 2 0 35.73 3.06
-1 2 0 36.48 3.03
-1 2 0 37.10 2.93
-1 2 0 41.16 2.94
0 -2 0 189.71 16.04
0 -2 0 187.99 16.62
0 -2 0 224.95 17.00
0 -2 0 201.60 16.58
0 -2 0 210.73 15.59
0 -2 0 217.82 15.56
0 -2 0 219.83 16.34
0 -2 0 199.44 16.05
0 -2 0 199.62 15.64
0 -2 0 209.60 16.81
0 -2 0 238.10 15.91
0 -2 0 204.61 15.65
0 -2 0 227.37 16.09
0 -2 0 231.54 16.66
0 -2 0 220.84 15.60
0 -2 0 240.47 16.08
0 -2 0 203.15 15.56
0 -2 0 212.24 15.91
0 2 0 225.89 15.57
0 2 0 223.90 17.00
0 2 0 223.30 16.65
0 2 0 201.55 16.58
0 2 0 201.83 16.05
0 2 0 232.82 15.92
0 2 0 250.96 16.10
0 2 0 211.65 16.06
0 2 0 239.23 15.61
0 2 0 232.43 15.93
0 2 0 183.51 15.65
0 2 0 204.96 16.06
-1 -2 0 164.18 12.30
-1 -2 0 165.26 12.58
-1 -2 0 171.91 12.71
-1 -2 0 176.47 12.70
-1 -2 0 169.29 13.28
-1 -2 0 179.72 12.71
-1 -2 0 169.14 13.15
-1 -2 0 166.17 12.56
-1 -2 0 157.16 12.91
-1 -2 0 189.03 13.12
-1 -2 0 182.05 12.73
-1 -2 0 179.18 12.35
-1 -2 0 174.34 12.57
-1 -2 0 164.02 12.30
1 2 0 178.04 12.55
1 2 0 160.03 13.15
1 2 0 170.91 12.28
1 2 0 179.15 13.29
1 2 0 164.43 12.70
1 2 0 156.66 12.88
1 2 0 173.25 12.93
1 2 0 146.06 12.65
1 2 0 175.51 12.34
1 2 0 172.01 13.11
1 2 0 157.24 12.56
1 2 0 191.68 13.02
1 2 0 165.89 12.32
1 2 0 150.85 12.27
1 2 0 163.41 12.69
-2 -2 0 2.33 0.46
-2 -2 0 3.15 0.52
-2 -2 0 2.81 0.53
-2 -2 0 2.81 0.55
-2 -2 0 2.82 0.48
-2 -2 0 2.66 0.50
-2 -2 0 2.52 0.50
-2 -2 0 3.86 0.49
-2 -2 0 2.89 0.52
-2 -2 0 2.62 0.55
-2 -2 0 2.10 0.48
-2 -2 0 2.32 0.57
-2 -2 0 3.15 0.41
-2 -2 0 3.31 0.46
-2 -2 0 2.82 0.48
-2 -2 0 2.90 0.44
-2 -2 0 3.99 0.53
-2 -2 0 2.10 0.45
2 2 0 3.12 0.40
2 2 0 2.85 0.42
2 2 0 2.57 0.45
2 2 0 4.02 0.53
2 2 0 2.36 0.46
2 2 0 2.56 0.48
2 2 0 3.26 0.48
2 2 0 2.83 0.46
2 2 0 2.54 0.50
2 2 0 2.97 0.34
2 2 0 2.20 0.45
2 2 0 4.19 0.66
2 2 0 2.46 0.58
2 2 0 2.17 0.40
2 2 0 3.57 0.53
2 2 0 3.27 0.42
-3 -2 0 1.09 0.44
-3 -2 0 -0.01 0.42
-3 -2 0 0.04 0.34
-3 -2 0 0.38 0.34
-3 -2 0 0.13 0.38
-3 -2 0 0.28 0.28
-3 -2 0 0.88 0.41
-3 -2 0 0.61 0.35
-3 -2 0 1.09 0.47
-3 -2 0 0.32 0.36
-3 -2 0 1.33 0.43
-3 -2 0 1.05 0.46
-3 -2 0 0.54 0.35
-3 -2 0 1.23 0.37
-3 -2 0 0.08 0.50
-3 -2 0 0.80 0.40
-3 -2 0 0.41 0.37
3 2 0 0.75 0.21
3 2 0 0.37 0.30
3 2 0 1.05 0.37
3 2 0 0.44 0.51
3 2 0 0.76 0.50
3 2 0 0.62 0.23
3 2 0 0.52 0.26
3 2 0 0.20 0.30
3 2 0 1.28 0.37
3 2 0 0.78 0.36
3 2 0 0.75 0.33
-4 -2 0 165.54 14.58
-4 -2 0 202.77 14.45
-4 -2 0 194.01 14.08
-4 -2 0 210.13 14.14
-4 -2 0 167.68 14.08
-4 -2 0 183.06 13.62
-4 -2 0 166.68 13.94
-4 -2 0 166.00 14.27
-4 -2 0 195.37 13.92
-4 -2 0 177.52 13.58
-4 -2 0 184.28 14.55
-4 -2 0 211.66 14.62
-4 -2 0 202.80 14.13
-4 -2 0 183.19 13.66
4 2 0 177.88 14.10
4 2 0 197.34 13.99
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3 1 -1 259.65 19.92
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3 1 -1 227.13 20.37
3 1 -1 255.46 20.22
3 1 -1 251.30 19.91
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-3 -1 1 304.58 20.45
-3 -1 1 222.98 19.96
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3 -4 2 37.72 2.70
3 -4 2 29.93 2.23
3 -4 2 27.82 2.24
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4 -4 2 27.98 2.31
4 -4 2 31.85 2.34
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6 -4 2 12.67 1.38
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7 -4 2 10.24 1.13
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8 -4 2 43.18 3.56
8 -4 2 46.96 3.59
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7 3 -2 9.79 1.45
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5 3 -2 63.63 5.53
5 3 -2 75.75 6.01
5 3 -2 68.59 5.63
5 3 -2 58.66 5.85
5 3 -2 70.29 5.53
5 3 -2 82.99 6.07
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-5 -3 2 74.63 5.76
-5 -3 2 75.07 5.75
-5 -3 2 70.42 5.51
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-5 -3 2 74.99 5.65
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-5 -3 2 67.92 5.46
-5 -3 2 75.99 5.85
-5 -3 2 81.51 5.73
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4 3 -2 3.40 0.49
4 3 -2 2.83 0.47
4 3 -2 3.19 0.59
4 3 -2 3.56 0.53
4 3 -2 2.45 0.62
4 3 -2 3.73 0.83
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3 3 -2 7.12 0.92
3 3 -2 7.95 0.70
3 3 -2 7.13 0.85
3 3 -2 7.00 0.89
3 3 -2 6.34 0.83
3 3 -2 7.50 0.81
3 3 -2 6.93 0.80
3 3 -2 7.40 0.70
3 3 -2 8.52 0.76
3 3 -2 7.59 0.86
3 3 -2 7.65 1.05
3 3 -2 7.62 1.03
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2 3 -2 215.85 15.78
2 3 -2 201.07 16.32
2 3 -2 211.88 15.83
2 3 -2 227.97 15.84
2 3 -2 222.66 15.83
2 3 -2 201.84 17.09
2 3 -2 246.66 17.01
2 3 -2 211.76 16.57
2 3 -2 211.49 16.16
2 3 -2 193.38 15.76
2 3 -2 240.21 16.98
2 3 -2 240.51 17.32
2 3 -2 228.30 16.89
2 3 -2 214.56 16.59
2 3 -2 199.69 16.34
2 3 -2 230.49 16.75
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-2 -3 2 197.62 16.34
-2 -3 2 203.72 16.19
-2 -3 2 222.54 16.95
-2 -3 2 196.65 15.86
-2 -3 2 192.35 16.35
-2 -3 2 228.95 17.32
-2 -3 2 204.05 15.81
-2 -3 2 207.19 16.16
-2 -3 2 195.87 16.93
-2 -3 2 208.12 16.40
-2 -3 2 254.71 16.97
-2 -3 2 228.48 17.16
-2 -3 2 246.15 16.66
-2 -3 2 221.50 15.84
-2 -3 2 243.62 16.38
1 3 -2 94.57 6.72
1 3 -2 93.64 6.86
1 3 -2 88.68 7.23
1 3 -2 92.21 7.28
1 3 -2 93.22 7.37
1 3 -2 86.36 6.67
1 3 -2 101.57 6.71
1 3 -2 101.30 7.23
1 3 -2 91.87 7.04
1 3 -2 84.33 7.10
1 3 -2 88.63 6.71
1 3 -2 93.80 6.73
1 3 -2 76.63 6.92
1 3 -2 94.12 6.98
1 3 -2 86.10 6.93
1 3 -2 81.64 7.19
1 3 -2 87.92 6.87
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-1 -3 2 76.97 7.16
-1 -3 2 89.24 7.28
-1 -3 2 98.49 7.24
-1 -3 2 80.30 6.83
-1 -3 2 101.11 6.76
-1 -3 2 92.64 6.95
-1 -3 2 94.68 6.98
-1 -3 2 90.50 6.71
-1 -3 2 80.02 6.68
-1 -3 2 87.68 6.96
-1 -3 2 102.32 6.91
-1 -3 2 94.72 7.37
-1 -3 2 99.80 6.96
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0 3 -2 139.84 10.87
0 3 -2 124.46 10.23
0 3 -2 129.84 10.26
0 3 -2 140.29 10.52
0 3 -2 130.89 10.59
0 3 -2 145.71 10.29
0 3 -2 149.79 10.17
0 3 -2 142.66 9.97
0 3 -2 125.45 10.23
0 3 -2 129.15 9.93
0 3 -2 152.58 9.94
0 3 -2 129.61 10.61
0 -3 2 137.43 10.14
0 -3 2 116.60 10.22
0 -3 2 137.20 9.93
0 -3 2 129.24 10.24
0 -3 2 160.62 10.78
0 -3 2 154.95 9.93
0 -3 2 138.18 10.26
0 -3 2 113.74 10.55
0 -3 2 132.83 9.93
0 -3 2 134.74 10.84
0 -3 2 150.21 10.64
0 -3 2 152.85 9.95
0 -3 2 132.73 10.25
0 -3 2 129.10 9.93
0 -3 2 125.89 10.62
0 -3 2 132.50 10.13
0 -3 2 123.59 10.40
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-1 3 -2 39.72 3.12
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-1 3 -2 37.96 3.07
-1 3 -2 36.05 3.14
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1 -3 2 37.31 2.93
1 -3 2 37.07 3.07
1 -3 2 40.81 3.12
1 -3 2 43.15 3.33
1 -3 2 38.55 2.85
1 -3 2 43.73 3.23
1 -3 2 38.74 3.20
1 -3 2 35.68 2.86
1 -3 2 39.55 2.95
1 -3 2 36.30 3.03
1 -3 2 36.03 3.05
1 -3 2 37.56 3.01
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-2 3 -2 259.02 17.97
-2 3 -2 240.14 17.68
-2 3 -2 232.75 18.27
-2 3 -2 270.56 17.18
-2 3 -2 219.10 17.13
-2 3 -2 220.81 18.27
-2 3 -2 227.68 18.24
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-2 3 -2 222.51 17.48
-2 3 -2 253.86 17.16
-2 3 -2 211.61 17.48
-2 3 -2 253.09 17.12
-2 3 -2 243.60 17.67
-2 3 -2 240.42 17.67
-2 3 -2 229.34 18.10
-2 3 -2 255.70 18.49
2 -3 2 237.16 17.88
2 -3 2 242.90 18.75
2 -3 2 221.07 17.43
2 -3 2 245.79 17.61
2 -3 2 243.85 17.63
2 -3 2 233.20 18.29
2 -3 2 216.12 17.60
2 -3 2 217.48 17.07
2 -3 2 225.38 18.29
2 -3 2 268.40 17.62
2 -3 2 233.06 17.06
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-3 3 -2 14.19 1.33
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-3 3 -2 15.37 1.26
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-3 3 -2 14.26 1.28
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-3 3 -2 16.89 1.34
-3 3 -2 16.03 1.25
-3 3 -2 17.01 1.38
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3 -3 2 13.22 1.23
3 -3 2 16.21 1.23
3 -3 2 14.01 1.41
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-4 3 -2 13.47 1.20
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-4 3 -2 12.10 1.15
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-5 3 -2 132.44 11.65
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-5 3 -2 162.51 11.31
-5 3 -2 156.70 11.57
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-5 3 -2 152.99 12.17
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-5 3 -2 165.72 11.18
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-7 3 -2 13.07 1.27
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7 -3 2 12.17 1.33
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-8 3 -2 16.35 1.49
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-9 -2 2 25.03 2.38
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-8 -2 2 40.28 3.29
-8 -2 2 38.11 3.47
-8 -2 2 34.46 3.38
-8 -2 2 36.40 3.25
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-7 -2 2 3.93 0.77
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-7 -2 2 4.16 0.77
-7 -2 2 5.65 0.83
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-6 -2 2 1.85 0.55
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5 2 -2 101.55 7.63
5 2 -2 104.80 8.17
5 2 -2 109.92 7.79
5 2 -2 93.82 8.11
5 2 -2 104.59 7.79
5 2 -2 118.05 7.65
5 2 -2 98.83 8.16
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-5 -2 2 94.67 7.84
-5 -2 2 102.54 8.36
-5 -2 2 94.41 7.70
-5 -2 2 93.77 7.53
-5 -2 2 107.77 7.96
-5 -2 2 104.29 8.14
-5 -2 2 87.90 7.48
-5 -2 2 93.06 7.49
-5 -2 2 115.12 7.98
-5 -2 2 99.69 7.54
-5 -2 2 105.28 7.75
-5 -2 2 99.89 7.86
-5 -2 2 90.95 7.71
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4 2 -2 49.66 3.90
4 2 -2 39.64 3.95
4 2 -2 45.65 3.74
4 2 -2 51.86 3.74
4 2 -2 49.23 3.82
4 2 -2 44.38 4.02
4 2 -2 51.78 3.82
4 2 -2 48.36 4.08
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-4 -2 2 46.41 4.01
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-4 -2 2 49.25 3.78
-4 -2 2 41.28 3.76
-4 -2 2 47.27 3.88
-4 -2 2 51.09 3.83
-4 -2 2 49.86 3.87
-4 -2 2 48.76 3.80
-4 -2 2 48.94 3.69
-4 -2 2 45.66 3.85
-4 -2 2 57.16 4.04
-4 -2 2 46.77 3.66
-4 -2 2 43.41 3.85
-4 -2 2 50.20 3.68
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3 2 -2 57.75 4.27
3 2 -2 50.77 4.52
3 2 -2 55.44 4.07
3 2 -2 47.23 4.49
3 2 -2 58.27 4.30
3 2 -2 54.01 4.26
3 2 -2 54.92 4.19
3 2 -2 52.16 4.27
3 2 -2 46.52 4.33
3 2 -2 60.27 4.47
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-3 -2 2 55.39 4.53
-3 -2 2 50.43 4.32
-3 -2 2 54.13 4.35
-3 -2 2 59.40 4.17
-3 -2 2 61.18 4.53
-3 -2 2 59.17 4.15
-3 -2 2 53.22 4.36
-3 -2 2 54.57 4.25
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-3 -2 2 53.68 4.33
-3 -2 2 57.52 4.17
-3 -2 2 54.28 4.60
-3 -2 2 59.17 4.30
-3 -2 2 62.22 4.60
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2 2 -2 32.86 2.44
2 2 -2 29.19 2.58
2 2 -2 24.58 2.44
2 2 -2 26.99 2.43
2 2 -2 31.05 2.44
2 2 -2 30.48 2.20
2 2 -2 27.53 2.55
2 2 -2 32.93 2.54
2 2 -2 26.08 2.41
2 2 -2 35.19 2.28
2 2 -2 29.54 2.29
2 2 -2 29.65 2.28
2 2 -2 28.07 2.56
2 2 -2 27.89 2.56
2 2 -2 31.41 2.37
-2 -2 2 29.42 2.45
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-2 -2 2 31.07 2.58
-2 -2 2 33.13 2.63
-2 -2 2 30.57 2.33
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-2 -2 2 33.31 2.38
-2 -2 2 34.01 2.51
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-2 -2 2 28.43 2.54
-2 -2 2 29.07 2.39
-2 -2 2 24.93 2.42
-2 -2 2 32.11 2.49
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1 2 -2 152.08 11.02
1 2 -2 145.13 11.04
1 2 -2 157.66 11.79
1 2 -2 144.56 11.91
1 2 -2 159.56 11.01
1 2 -2 145.70 11.06
1 2 -2 164.46 11.67
1 2 -2 154.13 11.01
1 2 -2 158.65 12.03
1 2 -2 139.73 11.26
1 2 -2 149.47 11.25
1 2 -2 149.85 11.37
1 2 -2 156.52 11.77
1 2 -2 161.08 11.80
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0 2 -2 19.01 1.52
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0 -2 2 18.16 1.47
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0 -2 2 17.89 1.55
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1 -2 2 0.94 0.26
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2 -2 2 71.62 5.65
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2 -2 2 79.18 5.52
2 -2 2 73.75 5.40
2 -2 2 74.34 5.60
2 -2 2 73.78 5.39
2 -2 2 68.05 5.51
2 -2 2 76.65 5.86
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3 1 -2 36.43 2.71
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3 -1 -2 12.04 1.07
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2 -1 -2 71.89 5.03
2 -1 -2 60.06 4.98
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0 -1 -2 489.36 33.80
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0 -1 -2 525.99 33.80
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0 1 2 469.12 34.97
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-2 -1 -2 24.60 2.08
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2 1 2 23.10 1.87
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-3 -1 -2 226.66 17.69
-3 -1 -2 255.49 16.64
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-3 -1 -2 228.07 16.56
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-3 -1 -2 234.35 16.60
-3 -1 -2 247.56 17.77
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3 1 2 218.96 16.45
3 1 2 203.79 17.71
3 1 2 227.25 16.46
3 1 2 239.84 17.07
3 1 2 217.53 17.63
3 1 2 215.27 17.30
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-4 -1 -2 52.38 3.98
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-4 -1 -2 47.80 4.26
-4 -1 -2 52.94 4.20
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4 1 2 51.75 4.30
4 1 2 55.18 3.92
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-5 -1 -2 20.99 1.94
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-6 -1 -2 22.20 2.08
-6 -1 -2 23.44 2.16
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-7 -1 -2 79.12 6.72
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-7 2 2 119.58 8.81
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1 -2 -2 20.14 1.64
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1 -2 -2 17.99 1.59
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1 2 2 12.90 1.34
1 2 2 12.40 1.23
1 2 2 12.51 1.20
1 2 2 15.79 1.39
1 2 2 13.96 1.23
1 2 2 15.37 1.18
1 2 2 12.82 1.24
1 2 2 13.53 1.21
1 2 2 13.37 1.16
1 2 2 13.80 1.21
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2 2 2 39.40 2.91
2 2 2 40.92 3.04
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2 2 2 31.83 2.79
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-7 -2 -2 71.06 5.95
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3 -3 -2 181.32 14.04
3 -3 -2 185.68 14.38
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-2 3 2 32.62 2.71
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-2 3 2 38.56 2.60
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-1 -3 -2 100.97 7.49
-1 -3 -2 85.41 7.36
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1 3 2 101.01 7.51
1 3 2 90.38 7.44
1 3 2 96.34 7.40
1 3 2 89.50 7.14
1 3 2 88.26 7.15
1 3 2 84.26 6.89
1 3 2 84.26 6.86
1 3 2 91.96 7.14
1 3 2 102.05 7.07
1 3 2 85.87 7.24
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1 3 2 80.90 7.12
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-2 -3 -2 25.18 2.44
-2 -3 -2 29.11 2.51
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2 3 2 30.33 2.65
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2 3 2 29.12 2.37
2 3 2 27.95 2.52
2 3 2 28.26 2.49
2 3 2 27.80 2.31
2 3 2 31.59 2.32
2 3 2 28.31 2.48
2 3 2 30.78 2.49
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3 3 2 14.00 1.18
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3 3 2 12.21 1.25
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3 3 2 11.89 1.23
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3 3 2 10.19 1.29
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4 3 2 173.17 11.78
4 3 2 148.76 11.76
4 3 2 129.24 11.82
4 3 2 156.35 11.19
4 3 2 154.15 12.28
4 3 2 165.87 11.33
4 3 2 170.71 11.85
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3 1 4 329.04 24.31
3 1 4 308.39 23.40
3 1 4 283.46 24.18
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1 3 -5 160.18 12.42
1 3 -5 164.20 12.40
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1 3 -5 164.69 12.46
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4 2 -5 177.54 12.48
4 2 -5 175.04 13.01
4 2 -5 174.40 12.69
4 2 -5 179.34 13.30
4 2 -5 162.05 13.37
4 2 -5 169.65 12.99
4 2 -5 164.17 13.27
4 2 -5 160.58 12.69
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-4 -2 5 153.70 12.42
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-4 -2 5 187.17 12.75
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-4 -2 5 150.55 12.34
-4 -2 5 159.36 13.24
-4 -2 5 172.29 13.25
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3 2 -5 41.97 3.65
3 2 -5 45.09 3.66
3 2 -5 46.04 3.50
3 2 -5 56.56 4.01
3 2 -5 45.68 3.86
3 2 -5 45.87 3.79
3 2 -5 45.58 3.94
3 2 -5 48.49 3.89
3 2 -5 44.98 3.84
3 2 -5 43.09 3.89
3 2 -5 48.34 3.64
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-3 -2 5 47.61 3.70
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-3 -2 5 47.11 3.72
-3 -2 5 39.84 3.73
-3 -2 5 49.73 3.93
-3 -2 5 52.95 3.67
-3 -2 5 45.82 3.81
-3 -2 5 48.86 3.94
-3 -2 5 44.44 3.85
-3 -2 5 46.14 3.61
-3 -2 5 45.81 3.60
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2 2 -5 21.61 2.12
2 2 -5 28.34 2.17
2 2 -5 24.02 1.99
2 2 -5 25.75 2.31
2 2 -5 23.67 2.05
2 2 -5 27.07 1.91
2 2 -5 21.48 2.17
2 2 -5 24.85 1.90
2 2 -5 29.53 2.04
2 2 -5 23.55 2.25
2 2 -5 28.67 2.24
2 2 -5 24.16 2.29
2 2 -5 23.10 2.30
2 2 -5 23.60 2.11
2 2 -5 22.91 2.15
2 2 -5 25.33 2.20
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-2 -2 5 25.93 2.09
-2 -2 5 23.51 2.06
-2 -2 5 24.69 2.22
-2 -2 5 26.85 2.19
-2 -2 5 24.69 2.13
-2 -2 5 24.46 2.10
-2 -2 5 29.08 2.15
-2 -2 5 31.13 2.24
-2 -2 5 24.49 2.30
-2 -2 5 25.27 2.24
-2 -2 5 23.62 2.19
-2 -2 5 22.62 2.28
-2 -2 5 26.70 2.32
-2 -2 5 24.66 2.17
-2 -2 5 23.15 2.19
1 2 -5 12.23 1.28
1 2 -5 13.23 1.30
1 2 -5 11.42 1.22
1 2 -5 14.58 1.29
1 2 -5 13.58 1.39
1 2 -5 14.71 1.22
1 2 -5 11.60 1.35
1 2 -5 14.60 1.47
1 2 -5 13.93 1.28
1 2 -5 15.14 1.24
1 2 -5 11.23 1.33
1 2 -5 15.13 1.24
1 2 -5 12.41 1.40
1 2 -5 12.66 1.15
1 2 -5 11.44 1.24
1 2 -5 13.26 1.32
1 2 -5 12.72 1.30
1 2 -5 11.88 1.27
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-1 -2 5 11.07 1.31
-1 -2 5 11.67 1.31
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0 2 -5 348.74 25.31
0 2 -5 315.62 24.48
0 2 -5 350.40 25.73
0 2 -5 329.36 26.13
0 2 -5 369.74 25.36
0 2 -5 368.38 26.67
0 2 -5 324.57 25.92
0 2 -5 320.97 24.53
0 2 -5 388.80 25.32
0 2 -5 354.84 25.31
0 2 -5 334.23 26.19
0 2 -5 335.22 24.64
0 2 -5 299.51 25.01
0 2 -5 335.21 26.20
0 -2 5 314.97 24.50
0 -2 5 294.53 25.23
0 -2 5 347.29 25.04
0 -2 5 343.72 26.18
0 -2 5 320.47 25.27
0 -2 5 325.79 25.28
0 -2 5 342.11 24.54
0 -2 5 364.61 25.33
0 -2 5 360.14 26.14
0 -2 5 329.03 24.54
0 -2 5 357.75 25.75
0 -2 5 322.27 26.09
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1 -2 5 1.86 0.45
1 -2 5 1.62 0.42
1 -2 5 0.24 0.38
1 -2 5 1.85 0.58
1 -2 5 1.72 0.44
1 -2 5 1.45 0.43
1 -2 5 1.05 0.36
1 -2 5 1.57 0.37
1 -2 5 0.81 0.36
1 -2 5 1.41 0.47
1 -2 5 2.17 0.52
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2 -2 5 11.72 1.20
2 -2 5 11.40 1.28
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2 -2 5 13.53 1.33
2 -2 5 11.58 1.42
2 -2 5 12.88 1.40
2 -2 5 15.42 1.53
2 -2 5 15.42 1.26
2 -2 5 13.20 1.33
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3 -2 5 99.44 8.29
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3 -2 5 106.07 7.52
3 -2 5 92.89 7.60
3 -2 5 93.93 7.52
3 -2 5 96.49 7.97
3 -2 5 103.24 7.88
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-4 2 -5 83.64 5.62
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-4 2 -5 78.90 5.73
-4 2 -5 64.59 5.73
-4 2 -5 77.64 5.81
-4 2 -5 63.49 5.53
-4 2 -5 71.39 5.32
-4 2 -5 71.69 5.60
-4 2 -5 70.59 5.46
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4 -2 5 58.98 5.27
4 -2 5 61.61 5.41
4 -2 5 68.58 5.79
4 -2 5 68.74 5.37
4 -2 5 71.26 5.44
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-5 2 -5 8.20 1.02
-5 2 -5 8.27 1.10
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-5 2 -5 6.27 0.96
-5 2 -5 7.37 1.23
-5 2 -5 6.25 0.95
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7 -2 5 113.79 9.32
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8 1 -5 12.41 1.40
-8 -1 5 11.24 1.24
-8 -1 5 8.48 1.14
-8 -1 5 10.22 1.17
-8 -1 5 8.07 1.26
-8 -1 5 9.79 1.15
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7 1 -5 178.92 12.46
-7 -1 5 148.09 11.57
-7 -1 5 173.35 11.52
-7 -1 5 155.13 12.34
-7 -1 5 150.41 12.00
-7 -1 5 149.27 11.47
-7 -1 5 161.55 11.97
-7 -1 5 159.21 11.54
-7 -1 5 159.70 11.78
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6 1 -5 4.40 0.84
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-6 -1 5 6.74 0.95
-6 -1 5 4.72 0.79
-6 -1 5 6.54 0.91
-6 -1 5 7.44 0.74
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-6 -1 5 6.09 0.77
-6 -1 5 5.17 0.76
-6 -1 5 6.22 0.89
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5 1 -5 4.64 0.63
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-5 -1 5 3.13 0.64
-5 -1 5 5.65 0.77
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4 1 -5 143.38 11.48
4 1 -5 168.12 11.35
4 1 -5 155.43 11.58
4 1 -5 157.69 11.19
4 1 -5 152.50 10.94
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3 1 -5 150.20 12.48
3 1 -5 165.86 12.41
3 1 -5 162.91 12.94
3 1 -5 175.37 12.44
3 1 -5 152.73 12.68
3 1 -5 150.37 12.83
3 1 -5 154.76 13.02
3 1 -5 173.45 12.25
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3 1 -5 189.55 12.39
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2 1 -5 -0.32 0.23
2 1 -5 -0.50 0.24
2 1 -5 0.39 0.24
2 1 -5 0.01 0.21
2 1 -5 -0.11 0.30
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1 1 -5 35.58 2.99
1 1 -5 37.29 2.99
1 1 -5 34.45 3.00
1 1 -5 32.69 3.10
1 1 -5 40.85 3.19
1 1 -5 33.39 2.86
1 1 -5 33.40 3.05
1 1 -5 36.97 3.13
1 1 -5 34.68 3.03
1 1 -5 39.78 2.83
1 1 -5 35.35 2.84
1 1 -5 35.08 2.83
1 1 -5 31.04 2.97
1 1 -5 42.66 3.22
1 1 -5 38.66 2.96
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-1 -1 5 35.10 3.10
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0 1 -5 332.10 23.94
0 1 -5 316.02 24.70
0 1 -5 315.58 25.13
0 1 -5 374.65 24.10
0 1 -5 315.75 25.60
0 1 -5 309.08 24.47
0 1 -5 323.09 26.01
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0 1 -5 287.23 25.52
0 1 -5 319.80 23.97
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0 -1 5 333.62 24.49
0 -1 5 332.58 24.72
0 -1 5 341.15 24.78
0 -1 5 387.86 24.75
0 -1 5 373.44 25.57
0 -1 5 319.58 24.47
0 -1 5 358.80 25.16
0 -1 5 350.85 24.00
0 -1 5 377.25 24.74
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1 -1 5 2.59 0.57
1 -1 5 1.77 0.45
1 -1 5 1.72 0.51
1 -1 5 2.10 0.48
1 -1 5 2.07 0.43
1 -1 5 1.87 0.50
1 -1 5 2.24 0.47
1 -1 5 1.70 0.40
1 -1 5 2.57 0.46
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2 -1 5 1.34 0.42
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3 -1 5 84.93 6.35
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1 4 -7 44.56 3.48
1 4 -7 39.16 3.53
1 4 -7 39.25 3.40
1 4 -7 38.19 3.56
1 4 -7 40.88 3.64
1 4 -7 40.06 3.38
1 4 -7 40.86 3.26
1 4 -7 44.26 3.49
1 4 -7 37.92 3.20
1 4 -7 38.83 3.53
1 4 -7 37.90 3.41
1 4 -7 37.77 3.62
1 4 -7 37.84 3.26
1 4 -7 44.23 3.25
1 4 -7 39.71 3.63
-1 -4 7 39.19 3.46
-1 -4 7 31.96 3.25
-1 -4 7 45.48 3.54
-1 -4 7 36.73 3.25
-1 -4 7 39.03 3.44
-1 -4 7 37.60 3.27
-1 -4 7 36.79 3.39
-1 -4 7 38.80 3.56
-1 -4 7 44.73 3.49
-1 -4 7 34.69 3.38
-1 -4 7 37.92 3.23
-1 -4 7 42.59 3.65
0 4 -7 3.22 0.78
0 4 -7 3.23 0.85
0 4 -7 3.40 0.76
0 4 -7 3.08 0.68
0 4 -7 4.03 0.78
0 4 -7 3.69 0.72
0 4 -7 3.78 0.91
0 4 -7 2.71 0.78
0 4 -7 4.19 0.78
0 4 -7 3.94 0.73
0 4 -7 4.21 0.80
0 4 -7 3.95 0.80
0 4 -7 3.57 0.79
0 4 -7 4.11 0.88
0 4 -7 3.84 0.79
0 -4 7 3.39 0.79
0 -4 7 5.99 0.89
0 -4 7 3.98 0.77
0 -4 7 2.97 0.68
0 -4 7 2.69 0.83
0 -4 7 4.36 0.78
0 -4 7 4.13 0.92
0 -4 7 3.08 0.76
0 -4 7 3.69 0.70
0 -4 7 2.92 0.79
0 -4 7 3.84 0.69
0 -4 7 4.58 0.81
0 -4 7 3.30 0.70
-1 4 -7 54.45 4.40
-1 4 -7 55.48 4.84
-1 4 -7 49.12 4.50
-1 4 -7 54.93 4.39
-1 4 -7 54.15 4.64
-1 4 -7 54.12 4.59
-1 4 -7 54.26 4.61
-1 4 -7 62.19 4.49
-1 4 -7 54.22 4.80
-1 4 -7 58.93 4.84
-1 4 -7 57.19 4.71
-1 4 -7 61.23 4.70
-1 4 -7 53.84 4.81
-1 4 -7 60.09 4.88
1 -4 7 54.58 4.80
1 -4 7 55.45 4.37
1 -4 7 53.91 4.59
1 -4 7 52.50 4.57
1 -4 7 54.15 4.34
1 -4 7 57.71 4.87
1 -4 7 51.02 4.56
1 -4 7 59.20 4.52
1 -4 7 50.23 4.56
1 -4 7 59.62 4.59
1 -4 7 55.82 4.61
1 -4 7 56.58 4.40
-2 4 -7 143.71 10.70
-2 4 -7 142.29 10.87
-2 4 -7 136.95 10.72
-2 4 -7 145.14 10.35
-2 4 -7 120.47 11.02
-2 4 -7 158.26 10.78
-2 4 -7 122.33 10.26
-2 4 -7 137.27 10.67
-2 4 -7 135.57 10.54
-2 4 -7 134.79 11.08
-2 4 -7 115.98 11.20
-2 4 -7 139.37 11.07
-2 4 -7 124.85 10.90
2 -4 7 158.14 10.71
2 -4 7 139.56 11.11
2 -4 7 130.93 10.07
2 -4 7 131.57 10.46
2 -4 7 137.44 10.07
2 -4 7 151.05 10.19
2 -4 7 155.98 11.19
-3 4 -7 3.79 0.93
-3 4 -7 5.76 1.03
-3 4 -7 5.45 0.89
-3 4 -7 4.44 0.98
-3 4 -7 4.73 0.90
-3 4 -7 5.72 0.96
-3 4 -7 4.41 0.95
-3 4 -7 3.99 0.88
3 -4 7 6.22 0.86
3 -4 7 6.67 1.12
3 -4 7 4.90 1.05
-4 4 -7 5.46 0.99
-4 4 -7 3.60 0.78
-4 4 -7 3.67 0.88
-4 4 -7 4.40 0.94
-4 4 -7 4.69 0.93
-4 4 -7 4.07 0.96
-4 4 -7 5.44 1.09
4 -4 7 3.60 0.95
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-5 4 -7 46.47 3.84
-5 4 -7 41.08 3.84
-5 4 -7 47.39 4.29
-6 4 -7 29.33 3.36
-6 4 -7 39.45 3.30
-6 4 -7 38.84 3.32
-7 4 -7 2.39 0.77
8 3 -7 47.21 4.02
8 3 -7 36.55 3.52
-8 -3 7 45.63 3.73
7 3 -7 2.63 0.90
7 3 -7 2.38 0.66
-7 -3 7 0.63 0.75
-7 -3 7 2.47 0.71
-7 -3 7 2.49 0.75
6 3 -7 1.08 0.57
6 3 -7 -0.68 0.57
-6 -3 7 -0.15 0.46
-6 -3 7 0.79 0.66
-6 -3 7 1.03 0.59
-6 -3 7 0.57 0.50
-6 -3 7 -0.16 0.61
5 3 -7 59.61 5.13
5 3 -7 69.44 5.22
5 3 -7 51.98 5.03
5 3 -7 65.66 4.79
-5 -3 7 60.51 4.80
-5 -3 7 55.59 5.09
-5 -3 7 47.49 4.84
-5 -3 7 55.58 4.94
-5 -3 7 64.29 4.75
-5 -3 7 58.73 4.68
4 3 -7 23.11 2.17
4 3 -7 19.08 1.83
4 3 -7 15.92 1.93
4 3 -7 20.07 2.11
4 3 -7 19.18 1.67
-4 -3 7 16.67 1.95
-4 -3 7 19.75 1.89
-4 -3 7 21.16 1.92
-4 -3 7 18.82 2.00
-4 -3 7 18.62 1.84
-4 -3 7 17.82 1.83
-4 -3 7 20.94 1.86
-4 -3 7 19.02 2.06
3 3 -7 23.18 2.23
3 3 -7 20.63 2.00
3 3 -7 19.45 1.88
3 3 -7 19.69 1.93
3 3 -7 23.13 2.12
3 3 -7 20.79 2.19
3 3 -7 21.78 1.95
3 3 -7 21.33 2.11
3 3 -7 23.65 2.00
-3 -3 7 20.92 2.03
-3 -3 7 18.58 2.02
-3 -3 7 20.06 2.03
-3 -3 7 19.51 1.93
-3 -3 7 18.42 1.91
-3 -3 7 19.35 1.92
-3 -3 7 20.87 1.92
-3 -3 7 19.32 1.92
-3 -3 7 22.59 2.20
-3 -3 7 19.26 2.03
-3 -3 7 19.71 2.13
-3 -3 7 23.52 2.10
2 3 -7 21.30 2.39
2 3 -7 21.88 2.23
2 3 -7 25.47 2.49
2 3 -7 28.60 2.02
2 3 -7 27.87 2.36
2 3 -7 23.87 2.23
2 3 -7 24.83 2.30
2 3 -7 24.85 2.13
2 3 -7 23.79 2.32
2 3 -7 28.23 2.24
2 3 -7 25.30 2.52
2 3 -7 21.80 2.24
2 3 -7 20.06 2.27
2 3 -7 23.82 2.00
2 3 -7 24.10 2.09
-2 -3 7 23.77 2.21
-2 -3 7 29.86 2.28
-2 -3 7 25.04 2.37
-2 -3 7 24.84 2.22
-2 -3 7 28.61 2.40
-2 -3 7 26.60 2.50
-2 -3 7 22.94 2.25
-2 -3 7 27.37 2.48
-2 -3 7 24.73 2.26
-2 -3 7 26.02 2.34
-2 -3 7 26.25 2.38
-2 -3 7 26.17 2.49
-2 -3 7 27.60 2.39
1 3 -7 132.94 11.11
1 3 -7 128.24 11.13
1 3 -7 119.36 11.02
1 3 -7 130.74 10.48
1 3 -7 139.98 10.23
1 3 -7 143.21 11.04
1 3 -7 150.09 10.32
1 3 -7 143.98 10.25
1 3 -7 139.64 10.66
1 3 -7 125.97 10.59
1 3 -7 147.48 11.08
1 3 -7 143.19 10.26
1 3 -7 156.19 11.05
1 3 -7 141.71 10.80
1 3 -7 136.14 10.89
-1 -3 7 129.99 10.99
-1 -3 7 143.53 10.53
-1 -3 7 146.82 11.12
-1 -3 7 140.44 10.82
-1 -3 7 135.38 10.30
-1 -3 7 131.35 10.66
-1 -3 7 145.65 10.31
-1 -3 7 119.08 10.60
-1 -3 7 150.75 11.12
-1 -3 7 128.08 10.62
-1 -3 7 130.78 10.63
-1 -3 7 150.83 11.11
-1 -3 7 135.55 10.32
0 3 -7 -0.22 0.43
0 3 -7 0.43 0.46
0 3 -7 -0.11 0.35
0 3 -7 1.17 0.43
0 3 -7 0.06 0.40
0 3 -7 0.45 0.35
0 3 -7 0.26 0.41
0 3 -7 0.49 0.43
0 3 -7 -0.03 0.44
0 3 -7 0.23 0.45
0 3 -7 0.65 0.42
0 3 -7 -0.05 0.32
0 3 -7 0.91 0.45
0 3 -7 0.15 0.37
0 3 -7 0.00 0.52
0 3 -7 0.41 0.45
0 -3 7 0.70 0.43
0 -3 7 -0.23 0.44
0 -3 7 0.36 0.41
0 -3 7 -0.11 0.41
0 -3 7 0.98 0.51
0 -3 7 0.39 0.43
0 -3 7 0.07 0.36
0 -3 7 0.16 0.45
0 -3 7 0.04 0.33
0 -3 7 -0.40 0.50
0 -3 7 0.16 0.37
0 -3 7 0.34 0.42
-1 3 -7 1.04 0.51
-1 3 -7 2.03 0.67
-1 3 -7 1.72 0.68
-1 3 -7 1.30 0.54
-1 3 -7 1.34 0.59
-1 3 -7 1.35 0.56
-1 3 -7 1.49 0.58
-1 3 -7 1.16 0.48
-1 3 -7 1.88 0.70
-1 3 -7 1.60 0.58
-1 3 -7 1.62 0.57
-1 3 -7 1.98 0.58
-1 3 -7 1.45 0.58
-1 3 -7 1.08 0.47
1 -3 7 1.58 0.48
1 -3 7 1.25 0.53
1 -3 7 1.22 0.61
1 -3 7 1.19 0.64
1 -3 7 1.73 0.61
1 -3 7 1.58 0.52
1 -3 7 1.35 0.61
1 -3 7 1.69 0.51
1 -3 7 1.42 0.57
1 -3 7 0.84 0.45
1 -3 7 2.10 0.60
-2 3 -7 57.62 4.98
-2 3 -7 60.46 5.09
-2 3 -7 63.00 5.35
-2 3 -7 56.26 5.06
-2 3 -7 56.78 5.26
-2 3 -7 64.12 5.18
-2 3 -7 57.16 5.02
-2 3 -7 64.40 5.34
-2 3 -7 66.43 5.29
-2 3 -7 56.60 4.81
-2 3 -7 70.23 5.35
-2 3 -7 66.35 5.10
-2 3 -7 67.76 5.23
2 -3 7 72.90 5.40
2 -3 7 64.72 4.84
2 -3 7 59.35 5.29
2 -3 7 59.43 5.05
2 -3 7 60.06 5.05
2 -3 7 61.23 4.93
2 -3 7 63.26 5.02
2 -3 7 59.54 4.74
2 -3 7 60.81 5.01
2 -3 7 61.59 4.66
-3 3 -7 96.63 6.83
-3 3 -7 79.30 6.65
-3 3 -7 85.89 6.56
-3 3 -7 84.13 7.08
-3 3 -7 94.03 6.85
-3 3 -7 76.51 6.85
-3 3 -7 86.46 6.50
-3 3 -7 82.72 6.93
-3 3 -7 76.88 7.14
-3 3 -7 87.12 6.81
3 -3 7 89.39 6.74
3 -3 7 89.33 7.06
3 -3 7 86.90 7.11
3 -3 7 72.56 6.65
-4 3 -7 10.35 1.36
-4 3 -7 7.63 1.19
-4 3 -7 7.97 1.29
-4 3 -7 7.05 1.10
-4 3 -7 7.02 1.17
-4 3 -7 8.33 1.07
-4 3 -7 7.56 1.14
-5 3 -7 7.18 1.11
-5 3 -7 7.49 1.26
-5 3 -7 6.98 1.31
-5 3 -7 6.51 1.12
-6 3 -7 78.38 6.10
-6 3 -7 71.60 6.12
-6 3 -7 73.60 6.41
-7 3 -7 5.85 1.14
8 2 -7 55.60 4.59
-8 -2 7 47.64 4.27
-8 -2 7 49.51 4.26
7 2 -7 11.14 1.26
7 2 -7 11.33 1.56
7 2 -7 10.95 1.64
-7 -2 7 14.42 1.58
-7 -2 7 10.79 1.55
-7 -2 7 13.41 1.43
-7 -2 7 12.29 1.41
-7 -2 7 12.17 1.47
6 2 -7 14.59 1.64
6 2 -7 11.97 1.52
6 2 -7 11.52 1.31
-6 -2 7 13.48 1.38
-6 -2 7 10.23 1.33
-6 -2 7 8.76 1.41
-6 -2 7 10.74 1.27
-6 -2 7 13.82 1.37
-6 -2 7 10.98 1.41
-6 -2 7 11.22 1.42
5 2 -7 25.77 1.94
5 2 -7 20.00 2.22
5 2 -7 25.55 2.36
5 2 -7 18.61 2.13
-5 -2 7 24.98 2.14
-5 -2 7 21.31 2.26
-5 -2 7 22.25 2.20
-5 -2 7 22.42 2.21
-5 -2 7 21.61 2.07
-5 -2 7 22.50 2.02
-5 -2 7 21.26 2.16
-5 -2 7 21.33 2.03
4 2 -7 124.46 10.07
4 2 -7 116.03 9.72
4 2 -7 117.99 9.53
4 2 -7 119.93 10.04
4 2 -7 114.53 10.07
4 2 -7 131.59 9.94
-4 -2 7 123.16 9.71
-4 -2 7 123.33 9.69
-4 -2 7 143.20 10.09
-4 -2 7 126.51 9.32
-4 -2 7 130.23 9.94
-4 -2 7 136.96 9.36
-4 -2 7 120.66 9.38
-4 -2 7 122.94 9.70
-4 -2 7 111.11 9.97
-4 -2 7 138.63 9.38
-4 -2 7 130.53 9.74
-4 -2 7 115.85 9.51
-4 -2 7 127.34 9.85
3 2 -7 24.02 2.34
3 2 -7 26.77 2.56
3 2 -7 25.68 2.34
3 2 -7 27.64 2.29
3 2 -7 25.00 2.51
3 2 -7 29.52 2.28
3 2 -7 23.34 2.25
3 2 -7 24.74 2.43
3 2 -7 31.06 2.56
-3 -2 7 24.36 2.34
-3 -2 7 24.91 2.24
-3 -2 7 23.18 2.26
-3 -2 7 26.01 2.25
-3 -2 7 27.84 2.34
-3 -2 7 26.97 2.27
-3 -2 7 26.63 2.50
-3 -2 7 28.24 2.44
-3 -2 7 25.03 2.35
-3 -2 7 29.77 2.48
-3 -2 7 27.78 2.54
-3 -2 7 24.98 2.50
-3 -2 7 26.16 2.38
-3 -2 7 25.33 2.41
2 2 -7 4.02 0.64
2 2 -7 5.36 0.78
2 2 -7 4.22 0.63
2 2 -7 3.72 0.57
2 2 -7 4.23 0.80
2 2 -7 4.64 0.73
2 2 -7 4.45 0.91
2 2 -7 4.36 0.72
2 2 -7 5.76 0.79
2 2 -7 4.04 0.65
2 2 -7 3.67 0.72
2 2 -7 4.36 0.70
2 2 -7 4.61 0.48
2 2 -7 4.02 0.86
-2 -2 7 3.52 0.82
-2 -2 7 4.24 0.83
-2 -2 7 5.33 0.84
-2 -2 7 4.21 0.69
-2 -2 7 4.80 0.78
-2 -2 7 4.43 0.75
-2 -2 7 3.89 0.70
-2 -2 7 4.21 0.81
-2 -2 7 3.89 0.67
-2 -2 7 5.03 0.75
-2 -2 7 4.43 0.81
-2 -2 7 4.29 0.88
-2 -2 7 3.85 0.73
-2 -2 7 3.93 0.78
1 2 -7 172.90 12.40
1 2 -7 151.81 11.54
1 2 -7 140.91 12.37
1 2 -7 164.38 12.45
1 2 -7 152.31 11.93
1 2 -7 152.57 12.46
1 2 -7 141.55 11.48
1 2 -7 156.29 11.49
1 2 -7 169.53 11.49
1 2 -7 130.99 12.03
1 2 -7 166.99 12.37
1 2 -7 153.12 11.48
1 2 -7 168.31 11.94
1 2 -7 154.15 11.92
1 2 -7 143.93 12.18
1 2 -7 154.44 12.41
-1 -2 7 170.35 12.43
-1 -2 7 183.48 11.99
-1 -2 7 148.42 11.94
-1 -2 7 161.50 11.95
-1 -2 7 133.28 11.52
-1 -2 7 139.76 11.76
-1 -2 7 175.58 11.97
-1 -2 7 155.91 12.35
-1 -2 7 163.23 12.41
-1 -2 7 153.06 12.13
-1 -2 7 162.78 11.54
0 2 -7 35.17 2.75
0 2 -7 30.09 2.86
0 2 -7 34.07 2.92
0 2 -7 35.79 3.10
0 2 -7 30.65 2.89
0 2 -7 29.45 2.96
0 2 -7 31.27 2.90
0 2 -7 33.16 3.06
0 2 -7 34.88 2.83
0 2 -7 38.47 2.72
0 2 -7 32.15 2.87
0 2 -7 28.63 2.80
0 2 -7 32.37 2.71
0 2 -7 32.56 3.00
0 -2 7 30.53 2.78
0 -2 7 41.12 2.81
0 -2 7 30.16 2.86
0 -2 7 35.89 2.90
0 -2 7 32.06 2.84
0 -2 7 31.13 2.88
0 -2 7 34.77 2.90
0 -2 7 34.04 3.02
0 -2 7 28.78 2.80
0 -2 7 32.49 2.74
0 -2 7 31.55 2.71
0 -2 7 35.60 3.04
-1 2 -7 48.93 4.10
-1 2 -7 51.35 4.07
-1 2 -7 47.79 3.88
-1 2 -7 40.71 4.23
-1 2 -7 53.28 4.22
-1 2 -7 45.07 4.04
-1 2 -7 60.36 4.44
-1 2 -7 56.79 3.97
-1 2 -7 52.22 3.94
-1 2 -7 48.53 4.26
-1 2 -7 46.99 4.17
-1 2 -7 38.47 4.02
-1 2 -7 48.45 4.25
-1 2 -7 47.46 4.11
1 -2 7 44.92 4.11
1 -2 7 53.50 3.95
1 -2 7 58.42 3.97
1 -2 7 44.81 3.87
1 -2 7 57.25 4.40
1 -2 7 40.07 4.00
1 -2 7 50.78 4.31
1 -2 7 57.39 4.15
1 -2 7 53.19 4.30
1 -2 7 52.93 4.05
1 -2 7 44.88 4.08
-2 2 -7 6.98 0.97
-2 2 -7 4.46 0.87
-2 2 -7 4.58 0.99
-2 2 -7 7.79 1.13
-2 2 -7 5.62 0.91
-2 2 -7 6.36 0.92
-2 2 -7 5.88 0.82
-2 2 -7 5.83 0.99
-2 2 -7 5.47 0.88
-2 2 -7 5.55 0.94
-2 2 -7 6.63 1.05
-2 2 -7 5.13 0.89
-2 2 -7 5.56 0.83
2 -2 7 4.85 0.74
2 -2 7 5.98 0.88
2 -2 7 5.42 0.83
2 -2 7 4.26 0.80
2 -2 7 6.20 0.90
2 -2 7 6.74 1.08
2 -2 7 5.50 0.76
2 -2 7 4.46 0.95
2 -2 7 4.95 0.86
2 -2 7 3.84 0.75
2 -2 7 6.00 0.83
-3 2 -7 148.97 12.04
-3 2 -7 151.82 12.26
-3 2 -7 134.12 11.64
-3 2 -7 168.84 11.89
-3 2 -7 162.37 11.49
-3 2 -7 153.58 12.23
-3 2 -7 152.05 11.84
-3 2 -7 134.13 12.45
-3 2 -7 151.16 12.31
-3 2 -7 166.99 11.92
-3 2 -7 158.88 12.13
-3 2 -7 162.50 11.46
-3 2 -7 148.68 11.80
3 -2 7 168.30 12.38
3 -2 7 172.67 11.82
3 -2 7 142.78 11.86
3 -2 7 138.35 11.22
-4 2 -7 1.44 0.67
-4 2 -7 0.45 0.59
-4 2 -7 1.25 0.58
-4 2 -7 1.15 0.64
-4 2 -7 1.35 0.65
-4 2 -7 1.58 0.63
-4 2 -7 1.98 0.67
4 -2 7 1.50 0.52
-5 2 -7 0.33 0.58
-5 2 -7 -0.16 0.62
-5 2 -7 0.18 0.47
-5 2 -7 0.29 0.59
-6 2 -7 45.56 3.76
-6 2 -7 42.12 3.94
-6 2 -7 38.10 3.72
-7 2 -7 11.78 1.61
8 1 -7 41.86 4.23
8 1 -7 55.60 4.29
-8 -1 7 48.47 4.01
-8 -1 7 46.71 4.00
7 1 -7 52.02 4.22
7 1 -7 42.58 3.83
7 1 -7 50.09 4.23
-7 -1 7 51.23 3.96
-7 -1 7 49.75 3.87
-7 -1 7 49.83 3.82
-7 -1 7 45.33 4.03
-7 -1 7 49.15 3.93
-7 -1 7 43.85 4.16
6 1 -7 12.98 1.34
6 1 -7 13.29 1.55
6 1 -7 15.38 1.64
-6 -1 7 10.62 1.42
-6 -1 7 10.46 1.37
-6 -1 7 14.89 1.37
-6 -1 7 15.48 1.57
-6 -1 7 13.53 1.41
-6 -1 7 14.21 1.37
-6 -1 7 13.20 1.42
-6 -1 7 12.40 1.53
5 1 -7 0.08 0.38
5 1 -7 0.31 0.49
5 1 -7 0.76 0.60
5 1 -7 0.21 0.24
-5 -1 7 0.19 0.45
-5 -1 7 0.31 0.38
-5 -1 7 0.41 0.37
-5 -1 7 1.22 0.54
-5 -1 7 -0.16 0.33
-5 -1 7 -0.20 0.41
-5 -1 7 1.23 0.57
-5 -1 7 0.84 0.54
-5 -1 7 0.00 0.42
-5 -1 7 0.54 0.37
4 1 -7 200.86 16.68
4 1 -7 223.05 17.19
4 1 -7 216.89 17.06
4 1 -7 236.28 16.34
4 1 -7 257.08 17.16
4 1 -7 230.82 16.90
-4 -1 7 179.15 16.43
-4 -1 7 190.94 16.70
-4 -1 7 230.44 16.00
-4 -1 7 218.10 15.93
-4 -1 7 207.33 16.27
-4 -1 7 221.57 17.02
-4 -1 7 209.28 16.44
-4 -1 7 238.44 16.54
-4 -1 7 214.80 16.47
-4 -1 7 216.42 15.93
-4 -1 7 204.45 15.93
-4 -1 7 227.26 17.05
3 1 -7 4.72 0.69
3 1 -7 4.57 0.72
3 1 -7 4.16 0.83
3 1 -7 2.13 0.51
3 1 -7 3.40 0.50
3 1 -7 3.70 0.71
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2 5 -8 9.96 1.28
2 5 -8 7.32 0.98
2 5 -8 8.74 1.27
-2 -5 8 10.24 1.42
-2 -5 8 9.55 1.48
-2 -5 8 8.86 1.37
-2 -5 8 10.67 1.42
-2 -5 8 11.69 1.36
1 5 -8 40.37 3.25
1 5 -8 29.78 2.88
1 5 -8 31.96 3.22
1 5 -8 38.99 3.19
1 5 -8 30.65 3.10
1 5 -8 35.85 2.97
-1 -5 8 37.97 3.23
-1 -5 8 36.88 3.10
-1 -5 8 34.81 3.18
-1 -5 8 30.93 3.17
-1 -5 8 33.18 3.30
0 5 -8 106.00 8.60
0 5 -8 118.32 8.51
0 5 -8 106.85 8.77
0 5 -8 108.22 8.48
0 5 -8 108.24 8.87
0 5 -8 91.20 8.02
0 5 -8 106.17 8.32
0 -5 8 100.10 8.44
0 -5 8 106.17 8.40
0 -5 8 112.56 8.31
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-1 5 -8 -0.26 0.49
-1 5 -8 0.34 0.57
-1 5 -8 -0.13 0.49
-1 5 -8 -0.25 0.54
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1 -5 8 0.00 0.36
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-2 5 -8 1.92 0.76
-2 5 -8 1.54 0.74
-2 5 -8 1.38 0.72
-2 5 -8 1.53 0.70
2 -5 8 2.11 0.74
2 -5 8 1.68 0.35
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-3 5 -8 34.07 3.42
-3 5 -8 37.53 3.39
-3 5 -8 39.03 3.31
-3 5 -8 35.37 3.56
-3 5 -8 34.57 3.47
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-4 5 -8 0.14 0.66
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7 4 -8 47.61 4.50
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6 4 -8 0.97 0.45
6 4 -8 0.32 0.61
6 4 -8 0.83 0.77
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-6 -4 8 0.90 0.58
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5 4 -8 7.86 1.36
5 4 -8 5.65 1.13
5 4 -8 7.41 1.00
-5 -4 8 5.70 1.27
-5 -4 8 6.80 1.11
-5 -4 8 7.20 1.27
4 4 -8 83.61 6.01
4 4 -8 64.59 6.16
4 4 -8 76.88 6.32
-4 -4 8 65.87 5.81
-4 -4 8 61.87 5.93
-4 -4 8 83.11 6.33
3 4 -8 27.13 2.92
3 4 -8 35.13 3.01
3 4 -8 37.02 2.94
3 4 -8 33.00 3.16
3 4 -8 40.52 3.37
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-3 -4 8 28.89 3.12
-3 -4 8 32.26 3.08
-3 -4 8 34.31 2.94
2 4 -8 1.90 0.82
2 4 -8 1.22 0.60
2 4 -8 0.41 0.39
2 4 -8 0.64 0.55
2 4 -8 1.46 0.56
2 4 -8 1.20 0.57
2 4 -8 0.77 0.54
2 4 -8 0.23 0.53
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-2 -4 8 0.22 0.62
-2 -4 8 0.46 0.48
-2 -4 8 0.53 0.62
-2 -4 8 1.40 0.70
1 4 -8 2.52 0.75
1 4 -8 4.15 0.72
1 4 -8 3.38 0.83
1 4 -8 4.21 0.72
1 4 -8 3.37 0.87
1 4 -8 1.83 0.75
1 4 -8 2.75 0.77
1 4 -8 2.60 0.75
1 4 -8 3.09 0.81
1 4 -8 3.39 0.91
1 4 -8 2.03 0.79
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-1 -4 8 2.73 0.69
-1 -4 8 3.05 0.85
-1 -4 8 3.26 0.87
-1 -4 8 3.65 0.85
-1 -4 8 3.19 0.82
0 4 -8 119.11 8.62
0 4 -8 103.99 8.86
0 4 -8 120.06 8.48
0 4 -8 107.59 8.68
0 4 -8 107.11 8.77
0 4 -8 105.56 8.19
0 4 -8 106.44 8.88
0 4 -8 105.69 8.58
0 4 -8 104.45 8.21
0 4 -8 95.91 8.89
0 -4 8 101.20 8.54
0 -4 8 109.36 8.69
0 -4 8 104.61 8.57
0 -4 8 127.06 8.60
0 -4 8 112.66 8.59
0 -4 8 106.93 8.41
-1 4 -8 1.43 0.77
-1 4 -8 0.70 0.56
-1 4 -8 1.26 0.56
-1 4 -8 0.46 0.55
-1 4 -8 0.31 0.51
-1 4 -8 1.40 0.54
-1 4 -8 1.14 0.60
-1 4 -8 0.95 0.67
-1 4 -8 0.91 0.60
1 -4 8 0.46 0.59
1 -4 8 0.63 0.58
1 -4 8 0.78 0.56
1 -4 8 0.40 0.49
1 -4 8 0.68 0.61
1 -4 8 1.59 0.69
1 -4 8 2.14 0.92
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-2 4 -8 11.89 1.48
-2 4 -8 10.45 1.43
-2 4 -8 10.04 1.23
-2 4 -8 8.59 1.32
-2 4 -8 9.26 1.29
-2 4 -8 9.44 1.37
-2 4 -8 9.25 1.38
2 -4 8 10.33 1.14
2 -4 8 9.30 0.97
2 -4 8 11.33 1.53
2 -4 8 11.21 1.33
-3 4 -8 99.07 7.31
-3 4 -8 87.90 7.43
-3 4 -8 80.38 7.21
-3 4 -8 83.26 6.94
-3 4 -8 96.51 7.62
-3 4 -8 83.40 7.67
-3 4 -8 93.79 7.19
3 -4 8 98.32 7.65
3 -4 8 90.68 7.17
-4 4 -8 59.74 4.56
-4 4 -8 48.75 4.95
-4 4 -8 53.93 4.88
-4 4 -8 53.60 4.75
-4 4 -8 56.59 5.13
-4 4 -8 53.32 4.70
4 -4 8 64.77 5.07
-5 4 -8 11.05 1.43
-5 4 -8 6.70 1.37
-6 4 -8 0.76 0.66
8 3 -8 1.52 0.56
7 3 -8 57.60 5.23
7 3 -8 69.90 5.60
-7 -3 8 61.24 5.17
6 3 -8 15.55 1.82
6 3 -8 12.08 1.52
-6 -3 8 12.06 1.51
-6 -3 8 14.01 1.77
-6 -3 8 14.66 1.73
-6 -3 8 10.68 1.41
5 3 -8 30.65 2.62
5 3 -8 23.63 2.80
5 3 -8 34.16 3.11
-5 -3 8 36.19 2.80
-5 -3 8 24.84 2.63
-5 -3 8 32.56 2.80
-5 -3 8 30.87 2.90
-5 -3 8 30.16 2.96
4 3 -8 18.88 2.10
4 3 -8 16.07 1.78
4 3 -8 19.77 2.03
-4 -3 8 18.05 1.82
-4 -3 8 20.46 2.06
-4 -3 8 21.10 1.90
-4 -3 8 16.53 2.02
-4 -3 8 19.30 1.87
-4 -3 8 16.24 1.94
3 3 -8 89.39 6.15
3 3 -8 75.29 6.49
3 3 -8 64.81 6.18
3 3 -8 63.24 6.37
3 3 -8 82.07 6.30
3 3 -8 78.12 6.51
-3 -3 8 73.85 6.08
-3 -3 8 85.49 6.29
-3 -3 8 82.41 6.00
-3 -3 8 77.49 5.99
-3 -3 8 80.89 6.26
-3 -3 8 67.12 6.17
-3 -3 8 72.35 6.40
-3 -3 8 78.63 6.30
2 3 -8 1.90 0.65
2 3 -8 1.99 0.76
2 3 -8 3.99 0.76
2 3 -8 2.64 0.66
2 3 -8 1.85 0.60
2 3 -8 3.65 0.73
2 3 -8 2.40 0.46
2 3 -8 2.39 0.64
2 3 -8 2.35 0.70
2 3 -8 2.25 0.60
2 3 -8 3.43 0.88
-2 -3 8 2.35 0.74
-2 -3 8 1.76 0.72
-2 -3 8 3.00 0.70
-2 -3 8 2.13 0.51
-2 -3 8 1.75 0.72
-2 -3 8 2.50 0.71
-2 -3 8 2.69 0.69
-2 -3 8 2.80 0.77
-2 -3 8 3.00 0.69
1 3 -8 13.93 1.66
1 3 -8 17.44 1.62
1 3 -8 12.53 1.57
1 3 -8 17.39 1.67
1 3 -8 10.95 1.62
1 3 -8 15.25 1.45
1 3 -8 16.83 1.47
1 3 -8 15.03 1.55
1 3 -8 13.48 1.73
1 3 -8 15.50 1.66
1 3 -8 13.49 1.54
1 3 -8 11.09 1.41
1 3 -8 14.64 1.61
1 3 -8 15.94 1.55
1 3 -8 14.59 1.80
-1 -3 8 17.29 1.66
-1 -3 8 15.02 1.60
-1 -3 8 15.30 1.75
-1 -3 8 11.94 1.65
-1 -3 8 15.70 1.54
-1 -3 8 11.91 1.58
-1 -3 8 15.65 1.77
-1 -3 8 16.16 1.60
-1 -3 8 14.87 1.56
-1 -3 8 13.68 1.61
-1 -3 8 16.49 1.58
-1 -3 8 13.27 1.57
0 3 -8 135.33 9.76
0 3 -8 141.60 10.49
0 3 -8 120.22 10.48
0 3 -8 124.12 10.50
0 3 -8 128.05 9.65
0 3 -8 142.30 9.98
0 3 -8 133.36 10.46
0 3 -8 140.86 10.10
0 3 -8 123.37 10.04
0 3 -8 123.47 10.49
0 3 -8 136.78 10.12
0 3 -8 140.04 10.28
0 3 -8 148.84 10.37
0 3 -8 117.67 9.64
0 3 -8 118.39 9.64
0 -3 8 123.88 9.68
0 -3 8 120.96 10.05
0 -3 8 148.93 10.13
0 -3 8 136.73 10.53
0 -3 8 121.34 9.70
0 -3 8 114.51 10.16
0 -3 8 127.79 10.03
0 -3 8 136.68 9.72
0 -3 8 126.65 9.91
0 -3 8 127.68 10.44
0 -3 8 123.56 10.08
0 -3 8 117.78 10.03
-1 3 -8 32.76 3.06
-1 3 -8 31.46 3.21
-1 3 -8 35.90 3.18
-1 3 -8 28.02 2.92
-1 3 -8 32.92 2.90
-1 3 -8 38.43 3.19
-1 3 -8 33.44 3.04
-1 3 -8 40.31 3.22
-1 3 -8 30.26 3.07
-1 3 -8 33.58 3.23
-1 3 -8 34.99 2.88
1 -3 8 38.65 2.91
1 -3 8 30.77 3.03
1 -3 8 34.15 3.03
1 -3 8 34.92 3.07
1 -3 8 37.34 3.02
1 -3 8 35.61 2.91
1 -3 8 34.57 3.04
1 -3 8 30.50 3.23
-2 3 -8 19.90 2.19
-2 3 -8 22.44 2.18
-2 3 -8 28.43 2.36
-2 3 -8 23.62 2.29
-2 3 -8 21.11 2.01
-2 3 -8 24.12 2.20
-2 3 -8 24.99 2.34
-2 3 -8 20.06 2.31
2 -3 8 19.15 2.13
2 -3 8 20.41 2.31
2 -3 8 20.60 2.06
2 -3 8 20.13 1.94
2 -3 8 22.76 2.15
-3 3 -8 16.29 1.73
-3 3 -8 12.14 1.73
-3 3 -8 15.14 1.72
-3 3 -8 14.99 1.75
-3 3 -8 14.97 1.75
-3 3 -8 17.63 1.93
-3 3 -8 13.45 1.51
3 -3 8 14.45 1.80
-4 3 -8 85.54 7.42
-4 3 -8 82.26 7.23
-4 3 -8 87.10 7.13
-4 3 -8 84.63 6.68
-4 3 -8 94.02 7.03
-4 3 -8 81.04 6.85
-5 3 -8 0.33 0.65
-5 3 -8 -0.41 0.49
-6 3 -8 3.23 0.91
-7 3 -8 31.14 3.07
-8 -2 8 5.95 1.07
7 2 -8 14.89 1.52
7 2 -8 11.93 1.78
-7 -2 8 15.56 1.65
-7 -2 8 15.90 1.68
6 2 -8 25.76 2.82
6 2 -8 35.34 3.14
6 2 -8 31.95 3.08
-6 -2 8 31.43 2.74
-6 -2 8 35.07 2.86
-6 -2 8 32.48 3.06
-6 -2 8 28.40 2.78
-6 -2 8 33.95 3.01
5 2 -8 1.21 0.59
5 2 -8 1.73 0.81
5 2 -8 0.87 0.72
5 2 -8 0.79 0.38
-5 -2 8 0.15 0.45
-5 -2 8 1.61 0.55
-5 -2 8 0.62 0.45
-5 -2 8 0.37 0.57
-5 -2 8 0.69 0.62
-5 -2 8 0.52 0.51
-5 -2 8 0.87 0.55
4 2 -8 -0.65 0.35
4 2 -8 0.47 0.40
4 2 -8 0.69 0.69
4 2 -8 0.41 0.55
-4 -2 8 0.45 0.46
-4 -2 8 -0.19 0.40
-4 -2 8 -0.31 0.50
-4 -2 8 0.41 0.50
-4 -2 8 -0.23 0.49
-4 -2 8 0.23 0.48
-4 -2 8 -0.02 0.53
-4 -2 8 0.39 0.40
3 2 -8 62.31 5.33
3 2 -8 66.89 5.63
3 2 -8 53.99 5.53
3 2 -8 71.70 5.26
3 2 -8 72.68 5.65
3 2 -8 64.35 5.23
-3 -2 8 75.75 5.22
-3 -2 8 61.61 5.24
-3 -2 8 62.61 5.43
-3 -2 8 63.18 5.38
-3 -2 8 78.27 5.22
-3 -2 8 60.24 5.52
-3 -2 8 56.29 5.31
-3 -2 8 75.98 5.42
-3 -2 8 67.32 5.15
2 2 -8 9.54 1.16
2 2 -8 8.10 1.13
2 2 -8 9.29 1.20
2 2 -8 9.64 1.19
2 2 -8 13.84 1.45
2 2 -8 9.96 1.39
2 2 -8 10.65 1.12
2 2 -8 10.58 1.11
2 2 -8 7.93 1.33
2 2 -8 11.75 1.28
-2 -2 8 10.18 1.32
-2 -2 8 9.96 1.23
-2 -2 8 12.12 1.25
-2 -2 8 14.92 1.46
-2 -2 8 10.24 1.39
-2 -2 8 11.33 1.31
-2 -2 8 8.89 1.33
-2 -2 8 8.35 1.19
-2 -2 8 9.57 1.24
-2 -2 8 10.71 1.20
-2 -2 8 11.70 1.35
-2 -2 8 9.76 1.33
-2 -2 8 11.14 1.26
1 2 -8 38.73 3.67
1 2 -8 42.47 3.21
1 2 -8 42.80 3.51
1 2 -8 45.06 3.66
1 2 -8 38.07 3.22
1 2 -8 42.74 3.50
1 2 -8 41.23 3.40
1 2 -8 40.73 3.33
1 2 -8 41.80 3.47
1 2 -8 45.67 3.77
1 2 -8 42.64 3.65
1 2 -8 35.57 3.39
1 2 -8 40.56 3.47
1 2 -8 39.37 3.50
1 2 -8 39.91 3.26
-1 -2 8 44.60 3.69
-1 -2 8 38.20 3.47
-1 -2 8 36.94 3.37
-1 -2 8 40.85 3.67
-1 -2 8 43.18 3.56
-1 -2 8 42.33 3.53
-1 -2 8 39.77 3.46
-1 -2 8 35.24 3.44
-1 -2 8 41.18 3.46
-1 -2 8 39.71 3.31
-1 -2 8 37.13 3.31
-1 -2 8 34.87 3.56
0 2 -8 18.97 2.22
0 2 -8 23.02 2.16
0 2 -8 25.23 2.19
0 2 -8 21.90 2.09
0 2 -8 20.58 2.00
0 2 -8 22.06 2.32
0 2 -8 22.60 1.97
0 2 -8 21.48 2.12
0 2 -8 21.30 2.07
0 2 -8 26.40 2.34
0 2 -8 21.68 2.15
0 2 -8 20.34 2.20
0 2 -8 16.55 1.89
0 -2 8 24.08 2.04
0 -2 8 21.19 2.09
0 -2 8 21.22 2.06
0 -2 8 22.79 2.01
0 -2 8 21.32 2.14
0 -2 8 24.61 2.34
0 -2 8 19.49 2.08
0 -2 8 22.85 2.26
0 -2 8 21.95 2.13
0 -2 8 23.51 2.03
-1 2 -8 89.87 7.21
-1 2 -8 86.28 7.51
-1 2 -8 86.38 7.24
-1 2 -8 108.13 7.51
-1 2 -8 107.62 7.90
-1 2 -8 103.63 7.91
-1 2 -8 104.09 7.69
-1 2 -8 88.68 7.49
-1 2 -8 92.32 7.23
-1 2 -8 98.94 7.73
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1 -2 8 92.75 7.24
1 -2 8 97.99 7.25
1 -2 8 92.20 7.64
1 -2 8 106.06 7.89
1 -2 8 98.83 7.86
1 -2 8 92.55 7.41
1 -2 8 97.26 7.24
1 -2 8 94.66 7.57
1 -2 8 92.00 7.50
1 -2 8 86.22 7.49
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-2 2 -8 2.78 0.74
-2 2 -8 4.52 0.93
-2 2 -8 2.63 0.76
-2 2 -8 3.83 0.84
-2 2 -8 2.82 0.72
-2 2 -8 4.01 0.87
-2 2 -8 4.48 0.93
-2 2 -8 2.69 0.84
-2 2 -8 3.62 1.00
2 -2 8 3.30 0.73
2 -2 8 4.61 0.74
2 -2 8 3.28 0.82
2 -2 8 3.90 0.73
2 -2 8 3.53 0.81
2 -2 8 3.85 0.95
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-3 2 -8 13.13 1.62
-3 2 -8 13.62 1.70
-3 2 -8 12.43 1.60
-3 2 -8 11.88 1.68
-3 2 -8 14.58 1.54
-3 2 -8 17.79 1.88
-3 2 -8 15.98 1.73
3 -2 8 16.36 1.61
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-4 2 -8 73.69 5.46
-4 2 -8 56.28 5.53
-4 2 -8 62.19 5.28
-4 2 -8 60.51 4.98
-4 2 -8 60.63 5.45
-5 2 -8 20.75 2.06
-5 2 -8 16.26 2.12
-6 2 -8 5.28 1.26
-6 2 -8 5.42 1.14
-7 2 -8 6.05 1.23
8 1 -8 0.24 0.83
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-8 -1 8 1.41 0.73
7 1 -8 6.04 0.81
7 1 -8 9.08 1.22
7 1 -8 7.58 1.25
-7 -1 8 9.05 1.14
-7 -1 8 8.67 1.13
-7 -1 8 7.84 1.05
-7 -1 8 8.22 1.22
6 1 -8 70.56 5.93
6 1 -8 56.84 5.73
6 1 -8 65.50 5.91
-6 -1 8 81.54 5.80
-6 -1 8 77.37 5.49
-6 -1 8 62.40 5.85
-6 -1 8 75.25 5.50
-6 -1 8 71.22 5.61
-6 -1 8 75.63 5.84
-6 -1 8 71.32 5.54
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5 1 -8 6.32 0.95
5 1 -8 8.18 1.20
-5 -1 8 7.87 1.04
-5 -1 8 6.15 0.89
-5 -1 8 7.61 1.07
-5 -1 8 4.18 0.86
-5 -1 8 5.49 0.99
-5 -1 8 6.40 0.96
-5 -1 8 7.47 0.94
-5 -1 8 5.98 1.01
4 1 -8 13.29 1.53
4 1 -8 16.06 1.42
4 1 -8 15.41 1.65
4 1 -8 17.22 1.75
-4 -1 8 13.92 1.52
-4 -1 8 15.36 1.43
-4 -1 8 14.08 1.53
-4 -1 8 15.53 1.48
-4 -1 8 12.69 1.50
-4 -1 8 11.27 1.37
-4 -1 8 9.78 1.47
-4 -1 8 11.84 1.42
-4 -1 8 15.02 1.56
3 1 -8 41.91 3.24
3 1 -8 33.64 3.53
3 1 -8 44.83 3.41
3 1 -8 43.27 3.64
3 1 -8 41.80 3.49
3 1 -8 36.57 3.51
-3 -1 8 45.21 3.30
-3 -1 8 35.67 3.51
-3 -1 8 41.81 3.37
-3 -1 8 35.12 3.52
-3 -1 8 39.39 3.47
-3 -1 8 42.06 3.30
-3 -1 8 42.90 3.47
-3 -1 8 38.63 3.51
-3 -1 8 39.65 3.41
-3 -1 8 41.89 3.44
-3 -1 8 32.78 3.24
-3 -1 8 37.16 3.37
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2 1 -8 92.12 7.29
2 1 -8 90.37 7.51
2 1 -8 94.68 7.20
2 1 -8 90.84 7.14
2 1 -8 85.69 7.45
2 1 -8 80.93 6.74
2 1 -8 100.50 7.59
2 1 -8 95.16 7.29
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-2 -1 8 89.65 6.95
-2 -1 8 97.41 7.49
-2 -1 8 89.48 7.21
-2 -1 8 85.13 7.08
-2 -1 8 90.96 6.94
-2 -1 8 77.61 7.39
-2 -1 8 85.11 7.18
-2 -1 8 81.98 7.17
-2 -1 8 97.43 7.19
-2 -1 8 104.74 7.37
-2 -1 8 97.91 7.25
-2 -1 8 100.17 7.52
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1 1 -8 3.09 0.58
1 1 -8 2.16 0.65
1 1 -8 2.96 0.84
1 1 -8 1.85 0.48
1 1 -8 2.57 0.52
1 1 -8 3.62 0.87
1 1 -8 3.07 0.68
1 1 -8 2.64 0.65
1 1 -8 2.84 0.69
1 1 -8 2.53 0.69
1 1 -8 2.87 0.74
1 1 -8 2.80 0.63
1 1 -8 2.97 0.64
-1 -1 8 1.44 0.67
-1 -1 8 2.71 0.66
-1 -1 8 2.60 0.67
-1 -1 8 1.86 0.53
-1 -1 8 2.29 0.63
-1 -1 8 2.45 0.71
-1 -1 8 2.59 0.75
-1 -1 8 3.03 0.72
-1 -1 8 2.03 0.62
-1 -1 8 2.07 0.66
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0 1 -8 3.42 0.77
0 1 -8 2.97 0.78
0 1 -8 2.80 0.71
0 1 -8 3.47 0.73
0 1 -8 2.79 0.62
0 1 -8 3.03 0.66
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1 3 -9 61.59 5.22
1 3 -9 75.19 5.51
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1 2 -9 92.20 7.24
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1 2 -9 95.93 7.15
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1 1 -9 140.24 10.55
1 1 -9 145.40 11.30
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3 2 -13 12.57 1.65
-3 -2 13 10.86 1.68
2 2 -13 25.81 2.73
1 2 -13 2.97 1.02
0 2 -13 2.26 0.89
0 2 -13 0.15 0.60
-1 2 -13 20.34 2.08
3 1 -13 1.01 0.74
-3 -1 13 0.63 0.74
2 1 -13 41.97 4.15
-2 -1 13 50.94 4.28
1 1 -13 4.03 1.12
0 1 -13 14.99 1.48
0 1 -13 11.99 1.87
3 0 -13 1.97 0.79
-3 0 13 1.61 0.90
2 0 -13 14.25 1.85
-2 0 13 14.58 1.95
1 0 -13 38.93 3.77
0 0 -13 2.63 1.05
0 0 -13 2.54 0.58
-3 1 13 1.55 0.80
2 -1 -13 7.68 1.39
-2 1 13 8.76 1.54
1 -1 -13 30.62 3.15
0 0 0 0.00 0.00
;
_shelx_hkl_checksum 20305
_shelx_res_file
;
Imw034_0m.res created by SHELXL-2014/7
TITL Imw034_0m in P-1
CELL 0.71073 7.4579 8.4601 9.8864 97.073 98.474 100.644
ZERR 1.00 0.0004 0.0005 0.0006 0.002 0.002 0.002
LATT 1
SFAC C H N F Sn O
UNIT 20 20 4 8 3 2
LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!!
OMIT 0 0 1
OMIT 1 0 0
OMIT -3 56
L.S. 10
ACTA
BOND $H
FMAP 2
PLAN 10
SIZE 0.047 0.150 0.168
HTAB
HTAB O1 F11_$1
HTAB O1 F11_$2
EQIV $1 -x, -y+1, -z+1
EQIV $2 x, y-1, z-1
rem DFIX 0.96 0.0001 O1 H101 O1 H102
rem dfix 1.523 0.001 H101 h102
TEMP -173
WGHT 0.024000 0.407800
EXTI 0.006110
FVAR 0.16181 0.01506 0.07274
MOLE 1
SN1 5 0.500000 1.000000 1.000000 10.50000 0.00996 0.01193 =
0.01123 0.00239 0.00360 0.00387
F11 4 0.226382 0.918954 0.966832 11.00000 0.01164 0.02372 =
0.01985 -0.00243 0.00304 0.00275
F12 4 0.506025 0.962031 0.802382 11.00000 0.02164 0.02306 =
0.01335 0.00265 0.00532 0.00416
F13 4 0.461778 1.219086 0.987948 11.00000 0.02549 0.01548 =
0.02239 0.00620 0.00691 0.00965
MOLE 2
SN2 5 0.219487 0.110334 0.429579 11.00000 0.01071 0.01044 =
0.01397 0.00069 0.00208 0.00390
F21 4 -0.055714 0.102522 0.411992 11.00000 0.01096 0.01613 =
0.01654 0.00154 0.00345 0.00436
N1 3 0.271896 0.372723 0.370217 11.00000 0.01039 0.01329 =
0.01338 0.00036 0.00272 0.00234
C1 1 0.323369 0.398732 0.247716 11.00000 0.01296 0.01651 =
0.01448 0.00085 0.00172 0.00232
AFIX 43
H1 2 0.336176 0.308319 0.185355 11.00000 21.00000
AFIX 0
C2 1 0.357770 0.551273 0.210319 11.00000 0.01199 0.02228 =
0.01500 0.00545 0.00216 0.00427
AFIX 43
H2 2 0.393909 0.565968 0.123744 11.00000 21.00000
AFIX 0
C3 1 0.338798 0.683201 0.301141 11.00000 0.01457 0.01519 =
0.02136 0.00712 0.00254 0.00202
AFIX 43
H3 2 0.359746 0.789464 0.276867 11.00000 21.00000
AFIX 0
C4 1 0.288986 0.658545 0.427655 11.00000 0.01385 0.01241 =
0.01856 0.00032 0.00194 0.00502
AFIX 43
H4 2 0.276112 0.747687 0.491386 11.00000 21.00000
AFIX 0
C5 1 0.258109 0.501753 0.460099 11.00000 0.00657 0.01519 =
0.01612 0.00234 0.00197 0.00306
C6 1 0.215896 0.465377 0.597125 11.00000 0.00908 0.01151 =
0.01447 0.00091 0.00036 0.00199
N2 3 0.208195 0.309586 0.617078 11.00000 0.01285 0.01071 =
0.01115 0.00096 0.00030 0.00245
C7 1 0.181062 0.267618 0.739413 11.00000 0.01561 0.01480 =
0.01324 0.00244 -0.00103 0.00076
AFIX 43
H7 2 0.179108 0.158245 0.753370 11.00000 21.00000
AFIX 0
C8 1 0.155737 0.378016 0.846361 11.00000 0.01682 0.02249 =
0.01180 0.00266 0.00258 0.00122
AFIX 43
H8 2 0.134258 0.344727 0.931925 11.00000 21.00000
AFIX 0
C9 1 0.162164 0.537328 0.826812 11.00000 0.01564 0.01897 =
0.01414 -0.00266 0.00139 0.00439
AFIX 43
H9 2 0.144989 0.615148 0.899072 11.00000 21.00000
AFIX 0
C10 1 0.194038 0.583840 0.700301 11.00000 0.01356 0.01208 =
0.01422 0.00003 0.00088 0.00319
AFIX 43
H10 2 0.200584 0.693362 0.685238 11.00000 21.00000
AFIX 0
O1 6 0.093761 0.050115 0.185936 11.00000 0.01617 0.02685 =
0.01318 -0.00158 0.00367 0.00675
AFIX 3
H101 2 -0.022947 0.066979 0.141187 11.00000 31.00000
H102 2 0.148112 0.003354 0.112607 11.00000 31.00000
AFIX 0
HKLF 4 1 1 0 0 0 1 0 0 0 1
REM Imw034_0m in P-1
REM R1 = 0.0223 for 2611 Fo > 4sig(Fo) and 0.0262 for all 2864 data
REM 172 parameters refined using 0 restraints
END
WGHT 0.0240 0.4078
REM Instructions for potential hydrogen bonds
HTAB C1 F13_$2
HTAB C1 O1
EQIV $3 -x+1, -y+2, -z+1
HTAB C2 F13_$3
HTAB C4 F21_$1
EQIV $4 -x, -y, -z+1
HTAB C7 F21_$4
HTAB C7 O1_$4
HTAB C10 F21_$1
HTAB O1 F11_$1
HTAB O1 F11_$2
REM Highest difference peak 0.887, deepest hole -0.693, 1-sigma level 0.129
Q1 1 0.4770 0.8797 0.9787 11.00000 0.05 0.89
Q2 1 0.2041 -0.0051 0.4217 11.00000 0.05 0.85
Q3 1 0.2374 0.2116 0.4245 11.00000 0.05 0.77
Q4 1 0.1814 0.0169 0.3608 11.00000 0.05 0.68
Q5 1 0.2333 0.4018 0.6338 11.00000 0.05 0.63
Q6 1 0.2374 0.0251 0.4735 11.00000 0.05 0.61
Q7 1 0.2320 0.5218 0.6598 11.00000 0.05 0.56
Q8 1 0.2919 0.2947 0.4011 11.00000 0.05 0.56
Q9 1 0.2161 0.4911 0.5224 11.00000 0.05 0.53
Q10 1 0.2408 0.5742 0.4124 11.00000 0.05 0.52
;
_shelx_res_checksum 20925
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn Sn1 0.5000 1.0000 1.0000 0.01059(8) Uani d 1 . .
F F11 0.22638(19) 0.91895(18) 0.96683(15) 0.0190(3) Uani d 1 . .
F F12 0.5060(2) 0.96203(18) 0.80238(14) 0.0192(3) Uani d 1 . .
F F13 0.4618(2) 1.21909(17) 0.98795(15) 0.0198(3) Uani d 1 . .
Sn Sn2 0.21949(2) 0.11033(2) 0.42958(2) 0.01159(8) Uani d 1 . .
F F21 -0.05571(18) 0.10252(17) 0.41199(14) 0.0143(3) Uani d 1 . .
N N1 0.2719(3) 0.3727(2) 0.3702(2) 0.0124(4) Uani d 1 . .
C C1 0.3234(3) 0.3987(3) 0.2477(3) 0.0150(5) Uani d 1 . .
H H1 0.3362 0.3083 0.1854 0.015(2) Uiso calc 1 . .
C C2 0.3578(3) 0.5513(3) 0.2103(2) 0.0161(6) Uani d 1 . .
H H2 0.3939 0.5660 0.1237 0.015(2) Uiso calc 1 . .
C C3 0.3388(3) 0.6832(3) 0.3011(3) 0.0169(5) Uani d 1 . .
H H3 0.3597 0.7895 0.2769 0.015(2) Uiso calc 1 . .
C C4 0.2890(3) 0.6585(3) 0.4277(3) 0.0149(5) Uani d 1 . .
H H4 0.2761 0.7477 0.4914 0.015(2) Uiso calc 1 . .
C C5 0.2581(3) 0.5018(3) 0.4601(2) 0.0125(5) Uani d 1 . .
C C6 0.2159(3) 0.4654(3) 0.5971(2) 0.0120(5) Uani d 1 . .
N N2 0.2082(3) 0.3096(2) 0.6171(2) 0.0118(4) Uani d 1 . .
C C7 0.1811(3) 0.2676(3) 0.7394(2) 0.0152(5) Uani d 1 . .
H H7 0.1791 0.1582 0.7534 0.015(2) Uiso calc 1 . .
C C8 0.1557(4) 0.3780(3) 0.8464(3) 0.0174(5) Uani d 1 . .
H H8 0.1343 0.3447 0.9319 0.015(2) Uiso calc 1 . .
C C9 0.1622(3) 0.5373(3) 0.8268(3) 0.0167(5) Uani d 1 . .
H H9 0.1450 0.6151 0.8991 0.015(2) Uiso calc 1 . .
C C10 0.1940(3) 0.5838(3) 0.7003(2) 0.0135(5) Uani d 1 . .
H H10 0.2006 0.6934 0.6852 0.015(2) Uiso calc 1 . .
O O1 0.0938(2) 0.0501(2) 0.18594(17) 0.0187(4) Uani d 1 . .
H H101 -0.0229 0.0670 0.1412 0.073(10) Uiso d 1 . .
H H102 0.1481 0.0034 0.1126 0.073(10) Uiso d 1 . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
Sn1 0.00996(13) 0.01193(14) 0.01123(13) 0.00387(9) 0.00360(9) 0.00239(9)
F11 0.0116(7) 0.0237(8) 0.0199(8) 0.0027(6) 0.0030(6) -0.0024(6)
F12 0.0216(8) 0.0231(8) 0.0133(7) 0.0042(6) 0.0053(6) 0.0027(6)
F13 0.0255(8) 0.0155(8) 0.0224(8) 0.0096(6) 0.0069(6) 0.0062(6)
Sn2 0.01071(11) 0.01044(11) 0.01397(12) 0.00390(7) 0.00208(7) 0.00069(7)
F21 0.0110(7) 0.0161(7) 0.0165(7) 0.0044(5) 0.0035(5) 0.0015(6)
N1 0.0104(10) 0.0133(10) 0.0134(10) 0.0023(8) 0.0027(8) 0.0004(8)
C1 0.0130(12) 0.0165(13) 0.0145(13) 0.0023(10) 0.0017(10) 0.0009(10)
C2 0.0120(13) 0.0223(15) 0.0150(14) 0.0043(11) 0.0022(11) 0.0054(12)
C3 0.0146(12) 0.0152(13) 0.0214(14) 0.0020(10) 0.0025(10) 0.0071(11)
C4 0.0138(12) 0.0124(12) 0.0186(13) 0.0050(9) 0.0019(10) 0.0003(10)
C5 0.0066(11) 0.0152(12) 0.0161(12) 0.0031(9) 0.0020(9) 0.0023(10)
C6 0.0091(11) 0.0115(12) 0.0145(12) 0.0020(9) 0.0004(9) 0.0009(10)
N2 0.0128(10) 0.0107(10) 0.0111(10) 0.0024(8) 0.0003(8) 0.0010(8)
C7 0.0156(12) 0.0148(12) 0.0132(12) 0.0008(10) -0.0010(10) 0.0024(10)
C8 0.0168(13) 0.0225(14) 0.0118(12) 0.0012(10) 0.0026(10) 0.0027(11)
C9 0.0156(12) 0.0190(13) 0.0141(13) 0.0044(10) 0.0014(10) -0.0027(10)
C10 0.0136(12) 0.0121(12) 0.0142(12) 0.0032(9) 0.0009(9) 0.0000(10)
O1 0.0162(9) 0.0269(10) 0.0132(9) 0.0068(8) 0.0037(7) -0.0016(8)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
F13 Sn1 F13 . 2_677 180.0 ?
F13 Sn1 F12 . 2_677 89.28(6) ?
F13 Sn1 F12 2_677 2_677 90.72(6) ?
F13 Sn1 F12 . . 90.72(6) ?
F13 Sn1 F12 2_677 . 89.28(6) ?
F12 Sn1 F12 2_677 . 180.00(9) ?
F13 Sn1 F11 . . 89.59(6) ?
F13 Sn1 F11 2_677 . 90.41(6) ?
F12 Sn1 F11 2_677 . 88.39(6) ?
F12 Sn1 F11 . . 91.61(6) ?
F13 Sn1 F11 . 2_677 90.41(6) ?
F13 Sn1 F11 2_677 2_677 89.59(6) ?
F12 Sn1 F11 2_677 2_677 91.62(6) ?
F12 Sn1 F11 . 2_677 88.39(6) ?
F11 Sn1 F11 . 2_677 180.00(3) ?
F21 Sn2 N1 . . 91.52(6) ?
F21 Sn2 N2 . . 78.11(6) ?
N1 Sn2 N2 . . 68.50(7) ?
F21 Sn2 O1 . . 73.42(6) ?
N1 Sn2 O1 . . 79.62(6) ?
N2 Sn2 O1 . . 136.22(6) ?
C5 N1 C1 . . 118.7(2) ?
C5 N1 Sn2 . . 120.40(15) ?
C1 N1 Sn2 . . 120.81(16) ?
N1 C1 C2 . . 122.4(2) ?
N1 C1 H1 . . 118.8 ?
C2 C1 H1 . . 118.8 ?
C1 C2 C3 . . 118.8(2) ?
C1 C2 H2 . . 120.6 ?
C3 C2 H2 . . 120.6 ?
C4 C3 C2 . . 119.3(2) ?
C4 C3 H3 . . 120.3 ?
C2 C3 H3 . . 120.3 ?
C3 C4 C5 . . 119.1(2) ?
C3 C4 H4 . . 120.4 ?
C5 C4 H4 . . 120.4 ?
N1 C5 C4 . . 121.6(2) ?
N1 C5 C6 . . 115.7(2) ?
C4 C5 C6 . . 122.7(2) ?
N2 C6 C10 . . 121.7(2) ?
N2 C6 C5 . . 115.3(2) ?
C10 C6 C5 . . 122.9(2) ?
C7 N2 C6 . . 119.5(2) ?
C7 N2 Sn2 . . 120.78(16) ?
C6 N2 Sn2 . . 119.55(15) ?
N2 C7 C8 . . 122.1(2) ?
N2 C7 H7 . . 118.9 ?
C8 C7 H7 . . 118.9 ?
C9 C8 C7 . . 118.8(2) ?
C9 C8 H8 . . 120.6 ?
C7 C8 H8 . . 120.6 ?
C8 C9 C10 . . 119.7(2) ?
C8 C9 H9 . . 120.2 ?
C10 C9 H9 . . 120.2 ?
C6 C10 C9 . . 118.1(2) ?
C6 C10 H10 . . 121.0 ?
C9 C10 H10 . . 121.0 ?
Sn2 O1 H101 . . 127.2 ?
Sn2 O1 H102 . . 127.9 ?
H101 O1 H102 . . 105.0 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Sn1 F13 . 1.9418(14) ?
Sn1 F13 2_677 1.9418(14) ?
Sn1 F12 2_677 1.9491(14) ?
Sn1 F12 . 1.9491(14) ?
Sn1 F11 . 1.9931(14) ?
Sn1 F11 2_677 1.9931(14) ?
Sn2 F21 . 2.0221(13) ?
Sn2 N1 . 2.344(2) ?
Sn2 N2 . 2.369(2) ?
Sn2 O1 . 2.4076(17) ?
N1 C5 . 1.350(3) ?
N1 C1 . 1.354(3) ?
C1 C2 . 1.375(3) ?
C1 H1 . 0.9500 ?
C2 C3 . 1.386(3) ?
C2 H2 . 0.9500 ?
C3 C4 . 1.385(4) ?
C3 H3 . 0.9500 ?
C4 C5 . 1.389(3) ?
C4 H4 . 0.9500 ?
C5 C6 . 1.490(3) ?
C6 N2 . 1.349(3) ?
C6 C10 . 1.389(3) ?
N2 C7 . 1.335(3) ?
C7 C8 . 1.381(4) ?
C7 H7 . 0.9500 ?
C8 C9 . 1.378(4) ?
C8 H8 . 0.9500 ?
C9 C10 . 1.396(3) ?
C9 H9 . 0.9500 ?
C10 H10 . 0.9500 ?
O1 H101 . 0.9600 ?
O1 H102 . 0.9600 ?
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
O1 H101 F11 2_566 0.96 1.75 2.705(2) 170.0
O1 H102 F11 1_544 0.96 1.75 2.710(2) 174.0