#------------------------------------------------------------------------------ #$Date: 2025-03-14 05:04:30 +0200 (Fri, 14 Mar 2025) $ #$Revision: 298434 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/34/2023439.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023439 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 8.74393(9) _cell_length_b 8.74393(9) _cell_length_c 8.74393(9) _exptl_crystal_F_000 1316 _reflns_d_resolution_high 0.3777 _cod_data_source_file dk5135330Ksup15.hkl _cod_data_source_block 330K _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 957.76 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, -z+1/2' '-y, -x+1/2, -z+1/2' 'y, -x+1/2, z+1/2' '-y, x+1/2, z+1/2' 'x, z+1/2, -y+1/2' '-x, z+1/2, y+1/2' '-x, -z+1/2, -y+1/2' 'x, -z+1/2, y+1/2' 'z, y+1/2, -x+1/2' 'z, -y+1/2, x+1/2' '-z, y+1/2, x+1/2' '-z, -y+1/2, -x+1/2' '-x, -y+1/2, -z+1/2' 'x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' '-z, -x+1/2, -y+1/2' '-z, x+1/2, y+1/2' 'z, x+1/2, -y+1/2' 'z, -x+1/2, y+1/2' '-y, -z+1/2, -x+1/2' 'y, -z+1/2, x+1/2' '-y, z+1/2, x+1/2' 'y, z+1/2, -x+1/2' '-y, -x+1/2, z+1/2' 'y, x+1/2, z+1/2' '-y, x+1/2, -z+1/2' 'y, -x+1/2, -z+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-z, -y+1/2, x+1/2' '-z, y+1/2, -x+1/2' 'z, -y+1/2, -x+1/2' 'z, y+1/2, x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, -z+1/2' '-y+1/2, -x, -z+1/2' 'y+1/2, -x, z+1/2' '-y+1/2, x, z+1/2' 'x+1/2, z, -y+1/2' '-x+1/2, z, y+1/2' '-x+1/2, -z, -y+1/2' 'x+1/2, -z, y+1/2' 'z+1/2, y, -x+1/2' 'z+1/2, -y, x+1/2' '-z+1/2, y, x+1/2' '-z+1/2, -y, -x+1/2' '-x+1/2, -y, -z+1/2' 'x+1/2, y, -z+1/2' 'x+1/2, -y, z+1/2' '-x+1/2, y, z+1/2' '-z+1/2, -x, -y+1/2' '-z+1/2, x, y+1/2' 'z+1/2, x, -y+1/2' 'z+1/2, -x, y+1/2' '-y+1/2, -z, -x+1/2' 'y+1/2, -z, x+1/2' '-y+1/2, z, x+1/2' 'y+1/2, z, -x+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, x, z+1/2' '-y+1/2, x, -z+1/2' 'y+1/2, -x, -z+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-z+1/2, -y, x+1/2' '-z+1/2, y, -x+1/2' 'z+1/2, -y, -x+1/2' 'z+1/2, y, x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y+1/2, -x+1/2, -z' 'y+1/2, -x+1/2, z' '-y+1/2, x+1/2, z' 'x+1/2, z+1/2, -y' '-x+1/2, z+1/2, y' '-x+1/2, -z+1/2, -y' 'x+1/2, -z+1/2, y' 'z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, x' '-z+1/2, y+1/2, x' '-z+1/2, -y+1/2, -x' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' '-z+1/2, -x+1/2, -y' '-z+1/2, x+1/2, y' 'z+1/2, x+1/2, -y' 'z+1/2, -x+1/2, y' '-y+1/2, -z+1/2, -x' 'y+1/2, -z+1/2, x' '-y+1/2, z+1/2, x' 'y+1/2, z+1/2, -x' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' '-y+1/2, x+1/2, -z' 'y+1/2, -x+1/2, -z' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-z+1/2, -y+1/2, x' '-z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, -x' 'z+1/2, y+1/2, x' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 1 2362.31 2258.12 12.10 o 0 0 2 19850.70 22825.20 66.23 o 0 2 2 88086.60 96595.30 100.98 o 2 2 2 758780.00 917298.00 827.94 o 1 1 3 6633.55 8429.52 16.35 o 1 3 3 32570.10 34568.70 43.68 o 3 3 3 67181.50 64633.60 143.58 o 0 0 4 829475.00 798111.00 1287.43 o 0 2 4 28142.00 30295.60 39.59 o 2 2 4 37683.30 41382.70 54.04 o 0 4 4 494651.00 452144.00 540.30 o 2 4 4 33773.20 34898.70 48.79 o 4 4 4 313518.00 295267.00 446.11 o 1 1 5 13060.20 12716.10 24.75 o 1 3 5 229.29 223.50 2.98 o 3 3 5 4432.77 5122.07 17.36 o 1 5 5 21340.80 20966.40 40.35 o 3 5 5 4430.26 4437.47 18.12 o 5 5 5 25669.90 24598.90 102.00 o 0 0 6 1033.82 1134.65 18.00 o 0 2 6 74826.80 73304.30 91.62 o 2 2 6 277364.00 258512.00 219.88 o 0 4 6 4630.19 4841.03 17.01 o 2 4 6 42420.70 42541.60 46.41 o 4 4 6 8725.86 8957.63 28.87 o 0 6 6 67130.60 68217.60 148.38 o 2 6 6 120954.00 119295.00 164.67 o 4 6 6 42858.90 42184.70 86.79 o 6 6 6 56885.10 55495.10 206.35 o 1 1 7 7049.40 7167.25 22.78 o 1 3 7 20806.60 20418.20 30.28 o 3 3 7 37907.00 36194.10 65.25 o 1 5 7 348.92 381.60 5.88 o 3 5 7 4948.32 5034.18 17.35 o 5 5 7 491.50 559.41 11.34 o 1 7 7 14580.70 14563.20 47.02 o 3 7 7 24196.60 24315.30 67.71 o 5 7 7 4697.19 4472.33 27.85 o 7 7 7 16758.00 15351.10 97.31 o 0 0 8 221841.00 214906.00 438.07 o 0 2 8 33530.70 33271.70 61.62 o 2 2 8 4853.50 4974.23 21.97 o 0 4 8 149998.00 140999.00 192.23 o 2 4 8 35230.40 35027.50 52.28 o 4 4 8 103323.00 98687.60 163.14 o 0 6 8 11997.20 12172.40 43.54 o 2 6 8 10301.50 10206.50 29.29 o 4 6 8 14096.20 14100.50 36.53 o 6 6 8 13535.10 12914.20 51.17 o 0 8 8 55637.50 56771.80 167.18 o 2 8 8 30954.10 30557.60 84.84 o 4 8 8 39757.70 38562.00 106.67 o 6 8 8 14922.90 14258.40 57.88 o 8 8 8 16476.90 14675.20 112.31 o 1 1 9 4080.80 3925.31 23.06 o 1 3 9 98.89 115.36 5.46 o 3 3 9 1356.95 1555.44 16.38 o 1 5 9 7350.29 7422.31 25.23 o 3 5 9 1598.19 1619.62 13.31 o 5 5 9 9760.40 9720.81 43.48 o 1 7 9 120.79 163.62 7.33 o 3 7 9 1911.70 1984.00 14.59 o 5 7 9 210.23 250.00 8.36 o 7 7 9 2115.33 2077.11 23.21 o 1 9 9 3123.66 3114.46 25.78 o 3 9 9 686.82 706.38 16.12 o 5 9 9 4503.35 4488.62 35.53 o 7 9 9 102.42 140.51 12.87 o 9 9 9 2405.91 2315.40 51.12 o 0 0 10 163.38 268.24 19.61 o 0 2 10 47884.80 44528.00 100.86 o 2 2 10 67907.80 64179.40 132.90 o 0 4 10 140.52 192.69 10.23 o 2 4 10 32203.00 30614.20 57.10 o 4 4 10 929.40 939.98 15.52 o 0 6 10 42879.80 42928.70 103.44 o 2 6 10 33929.90 33450.10 65.23 o 4 6 10 30365.20 29026.50 62.19 o 6 6 10 17268.30 16915.40 65.40 o 0 8 10 2218.58 2245.31 23.47 o 2 8 10 11413.00 11376.50 36.91 o 4 8 10 3162.31 3151.44 21.17 o 6 8 10 12257.80 11749.80 39.66 o 8 8 10 4547.23 4428.85 38.43 o 0 10 10 28959.60 29518.70 123.96 o 2 10 10 11129.60 11562.30 53.60 o 4 10 10 21824.10 21291.40 84.86 o 6 10 10 5737.41 5513.56 40.93 o 8 10 10 10303.30 9834.45 64.46 o 10 10 10 1885.05 1909.34 57.00 o 1 1 11 772.51 695.07 13.22 o 1 3 11 3771.42 3639.53 19.13 o 3 3 11 8299.38 8028.80 41.06 o 1 5 11 5.18 90.20 8.53 o 3 5 11 767.84 752.20 11.09 o 5 5 11 542.85 595.82 15.43 o 1 7 11 3521.47 3526.07 21.43 o 3 7 11 6682.00 6564.96 29.06 o 5 7 11 1061.38 1006.71 13.82 o 7 7 11 5521.27 5374.41 39.05 o 1 9 11 3.66 73.83 10.49 o 3 9 11 375.38 385.42 11.00 o 5 9 11 290.26 299.55 10.74 o 7 9 11 567.81 536.31 12.88 o 9 9 11 173.78 185.45 16.54 o 1 11 11 1007.74 1007.38 21.24 o 3 11 11 2257.56 2292.83 29.95 o 5 11 11 237.75 277.54 17.91 o 7 11 11 2113.49 2105.94 29.27 o 9 11 11 137.11 142.13 15.69 o 11 11 11 857.71 880.50 38.72 o 0 0 12 53328.00 51078.00 227.94 o 0 2 12 19989.30 19097.40 65.82 o 2 2 12 667.18 631.16 14.67 o 0 4 12 38960.50 37276.80 101.59 o 2 4 12 20154.60 19420.20 50.00 o 4 4 12 28594.60 27459.40 88.08 o 0 6 12 9456.80 9526.58 48.09 o 2 6 12 2193.93 2111.82 17.75 o 4 6 12 10089.70 10074.80 37.83 o 6 6 12 3565.22 3417.48 33.38 o 0 8 12 17076.30 17580.10 69.43 o 2 8 12 17729.60 18422.60 51.68 o 4 8 12 12622.40 12472.10 45.49 o 6 8 12 9936.88 9695.81 39.03 o 8 8 12 5598.35 5275.42 51.01 o 0 10 12 2743.28 2808.42 30.38 o 2 10 12 3323.04 3341.77 24.07 o 4 10 12 3234.08 3278.68 26.12 o 6 10 12 4082.08 4069.81 30.06 o 8 10 12 3849.49 3804.32 29.89 o 10 10 12 4051.95 4093.37 45.17 o 0 12 12 6154.13 6406.15 63.84 o 2 12 12 11393.00 12559.50 68.09 o 4 12 12 4571.80 4638.62 44.24 o 6 12 12 7058.10 7223.64 50.02 o 8 12 12 2019.55 2040.82 33.53 o 10 12 12 3203.77 3184.22 34.91 o 12 12 12 717.36 772.48 39.14 o 1 1 13 68.05 127.63 12.11 o 1 3 13 310.42 330.07 9.98 o 3 3 13 1676.57 1697.72 23.46 o 1 5 13 643.61 671.66 12.37 o 3 5 13 5.49 74.00 10.91 o 5 5 13 1455.46 1510.34 24.57 o 1 7 13 570.00 575.11 11.85 o 3 7 13 1776.34 1791.99 18.09 o 5 7 13 47.84 87.82 11.00 o 7 7 13 1777.37 1711.22 30.29 o 1 9 13 348.18 384.91 11.51 o 3 9 13 2.84 79.89 13.64 o 5 9 13 831.78 861.82 16.97 o 7 9 13 28.19 80.65 13.22 o 9 9 13 518.17 516.34 19.78 o 1 11 13 118.34 145.20 10.74 o 3 11 13 583.85 622.36 15.09 o 5 11 13 0.72 68.04 15.52 o 7 11 13 668.95 695.46 16.46 o 9 11 13 0.72 61.64 13.47 o 11 11 13 244.35 231.41 17.14 o 1 13 13 7.63 64.88 18.50 o 3 13 13 74.88 86.62 16.20 o 5 13 13 120.90 125.17 14.41 o 7 13 13 142.44 131.30 14.58 o 9 13 13 82.22 93.53 13.81 o 11 13 13 33.80 58.57 15.09 o 13 13 13 1.77 25.07 31.20 < 0 0 14 74.02 122.94 25.75 o 0 2 14 19330.90 18465.50 76.35 o 2 2 14 17921.60 17609.50 73.40 o 0 4 14 13.88 102.57 14.84 o 2 4 14 14206.50 13774.30 45.86 o 4 4 14 178.08 205.15 14.58 o 0 6 14 18264.30 18486.40 77.71 o 2 6 14 9968.78 10038.30 39.11 o 4 6 14 13862.90 13840.10 48.95 o 6 6 14 5471.99 5450.29 48.45 o 0 8 14 545.15 537.16 19.27 o 2 8 14 6239.18 6339.42 35.90 o 4 8 14 871.42 902.51 16.80 o 6 8 14 6636.25 6608.97 36.59 o 8 8 14 1537.71 1493.44 25.93 o 0 10 14 13979.60 15446.60 79.05 o 2 10 14 3785.12 3957.32 28.43 o 4 10 14 11042.50 11285.10 48.30 o 6 10 14 2008.11 2076.49 23.46 o 8 10 14 5862.07 5844.34 31.53 o 10 10 14 676.95 671.07 20.04 o 0 12 14 911.28 955.06 23.80 o 2 12 14 2264.18 2386.20 23.04 o 4 12 14 1152.13 1169.41 16.55 o 6 12 14 2650.30 2706.23 22.02 o 8 12 14 1568.08 1539.06 18.43 o 10 12 14 2618.17 2621.84 21.68 o 12 12 14 1466.61 1313.76 26.70 o 0 14 14 7835.81 8042.61 70.38 o 2 14 14 1486.34 1546.18 24.40 o 4 14 14 6368.55 6581.72 46.41 o 6 14 14 784.89 794.33 19.19 o 8 14 14 3633.79 3508.80 35.26 o 10 14 14 259.40 245.74 16.03 o 1 1 15 31.43 115.10 15.35 o 1 3 15 170.92 164.73 9.98 o 3 3 15 911.57 919.84 20.98 o 1 5 15 349.31 360.43 12.11 o 3 5 15 3.27 71.45 13.22 o 5 5 15 842.61 839.22 23.28 o 1 7 15 316.74 338.77 12.79 o 3 7 15 1008.71 994.51 15.69 o 5 7 15 23.99 79.38 12.70 o 7 7 15 1047.19 1042.63 22.09 o 1 9 15 221.13 241.56 12.02 o 3 9 15 3.14 71.11 14.66 o 5 9 15 540.91 543.89 13.81 o 7 9 15 12.32 66.16 12.62 o 9 9 15 367.26 358.90 16.71 o 1 11 15 61.54 108.96 11.51 o 3 11 15 339.38 367.60 11.60 o 5 11 15 2.01 60.19 12.45 o 7 11 15 399.19 398.47 11.60 o 9 11 15 2.38 49.19 12.36 o 11 11 15 140.49 141.54 14.24 o 1 13 15 9.08 60.19 11.60 o 3 13 15 38.51 77.42 10.06 o 5 13 15 95.96 97.37 9.81 o 7 13 15 78.89 91.31 9.21 o 9 13 15 69.90 71.36 9.63 o 11 13 15 15.18 35.98 14.15 < 1 15 15 12.41 45.02 15.77 < 3 15 15 16.27 64.37 16.03 o 5 15 15 83.13 69.74 13.56 o 7 15 15 39.53 53.03 16.80 o 9 15 15 62.74 28.90 23.19 < 0 0 16 16117.10 15315.70 152.63 o 0 2 16 6819.73 6715.87 53.86 o 2 2 16 376.33 373.83 19.44 o 0 4 16 12460.40 11953.70 73.77 o 2 4 16 7115.27 7175.55 39.50 o 4 4 16 9614.29 9421.51 54.94 o 0 6 16 3691.51 3823.12 36.37 o 2 6 16 901.40 875.15 16.29 o 4 6 16 4020.20 4116.10 30.06 o 6 6 16 1423.34 1442.53 25.25 o 0 8 16 6237.60 6451.57 46.75 o 2 8 16 6980.71 7313.96 34.97 o 4 8 16 4774.69 4977.45 33.40 o 6 8 16 4284.60 4452.40 29.21 o 8 8 16 2302.33 2337.89 29.61 o 0 10 16 1327.42 1399.56 24.57 o 2 10 16 1373.98 1423.38 16.98 o 4 10 16 1560.76 1635.98 17.66 o 6 10 16 1745.65 1729.43 18.51 o 8 10 16 1911.18 1933.95 19.28 o 10 10 16 1858.22 1821.83 25.94 o 0 12 16 2585.14 2639.30 31.15 o 2 12 16 5204.02 5393.75 29.05 o 4 12 16 1960.69 2039.19 18.94 o 6 12 16 3414.26 3382.94 22.96 o 8 12 16 914.08 963.08 14.93 o 10 12 16 1691.07 1582.86 21.16 o 0 14 16 537.12 543.63 15.78 o 2 14 16 1052.18 1091.32 14.93 o 4 14 16 661.49 647.45 13.64 o 6 14 16 1259.89 1233.22 19.36 o 8 14 16 879.86 834.67 23.97 o 0 16 16 1218.41 1234.03 65.00 o 2 16 16 2680.43 2695.20 61.12 o 4 16 16 937.12 1120.98 85.04 o 1 1 17 130.54 159.87 14.67 o 1 3 17 607.02 593.54 14.75 o 3 3 17 1367.26 1360.61 25.93 o 1 5 17 0.43 67.01 14.66 o 3 5 17 154.19 169.08 10.40 o 5 5 17 85.30 99.50 15.77 o 1 7 17 695.36 743.91 15.69 o 3 7 17 1351.66 1411.17 20.05 o 5 7 17 242.58 246.42 11.00 o 7 7 17 1307.96 1322.76 23.29 o 1 9 17 0.31 55.84 13.13 o 3 9 17 99.88 120.22 9.81 o 5 9 17 56.28 81.68 10.15 o 7 9 17 160.83 158.16 9.98 o 9 9 17 38.20 51.67 14.58 o 1 11 17 264.97 263.47 10.57 o 3 11 17 595.90 606.58 12.62 o 5 11 17 70.89 85.77 9.21 o 7 11 17 611.81 615.37 13.05 o 9 11 17 47.78 52.61 10.57 o 11 11 17 280.91 275.00 29.42 o 1 13 17 42.78 56.61 9.29 o 3 13 17 185.86 174.45 9.72 o 5 13 17 0.39 35.55 13.73 < 7 13 17 222.13 190.14 12.79 o 1 15 17 21.61 38.79 21.57 < 3 15 17 110.53 132.16 24.21 o 0 0 18 14.76 92.68 32.99 < 0 2 18 5658.62 5428.34 43.41 o 2 2 18 6495.80 6392.77 55.47 o 0 4 18 89.25 123.20 16.63 o 2 4 18 4327.71 4419.89 31.51 o 4 4 18 209.59 220.41 14.92 o 0 6 18 5801.35 6047.92 43.49 o 2 6 18 4009.85 4046.28 26.22 o 4 6 18 4550.32 4669.97 27.42 o 6 6 18 2425.69 2408.22 28.93 o 0 8 18 392.53 405.29 16.54 o 2 8 18 2087.80 2229.67 20.56 o 4 8 18 548.71 527.77 12.45 o 6 8 18 2355.64 2424.19 20.31 o 8 8 18 866.22 789.16 19.10 o 0 10 18 5029.89 5276.51 42.11 o 2 10 18 1794.79 1810.16 19.37 o 4 10 18 4058.70 4263.05 26.47 o 6 10 18 1047.26 1047.14 15.52 o 8 10 18 2268.31 2264.71 24.41 o 10 10 18 423.76 393.63 25.24 o 0 12 18 568.89 536.14 18.85 o 2 12 18 840.71 877.68 15.61 o 4 12 18 687.56 617.44 15.18 o 6 12 18 1026.44 1051.96 20.30 o 8 12 18 889.75 711.63 30.45 o 0 14 18 3145.09 3228.84 70.10 o 2 14 18 818.87 785.37 34.88 o 1 1 19 146.74 164.98 14.07 o 1 3 19 3.04 56.61 11.08 o 3 3 19 67.41 95.66 15.26 o 1 5 19 362.83 349.35 11.00 o 3 5 19 86.02 101.97 9.80 o 5 5 19 615.49 583.05 17.31 o 1 7 19 5.50 49.79 11.51 o 3 7 19 114.85 130.96 9.72 o 5 7 19 21.80 52.78 9.38 o 7 7 19 154.74 152.02 12.36 o 1 9 19 261.66 257.25 10.49 o 3 9 19 66.66 75.80 9.12 o 5 9 19 439.60 413.23 11.94 o 7 9 19 19.00 41.18 12.36 o 9 9 19 317.93 274.57 23.53 o 1 11 19 3.70 37.09 15.77 < 3 11 19 22.95 39.65 13.30 < 5 11 19 49.73 44.08 13.47 o 7 11 19 43.65 42.29 21.66 < 1 13 19 57.19 65.65 26.26 < 0 0 20 6140.40 6076.72 91.44 o 0 2 20 1756.33 1629.69 25.68 o 2 2 20 374.81 389.26 16.46 o 0 4 20 4962.01 4820.49 39.46 o 2 4 20 1926.79 1861.87 18.26 o 4 4 20 3996.06 3975.25 36.12 o 0 6 20 979.76 1003.35 19.53 o 2 6 20 622.04 624.15 11.85 o 4 6 20 1122.14 1126.15 15.10 o 6 6 20 854.54 844.68 19.70 o 0 8 20 2785.81 2850.74 32.18 o 2 8 20 2110.72 2109.08 20.99 o 4 8 20 2222.23 2243.37 23.81 o 6 8 20 1326.41 1265.02 20.47 o 8 8 20 1203.12 1133.59 50.93 o 0 10 20 364.65 389.69 21.40 o 2 10 20 826.10 819.80 17.74 o 4 10 20 452.64 464.41 20.13 o 6 10 20 989.36 1036.17 152.95 o 1 1 21 104.39 108.88 12.62 o 1 3 21 308.79 311.48 9.89 o 3 3 21 601.70 580.40 16.97 o 1 5 21 13.59 45.19 10.32 o 3 5 21 112.66 123.46 9.46 o 5 5 21 3.80 34.44 22.85 < 1 7 21 344.48 357.62 12.88 o 3 7 21 603.42 575.21 15.78 o 5 7 21 150.12 143.24 14.24 o 1 9 21 10.05 29.84 25.24 < 3 9 21 79.40 93.62 20.63 o 0 0 22 107.52 135.65 33.51 o 0 2 22 1403.25 1370.72 27.90 o 2 2 22 2759.82 2867.56 36.11 o 0 4 22 179.52 171.04 16.46 o 2 4 22 1072.42 1044.22 19.45 o 4 4 22 259.14 236.62 21.06 o 0 6 22 1528.93 1481.75 42.23 o 2 6 22 1863.02 1817.38 34.39 o 1 1 23 61.26 36.92 20.21 <