#------------------------------------------------------------------------------ #$Date: 2025-03-14 05:04:30 +0200 (Fri, 14 Mar 2025) $ #$Revision: 298434 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/02/34/2023441.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2023441 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 8.74867(12) _cell_length_b 8.74867(12) _cell_length_c 8.74867(12) _exptl_crystal_F_000 1316 _reflns_d_resolution_high 0.3779 _cod_data_source_file dk5135370Ksup17.hkl _cod_data_source_block 370K _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 960.21 _shelx_f_squared_multiplier 1.000 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, -z+1/2' '-y, -x+1/2, -z+1/2' 'y, -x+1/2, z+1/2' '-y, x+1/2, z+1/2' 'x, z+1/2, -y+1/2' '-x, z+1/2, y+1/2' '-x, -z+1/2, -y+1/2' 'x, -z+1/2, y+1/2' 'z, y+1/2, -x+1/2' 'z, -y+1/2, x+1/2' '-z, y+1/2, x+1/2' '-z, -y+1/2, -x+1/2' '-x, -y+1/2, -z+1/2' 'x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' '-z, -x+1/2, -y+1/2' '-z, x+1/2, y+1/2' 'z, x+1/2, -y+1/2' 'z, -x+1/2, y+1/2' '-y, -z+1/2, -x+1/2' 'y, -z+1/2, x+1/2' '-y, z+1/2, x+1/2' 'y, z+1/2, -x+1/2' '-y, -x+1/2, z+1/2' 'y, x+1/2, z+1/2' '-y, x+1/2, -z+1/2' 'y, -x+1/2, -z+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-z, -y+1/2, x+1/2' '-z, y+1/2, -x+1/2' 'z, -y+1/2, -x+1/2' 'z, y+1/2, x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, -z+1/2' '-y+1/2, -x, -z+1/2' 'y+1/2, -x, z+1/2' '-y+1/2, x, z+1/2' 'x+1/2, z, -y+1/2' '-x+1/2, z, y+1/2' '-x+1/2, -z, -y+1/2' 'x+1/2, -z, y+1/2' 'z+1/2, y, -x+1/2' 'z+1/2, -y, x+1/2' '-z+1/2, y, x+1/2' '-z+1/2, -y, -x+1/2' '-x+1/2, -y, -z+1/2' 'x+1/2, y, -z+1/2' 'x+1/2, -y, z+1/2' '-x+1/2, y, z+1/2' '-z+1/2, -x, -y+1/2' '-z+1/2, x, y+1/2' 'z+1/2, x, -y+1/2' 'z+1/2, -x, y+1/2' '-y+1/2, -z, -x+1/2' 'y+1/2, -z, x+1/2' '-y+1/2, z, x+1/2' 'y+1/2, z, -x+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, x, z+1/2' '-y+1/2, x, -z+1/2' 'y+1/2, -x, -z+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-z+1/2, -y, x+1/2' '-z+1/2, y, -x+1/2' 'z+1/2, -y, -x+1/2' 'z+1/2, y, x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y+1/2, -x+1/2, -z' 'y+1/2, -x+1/2, z' '-y+1/2, x+1/2, z' 'x+1/2, z+1/2, -y' '-x+1/2, z+1/2, y' '-x+1/2, -z+1/2, -y' 'x+1/2, -z+1/2, y' 'z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, x' '-z+1/2, y+1/2, x' '-z+1/2, -y+1/2, -x' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' '-z+1/2, -x+1/2, -y' '-z+1/2, x+1/2, y' 'z+1/2, x+1/2, -y' 'z+1/2, -x+1/2, y' '-y+1/2, -z+1/2, -x' 'y+1/2, -z+1/2, x' '-y+1/2, z+1/2, x' 'y+1/2, z+1/2, -x' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' '-y+1/2, x+1/2, -z' 'y+1/2, -x+1/2, -z' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-z+1/2, -y+1/2, x' '-z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, -x' 'z+1/2, y+1/2, x' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 1 2386.08 2282.51 11.83 o 0 0 2 19814.20 23028.20 68.19 o 0 2 2 87845.10 96119.60 102.57 o 2 2 2 752949.00 921997.00 828.67 o 1 1 3 6605.48 8441.66 16.22 o 1 3 3 32310.90 34390.60 42.16 o 3 3 3 66315.70 63747.00 139.85 o 0 0 4 821145.00 783552.00 1068.41 o 0 2 4 27962.40 30300.10 37.76 o 2 2 4 37293.90 41133.30 53.89 o 0 4 4 484749.00 464862.00 480.48 o 2 4 4 33306.90 34330.40 49.21 o 4 4 4 304170.00 282330.00 448.38 o 1 1 5 12914.40 12612.30 24.20 o 1 3 5 226.65 211.54 3.02 o 3 3 5 4328.19 4970.92 17.33 o 1 5 5 20745.70 20507.60 39.10 o 3 5 5 4282.25 4340.79 17.58 o 5 5 5 24560.40 23833.20 98.28 o 0 0 6 1029.49 1098.08 17.81 o 0 2 6 73533.60 72835.10 84.72 o 2 2 6 269687.00 234289.00 200.96 o 0 4 6 4555.83 4791.53 17.24 o 2 4 6 41347.80 41373.90 46.08 o 4 4 6 8497.17 8792.66 28.20 o 0 6 6 64836.90 64634.70 143.17 o 2 6 6 115305.00 113542.00 149.27 o 4 6 6 41046.50 40099.50 87.83 o 6 6 6 53178.40 53661.50 186.13 o 1 1 7 6862.79 7010.72 22.30 o 1 3 7 20134.70 19924.00 29.01 o 3 3 7 36488.40 34809.70 62.77 o 1 5 7 335.21 356.88 5.70 o 3 5 7 4718.57 4877.43 16.97 o 5 5 7 462.50 538.71 11.23 o 1 7 7 13747.90 13627.10 45.89 o 3 7 7 22710.20 22337.50 64.10 o 5 7 7 4363.48 4259.33 27.26 o 7 7 7 15345.90 14170.00 93.85 o 0 0 8 213258.00 205955.00 474.14 o 0 2 8 32536.70 32001.20 61.94 o 2 2 8 4730.37 4805.69 21.91 o 0 4 8 142805.00 135405.00 179.30 o 2 4 8 33867.40 33571.60 50.28 o 4 4 8 97417.50 93017.90 152.63 o 0 6 8 11468.00 11713.40 42.54 o 2 6 8 9835.52 9834.19 28.37 o 4 6 8 13343.00 13454.20 35.09 o 6 6 8 12675.30 12204.10 48.62 o 0 8 8 51531.90 52229.50 155.73 o 2 8 8 28954.80 28795.50 81.60 o 4 8 8 36464.60 34481.40 99.85 o 6 8 8 13733.70 13307.40 54.80 o 8 8 8 14697.20 13281.00 107.80 o 1 1 9 3892.90 3769.81 22.24 o 1 3 9 93.92 111.29 5.44 o 3 3 9 1282.07 1475.11 16.17 o 1 5 9 6894.37 6927.60 24.17 o 3 5 9 1487.98 1556.70 13.05 o 5 5 9 9019.01 9021.28 40.92 o 1 7 9 112.11 149.82 7.26 o 3 7 9 1765.29 1822.41 14.09 o 5 7 9 190.79 220.07 8.12 o 7 7 9 1905.90 1897.94 22.57 o 1 9 9 2824.72 2882.24 24.74 o 3 9 9 613.01 620.39 15.47 o 5 9 9 4019.76 4008.51 33.57 o 7 9 9 88.52 131.59 13.39 o 9 9 9 2074.64 2045.86 48.94 o 0 0 10 139.90 217.48 17.45 o 0 2 10 45514.00 42293.50 94.83 o 2 2 10 63610.80 59816.10 120.77 o 0 4 10 147.02 179.89 10.11 o 2 4 10 30341.20 28498.10 54.74 o 4 4 10 903.42 926.68 15.56 o 0 6 10 40004.40 39901.40 98.86 o 2 6 10 31198.30 30939.80 61.81 o 4 6 10 28081.20 26700.50 59.54 o 6 6 10 15576.10 15637.70 64.22 o 0 8 10 2080.60 2142.34 22.74 o 2 8 10 10500.70 10454.20 34.78 o 4 8 10 2926.64 2912.69 20.33 o 6 8 10 11066.20 10633.50 37.65 o 8 8 10 4073.58 3982.89 35.91 o 0 10 10 26064.30 26637.90 114.71 o 2 10 10 9892.04 10373.70 50.03 o 4 10 10 19467.50 19295.80 78.67 o 6 10 10 4997.85 4900.46 39.04 o 8 10 10 8965.74 8688.48 60.60 o 10 10 10 1584.32 1535.62 53.08 o 1 1 11 721.94 673.15 13.05 o 1 3 11 3498.59 3363.63 18.34 o 3 3 11 7659.29 7494.97 39.34 o 1 5 11 4.63 80.26 8.47 o 3 5 11 703.22 686.70 10.98 o 5 5 11 491.10 538.79 14.86 o 1 7 11 3179.31 3194.96 20.50 o 3 7 11 6013.44 5919.74 27.62 o 5 7 11 943.36 926.51 13.48 o 7 7 11 4850.02 4760.76 36.61 o 1 9 11 3.18 74.73 10.28 o 3 9 11 334.20 340.88 10.54 o 5 9 11 254.30 260.51 10.54 o 7 9 11 490.94 478.56 12.53 o 9 9 11 146.65 147.58 16.68 o 1 11 11 868.92 918.19 20.40 o 3 11 11 1946.97 1951.27 27.58 o 5 11 11 200.28 192.42 16.94 o 7 11 11 1779.29 1779.29 27.41 o 9 11 11 112.67 144.55 15.98 o 11 11 11 690.18 736.91 37.68 o 0 0 12 49045.80 45631.90 224.67 o 0 2 12 18622.00 17691.90 63.25 o 2 2 12 649.01 593.44 14.60 o 0 4 12 35505.60 33334.20 95.33 o 2 4 12 18591.40 17919.70 47.85 o 4 4 12 25816.20 24712.00 83.47 o 0 6 12 8664.44 8702.95 46.02 o 2 6 12 2043.45 2012.08 17.55 o 4 6 12 9152.70 9071.77 36.41 o 6 6 12 3237.96 3134.24 32.01 o 0 8 12 15163.10 15408.40 64.03 o 2 8 12 15893.80 16371.40 48.06 o 4 8 12 11097.80 10961.50 42.25 o 6 8 12 8757.20 8544.14 37.19 o 8 8 12 4786.89 4563.69 47.61 o 0 10 12 2445.99 2512.70 29.23 o 2 10 12 2956.85 2971.96 22.58 o 4 10 12 2852.59 2905.96 24.56 o 6 10 12 3558.56 3520.95 28.12 o 8 10 12 3292.89 3215.05 27.68 o 10 10 12 3397.81 3428.57 41.78 o 0 12 12 5249.83 5543.76 58.96 o 2 12 12 9767.91 10484.80 60.01 o 4 12 12 3860.09 3914.63 40.93 o 6 12 12 5945.50 6095.20 46.33 o 8 12 12 1657.25 1681.84 30.95 o 10 12 12 2614.82 2628.97 32.34 o 12 12 12 565.77 632.57 36.29 o 1 1 13 62.30 111.28 12.27 o 1 3 13 279.21 297.24 9.76 o 3 3 13 1505.43 1482.20 22.39 o 1 5 13 575.32 593.07 11.93 o 3 5 13 4.79 72.57 11.75 o 5 5 13 1282.48 1287.86 23.08 o 1 7 13 500.37 502.15 11.41 o 3 7 13 1558.43 1551.06 17.12 o 5 7 13 41.32 89.60 11.58 o 7 7 13 1523.96 1449.13 28.70 o 1 9 13 298.99 327.14 11.15 o 3 9 13 2.14 77.93 12.70 o 5 9 13 707.23 705.54 15.99 o 7 9 13 24.42 70.93 13.91 o 9 9 13 424.57 400.17 18.58 o 1 11 13 99.32 131.93 10.89 o 3 11 13 492.30 487.03 14.09 o 5 11 13 0.65 66.01 14.00 o 7 11 13 550.59 569.83 15.47 o 9 11 13 0.56 61.60 13.65 o 11 11 13 192.15 226.21 17.02 o 1 13 13 6.03 68.69 18.92 o 3 13 13 63.01 90.98 16.76 o 5 13 13 97.52 116.73 15.03 o 7 13 13 115.92 127.61 15.12 o 9 13 13 63.33 83.38 14.08 o 11 13 13 26.38 41.82 14.86 < 13 13 13 1.12 19.53 28.42 < 0 0 14 54.71 111.71 26.01 o 0 2 14 17522.30 16799.50 70.61 o 2 2 14 15970.20 15361.40 70.05 o 0 4 14 17.89 95.90 15.47 o 2 4 14 12761.10 12400.00 43.75 o 4 4 14 176.67 196.14 14.69 o 0 6 14 16234.60 16199.70 73.63 o 2 6 14 8727.37 8846.01 36.75 o 4 6 14 12211.10 12100.20 45.92 o 6 6 14 4701.58 4705.39 45.09 o 0 8 14 502.24 533.70 19.53 o 2 8 14 5465.93 5491.41 33.42 o 4 8 14 785.71 800.37 16.33 o 6 8 14 5700.28 5687.60 34.12 o 8 8 14 1329.23 1328.87 25.07 o 0 10 14 11966.20 12600.90 69.61 o 2 10 14 3209.73 3409.41 26.56 o 4 10 14 9365.65 9651.67 43.53 o 6 10 14 1669.25 1707.54 21.53 o 8 10 14 4845.88 4865.17 28.91 o 10 10 14 544.09 572.50 18.75 o 0 12 14 784.68 817.66 22.38 o 2 12 14 1912.44 1984.88 21.36 o 4 12 14 979.07 986.77 15.47 o 6 12 14 2192.79 2259.09 20.32 o 8 12 14 1287.23 1259.16 17.03 o 10 12 14 2081.73 2092.36 19.63 o 12 12 14 1144.99 1053.67 24.98 o 0 14 14 6360.50 6691.80 64.95 o 2 14 14 1205.76 1240.88 22.47 o 4 14 14 5121.29 5322.69 41.46 o 6 14 14 624.81 610.89 17.80 o 8 14 14 2846.15 2822.27 31.31 o 10 14 14 200.53 185.68 15.55 o 12 14 14 1319.11 791.85 67.44 o 1 1 15 27.13 93.05 16.67 o 1 3 15 151.04 159.67 10.02 o 3 3 15 798.51 783.00 19.88 o 1 5 15 301.14 308.30 11.75 o 3 5 15 2.62 67.82 13.31 o 5 5 15 718.93 733.55 22.64 o 1 7 15 270.91 280.65 12.44 o 3 7 15 860.88 862.19 14.95 o 5 7 15 20.24 82.16 13.39 o 7 7 15 871.76 900.39 21.26 o 1 9 15 183.74 190.00 11.75 o 3 9 15 2.32 65.32 13.82 o 5 9 15 446.25 443.47 13.13 o 7 9 15 10.38 63.93 12.61 o 9 9 15 292.66 261.04 15.55 o 1 11 15 49.83 91.67 11.58 o 3 11 15 277.12 292.49 11.23 o 5 11 15 1.78 57.45 11.58 o 7 11 15 317.65 322.39 11.32 o 9 11 15 1.92 42.77 14.17 o 11 11 15 106.13 111.63 13.91 o 1 13 15 7.10 52.62 12.44 o 3 13 15 31.37 62.03 10.71 o 5 13 15 75.49 90.55 10.11 o 7 13 15 61.92 73.18 9.24 o 9 13 15 52.78 54.52 10.11 o 11 13 15 11.25 41.30 14.51 < 1 15 15 9.73 41.38 14.77 < 3 15 15 12.61 50.37 15.03 o 5 15 15 64.10 50.37 13.39 o 7 15 15 29.60 55.38 15.81 o 9 15 15 46.57 22.90 21.17 < 0 0 16 13992.20 13550.00 144.62 o 0 2 16 6047.84 5969.16 49.97 o 2 2 16 352.01 355.32 19.79 o 0 4 16 10720.10 10464.10 71.14 o 2 4 16 6240.88 6380.97 37.15 o 4 4 16 8194.93 7925.68 51.31 o 0 6 16 3220.30 3311.50 34.34 o 2 6 16 804.73 789.40 15.82 o 4 6 16 3467.50 3544.11 28.12 o 6 6 16 1234.40 1232.36 23.77 o 0 8 16 5231.35 5382.18 44.58 o 2 8 16 5933.80 6231.64 32.13 o 4 8 16 3965.39 4195.45 31.41 o 6 8 16 3579.06 3724.83 27.17 o 8 8 16 1861.09 1915.05 27.23 o 0 10 16 1126.28 1241.20 23.34 o 2 10 16 1165.20 1223.76 16.16 o 4 10 16 1307.71 1370.77 16.51 o 6 10 16 1447.55 1429.71 16.94 o 8 10 16 1547.50 1571.70 17.89 o 10 10 16 1478.62 1448.92 23.25 o 0 12 16 2085.55 2125.31 28.10 o 2 12 16 4214.55 4311.85 25.87 o 4 12 16 1566.21 1623.75 17.38 o 6 12 16 2715.60 2724.19 20.93 o 8 12 16 710.97 722.40 13.48 o 10 12 16 1301.60 1260.97 19.45 o 0 14 16 438.27 426.44 14.95 o 2 14 16 843.95 862.96 13.66 o 4 14 16 531.90 495.77 12.70 o 6 14 16 988.48 961.04 17.72 o 8 14 16 681.45 606.78 20.74 o 0 16 16 930.66 976.00 54.71 o 2 16 16 2040.70 2110.56 54.74 o 4 16 16 709.33 619.86 56.18 o 1 1 17 109.47 126.92 14.60 o 1 3 17 510.89 491.61 14.17 o 3 3 17 1148.65 1136.63 24.29 o 1 5 17 0.35 61.08 14.00 o 3 5 17 127.59 152.15 10.63 o 5 5 17 71.70 101.52 16.76 o 1 7 17 570.32 629.80 14.78 o 3 7 17 1108.12 1161.85 18.67 o 5 7 17 195.47 193.11 10.54 o 7 7 17 1047.44 1009.87 21.44 o 1 9 17 0.25 63.59 12.35 o 3 9 17 80.92 108.09 9.76 o 5 9 17 45.39 73.79 10.63 o 7 9 17 126.71 134.87 10.02 o 9 9 17 29.41 48.47 14.86 o 1 11 17 207.21 208.49 10.20 o 3 11 17 467.59 460.23 11.93 o 5 11 17 53.99 69.21 9.42 o 7 11 17 469.02 457.04 11.93 o 9 11 17 35.73 51.06 11.49 o 11 11 17 205.68 191.99 26.35 o 1 13 17 32.95 52.96 9.94 o 3 13 17 143.36 138.59 9.33 o 5 13 17 0.29 26.26 13.82 < 7 13 17 167.10 150.86 12.18 o 1 15 17 15.85 32.83 17.37 < 3 15 17 81.95 102.90 22.55 o 0 0 18 17.76 67.39 30.67 < 0 2 18 4855.23 4718.42 40.34 o 2 2 18 5427.54 5258.22 49.00 o 0 4 18 86.92 108.52 17.02 o 2 4 18 3681.19 3759.96 29.42 o 4 4 18 191.54 210.48 14.95 o 0 6 18 4869.61 5045.43 40.16 o 2 6 18 3291.56 3344.39 23.79 o 4 6 18 3785.60 3904.17 25.44 o 6 6 18 1955.07 1972.51 26.37 o 0 8 18 340.39 371.82 16.16 o 2 8 18 1734.13 1838.44 18.93 o 4 8 18 466.33 454.27 11.84 o 6 8 18 1911.80 1958.56 18.68 o 8 8 18 704.92 626.12 17.98 o 0 10 18 4050.70 4213.97 37.73 o 2 10 18 1427.42 1457.26 17.81 o 4 10 18 3238.70 3337.24 23.87 o 6 10 18 817.71 817.58 14.17 o 8 10 18 1763.92 1772.67 21.87 o 10 10 18 321.00 299.67 23.33 o 0 12 18 460.81 433.62 17.28 o 2 12 18 673.92 697.41 14.52 o 4 12 18 549.32 500.52 14.17 o 6 12 18 802.22 793.40 18.50 o 8 12 18 685.60 591.68 28.52 o 0 14 18 2391.43 2513.56 62.97 o 2 14 18 623.10 641.17 32.50 o 4 14 18 1946.39 1986.01 93.58 o 1 1 19 120.32 130.81 13.91 o 1 3 19 2.46 57.71 11.75 o 3 3 19 54.97 85.71 15.12 o 1 5 19 292.31 288.86 10.37 o 3 5 19 68.60 84.59 9.94 o 5 5 19 488.74 481.50 16.59 o 1 7 19 4.35 47.69 11.66 o 3 7 19 91.26 104.46 9.50 o 5 7 19 17.04 55.81 10.54 o 7 7 19 119.86 122.95 12.01 o 1 9 19 202.47 203.65 10.02 o 3 9 19 50.63 62.90 9.42 o 5 9 19 336.31 285.58 10.97 o 7 9 19 14.02 37.24 13.56 < 9 9 19 234.44 216.10 21.60 o 1 11 19 2.87 33.44 14.86 < 3 11 19 17.45 41.21 13.48 o 5 11 19 37.60 50.03 15.03 o 7 11 19 32.25 38.79 19.61 < 1 13 19 41.64 45.53 25.40 < 0 0 20 4953.32 4680.31 85.00 o 0 2 20 1480.43 1426.78 24.29 o 2 2 20 323.55 357.04 16.24 o 0 4 20 3965.99 3897.94 35.39 o 2 4 20 1601.14 1524.44 16.94 o 4 4 20 3164.32 3162.41 32.26 o 0 6 20 815.82 848.34 18.41 o 2 6 20 516.97 510.28 11.15 o 4 6 20 919.76 909.39 13.91 o 6 6 20 690.08 679.79 18.15 o 0 8 20 2169.75 2224.51 28.28 o 2 8 20 1688.71 1696.31 19.11 o 4 8 20 1714.59 1765.78 21.18 o 6 8 20 1044.36 997.72 18.76 o 8 8 20 904.60 834.97 42.70 o 0 10 20 297.90 287.65 20.22 o 2 10 20 652.07 656.89 16.07 o 4 10 20 362.47 345.39 18.92 o 6 10 20 762.64 712.71 49.70 o 1 1 21 82.67 95.30 12.53 o 1 3 21 242.15 239.86 9.42 o 3 3 21 468.79 466.29 15.90 o 1 5 21 10.72 45.45 10.97 o 3 5 21 87.22 91.33 8.90 o 5 5 21 2.82 42.25 17.45 < 1 7 21 261.94 275.21 11.75 o 3 7 21 457.04 452.12 14.69 o 5 7 21 112.39 107.83 14.34 o 1 9 21 7.67 41.64 25.66 < 3 9 21 59.58 68.77 20.22 o 0 0 22 96.08 113.36 31.88 o 0 2 22 1132.22 1130.42 26.19 o 2 2 22 2129.29 2253.47 33.21 o 0 4 22 153.11 123.73 15.90 o 2 4 22 859.78 811.14 17.63 o 4 4 22 214.22 212.04 20.82 o 0 6 22 1201.12 1112.72 38.73 o 2 6 22 1411.88 1348.01 30.00 o 4 6 22 935.25 1436.27 134.50 o 1 1 23 47.65 33.87 21.95 <